# Supplementary Material (ESI) for ChemComm # This journal is © The Royal Society of Chemistry 2000 # CCDC Number: 182/1784 data_fefa _audit_creation_method SHELXL-97 _chemical_name_systematic ; ? ; _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'C130 H90 N3 O22 P7 Rh10' _chemical_formula_weight 3291.94 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'P' 'P' 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Rh' 'Rh' -1.1178 0.9187 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _symmetry_cell_setting triclinic _symmetry_space_group_name_H-M P-1 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 16.2084(7) _cell_length_b 16.3039(7) _cell_length_c 23.9367(11) _cell_angle_alpha 91.241(1) _cell_angle_beta 94.880(1) _cell_angle_gamma 90.067(1) _cell_volume 6301.1(5) _cell_formula_units_Z 2 _cell_measurement_temperature 293(2) _cell_measurement_reflns_used ? _cell_measurement_theta_min ? _cell_measurement_theta_max ? _exptl_crystal_description ? _exptl_crystal_colour ? _exptl_crystal_size_max 0.23 _exptl_crystal_size_mid 0.17 _exptl_crystal_size_min 0.15 _exptl_crystal_density_meas ? _exptl_crystal_density_diffrn 1.735 _exptl_crystal_density_method 'not measured' _exptl_crystal_F_000 3244 _exptl_absorpt_coefficient_mu 1.431 _exptl_absorpt_correction_type ? _exptl_absorpt_correction_T_min ? _exptl_absorpt_correction_T_max ? _exptl_absorpt_process_details ? _exptl_special_details ; ? ; _diffrn_ambient_temperature 293(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_radiation_source 'fine-focus sealed tube' _diffrn_radiation_monochromator graphite _diffrn_measurement_device_type SMART _diffrn_measurement_method ? _diffrn_detector_area_resol_mean ? _diffrn_standards_number ? _diffrn_standards_interval_count ? _diffrn_standards_interval_time ? _diffrn_standards_decay_% No _diffrn_reflns_number 66631 _diffrn_reflns_av_R_equivalents 0.0432 _diffrn_reflns_av_sigmaI/netI 0.0505 _diffrn_reflns_limit_h_min -20 _diffrn_reflns_limit_h_max 20 _diffrn_reflns_limit_k_min -20 _diffrn_reflns_limit_k_max 20 _diffrn_reflns_limit_l_min -30 _diffrn_reflns_limit_l_max 30 _diffrn_reflns_theta_min 0.85 _diffrn_reflns_theta_max 27.33 _reflns_number_total 24974 _reflns_number_gt 17154 _reflns_threshold_expression >2sigma(I) _computing_data_collection ? _computing_cell_refinement ? _computing_data_reduction ? _computing_structure_solution 'SHELXS-97 (Sheldrick, 1990)' _computing_structure_refinement 'SHELXL-97 (Sheldrick, 1997)' _computing_molecular_graphics ? _computing_publication_material ? _refine_special_details ; Refinement of F^2^ against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F^2^, conventional R-factors R are based on F, with F set to zero for negative F^2^. The threshold expression of F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F^2^ are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger. ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type fullcycle _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'calc w=1/[\s^2^(Fo^2^)+(0.0659P)^2^+27.8601P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment mixed _refine_ls_extinction_method none _refine_ls_extinction_coef ? _refine_ls_number_reflns 24974 _refine_ls_number_parameters 882 _refine_ls_number_restraints 55 _refine_ls_R_factor_all 0.0980 _refine_ls_R_factor_gt 0.0634 _refine_ls_wR_factor_ref 0.1696 _refine_ls_wR_factor_gt 0.1494 _refine_ls_goodness_of_fit_ref 1.035 _refine_ls_restrained_S_all 1.049 _refine_ls_shift/su_max 0.006 _refine_ls_shift/su_mean 0.002 _exptl_absorpt_correction_nazim SADABS _diffrn_measurement_domega 0.3 _diffrn_measurement_rtime 30 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_symmetry_multiplicity _atom_site_calc_flag _atom_site_refinement_flags _atom_site_disorder_assembly _atom_site_disorder_group Rh1A Rh 0.49103(4) 0.68175(3) 0.47058(3) 0.05222(15) Uani 1 1 d D . . Rh2A Rh 0.37867(6) 0.54738(6) 0.43841(4) 0.0352(2) Uani 0.50 1 d PD . . Rh3A Rh 0.55837(6) 0.54462(6) 0.41528(4) 0.0392(2) Uani 0.50 1 d PD . . Rh4A Rh 0.61321(6) 0.59040(6) 0.53426(4) 0.0361(2) Uani 0.50 1 d PD . . Rh5A Rh 0.43092(6) 0.59223(6) 0.56251(4) 0.0361(2) Uani 0.50 1 d PD . . Rh6A Rh 0.37087(6) 0.43130(6) 0.52445(4) 0.0366(2) Uani 0.50 1 d P . . Rh7A Rh 0.46639(6) 0.39683(6) 0.42473(4) 0.0351(2) Uani 0.50 1 d P . . Rh8A Rh 0.62645(6) 0.42581(6) 0.49349(4) 0.0377(2) Uani 0.50 1 d P . . Rh9A Rh 0.53803(6) 0.46399(6) 0.59598(4) 0.0359(2) Uani 0.50 1 d P . . PA P 0.5000 0.5000 0.5000 0.0341(5) Uani 1 2 d S . . C1A C 0.4897(5) 0.7918(4) 0.4559(3) 0.062(2) Uiso 1 1 d D . . O1A O 0.4901(5) 0.8635(3) 0.4479(3) 0.116(3) Uiso 1 1 d D . . C2A C 0.3263(9) 0.5497(9) 0.3680(3) 0.048(3) Uiso 0.50 1 d PD . . C2A' C 0.3694(6) 0.5389(9) 0.3511(5) 0.050(3) Uiso 0.50 1 d PD . . O2A O 0.3041(4) 0.5430(4) 0.3208(2) 0.091(2) Uiso 1 1 d D . . C3A C 0.6638(6) 0.5587(10) 0.3907(7) 0.061(4) Uiso 0.50 1 d PD . . C3A' C 0.7006(9) 0.5680(10) 0.4206(5) 0.056(4) Uiso 0.50 1 d PD . . O3A O 0.7367(4) 0.5639(5) 0.3805(3) 0.104(2) Uiso 1 1 d D . . C4A C 0.6574(9) 0.6388(8) 0.6006(4) 0.052(3) Uiso 0.50 1 d PD . . C4A' C 0.6206(7) 0.6410(10) 0.6232(6) 0.065(4) Uiso 0.50 1 d PD . . O4A O 0.6846(4) 0.6667(5) 0.6452(3) 0.121(3) Uiso 1 1 d D . . C5A C 0.3344(6) 0.6250(9) 0.5900(7) 0.055(4) Uiso 0.50 1 d PD . . C5A' C 0.3075(8) 0.6202(8) 0.5593(5) 0.047(3) Uiso 0.50 1 d PD . . O5A O 0.2684(4) 0.6482(4) 0.5969(3) 0.0904(19) Uiso 1 1 d D . . C12A C 0.3623(5) 0.6678(5) 0.4551(3) 0.0558(18) Uiso 1 1 d . . . O12A O 0.3077(5) 0.7134(5) 0.4418(3) 0.102(2) Uiso 1 1 d . . . C13A C 0.5085(5) 0.6418(5) 0.3830(3) 0.0601(19) Uiso 1 1 d . . . O13A O 0.5139(5) 0.6762(5) 0.3412(4) 0.115(3) Uiso 1 1 d . . . C14A C 0.6295(5) 0.6876(5) 0.4887(3) 0.0597(19) Uiso 1 1 d . . . O14A O 0.6745(4) 0.7441(5) 0.4870(3) 0.095(2) Uiso 1 1 d . . . C15A C 0.4738(4) 0.7061(4) 0.5618(3) 0.0497(16) Uiso 1 1 d . . . O15A O 0.4608(4) 0.7662(4) 0.5864(3) 0.0806(17) Uiso 1 1 d . . . C48A C 0.7106(4) 0.5120(4) 0.5291(3) 0.0469(16) Uiso 1 1 d . . . O48A O 0.7843(4) 0.5151(4) 0.5393(2) 0.0748(16) Uiso 1 1 d . . . C59A C 0.4758(4) 0.5487(4) 0.6376(3) 0.0454(15) Uiso 1 1 d . . . O59A O 0.4670(4) 0.5660(4) 0.6854(3) 0.0739(16) Uiso 1 1 d . . . Rh1B Rh -0.18471(4) 0.00201(4) -0.03833(3) 0.06041(17) Uani 1 1 d D . . Rh2B Rh -0.06677(6) -0.12943(6) -0.01567(4) 0.0380(2) Uani 0.50 1 d PD . . Rh3B Rh -0.03908(6) -0.00074(6) -0.09799(4) 0.0361(2) Uani 0.50 1 d PD . . Rh4B Rh -0.06159(6) 0.13496(6) -0.01228(4) 0.0371(2) Uani 0.50 1 d PD . . Rh5B Rh -0.09167(6) 0.00314(6) 0.07612(4) 0.0370(2) Uani 0.50 1 d PD . . Rh6B Rh 0.05477(6) -0.09719(6) 0.07506(4) 0.0343(2) Uani 0.50 1 d PD . . Rh7B Rh 0.09655(6) -0.09262(6) -0.04519(4) 0.0350(2) Uani 0.50 1 d PD . . Rh8B Rh 0.09836(6) 0.08843(6) -0.04207(4) 0.0357(2) Uani 0.50 1 d PD . . Rh9B Rh 0.05621(6) 0.09330(6) 0.08033(4) 0.0360(2) Uani 0.50 1 d PD . . PB P 0.0000 0.0000 0.0000 0.0399(5) Uani 1 2 d S . . C1B C -0.2956(3) 0.0078(4) -0.0617(3) 0.0504(17) Uiso 1 1 d D . . O1B O -0.3662(3) 0.0090(4) -0.0766(3) 0.0882(19) Uiso 1 1 d D . . C2B' C -0.0811(9) -0.2032(5) -0.0945(6) 0.053(3) Uiso 0.50 1 d PD . . C2B C -0.0786(10) -0.2252(7) -0.0579(6) 0.059(4) Uiso 0.50 1 d PD . . O2B O -0.0911(5) -0.2772(4) -0.0939(3) 0.111(2) Uiso 1 1 d D . . C3B' C -0.0536(9) 0.1219(10) -0.1484(3) 0.056(4) Uiso 0.50 1 d PD . . C3B C -0.0347(10) 0.0764(8) -0.1551(5) 0.055(4) Uiso 0.50 1 d PD . . O3B O -0.0386(5) 0.1260(4) -0.1941(2) 0.106(2) Uiso 1 1 d D . . C4B' C -0.1153(10) 0.2051(5) 0.0501(7) 0.059(4) Uiso 0.50 1 d PD . . C4B C -0.0913(10) 0.2306(7) 0.0215(6) 0.062(4) Uiso 0.50 1 d PD . . O4B O -0.1214(5) 0.2803(4) 0.0501(3) 0.123(3) Uiso 1 1 d D . . C5B C -0.1334(9) -0.0529(8) 0.1338(5) 0.062(4) Uiso 0.50 1 d PD . . C5B' C -0.1523(8) -0.1069(9) 0.1064(4) 0.053(3) Uiso 0.50 1 d PD . . O5B O -0.1727(6) -0.1055(5) 0.1549(3) 0.144(3) Uiso 1 1 d D . . C12B C -0.1926(5) -0.1171(5) -0.0086(3) 0.0537(18) Uiso 1 1 d . . . O12B O -0.2446(4) -0.1688(4) -0.0116(3) 0.092(2) Uiso 1 1 d . . . C13B C -0.1528(5) -0.0500(5) -0.1222(3) 0.0526(17) Uiso 1 1 d . . . O13B O -0.1940(4) -0.0661(4) -0.1628(3) 0.0816(17) Uiso 1 1 d . . . C14B C -0.1652(5) 0.1313(5) -0.0677(3) 0.061(2) Uiso 1 1 d . . . O14B O -0.2133(4) 0.1780(4) -0.0877(3) 0.0854(18) Uiso 1 1 d . . . C15B C -0.2050(5) 0.0507(5) 0.0506(3) 0.0534(17) Uiso 1 1 d . . . O15B O -0.2652(4) 0.0603(4) 0.0729(3) 0.0832(18) Uiso 1 1 d . . . C48B C 0.0288(4) 0.1924(4) -0.0487(3) 0.0469(16) Uiso 1 1 d . . . O48B O 0.0407(4) 0.2591(4) -0.0667(3) 0.0743(16) Uiso 1 1 d . . . C59B C -0.0420(4) 0.0842(4) 0.1276(3) 0.0468(16) Uiso 1 1 d . . . O59B O -0.0586(4) 0.1146(4) 0.1708(2) 0.0716(15) Uiso 1 1 d . . . P1 P 0.50671(10) 0.10047(10) 0.24419(7) 0.0381(4) Uani 1 1 d . . . P2 P 0.50590(10) -0.07599(10) 0.21125(7) 0.0403(4) Uani 1 1 d . . . N1 N 0.4935(3) 0.0201(3) 0.2061(2) 0.0451(13) Uiso 1 1 d . . . C111 C 0.6153(4) 0.1259(4) 0.2565(3) 0.0433(15) Uiso 1 1 d . . . C112 C 0.6503(5) 0.1614(5) 0.3061(3) 0.0590(19) Uiso 1 1 d . . . H112 H 0.6177 0.1729 0.3354 0.071 Uiso 1 1 calc R . . C113 C 0.7347(6) 0.1799(6) 0.3118(4) 0.075(2) Uiso 1 1 d . . . H113 H 0.7583 0.2037 0.3451 0.090 Uiso 1 1 calc R . . C114 C 0.7829(6) 0.1632(5) 0.2688(4) 0.072(2) Uiso 1 1 d . . . H114 H 0.8394 0.1745 0.2733 0.086 Uiso 1 1 calc R . . C115 C 0.7482(5) 0.1295(5) 0.2186(4) 0.069(2) Uiso 1 1 d . . . H115 H 0.7808 0.1198 0.1890 0.083 Uiso 1 1 calc R . . C116 C 0.6650(5) 0.1106(5) 0.2129(3) 0.0573(19) Uiso 1 1 d . . . H116 H 0.6418 0.0872 0.1794 0.069 Uiso 1 1 calc R . . C121 C 0.4601(4) 0.0979(4) 0.3100(3) 0.0427(15) Uiso 1 1 d . . . C122 C 0.3861(5) 0.1378(5) 0.3163(3) 0.062(2) Uiso 1 1 d . . . H122 H 0.3613 0.1680 0.2870 0.074 Uiso 1 1 calc R . . C123 C 0.3487(6) 0.1329(6) 0.3663(4) 0.080(3) Uiso 1 1 d . . . H123 H 0.2994 0.1606 0.3706 0.096 Uiso 1 1 calc R . . C124 C 0.3842(6) 0.0877(6) 0.4092(4) 0.079(3) Uiso 1 1 d . . . H124 H 0.3590 0.0843 0.4426 0.095 Uiso 1 1 calc R . . C125 C 0.4576(5) 0.0469(5) 0.4032(4) 0.070(2) Uiso 1 1 d . . . H125 