Additions and corrections
2D and 3D lanthanide coordination polymers
constructed from benzimidazole-5,6-dicarboxylic acid
and sulfate bridged secondary building units
Zhao-Xi
Wang,
Qiong-Fang Wu,
Hong-Jiang Liu, Min
Shao, Hong-Ping
Xiao and Ming-Xing Li
CrystEngComm, 2010, 12, 1139 (DOI: 10.1039/b910701k). Amendment published 1st November 2010
The crystallographic data for 5–8 contained errors (Table 2, p. 1141).
The corrected crystallographic data for 5–8 are as follows:
Complexes |
5 |
6 |
7 |
8 |
Formula |
C18H10N4O13SEu2 |
C18H10N4O13STb2 |
C18H10N4O13SDy2 |
C18H10N4O13Ser2 |
Formula weight
|
826.28 |
872.26 |
847.36 |
856.88 |
|
Monoclinic |
Monoclinic |
Monoclinic |
Monoclinic |
Space group |
P 21/c |
P 21/c |
P 21/c |
P 21/c |
a/Å |
9.5725(6) |
9.5506(9) |
9.5378(8) |
9.512(3) |
b/Å |
6.7130(5) |
6.6934(6) |
6.6828(5) |
6.658(2) |
c/Å |
16.2444(11) |
16.1734(14) |
16.1310(13) |
16.071(5) |
β/° |
96.9130(10) |
96.7540(10) |
96.7490(10) |
96.666(4) |
V/Å3 |
1036.28(12) |
1026.73(16) |
1021.05(14) |
1011.0(6) |
Z |
2 |
2 |
2 |
2 |
Dc/g cm-3 |
2.648 |
2.821 |
2.756 |
2.815 |
μ/mm-1 |
6.185 |
7.125 |
7.452 |
8.437 |
F(000) |
784 |
824 |
796 |
804 |
Reflections
collected / unique |
5374 / 1911 |
5298 / 1901 |
5263 / 1876 |
4962 / 1873 |
Data/restraints/
parameters |
1911 / 0 / 190 |
1901 / 0 / 190 |
1876 / 0 / 190 |
1873 / 31 / 190 |
GOF (F2) |
1.184 |
1.109 |
1.167 |
1.118 |
R |
0.0633 |
0.0644 |
0.0443 |
0.0614 |
wR2b[I > 2σ(I)] |
0.1542 |
0.1682 |
0.1049 |
0.1648 |
a R1 = Σ||Fo|–|Fc||/Σ|Fo|. b wR2 = [Σw(|Fo2|–|Fc2|)2/Σw(|Fo2|2]1/2
The Royal Society of Chemistry apologises for this error and any consequent inconvenience to authors and readers.