 
data_exp_K2Te4U3O18
 
_audit_creation_method            SHELXL-97
_chemical_name_systematic
;
 ?
;
_chemical_name_common             ?
_chemical_melting_point           ?
_chemical_formula_moiety          ?
_chemical_formula_sum
 'K2 O18 Te4 U3'
_chemical_formula_weight          1590.69
 
loop_
 _atom_type_symbol
 _atom_type_description
 _atom_type_scat_dispersion_real
 _atom_type_scat_dispersion_imag
 _atom_type_scat_source
 'K'  'K'   0.2009   0.2494
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'O'  'O'   0.0106   0.0060
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'Te'  'Te'  -0.5308   1.6751
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'U'  'U'  -9.6767   9.6646
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 
_symmetry_cell_setting            triclinic
_symmetry_space_group_name_H-M    'P -1'
_symmetry_space_group_name_Hall     '-P 1'
 
loop_
 _symmetry_equiv_pos_as_xyz
 'x, y, z'
 '-x, -y, -z'
 
_cell_length_a                    6.8463(6)
_cell_length_b                    7.0274(7)
_cell_length_c                    9.4044(9)
_cell_angle_alpha                 73.579(9)
_cell_angle_beta                  81.098(8)
_cell_angle_gamma                 81.761(8)
_cell_volume                      426.41(7)
_cell_formula_units_Z             1
_cell_measurement_temperature     293(2)
_cell_measurement_reflns_used     1015
_cell_measurement_theta_min       3.0223
_cell_measurement_theta_max       29.0396
 
_exptl_crystal_description
;
'Fri Feb 13 10:12:54 2015'
;
_exptl_crystal_colour
;
'Fri Feb 13 10:12:54 2015'
;
_exptl_crystal_size_max           0.09
_exptl_crystal_size_mid           0.08
_exptl_crystal_size_min           0.08
_exptl_crystal_density_meas       ?
_exptl_crystal_density_diffrn     6.195
_exptl_crystal_density_method     'not measured'
_exptl_crystal_F_000              666
_exptl_absorpt_coefficient_mu     35.700
_exptl_absorpt_correction_type    multi-scan
_exptl_absorpt_correction_T_min   0.71045
_exptl_absorpt_correction_T_max   1.00000
_exptl_absorpt_process_details
;
'Fri Feb 13 10:12:54 2015'
;
 
_exptl_special_details
;
 ?
;
 
_diffrn_ambient_temperature       293(2)
_diffrn_radiation_wavelength      0.71073
_diffrn_radiation_type            MoK\a
_diffrn_radiation_source          'fine-focus sealed tube'
_diffrn_radiation_monochromator   graphite
_diffrn_measurement_device_type   'SuperNova, Dual, Cu at zero, Eos'
_diffrn_measurement_method        'ω scans'
_diffrn_detector_area_resol_mean  15.9834
_diffrn_standards_number          ?
_diffrn_standards_interval_count  ?
_diffrn_standards_interval_time   ?
_diffrn_standards_decay_%         ?
_diffrn_reflns_number             2843
_diffrn_reflns_av_R_equivalents   0.0244
_diffrn_reflns_av_sigmaI/netI     0.0526
_diffrn_reflns_limit_h_min        -8
_diffrn_reflns_limit_h_max        8
_diffrn_reflns_limit_k_min        -8
_diffrn_reflns_limit_k_max        8
_diffrn_reflns_limit_l_min        -9
_diffrn_reflns_limit_l_max        12
_diffrn_reflns_theta_min          3.03
_diffrn_reflns_theta_max          27.06
_reflns_number_total              1832
_reflns_number_gt                 1608
_reflns_threshold_expression      >2sigma(I)
 
_computing_data_collection
;
'Fri Feb 13 10:12:54 2015'
;
_computing_cell_refinement
;
'Fri Feb 13 10:12:54 2015'
;
_computing_data_reduction
;
'Fri Feb 13 10:12:54 2015'
;
_computing_structure_solution     'SHELXS-97 (Sheldrick, 1990)'
_computing_structure_refinement   'SHELXL-97 (Sheldrick, 1997)'
_computing_molecular_graphics     ?
_computing_publication_material   ?
 