H 0.4816 0.0159 0.4324 0.084 Uiso 1 1 calc R . . C126 C 0.4953(5) 0.0519(5) 0.3539(3) 0.0559(18) Uiso 1 1 d . . . H126 H 0.5448 0.0244 0.3501 0.067 Uiso 1 1 calc R . . C131 C 0.4570(4) 0.1847(4) 0.2072(3) 0.0397(14) Uiso 1 1 d . . . C132 C 0.4732(5) 0.2647(5) 0.2252(3) 0.0555(18) Uiso 1 1 d . . . H132 H 0.5133 0.2752 0.2547 0.067 Uiso 1 1 calc R . . C133 C 0.4306(5) 0.3292(5) 0.2000(4) 0.067(2) Uiso 1 1 d . . . H133 H 0.4420 0.3828 0.2124 0.080 Uiso 1 1 calc R . . C134 C 0.3720(5) 0.3141(5) 0.1568(4) 0.069(2) Uiso 1 1 d . . . H134 H 0.3429 0.3578 0.1404 0.083 Uiso 1 1 calc R . . C135 C 0.3547(5) 0.2354(5) 0.1370(4) 0.065(2) Uiso 1 1 d . . . H135 H 0.3152 0.2258 0.1071 0.078 Uiso 1 1 calc R . . C136 C 0.3981(4) 0.1703(5) 0.1628(3) 0.0530(17) Uiso 1 1 d . . . H136 H 0.3871 0.1168 0.1501 0.064 Uiso 1 1 calc R . . C211 C 0.5324(4) -0.1152(4) 0.1442(3) 0.0444(15) Uiso 1 1 d . . . C212 C 0.5519(5) -0.0628(5) 0.1034(3) 0.066(2) Uiso 1 1 d . . . H212 H 0.5474 -0.0063 0.1087 0.079 Uiso 1 1 calc R . . C213 C 0.5792(6) -0.0961(7) 0.0525(4) 0.089(3) Uiso 1 1 d . . . H213 H 0.5921 -0.0620 0.0238 0.107 Uiso 1 1 calc R . . C214 C 0.5861(6) -0.1796(6) 0.0469(4) 0.079(3) Uiso 1 1 d . . . H214 H 0.6066 -0.2013 0.0147 0.095 Uiso 1 1 calc R . . C215 C 0.5649(6) -0.2305(6) 0.0852(4) 0.074(2) Uiso 1 1 d . . . H215 H 0.5682 -0.2869 0.0789 0.089 Uiso 1 1 calc R . . C216 C 0.5377(5) -0.1999(5) 0.1347(3) 0.061(2) Uiso 1 1 d . . . H216 H 0.5229 -0.2359 0.1618 0.073 Uiso 1 1 calc R . . C221 C 0.4117(4) -0.1249(4) 0.2287(3) 0.0484(16) Uiso 1 1 d . . . C222 C 0.4106(6) -0.2038(6) 0.2486(4) 0.082(3) Uiso 1 1 d . . . H222 H 0.4597 -0.2331 0.2538 0.098 Uiso 1 1 calc R . . C223 C 0.3346(8) -0.2403(8) 0.2612(5) 0.107(4) Uiso 1 1 d . . . H223 H 0.3332 -0.2924 0.2762 0.128 Uiso 1 1 calc R . . C224 C 0.2640(7) -0.1959(7) 0.2504(4) 0.095(3) Uiso 1 1 d . . . H224 H 0.2136 -0.2188 0.2578 0.114 Uiso 1 1 calc R . . C225 C 0.2644(7) -0.1200(7) 0.2292(4) 0.088(3) Uiso 1 1 d . . . H225 H 0.2148 -0.0924 0.2215 0.106 Uiso 1 1 calc R . . C226 C 0.3388(5) -0.0828(6) 0.2190(4) 0.070(2) Uiso 1 1 d . . . H226 H 0.3391 -0.0296 0.2057 0.084 Uiso 1 1 calc R . . C231 C 0.5911(4) -0.1073(4) 0.2603(3) 0.0467(16) Uiso 1 1 d . . . C232 C 0.6705(5) -0.0985(5) 0.2447(4) 0.066(2) Uiso 1 1 d . . . H232 H 0.6787 -0.0801 0.2090 0.080 Uiso 1 1 calc R . . C233 C 0.7389(7) -0.1170(6) 0.2819(4) 0.086(3) Uiso 1 1 d . . . H233 H 0.7925 -0.1092 0.2719 0.104 Uiso 1 1 calc R . . C234 C 0.7250(7) -0.1473(6) 0.3338(5) 0.090(3) Uiso 1 1 d . . . H234 H 0.7698 -0.1618 0.3584 0.108 Uiso 1 1 calc R . . C235 C 0.6481(6) -0.1559(6) 0.3492(4) 0.085(3) Uiso 1 1 d . . . H235 H 0.6400 -0.1762 0.3843 0.102 Uiso 1 1 calc R . . C236 C 0.5799(5) -0.1350(5) 0.3130(4) 0.067(2) Uiso 1 1 d . . . H236 H 0.5268 -0.1397 0.3245 0.081 Uiso 1 1 calc R . . P3 P 0.97832(11) 0.58816(11) 0.25192(7) 0.0438(4) Uani 1 1 d . . . P4 P 0.95812(11) 0.41247(11) 0.28694(7) 0.0431(4) Uani 1 1 d . . . N2 N 0.9776(4) 0.5075(4) 0.2864(3) 0.0550(15) Uiso 1 1 d . . . C311 C 0.8766(4) 0.6262(4) 0.2308(3) 0.0491(16) Uiso 1 1 d . . . C312 C 0.8587(6) 0.6638(6) 0.1803(4) 0.080(3) Uiso 1 1 d . . . H312 H 0.8992 0.6698 0.1554 0.096 Uiso 1 1 calc R . . C313 C 0.7777(7) 0.6931(7) 0.1673(5) 0.101(3) Uiso 1 1 d . . . H313 H 0.7642 0.7180 0.1331 0.122 Uiso 1 1 calc R . . C314 C 0.7200(7) 0.6853(7) 0.2038(5) 0.098(3) Uiso 1 1 d . . . H314 H 0.6668 0.7046 0.1943 0.118 Uiso 1 1 calc R . . C315 C 0.7370(7) 0.6503(7) 0.2538(5) 0.095(3) Uiso 1 1 d . . . H315 H 0.6963 0.6464 0.2788 0.114 Uiso 1 1 calc R . . C316 C 0.8158(6) 0.6200(5) 0.2678(4) 0.072(2) Uiso 1 1 d . . . H316 H 0.8279 0.5954 0.3022 0.086 Uiso 1 1 calc R . . C321 C 1.0334(5) 0.5808(5) 0.1900(3) 0.0529(17) Uiso 1 1 d . . . C322 C 1.0864(6) 0.6421(6) 0.1757(4) 0.079(3) Uiso 1 1 d . . . H322 H 1.0962 0.6876 0.1994 0.095 Uiso 1 1 calc R . . C323 C 1.1253(7) 0.6359(7) 0.1256(5) 0.098(3) Uiso 1 1 d . . . H323 H 1.1602 0.6777 0.1159 0.118 Uiso 1 1 calc R . . C324 C 1.1121(7) 0.5688(7) 0.0913(5) 0.091(3) Uiso 1 1 d . . . H324 H 1.1382 0.5650 0.0583 0.109 Uiso 1 1 calc R . . C325 C 1.0614(7) 0.5076(7) 0.1045(5) 0.099(3) Uiso 1 1 d . . . H325 H 1.0541 0.4613 0.0812 0.118 Uiso 1 1 calc R . . C326 C 1.0198(6) 0.5138(6) 0.1533(4) 0.080(3) Uiso 1 1 d . . . H326 H 0.9828 0.4729 0.1613 0.096 Uiso 1 1 calc R . . C331 C 1.0308(4) 0.6651(4) 0.2984(3) 0.0512(17) Uiso 1 1 d . . . C332 C 1.0131(5) 0.7472(5) 0.2925(4) 0.068(2) Uiso 1 1 d . . . H332 H 0.9716 0.7648 0.2663 0.082 Uiso 1 1 calc R . . C333 C 1.0604(7) 0.8042(7) 0.3277(4) 0.092(3) Uiso 1 1 d . . . H333 H 1.0504 0.8602 0.3251 0.110 Uiso 1 1 calc R . . C334 C 1.1196(7) 0.7759(7) 0.3645(5) 0.094(3) Uiso 1 1 d . . . H334 H 1.1517 0.8141 0.3860 0.113 Uiso 1 1 calc R . . C335 C 1.1356(7) 0.6973(7) 0.3724(5) 0.093(3) Uiso 1 1 d . . . H335 H 1.1759 0.6811 0.3999 0.111 Uiso 1 1 calc R . . C336 C 1.0901(6) 0.6386(6) 0.3380(4) 0.075(2) Uiso 1 1 d . . . H336 H 1.1002 0.5829 0.3423 0.090 Uiso 1 1 calc R . . C411 C 0.8617(4) 0.3836(4) 0.2474(3) 0.0488(16) Uiso 1 1 d . . . C412 C 0.8569(6) 0.3521(5) 0.1928(4) 0.069(2) Uiso 1 1 d . . . H412 H 0.9048 0.3411 0.1752 0.083 Uiso 1 1 calc R . . C413 C 0.7789(7) 0.3373(7) 0.1646(5) 0.092(3) Uiso 1 1 d . . . H413 H 0.7750 0.3148 0.1284 0.111 Uiso 1 1 calc R . . C414 C 0.7091(7) 0.3553(7) 0.1894(5) 0.093(3) Uiso 1 1 d . . . H414 H 0.6579 0.3464 0.1697 0.111 Uiso 1 1 calc R . . C415 C 0.7127(6) 0.3864(6) 0.2431(4) 0.085(3) Uiso 1 1 d . . . H415 H 0.6643 0.3982 0.2600 0.102 Uiso 1 1 calc R . . C416 C 0.7899(5) 0.4000(5) 0.2722(4) 0.065(2) Uiso 1 1 d . . . H416 H 0.7928 0.4204 0.3089 0.079 Uiso 1 1 calc R . . C421 C 1.0424(4) 0.3530(4) 0.2630(3) 0.0515(17) Uiso 1 1 d . . . C422 C 1.1199(5) 0.3911(6) 0.2641(4) 0.068(2) Uiso 1 1 d . . . H422 H 1.1263 0.4457 0.2758 0.081 Uiso 1 1 calc R . . C423 C 1.1875(6) 0.3468(6) 0.2476(4) 0.082(3) Uiso 1 1 d . . . H423 H 1.2390 0.3721 0.2476 0.098 Uiso 1 1 calc R . . C424 C 1.1781(7) 0.2657(6) 0.2313(4) 0.088(3) Uiso 1 1 d . . . H424 H 1.2236 0.2363 0.2207 0.105 Uiso 1 1 calc R . . C425 C 1.1033(6) 0.2279(7) 0.2303(4) 0.087(3) Uiso 1 1 d . . . H425 H 1.0978 0.1730 0.2193 0.105 Uiso 1 1 calc R . . C426 C 1.0347(6) 0.2715(6) 0.2459(4) 0.073(2) Uiso 1 1 d . . . H426 H 0.9834 0.2456 0.2449 0.088 Uiso 1 1 calc R . . C431 C 0.9458(4) 0.3869(4) 0.3584(3) 0.0463(16) Uiso 1 1 d . . . C432 C 0.9381(5) 0.3054(5) 0.3732(3) 0.063(2) Uiso 1 1 d . . . H432 H 0.9433 0.2639 0.3466 0.075 Uiso 1 1 calc R . . C433 C 0.9224(6) 0.2855(6) 0.4278(4) 0.080(3) Uiso 1 1 d . . . H433 H 0.9165 0.2311 0.4377 0.096 Uiso 1 1 calc R . . C434 C 0.9160(6) 0.3464(6) 0.4656(4) 0.085(3) Uiso 1 1 d . . . H434 H 0.9055 0.3328 0.5018 0.102 Uiso 1 1 calc R . . C435 C 0.9239(6) 0.4263(7) 0.4540(4) 0.086(3) Uiso 1 1 d . . . H435 H 0.9192 0.4665 0.4817 0.103 Uiso 1 1 calc R . . C436 C 0.9395(5) 0.4478(6) 0.3991(4) 0.069(2) Uiso 1 1 d . . . H436 H 0.9454 0.5027 0.3902 0.083 Uiso 1 1 calc R . . P5 P 0.07613(11) 0.04038(11) 0.47637(8) 0.0483(4) Uani 1 1 d . . . N3 N 0.0000 0.0000 0.5000 0.083(3) Uiso 1 2 d S . . C511 C 0.0875(4) 0.1479(4) 0.4952(3) 0.0495(16) Uiso 1 1 d . . . C512 C 0.0686(5) 0.1746(6) 0.5475(4) 0.070(2) Uiso 1 1 d . . . H512 H 0.0461 0.1385 0.5716 0.085 Uiso 1 1 calc R . . C513 C 0.0836(6) 0.2570(6) 0.5642(4) 0.085(3) Uiso 1 1 d . . . H513 H 0.0706 0.2761 0.5993 0.102 Uiso 1 1 calc R . . C514 C 0.1172(6) 0.3078(6) 0.5285(4) 0.082(3) Uiso 1 1 d . . . H514 H 0.1282 0.3618 0.5403 0.099 Uiso 1 1 calc R . . C515 C 0.1354(6) 0.2844(6) 0.4772(4) 0.081(3) Uiso 1 1 d . . . H515 H 0.1573 0.3217 0.4535 0.097 Uiso 1 1 calc R . . C516 C 0.1208(5) 0.2020(5) 0.4593(4) 0.066(2) Uiso 1 1 d . . . H516 H 0.1333 0.1843 0.4239 0.080 Uiso 1 1 calc R . . C521 C 0.1708(4) -0.0091(4) 0.5022(3) 0.0467(16) Uiso 1 1 d . . . C522 C 0.2405(5) 0.0349(5) 0.5217(3) 0.0601(19) Uiso 1 1 d . . . H522 H 0.2395 0.0919 0.5227 0.072 Uiso 1 1 calc R . . C523 C 0.3123(6) -0.0069(6) 0.5400(4) 0.078(3) Uiso 1 1 d . . . H523 H 0.3598 0.0222 0.5528 0.094 Uiso 1 1 calc R . . C524 C 0.3129(6) -0.0911(6) 0.5390(4) 0.085(3) Uiso 1 1 d . . . H524 H 0.3612 -0.1187 0.5509 0.102 Uiso 1 1 calc R . . C525 C 0.2443(6) -0.1345(6) 0.5208(4) 0.082(3) Uiso 1 1 d . . . H525 H 0.2454 -0.1915 0.5211 0.098 Uiso 1 1 calc R . . C526 C 0.1726(5) -0.0947(5) 0.5017(4) 0.067(2) Uiso 1 1 d . . . H526 H 0.1258 -0.1247 0.4886 0.081 Uiso 1 1 calc R . . C531 C 0.0681(5) 0.0332(5) 0.4006(3) 0.0595(19) Uiso 1 1 d . . . C532 C 0.1385(6) 0.0260(6) 0.3723(4) 0.078(3) Uiso 1 1 d . . . H532 H 0.1899 0.0199 0.3922 0.094 Uiso 1 1 calc R . . C533 C 0.1330(8) 0.0279(7) 0.3129(5) 0.106(4) Uiso 1 1 d . . . H533 H 0.1801 0.0251 0.2934 0.127 Uiso 1 1 calc R . . C534 C 0.0568(8) 0.0339(7) 0.2858(5) 0.106(4) Uiso 1 1 d . . . H534 H 0.0528 0.0346 0.2468 0.127 Uiso 1 1 calc R . . C535 C -0.0111(8) 0.0389(8) 0.3108(5) 0.113(4) Uiso 1 1 d . . . H535 H -0.0616 0.0426 0.2895 0.135 Uiso 1 1 calc R . . C536 C -0.0091(7) 0.0387(6) 0.3714(4) 0.088(3) Uiso 1 1 d . . . H536 H -0.0574 0.0420 0.3897 0.106 Uiso 1 1 calc R . . P6 P 0.42372(12) 0.54492(10) 0.02104(7) 0.0447(4) Uani 1 1 d . . . N4 N 0.5000 0.5000 0.0000 0.078(3) Uiso 1 2 d S . . C611 C 0.3276(4) 0.4950(4) -0.0018(3) 0.0501(17) Uiso 1 1 d . . . C612 C 0.3157(6) 0.4128(6) 0.0107(4) 0.081(3) Uiso 1 1 d . . . H612 H 0.3573 0.3834 0.0305 0.097 Uiso 1 1 calc R . . C613 C 0.2399(7) 0.3755(8) -0.0073(5) 0.101(3) Uiso 1 1 d . . . H613 H 0.2325 0.3203 0.0000 0.121 Uiso 1 1 calc R . . C614 C 0.1782(7) 0.4161(7) -0.0344(5) 0.096(3) Uiso 1 1 d . . . H614 H 0.1282 0.3895 -0.0446 0.115 Uiso 1 1 calc R . . C615 C 0.1877(7) 0.4971(7) -0.0472(4) 0.090(3) Uiso 1 1 d . . . H615 H 0.1448 0.5258 -0.0663 0.109 Uiso 1 1 calc R . . C616 C 0.2638(6) 0.5355(6) -0.0309(4) 0.074(2) Uiso 1 1 d . . . H616 H 0.2713 0.5900 -0.0400 0.089 Uiso 1 1 calc R . . C621 C 0.4163(4) 0.6479(4) -0.0046(3) 0.0424(15) Uiso 1 1 d . . . C622 C 0.3733(5) 0.7091(5) 0.0222(3) 0.0563(18) Uiso 1 1 d . . . H622 H 0.3497 0.6981 0.0553 0.068 Uiso 1 1 calc R . . C623 C 0.3659(5) 0.7861(5) -0.0006(4) 0.068(2) Uiso 1 1 d . . . H623 H 0.3370 0.8268 0.0172 0.082 Uiso 1 1 calc R . . C624 C 0.4008(5) 0.8029(6) -0.0492(4) 0.068(2) Uiso 1 1 d . . . H624 H 0.3951 0.8549 -0.0643 0.082 Uiso 1 1 calc R . . C625 C 0.4438(5) 0.7444(5) -0.0757(4) 0.066(2) Uiso 1 1 d . . . H625 H 0.4679 0.7564 -0.1085 0.079 Uiso 1 1 calc R . . C626 C 0.4517(4) 0.6666(5) -0.0535(3) 0.0527(17) Uiso 1 1 d . . . H626 H 0.4810 0.6265 -0.0716 0.063 Uiso 1 1 calc R . . C631 C 0.4310(4) 0.5497(4) 0.0969(3) 0.0462(16) Uiso 1 1 d . . . C632 C 0.5081(5) 0.5503(5) 0.1265(4) 0.067(2) Uiso 1 1 d . . . H632 H 0.5559 0.5468 0.1076 0.080 Uiso 1 1 calc R . . C633 C 0.5139(6) 0.5564(6) 0.1855(4) 0.084(3) Uiso 1 1 d . . . H633 H 0.5653 0.5559 0.2059 0.101 Uiso 1 1 calc R . . C634 C 0.4453(6) 0.5628(6) 0.2118(4) 0.086(3) Uiso 1 1 d . . . H634 H 0.4502 0.5690 0.2506 0.103 Uiso 1 1 calc R . . C635 C 0.3689(7) 0.5607(6) 0.1850(4) 0.089(3) Uiso 1 1 d . . . H635 H 0.3224 0.5632 0.2052 0.107 Uiso 1 1 calc R . . C636 C 0.3604(5) 0.5547(5) 0.1256(4) 0.066(2) Uiso 1 1 d . . . H636 H 0.3082 0.5541 0.1062 0.079 Uiso 1 1 calc R . