data_scd0906_muR
_publcif_datablock.id '{f2d54345-305e-4bad-bbf3-6146cd58ff9a}'

_diffrn_radiation_monochromator   'HELIOS optics'
#Added by publCIF




_symmetry_space_group_name_hall   '-I 4bd 2'
#Added by publCIF



_audit_update_record
;
2017-02-27 # Formatted by publCIF

;

# publcif _publ_body_element loop start
loop_
_publ_body_element
_publ_body_title
_publ_body_contents

 section 
;
Introduction
; 
;

;
 section 
;
Experimental
; 
;

;
 subsection 
;
Synthesis and crystallization
; 
;

;
 subsection 
;
Refinement
;
;
Crystal data, data collection and structure refinement details are summarized
in Table 1.
;

 section 
;
Results and discussion
; 
;

;
# publcif _publ_body_element loop end
 
_audit_creation_method            'SHELXL-2014/7'
_shelx_SHELXL_version_number      '2014/7'
_chemical_name_systematic         ?
_chemical_name_common             ?
_chemical_melting_point           ?
_chemical_formula_moiety          'Ge13 Ir4 Lu3'
_chemical_formula_sum
 'Ge13 Ir4 Lu3' 
_chemical_formula_weight          2237.38

loop_
 _atom_type_symbol
 _atom_type_description
 _atom_type_scat_dispersion_real
 _atom_type_scat_dispersion_imag
 _atom_type_scat_source
 'Ge'  'Ge'   0.1547   1.8001
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'Ir'  'Ir'  -1.4442   7.9887
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'Lu'  'Lu'  -0.4720   5.8584
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 
_space_group_crystal_system       tetragonal
_space_group_IT_number            141
_space_group_name_H-M_alt         'I 41/a m d'
_space_group_name_Hall            '-I 4bd 2'
 
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
 
loop_
 _space_group_symop_operation_xyz
 'x, y, z'
 '-x+1/2, -y, z+1/2'
 '-y+1/4, x+3/4, z+1/4'
 'y+1/4, -x+1/4, z+3/4'
 '-x+1/2, y, -z+1/2'
 'x, -y, -z'
 'y+1/4, x+3/4, -z+1/4'
 '-y+1/4, -x+1/4, -z+3/4'
 'x+1/2, y+1/2, z+1/2'
 '-x+1, -y+1/2, z+1'
 '-y+3/4, x+5/4, z+3/4'
 'y+3/4, -x+3/4, z+5/4'
 '-x+1, y+1/2, -z+1'
 'x+1/2, -y+1/2, -z+1/2'
 'y+3/4, x+5/4, -z+3/4'
 '-y+3/4, -x+3/4, -z+5/4'
 '-x, -y, -z'
 'x-1/2, y, -z-1/2'
 'y-1/4, -x-3/4, -z-1/4'
 '-y-1/4, x-1/4, -z-3/4'
 'x-1/2, -y, z-1/2'
 '-x, y, z'
 '-y-1/4, -x-3/4, z-1/4'
 'y-1/4, x-1/4, z-3/4'
 '-x+1/2, -y+1/2, -z+1/2'
 'x, y+1/2, -z'
 'y+1/4, -x-1/4, -z+1/4'
 '-y+1/4, x+1/4, -z-1/4'
 'x, -y+1/2, z'
 '-x+1/2, y+1/2, z+1/2'
 '-y+1/4, -x-1/4, z+1/4'
 'y+1/4, x+1/4, z-1/4'
 
_cell_length_a                    17.764(3)
_cell_length_b                    17.764(3)
_cell_length_c                    17.822(4)
_cell_angle_alpha                 90
_cell_angle_beta                  90
_cell_angle_gamma                 90
_cell_volume                      5624(2)
_cell_formula_units_Z             16
_cell_measurement_temperature     298(2)
_cell_measurement_reflns_used     9897
_cell_measurement_theta_min       3.24
_cell_measurement_theta_max       30.52
 
_exptl_crystal_description        fragment
_exptl_crystal_colour             black
_exptl_crystal_density_meas       ?
_exptl_crystal_density_method     ?
_exptl_crystal_density_diffrn     10.570         
_exptl_crystal_F_000              14992
_exptl_transmission_factor_min    ?
_exptl_transmission_factor_max    ?
_exptl_crystal_size_max           0.100
_exptl_crystal_size_mid           0.080
_exptl_crystal_size_min           0.050
_exptl_absorpt_coefficient_mu     85.792
_shelx_estimated_absorpt_T_min    0.042
_shelx_estimated_absorpt_T_max    0.099
_exptl_absorpt_correction_type    multi-scan
_exptl_absorpt_correction_T_min   0.0043  
_exptl_absorpt_correction_T_max   0.0294
_exptl_absorpt_process_details    
;
SADABS (Krause, Herbst-Irmer, Sheldrick, & Stalke;  J. Appl. Cryst. 2015, 48,
3-10)
;

_exptl_absorpt_special_details    ?
_diffrn_ambient_temperature       298(2)
_diffrn_radiation_wavelength      0.71073
_diffrn_radiation_type            MoK\a
_diffrn_source                    'I\mS microfocus tube'
_diffrn_measurement_device_type   'Bruker Kappa D8 Quest CMOS'
_diffrn_measurement_method        'φ and ω scans'
_diffrn_detector_area_resol_mean  ?
_diffrn_reflns_number             75394
_diffrn_reflns_av_unetI/netI      0.0207
_diffrn_reflns_av_R_equivalents   0.0773
_diffrn_reflns_limit_h_min        -25
_diffrn_reflns_limit_h_max        25
_diffrn_reflns_limit_k_min        -25
_diffrn_reflns_limit_k_max        25
_diffrn_reflns_limit_l_min        -25
_diffrn_reflns_limit_l_max        25
_diffrn_reflns_theta_min          2.293
_diffrn_reflns_theta_max          30.604
_diffrn_reflns_theta_full         25.242
_diffrn_measured_fraction_theta_max   0.998
_diffrn_measured_fraction_theta_full  0.999
_diffrn_reflns_Laue_measured_fraction_max    0.998
_diffrn_reflns_Laue_measured_fraction_full   0.999
_diffrn_reflns_point_group_measured_fraction_max   0.998
_diffrn_reflns_point_group_measured_fraction_full  0.999
_reflns_number_total              2294
_reflns_number_gt                 1671
_reflns_threshold_expression      'I > 2σ(I)'
_reflns_Friedel_coverage          0.000
_reflns_Friedel_fraction_max      .
_reflns_Friedel_fraction_full     .
 