_refine_special_details
;
 Refinement of F² against ALL reflections.  The weighted R-factor wR and
 goodness of fit S are based on F², conventional R-factors R are based
 on F, with F set to zero for negative F². The threshold expression of
 F² > 2sigma(F²) is used only for calculating R-factors(gt) etc. and is
 not relevant to the choice of reflections for refinement.  R-factors based
 on F² are statistically about twice as large as those based on F, and R-
 factors based on ALL data will be even larger.
;
 
_refine_ls_structure_factor_coef  Fsqd
_refine_ls_matrix_type            full
_refine_ls_weighting_scheme       calc
_refine_ls_weighting_details
 'calc w=1/[σ²(Fo²)+(0.0273P)²+5.0493P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary      direct
_atom_sites_solution_secondary    difmap
_atom_sites_solution_hydrogens    .
_refine_ls_hydrogen_treatment     .
_refine_ls_extinction_method      none
_refine_ls_extinction_coef        ?
_refine_ls_number_reflns          1832
_refine_ls_number_parameters      124
_refine_ls_number_restraints      18
_refine_ls_R_factor_all           0.0456
_refine_ls_R_factor_gt            0.0377
_refine_ls_wR_factor_ref          0.0886
_refine_ls_wR_factor_gt           0.0791
_refine_ls_goodness_of_fit_ref    1.076
_refine_ls_restrained_S_all       1.071
_refine_ls_shift/su_max           0.000
_refine_ls_shift/su_mean          0.000
 
loop_
 _atom_site_label
 _atom_site_type_symbol
 _atom_site_fract_x
 _atom_site_fract_y
 _atom_site_fract_z
 _atom_site_U_iso_or_equiv
 _atom_site_adp_type
 _atom_site_occupancy
 _atom_site_symmetry_multiplicity
 _atom_site_calc_flag
 _atom_site_refinement_flags
 _atom_site_disorder_assembly
 _atom_site_disorder_group
U1 U 0.0000 0.0000 0.5000 0.01068(18) Uani 1 2 d S . .
U2 U 0.12542(7) 0.54009(6) 0.30398(5) 0.00792(15) Uani 1 1 d . . .
Te1 Te 0.19828(12) 0.11721(11) 0.09787(8) 0.00832(19) Uani 1 1 d . . .
Te2 Te 0.66998(12) 0.30417(12) 0.12564(9) 0.0096(2) Uani 1 1 d . . .
K1 K 0.4313(4) 0.2122(4) 0.6365(3) 0.0181(6) Uani 1 1 d . . .
O1 O 0.3664(13) 0.4753(13) 0.3731(10) 0.0135(19) Uani 1 1 d . . .
O2 O -0.1079(13) 0.6014(13) 0.2230(10) 0.014(2) Uani 1 1 d . . .
O3 O 0.2482(14) -0.0670(14) 0.5552(11) 0.020(2) Uani 1 1 d . . .
O4 O -0.0060(14) -0.3050(13) 0.4837(9) 0.014(2) Uani 1 1 d . . .
O5 O 0.1302(14) 0.2182(13) 0.2660(10) 0.016(2) Uani 1 1 d U . .
O6 O 0.5097(13) 0.1162(13) 0.1193(10) 0.015(2) Uani 1 1 d U . .
O7 O 0.6927(14) 0.4659(13) -0.0714(10) 0.018(2) Uani 1 1 d . . .
O8 O 0.2131(14) -0.1385(14) 0.2223(10) 0.019(2) Uani 1 1 d U . .
O9 O -0.1083(13) 0.1185(14) 0.0984(11) 0.020(2) Uani 1 1 d . . .
 