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Rh1A 0.0628(4) 0.0290(3) 0.0629(4) 0.0083(2) -0.0082(3) 0.0017(2) Rh2A 0.0364(5) 0.0338(5) 0.0348(5) 0.0008(4) -0.0011(4) 0.0047(4) Rh3A 0.0456(6) 0.0394(5) 0.0338(5) 0.0025(4) 0.0099(4) -0.0014(4) Rh4A 0.0376(5) 0.0335(5) 0.0368(5) 0.0007(4) -0.0003(4) -0.0011(4) Rh5A 0.0388(5) 0.0327(5) 0.0371(5) -0.0020(4) 0.0048(4) 0.0057(4) Rh6A 0.0367(5) 0.0353(5) 0.0385(5) 0.0023(4) 0.0076(4) -0.0006(4) Rh7A 0.0405(5) 0.0306(5) 0.0337(5) -0.0036(4) 0.0015(4) 0.0038(4) Rh8A 0.0330(5) 0.0365(5) 0.0436(6) -0.0036(4) 0.0050(4) 0.0050(4) Rh9A 0.0418(5) 0.0351(5) 0.0309(5) 0.0039(4) 0.0023(4) 0.0037(4) PA 0.0350(11) 0.0378(12) 0.0295(11) -0.0018(9) 0.0043(9) 0.0014(9) Rh1B 0.0381(3) 0.0514(3) 0.0941(5) 0.0166(3) 0.0157(3) 0.0018(3) Rh2B 0.0419(5) 0.0312(5) 0.0414(5) 0.0016(4) 0.0057(4) -0.0051(4) Rh3B 0.0422(5) 0.0353(5) 0.0314(5) 0.0011(4) 0.0055(4) -0.0006(4) Rh4B 0.0392(5) 0.0319(5) 0.0408(5) 0.0011(4) 0.0070(4) 0.0010(4) Rh5B 0.0356(5) 0.0380(5) 0.0385(5) 0.0032(4) 0.0089(4) 0.0007(4) Rh6B 0.0369(5) 0.0333(5) 0.0336(5) 0.0040(4) 0.0075(4) -0.0002(4) Rh7B 0.0400(5) 0.0318(5) 0.0337(5) -0.0022(4) 0.0072(4) 0.0014(4) Rh8B 0.0407(5) 0.0331(5) 0.0348(5) 0.0035(4) 0.0102(4) -0.0027(4) Rh9B 0.0374(5) 0.0349(5) 0.0364(5) -0.0017(4) 0.0075(4) -0.0010(4) PB 0.0524(14) 0.0295(11) 0.0404(13) 0.0032(9) 0.0173(11) -0.0006(10) P1 0.0399(9) 0.0309(8) 0.0439(9) 0.0007(7) 0.0066(7) -0.0008(7) P2 0.0424(9) 0.0316(8) 0.0474(10) -0.0013(7) 0.0074(7) -0.0013(7) P3 0.0488(10) 0.0383(9) 0.0445(10) 0.0022(7) 0.0041(8) -0.0042(7) P4 0.0457(10) 0.0401(9) 0.0440(9) 0.0024(7) 0.0067(8) -0.0019(7) P5 0.0414(10) 0.0414(10) 0.0631(12) 0.0013(8) 0.0100(8) -0.0046(7) P6 0.0588(11) 0.0335(9) 0.0439(9) 0.0059(7) 0.0151(8) 0.0124(8) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Rh1A C1A 1.835(6) . ? Rh1A C12A 2.099(8) . ? Rh1A C13A 2.223(8) . ? Rh1A C14A 2.251(8) . ? Rh1A C15A 2.252(7) . ? Rh1A Rh4A 2.8381(11) . y Rh1A Rh3A 2.8399(12) . y Rh1A Rh2A 2.8962(11) . y Rh1A Rh5A 2.9021(12) . y Rh2A C2A 1.823(7) . ? Rh2A C48A 1.964(7) 2_666 ? Rh2A C12A 2.017(8) . ? Rh2A C2A' 2.085(13) . ? Rh2A Rh4A 2.3540(13) 2_666 ? Rh2A PA 2.4894(9) . y Rh2A Rh6A 2.8376(13) . y Rh2A Rh7A 2.8646(13) . y Rh2A Rh3A 3.0109(14) . y Rh2A Rh5A 3.0907(14) . y Rh3A C3A 1.869(8) . ? Rh3A C13A 1.927(8) . ? Rh3A C59A 2.004(7) 2_666 ? Rh3A Rh5A 2.3081(14) 2_666 ? Rh3A C3A' 2.329(14) . ? Rh3A PA 2.4341(9) . y Rh3A Rh7A 2.8552(14) . y Rh3A Rh8A 2.8783(14) . y Rh3A Rh4A 2.9888(14) . y Rh4A C4A 1.846(7) . ? Rh4A C14A 1.973(8) . ? Rh4A C48A 2.044(7) . ? Rh4A C4A' 2.261(15) . ? Rh4A Rh2A 2.3540(13) 2_666 ? Rh4A PA 2.4284(9) . y Rh4A Rh8A 2.8501(14) . y Rh4A Rh9A 2.8891(14) . y Rh4A Rh5A 3.0866(14) . y Rh5A C5A 1.824(7) . ? Rh5A C15A 1.982(7) . ? Rh5A C59A 2.023(7) . ? Rh5A C5A' 2.047(12) . ? Rh5A Rh3A 2.3081(14) 2_666 ? Rh5A PA 2.4383(9) . y Rh5A Rh9A 2.8057(13) . y Rh5A Rh6A 2.8985(14) . y Rh6A Rh4A 1.4857(14) 2_666 ? Rh6A Rh3A 1.8009(14) 2_666 ? Rh6A C3A' 1.825(7) 2_666 ? Rh6A C14A 1.957(8) 2_666 ? Rh6A C48A 2.002(7) 2_666 ? Rh6A C3A 2.155(15) 2_666 ? Rh6A Rh8A 2.3791(14) 2_666 ? Rh6A PA 2.4919(9) . y Rh6A Rh1A 2.8976(11) 2_666 y Rh6A Rh7A 2.9972(13) . y Rh7A Rh5A 1.6750(14) 2_666 ? Rh7A Rh4A 1.6967(14) 2_666 ? Rh7A C4A' 1.838(8) 2_666 ? Rh7A C15A 1.958(7) 2_666 ? Rh7A C59A 2.046(7) 2_666 ? Rh7A C4A 2.122(13) 2_666 ? Rh7A Rh9A 2.3330(13) 2_666 ? Rh7A PA 2.4640(9) . y Rh7A Rh1A 2.8712(11) 2_666 y Rh7A Rh8A 2.9831(14) . y Rh8A Rh5A 1.5869(14) 2_666 ? Rh8A Rh2A 1.6874(14) 2_666 ? Rh8A C5A' 1.869(7) 2_666 ? Rh8A C12A 1.979(8) 2_666 ? Rh8A C48A 2.075(7) . ? Rh8A C5A 2.286(13) 2_666 ? Rh8A Rh6A 2.3791(14) 2_666 ? Rh8A PA 2.3958(9) . y Rh8A Rh1A 2.7887(12) 2_666 y Rh9A Rh3A 1.5685(14) 2_666 ? Rh9A Rh2A 1.6486(14) 2_666 ? Rh9A C2A' 1.881(7) 2_666 ? Rh9A C13A 1.974(8) 2_666 ? Rh9A C59A 2.007(7) . ? Rh9A C2A 2.306(12) 2_666 ? Rh9A Rh7A 2.3330(13) 2_666 ? Rh9A PA 2.4126(9) . y Rh9A Rh1A 2.8481(11) 2_666 y PA Rh8A 2.3958(9) 2_666 ? PA Rh9A 2.4126(9) 2_666 ? PA Rh4A 2.4284(10) 2_666 ? PA Rh3A 2.4341(9) 2_666 ? PA Rh5A 2.4383(9) 2_666 ? PA Rh7A 2.4640(9) 2_666 ? C1A O1A 1.189(6) . ? C2A C2A' 0.853(16) . ? C2A O2A 1.160(7) . ? C2A Rh9A 2.306(12) 2_666 ? C2A' O2A 1.234(7) . ? C2A' Rh9A 1.881(7) 2_666 ? C3A C3A' 0.902(18) . ? C3A O3A 1.231(8) . ? C3A Rh6A 2.155(15) 2_666 ? C3A' O3A 1.167(7) . ? C3A' Rh6A 1.825(7) 2_666 ? C4A C4A' 0.839(18) . ? C4A O4A 1.199(7) . ? C4A Rh7A 2.122(13) 2_666 ? C4A' O4A 1.194(8) . ? C4A' Rh7A 1.838(8) 2_666 ? C5A C5A' 0.824(17) . ? C5A O5A 1.158(7) . ? C5A Rh8A 2.286(13) 2_666 ? C5A' O5A 1.225(7) . ? C5A' Rh8A 1.869(7) 2_666 ? C12A O12A 1.185(10) . ? C12A Rh8A 1.979(8) 2_666 ? C13A O13A 1.167(10) . ? C13A Rh9A 1.974(8) 2_666 ? C14A O14A 1.178(9) . ? C14A Rh6A 1.957(8) 2_666 ? C15A O15A 1.161(9) . ? C15A Rh7A 1.958(7) 2_666 ? C48A O48A 1.199(8) . ? C48A Rh2A 1.964(7) 2_666 ? C48A Rh6A 2.002(7) 2_666 ? C59A O59A 1.194(8) . ? C59A Rh3A 2.004(7) 2_666 ? C59A Rh7A 2.046(7) 2_666 ? Rh1B C1B 1.840(6) . ? Rh1B C12B 2.090(8) . ? Rh1B C13B 2.263(7) . ? Rh1B C14B 2.266(8) . ? Rh1B C15B 2.306(8) . ? Rh1B Rh3B 2.8608(11) . y Rh1B Rh2B 2.9026(12) . y Rh1B Rh4B 2.9646(12) . y Rh1B Rh5B 3.0124(12) . y Rh2B C2B 1.842(8) . ? Rh2B C48B 1.928(7) 2 ? Rh2B C12B 2.071(8) . ? Rh2B Rh4B 2.1332(14) 2 ? Rh2B C2B' 2.211(13) . ? Rh2B PB 2.3783(9) . y Rh2B Rh6B 2.8450(14) . y Rh2B Rh7B 2.8635(14) . y Rh2B Rh3B 2.9688(13) . y Rh2B Rh5B 3.0999(14) . y Rh3B C3B 1.883(7) . ? Rh3B C13B 2.042(8) . ? Rh3B C59B 2.049(7) 2 ? Rh3B Rh5B 2.1399(14) 2 ? Rh3B C3B' 2.360(14) . ? Rh3B PB 2.3768(9) . y Rh3B Rh8B 2.8755(14) . y Rh3B Rh7B 2.8795(14) . y Rh3B Rh4B 3.0283(13) . y Rh4B C4B 1.825(8) . ? Rh4B C48B 2.009(7) . ? Rh4B C14B 2.049(8) . ? Rh4B C4B' 2.109(14) . ? Rh4B Rh2B 2.1332(14) 2 ? Rh4B PB 2.4307(9) . y Rh4B Rh8B 2.8464(14) . y Rh4B Rh9B 2.8930(14) . y Rh4B Rh5B 3.1151(13) . y Rh5B C5B 1.846(8) . ? Rh5B C59B 1.915(7) . ? Rh5B C15B 2.045(8) . ? Rh5B Rh3B 2.1399(14) 2 ? Rh5B C5B' 2.209(13) . ? Rh5B PB 2.4468(9) . y Rh5B Rh9B 2.8035(14) . y Rh5B Rh6B 2.8857(13) . y Rh6B Rh4B 1.6243(14) 2 ? Rh6B Rh3B 1.7035(13) 2 ? Rh6B C3B' 1.811(8) 2 ? Rh6B C14B 1.896(8) 2 ? Rh6B C3B 1.991(14) 2 ? Rh6B C48B 2.110(7) 2 ? Rh6B PB 2.5264(9) . y Rh6B Rh8B 2.5449(14) 2 ? Rh6B Rh1B 2.8255(11) 2 y Rh6B Rh7B 3.0151(13) . y Rh7B Rh5B 1.6492(13) 2 ? Rh7B Rh4B 1.6919(13) 2 ? Rh7B C4B' 1.863(7) 2 ? Rh7B C15B 1.901(8) 2 ? Rh7B C59B 2.099(7) 2 ? Rh7B C4B 2.335(14) 2 ? Rh7B PB 2.4743(9) . y Rh7B Rh9B 2.5462(14) 2 ? Rh7B Rh1B 2.7572(12) 2 y Rh7B Rh8B 2.9512(13) . y Rh8B Rh2B 1.6434(14) 2 ? Rh8B Rh5B 1.6842(14) 2 ? Rh8B C5B' 1.863(8) 2 ? Rh8B C12B 1.919(8) 2 ? Rh8B C48B 2.039(7) . ? Rh8B C5B 2.373(13) 2 ? Rh8B PB 2.4424(9) . y Rh8B Rh6B 2.5449(14) 2 ? Rh8B Rh1B 2.7398(12) 2 y Rh9B Rh3B 1.6062(13) 2 ? Rh9B Rh2B 1.6901(14) 2 ? Rh9B C2B' 1.854(7) 2 ? Rh9B C13B 1.928(7) 2 ? Rh9B C59B 2.037(7) . ? Rh9B C2B 2.264(14) 2 ? Rh9B PB 2.5325(10) . y Rh9B Rh7B 2.5462(14) 2 ? Rh9B Rh1B 2.8391(11) 2 y PB Rh3B 2.3768(9) 2 ? PB Rh2B 2.3783(9) 2 ? PB Rh4B 2.4307(9) 2 ? PB Rh8B 2.4424(9) 2 ? PB Rh5B 2.4468(9) 2 ? PB Rh7B 2.4743(9) 2 ? C1B O1B 1.169(6) . ? C2B' C2B 0.952(18) . ? C2B' O2B 1.216(8) . ? C2B' Rh9B 1.854(7) 2 ? C2B O2B 1.200(8) . ? C2B Rh9B 2.264(14) 2 ? C3B' C3B 0.820(18) . ? C3B' O3B 1.143(8) . ? C3B' Rh6B 1.811(8) 2 ? C3B O3B 1.246(7) . ? C3B Rh6B 1.991(14) 2 ? C4B' C4B 0.922(19) . ? C4B' O4B 1.229(8) . ? C4B' Rh7B 1.863(7) 2 ? C4B O4B 1.182(8) . ? C4B Rh7B 2.335(14) 2 ? C5B C5B' 1.112(19) . ? C5B O5B 1.212(8) . ? C5B Rh8B 2.373(13) 2 ? C5B' O5B 1.234(8) . ? C5B' Rh8B 1.863(8) 2 ? C12B O12B 1.188(9) . ? C12B Rh8B 1.919(8) 2 ? C13B O13B 1.158(9) . ? C13B Rh9B 1.928(7) 2 ? C14B O14B 1.171(9) . ? C14B Rh6B 1.896(8) 2 ? C15B O15B 1.159(9) . ? C15B Rh7B 1.901(8) 2 ? C48B O48B 1.199(8) . ? C48B Rh2B 1.928(7) 2 ? C48B Rh6B 2.110(7) 2 ? C59B O59B 1.190(8) . ? C59B Rh3B 2.049(7) 2 ? C59B Rh7B 2.099(7) 2 ? P1 N1 1.584(6) . ? P1 C131 1.804(6) . ? P1 C121 1.806(7) . ? P1 C111 1.806(7) . ? P2 N1 1.586(6) . ? P2 C211 1.800(7) . ? P2 C221 1.806(7) . ? P2 C231 1.816(7) . ? C111 C112 1.387(10) . ? C111 C116 1.390(10) . ? C112 C113 1.395(11) . ? C113 C114 1.367(12) . ? C114 C115 1.385(12) . ? C115 C116 1.378(11) . ? C121 C122 1.383(10) . ? C121 C126 1.388(10) . ? C122 C123 1.391(12) . ? C123 C124 1.365(13) . ? C124 C125 1.380(12) . ? C125 C126 1.377(11) . ? C131 C136 1.382(9) . ? C131 C132 1.384(9) . ? C132 C133 1.380(11) . ? C133 C134 1.362(11) . ? C134 C135 1.378(11) . ? C135 C136 1.400(11) . ? C211 C212 1.369(10) . ? C211 C216 1.400(10) . ? C212 C213 1.428(13) . ? C213 C214 1.371(13) . ? C214 C215 1.316(12) . ? C215 C216 1.382(11) . ? C221 C226 1.373(11) . ? C221 C222 1.381(11) . ? C222 C223 1.425(14) . ? C223 C224 1.365(15) . ? C224 C225 1.346(14) . ? C225 C226 1.392(13) . ? C231 C236 1.375(10) . ? C231 C232 1.380(10) . ? C232 C233 1.399(12) . ? C233 C234 1.383(13) . ? C234 C235 1.338(13) . ? C235 