# Electronic Supplementary Material (ESI) for ChemComm.
# This journal is © The Royal Society of Chemistry 2020

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_shelx
_database_code_depnum_ccdc_archive 'CCDC 1986098'
loop_
_audit_author_name
_audit_author_address
'Won-Sik Han'
;Seoul Womens University
South Korea
;
_audit_update_record             
;
2020-02-25 deposited with the CCDC.	2020-09-10 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-2014/7
_shelx_SHELXL_version_number     2014/7
_chemical_name_systematic        ?
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'C16 H20 B10'
_chemical_formula_weight         320.42

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_H-M_alt        'P -1'
_space_group_name_Hall           '-P 1'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;

loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'

_cell_length_a                   7.2684(6)
_cell_length_b                   10.4070(10)
_cell_length_c                   12.7741(13)
_cell_angle_alpha                74.227(3)
_cell_angle_beta                 81.330(3)
_cell_angle_gamma                86.111(3)
_cell_volume                     918.89(15)
_cell_formula_units_Z            2
_cell_measurement_temperature    223(2)
_cell_measurement_reflns_used    6278
_cell_measurement_theta_min      2.826
_cell_measurement_theta_max      27.9765

_exptl_crystal_description       Block
_exptl_crystal_colour            Colourless
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_density_diffrn    1.158
_exptl_crystal_F_000             332
_exptl_transmission_factor_min   ?
_exptl_transmission_factor_max   ?
_exptl_crystal_size_max          0.220
_exptl_crystal_size_mid          0.160
_exptl_crystal_size_min          0.090
_exptl_absorpt_coefficient_mu    0.057
_shelx_estimated_absorpt_T_min   0.988
_shelx_estimated_absorpt_T_max   0.995
_exptl_absorpt_correction_type   Multi-scan
_exptl_absorpt_correction_T_min  0.941
_exptl_absorpt_correction_T_max  0.995
_exptl_absorpt_process_details   'Bruker SADABS'
_exptl_absorpt_special_details   ?
_diffrn_ambient_temperature      223(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_source                   ?
_diffrn_measurement_device_type  'PHOTON 100 CMOS'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_detector_area_resol_mean ?
_diffrn_reflns_number            29616
_diffrn_reflns_av_unetI/netI     0.0517
_diffrn_reflns_av_R_equivalents  0.0798
_diffrn_reflns_limit_h_min       -9
_diffrn_reflns_limit_h_max       9
_diffrn_reflns_limit_k_min       -13
_diffrn_reflns_limit_k_max       13
_diffrn_reflns_limit_l_min       -17
_diffrn_reflns_limit_l_max       17
_diffrn_reflns_theta_min         2.265
_diffrn_reflns_theta_max         28.426
_diffrn_reflns_theta_full        25.242
_diffrn_measured_fraction_theta_max 0.997
_diffrn_measured_fraction_theta_full 0.999
_diffrn_reflns_Laue_measured_fraction_max 0.997
_diffrn_reflns_Laue_measured_fraction_full 0.999
_diffrn_reflns_point_group_measured_fraction_max 0.997
_diffrn_reflns_point_group_measured_fraction_full 0.999
_reflns_number_total             4611
_reflns_number_gt                2892
_reflns_threshold_expression     'I > 2σ(I)'
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_max     .
_reflns_Friedel_fraction_full    .

_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;