 
_geom_special_details
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
 
loop_
 _geom_bond_atom_site_label_1
 _geom_bond_atom_site_label_2
 _geom_bond_distance
 _geom_bond_site_symmetry_2
 _geom_bond_publ_flag
U1 O3 1.812(9) 2_556 ?
U1 O3 1.812(9) . ?
U1 O4 2.198(9) . ?
U1 O4 2.198(9) 2_556 ?
U1 O5 2.422(9) . ?
U1 O5 2.422(9) 2_556 ?
U1 U2 3.8767(6) . ?
U1 U2 3.8767(6) 2_556 ?
U1 K1 4.013(3) 2_556 ?
U1 K1 4.013(3) . ?
U1 U2 4.0822(6) 1_545 ?
U1 U2 4.0822(6) 2_566 ?
U2 O1 1.817(9) . ?
U2 O2 1.820(9) . ?
U2 O4 2.268(8) 1_565 ?
U2 O8 2.306(10) 1_565 ?
U2 O4 2.324(9) 2_556 ?
U2 O7 2.351(9) 2_665 ?
U2 O5 2.383(9) . ?
U2 U2 3.7420(10) 2_566 ?
U2 K1 3.892(3) 2_666 ?
U2 K1 3.983(3) 2_566 ?
U2 K1 4.005(3) . ?
Te1 O8 1.845(9) . ?
Te1 O5 1.880(9) . ?
Te1 O9 2.097(9) . ?
Te1 O6 2.171(9) . ?
Te1 K1 3.878(3) 2_656 ?
Te2 O6 1.853(10) . ?
Te2 O7 1.877(9) . ?
Te2 O9 1.890(9) 1_655 ?
Te2 K1 3.782(3) 2_656 ?
K1 O1 2.696(9) . ?
K1 O1 2.733(10) 2_666 ?
K1 O2 2.758(9) 2_566 ?
K1 O6 2.791(9) 2_656 ?
K1 O3 2.803(10) . ?
K1 O8 2.866(10) 2_656 ?
K1 O3 2.877(10) 2_656 ?
K1 O4 3.200(10) 2_556 ?
K1 Te2 3.782(3) 2_656 ?
K1 Te1 3.878(3) 2_656 ?
K1 U2 3.892(3) 2_666 ?
K1 U2 3.983(3) 2_566 ?
O1 K1 2.733(10) 2_666 ?
O2 K1 2.758(9) 2_566 ?
O3 K1 2.877(10) 2_656 ?
O4 U2 2.268(8) 1_545 ?
O4 U2 2.324(9) 2_556 ?
O4 K1 3.200(10) 2_556 ?
O6 K1 2.791(9) 2_656 ?
O7 U2 2.352(9) 2_665 ?
O8 U2 2.306(10) 1_545 ?
O8 K1 2.866(10) 2_656 ?
O9 Te2 1.890(9) 1_455 ?
 