C236 1.391(12) . ? P3 N2 1.567(6) . ? P3 C321 1.797(8) . ? P3 C311 1.797(7) . ? P3 C331 1.820(7) . ? P4 N2 1.582(6) . ? P4 C431 1.798(7) . ? P4 C421 1.802(7) . ? P4 C411 1.813(7) . ? C311 C312 1.376(11) . ? C311 C316 1.384(11) . ? C312 C313 1.411(14) . ? C313 C314 1.341(14) . ? C314 C315 1.346(14) . ? C315 C316 1.387(13) . ? C321 C322 1.385(12) . ? C321 C326 1.391(12) . ? C322 C323 1.402(14) . ? C323 C324 1.360(14) . ? C324 C325 1.352(14) . ? C325 C326 1.399(14) . ? C331 C336 1.368(11) . ? C331 C332 1.378(11) . ? C332 C333 1.419(13) . ? C333 C334 1.336(14) . ? C334 C335 1.322(14) . ? C335 C336 1.414(13) . ? C411 C416 1.375(10) . ? C411 C412 1.390(11) . ? C412 C413 1.399(13) . ? C413 C414 1.351(14) . ? C414 C415 1.368(13) . ? C415 C416 1.394(12) . ? C421 C426 1.384(11) . ? C421 C422 1.398(11) . ? C422 C423 1.393(12) . ? C423 C424 1.376(13) . ? C424 C425 1.357(13) . ? C425 C426 1.393(13) . ? C431 C436 1.385(11) . ? C431 C432 1.391(10) . ? C432 C433 1.397(12) . ? C433 C434 1.339(13) . ? C434 C435 1.345(13) . ? C435 C436 1.413(12) . ? P5 N3 1.5520(17) . ? P5 C521 1.803(7) . ? P5 C511 1.807(7) . ? P5 C531 1.808(8) . ? N3 P5 1.5520(18) 2_556 ? C511 C512 1.375(11) . ? C511 C516 1.384(11) . ? C512 C513 1.408(13) . ? C513 C514 1.349(13) . ? C514 C515 1.337(13) . ? C515 C516 1.414(12) . ? C521 C522 1.379(10) . ? C521 C526 1.396(11) . ? C522 C523 1.393(12) . ? C523 C524 1.372(13) . ? C524 C525 1.353(13) . ? C525 C526 1.380(12) . ? C531 C532 1.380(12) . ? C531 C536 1.386(12) . ? C532 C533 1.416(14) . ? C533 C534 1.349(15) . ? C534 C535 1.299(15) . ? C535 C536 1.448(15) . ? P6 N4 1.5526(17) . ? P6 C611 1.795(7) . ? P6 C621 1.801(7) . ? P6 C631 1.809(7) . ? N4 P6 1.5526(17) 2_665 ? C611 C616 1.373(11) . ? C611 C612 1.396(12) . ? C612 C613 1.400(14) . ? C613 C614 1.331(14) . ? C614 C615 1.373(14) . ? C615 C616 1.405(13) . ? C621 C626 1.386(9) . ? C621 C622 1.392(10) . ? C622 C623 1.382(11) . ? C623 C624 1.370(11) . ? C624 C625 1.360(11) . ? C625 C626 1.389(11) . ? C631 C632 1.385(10) . ? C631 C636 1.385(10) . ? C632 C633 1.409(12) . ? C633 C634 1.326(13) . ? C634 C635 1.344(13) . ? C635 C636 1.419(13) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C1A Rh1A C12A 94.2(3) . . ? C1A Rh1A C13A 95.0(3) . . ? C12A Rh1A C13A 90.6(3) . . ? C1A Rh1A C14A 89.8(3) . . ? C12A Rh1A C14A 176.0(3) . . ? C13A Rh1A C14A 89.2(3) . . ? C1A Rh1A C15A 91.9(3) . . ? C12A Rh1A C15A 89.1(3) . . ? C13A Rh1A C15A 173.1(3) . . ? C14A Rh1A C15A 90.6(3) . . ? C1A Rh1A Rh4A 128.8(3) . . ? C12A Rh1A Rh4A 132.6(2) . . ? C13A Rh1A Rh4A 102.8(2) . . ? C14A Rh1A Rh4A 43.7(2) . . ? C15A Rh1A Rh4A 72.62(18) . . ? C1A Rh1A Rh3A 132.3(3) . . ? C12A Rh1A Rh3A 104.6(2) . . ? C13A Rh1A Rh3A 42.6(2) . . ? C14A Rh1A Rh3A 72.7(2) . . ? C15A Rh1A Rh3A 131.06(18) . . ? Rh4A Rh1A Rh3A 63.52(3) . . ? C1A Rh1A Rh2A 133.5(3) . . ? C12A Rh1A Rh2A 44.1(2) . . ? C13A Rh1A Rh2A 70.9(2) . . ? C14A Rh1A Rh2A 132.3(2) . . ? C15A Rh1A Rh2A 104.30(18) . . ? Rh4A Rh1A Rh2A 97.70(3) . . ? Rh3A Rh1A Rh2A 63.31(3) . . ? C1A Rh1A Rh5A 130.9(3) . . ? C12A Rh1A Rh5A 71.8(2) . . ? C13A Rh1A Rh5A 130.6(2) . . ? C14A Rh1A Rh5A 105.5(2) . . ? C15A Rh1A Rh5A 42.97(18) . . ? Rh4A Rh1A Rh5A 65.04(3) . . ? Rh3A Rh1A Rh5A 96.71(3) . . ? Rh2A Rh1A Rh5A 64.42(3) . . ? C2A Rh2A C48A 94.9(5) . 2_666 ? C2A Rh2A C12A 94.8(5) . . ? C48A Rh2A C12A 107.0(3) 2_666 . ? C2A Rh2A C2A' 24.0(5) . . ? C48A Rh2A C2A' 112.5(4) 2_666 . ? C12A Rh2A C2A' 104.0(4) . . ? C2A Rh2A Rh4A 107.9(4) . 2_666 ? C48A Rh2A Rh4A 55.6(2) 2_666 2_666 ? C12A Rh2A Rh4A 151.7(2) . 2_666 ? C2A' Rh2A Rh4A 103.5(4) . 2_666 ? C2A Rh2A PA 147.5(5) . . ? C48A Rh2A PA 100.1(2) 2_666 . ? C12A Rh2A PA 107.9(2) . . ? C2A' Rh2A PA 124.4(3) . . ? Rh4A Rh2A PA 60.11(3) 2_666 . ? C2A Rh2A Rh6A 130.8(5) . . ? C48A Rh2A Rh6A 44.9(2) 2_666 . ? C12A Rh2A Rh6A 120.2(2) . . ? C2A' Rh2A Rh6A 133.9(4) . . ? Rh4A Rh2A Rh6A 31.54(3) 2_666 . ? PA Rh2A Rh6A 55.31(3) . . ? C2A Rh2A Rh7A 97.3(5) . . ? C48A Rh2A Rh7A 90.4(2) 2_666 . ? C12A Rh2A Rh7A 157.8(2) . . ? C2A' Rh2A Rh7A 80.9(4) . . ? Rh4A Rh2A Rh7A 36.30(3) 2_666 . ? PA Rh2A Rh7A 54.25(3) . . ? Rh6A Rh2A Rh7A 63.42(3) . . ? C2A Rh2A Rh1A 116.6(5) . . ? C48A Rh2A Rh1A 137.5(2) 2_666 . ? C12A Rh2A Rh1A 46.5(2) . . ? C2A' Rh2A Rh1A 106.9(4) . . ? Rh4A Rh2A Rh1A 128.85(4) 2_666 . ? PA Rh2A Rh1A 68.81(3) . . ? Rh6A Rh2A Rh1A 112.64(4) . . ? Rh7A Rh2A Rh1A 111.38(4) . . ? C2A Rh2A Rh3A 102.3(5) . . ? C48A Rh2A Rh3A 145.5(2) 2_666 . ? C12A Rh2A Rh3A 101.2(2) . . ? C2A' Rh2A Rh3A 78.7(3) . . ? Rh4A Rh2A Rh3A 90.42(4) 2_666 . ? PA Rh2A Rh3A 51.47(3) . . ? Rh6A Rh2A Rh3A 103.22(4) . . ? Rh7A Rh2A Rh3A 58.08(3) . . ? Rh1A Rh2A Rh3A 57.43(3) . . ? C2A Rh2A Rh5A 161.3(5) . . ? C48A Rh2A Rh5A 83.0(2) 2_666 . ? C12A Rh2A Rh5A 68.3(2) . . ? C2A' Rh2A Rh5A 164.5(4) . . ? Rh4A Rh2A Rh5A 86.31(4) 2_666 . ? PA Rh2A Rh5A 50.42(2) . . ? Rh6A Rh2A Rh5A 58.35(3) . . ? Rh7A Rh2A Rh5A 101.30(4) . . ? Rh1A Rh2A Rh5A 57.88(3) . . ? Rh3A Rh2A Rh5A 89.37(4) . . ? C3A Rh3A C13A 97.5(6) . . ? C3A Rh3A C59A 96.2(6) . 2_666 ? C13A Rh3A C59A 106.4(3) . 2_666 ? C3A Rh3A Rh5A 98.3(5) . 2_666 ? C13A Rh3A Rh5A 157.1(2) . 2_666 ? C59A Rh3A Rh5A 55.4(2) 2_666 2_666 ? C3A Rh3A C3A' 21.4(5) . . ? C13A Rh3A C3A' 105.5(5) . . ? C59A Rh3A C3A' 112.0(4) 2_666 . ? Rh5A Rh3A C3A' 95.1(4) 2_666 . ? C3A Rh3A PA 137.2(5) . . ? C13A Rh3A PA 114.7(2) . . ? C59A Rh3A PA 100.6(2) 2_666 . ? Rh5A Rh3A PA 61.82(3) 2_666 . ? C3A' Rh3A PA 117.3(3) . . ? C3A Rh3A Rh1A 116.4(5) . . ? C13A Rh3A Rh1A 51.4(2) . . ? C59A Rh3A Rh1A 141.0(2) 2_666 . ? Rh5A Rh3A Rh1A 132.28(5) 2_666 . ? C3A' Rh3A Rh1A 105.5(3) . . ? PA Rh3A Rh1A 70.49(3) . . ? C3A Rh3A Rh7A 129.1(5) . . ? C13A Rh3A Rh7A 122.0(2) . . ? C59A Rh3A Rh7A 45.8(2) 2_666 . ? Rh5A Rh3A Rh7A 35.92(3) 2_666 . ? C3A' Rh3A Rh7A 130.8(4) . . ? PA Rh3A Rh7A 54.83(3) . . ? Rh1A Rh3A Rh7A 113.34(4) . . ? C3A Rh3A Rh8A 89.0(5) . . ? C13A Rh3A Rh8A 163.2(2) . . ? C59A Rh3A Rh8A 88.2(2) 2_666 . ? Rh5A Rh3A Rh8A 33.39(3) 2_666 . ? C3A' Rh3A Rh8A 75.7(4) . . ? PA Rh3A Rh8A 52.81(3) . . ? Rh1A Rh3A Rh8A 111.90(4) . . ? Rh7A Rh3A Rh8A 62.70(3) . . ? C3A Rh3A Rh4A 93.7(5) . . ? C13A Rh3A Rh4A 105.8(2) . . ? C59A Rh3A Rh4A 144.6(2) 2_666 . ? Rh5A Rh3A Rh4A 89.57(4) 2_666 . ? C3A' Rh3A Rh4A 72.4(3) . . ? PA Rh3A Rh4A 51.98(3) . . ? Rh1A Rh3A Rh4A 58.21(3) . . ? Rh7A Rh3A Rh4A 103.46(4) . . ? Rh8A Rh3A Rh4A 58.09(3) . . ? C3A Rh3A Rh2A 168.7(5) . . ? C13A Rh3A Rh2A 71.6(2) . . ? C59A Rh3A Rh2A 84.6(2) 2_666 . ? Rh5A Rh3A Rh2A 91.40(4) 2_666 . ? C3A' Rh3A Rh2A 163.1(3) . . ? PA Rh3A Rh2A 53.14(3) . . ? Rh1A Rh3A Rh2A 59.25(3) . . ? Rh7A Rh3A Rh2A 58.39(3) . . ? Rh8A Rh3A Rh2A 102.25(4) . . ? Rh4A Rh3A Rh2A 92.06(4) . . ? C4A Rh4A C14A 94.7(5) . . ? C4A Rh4A C48A 93.6(5) . . ? C14A Rh4A C48A 109.6(3) . . ? C4A Rh4A C4A' 20.6(5) . . ? C14A Rh4A C4A' 103.9(5) . . ? C48A Rh4A C4A' 107.1(4) . . ? C4A Rh4A Rh2A 98.3(5) . 2_666 ? C14A Rh4A Rh2A 158.3(2) . 2_666 ? C48A Rh4A Rh2A 52.5(2) . 2_666 ? C4A' Rh4A Rh2A 94.1(4) . 2_666 ? C4A Rh4A PA 139.6(5) . . ? C14A Rh4A PA 115.7(2) . . ? C48A Rh4A PA 99.8(2) . . ? C4A' Rh4A PA 120.1(3) . . ? Rh2A Rh4A PA 62.71(3) 2_666 . ? C4A Rh4A Rh1A 116.4(5) . . ? C14A Rh4A Rh1A 52.1(2) . . ? C48A Rh4A Rh1A 144.2(2) . . ? C4A' Rh4A Rh1A 107.4(4) . . ? Rh2A Rh4A Rh1A 133.24(5) 2_666 . ? PA Rh4A Rh1A 70.59(3) . . ? C4A Rh4A Rh8A 129.8(5) . . ? C14A Rh4A Rh8A 123.7(2) . . ? C48A Rh4A Rh8A 46.7(2) . . ? C4A' Rh4A Rh8A 130.2(4) . . ? Rh2A Rh4A Rh8A 36.28(3) 2_666 . ? PA Rh4A Rh8A 53.26(3) . . ? Rh1A Rh4A Rh8A 112.80(4) . . ? C4A Rh4A Rh9A 90.3(5) . . ? C14A Rh4A Rh9A 162.7(2) . . ? C48A Rh4A Rh9A 86.6(2) . . ? C4A' Rh4A Rh9A 76.0(4) . . ? Rh2A Rh4A Rh9A 34.79(3) 2_666 . ? PA Rh4A Rh9A 53.11(3) . . ? Rh1A Rh4A Rh9A 110.98(4) . . ? Rh8A Rh4A Rh9A 63.00(3) . . ? C4A Rh4A Rh3A 167.1(5) . . ? C14A Rh4A Rh3A 72.7(2) . . ? C48A Rh4A Rh3A 88.1(2) . . ? C4A' Rh4A Rh3A 164.5(4) . . ? Rh2A Rh4A Rh3A 92.87(4) 2_666 . ? PA Rh4A Rh3A 52.16(3) . . ? Rh1A Rh4A Rh3A 58.27(3) . . ? Rh8A Rh4A Rh3A 59.01(3) . . ? Rh9A Rh4A Rh3A 102.55(4) . . ? C4A Rh4A Rh5A 96.7(5) . . ? C14A Rh4A Rh5A 107.0(2) . . ? C48A Rh4A Rh5A 140.9(2) . . ? C4A' Rh4A Rh5A 76.5(3) . . ? Rh2A Rh4A Rh5A 88.68(4) 2_666 . ? PA Rh4A Rh5A 50.78(3) . . ? Rh1A Rh4A Rh5A 58.48(3) . . ? Rh8A Rh4A Rh5A 100.49(4) . . ? Rh9A Rh4A Rh5A 55.89(3) . . ? Rh3A Rh4A Rh5A 89.85(4) . . ? C5A Rh5A C15A 92.7(5) . . ? C5A Rh5A C59A 92.3(5) . . ? C15A Rh5A C59A 104.7(3) . . ? C5A Rh5A C5A' 23.7(5) . . ? C15A Rh5A C5A' 97.6(4) . . ? C59A Rh5A C5A' 113.1(4) . . ? C5A Rh5A Rh3A 104.2(5) . 2_666 ? C15A Rh5A Rh3A 153.1(2) . 2_666 ? C59A Rh5A Rh3A 54.6(2) . 2_666 ? C5A' Rh5A Rh3A 106.3(4) . 