_reflns_special_details
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
 
_computing_data_collection        'Bruker APEX2'
_computing_cell_refinement        'Bruker SAINT'
_computing_data_reduction         'Bruker SAINT'
_computing_structure_solution     
'SHELXTL Intrinsic Phasing (Sheldrick, 2014)'
_computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)'
_computing_molecular_graphics     'CrystalMaker for Windows (Palmer, 2014)'
_computing_publication_material   'publCIF (Westrip, 2010)'
_refine_special_details           ?
_refine_ls_structure_factor_coef  Fsqd
_refine_ls_matrix_type            full
_refine_ls_weighting_scheme       calc
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0438P)²+229.8892P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary      ?
_atom_sites_solution_secondary    ?
_atom_sites_solution_hydrogens    .
_refine_ls_hydrogen_treatment     undef
_refine_ls_extinction_method      'SHELXL-2014/7 (Sheldrick 2014'
_refine_ls_extinction_coef        0.000052(3)
_refine_ls_extinction_expression
 'Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^'
_refine_ls_number_reflns          2294
_refine_ls_number_parameters      107
_refine_ls_number_restraints      0
_refine_ls_R_factor_all           0.0582
_refine_ls_R_factor_gt            0.0389
_refine_ls_wR_factor_ref          0.1093
_refine_ls_wR_factor_gt           0.0949
_refine_ls_goodness_of_fit_ref    1.147
_refine_ls_restrained_S_all       1.147
_refine_ls_shift/su_max           0.001
_refine_ls_shift/su_mean          0.000
 
loop_
 _atom_site_label
 _atom_site_type_symbol
 _atom_site_fract_x
 _atom_site_fract_y
 _atom_site_fract_z
 _atom_site_U_iso_or_equiv
 _atom_site_adp_type
 _atom_site_occupancy
 _atom_site_site_symmetry_order  
 _atom_site_calc_flag
 _atom_site_refinement_flags_posn
 _atom_site_refinement_flags_adp
 _atom_site_refinement_flags_occupancy
 _atom_site_disorder_assembly
 _atom_site_disorder_group
Lu1 Lu 0.5000 0.37512(4) 0.00090(4) 0.01787(17) Uani 1 2 d S T P . .
Lu2 Lu 0.25127(2) 0.49873(2) 0.1250 0.01803(17) Uani 1 2 d S T P . .
Lu3 Lu 0.0000 0.37479(4) 0.00139(4) 0.01794(16) Uani 1 2 d S T P . .
Ir1 Ir 0.12521(2) 0.37489(2) 0.12510(2) 0.01447(16) Uani 1 1 d . . . . .
Ir2 Ir 0.37493(2) 0.37507(2) 0.1250 0.01462(17) Uani 1 2 d S T P . .
Ir3 Ir 0.12524(2) 0.62476(2) 0.1250 0.01441(17) Uani 1 2 d S T P . .
Ge1A Ge 0.25101(9) 0.7500 0.00572(9) 0.0188(4) Uani 0.921(4) 2 d S T P . .
Ge1B Ge 0.2560(11) 0.7500 -0.0512(12) 0.0188(4) Uani 0.079(4) 2 d S T P . .
Ge2 Ge 0.0000 0.32683(9) 0.16875(8) 0.0163(3) Uani 1 2 d S T P . .
Ge3 Ge 0.25016(6) 0.32921(6) 0.17106(7) 0.0187(2) Uani 1 1 d . . . . .
Ge4 Ge 0.17331(7) 0.41701(7) 0.00032(6) 0.0206(3) Uani 1 1 d . . . . .
Ge5 Ge 0.0000 0.66070(9) 0.17652(9) 0.0197(3) Uani 1 2 d S T P . .
Ge6 Ge 0.12683(10) 0.2500 0.06517(10) 0.0232(4) Uani 1 2 d S T P . .
Ge7 Ge 0.31496(7) 0.38480(8) 0.00042(7) 0.0263(3) Uani 1 1 d . . . . .
Ge8 Ge 0.06910(7) 0.50008(6) 0.10763(8) 0.0268(3) Uani 1 1 d . . . . .
Ge9 Ge 0.5000 0.35237(13) 0.18191(11) 0.0356(5) Uani 1 2 d S T P . .
 
 
_geom_special_details
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
 
loop_
 _geom_bond_atom_site_label_1
 _geom_bond_atom_site_label_2
 _geom_bond_distance
 _geom_bond_site_symmetry_2
 _geom_bond_publ_flag
Lu1 Ge3 2.9701(13) 27_565 ?
Lu1 Ge3 2.9701(13) 16_554 ?
Lu1 Ge3 2.9898(13) 32 ?
Lu1 Ge3 2.9898(13) 11_544 ?
Lu1 Ge2 2.9910(12) 11_544 ?
Lu1 Ge2 2.9910(12) 4_554 ?
Lu1 Ge9 3.1114(16) 20_656 ?
Lu1 Ge9 3.1114(16) 27_565 ?
Lu1 Ir2 3.1348(7) . ?
Lu1 Ir2 3.1348(7) 27_565 ?
Lu1 Ir1 3.1542(8) 11_544 ?
Lu1 Ir1 3.1542(8) 32 ?
Lu2 Ge4 2.9937(13) 16_554 ?
Lu2 Ge4 2.9937(13) . ?
Lu2 Ge4 3.0242(13) 6_565 ?
Lu2 Ge4 3.0242(13) 12_454 ?
Lu2 Ir2 3.1067(9) . ?
Lu2 Ge3 3.1211(13) 16_554 ?
Lu2 Ge3 3.1211(13) . ?
Lu2 Ir1 3.1390(6) 16_554 ?
Lu2 Ir1 3.1390(6) . ?
Lu2 Ir3 3.1660(9) . ?
Lu2 Ge7 3.2102(14) . ?
Lu2 Ge7 3.2102(14) 16_554 ?
Lu3 Ge5 3.0348(13) 4_454 ?
Lu3 Ge5 3.0348(13) 11_544 ?
Lu3 Ge2 3.1020(18) . ?
Lu3 Ir1 3.1317(8) . ?
Lu3 Ir1 3.1318(7) 22 ?
Lu3 Ir3 3.1660(7) 17_565 ?
Lu3 Ir3 3.1660(7) 11_544 ?
Lu3 Ge4 3.1687(13) . ?
Lu3 Ge4 3.1687(13) 22 ?
Lu3 Ge8 3.1695(15) 22 ?
Lu3 Ge8 3.1695(15) . ?
Lu3 Ge8 3.1972(15) 6_565 ?
Ir1 Ge8 2.4568(13) . ?
Ir1 Ge6 2.4623(9) . ?
Ir1 Ge7 2.4818(13) 12_454 ?
Ir1 Ge4 2.4970(13) . ?
Ir1 Ge3 2.5012(12) . ?
Ir1 Ge2 2.5063(9) . ?
Ir1 Lu1 3.1541(8) 12_454 ?
Ir2 Ge7 2.4687(13) . ?
Ir2 Ge7 2.4687(13) 16_554 ?
Ir2 Ge9 2.4752(10) . ?
Ir2 Ge9 2.4752(10) 20_656 ?
Ir2 Ge3 2.4998(11) 16_554 ?
Ir2 Ge3 2.4999(11) . ?
Ir2 Lu1 3.1348(7) 20_656 ?
Ir3 Ge8 2.4485(12) . ?
Ir3 Ge8 2.4485(12) 16_554 ?
Ir3 Ge5 2.4900(9) . ?
Ir3 Ge5 2.4900(9) 20_666 ?
Ir3 Ge4 2.5036(13) 6_565 ?
Ir3 Ge4 2.5036(13) 12_454 ?
Ir3 Lu3 3.1660(7) 17_565 ?
Ir3 Lu3 3.1660(7) 12_454 ?
Ge1A Ge1B 1.02(2) . ?
Ge1A Ge6 2.542(2) 26 ?
Ge1A Ge7 2.6525(17) 26 ?
Ge1A Ge7 2.6525(17) 6_565 ?
Ge1A Ge8 2.727(2) 20_666 ?
Ge1A Ge8 2.727(2) 16_554 ?
Ge1A Ge9 2.918(3) 11_544 ?
Ge1B Ge6 2.31(2) 26 ?
Ge1B Ge9 2.53(2) 11_544 ?
Ge1B Ge3 2.561(17) 6_565 ?
Ge1B Ge3 2.561(17) 26 ?
Ge1B Ge7 2.765(10) 26 ?
Ge1B Ge7 2.765(10) 6_565 ?
Ge2 Ir1 2.5063(9) 22 ?
Ge2 Ge9 2.700(3) 18_556 ?
Ge2 Ge2 2.729(3) 10_454 ?
Ge2 Lu1 2.9910(12) 3_545 ?
Ge2 Lu1 2.9910(12) 12_454 ?
Ge3 Ge1B 2.561(17) 26_545 ?
Ge3 Ge3 2.814(3) 5 ?
Ge3 Ge3 2.814(2) 29 ?
Ge3 Lu1 2.9702(13) 20_656 ?
Ge3 Lu1 2.9897(13) 12_454 ?
Ge4 Ir3 2.5036(13) 11_544 ?
Ge4 Ge7 2.5804(18) . ?
Ge4 Lu2 3.0242(13) 11_544 ?
Ge5 Ir3 2.4901(9) 27_465 ?
Ge5 Ge6 2.559(3) 12_454 ?
Ge5 Ge5 2.899(3) 27_465 ?
Ge5 Ge5 2.899(3) 20_666 ?
Ge5 Lu3 3.0348(13) 12_454 ?
Ge5 Lu3 3.0348(13) 3 ?
Ge5 Lu3 3.2328(19) 17_565 ?
Ge6 Ge1B 2.31(2) 26_545 ?
Ge6 Ir1 2.4624(9) 29 ?
Ge6 Ge1A 2.542(2) 26_545 ?
Ge6 Ge5 2.559(3) 11_544 ?
Ge6 Lu1 3.310(2) 12_454 ?
Ge6 Lu3 3.3588(15) 10_454 ?
Ge7 Ir1 2.4818(13) 11_544 ?
Ge7 Ge1A 2.6525(17) 26_545 ?
Ge7 Ge1B 2.765(10) 26_545 ?
Ge7 Lu2 3.2491(14) 11_544 ?
Ge8 Ge8 2.455(3) 22 ?
Ge8 Ge1A 2.727(2) 27_465 ?
Ge8 Lu3 3.1972(15) 17_565 ?
Ge9 Ir2 2.4753(10) 27_565 ?
Ge9 Ge1B 2.53(2) 12_454 ?
Ge9 Ge2 2.700(3) 18_656 ?
Ge9 Ge1A 2.918(3) 12_454 ?
Ge9 Lu1 3.1114(16) 20_656 ?
Ge9 Lu1 3.1114(16) 27_565 ?
 