loop_
 _geom_angle_atom_site_label_1
 _geom_angle_atom_site_label_2
 _geom_angle_atom_site_label_3
 _geom_angle
 _geom_angle_site_symmetry_1
 _geom_angle_site_symmetry_3
 _geom_angle_publ_flag
O3 U1 O3 180.00(19) 2_556 . ?
O3 U1 O4 90.0(4) 2_556 . ?
O3 U1 O4 90.0(4) . . ?
O3 U1 O4 90.0(4) 2_556 2_556 ?
O3 U1 O4 90.0(4) . 2_556 ?
O4 U1 O4 179.999(1) . 2_556 ?
O3 U1 O5 89.7(4) 2_556 . ?
O3 U1 O5 90.3(4) . . ?
O4 U1 O5 112.2(3) . . ?
O4 U1 O5 67.8(3) 2_556 . ?
O3 U1 O5 90.3(4) 2_556 2_556 ?
O3 U1 O5 89.7(4) . 2_556 ?
O4 U1 O5 67.8(3) . 2_556 ?
O4 U1 O5 112.2(3) 2_556 2_556 ?
O5 U1 O5 179.999(1) . 2_556 ?
O3 U1 U2 89.7(3) 2_556 . ?
O3 U1 U2 90.3(3) . . ?
O4 U1 U2 148.0(2) . . ?
O4 U1 U2 32.0(2) 2_556 . ?
O5 U1 U2 35.9(2) . . ?
O5 U1 U2 144.1(2) 2_556 . ?
O3 U1 U2 90.3(3) 2_556 2_556 ?
O3 U1 U2 89.7(3) . 2_556 ?
O4 U1 U2 32.0(2) . 2_556 ?
O4 U1 U2 148.0(2) 2_556 2_556 ?
O5 U1 U2 144.1(2) . 2_556 ?
O5 U1 U2 35.9(2) 2_556 2_556 ?
U2 U1 U2 180.0 . 2_556 ?
O3 U1 K1 37.5(3) 2_556 2_556 ?
O3 U1 K1 142.5(3) . 2_556 ?
O4 U1 K1 52.7(2) . 2_556 ?
O4 U1 K1 127.3(2) 2_556 2_556 ?
O5 U1 K1 100.3(2) . 2_556 ?
O5 U1 K1 79.7(2) 2_556 2_556 ?
U2 U1 K1 119.01(4) . 2_556 ?
U2 U1 K1 60.99(4) 2_556 2_556 ?
O3 U1 K1 142.5(3) 2_556 . ?
O3 U1 K1 37.5(3) . . ?
O4 U1 K1 127.3(2) . . ?
O4 U1 K1 52.7(2) 2_556 . ?
O5 U1 K1 79.7(2) . . ?
O5 U1 K1 100.3(2) 2_556 . ?
U2 U1 K1 60.99(4) . . ?
U2 U1 K1 119.01(4) 2_556 . ?
K1 U1 K1 180.000(1) 2_556 . ?
O3 U1 U2 94.1(3) 2_556 1_545 ?
O3 U1 U2 85.9(3) . 1_545 ?
O4 U1 U2 24.3(2) . 1_545 ?
O4 U1 U2 155.7(2) 2_556 1_545 ?
O5 U1 U2 88.2(2) . 1_545 ?
O5 U1 U2 91.8(2) 2_556 1_545 ?
U2 U1 U2 123.982(13) . 1_545 ?
U2 U1 U2 56.018(13) 2_556 1_545 ?
K1 U1 U2 58.93(4) 2_556 1_545 ?
K1 U1 U2 121.07(4) . 1_545 ?
O3 U1 U2 85.9(3) 2_556 2_566 ?
O3 U1 U2 94.1(3) . 2_566 ?
O4 U1 U2 155.7(2) . 2_566 ?
O4 U1 U2 24.3(2) 2_556 2_566 ?
O5 U1 U2 91.8(2) . 2_566 ?
O5 U1 U2 88.2(2) 2_556 2_566 ?
U2 U1 U2 56.018(13) . 2_566 ?
U2 U1 U2 123.982(13) 2_556 2_566 ?
K1 U1 U2 121.07(4) 2_556 2_566 ?
K1 U1 U2 58.93(4) . 2_566 ?
U2 U1 U2 180.0 1_545 2_566 ?
O1 U2 O2 176.1(4) . . ?
O1 U2 O4 93.4(4) . 1_565 ?
O2 U2 O4 90.4(4) . 1_565 ?
O1 U2 O8 85.4(4) . 1_565 ?
O2 U2 O8 94.7(4) . 1_565 ?
O4 U2 O8 73.0(3) 1_565 1_565 ?
O1 U2 O4 86.9(4) . 2_556 ?
O2 U2 O4 95.4(4) . 2_556 ?
O4 U2 O4 70.8(3) 1_565 2_556 ?
O8 U2 O4 142.4(3) 1_565 2_556 ?
O1 U2 O7 84.6(4) . 2_665 ?
O2 U2 O7 91.6(4) . 2_665 ?
O4 U2 O7 152.4(3) 1_565 2_665 ?