2_666 ? C5A Rh5A PA 147.8(5) . . ? C15A Rh5A PA 112.4(2) . . ? C59A Rh5A PA 99.9(2) . . ? C5A' Rh5A PA 127.6(3) . . ? Rh3A Rh5A PA 61.63(3) 2_666 . ? C5A Rh5A Rh9A 129.9(5) . . ? C15A Rh5A Rh9A 119.8(2) . . ? C59A Rh5A Rh9A 45.65(19) . . ? C5A' Rh5A Rh9A 139.3(4) . . ? Rh3A Rh5A Rh9A 33.99(4) 2_666 . ? PA Rh5A Rh9A 54.24(3) . . ? C5A Rh5A Rh6A 95.4(5) . . ? C15A Rh5A Rh6A 161.2(2) . . ? C59A Rh5A Rh6A 91.8(2) . . ? C5A' Rh5A Rh6A 83.6(4) . . ? Rh3A Rh5A Rh6A 38.40(4) 2_666 . ? PA Rh5A Rh6A 54.85(3) . . ? Rh9A Rh5A Rh6A 66.26(3) . . ? C5A Rh5A Rh1A 118.6(5) . . ? C15A Rh5A Rh1A 50.8(2) . . ? C59A Rh5A Rh1A 138.3(2) . . ? C5A' Rh5A Rh1A 104.2(4) . . ? Rh3A Rh5A Rh1A 130.94(5) 2_666 . ? PA Rh5A Rh1A 69.33(3) . . ? Rh9A Rh5A Rh1A 111.54(4) . . ? Rh6A Rh5A Rh1A 110.69(4) . . ? C5A Rh5A Rh4A 161.3(5) . . ? C15A Rh5A Rh4A 70.2(2) . . ? C59A Rh5A Rh4A 85.05(19) . . ? C5A' Rh5A Rh4A 160.6(4) . . ? Rh3A Rh5A Rh4A 89.42(4) 2_666 . ? PA Rh5A Rh4A 50.49(2) . . ? Rh9A Rh5A Rh4A 58.49(3) . . ? Rh6A Rh5A Rh4A 103.17(4) . . ? Rh1A Rh5A Rh4A 56.48(3) . . ? C5A Rh5A Rh2A 103.6(5) . . ? C15A Rh5A Rh2A 105.1(2) . . ? C59A Rh5A Rh2A 145.2(2) . . ? C5A' Rh5A Rh2A 79.9(3) . . ? Rh3A Rh5A Rh2A 91.20(4) 2_666 . ? PA Rh5A Rh2A 51.90(2) . . ? Rh9A Rh5A Rh2A 102.97(4) . . ? Rh6A Rh5A Rh2A 56.45(3) . . ? Rh1A Rh5A Rh2A 57.70(3) . . ? Rh4A Rh5A Rh2A 88.70(3) . . ? Rh4A Rh6A Rh3A 130.60(8) 2_666 2_666 ? Rh4A Rh6A C3A' 148.4(5) 2_666 2_666 ? Rh3A Rh6A C3A' 79.9(5) 2_666 2_666 ? Rh4A Rh6A C14A 68.3(2) 2_666 2_666 ? Rh3A Rh6A C14A 108.6(2) 2_666 2_666 ? C3A' Rh6A C14A 96.5(5) 2_666 2_666 ? Rh4A Rh6A C48A 70.0(2) 2_666 2_666 ? Rh3A Rh6A C48A 139.2(2) 2_666 2_666 ? C3A' Rh6A C48A 92.3(5) 2_666 2_666 ? C14A Rh6A C48A 112.0(3) 2_666 2_666 ? Rh4A Rh6A C3A 169.4(4) 2_666 2_666 ? Rh3A Rh6A C3A 55.5(3) 2_666 2_666 ? C3A' Rh6A C3A 24.4(5) 2_666 2_666 ? C14A Rh6A C3A 102.1(5) 2_666 2_666 ? C48A Rh6A C3A 111.4(4) 2_666 2_666 ? Rh4A Rh6A Rh8A 92.07(6) 2_666 2_666 ? Rh3A Rh6A Rh8A 85.86(5) 2_666 2_666 ? C3A' Rh6A Rh8A 99.3(5) 2_666 2_666 ? C14A Rh6A Rh8A 160.2(2) 2_666 2_666 ? C48A Rh6A Rh8A 55.7(2) 2_666 2_666 ? C3A Rh6A Rh8A 97.2(4) 2_666 2_666 ? Rh4A Rh6A PA 70.10(5) 2_666 . ? Rh3A Rh6A PA 66.86(4) 2_666 . ? C3A' Rh6A PA 140.4(5) 2_666 . ? C14A Rh6A PA 113.6(2) 2_666 . ? C48A Rh6A PA 98.9(2) 2_666 . ? C3A Rh6A PA 119.2(3) 2_666 . ? Rh8A Rh6A PA 58.87(3) 2_666 . ? Rh4A Rh6A Rh2A 55.97(5) 2_666 . ? Rh3A Rh6A Rh2A 112.33(6) 2_666 . ? C3A' Rh6A Rh2A 126.8(5) 2_666 . ? C14A Rh6A Rh2A 123.8(2) 2_666 . ? C48A Rh6A Rh2A 43.8(2) 2_666 . ? C3A Rh6A Rh2A 132.6(4) 2_666 . ? Rh8A Rh6A Rh2A 36.42(3) 2_666 . ? PA Rh6A Rh2A 55.23(3) . . ? Rh4A Rh6A Rh1A 72.78(5) 2_666 2_666 ? Rh3A Rh6A Rh1A 69.97(5) 2_666 2_666 ? C3A' Rh6A Rh1A 120.0(5) 2_666 2_666 ? C14A Rh6A Rh1A 50.9(2) 2_666 2_666 ? C48A Rh6A Rh1A 142.7(2) 2_666 2_666 ? C3A Rh6A Rh1A 105.0(4) 2_666 2_666 ? Rh8A Rh6A Rh1A 127.49(5) 2_666 2_666 ? PA Rh6A Rh1A 68.75(3) . 2_666 ? Rh2A Rh6A Rh1A 112.53(4) . 2_666 ? Rh4A Rh6A Rh5A 114.34(6) 2_666 . ? Rh3A Rh6A Rh5A 52.77(4) 2_666 . ? C3A' Rh6A Rh5A 89.9(5) 2_666 . ? C14A Rh6A Rh5A 159.0(2) 2_666 . ? C48A Rh6A Rh5A 87.6(2) 2_666 . ? C3A Rh6A Rh5A 76.2(4) 2_666 . ? Rh8A Rh6A Rh5A 33.18(3) 2_666 . ? PA Rh6A Rh5A 53.14(3) . . ? Rh2A Rh6A Rh5A 65.20(3) . . ? Rh1A Rh6A Rh5A 108.81(4) 2_666 . ? Rh4A Rh6A Rh7A 21.04(5) 2_666 . ? Rh3A Rh6A Rh7A 109.56(5) 2_666 . ? C3A' Rh6A Rh7A 167.1(5) 2_666 . ? C14A Rh6A Rh7A 72.4(2) 2_666 . ? C48A Rh6A Rh7A 86.0(2) 2_666 . ? C3A Rh6A Rh7A 162.4(4) 2_666 . ? Rh8A Rh6A Rh7A 90.32(4) 2_666 . ? PA Rh6A Rh7A 52.36(3) . . ? Rh2A Rh6A Rh7A 58.73(3) . . ? Rh1A Rh6A Rh7A 58.27(3) 2_666 . ? Rh5A Rh6A Rh7A 102.78(4) . . ? Rh5A Rh7A Rh4A 132.54(7) 2_666 2_666 ? Rh5A Rh7A C4A' 147.5(6) 2_666 2_666 ? Rh4A Rh7A C4A' 79.4(6) 2_666 2_666 ? Rh5A Rh7A C15A 65.6(2) 2_666 2_666 ? Rh4A Rh7A C15A 113.0(2) 2_666 2_666 ? C4A' Rh7A C15A 99.7(6) 2_666 2_666 ? Rh5A Rh7A C59A 65.00(19) 2_666 2_666 ? Rh4A Rh7A C59A 142.2(2) 2_666 2_666 ? C4A' Rh7A C59A 93.7(6) 2_666 2_666 ? C15A Rh7A C59A 104.8(3) 2_666 2_666 ? Rh5A Rh7A C4A 168.4(4) 2_666 2_666 ? Rh4A Rh7A C4A 56.5(3) 2_666 2_666 ? C4A' Rh7A C4A 23.1(5) 2_666 2_666 ? C15A Rh7A C4A 105.1(4) 2_666 2_666 ? C59A Rh7A C4A 113.1(4) 2_666 2_666 ? Rh5A Rh7A Rh9A 87.24(6) 2_666 2_666 ? Rh4A Rh7A Rh9A 90.18(6) 2_666 2_666 ? C4A' Rh7A Rh9A 100.0(5) 2_666 2_666 ? C15A Rh7A Rh9A 151.9(2) 2_666 2_666 ? C59A Rh7A Rh9A 54.09(19) 2_666 2_666 ? C4A Rh7A Rh9A 100.8(4) 2_666 2_666 ? Rh5A Rh7A PA 69.20(4) 2_666 . ? Rh4A Rh7A PA 68.58(4) 2_666 . ? C4A' Rh7A PA 141.3(6) 2_666 . ? C15A Rh7A PA 112.2(2) 2_666 . ? C59A Rh7A PA 98.43(19) 2_666 . ? C4A Rh7A PA 122.1(3) 2_666 . ? Rh9A Rh7A PA 60.32(3) 2_666 . ? Rh5A Rh7A Rh3A 53.94(5) 2_666 . ? Rh4A Rh7A Rh3A 112.33(6) 2_666 . ? C4A' Rh7A Rh3A 126.9(5) 2_666 . ? C15A Rh7A Rh3A 119.1(2) 2_666 . ? C59A Rh7A Rh3A 44.58(19) 2_666 . ? C4A Rh7A Rh3A 133.6(4) 2_666 . ? Rh9A Rh7A Rh3A 33.30(3) 2_666 . ? PA Rh7A Rh3A 53.86(3) . . ? Rh5A Rh7A Rh2A 112.81(6) 2_666 . ? Rh4A Rh7A Rh2A 55.23(5) 2_666 . ? C4A' Rh7A Rh2A 89.1(5) 2_666 . ? C15A Rh7A Rh2A 164.0(2) 2_666 . ? C59A Rh7A Rh2A 87.80(19) 2_666 . ? C4A Rh7A Rh2A 78.1(4) 2_666 . ? Rh9A Rh7A Rh2A 35.13(3) 2_666 . ? PA Rh7A Rh2A 55.08(3) . . ? Rh3A Rh7A Rh2A 63.53(3) . . ? Rh5A Rh7A Rh1A 74.15(5) 2_666 2_666 ? Rh4A Rh7A Rh1A 71.65(5) 2_666 2_666 ? C4A' Rh7A Rh1A 120.7(5) 2_666 2_666 ? C15A Rh7A Rh1A 51.5(2) 2_666 2_666 ? C59A Rh7A Rh1A 138.95(19) 2_666 2_666 ? C4A Rh7A Rh1A 106.1(4) 2_666 2_666 ? Rh9A Rh7A Rh1A 129.86(4) 2_666 2_666 ? PA Rh7A Rh1A 69.55(3) . 2_666 ? Rh3A Rh7A Rh1A 111.97(4) . 2_666 ? Rh2A Rh7A Rh1A 112.52(4) . 2_666 ? Rh5A Rh7A Rh8A 23.19(4) 2_666 . ? Rh4A Rh7A Rh8A 109.47(6) 2_666 . ? C4A' Rh7A Rh8A 167.4(6) 2_666 . ? C15A Rh7A Rh8A 68.9(2) 2_666 . ? C59A Rh7A Rh8A 84.59(19) 2_666 . ? C4A Rh7A Rh8A 162.3(4) 2_666 . ? Rh9A Rh7A Rh8A 89.12(4) 2_666 . ? PA Rh7A Rh8A 51.11(3) . . ? Rh3A Rh7A Rh8A 59.03(3) . . ? Rh2A Rh7A Rh8A 103.27(4) . . ? Rh1A Rh7A Rh8A 56.86(3) 2_666 . ? Rh5A Rh8A Rh2A 141.43(8) 2_666 2_666 ? Rh5A Rh8A C5A' 72.1(5) 2_666 2_666 ? Rh2A Rh8A C5A' 145.4(5) 2_666 2_666 ? Rh5A Rh8A C12A 114.3(2) 2_666 2_666 ? Rh2A Rh8A C12A 66.2(2) 2_666 2_666 ? C5A' Rh8A C12A 95.1(5) 2_666 2_666 ? Rh5A Rh8A C48A 140.8(2) 2_666 . ? Rh2A Rh8A C48A 61.94(19) 2_666 . ? C5A' Rh8A C48A 98.1(5) 2_666 . ? C12A Rh8A C48A 104.2(3) 2_666 . ? Rh5A Rh8A C5A 52.5(3) 2_666 2_666 ? Rh2A Rh8A C5A 165.0(3) 2_666 2_666 ? C5A' Rh8A C5A 19.8(5) 2_666 2_666 ? C12A Rh8A C5A 104.8(4) 2_666 2_666 ? C48A Rh8A C5A 111.4(4) . 2_666 ? Rh5A Rh8A Rh6A 91.69(6) 2_666 2_666 ? Rh2A Rh8A Rh6A 86.75(6) 2_666 2_666 ? C5A' Rh8A Rh6A 103.8(4) 2_666 2_666 ? C12A Rh8A Rh6A 151.8(2) 2_666 2_666 ? C48A Rh8A Rh6A 52.88(19) . 2_666 ? C5A Rh8A Rh6A 99.7(4) 2_666 2_666 ? Rh5A Rh8A PA 72.29(5) 2_666 . ? Rh2A Rh8A PA 72.81(5) 2_666 . ? C5A' Rh8A PA 141.4(5) 2_666 . ? C12A Rh8A PA 112.9(2) 2_666 . ? C48A Rh8A PA 99.96(19) . . ? C5A Rh8A PA 122.2(3) 2_666 . ? Rh6A Rh8A PA 62.91(3) 2_666 . ? Rh5A Rh8A Rh1A 77.79(5) 2_666 2_666 ? Rh2A Rh8A Rh1A 76.25(5) 2_666 2_666 ? C5A' Rh8A Rh1A 114.1(4) 2_666 2_666 ? C12A Rh8A Rh1A 48.7(2) 2_666 2_666 ? C48A Rh8A Rh1A 137.69(19) . 2_666 ? C5A Rh8A Rh1A 107.4(4) 2_666 2_666 ? Rh6A Rh8A Rh1A 134.68(5) 2_666 2_666 ? PA Rh8A Rh1A 71.93(3) . 2_666 ? Rh5A Rh8A Rh4A 112.88(6) 2_666 . ? Rh2A Rh8A Rh4A 55.64(5) 2_666 . ? C5A' Rh8A Rh4A 131.1(4) 2_666 . ? C12A Rh8A Rh4A 121.7(2) 2_666 . ? C48A Rh8A Rh4A 45.75(19) . . ? C5A Rh8A Rh4A 130.9(4) 2_666 . ? Rh6A Rh8A Rh4A 31.39(3) 2_666 . ? PA Rh8A Rh4A 54.32(3) . . ? Rh1A Rh8A Rh4A 114.46(4) 2_666 . ? Rh5A Rh8A Rh3A 53.17(5) 2_666 . ? Rh2A Rh8A Rh3A 114.62(6) 2_666 . ? C5A' Rh8A Rh3A 92.1(4) 2_666 . ? C12A Rh8A Rh3A 162.4(2) 2_666 . ? C48A Rh8A Rh3A 90.59(19) . . ? C5A Rh8A Rh3A 77.7(4) 2_666 . ? Rh6A Rh8A Rh3A 38.61(3) 2_666 . ? PA Rh8A Rh3A 54.04(3) . . ? Rh1A Rh8A Rh3A 113.76(4) 2_666 . ? Rh4A Rh8A Rh3A 62.90(3) . . ? Rh5A Rh8A Rh7A 24.56(4) 2_666 . ? Rh2A Rh8A Rh7A 117.09(6) 2_666 . ? C5A' Rh8A Rh7A 95.3(5) 2_666 . ? C12A Rh8A Rh7A 105.0(2) 2_666 . ? C48A Rh8A Rh7A 146.5(2) . . ? C5A Rh8A Rh7A 76.2(3) 2_666 . ? Rh6A Rh8A Rh7A 94.12(4) 2_666 . ? PA Rh8A Rh7A 53.17(3) . . ? Rh1A Rh8A Rh7A 59.55(3) 2_666 . ? Rh4A Rh8A Rh7A 103.73(4) . . ? Rh3A Rh8A Rh7A 58.27(3) . . ? Rh3A Rh9A Rh2A 138.74(8) 2_666 2_666 ? Rh3A Rh9A C2A' 147.0(5) 2_666 2_666 ? Rh2A Rh9A C2A' 72.0(5) 2_666 2_666 ? Rh3A Rh9A C13A 64.7(2) 2_666 2_666 ? Rh2A Rh9A C13A 112.6(2) 2_666 2_666 ? C2A' Rh9A C13A 95.3(5) 2_666 2_666 ? Rh3A Rh9A C59A 66.9(2) 2_666 . ? Rh2A Rh9A C59A 141.7(2) 2_666 . ? C2A' Rh9A C59A 95.7(5) 2_666 . ? C13A Rh9A C59A 104.5(3) 2_666 . ? Rh3A Rh9A C2A 163.7(3) 2_666 2_666 ? Rh2A Rh9A C2A 51.7(3) 2_666 2_666 ? C2A' Rh9A C2A 20.5(5) 2_666 2_666 ? C13A Rh9A C2A 100.6(4) 2_666 2_666 ? C59A Rh9A C2A 113.0(4) . 2_666 ? Rh3A Rh9A Rh7A 91.95(6) 2_666 2_666 ? Rh2A Rh9A Rh7A 90.34(6) 2_666 2_666 ? C2A' Rh9A Rh7A 101.0(4) 2_666 2_666 ? C13A Rh9A Rh7A 155.2(2) 2_666 2_666 ? C59A Rh9A Rh7A 55.6(2) . 2_666 ? C2A Rh9A Rh7A 101.2(4) 2_666 2_666 ? Rh3A Rh9A PA 71.86(5) 2_666 . ? Rh2A Rh9A PA 72.88(5) 2_666 . ? C2A' Rh9A PA 140.9(5) 2_666 . ? C13A Rh9A PA 113.8(2) 2_666 . ? C59A Rh9A PA 101.2(2) . . ? C2A Rh9A PA 122.8(3) 2_666 . ? Rh7A Rh9A PA 62.53(3) 2_666 . ? Rh3A Rh9A Rh5A 55.35(5) 2_666 . ? Rh2A Rh9A Rh5A 116.60(6) 2_666 . ? C2A' Rh9A Rh5A 131.4(4) 2_666 . ? C13A Rh9A Rh5A 119.5(2) 2_666 . ? C59A Rh9A Rh5A 46.12(19) . . ? C2A Rh9A Rh5A 137.2(4) 2_666 . ? Rh7A Rh9A Rh5A 36.61(3) 2_666 . ? PA Rh9A Rh5A 55.09(3) . . ? Rh3A Rh9A Rh1A 73.71(5) 2_666 2_666 ? Rh2A Rh9A Rh1A 74.93(5) 2_666 2_666 ? C2A' Rh9A Rh1A 115.3(4) 2_666 2_666 ? C13A Rh9A Rh1A 51.1(2) 2_666 2_666 ? C59A Rh9A Rh1A 140.2(2) . 2_666 ? C2A Rh9A Rh1A 103.2(3) 2_666 2_666 ? Rh7A Rh9A Rh1A 133.15(5) 2_666 2_666 ? PA Rh9A Rh1A 70.62(3) . 2_666 ? Rh5A Rh9A Rh1A 112.94(4) . 2_666 ? Rh3A Rh9A Rh4A 115.52(6) 2_666 . ? Rh2A Rh9A Rh4A 54.56(5) 2_666 . ? C2A' Rh9A Rh4A 91.5(4) 2_666 . ? C13A Rh9A Rh4A 162.5(2) 2_666 . ? C59A Rh9A Rh4A 90.8(2) . . ? C2A Rh9A Rh4A 80.7(3) 2_666 . ? Rh7A Rh9A Rh4A 35.96(3) 2_666 . ? PA Rh9A Rh4A 53.61(3) . . ? Rh5A Rh9A Rh4A 65.62(3) . . ? Rh1A Rh9A Rh4A 111.47(4) 2_666 . ? Rh3A Rh9A Rh8A 112.44(6) 2_666 . ? Rh2A Rh9A Rh8A 26.30(4) 2_666 . ? C2A' Rh9A Rh8A 97.7(5) 2_666 . ? C13A Rh9A Rh8A 105.1(2) 2_666 . ? C59A Rh9A Rh8A 146.1(2) . . ? C2A Rh9A Rh8A 77.2(3) 2_666 . ? Rh7A Rh9A Rh8A 91.18(4) 2_666 . ? PA Rh9A Rh8A 51.16(3) . . ? Rh5A Rh9A Rh8A 103.71(4) . . ? Rh1A Rh9A Rh8A 56.90(3) 2_666 . ? Rh4A Rh9A Rh8A 57.86(3) . . ? Rh8A PA Rh8A 180.00(5) . 2_666 ? Rh8A PA Rh9A 102.83(3) . 2_666 ? Rh8A PA Rh9A 77.17(3) 2_666 2_666 ? Rh8A PA Rh9A 77.17(3) . . ? Rh8A PA Rh9A 102.83(3) 2_666 . ? Rh9A PA Rh9A 180.0 2_666 . ? Rh8A PA Rh4A 107.58(3) . 2_666 ? Rh8A PA Rh4A 72.42(3) 2_666 2_666 ? Rh9A PA Rh4A 73.28(3) 2_666 2_666 ? Rh9A PA Rh4A 106.72(3) . 2_666 ? Rh8A PA Rh4A 72.42(3) . . ? Rh8A PA Rh4A 107.58(3) 2_666 . ? Rh9A PA Rh4A 106.72(3) 2_666 . ? Rh9A PA Rh4A 73.28(3) . . ? Rh4A PA Rh4A 180.00(4) 2_666 . ? Rh8A PA Rh3A 73.15(3) . . ? Rh8A PA Rh3A 106.85(3) 2_666 . ? Rh9A PA Rh3A 37.76(3) 2_666 . ? Rh9A PA Rh3A 142.24(3) . . ? Rh4A PA Rh3A 104.14(3) 2_666 . ? Rh4A PA Rh3A 75.86(3) . . ? Rh8A PA Rh3A 106.85(3) . 2_666 ? Rh8A PA Rh3A 73.15(3) 2_666 2_666 ? Rh9A PA Rh3A 142.24(3) 2_666 2_666 ? Rh9A PA Rh3A 37.76(3) . 2_666 ? Rh4A PA Rh3A 75.86(3) 2_666 2_666 ? Rh4A PA Rh3A 104.14(3) . 2_666 ? Rh3A PA Rh3A 180.0 . 