_computing_data_collection       'Bruker APEX2'
_computing_cell_refinement       'Bruker SAINT'
_computing_data_reduction        'Bruker SAINT'
_computing_structure_solution    'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_refine_special_details          ?
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0569P)²+0.4248P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    constr
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       .
_refine_ls_number_reflns         4611
_refine_ls_number_parameters     235
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.1110
_refine_ls_R_factor_gt           0.0597
_refine_ls_wR_factor_ref         0.1559
_refine_ls_wR_factor_gt          0.1319
_refine_ls_goodness_of_fit_ref   1.035
_refine_ls_restrained_S_all      1.035
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
C1 C 0.1737(2) 0.20673(17) 0.68239(14) 0.0283(4) Uani 1 1 d . . . . .
C2 C 0.3188(3) 0.13392(17) 0.77674(15) 0.0311(4) Uani 1 1 d . . . . .
C3 C 0.1749(2) 0.35651(17) 0.63882(15) 0.0287(4) Uani 1 1 d . . . . .
C4 C 0.2488(3) 0.41271(19) 0.53042(16) 0.0380(5) Uani 1 1 d . . . . .
H4 H 0.2954 0.3571 0.4850 0.046 Uiso 1 1 calc R U . . .
C5 C 0.2546(3) 0.5500(2) 0.48868(18) 0.0433(5) Uani 1 1 d . . . . .
H5 H 0.3035 0.5871 0.4149 0.052 Uiso 1 1 calc R U . . .
C6 C 0.1890(3) 0.63239(19) 0.55502(18) 0.0412(5) Uani 1 1 d . . . . .
H6 H 0.1951 0.7256 0.5270 0.049 Uiso 1 1 calc R U . . .
C7 C 0.1150(3) 0.57806(19) 0.66185(18) 0.0412(5) Uani 1 1 d . . . . .
H7 H 0.0696 0.6345 0.7068 0.049 Uiso 1 1 calc R U . . .
C8 C 0.1062(3) 0.44038(18) 0.70468(16) 0.0359(4) Uani 1 1 d . . . . .
H8 H 0.0539 0.4041 0.7780 0.043 Uiso 1 1 calc R U . . .
C9 C 0.4243(3) 0.22575(18) 0.80859(15) 0.0350(4) Uani 1 1 d . . . . .
C10 C 0.5041(3) 0.30934(18) 0.82969(15) 0.0337(4) Uani 1 1 d . . . . .
C11 C 0.5955(2) 0.41407(18) 0.85338(15) 0.0313(4) Uani 1 1 d . . . . .
C12 C 0.5904(3) 0.54313(19) 0.78468(18) 0.0415(5) Uani 1 1 d . . . . .
H12 H 0.5297 0.5617 0.7220 0.050 Uiso 1 1 calc R U . . .
C13 C 0.6758(3) 0.6439(2) 0.8099(2) 0.0556(7) Uani 1 1 d . . . . .
H13 H 0.6741 0.7312 0.7637 0.067 Uiso 1 1 calc R U . . .
C14 C 0.7633(3) 0.6168(2) 0.9024(2) 0.0587(7) Uani 1 1 d . . . . .
H14 H 0.8208 0.6858 0.9189 0.070 Uiso 1 1 calc R U . . .
C15 C 0.7670(3) 0.4897(2) 0.9703(2) 0.0511(6) Uani 1 1 d . . . . .
H15 H 0.8259 0.4721 1.0336 0.061 Uiso 1 1 calc R U . . .
C16 C 0.6850(3) 0.3881(2) 0.94620(17) 0.0389(5) Uani 1 1 d . . . . .
H16 H 0.6893 0.3009 0.9924 0.047 Uiso 1 1 calc R U . . .
B1 B 0.0814(3) 0.1365(2) 0.81822(18) 0.0343(5) Uani 1 1 d . . . . .
H1 H 0.0105 0.1959 0.8736 0.041 Uiso 1 1 calc R U . . .
B2 B 0.2253(3) -0.0065(2) 0.86638(19) 0.0388(5) Uani 1 1 d . . . . .
H2 H 0.2467 -0.0420 0.9539 0.047 Uiso 1 1 calc R U . . .
B3 B 0.4078(3) -0.0154(2) 0.7587(2) 0.0385(5) Uani 1 1 d . . . . .
H3 H 0.5484 -0.0565 0.7760 0.046 Uiso 1 1 calc R U . . .