O8 U2 O7 79.4(3) 1_565 2_665 ?
O4 U2 O7 136.2(3) 2_556 2_665 ?
O1 U2 O5 91.9(4) . . ?
O2 U2 O5 86.1(3) . . ?
O4 U2 O5 136.7(3) 1_565 . ?
O8 U2 O5 150.3(3) 1_565 . ?
O4 U2 O5 66.6(3) 2_556 . ?
O7 U2 O5 70.9(3) 2_665 . ?
O1 U2 U2 90.1(3) . 2_566 ?
O2 U2 U2 93.6(3) . 2_566 ?
O4 U2 U2 35.9(2) 1_565 2_566 ?
O8 U2 U2 108.4(2) 1_565 2_566 ?
O4 U2 U2 34.9(2) 2_556 2_566 ?
O7 U2 U2 170.2(2) 2_665 2_566 ?
O5 U2 U2 101.2(2) . 2_566 ?
O1 U2 U1 89.0(3) . . ?
O2 U2 U1 91.3(3) . . ?
O4 U2 U1 100.6(2) 1_565 . ?
O8 U2 U1 171.2(2) 1_565 . ?
O4 U2 U1 30.0(2) 2_556 . ?
O7 U2 U1 106.8(2) 2_665 . ?
O5 U2 U1 36.6(2) . . ?
U2 U2 U1 64.769(15) 2_566 . ?
O1 U2 K1 39.1(3) . 2_666 ?
O2 U2 K1 141.5(3) . 2_666 ?
O4 U2 K1 76.4(3) 1_565 2_666 ?
O8 U2 K1 46.9(2) 1_565 2_666 ?
O4 U2 K1 113.3(2) 2_556 2_666 ?
O7 U2 K1 85.2(3) 2_665 2_666 ?
O5 U2 K1 128.0(2) . 2_666 ?
U2 U2 K1 95.89(5) 2_566 2_666 ?
U1 U2 K1 126.38(4) . 2_666 ?
O1 U2 K1 146.7(3) . 2_566 ?
O2 U2 K1 37.1(3) . 2_566 ?
O4 U2 K1 53.4(2) 1_565 2_566 ?
O8 U2 K1 86.2(2) 1_565 2_566 ?
O4 U2 K1 80.5(2) 2_556 2_566 ?
O7 U2 K1 125.2(2) 2_665 2_566 ?
O5 U2 K1 110.6(2) . 2_566 ?
U2 U2 K1 62.38(5) 2_566 2_566 ?
U1 U2 K1 94.83(4) . 2_566 ?
K1 U2 K1 120.79(7) 2_666 2_566 ?
O1 U2 K1 33.9(3) . . ?
O2 U2 K1 148.4(3) . . ?
O4 U2 K1 80.6(2) 1_565 . ?
O8 U2 K1 111.2(2) 1_565 . ?
O4 U2 K1 53.0(2) 2_556 . ?
O7 U2 K1 110.3(2) 2_665 . ?
O5 U2 K1 80.3(2) . . ?
U2 U2 K1 61.76(4) 2_566 . ?
U1 U2 K1 61.19(5) . . ?
K1 U2 K1 65.60(7) 2_666 . ?
K1 U2 K1 124.13(4) 2_566 . ?
O8 Te1 O5 89.5(4) . . ?
O8 Te1 O9 90.9(4) . . ?
O5 Te1 O9 86.1(4) . . ?
O8 Te1 O6 87.1(4) . . ?
O5 Te1 O6 88.9(4) . . ?
O9 Te1 O6 174.6(3) . . ?
O8 Te1 K1 44.4(3) . 2_656 ?
O5 Te1 K1 78.6(3) . 2_656 ?
O9 Te1 K1 132.0(3) . 2_656 ?
O6 Te1 K1 44.7(2) . 2_656 ?
O6 Te2 O7 103.0(4) . . ?
O6 Te2 O9 87.7(4) . 1_655 ?
O7 Te2 O9 96.4(4) . 1_655 ?
O6 Te2 K1 44.8(3) . 2_656 ?
O7 Te2 K1 143.4(3) . 2_656 ?
O9 Te2 K1 70.0(3) 1_655 2_656 ?
O1 K1 O1 76.0(3) . 2_666 ?
O1 K1 O2 90.0(3) . 2_566 ?
O1 K1 O2 87.3(3) 2_666 2_566 ?
O1 K1 O6 168.8(3) . 2_656 ?
O1 K1 O6 113.8(3) 2_666 2_656 ?
O2 K1 O6 95.9(3) 2_566 2_656 ?
O1 K1 O3 89.1(3) . . ?
O1 K1 O3 163.1(3) 2_666 . ?
O2 K1 O3 100.7(3) 2_566 . ?
O6 K1 O3 80.5(3) 2_656 . ?
O1 K1 O8 126.7(3) . 2_656 ?
O1 K1 O8 60.4(3) 2_666 2_656 ?
O2 K1 O8 115.1(3) 2_566 2_656 ?
O6 K1 O8 58.8(3) 2_656 2_656 ?
O3 K1 O8 126.8(3) . 2_656 ?
O1 K1 O3 80.3(3) . 2_656 ?
O1 K1 O3 90.4(3) 2_666 2_656 ?
O2 K1 O3 170.4(3) 2_566 2_656 ?