2_666 ? Rh8A PA Rh5A 141.69(3) . . ? Rh8A PA Rh5A 38.31(3) 2_666 . ? Rh9A PA Rh5A 109.33(3) 2_666 . ? Rh9A PA Rh5A 70.67(3) . . ? Rh4A PA Rh5A 101.27(3) 2_666 . ? Rh4A PA Rh5A 78.73(3) . . ? Rh3A PA Rh5A 123.45(3) . . ? Rh3A PA Rh5A 56.55(3) 2_666 . ? Rh8A PA Rh5A 38.31(3) . 2_666 ? Rh8A PA Rh5A 141.69(3) 2_666 2_666 ? Rh9A PA Rh5A 70.67(3) 2_666 2_666 ? Rh9A PA Rh5A 109.33(3) . 2_666 ? Rh4A PA Rh5A 78.73(3) 2_666 2_666 ? Rh4A PA Rh5A 101.27(3) . 2_666 ? Rh3A PA Rh5A 56.55(3) . 2_666 ? Rh3A PA Rh5A 123.45(3) 2_666 2_666 ? Rh5A PA Rh5A 180.00(3) . 2_666 ? Rh8A PA Rh7A 75.72(3) . . ? Rh8A PA Rh7A 104.28(3) 2_666 . ? Rh9A PA Rh7A 57.15(3) 2_666 . ? Rh9A PA Rh7A 122.85(3) . . ? Rh4A PA Rh7A 40.58(3) 2_666 . ? Rh4A PA Rh7A 139.42(3) . . ? Rh3A PA Rh7A 71.31(3) . . ? Rh3A PA Rh7A 108.69(3) 2_666 . ? Rh5A PA Rh7A 140.05(3) . . ? Rh5A PA Rh7A 39.95(3) 2_666 . ? Rh8A PA Rh7A 104.28(3) . 2_666 ? Rh8A PA Rh7A 75.72(3) 2_666 2_666 ? Rh9A PA Rh7A 122.85(3) 2_666 2_666 ? Rh9A PA Rh7A 57.15(3) . 2_666 ? Rh4A PA Rh7A 139.42(3) 2_666 2_666 ? Rh4A PA Rh7A 40.58(3) . 2_666 ? Rh3A PA Rh7A 108.69(3) . 2_666 ? Rh3A PA Rh7A 71.31(3) 2_666 2_666 ? Rh5A PA Rh7A 39.95(3) . 2_666 ? Rh5A PA Rh7A 140.05(3) 2_666 2_666 ? Rh7A PA Rh7A 180.000(1) . 2_666 ? O1A C1A Rh1A 178.0(8) . . ? C2A' C2A O2A 73.9(8) . . ? C2A' C2A Rh2A 95.4(11) . . ? O2A C2A Rh2A 168.3(12) . . ? C2A' C2A Rh9A 50.4(8) . 2_666 ? O2A C2A Rh9A 124.3(10) . 2_666 ? Rh2A C2A Rh9A 45.2(3) . 2_666 ? C2A C2A' O2A 64.5(7) . . ? C2A C2A' Rh9A 109.1(11) . 2_666 ? O2A C2A' Rh9A 173.6(12) . 2_666 ? C2A C2A' Rh2A 60.5(9) . . ? O2A C2A' Rh2A 124.9(10) . . ? Rh9A C2A' Rh2A 48.8(2) 2_666 . ? C2A O2A C2A' 41.6(8) . . ? C3A' C3A O3A 64.2(7) . . ? C3A' C3A Rh3A 109.4(12) . . ? O3A C3A Rh3A 172.3(14) . . ? C3A' C3A Rh6A 56.8(9) . 2_666 ? O3A C3A Rh6A 121.0(11) . 2_666 ? Rh3A C3A Rh6A 52.6(3) . 2_666 ? C3A C3A' O3A 71.7(8) . . ? C3A C3A' Rh6A 98.7(11) . 2_666 ? O3A C3A' Rh6A 170.3(14) . 2_666 ? C3A C3A' Rh3A 49.2(9) . . ? O3A C3A' Rh3A 120.8(11) . . ? Rh6A C3A' Rh3A 49.6(3) 2_666 . ? C3A' O3A C3A 44.1(9) . . ? C4A' C4A O4A 69.1(8) . . ? C4A' C4A Rh4A 108.8(12) . . ? O4A C4A Rh4A 176.6(13) . . ? C4A' C4A Rh7A 59.1(10) . 2_666 ? O4A C4A Rh7A 128.1(11) . 2_666 ? Rh4A C4A Rh7A 50.0(3) . 2_666 ? C4A C4A' O4A 69.8(8) . . ? C4A C4A' Rh7A 97.9(12) . 2_666 ? O4A C4A' Rh7A 167.4(15) . 2_666 ? C4A C4A' Rh4A 50.6(10) . . ? O4A C4A' Rh4A 120.4(12) . . ? Rh7A C4A' Rh4A 47.5(3) 2_666 . ? C4A' O4A C4A 41.1(9) . . ? C5A' C5A O5A 74.2(9) . . ? C5A' C5A Rh5A 93.5(11) . . ? O5A C5A Rh5A 167.1(13) . . ? C5A' C5A Rh8A 50.2(9) . 2_666 ? O5A C5A Rh8A 124.4(11) . 2_666 ? Rh5A C5A Rh8A 43.6(3) . 2_666 ? C5A C5A' O5A 65.5(7) . . ? C5A C5A' Rh8A 110.0(11) . 2_666 ? O5A C5A' Rh8A 175.2(12) . 2_666 ? C5A C5A' Rh5A 62.8(10) . . ? O5A C5A' Rh5A 128.1(10) . . ? Rh8A C5A' Rh5A 47.5(2) 2_666 . ? C5A O5A C5A' 40.3(9) . . ? O12A C12A Rh8A 133.8(7) . 2_666 ? O12A C12A Rh2A 132.1(7) . . ? Rh8A C12A Rh2A 49.95(19) 2_666 . ? O12A C12A Rh1A 133.6(7) . . ? Rh8A C12A Rh1A 86.2(3) 2_666 . ? Rh2A C12A Rh1A 89.4(3) . . ? O13A C13A Rh3A 134.4(7) . . ? O13A C13A Rh9A 135.6(7) . 2_666 ? Rh3A C13A Rh9A 47.4(2) . 2_666 ? O13A C13A Rh1A 134.2(7) . . ? Rh3A C13A Rh1A 86.1(3) . . ? Rh9A C13A Rh1A 85.2(3) 2_666 . ? O14A C14A Rh6A 139.4(7) . 2_666 ? O14A C14A Rh4A 140.2(7) . . ? Rh6A C14A Rh4A 44.43(19) 2_666 . ? O14A C14A Rh1A 129.2(7) . . ? Rh6A C14A Rh1A 86.7(3) 2_666 . ? Rh4A C14A Rh1A 84.2(3) . . ? O15A C15A Rh7A 138.0(6) . 2_666 ? O15A C15A Rh5A 134.2(6) . . ? Rh7A C15A Rh5A 50.31(18) 2_666 . ? O15A C15A Rh1A 131.6(6) . . ? Rh7A C15A Rh1A 85.7(3) 2_666 . ? Rh5A C15A Rh1A 86.3(3) . . ? O48A C48A Rh2A 133.8(6) . 2_666 ? O48A C48A Rh6A 134.8(6) . 2_666 ? Rh2A C48A Rh6A 91.4(3) 2_666 2_666 ? O48A C48A Rh4A 136.5(6) . . ? Rh2A C48A Rh4A 71.9(2) 2_666 . ? Rh6A C48A Rh4A 43.08(15) 2_666 . ? O48A C48A Rh8A 135.8(6) . . ? Rh2A C48A Rh8A 49.29(17) 2_666 . ? Rh6A C48A Rh8A 71.4(2) 2_666 . ? Rh4A C48A Rh8A 87.6(3) . . ? O59A C59A Rh3A 135.8(6) . 2_666 ? O59A C59A Rh9A 136.7(6) . . ? Rh3A C59A Rh9A 46.03(16) 2_666 . ? O59A C59A Rh5A 135.1(6) . . ? Rh3A C59A Rh5A 69.9(2) 2_666 . ? Rh9A C59A Rh5A 88.2(3) . . ? O59A C59A Rh7A 134.6(6) . 2_666 ? Rh3A C59A Rh7A 89.7(3) 2_666 2_666 ? Rh9A C59A Rh7A 70.3(2) . 2_666 ? Rh5A C59A Rh7A 48.61(16) . 2_666 ? C1B Rh1B C12B 94.1(3) . . ? C1B Rh1B C13B 92.5(3) . . ? C12B Rh1B C13B 89.6(3) . . ? C1B Rh1B C14B 90.5(3) . . ? C12B Rh1B C14B 175.3(3) . . ? C13B Rh1B C14B 90.6(3) . . ? C1B Rh1B C15B 92.8(3) . . ? C12B Rh1B C15B 88.4(3) . . ? C13B Rh1B C15B 174.5(3) . . ? C14B Rh1B C15B 91.0(3) . . ? C1B Rh1B Rh3B 132.5(2) . . ? C12B Rh1B Rh3B 104.0(2) . . ? C13B Rh1B Rh3B 45.13(19) . . ? C14B Rh1B Rh3B 73.0(2) . . ? C15B Rh1B Rh3B 130.62(19) . . ? C1B Rh1B Rh2B 135.3(2) . . ? C12B Rh1B Rh2B 45.5(2) . . ? C13B Rh1B Rh2B 72.80(19) . . ? C14B Rh1B Rh2B 130.3(2) . . ? C15B Rh1B Rh2B 102.25(19) . . ? Rh3B Rh1B Rh2B 62.01(3) . . ? C1B Rh1B Rh4B 130.1(2) . . ? C12B Rh1B Rh4B 131.9(2) . . ? C13B Rh1B Rh4B 104.13(19) . . ? C14B Rh1B Rh4B 43.6(2) . . ? C15B Rh1B Rh4B 73.54(19) . . ? Rh3B Rh1B Rh4B 62.61(3) . . ? Rh2B Rh1B Rh4B 94.55(3) . . ? C1B Rh1B Rh5B 132.7(2) . . ? C12B Rh1B Rh5B 73.6(2) . . ? C13B Rh1B Rh5B 131.80(19) . . ? C14B Rh1B Rh5B 102.9(2) . . ? C15B Rh1B Rh5B 42.70(19) . . ? Rh3B Rh1B Rh5B 94.77(3) . . ? Rh2B Rh1B Rh5B 63.18(3) . . ? Rh4B Rh1B Rh5B 62.82(3) . . ? C2B Rh2B C48B 89.4(5) . 2 ? C2B Rh2B C12B 93.9(5) . . ? C48B Rh2B C12B 103.7(3) 2 . ? C2B Rh2B Rh4B 100.6(5) . 2 ? C48B Rh2B Rh4B 59.0(2) 2 2 ? C12B Rh2B Rh4B 157.0(2) . 2 ? C2B Rh2B C2B' 25.1(5) . . ? C48B Rh2B C2B' 113.3(4) 2 . ? C12B Rh2B C2B' 95.0(4) . . ? Rh4B Rh2B C2B' 105.7(4) 2 . ? C2B Rh2B PB 148.2(5) . . ? C48B Rh2B PB 104.5(2) 2 . ? C12B Rh2B PB 109.9(2) . . ? Rh4B Rh2B PB 64.93(4) 2 . ? C2B' Rh2B PB 127.7(3) . . ? C2B Rh2B Rh6B 126.3(5) . . ? C48B Rh2B Rh6B 47.9(2) 2 . ? C12B Rh2B Rh6B 123.0(2) . . ? Rh4B Rh2B Rh6B 34.48(4) 2 . ? C2B' Rh2B Rh6B 139.0(4) . . ? PB Rh2B Rh6B 57.01(3) . . ? C2B Rh2B Rh7B 95.7(5) . . ? C48B Rh2B Rh7B 94.4(2) 2 . ? C12B Rh2B Rh7B 159.6(2) . . ? Rh4B Rh2B Rh7B 35.97(4) 2 . ? C2B' Rh2B Rh7B 86.2(4) . . ? PB Rh2B Rh7B 55.40(3) . . ? Rh6B Rh2B Rh7B 63.76(3) . . ? C2B Rh2B Rh1B 118.8(5) . . ? C48B Rh2B Rh1B 135.9(2) 2 . ? C12B Rh2B Rh1B 46.0(2) . . ? Rh4B Rh2B Rh1B 134.84(5) 2 . ? C2B' Rh2B Rh1B 102.2(3) . . ? PB Rh2B Rh1B 69.92(3) . . ? Rh6B Rh2B Rh1B 114.86(4) . . ? Rh7B Rh2B Rh1B 113.76(4) . . ? C2B Rh2B Rh3B 104.7(5) . . ? C48B Rh2B Rh3B 150.6(2) 2 . ? C12B Rh2B Rh3B 101.0(2) . . ? Rh4B Rh2B Rh3B 92.62(5) 2 . ? C2B' Rh2B Rh3B 79.8(3) . . ? PB Rh2B Rh3B 51.34(3) . . ? Rh6B Rh2B Rh3B 104.58(4) . . ? Rh7B Rh2B Rh3B 59.14(3) . . ? Rh1B Rh2B Rh3B 58.31(3) . . ? C2B Rh2B Rh5B 160.8(5) . . ? C48B Rh2B Rh5B 82.0(2) 2 . ? C12B Rh2B Rh5B 71.8(2) . . ? Rh4B Rh2B Rh5B 89.68(4) 2 . ? C2B' Rh2B Rh5B 162.3(4) . . ? PB Rh2B Rh5B 51.00(3) . . ? Rh6B Rh2B Rh5B 57.89(3) . . ? Rh7B Rh2B Rh5B 101.99(4) . . ? Rh1B Rh2B Rh5B 60.14(3) . . ? Rh3B Rh2B Rh5B 90.84(4) . . ? C3B Rh3B C13B 98.5(5) . . ? C3B Rh3B C59B 97.7(5) . 2 ? C13B Rh3B C59B 103.8(3) . 2 ? C3B Rh3B Rh5B 95.5(5) . 2 ? C13B Rh3B Rh5B 155.6(2) . 2 ? C59B Rh3B Rh5B 54.36(19) 2 2 ? C3B Rh3B C3B' 18.2(5) . . ? C13B Rh3B C3B' 98.0(4) . . ? C59B Rh3B C3B' 115.3(4) 2 . ? Rh5B Rh3B C3B' 101.5(4) 2 . ? C3B Rh3B PB 134.7(5) . . ? C13B Rh3B PB 115.6(2) . . ? C59B Rh3B PB 101.8(2) 2 . ? Rh5B Rh3B PB 65.36(4) 2 . ? C3B' Rh3B PB 121.7(3) . . ? C3B Rh3B Rh1B 116.2(5) . . ? C13B Rh3B Rh1B 51.8(2) . . ? C59B Rh3B Rh1B 139.2(2) 2 . ? Rh5B Rh3B Rh1B 136.06(5) 2 . ? C3B' Rh3B Rh1B 101.5(3) . . ? PB Rh3B Rh1B 70.71(3) . . ? C3B Rh3B Rh8B 85.6(5) . . ? C13B Rh3B Rh8B 165.3(2) . . ? C59B Rh3B Rh8B 89.51(19) 2 . ? Rh5B Rh3B Rh8B 35.56(4) 2 . ? C3B' Rh3B Rh8B 81.5(4) . . ? PB Rh3B Rh8B 54.42(3) . . ? Rh1B Rh3B Rh8B 113.85(4) . . ? C3B Rh3B Rh7B 127.3(5) . . ? C13B Rh3B Rh7B 123.8(2) . . ? C59B Rh3B Rh7B 46.75(19) 2 . ? Rh5B Rh3B Rh7B 34.54(3) 2 . ? C3B' Rh3B Rh7B 136.0(4) . . ? PB Rh3B Rh7B 55.17(3) . . ? Rh1B Rh3B Rh7B 114.56(4) . . ? Rh8B Rh3B Rh7B 61.70(3) . . ? C3B Rh3B Rh2B 172.6(5) . . ? C13B Rh3B Rh2B 74.1(2) . . ? C59B Rh3B Rh2B 83.87(19) 2 . ? Rh5B Rh3B Rh2B 91.28(5) 2 . ? C3B' Rh3B Rh2B 160.8(3) . . ? PB Rh3B Rh2B 51.39(3) . . ? Rh1B Rh3B Rh2B 59.69(3) . . ? Rh8B Rh3B Rh2B 101.69(4) . . ? Rh7B Rh3B Rh2B 58.61(3) . . ? C3B Rh3B Rh4B 90.9(5) . . ? C13B Rh3B Rh4B 108.1(2) . . ? C59B Rh3B Rh4B 145.3(2) 2 . ? Rh5B Rh3B Rh4B 91.49(5) 2 . ? C3B' Rh3B Rh4B 73.7(3) . . ? PB Rh3B Rh4B 51.75(3) . . ? Rh1B Rh3B Rh4B 60.37(3) . . ? Rh8B Rh3B Rh4B 57.58(3) . . ? Rh7B Rh3B Rh4B 102.37(4) . . ? Rh2B Rh3B Rh4B 91.89(4) . . ? C4B Rh4B C48B 91.2(6) . . ? C4B Rh4B C14B 93.8(6) . . ? C48B Rh4B C14B 108.3(3) . . ? C4B Rh4B C4B' 25.8(5) . . ? C48B Rh4B C4B' 114.7(4) . . ? C14B Rh4B C4B' 95.8(5) . . ? C4B Rh4B Rh2B 101.0(5) . 2 ? C48B Rh4B Rh2B 55.4(2) . 2 ? C14B Rh4B Rh2B 157.8(2) . 2 ? C4B' Rh4B Rh2B 104.8(4) . 2 ? C4B Rh4B PB 146.6(5) . . ? C48B Rh4B PB 100.2(2) . . ? C14B Rh4B PB 111.8(2) . . ? C4B' Rh4B PB 125.7(3) . . ? Rh2B Rh4B PB 62.41(4) 2 . ? C4B Rh4B Rh8B 127.8(5) . . ? C48B Rh4B Rh8B 45.7(2) . . ? C14B Rh4B Rh8B 123.2(2) . . ? C4B' Rh4B Rh8B 139.1(4) . . ? Rh2B Rh4B Rh8B 34.97(4) 2 . ? PB Rh4B Rh8B 54.45(3) . . ? C4B Rh4B Rh9B 93.2(5) . . ? C48B Rh4B Rh9B 89.7(2) . . ? C14B Rh4B Rh9B 160.6(2) . . ? C4B' Rh4B Rh9B 82.9(4) . . ? Rh2B Rh4B Rh9B 35.38(4) 2 . ? PB Rh4B Rh9B 56.00(3) . . ? Rh8B Rh4B Rh9B 64.53(3) . . ? C4B Rh4B Rh1B 120.6(5) . . ? C48B Rh4B Rh1B 139.1(2) . . ? C14B Rh4B Rh1B 49.7(2) . . ? C4B' Rh4B Rh1B 102.8(4) . . ? Rh2B Rh4B Rh1B 130.58(5) 2 . ? PB Rh4B Rh1B 68.18(3) . . ? Rh8B Rh4B Rh1B 111.60(4) . . ? Rh9B Rh4B Rh1B 111.51(4) . . ? C4B Rh4B Rh3B 163.1(5) . . ? C48B Rh4B Rh3B 84.9(2) . . ? C14B Rh4B Rh3B 72.0(2) . . ? C4B' Rh4B Rh3B 159.8(4) . . ? Rh2B Rh4B Rh3B 90.34(4) 2 . ? PB Rh4B Rh3B 50.17(3) . . ? Rh8B Rh4B Rh3B 58.52(3) . . ? Rh9B Rh4B Rh3B 103.22(4) . . ? Rh1B Rh4B Rh3B 57.01(3) . . ? C4B Rh4B Rh5B 103.4(5) . . ? C48B Rh4B Rh5B 142.3(2) . . ? C14B Rh4B Rh5B 105.2(2) . . ? C4B' Rh4B Rh5B 78.0(3) . . ? Rh2B Rh4B Rh5B 87.51(4) 2 . ? PB Rh4B Rh5B 50.54(2) . . ? Rh8B Rh4B Rh5B 100.60(4) . . ? Rh9B Rh4B Rh5B 55.48(3) . . ? Rh1B Rh4B Rh5B 59.34(3) . . ? Rh3B Rh4B Rh5B 89.45(4) . . ? C5B Rh5B C59B 91.4(5) . . ? C5B Rh5B C15B 92.5(5) . . ? C59B Rh5B C15B 104.4(3) . . ? C5B Rh5B Rh3B 102.9(5) . 