loop_
 _geom_angle_atom_site_label_1
 _geom_angle_atom_site_label_2
 _geom_angle_atom_site_label_3
 _geom_angle
 _geom_angle_site_symmetry_1
 _geom_angle_site_symmetry_3
 _geom_angle_publ_flag
Ge3 Lu1 Ge3 56.56(5) 27_565 16_554 ?
Ge3 Lu1 Ge3 56.34(5) 27_565 32 ?
Ge3 Lu1 Ge3 83.78(4) 16_554 32 ?
Ge3 Lu1 Ge3 83.78(4) 27_565 11_544 ?
Ge3 Lu1 Ge3 56.34(5) 16_554 11_544 ?
Ge3 Lu1 Ge3 56.15(5) 32 11_544 ?
Ge3 Lu1 Ge2 178.42(4) 27_565 11_544 ?
Ge3 Lu1 Ge2 124.56(4) 16_554 11_544 ?
Ge3 Lu1 Ge2 122.27(4) 32 11_544 ?
Ge3 Lu1 Ge2 95.99(3) 11_544 11_544 ?
Ge3 Lu1 Ge2 124.56(4) 27_565 4_554 ?
Ge3 Lu1 Ge2 178.42(4) 16_554 4_554 ?
Ge3 Lu1 Ge2 95.99(3) 32 4_554 ?
Ge3 Lu1 Ge2 122.27(4) 11_544 4_554 ?
Ge2 Lu1 Ge2 54.29(6) 11_544 4_554 ?
Ge3 Lu1 Ge9 129.01(5) 27_565 20_656 ?
Ge3 Lu1 Ge9 94.34(4) 16_554 20_656 ?
Ge3 Lu1 Ge9 171.48(5) 32 20_656 ?
Ge3 Lu1 Ge9 116.03(5) 11_544 20_656 ?
Ge2 Lu1 Ge9 52.47(5) 11_544 20_656 ?
Ge2 Lu1 Ge9 85.65(4) 4_554 20_656 ?
Ge3 Lu1 Ge9 94.34(4) 27_565 27_565 ?
Ge3 Lu1 Ge9 129.01(5) 16_554 27_565 ?
Ge3 Lu1 Ge9 116.03(5) 32 27_565 ?
Ge3 Lu1 Ge9 171.48(5) 11_544 27_565 ?
Ge2 Lu1 Ge9 85.65(4) 11_544 27_565 ?
Ge2 Lu1 Ge9 52.47(5) 4_554 27_565 ?
Ge9 Lu1 Ge9 71.53(8) 20_656 27_565 ?
Ge3 Lu1 Ir2 90.32(3) 27_565 . ?
Ge3 Lu1 Ir2 48.25(2) 16_554 . ?
Ge3 Lu1 Ir2 132.04(3) 32 . ?
Ge3 Lu1 Ir2 90.14(3) 11_544 . ?
Ge2 Lu1 Ir2 91.25(3) 11_544 . ?
Ge2 Lu1 Ir2 131.95(3) 4_554 . ?
Ge9 Lu1 Ir2 46.69(3) 20_656 . ?
Ge9 Lu1 Ir2 98.19(5) 27_565 . ?
Ge3 Lu1 Ir2 48.25(2) 27_565 27_565 ?
Ge3 Lu1 Ir2 90.32(3) 16_554 27_565 ?
Ge3 Lu1 Ir2 90.14(3) 32 27_565 ?
Ge3 Lu1 Ir2 132.03(3) 11_544 27_565 ?
Ge2 Lu1 Ir2 131.95(3) 11_544 27_565 ?
Ge2 Lu1 Ir2 91.25(3) 4_554 27_565 ?
Ge9 Lu1 Ir2 98.19(5) 20_656 27_565 ?
Ge9 Lu1 Ir2 46.69(3) 27_565 27_565 ?
Ir2 Lu1 Ir2 90.26(3) . 27_565 ?
Ge3 Lu1 Ir1 131.74(3) 27_565 11_544 ?
Ge3 Lu1 Ir1 89.96(3) 16_554 11_544 ?
Ge3 Lu1 Ir1 89.56(3) 32 11_544 ?
Ge3 Lu1 Ir1 47.95(2) 11_544 11_544 ?
Ge2 Lu1 Ir1 48.05(2) 11_544 11_544 ?
Ge2 Lu1 Ir1 88.47(4) 4_554 11_544 ?
Ge9 Lu1 Ir1 82.12(5) 20_656 11_544 ?
Ge9 Lu1 Ir1 133.24(3) 27_565 11_544 ?
Ir2 Lu1 Ir1 90.174(18) . 11_544 ?
Ir2 Lu1 Ir1 179.57(2) 27_565 11_544 ?
Ge3 Lu1 Ir1 89.96(3) 27_565 32 ?
Ge3 Lu1 Ir1 131.74(3) 16_554 32 ?
Ge3 Lu1 Ir1 47.95(2) 32 32 ?
Ge3 Lu1 Ir1 89.56(3) 11_544 32 ?
Ge2 Lu1 Ir1 88.47(4) 11_544 32 ?
Ge2 Lu1 Ir1 48.05(2) 4_554 32 ?
Ge9 Lu1 Ir1 133.24(3) 20_656 32 ?
Ge9 Lu1 Ir1 82.12(5) 27_565 32 ?
Ir2 Lu1 Ir1 179.57(2) . 32 ?
Ir2 Lu1 Ir1 90.173(19) 27_565 32 ?
Ir1 Lu1 Ir1 89.40(3) 11_544 32 ?
Ge4 Lu2 Ge4 178.19(5) 16_554 . ?
Ge4 Lu2 Ge4 122.77(3) 16_554 6_565 ?
Ge4 Lu2 Ge4 58.67(5) . 6_565 ?
Ge4 Lu2 Ge4 58.67(5) 16_554 12_454 ?
Ge4 Lu2 Ge4 122.77(3) . 12_454 ?
Ge4 Lu2 Ge4 95.29(5) 6_565 12_454 ?
Ge4 Lu2 Ir2 89.10(3) 16_554 . ?
Ge4 Lu2 Ir2 89.10(3) . . ?
Ge4 Lu2 Ir2 132.36(3) 6_565 . ?
Ge4 Lu2 Ir2 132.36(3) 12_454 . ?
Ge4 Lu2 Ge3 74.01(3) 16_554 16_554 ?
Ge4 Lu2 Ge3 104.72(3) . 16_554 ?
Ge4 Lu2 Ge3 104.15(3) 6_565 16_554 ?
Ge4 Lu2 Ge3 131.98(3) 12_454 16_554 ?
Ir2 Lu2 Ge3 47.33(2) . 16_554 ?
Ge4 Lu2 Ge3 104.72(3) 16_554 . ?