O6 K1 O3 93.6(3) 2_656 2_656 ?
O3 K1 O3 79.2(3) . 2_656 ?
O8 K1 O3 71.5(3) 2_656 2_656 ?
O1 K1 O4 57.5(3) . 2_556 ?
O1 K1 O4 118.7(3) 2_666 2_556 ?
O2 K1 O4 58.1(2) 2_566 2_556 ?
O6 K1 O4 118.2(3) 2_656 2_556 ?
O3 K1 O4 56.2(2) . 2_556 ?
O8 K1 O4 172.9(3) 2_656 2_556 ?
O3 K1 O4 115.5(3) 2_656 2_556 ?
O1 K1 Te2 142.4(2) . 2_656 ?
O1 K1 Te2 141.6(2) 2_666 2_656 ?
O2 K1 Te2 93.7(2) 2_566 2_656 ?
O6 K1 Te2 27.9(2) 2_656 2_656 ?
O3 K1 Te2 53.4(2) . 2_656 ?
O8 K1 Te2 84.9(2) 2_656 2_656 ?
O3 K1 Te2 93.9(2) 2_656 2_656 ?
O4 K1 Te2 93.51(18) 2_556 2_656 ?
O1 K1 Te1 149.3(2) . 2_656 ?
O1 K1 Te1 86.5(2) 2_666 2_656 ?
O2 K1 Te1 114.4(2) 2_566 2_656 ?
O6 K1 Te1 33.2(2) 2_656 2_656 ?
O3 K1 Te1 103.4(2) . 2_656 ?
O8 K1 Te1 26.75(19) 2_656 2_656 ?
O3 K1 Te1 74.8(2) 2_656 2_656 ?
O4 K1 Te1 151.29(19) 2_556 2_656 ?
Te2 K1 Te1 58.22(4) 2_656 2_656 ?
O1 K1 U2 95.2(2) . 2_666 ?
O1 K1 U2 24.78(18) 2_666 2_666 ?
O2 K1 U2 102.9(2) 2_566 2_666 ?
O6 K1 U2 92.8(2) 2_656 2_666 ?
O3 K1 U2 156.1(2) . 2_666 ?
O8 K1 U2 36.02(19) 2_656 2_666 ?
O3 K1 U2 78.3(2) 2_656 2_666 ?
O4 K1 U2 143.52(18) 2_556 2_666 ?
Te2 K1 U2 120.19(8) 2_656 2_666 ?
Te1 K1 U2 62.59(5) 2_656 2_666 ?
O1 K1 U2 74.32(19) . 2_566 ?
O1 K1 U2 99.97(19) 2_666 2_566 ?
O2 K1 U2 23.43(19) 2_566 2_566 ?
O6 K1 U2 108.2(2) 2_656 2_566 ?
O3 K1 U2 83.06(19) . 2_566 ?
O8 K1 U2 138.5(2) 2_656 2_566 ?
O3 K1 U2 149.2(2) 2_656 2_566 ?
O4 K1 U2 34.69(15) 2_556 2_566 ?
Te2 K1 U2 95.58(7) 2_656 2_566 ?
Te1 K1 U2 134.32(8) 2_656 2_566 ?
U2 K1 U2 120.78(7) 2_666 2_566 ?
U2 O1 K1 124.0(4) . . ?
U2 O1 K1 116.1(4) . 2_666 ?
K1 O1 K1 104.0(3) . 2_666 ?
U2 O2 K1 119.5(4) . 2_566 ?
U1 O3 K1 119.3(4) . . ?
U1 O3 K1 120.8(4) . 2_656 ?
K1 O3 K1 100.8(3) . 2_656 ?
U1 O4 U2 132.2(4) . 1_545 ?
U1 O4 U2 118.0(4) . 2_556 ?
U2 O4 U2 109.2(3) 1_545 2_556 ?
U1 O4 K1 94.2(3) . 2_556 ?
U2 O4 K1 91.9(3) 1_545 2_556 ?
U2 O4 K1 91.6(3) 2_556 2_556 ?
Te1 O5 U2 133.5(5) . . ?
Te1 O5 U1 118.9(4) . . ?
U2 O5 U1 107.6(3) . . ?
Te2 O6 Te1 135.6(4) . . ?
Te2 O6 K1 107.3(4) . 2_656 ?
Te1 O6 K1 102.1(3) . 2_656 ?
Te2 O7 U2 138.6(4) . 2_665 ?
Te1 O8 U2 152.8(5) . 1_545 ?
Te1 O8 K1 108.9(4) . 2_656 ?
U2 O8 K1 97.0(3) 1_545 2_656 ?
Te2 O9 Te1 133.4(5) 1_455 . ?
 
_diffrn_measured_fraction_theta_max    0.980
_diffrn_reflns_theta_full              27.06
_diffrn_measured_fraction_theta_full   0.980
_refine_diff_density_max    1.799
_refine_diff_density_min   -2.044
_refine_diff_density_rms    0.447