2 ? C59B Rh5B Rh3B 60.4(2) . 2 ? C15B Rh5B Rh3B 158.2(2) . 2 ? C5B Rh5B C5B' 30.2(5) . . ? C59B Rh5B C5B' 121.1(4) . . ? C15B Rh5B C5B' 90.1(4) . . ? Rh3B Rh5B C5B' 111.0(4) 2 . ? C5B Rh5B PB 146.9(5) . . ? C59B Rh5B PB 103.5(2) . . ? C15B Rh5B PB 111.5(2) . . ? Rh3B Rh5B PB 62.00(3) 2 . ? C5B' Rh5B PB 123.7(3) . . ? C5B Rh5B Rh9B 127.3(5) . . ? C59B Rh5B Rh9B 46.6(2) . . ? C15B Rh5B Rh9B 123.5(2) . . ? Rh3B Rh5B Rh9B 34.74(4) 2 . ? C5B' Rh5B Rh9B 145.0(4) . . ? PB Rh5B Rh9B 57.20(3) . . ? C5B Rh5B Rh6B 94.0(5) . . ? C59B Rh5B Rh6B 95.0(2) . . ? C15B Rh5B Rh6B 159.3(2) . . ? Rh3B Rh5B Rh6B 35.90(4) 2 . ? C5B' Rh5B Rh6B 85.8(4) . . ? PB Rh5B Rh6B 55.83(3) . . ? Rh9B Rh5B Rh6B 66.15(3) . . ? C5B Rh5B Rh1B 120.0(5) . . ? C59B Rh5B Rh1B 136.5(2) . . ? C15B Rh5B Rh1B 49.9(2) . . ? Rh3B Rh5B Rh1B 129.16(5) 2 . ? C5B' Rh5B Rh1B 96.2(3) . . ? PB Rh5B Rh1B 67.16(3) . . ? Rh9B Rh5B Rh1B 112.68(4) . . ? Rh6B Rh5B Rh1B 110.40(4) . . ? C5B Rh5B Rh2B 105.0(5) . . ? C59B Rh5B Rh2B 147.5(2) . . ? C15B Rh5B Rh2B 102.7(2) . . ? Rh3B Rh5B Rh2B 88.31(4) 2 . ? C5B' Rh5B Rh2B 76.2(3) . . ? PB Rh5B Rh2B 49.06(2) . . ? Rh9B Rh5B Rh2B 102.68(4) . . ? Rh6B Rh5B Rh2B 56.62(3) . . ? Rh1B Rh5B Rh2B 56.68(3) . . ? C5B Rh5B Rh4B 162.9(5) . . ? C59B Rh5B Rh4B 83.1(2) . . ? C15B Rh5B Rh4B 73.3(2) . . ? Rh3B Rh5B Rh4B 88.54(4) 2 . ? C5B' Rh5B Rh4B 154.0(3) . . ? PB Rh5B Rh4B 50.08(2) . . ? Rh9B Rh5B Rh4B 58.24(3) . . ? Rh6B Rh5B Rh4B 102.57(4) . . ? Rh1B Rh5B Rh4B 57.84(3) . . ? Rh2B Rh5B Rh4B 87.82(3) . . ? Rh4B Rh6B Rh3B 130.99(7) 2 2 ? Rh4B Rh6B C3B' 144.7(5) 2 2 ? Rh3B Rh6B C3B' 84.3(5) 2 2 ? Rh4B Rh6B C14B 70.7(2) 2 2 ? Rh3B Rh6B C14B 118.0(3) 2 2 ? C3B' Rh6B C14B 96.1(5) 2 2 ? Rh4B Rh6B C3B 166.5(4) 2 2 ? Rh3B Rh6B C3B 60.7(3) 2 2 ? C3B' Rh6B C3B 24.3(5) 2 2 ? C14B Rh6B C3B 111.5(5) 2 2 ? Rh4B Rh6B C48B 63.54(19) 2 2 ? Rh3B Rh6B C48B 131.7(2) 2 2 ? C3B' Rh6B C48B 93.0(5) 2 2 ? C14B Rh6B C48B 110.3(3) 2 2 ? C3B Rh6B C48B 104.0(4) 2 2 ? Rh4B Rh6B PB 67.71(5) 2 . ? Rh3B Rh6B PB 65.02(4) 2 . ? C3B' Rh6B PB 144.4(5) 2 . ? C14B Rh6B PB 113.5(3) 2 . ? C3B Rh6B PB 120.8(4) 2 . ? C48B Rh6B PB 94.49(19) 2 . ? Rh4B Rh6B Rh8B 82.96(6) 2 2 ? Rh3B Rh6B Rh8B 82.65(5) 2 2 ? C3B' Rh6B Rh8B 103.1(5) 2 2 ? C14B Rh6B Rh8B 153.3(3) 2 2 ? C3B Rh6B Rh8B 93.1(4) 2 2 ? C48B Rh6B Rh8B 50.91(19) 2 2 ? PB Rh6B Rh8B 57.58(3) . 2 ? Rh4B Rh6B Rh1B 78.48(5) 2 2 ? Rh3B Rh6B Rh1B 73.70(5) 2 2 ? C3B' Rh6B Rh1B 120.4(5) 2 2 ? C14B Rh6B Rh1B 53.0(2) 2 2 ? C3B Rh6B Rh1B 113.8(4) 2 2 ? C48B Rh6B Rh1B 142.02(19) 2 2 ? PB Rh6B Rh1B 69.39(3) . 2 ? Rh8B Rh6B Rh1B 126.95(4) 2 2 ? Rh4B Rh6B Rh2B 48.02(5) 2 . ? Rh3B Rh6B Rh2B 106.80(6) 2 . ? C3B' Rh6B Rh2B 129.4(5) 2 . ? C14B Rh6B Rh2B 118.5(2) 2 . ? C3B Rh6B Rh2B 126.8(4) 2 . ? C48B Rh6B Rh2B 42.66(19) 2 . ? PB Rh6B Rh2B 52.15(3) . . ? Rh8B Rh6B Rh2B 34.95(3) 2 . ? Rh1B Rh6B Rh2B 109.97(4) 2 . ? Rh4B Rh6B Rh5B 109.44(6) 2 . ? Rh3B Rh6B Rh5B 47.44(5) 2 . ? C3B' Rh6B Rh5B 93.1(5) 2 . ? C14B Rh6B Rh5B 161.9(3) 2 . ? C3B Rh6B Rh5B 72.8(4) 2 . ? C48B Rh6B Rh5B 84.75(19) 2 . ? PB Rh6B Rh5B 53.25(3) . . ? Rh8B Rh6B Rh5B 35.43(3) 2 . ? Rh1B Rh6B Rh5B 108.85(4) 2 . ? Rh2B Rh6B Rh5B 65.49(3) . . ? Rh4B Rh6B Rh7B 25.15(4) 2 . ? Rh3B Rh6B Rh7B 108.50(5) 2 . ? C3B' Rh6B Rh7B 163.2(5) 2 . ? C14B Rh6B Rh7B 68.5(2) 2 . ? C3B Rh6B Rh7B 168.3(4) 2 . ? C48B Rh6B Rh7B 86.46(19) 2 . ? PB Rh6B Rh7B 52.14(2) . . ? Rh8B Rh6B Rh7B 89.62(4) 2 . ? Rh1B Rh6B Rh7B 56.23(3) 2 . ? Rh2B Rh6B Rh7B 58.42(3) . . ? Rh5B Rh6B Rh7B 103.56(4) . . ? Rh5B Rh7B Rh4B 137.60(7) 2 2 ? Rh5B Rh7B C4B' 148.5(5) 2 2 ? Rh4B Rh7B C4B' 72.6(5) 2 2 ? Rh5B Rh7B C15B 69.9(2) 2 2 ? Rh4B Rh7B C15B 125.7(2) 2 2 ? C4B' Rh7B C15B 101.1(5) 2 2 ? Rh5B Rh7B C59B 60.04(19) 2 2 ? Rh4B Rh7B C59B 131.1(2) 2 2 ? C4B' Rh7B C59B 94.8(5) 2 2 ? C15B Rh7B C59B 102.9(3) 2 2 ? Rh5B Rh7B C4B 166.9(4) 2 2 ? Rh4B Rh7B C4B 50.9(3) 2 2 ? C4B' Rh7B C4B 21.9(5) 2 2 ? C15B Rh7B C4B 114.7(4) 2 2 ? C59B Rh7B C4B 106.9(4) 2 2 ? Rh5B Rh7B PB 69.52(5) 2 . ? Rh4B Rh7B PB 68.44(4) 2 . ? C4B' Rh7B PB 137.1(5) 2 . ? C15B Rh7B PB 115.9(2) 2 . ? C59B Rh7B PB 97.30(19) 2 . ? C4B Rh7B PB 116.0(3) 2 . ? Rh5B Rh7B Rh9B 80.80(5) 2 2 ? Rh4B Rh7B Rh9B 83.49(5) 2 2 ? C4B' Rh7B Rh9B 98.2(5) 2 2 ? C15B Rh7B Rh9B 148.7(2) 2 2 ? C59B Rh7B Rh9B 50.91(19) 2 2 ? C4B Rh7B Rh9B 91.7(4) 2 2 ? PB Rh7B Rh9B 60.57(3) . 2 ? Rh5B Rh7B Rh1B 82.12(5) 2 2 ? Rh4B Rh7B Rh1B 79.65(5) 2 2 ? C4B' Rh7B Rh1B 118.7(5) 2 2 ? C15B Rh7B Rh1B 55.8(2) 2 2 ? C59B Rh7B Rh1B 141.89(19) 2 2 ? C4B Rh7B Rh1B 110.8(4) 2 2 ? PB Rh7B Rh1B 71.26(3) . 2 ? Rh9B Rh7B Rh1B 131.82(4) 2 2 ? Rh5B Rh7B Rh2B 106.97(6) 2 . ? Rh4B Rh7B Rh2B 47.78(5) 2 . ? C4B' Rh7B Rh2B 88.0(5) 2 . ? C15B Rh7B Rh2B 166.8(2) 2 . ? C59B Rh7B Rh2B 85.76(19) 2 . ? C4B Rh7B Rh2B 71.3(4) 2 . ? PB Rh7B Rh2B 52.30(3) . . ? Rh9B Rh7B Rh2B 35.80(3) 2 . ? Rh1B Rh7B Rh2B 111.42(4) 2 . ? Rh5B Rh7B Rh3B 47.37(5) 2 . ? Rh4B Rh7B Rh3B 106.64(6) 2 . ? C4B' Rh7B Rh3B 128.1(5) 2 . ? C15B Rh7B Rh3B 117.1(2) 2 . ? C59B Rh7B Rh3B 45.33(19) 2 . ? C4B Rh7B Rh3B 125.3(4) 2 . ? PB Rh7B Rh3B 52.04(3) . . ? Rh9B Rh7B Rh3B 33.73(3) 2 . ? Rh1B Rh7B Rh3B 111.82(4) 2 . ? Rh2B Rh7B Rh3B 62.25(3) . . ? Rh5B Rh7B Rh8B 28.02(4) 2 . ? Rh4B Rh7B Rh8B 114.07(6) 2 . ? C4B' Rh7B Rh8B 169.6(5) 2 . ? C15B Rh7B Rh8B 68.6(2) 2 . ? C59B Rh7B Rh8B 86.54(19) 2 . ? C4B Rh7B Rh8B 164.3(3) 2 . ? PB Rh7B Rh8B 52.62(3) . . ? Rh9B Rh7B Rh8B 90.67(4) 2 . ? Rh1B Rh7B Rh8B 57.24(3) 2 . ? Rh2B Rh7B Rh8B 102.41(4) . . ? Rh3B Rh7B Rh8B 59.08(3) . . ? Rh2B Rh8B Rh5B 137.35(7) 2 2 ? Rh2B Rh8B C5B' 145.7(5) 2 2 ? Rh5B Rh8B C5B' 76.8(5) 2 2 ? Rh2B Rh8B C12B 70.6(2) 2 2 ? Rh5B Rh8B C12B 121.4(2) 2 2 ? C5B' Rh8B C12B 94.4(5) 2 2 ? Rh2B Rh8B C48B 62.1(2) 2 . ? Rh5B Rh8B C48B 132.9(2) 2 . ? C5B' Rh8B C48B 94.7(5) 2 . ? C12B Rh8B C48B 105.3(3) 2 . ? Rh2B Rh8B C5B 168.8(4) 2 2 ? Rh5B Rh8B C5B 50.7(3) 2 2 ? C5B' Rh8B C5B 27.2(5) 2 2 ? C12B Rh8B C5B 113.3(4) 2 2 ? C48B Rh8B C5B 106.8(4) . 2 ? Rh2B Rh8B PB 67.98(4) 2 . ? Rh5B Rh8B PB 69.99(4) 2 . ? C5B' Rh8B PB 144.7(4) 2 . ? C12B Rh8B PB 112.9(2) 2 . ? C48B Rh8B PB 98.9(2) . . ? C5B Rh8B PB 117.6(3) 2 . ? Rh2B Rh8B Rh6B 82.56(6) 2 2 ? Rh5B Rh8B Rh6B 83.40(5) 2 2 ? C5B' Rh8B Rh6B 104.3(4) 2 2 ? C12B Rh8B Rh6B 152.2(2) 2 2 ? C48B Rh8B Rh6B 53.4(2) . 2 ? C5B Rh8B Rh6B 91.8(4) 2 2 ? PB Rh8B Rh6B 60.83(3) . 2 ? Rh2B Rh8B Rh1B 78.58(5) 2 2 ? Rh5B Rh8B Rh1B 82.10(5) 2 2 ? C5B' Rh8B Rh1B 115.6(5) 2 2 ? C12B Rh8B Rh1B 49.6(2) 2 2 ? C48B Rh8B Rh1B 139.7(2) . 2 ? C5B Rh8B Rh1B 112.1(4) 2 2 ? PB Rh8B Rh1B 72.02(3) . 2 ? Rh6B Rh8B Rh1B 132.82(4) 2 2 ? Rh2B Rh8B Rh4B 48.07(5) 2 . ? Rh5B Rh8B Rh4B 109.16(6) 2 . ? C5B' Rh8B Rh4B 131.4(5) 2 . ? C12B Rh8B Rh4B 118.3(2) 2 . ? C48B Rh8B Rh4B 44.88(19) . . ? C5B Rh8B Rh4B 125.8(4) 2 . ? PB Rh8B Rh4B 54.07(3) . . ? Rh6B Rh8B Rh4B 34.50(3) 2 . ? Rh1B Rh8B Rh4B 113.02(4) 2 . ? Rh2B Rh8B Rh3B 107.41(6) 2 . ? Rh5B Rh8B Rh3B 47.64(5) 2 . ? C5B' Rh8B Rh3B 95.9(4) 2 . ? C12B Rh8B Rh3B 162.0(2) 2 . ? C48B Rh8B Rh3B 88.6(2) . . ? C5B Rh8B Rh3B 72.3(3) 2 . ? PB Rh8B Rh3B 52.33(3) . . ? Rh6B Rh8B Rh3B 35.98(3) 2 . ? Rh1B Rh8B Rh3B 112.46(4) 2 . ? Rh4B Rh8B Rh3B 63.91(3) . . ? Rh2B Rh8B Rh7B 114.01(6) 2 . ? Rh5B Rh8B Rh7B 27.39(4) 2 . ? C5B' Rh8B Rh7B 99.3(5) 2 . ? C12B Rh8B Rh7B 104.5(2) 2 . ? C48B Rh8B Rh7B 145.8(2) . . ? C5B Rh8B Rh7B 75.8(3) 2 . ? PB Rh8B Rh7B 53.61(3) . . ? Rh6B Rh8B Rh7B 92.80(4) 2 . ? Rh1B Rh8B Rh7B 57.81(3) 2 . ? Rh4B Rh8B Rh7B 105.14(4) . . ? Rh3B Rh8B Rh7B 59.21(3) . . ? Rh3B Rh9B Rh2B 128.47(8) 2 2 ? Rh3B Rh9B C2B' 154.3(5) 2 2 ? Rh2B Rh9B C2B' 77.0(5) 2 2 ? Rh3B Rh9B C13B 69.9(2) 2 2 ? Rh2B Rh9B C13B 118.3(2) 2 2 ? C2B' Rh9B C13B 96.6(5) 2 2 ? Rh3B Rh9B C59B 67.3(2) 2 . ? Rh2B Rh9B C59B 133.2(2) 2 . ? C2B' Rh9B C59B 98.5(5) 2 . ? C13B Rh9B C59B 108.5(3) 2 . ? Rh3B Rh9B C2B 178.2(3) 2 2 ? Rh2B Rh9B C2B 53.1(3) 2 2 ? C2B' Rh9B C2B 24.2(5) 2 2 ? C13B Rh9B C2B 110.2(4) 2 2 ? C59B Rh9B C2B 111.2(4) . 2 ? Rh3B Rh9B PB 65.73(5) 2 . ? Rh2B Rh9B PB 65.03(4) 2 . ? C2B' Rh9B PB 139.4(5) 2 . ? C13B Rh9B PB 113.4(2) 2 . ? C59B Rh9B PB 97.1(2) . . ? C2B Rh9B PB 115.6(3) 2 . ? Rh3B Rh9B Rh7B 84.59(6) 2 2 ? Rh2B Rh9B Rh7B 82.39(5) 2 2 ? C2B' Rh9B Rh7B 104.3(5) 2 2 ? C13B Rh9B Rh7B 153.7(2) 2 2 ? C59B Rh9B Rh7B 53.10(19) . 2 ? C2B Rh9B Rh7B 95.1(4) 2 2 ? PB Rh9B Rh7B 58.31(3) . 2 ? Rh3B Rh9B Rh5B 49.40(5) 2 . ? Rh2B Rh9B Rh5B 108.20(6) 2 . ? C2B' Rh9B Rh5B 132.9(5) 2 . ? C13B Rh9B Rh5B 118.3(2) 2 . ? C59B Rh9B Rh5B 43.1(2) . . ? C2B Rh9B Rh5B 130.1(4) 2 . ? PB Rh9B Rh5B 54.30(3) . . ? Rh7B Rh9B Rh5B 35.50(3) 2 . ? Rh3B Rh9B Rh1B 74.38(5) 2 2 ? Rh2B Rh9B Rh1B 74.95(5) 2 2 ? C2B' Rh9B Rh1B 115.5(5) 2 2 ? C13B Rh9B Rh1B 52.6(2) 2 2 ? C59B Rh9B Rh1B 141.5(2) . 2 ? C2B Rh9B Rh1B 107.1(4) 2 2 ? PB Rh9B Rh1B 69.08(3) . 2 ? Rh7B Rh9B Rh1B 127.39(4) 2 2 ? Rh5B Rh9B Rh1B 110.82(4) . 2 ? Rh3B Rh9B Rh4B 108.80(6) 2 . ? Rh2B Rh9B Rh4B 46.95(5) 2 . ? C2B' Rh9B Rh4B 90.9(5) 2 . ? C13B Rh9B Rh4B 161.3(2) 2 . ? C59B Rh9B Rh4B 87.2(2) . . ? C2B Rh9B Rh4B 71.7(4) 2 . ? PB Rh9B Rh4B 52.72(3) . . ? Rh7B Rh9B Rh4B 35.53(3) 2 . ? Rh5B Rh9B Rh4B 66.28(4) . . ? Rh1B Rh9B Rh4B 108.74(4) 2 . ? Rh3B Rh9B Rh8B 107.69(6) 2 . ? Rh2B Rh9B Rh8B 22.85(4) 2 . ? C2B' Rh9B Rh8B 96.7(5) 2 . ? C13B Rh9B Rh8B 104.9(2) 2 . ? C59B Rh9B Rh8B 141.1(2) . . ? C2B Rh9B Rh8B 74.0(3) 2 . ? PB Rh9B Rh8B 50.66(2) . . ? Rh7B Rh9B Rh8B 88.51(4) 2 . ? Rh5B Rh9B Rh8B 102.84(4) . . ? Rh1B Rh9B Rh8B 55.15(3) 2 . ? Rh4B Rh9B Rh8B 57.00(3) . . ? Rh3B PB Rh3B 180.000(12) 2 . ? Rh3B PB Rh2B 102.73(3) 2 . ? Rh3B PB Rh2B 77.27(3) . . ? Rh3B PB Rh2B 77.27(3) 2 2 ? Rh3B PB Rh2B 102.73(3) . 2 ? Rh2B PB Rh2B 180.00(5) . 2 ? Rh3B PB Rh4B 101.92(3) 2 . ? Rh3B PB Rh4B 78.08(3) . . ? Rh2B PB Rh4B 127.35(3) . . ? Rh2B PB Rh4B 52.65(3) 2 . ? Rh3B PB Rh4B 78.08(3) 2 2 ? Rh3B PB Rh4B 101.92(3) . 