Ge4 Lu2 Ge3 74.01(3) . . ?
Ge4 Lu2 Ge3 131.97(3) 6_565 . ?
Ge4 Lu2 Ge3 104.15(3) 12_454 . ?
Ir2 Lu2 Ge3 47.33(2) . . ?
Ge3 Lu2 Ge3 94.66(4) 16_554 . ?
Ge4 Lu2 Ir1 47.98(2) 16_554 16_554 ?
Ge4 Lu2 Ir1 132.04(2) . 16_554 ?
Ge4 Lu2 Ir1 88.14(3) 6_565 16_554 ?
Ge4 Lu2 Ir1 91.18(3) 12_454 16_554 ?
Ir2 Lu2 Ir1 90.508(12) . 16_554 ?
Ge3 Lu2 Ir1 47.10(2) 16_554 16_554 ?
Ge3 Lu2 Ir1 133.85(3) . 16_554 ?
Ge4 Lu2 Ir1 132.04(2) 16_554 . ?
Ge4 Lu2 Ir1 47.98(2) . . ?
Ge4 Lu2 Ir1 91.18(3) 6_565 . ?
Ge4 Lu2 Ir1 88.14(3) 12_454 . ?
Ir2 Lu2 Ir1 90.508(12) . . ?
Ge3 Lu2 Ir1 133.85(3) 16_554 . ?
Ge3 Lu2 Ir1 47.10(2) . . ?
Ir1 Lu2 Ir1 178.98(2) 16_554 . ?
Ge4 Lu2 Ir3 90.90(3) 16_554 . ?
Ge4 Lu2 Ir3 90.90(3) . . ?
Ge4 Lu2 Ir3 47.64(3) 6_565 . ?
Ge4 Lu2 Ir3 47.64(3) 12_454 . ?
Ir2 Lu2 Ir3 180.00(2) . . ?
Ge3 Lu2 Ir3 132.67(2) 16_554 . ?
Ge3 Lu2 Ir3 132.67(2) . . ?
Ir1 Lu2 Ir3 89.492(13) 16_554 . ?
Ir1 Lu2 Ir3 89.492(13) . . ?
Ge4 Lu2 Ge7 129.35(4) 16_554 . ?
Ge4 Lu2 Ge7 49.00(3) . . ?
Ge4 Lu2 Ge7 87.86(4) 6_565 . ?
Ge4 Lu2 Ge7 166.87(4) 12_454 . ?
Ir2 Lu2 Ge7 45.97(2) . . ?
Ge3 Lu2 Ge7 58.81(3) 16_554 . ?
Ge3 Lu2 Ge7 64.90(4) . . ?
Ir1 Lu2 Ge7 101.68(3) 16_554 . ?
Ir1 Lu2 Ge7 79.04(3) . . ?
Ir3 Lu2 Ge7 134.03(2) . . ?
Ge4 Lu2 Ge7 49.00(3) 16_554 16_554 ?
Ge4 Lu2 Ge7 129.35(4) . 16_554 ?
Ge4 Lu2 Ge7 166.87(4) 6_565 16_554 ?
Ge4 Lu2 Ge7 87.86(4) 12_454 16_554 ?
Ir2 Lu2 Ge7 45.97(2) . 16_554 ?
Ge3 Lu2 Ge7 64.90(4) 16_554 16_554 ?
Ge3 Lu2 Ge7 58.81(3) . 16_554 ?
Ir1 Lu2 Ge7 79.04(3) 16_554 16_554 ?
Ir1 Lu2 Ge7 101.68(3) . 16_554 ?
Ir3 Lu2 Ge7 134.03(2) . 16_554 ?
Ge7 Lu2 Ge7 91.95(5) . 16_554 ?
Ge5 Lu3 Ge5 63.02(6) 4_454 11_544 ?
Ge5 Lu3 Ge2 102.84(4) 4_454 . ?
Ge5 Lu3 Ge2 102.84(4) 11_544 . ?
Ge5 Lu3 Ir1 132.93(3) 4_454 . ?
Ge5 Lu3 Ir1 86.49(3) 11_544 . ?
Ge2 Lu3 Ir1 47.409(17) . . ?
Ge5 Lu3 Ir1 86.49(3) 4_454 22 ?
Ge5 Lu3 Ir1 132.94(3) 11_544 22 ?
Ge2 Lu3 Ir1 47.410(17) . 22 ?
Ir1 Lu3 Ir1 90.50(3) . 22 ?
Ge5 Lu3 Ir3 47.30(2) 4_454 17_565 ?
Ge5 Lu3 Ir3 93.23(4) 11_544 17_565 ?
Ge2 Lu3 Ir3 133.221(16) . 17_565 ?
Ir1 Lu3 Ir3 179.37(2) . 17_565 ?
Ir1 Lu3 Ir3 90.103(18) 22 17_565 ?
Ge5 Lu3 Ir3 93.23(4) 4_454 11_544 ?
Ge5 Lu3 Ir3 47.30(2) 11_544 11_544 ?
Ge2 Lu3 Ir3 133.221(16) . 11_544 ?
Ir1 Lu3 Ir3 90.103(19) . 11_544 ?
Ir1 Lu3 Ir3 179.37(2) 22 11_544 ?
Ir3 Lu3 Ir3 89.29(3) 17_565 11_544 ?
Ge5 Lu3 Ge4 132.69(4) 4_454 . ?
Ge5 Lu3 Ge4 70.27(4) 11_544 . ?
Ge2 Lu3 Ge4 94.06(2) . . ?
Ir1 Lu3 Ge4 46.69(2) . . ?
Ir1 Lu3 Ge4 133.96(3) 22 . ?
Ir3 Lu3 Ge4 132.68(3) 17_565 . ?
Ir3 Lu3 Ge4 46.56(2) 11_544 . ?
Ge5 Lu3 Ge4 70.27(4) 4_454 22 ?
Ge5 Lu3 Ge4 132.69(4) 11_544 22 ?
Ge2 Lu3 Ge4 94.06(2) . 22 ?
Ir1 Lu3 Ge4 133.96(3) . 22 ?
Ir1 Lu3 Ge4 46.69(2) 22 22 ?
Ir3 Lu3 Ge4 46.56(2) 17_565 22 ?
Ir3 Lu3 Ge4 132.67(3) 11_544 22 ?
Ge4 Lu3 Ge4 152.60(5) . 22 ?
Ge5 Lu3 Ge8 124.97(4) 4_454 22 ?
Ge5 Lu3 Ge8 167.96(4) 11_544 22 ?
Ge2 Lu3 Ge8 67.57(4) . 22 ?
Ir1 Lu3 Ge8 81.61(3) . 22 ?
Ir1 Lu3 Ge8 45.89(2) 22 22 ?
Ir3 Lu3 Ge8 98.69(3) 17_565 22 ?
Ir3 Lu3 Ge8 134.06(3) 11_544 22 ?
Ge4 Lu3 Ge8 102.33(4) . 22 ?
Ge4 Lu3 Ge8 57.39(3) 22 22 ?