B4 B 0.3764(3) 0.1219(2) 0.64381(18) 0.0326(5) Uani 1 1 d . . . . .
H4A H 0.4963 0.1718 0.5862 0.039 Uiso 1 1 calc R U . . .
B5 B 0.1623(3) 0.1046(2) 0.59965(18) 0.0341(5) Uani 1 1 d . . . . .
H5A H 0.1420 0.1419 0.5120 0.041 Uiso 1 1 calc R U . . .
B6 B 0.3065(3) -0.0380(2) 0.64707(19) 0.0381(5) Uani 1 1 d . . . . .
H6A H 0.3802 -0.0952 0.5907 0.046 Uiso 1 1 calc R U . . .
B7 B 0.2122(3) -0.1174(2) 0.78443(19) 0.0396(5) Uani 1 1 d . . . . .
H7A H 0.2237 -0.2273 0.8182 0.047 Uiso 1 1 calc R U . . .
B8 B 0.0110(3) -0.0233(2) 0.82208(19) 0.0395(5) Uani 1 1 d . . . . .
H8A H -0.1091 -0.0712 0.8808 0.047 Uiso 1 1 calc R U . . .
B9 B -0.0208(3) 0.1138(2) 0.70741(19) 0.0363(5) Uani 1 1 d . . . . .
H9 H -0.1608 0.1567 0.6907 0.044 Uiso 1 1 calc R U . . .
B10 B 0.0606(3) -0.0439(2) 0.68665(19) 0.0385(5) Uani 1 1 d . . . . .
H10 H -0.0270 -0.1056 0.6564 0.046 Uiso 1 1 calc R U . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
C1 C3 1.506(2) . ?
C1 B5 1.703(3) . ?
C1 C2 1.708(3) . ?
C1 B9 1.708(3) . ?
C1 B1 1.738(3) . ?
C1 B4 1.742(3) . ?
C2 C9 1.440(2) . ?
C2 B2 1.702(3) . ?
C2 B3 1.703(3) . ?
C2 B4 1.723(3) . ?
C2 B1 1.727(3) . ?
C3 C4 1.388(3) . ?
C3 C8 1.390(3) . ?
C4 C5 1.384(3) . ?
C5 C6 1.378(3) . ?
C6 C7 1.368(3) . ?
C7 C8 1.390(3) . ?
C9 C10 1.187(2) . ?
C10 C11 1.435(2) . ?
C11 C16 1.392(3) . ?
C11 C12 1.392(3) . ?
C12 C13 1.386(3) . ?
C13 C14 1.378(4) . ?
C14 C15 1.372(3) . ?
C15 C16 1.374(3) . ?
B1 B8 1.760(3) . ?
B1 B9 1.771(3) . ?
B1 B2 1.781(3) . ?
B2 B8 1.771(3) . ?
B2 B7 1.772(3) . ?
B2 B3 1.778(3) . ?
B3 B7 1.770(3) . ?
B3 B6 1.777(3) . ?
B3 B4 1.779(3) . ?
B4 B6 1.761(3) . ?
B4 B5 1.769(3) . ?
B5 B10 1.773(3) . ?
B5 B6 1.777(3) . ?
B5 B9 1.783(3) . ?
B6 B7 1.777(3) . ?
B6 B10 1.783(3) . ?
B7 B10 1.772(3) . ?
B7 B8 1.783(3) . ?
B8 B9 1.777(3) . ?
B8 B10 1.781(3) . ?
B9 B10 1.781(3) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C3 C1 B5 122.00(15) . . ?
C3 C1 C2 117.66(14) . . ?
B5 C1 C2 108.87(14) . . ?
C3 C1 B9 124.21(15) . . ?
B5 C1 B9 63.00(12) . . ?
C2 C1 B9 109.17(14) . . ?
C3 C1 B1 119.20(15) . . ?
B5 C1 B1 112.98(14) . . ?
C2 C1 B1 60.17(11) . . ?
B9 C1 B1 61.82(12) . . ?
C3 C1 B4 115.62(14) . . ?
B5 C1 B4 61.77(12) . . ?
C2 C1 B4 59.92(11) . . ?
B9 C1 B4 113.14(14) . . ?
B1 C1 B4 111.61(14) . . ?
C9 C2 B2 123.29(16) . . ?
C9 C2 B3 123.12(16) . . ?
B2 C2 B3 62.96(13) . . ?
C9 C2 C1 114.96(14) . . ?
B2 C2 C1 111.07(14) . . ?
B3 C2 C1 111.33(14) . . ?
C9 C2 B4 116.19(15) . . ?
B2 C2 B4 114.14(14) . . ?
B3 C2 B4 62.58(12) . . ?
C1 C2 B4 61.02(11) . . ?
C9 C2 B1 116.15(16) . . ?
B2 C2 B1 62.57(13) . . ?
B3 C2 B1 114.34(14) . . ?
C1 C2 B1 60.78(11) . . ?
B4 C2 B1 113.06(14) . . ?
C4 C3 C8 118.93(17) . . ?
C4 C3 C1 119.27(16) . . ?
C8 C3 C1 121.80(16) . . ?
C5 C4 C3 120.54(19) . . ?
C6 C5 C4 120.16(19) . . ?
C7 C6 C5 119.77(18) . . ?
C6 C7 C8 120.77(19) . . ?
C7 C8 C3 119.82(18) . . ?
C10 C9 C2 174.9(2) . . ?
C9 C10 C11 177.8(2) . . ?
C16 C11 C12 119.83(17) . . ?