2 ? Rh2B PB Rh4B 52.65(3) . 2 ? Rh2B PB Rh4B 127.35(3) 2 2 ? Rh4B PB Rh4B 180.00(5) . 2 ? Rh3B PB Rh8B 73.25(3) 2 2 ? Rh3B PB Rh8B 106.75(3) . 2 ? Rh2B PB Rh8B 39.84(3) . 2 ? Rh2B PB Rh8B 140.16(3) 2 2 ? Rh4B PB Rh8B 108.52(3) . 2 ? Rh4B PB Rh8B 71.48(3) 2 2 ? Rh3B PB Rh8B 106.75(3) 2 . ? Rh3B PB Rh8B 73.25(3) . . ? Rh2B PB Rh8B 140.16(3) . . ? Rh2B PB Rh8B 39.84(3) 2 . ? Rh4B PB Rh8B 71.48(3) . . ? Rh4B PB Rh8B 108.52(3) 2 . ? Rh8B PB Rh8B 180.00(6) 2 . ? Rh3B PB Rh5B 127.35(3) 2 2 ? Rh3B PB Rh5B 52.65(3) . 2 ? Rh2B PB Rh5B 100.06(3) . 2 ? Rh2B PB Rh5B 79.94(3) 2 2 ? Rh4B PB Rh5B 100.61(3) . 2 ? Rh4B PB Rh5B 79.39(3) 2 2 ? Rh8B PB Rh5B 139.70(3) 2 2 ? Rh8B PB Rh5B 40.30(3) . 2 ? Rh3B PB Rh5B 52.65(3) 2 . ? Rh3B PB Rh5B 127.35(3) . . ? Rh2B PB Rh5B 79.94(3) . . ? Rh2B PB Rh5B 100.06(3) 2 . ? Rh4B PB Rh5B 79.39(3) . . ? Rh4B PB Rh5B 100.61(3) 2 . ? Rh8B PB Rh5B 40.30(3) 2 . ? Rh8B PB Rh5B 139.70(3) . . ? Rh5B PB Rh5B 180.00(4) 2 . ? Rh3B PB Rh7B 107.21(3) 2 . ? Rh3B PB Rh7B 72.79(3) . . ? Rh2B PB Rh7B 72.30(3) . . ? Rh2B PB Rh7B 107.70(3) 2 . ? Rh4B PB Rh7B 139.66(3) . . ? Rh4B PB Rh7B 40.34(3) 2 . ? Rh8B PB Rh7B 106.23(3) 2 . ? Rh8B PB Rh7B 73.77(3) . . ? Rh5B PB Rh7B 39.16(3) 2 . ? Rh5B PB Rh7B 140.84(3) . . ? Rh3B PB Rh7B 72.79(3) 2 2 ? Rh3B PB Rh7B 107.21(3) . 2 ? Rh2B PB Rh7B 107.70(3) . 2 ? Rh2B PB Rh7B 72.30(3) 2 2 ? Rh4B PB Rh7B 40.34(3) . 2 ? Rh4B PB Rh7B 139.66(3) 2 2 ? Rh8B PB Rh7B 73.77(3) 2 2 ? Rh8B PB Rh7B 106.23(3) . 2 ? Rh5B PB Rh7B 140.84(3) 2 2 ? Rh5B PB Rh7B 39.16(3) . 2 ? Rh7B PB Rh7B 180.00(6) . 2 ? O1B C1B Rh1B 178.1(7) . . ? C2B C2B' O2B 65.9(7) . . ? C2B C2B' Rh9B 102.8(10) . 2 ? O2B C2B' Rh9B 168.1(12) . 2 ? C2B C2B' Rh2B 55.2(8) . . ? O2B C2B' Rh2B 121.0(10) . . ? Rh9B C2B' Rh2B 48.2(3) 2 . ? C2B' C2B O2B 67.7(8) . . ? C2B' C2B Rh2B 99.7(11) . . ? O2B C2B Rh2B 166.9(13) . . ? C2B' C2B Rh9B 53.0(8) . 2 ? O2B C2B Rh9B 120.6(11) . 2 ? Rh2B C2B Rh9B 47.2(3) . 2 ? C2B O2B C2B' 46.4(9) . . ? C3B C3B' O3B 76.8(10) . . ? C3B C3B' Rh6B 90.2(12) . 2 ? O3B C3B' Rh6B 165.0(14) . 2 ? C3B C3B' Rh3B 45.9(9) . . ? O3B C3B' Rh3B 122.4(11) . . ? Rh6B C3B' Rh3B 45.9(3) 2 . ? C3B' C3B O3B 63.3(7) . . ? C3B' C3B Rh3B 115.9(13) . . ? O3B C3B Rh3B 174.7(12) . . ? C3B' C3B Rh6B 65.4(11) . 2 ? O3B C3B Rh6B 128.3(11) . 2 ? Rh3B C3B Rh6B 52.1(3) . 2 ? C3B' O3B C3B 39.9(9) . . ? C4B C4B' O4B 64.8(7) . . ? C4B C4B' Rh7B 109.2(12) . 2 ? O4B C4B' Rh7B 173.7(14) . 2 ? C4B C4B' Rh4B 59.6(9) . . ? O4B C4B' Rh4B 124.3(11) . . ? Rh7B C4B' Rh4B 50.0(3) 2 . ? C4B' C4B O4B 70.3(8) . . ? C4B' C4B Rh4B 94.6(11) . . ? O4B C4B Rh4B 164.4(14) . . ? C4B' C4B Rh7B 48.9(9) . 2 ? O4B C4B Rh7B 119.1(11) . 2 ? Rh4B C4B Rh7B 46.0(3) . 2 ? C4B O4B C4B' 44.9(9) . . ? C5B' C5B O5B 64.0(7) . . ? C5B' C5B Rh5B 93.3(9) . . ? O5B C5B Rh5B 156.4(12) . . ? C5B' C5B Rh8B 49.9(7) . 2 ? O5B C5B Rh8B 113.6(10) . 2 ? Rh5B C5B Rh8B 44.9(3) . 2 ? C5B C5B' O5B 61.9(7) . . ? C5B C5B' Rh8B 102.9(9) . 2 ? O5B C5B' Rh8B 163.7(12) . 2 ? C5B C5B' Rh5B 56.6(7) . . ? O5B C5B' Rh5B 118.2(10) . . ? Rh8B C5B' Rh5B 47.9(3) 2 . ? C5B O5B C5B' 54.1(10) . . ? O12B C12B Rh8B 136.2(7) . 2 ? O12B C12B Rh2B 128.7(6) . . ? Rh8B C12B Rh2B 48.46(18) 2 . ? O12B C12B Rh1B 134.9(6) . . ? Rh8B C12B Rh1B 86.1(3) 2 . ? Rh2B C12B Rh1B 88.5(3) . . ? O13B C13B Rh9B 138.0(7) . 2 ? O13B C13B Rh3B 139.5(6) . . ? Rh9B C13B Rh3B 47.62(18) 2 . ? O13B C13B Rh1B 131.3(6) . . ? Rh9B C13B Rh1B 84.9(3) 2 . ? Rh3B C13B Rh1B 83.1(3) . . ? O14B C14B Rh6B 139.1(7) . 2 ? O14B C14B Rh4B 137.4(7) . . ? Rh6B C14B Rh4B 48.4(2) 2 . ? O14B C14B Rh1B 129.7(7) . . ? Rh6B C14B Rh1B 85.0(3) 2 . ? Rh4B C14B Rh1B 86.6(3) . . ? O15B C15B Rh7B 143.6(7) . 2 ? O15B C15B Rh5B 132.9(6) . . ? Rh7B C15B Rh5B 49.25(19) 2 . ? O15B C15B Rh1B 131.0(6) . . ? Rh7B C15B Rh1B 81.3(3) 2 . ? Rh5B C15B Rh1B 87.4(3) . . ? O48B C48B Rh2B 137.7(6) . 2 ? O48B C48B Rh4B 137.4(6) . . ? Rh2B C48B Rh4B 65.6(2) 2 . ? O48B C48B Rh8B 133.3(6) . . ? Rh2B C48B Rh8B 48.86(17) 2 . ? Rh4B C48B Rh8B 89.4(3) . . ? O48B C48B Rh6B 132.7(6) . 2 ? Rh2B C48B Rh6B 89.5(3) 2 2 ? Rh4B C48B Rh6B 46.38(16) . 2 ? Rh8B C48B Rh6B 75.7(2) . 2 ? O59B C59B Rh5B 135.6(6) . . ? O59B C59B Rh9B 134.0(6) . . ? Rh5B C59B Rh9B 90.3(3) . . ? O59B C59B Rh3B 139.6(6) . 2 ? Rh5B C59B Rh3B 65.2(2) . 2 ? Rh9B C59B Rh3B 46.29(16) . 2 ? O59B C59B Rh7B 132.4(6) . 2 ? Rh5B C59B Rh7B 48.25(17) . 2 ? Rh9B C59B Rh7B 76.0(2) . 2 ? Rh3B C59B Rh7B 87.9(3) 2 2 ? N1 P1 C131 108.2(3) . . ? N1 P1 C121 115.0(3) . . ? C131 P1 C121 105.0(3) . . ? N1 P1 C111 111.1(3) . . ? C131 P1 C111 107.2(3) . . ? C121 P1 C111 109.9(3) . . ? N1 P2 C211 107.5(3) . . ? N1 P2 C221 110.8(3) . . ? C211 P2 C221 109.0(3) . . ? N1 P2 C231 115.3(3) . . ? C211 P2 C231 104.5(3) . . ? C221 P2 C231 109.3(3) . . ? P1 N1 P2 138.7(4) . . ? C112 C111 C116 119.1(7) . . ? C112 C111 P1 123.5(5) . . ? C116 C111 P1 117.4(5) . . ? C111 C112 C113 119.7(8) . . ? C114 C113 C112 120.4(9) . . ? C113 C114 C115 120.4(9) . . ? C116 C115 C114 119.4(8) . . ? C115 C116 C111 121.0(8) . . ? C122 C121 C126 118.9(7) . . ? C122 C121 P1 120.4(5) . . ? C126 C121 P1 120.6(5) . . ? C121 C122 C123 120.3(8) . . ? C124 C123 C122 120.1(9) . . ? C123 C124 C125 120.1(10) . . ? C126 C125 C124 120.1(9) . . ? C125 C126 C121 120.5(7) . . ? C136 C131 C132 118.9(6) . . ? C136 C131 P1 120.7(5) . . ? C132 C131 P1 120.3(5) . . ? C133 C132 C131 120.8(7) . . ? C134 C133 C132 119.8(8) . . ? C133 C134 C135 121.4(9) . . ? C134 C135 C136 118.6(8) . . ? C131 C136 C135 120.7(7) . . ? C212 C211 C216 119.4(7) . . ? C212 C211 P2 120.6(6) . . ? C216 C211 P2 119.9(5) . . ? C211 C212 C213 119.0(8) . . ? C214 C213 C212 118.4(10) . . ? C215 C214 C213 123.0(10) . . ? C214 C215 C216 119.8(9) . . ? C215 C216 C211 120.4(8) . . ? C226 C221 C222 119.7(8) . . ? C226 C221 P2 117.9(6) . . ? C222 C221 P2 122.3(6) . . ? C221 C222 C223 120.4(10) . . ? C224 C223 C222 117.3(12) . . ? C225 C224 C223 122.5(12) . . ? C224 C225 C226 120.4(10) . . ? C221 C226 C225 119.6(9) . . ? C236 C231 C232 119.1(7) . . ? C236 C231 P2 123.0(6) . . ? C232 C231 P2 117.9(6) . . ? C231 C232 C233 120.6(8) . . ? C234 C233 C232 118.6(10) . . ? C235 C234 C233 121.0(11) . . ? C234 C235 C236 120.7(10) . . ? C231 C236 C235 120.1(8) . . ? N2 P3 C321 114.7(3) . . ? N2 P3 C311 113.6(3) . . ? C321 P3 C311 107.1(3) . . ? N2 P3 C331 106.0(3) . . ? C321 P3 C331 107.4(3) . . ? C311 P3 C331 107.7(3) . . ? N2 P4 C431 107.1(3) . . ? N2 P4 C421 111.1(3) . . ? C431 P4 C421 108.5(3) . . ? N2 P4 C411 113.7(3) . . ? C431 P4 C411 105.9(3) . . ? C421 P4 C411 110.2(3) . . ? P3 N2 P4 148.0(4) . . ? C312 C311 C316 119.5(8) . . ? C312 C311 P3 122.0(6) . . ? C316 C311 P3 118.4(6) . . ? C311 C312 C313 118.5(10) . . ? C314 C313 C312 120.4(12) . . ? C313 C314 C315 121.7(12) . . ? C314 C315 C316 119.3(11) . . ? C311 C316 C315 120.4(9) . . ? C322 C321 C326 118.2(8) . . ? C322 C321 P3 122.0(6) . . ? C326 C321 P3 119.7(6) . . ? C321 C322 C323 120.3(9) . . ? C324 C323 C322 119.9(11) . . ? C325 C324 C323 121.0(11) . . ? C324 C325 C326 120.0(11) . . ? C321 C326 C325 120.5(10) . . ? C336 C331 C332 121.5(8) . . ? C336 C331 P3 117.7(6) . . ? C332 C331 P3 120.8(6) . . ? C331 C332 C333 117.8(9) . . ? C334 C333 C332 118.8(11) . . ? C335 C334 C333 124.5(12) . . ? C334 C335 C336 118.4(11) . . ? C331 C336 C335 119.0(9) . . ? C416 C411 C412 119.2(7) . . ? C416 C411 P4 116.9(6) . . ? C412 C411 P4 123.7(6) . . ? C411 C412 C413 119.1(9) . . ? C414 C413 C412 120.7(11) . . ? C413 C414 C415 121.1(11) . . ? C414 C415 C416 119.0(10) . . ? C411 C416 C415 120.9(8) . . ? C426 C421 C422 119.1(7) . . ? C426 C421 P4 123.3(6) . . ? C422 C421 P4 117.6(6) . . ? C423 C422 C421 119.6(8) . . ? C424 C423 C422 119.9(10) . . ? C425 C424 C423 121.0(10) . . ? C424 C425 C426 120.0(10) . . ? C421 C426 C425 120.4(9) . . ? C436 C431 C432 118.8(7) . . ? C436 C431 P4 120.8(6) . . ? C432 C431 P4 120.3(6) . . ? C431 C432 C433 120.6(8) . . ? C434 C433 C432 118.5(10) . . ? C433 C434 C435 123.7(11) . . ? C434 C435 C436 118.7(10) . . ? C431 C436 C435 119.7(8) . . ? N3 P5 C521 111.0(2) . . ? N3 P5 C511 113.1(2) . . ? C521 P5 C511 106.7(3) . . ? N3 P5 C531 110.8(3) . . ? C521 P5 C531 108.1(3) . . ? C511 P5 C531 106.8(4) . . ? P5 N3 P5 180.0 . 2_556 ? C512 C511 C516 120.0(7) . . ? C512 C511 P5 119.2(6) . . ? C516 C511 P5 120.6(6) . . ? C511 C512 C513 119.6(9) . . ? C514 C513 C512 118.9(10) . . ? C515 C514 C513 123.2(10) . . ? C514 C515 C516 119.0(10) . . ? C511 C516 C515 119.3(8) . . ? C522 C521 C526 119.8(7) . . ? C522 C521 P5 122.1(6) . . ? C526 C521 P5 118.0(6) . . ? C521 C522 C523 119.4(8) . . ? C524 C523 C522 119.9(9) . . ? C525 C524 C523 120.9(10) . . ? C524 C525 C526 120.4(10) . . ? C525 C526 C521 119.6(8) . . ? C532 C531 C536 120.5(9) . . ? C532 C531 P5 120.3(7) . . ? C536 C531 P5 119.2(7) . . ? C531 C532 C533 120.3(10) . . ? C534 C533 C532 117.6(12) . . ? C535 C534 C533 124.0(13) . . ? C534 C535 C536 120.8(13) . . ? C531 C536 C535 116.7(10) . . ? N4 P6 C611 112.9(2) . . ? N4 P6 C621 111.1(2) . . ? C611 P6 C621 106.5(3) . . ? N4 P6 C631 110.5(2) . . ? C611 P6 C631 107.2(3) . . ? C621 P6 C631 108.6(3) . . ? P6 N4 P6 180.00(13) 2_665 . ? C616 C611 C612 118.1(8) . . ? C616 C611 P6 122.1(6) . . ? C612 C611 P6 119.8(6) . . ? C611 C612 C613 118.6(10) . . ? C614 C613 C612 122.4(12) . . ? C613 C614 C615 120.5(12) . . ? C614 C615 C616 118.3(10) . . ? C611 C616 C615 122.0(9) . . ? C626 C621 C622 118.7(7) . . ? C626 C621 P6 119.3(5) . . ? C622 C621 P6 121.9(5) . . ? C623 C622 C621 119.8(7) . . ? C624 C623 C622 120.5(8) . . ? C625 C624 C623 120.7(9) . . ? C624 C625 C626 119.6(8) . . ? C621 C626 C625 120.8(7) . . ? C632 C631 C636 119.6(7) . . ? C632 C631 P6 119.5(6) . . ? C636 C631 P6 120.9(6) . . ? C631 C632 C633 119.5(8) . . ? C634 C633 C632 119.5(10) . . ? C633 C634 C635 123.2(11) . . ? C634 C635 C636 119.0(10) . . ? C631 C636 C635 119.1(8) . . ? _diffrn_measured_fraction_theta_max 0.878 _diffrn_reflns_theta_full 27.33 _diffrn_measured_fraction_theta_full 0.878 _refine_diff_density_max 1.407 _refine_diff_density_min -1.102 _refine_diff_density_rms 0.117