Ge5 Lu3 Ge8 167.96(4) 4_454 . ?
Ge5 Lu3 Ge8 124.97(4) 11_544 . ?
Ge2 Lu3 Ge8 67.57(4) . . ?
Ir1 Lu3 Ge8 45.89(2) . . ?
Ir1 Lu3 Ge8 81.61(3) 22 . ?
Ir3 Lu3 Ge8 134.06(3) 17_565 . ?
Ir3 Lu3 Ge8 98.69(3) 11_544 . ?
Ge4 Lu3 Ge8 57.39(3) . . ?
Ge4 Lu3 Ge8 102.33(4) 22 . ?
Ge8 Lu3 Ge8 45.57(5) 22 . ?
Ge5 Lu3 Ge8 116.19(4) 4_454 6_565 ?
Ge5 Lu3 Ge8 92.29(4) 11_544 6_565 ?
Ge2 Lu3 Ge8 140.83(4) . 6_565 ?
Ir1 Lu3 Ge8 98.90(3) . 6_565 ?
Ir1 Lu3 Ge8 134.43(3) 22 6_565 ?
Ir3 Lu3 Ge8 80.54(3) 17_565 6_565 ?
Ir3 Lu3 Ge8 45.26(2) 11_544 6_565 ?
Ge4 Lu3 Ge8 57.23(3) . 6_565 ?
Ge4 Lu3 Ge8 101.82(4) 22 6_565 ?
Ge8 Lu3 Ge8 91.35(4) 22 6_565 ?
Ge8 Lu3 Ge8 74.11(5) . 6_565 ?
Ge8 Ir1 Ge6 139.94(5) . . ?
Ge8 Ir1 Ge7 75.65(5) . 12_454 ?
Ge6 Ir1 Ge7 141.03(5) . 12_454 ?
Ge8 Ir1 Ge4 75.80(5) . . ?
Ge6 Ir1 Ge4 83.09(5) . . ?
Ge7 Ir1 Ge4 130.47(5) 12_454 . ?
Ge8 Ir1 Ge3 134.04(4) . . ?
Ge6 Ir1 Ge3 80.76(5) . . ?
Ge7 Ir1 Ge3 77.53(5) 12_454 . ?
Ge4 Ir1 Ge3 94.89(4) . . ?
Ge8 Ir1 Ge2 89.29(4) . . ?
Ge6 Ir1 Ge2 80.68(6) . . ?
Ge7 Ir1 Ge2 85.88(5) 12_454 . ?
Ge4 Ir1 Ge2 133.02(4) . . ?
Ge3 Ir1 Ge2 125.13(4) . . ?
Ge8 Ir1 Lu3 67.86(3) . . ?
Ge6 Ir1 Lu3 72.69(4) . . ?
Ge7 Ir1 Lu3 133.04(4) 12_454 . ?
Ge4 Ir1 Lu3 67.43(3) . . ?
Ge3 Ir1 Lu3 149.39(3) . . ?
Ge2 Ir1 Lu3 65.67(4) . . ?
Ge8 Ir1 Lu2 69.82(3) . . ?
Ge6 Ir1 Lu2 128.52(4) . . ?
Ge7 Ir1 Lu2 69.50(3) 12_454 . ?
Ge4 Ir1 Lu2 62.96(3) . . ?
Ge3 Ir1 Lu2 66.08(3) . . ?
Ge2 Ir1 Lu2 150.69(4) . . ?
Lu3 Ir1 Lu2 120.442(18) . . ?
Ge8 Ir1 Lu1 136.60(4) . 12_454 ?
Ge6 Ir1 Lu1 71.01(4) . 12_454 ?
Ge7 Ir1 Lu1 70.31(3) 12_454 12_454 ?
Ge4 Ir1 Lu1 147.56(3) . 12_454 ?
Ge3 Ir1 Lu1 62.58(3) . 12_454 ?
Ge2 Ir1 Lu1 62.57(3) . 12_454 ?
Lu3 Ir1 Lu1 119.98(2) . 12_454 ?
Lu2 Ir1 Lu1 119.582(18) . 12_454 ?
Ge7 Ir2 Ge7 138.45(7) . 16_554 ?
Ge7 Ir2 Ge9 140.11(5) . . ?
Ge7 Ir2 Ge9 76.39(6) 16_554 . ?
Ge7 Ir2 Ge9 76.39(6) . 20_656 ?
Ge7 Ir2 Ge9 140.11(5) 16_554 20_656 ?
Ge9 Ir2 Ge9 82.85(12) . 20_656 ?
Ge7 Ir2 Ge3 77.48(5) . 16_554 ?
Ge7 Ir2 Ge3 86.30(4) 16_554 16_554 ?
Ge9 Ir2 Ge3 89.23(6) . 16_554 ?
Ge9 Ir2 Ge3 127.45(5) 20_656 16_554 ?
Ge7 Ir2 Ge3 86.30(4) . . ?
Ge7 Ir2 Ge3 77.48(5) 16_554 . ?
Ge9 Ir2 Ge3 127.46(5) . . ?
Ge9 Ir2 Ge3 89.23(6) 20_656 . ?
Ge3 Ir2 Ge3 133.28(6) 16_554 . ?
Ge7 Ir2 Lu2 69.23(3) . . ?
Ge7 Ir2 Lu2 69.23(3) 16_554 . ?
Ge9 Ir2 Lu2 138.58(6) . . ?
Ge9 Ir2 Lu2 138.57(6) 20_656 . ?
Ge3 Ir2 Lu2 66.64(3) 16_554 . ?
Ge3 Ir2 Lu2 66.64(3) . . ?
Ge7 Ir2 Lu1 70.81(3) . . ?
Ge7 Ir2 Lu1 133.16(4) 16_554 . ?
Ge9 Ir2 Lu1 69.70(5) . . ?
Ge9 Ir2 Lu1 66.16(4) 20_656 . ?
Ge3 Ir2 Lu1 62.43(3) 16_554 . ?
Ge3 Ir2 Lu1 149.33(3) . . ?
Lu2 Ir2 Lu1 120.059(15) . . ?
Ge7 Ir2 Lu1 133.16(4) . 20_656 ?
Ge7 Ir2 Lu1 70.81(3) 16_554 20_656 ?
Ge9 Ir2 Lu1 66.16(4) . 20_656 ?
Ge9 Ir2 Lu1 69.70(5) 20_656 20_656 ?
Ge3 Ir2 Lu1 149.33(3) 16_554 20_656 ?
Ge3 Ir2 Lu1 62.43(3) . 20_656 ?
Lu2 Ir2 Lu1 120.059(15) . 20_656 ?
Lu1 Ir2 Lu1 119.88(3) . 20_656 ?
Ge8 Ir3 Ge8 138.83(6) . 16_554 ?
Ge8 Ir3 Ge5 85.10(5) . . ?
Ge8 Ir3 Ge5 131.08(5) 16_554 . ?
Ge8 Ir3 Ge5 131.08(5) . 20_666 ?
Ge8 Ir3 Ge5 85.10(5) 16_554 20_666 ?
Ge5 Ir3 Ge5 71.20(8) . 20_666 ?
Ge8 Ir3 Ge4 76.00(5) . 6_565 ?
Ge8 Ir3 Ge4 85.70(4) 16_554 6_565 ?
Ge5 Ir3 Ge4 135.21(4) . 6_565 ?
Ge5 Ir3 Ge4 91.34(5) 20_666 6_565 ?
Ge8 Ir3 Ge4 85.70(4) . 12_454 ?
Ge8 Ir3 Ge4 76.00(5) 16_554 12_454 ?
Ge5 Ir3 Ge4 91.33(5) . 12_454 ?
Ge5 Ir3 Ge4 135.21(4) 20_666 12_454 ?
Ge4 Ir3 Ge4 126.42(6) 6_565 12_454 ?
Ge8 Ir3 Lu3 68.05(3) . 17_565 ?
Ge8 Ir3 Lu3 136.43(4) 16_554 17_565 ?
Ge5 Ir3 Lu3 68.52(4) . 17_565 ?
Ge5 Ir3 Lu3 63.59(4) 20_666 17_565 ?
Ge4 Ir3 Lu3 66.78(3) 6_565 17_565 ?
Ge4 Ir3 Lu3 147.55(3) 12_454 17_565 ?
Ge8 Ir3 Lu3 136.43(4) . 12_454 ?
Ge8 Ir3 Lu3 68.05(3) 16_554 12_454 ?
Ge5 Ir3 Lu3 63.59(4) . 12_454 ?
Ge5 Ir3 Lu3 68.52(4) 20_666 12_454 ?
Ge4 Ir3 Lu3 147.55(3) 6_565 12_454 ?
Ge4 Ir3 Lu3 66.78(3) 12_454 12_454 ?
Lu3 Ir3 Lu3 120.17(3) 17_565 12_454 ?
Ge8 Ir3 Lu2 69.42(3) . . ?
Ge8 Ir3 Lu2 69.42(3) 16_554 . ?
Ge5 Ir3 Lu2 144.40(4) . . ?
Ge5 Ir3 Lu2 144.40(4) 20_666 . ?
Ge4 Ir3 Lu2 63.21(3) 6_565 . ?
Ge4 Ir3 Lu2 63.21(3) 12_454 . ?
Lu3 Ir3 Lu2 119.913(14) 17_565 . ?
Lu3 Ir3 Lu2 119.914(15) 12_454 . ?
Ge1B Ge1A Ge6 65.2(11) . 26 ?
Ge1B Ge1A Ge7 85.5(5) . 26 ?
Ge6 Ge1A Ge7 110.55(5) 26 26 ?
Ge1B Ge1A Ge7 85.5(5) . 6_565 ?
Ge6 Ge1A Ge7 110.55(5) 26 6_565 ?
Ge7 Ge1A Ge7 129.04(9) 26 6_565 ?
Ge1B Ge1A Ge8 152.89(18) . 20_666 ?
Ge6 Ge1A Ge8 115.95(7) 26 20_666 ?
Ge7 Ge1A Ge8 68.51(4) 26 20_666 ?
Ge7 Ge1A Ge8 116.50(7) 6_565 20_666 ?
Ge1B Ge1A Ge8 152.89(18) . 16_554 ?
Ge6 Ge1A Ge8 115.95(7) 26 16_554 ?
Ge7 Ge1A Ge8 116.50(7) 26 16_554 ?
Ge7 Ge1A Ge8 68.51(4) 6_565 16_554 ?
Ge8 Ge1A Ge8 53.50(6) 20_666 16_554 ?
Ge1B Ge1A Ge9 58.2(11) . 11_544 ?
Ge6 Ge1A Ge9 123.40(8) 26 11_544 ?
Ge7 Ge1A Ge9 66.37(4) 26 11_544 ?
Ge7 Ge1A Ge9 66.37(4) 6_565 11_544 ?
Ge8 Ge1A Ge9 114.14(7) 20_666 11_544 ?
Ge8 Ge1A Ge9 114.14(7) 16_554 11_544 ?
Ge1A Ge1B Ge6 91.2(13) . 26 ?
Ge1A Ge1B Ge9 101.9(13) . 11_544 ?
Ge6 Ge1B Ge9 167.0(10) 26 11_544 ?
Ge1A Ge1B Ge3 145.9(4) . 6_565 ?
Ge6 Ge1B Ge3 82.5(6) 26 6_565 ?
Ge9 Ge1B Ge3 86.6(6) 11_544 6_565 ?
Ge1A Ge1B Ge3 145.9(4) . 26 ?
Ge6 Ge1B Ge3 82.5(6) 26 26 ?
Ge9 Ge1B Ge3 86.6(6) 11_544 26 ?
Ge3 Ge1B Ge3 66.7(5) 6_565 26 ?
Ge1A Ge1B Ge7 73.0(6) . 26 ?
Ge6 Ge1B Ge7 114.3(4) 26 26 ?
Ge9 Ge1B Ge7 70.3(4) 11_544 26 ?
Ge3 Ge1B Ge7 139.8(7) 6_565 26 ?
Ge3 Ge1B Ge7 79.2(2) 26 26 ?
Ge1A Ge1B Ge7 73.0(6) . 6_565 ?
Ge6 Ge1B Ge7 114.3(4) 26 6_565 ?
Ge9 Ge1B Ge7 70.3(4) 11_544 6_565 ?
Ge3 Ge1B Ge7 79.2(2) 6_565 6_565 ?
Ge3 Ge1B Ge7 139.8(7) 26 6_565 ?
Ge7 Ge1B Ge7 120.0(7) 26 6_565 ?
Ir1 Ge2 Ir1 125.11(6) . 22 ?
Ir1 Ge2 Ge9 104.40(4) . 18_556 ?
Ir1 Ge2 Ge9 104.40(4) 22 18_556 ?
Ir1 Ge2 Ge2 109.92(3) . 10_454 ?
Ir1 Ge2 Ge2 109.92(3) 22 10_454 ?
Ge9 Ge2 Ge2 99.67(6) 18_556 10_454 ?
Ir1 Ge2 Lu1 165.21(5) . 3_545 ?
Ir1 Ge2 Lu1 69.384(17) 22 3_545 ?
Ge9 Ge2 Lu1 66.06(4) 18_556 3_545 ?
Ge2 Ge2 Lu1 62.85(3) 10_454 3_545 ?
Ir1 Ge2 Lu1 69.385(17) . 12_454 ?
Ir1 Ge2 Lu1 165.21(5) 22 12_454 ?
Ge9 Ge2 Lu1 66.06(4) 18_556 12_454 ?
Ge2 Ge2 Lu1 62.85(3) 10_454 12_454 ?
Lu1 Ge2 Lu1 95.99(5) 3_545 12_454 ?
Ir1 Ge2 Lu3 66.92(3) . . ?
Ir1 Ge2 Lu3 66.92(3) 22 . ?
Ge9 Ge2 Lu3 154.38(8) 18_556 . ?
Ge2 Ge2 Lu3 105.94(3) 10_454 . ?
Lu1 Ge2 Lu3 126.58(3) 3_545 . ?
Lu1 Ge2 Lu3 126.58(3) 12_454 . ?
Ir2 Ge3 Ir1 125.00(5) . . ?
Ir2 Ge3 Ge1B 82.5(4) . 26_545 ?
Ir1 Ge3 Ge1B 86.6(4) . 26_545 ?
Ir2 Ge3 Ge3 109.28(5) . 5 ?
Ir1 Ge3 Ge3 109.00(5) . 5 ?
Ge1B Ge3 Ge3 146.6(3) 26_545 5 ?
Ir2 Ge3 Ge3 109.01(3) . 29 ?
Ir1 Ge3 Ge3 108.93(3) . 29 ?
Ge1B Ge3 Ge3 56.7(3) 26_545 29 ?
Ge3 Ge3 Ge3 90.0 5 29 ?
Ir2 Ge3 Lu1 69.32(3) . 20_656 ?
Ir1 Ge3 Lu1 165.68(5) . 20_656 ?
Ge1B Ge3 Lu1 95.7(4) 26_545 20_656 ?
Ge3 Ge3 Lu1 62.18(4) 5 20_656 ?
Ge3 Ge3 Lu1 61.72(2) 29 20_656 ?
Ir2 Ge3 Lu1 165.54(5) . 12_454 ?
Ir1 Ge3 Lu1 69.47(3) . 12_454 ?
Ge1B Ge3 Lu1 99.7(4) 26_545 12_454 ?
Ge3 Ge3 Lu1 61.48(4) 5 12_454 ?
Ge3 Ge3 Lu1 61.92(2) 29 12_454 ?
Lu1 Ge3 Lu1 96.22(4) 20_656 12_454 ?
Ir2 Ge3 Lu2 66.03(3) . . ?
Ir1 Ge3 Lu2 66.83(3) . . ?
Ge1B Ge3 Lu2 108.1(3) 26_545 . ?
Ge3 Ge3 Lu2 105.25(2) 5 . ?
Ge3 Ge3 Lu2 164.75(2) 29 . ?
Lu1 Ge3 Lu2 125.14(4) 20_656 . ?
Lu1 Ge3 Lu2 125.73(4) 12_454 . ?
Ir1 Ge4 Ir3 126.09(5) . 11_544 ?
Ir1 Ge4 Ge7 105.46(5) . . ?
Ir3 Ge4 Ge7 105.51(5) 11_544 . ?
Ir1 Ge4 Lu2 69.06(3) . . ?
Ir3 Ge4 Lu2 164.50(5) 11_544 . ?
Ge7 Ge4 Lu2 69.88(4) . . ?
Ir1 Ge4 Lu2 164.30(5) . 11_544 ?
Ir3 Ge4 Lu2 69.14(3) 11_544 11_544 ?
Ge7 Ge4 Lu2 70.35(4) . 11_544 ?
Lu2 Ge4 Lu2 95.53(4) . 11_544 ?
Ir1 Ge4 Lu3 65.88(3) . . ?
Ir3 Ge4 Lu3 66.66(3) 11_544 . ?
Ge7 Ge4 Lu3 153.49(6) . . ?
Lu2 Ge4 Lu3 124.04(4) . . ?
Lu2 Ge4 Lu3 124.50(4) 11_544 . ?
Ir3 Ge5 Ir3 126.62(7) . 27_465 ?
Ir3 Ge5 Ge6 106.81(4) . 12_454 ?
Ir3 Ge5 Ge6 106.81(4) 27_465 12_454 ?
Ir3 Ge5 Ge5 113.30(8) . 27_465 ?
Ir3 Ge5 Ge5 54.40(4) 27_465 27_465 ?
Ge6 Ge5 Ge5 138.95(7) 12_454 27_465 ?
Ir3 Ge5 Ge5 54.40(4) . 20_666 ?
Ir3 Ge5 Ge5 113.30(8) 27_465 20_666 ?
Ge6 Ge5 Ge5 138.95(7) 12_454 20_666 ?
Ge5 Ge5 Ge5 66.34(6) 27_465 20_666 ?
Ir3 Ge5 Lu3 69.118(18) . 12_454 ?
Ir3 Ge5 Lu3 161.58(6) 27_465 12_454 ?
Ge6 Ge5 Lu3 73.24(5) 12_454 12_454 ?
Ge5 Ge5 Lu3 113.09(3) 27_465 12_454 ?
Ge5 Ge5 Lu3 65.98(5) 20_666 12_454 ?
Ir3 Ge5 Lu3 161.58(6) . 3 ?
Ir3 Ge5 Lu3 69.119(18) 27_465 3 ?
Ge6 Ge5 Lu3 73.24(5) 12_454 3 ?
Ge5 Ge5 Lu3 65.98(5) 27_465 3 ?
Ge5 Ge5 Lu3 113.09(3) 20_666 3 ?
Lu3 Ge5 Lu3 93.84(5) 12_454 3 ?
Ir3 Ge5 Lu3 65.69(3) . 17_565 ?
Ir3 Ge5 Lu3 65.69(3) 27_465 17_565 ?
Ge6 Ge5 Lu3 153.66(8) 12_454 17_565 ?
Ge5 Ge5 Lu3 59.03(6) 27_465 17_565 ?
Ge5 Ge5 Lu3 59.03(6) 20_666 17_565 ?
Lu3 Ge5 Lu3 122.22(4) 12_454 17_565 ?
Lu3 Ge5 Lu3 122.22(4) 3 17_565 ?
Ge1B Ge6 Ir1 93.4(2) 26_545 . ?
Ge1B Ge6 Ir1 93.4(2) 26_545 29 ?
Ir1 Ge6 Ir1 128.57(8) . 29 ?
Ge1B Ge6 Ge1A 23.6(5) 26_545 26_545 ?
Ir1 Ge6 Ge1A 103.04(5) . 26_545 ?
Ir1 Ge6 Ge1A 103.04(5) 29 26_545 ?
Ge1B Ge6 Ge5 98.9(5) 26_545 11_544 ?
Ir1 Ge6 Ge5 114.56(4) . 11_544 ?
Ir1 Ge6 Ge5 114.56(4) 29 11_544 ?
Ge1A Ge6 Ge5 75.30(7) 26_545 11_544 ?
Ge1B Ge6 Lu1 96.7(5) 26_545 12_454 ?
Ir1 Ge6 Lu1 64.29(4) . 12_454 ?
Ir1 Ge6 Lu1 64.29(4) 29 12_454 ?
Ge1A Ge6 Lu1 120.33(7) 26_545 12_454 ?
Ge5 Ge6 Lu1 164.37(8) 11_544 12_454 ?
Ge1B Ge6 Lu3 129.1(3) 26_545 . ?
Ir1 Ge6 Lu3 62.89(3) . . ?
Ir1 Ge6 Lu3 137.19(7) 29 . ?
Ge1A Ge6 Lu3 114.45(5) 26_545 . ?
Ge5 Ge6 Lu3 59.90(4) 11_544 . ?
Lu1 Ge6 Lu3 109.41(4) 12_454 . ?
Ge1B Ge6 Lu3 129.1(3) 26_545 10_454 ?
Ir1 Ge6 Lu3 137.19(7) . 10_454 ?
Ir1 Ge6 Lu3 62.89(3) 29 10_454 ?
Ge1A Ge6 Lu3 114.45(5) 26_545 10_454 ?
Ge5 Ge6 Lu3 59.90(4) 11_544 10_454 ?
Lu1 Ge6 Lu3 109.41(4) 12_454 10_454 ?
Lu3 Ge6 Lu3 82.59(4) . 10_454 ?
Ir2 Ge7 Ir1 128.23(6) . 11_544 ?
Ir2 Ge7 Ge4 115.91(6) . . ?
Ir1 Ge7 Ge4 115.75(5) 11_544 . ?
Ir2 Ge7 Ge1A 99.13(6) . 26_545 ?
Ir1 Ge7 Ge1A 94.89(6) 11_544 26_545 ?
Ge4 Ge7 Ge1A 77.44(6) . 26_545 ?
Ir2 Ge7 Ge1B 79.0(4) . 26_545 ?
Ir1 Ge7 Ge1B 113.4(4) 11_544 26_545 ?
Ge4 Ge7 Ge1B 79.8(4) . 26_545 ?
Ge1A Ge7 Ge1B 21.5(4) 26_545 26_545 ?
Ir2 Ge7 Lu2 64.80(3) . . ?
Ir1 Ge7 Lu2 144.83(6) 11_544 . ?
Ge4 Ge7 Lu2 61.12(4) . . ?
Ge1A Ge7 Lu2 116.54(6) 26_545 . ?
Ge1B Ge7 Lu2 100.7(4) 26_545 . ?
Ir2 Ge7 Lu2 144.45(6) . 11_544 ?
Ir1 Ge7 Lu2 64.81(3) 11_544 11_544 ?
Ge4 Ge7 Lu2 61.23(4) . 11_544 ?
Ge1A Ge7 Lu2 113.41(5) 26_545 11_544 ?
Ge1B Ge7 Lu2 130.1(4) 26_545 11_544 ?
Lu2 Ge7 Lu2 87.23(4) . 11_544 ?
Ir2 Ge7 Lu1 64.09(3) . . ?
Ir1 Ge7 Lu1 64.46(3) 11_544 . ?
Ge4 Ge7 Lu1 170.18(6) . . ?
Ge1A Ge7 Lu1 112.37(6) 26_545 . ?
Ge1B Ge7 Lu1 109.4(4) 26_545 . ?
Lu2 Ge7 Lu1 112.52(4) . . ?
Lu2 Ge7 Lu1 112.51(4) 11_544 . ?
Ir3 Ge8 Ge8 114.03(3) . 22 ?
Ir3 Ge8 Ir1 129.60(6) . . ?
Ge8 Ge8 Ir1 113.93(3) 22 . ?
Ir3 Ge8 Ge1A 94.41(5) . 27_465 ?
Ge8 Ge8 Ge1A 63.25(3) 22 27_465 ?
Ir1 Ge8 Ge1A 93.61(6) . 27_465 ?
Ir3 Ge8 Lu3 150.28(6) . . ?
Ge8 Ge8 Lu3 67.21(2) 22 . ?
Ir1 Ge8 Lu3 66.24(3) . . ?
Ge1A Ge8 Lu3 110.74(5) 27_465 . ?
Ir3 Ge8 Lu3 66.70(3) . 17_565 ?
Ge8 Ge8 Lu3 67.42(2) 22 17_565 ?
Ir1 Ge8 Lu3 149.55(6) . 17_565 ?
Ge1A Ge8 Lu3 112.01(5) 27_465 17_565 ?
Lu3 Ge8 Lu3 88.65(4) . 17_565 ?
Ir3 Ge8 Lu2 65.75(3) . . ?
Ge8 Ge8 Lu2 174.52(3) 22 . ?
Ir1 Ge8 Lu2 65.00(3) . . ?
Ge1A Ge8 Lu2 111.28(5) 27_465 . ?
Lu3 Ge8 Lu2 115.93(4) . . ?
Lu3 Ge8 Lu2 116.43(4) 17_565 . ?
Ir2 Ge9 Ir2 127.67(8) . 27_565 ?
Ir2 Ge9 Ge1B 83.5(2) . 12_454 ?
Ir2 Ge9 Ge1B 83.5(2) 27_565 12_454 ?
Ir2 Ge9 Ge2 115.55(4) . 18_656 ?
Ir2 Ge9 Ge2 115.55(4) 27_565 18_656 ?
Ge1B Ge9 Ge2 92.8(5) 12_454 18_656 ?
Ir2 Ge9 Ge1A 92.26(6) . 12_454 ?
Ir2 Ge9 Ge1A 92.25(6) 27_565 12_454 ?
Ge1B Ge9 Ge1A 20.0(5) 12_454 12_454 ?
Ge2 Ge9 Ge1A 72.87(7) 18_656 12_454 ?
Ir2 Ge9 Lu1 67.15(2) . 20_656 ?
Ir2 Ge9 Lu1 153.39(9) 27_565 20_656 ?
Ge1B Ge9 Lu1 122.3(3) 12_454 20_656 ?
Ge2 Ge9 Lu1 61.47(4) 18_656 20_656 ?
Ge1A Ge9 Lu1 110.37(6) 12_454 20_656 ?
Ir2 Ge9 Lu1 153.39(9) . 27_565 ?
Ir2 Ge9 Lu1 67.15(2) 27_565 27_565 ?
Ge1B Ge9 Lu1 122.3(3) 12_454 27_565 ?
Ge2 Ge9 Lu1 61.47(4) 18_656 27_565 ?
Ge1A Ge9 Lu1 110.37(6) 12_454 27_565 ?
Lu1 Ge9 Lu1 91.18(6) 20_656 27_565 ?
Ir2 Ge9 Lu1 64.74(4) . . ?
Ir2 Ge9 Lu1 64.74(4) 27_565 . ?
Ge1B Ge9 Lu1 89.7(5) 12_454 . ?
Ge2 Ge9 Lu1 177.47(10) 18_656 . ?
Ge1A Ge9 Lu1 109.66(7) 12_454 . ?
Lu1 Ge9 Lu1 117.04(6) 20_656 . ?
Lu1 Ge9 Lu1 117.04(6) 27_565 . ?
 
_refine_diff_density_max    3.441
_refine_diff_density_min   -3.657
_refine_diff_density_rms    0.663