C16 C11 C10 120.37(17) . . ?
C12 C11 C10 119.79(18) . . ?
C13 C12 C11 119.1(2) . . ?
C14 C13 C12 120.4(2) . . ?
C15 C14 C13 120.3(2) . . ?
C14 C15 C16 120.2(2) . . ?
C15 C16 C11 120.1(2) . . ?
C2 B1 C1 59.05(11) . . ?
C2 B1 B8 104.57(15) . . ?
C1 B1 B8 105.39(15) . . ?
C2 B1 B9 105.47(15) . . ?
C1 B1 B9 58.26(11) . . ?
B8 B1 B9 60.43(13) . . ?
C2 B1 B2 58.03(12) . . ?
C1 B1 B2 106.05(15) . . ?
B8 B1 B2 60.00(13) . . ?
B9 B1 B2 108.41(16) . . ?
C2 B2 B8 105.16(15) . . ?
C2 B2 B7 104.65(15) . . ?
B8 B2 B7 60.43(13) . . ?
C2 B2 B3 58.52(12) . . ?
B8 B2 B3 108.31(16) . . ?
B7 B2 B3 59.81(13) . . ?
C2 B2 B1 59.40(11) . . ?
B8 B2 B1 59.39(13) . . ?
B7 B2 B1 107.68(16) . . ?
B3 B2 B1 108.14(15) . . ?
C2 B3 B7 104.72(16) . . ?
C2 B3 B6 105.10(16) . . ?
B7 B3 B6 60.14(13) . . ?
C2 B3 B2 58.52(12) . . ?
B7 B3 B2 59.92(13) . . ?
B6 B3 B2 108.08(17) . . ?
C2 B3 B4 59.27(11) . . ?
B7 B3 B4 107.37(16) . . ?
B6 B3 B4 59.36(12) . . ?
B2 B3 B4 107.86(16) . . ?
C2 B4 C1 59.07(11) . . ?
C2 B4 B6 104.93(15) . . ?
C1 B4 B6 105.60(15) . . ?
C2 B4 B5 105.26(15) . . ?
C1 B4 B5 58.05(11) . . ?
B6 B4 B5 60.48(12) . . ?
C2 B4 B3 58.15(12) . . ?
C1 B4 B3 106.23(15) . . ?
B6 B4 B3 60.26(13) . . ?
B5 B4 B3 108.45(15) . . ?
C1 B5 B4 60.18(11) . . ?
C1 B5 B10 105.72(15) . . ?
B4 B5 B10 107.78(16) . . ?
C1 B5 B6 106.51(15) . . ?
B4 B5 B6 59.53(12) . . ?
B10 B5 B6 60.27(13) . . ?
C1 B5 B9 58.63(11) . . ?
B4 B5 B9 108.34(15) . . ?
B10 B5 B9 60.11(13) . . ?
B6 B5 B9 108.50(16) . . ?
B4 B6 B3 60.39(12) . . ?
B4 B6 B7 107.87(15) . . ?
B3 B6 B7 59.74(13) . . ?
B4 B6 B5 59.99(12) . . ?
B3 B6 B5 108.17(15) . . ?
B7 B6 B5 107.54(16) . . ?
B4 B6 B10 107.73(16) . . ?
B3 B6 B10 107.66(16) . . ?
B7 B6 B10 59.70(13) . . ?
B5 B6 B10 59.75(13) . . ?
B3 B7 B10 108.45(16) . . ?
B3 B7 B2 60.27(13) . . ?
B10 B7 B2 108.15(16) . . ?
B3 B7 B6 60.12(13) . . ?
B10 B7 B6 60.31(13) . . ?
B2 B7 B6 108.35(15) . . ?
B3 B7 B8 108.14(15) . . ?
B10 B7 B8 60.14(14) . . ?
B2 B7 B8 59.75(13) . . ?
B6 B7 B8 108.33(16) . . ?
B1 B8 B2 60.61(12) . . ?
B1 B8 B9 60.09(12) . . ?
B2 B8 B9 108.63(15) . . ?
B1 B8 B10 108.02(15) . . ?
B2 B8 B10 107.79(17) . . ?
B9 B8 B10 60.09(13) . . ?
B1 B8 B7 108.17(16) . . ?
B2 B8 B7 59.82(13) . . ?
B9 B8 B7 107.96(16) . . ?
B10 B8 B7 59.63(13) . . ?
C1 B9 B1 59.92(11) . . ?
C1 B9 B8 105.94(16) . . ?
B1 B9 B8 59.48(12) . . ?
C1 B9 B10 105.18(16) . . ?
B1 B9 B10 107.52(16) . . ?
B8 B9 B10 60.08(13) . . ?
C1 B9 B5 58.37(11) . . ?
B1 B9 B5 107.72(15) . . ?
B8 B9 B5 107.67(17) . . ?
B10 B9 B5 59.69(13) . . ?
B7 B10 B5 107.95(15) . . ?
B7 B10 B8 60.23(13) . . ?
B5 B10 B8 107.88(15) . . ?
B7 B10 B9 108.24(16) . . ?
B5 B10 B9 60.20(12) . . ?
B8 B10 B9 59.83(13) . . ?
B7 B10 B6 59.99(13) . . ?
B5 B10 B6 59.98(13) . . ?
B8 B10 B6 108.15(16) . . ?
B9 B10 B6 108.34(14) . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
C3 C1 C2 C9 2.3(2) . . . . ?
B5 C1 C2 C9 146.50(16) . . . . ?
B9 C1 C2 C9 -146.40(17) . . . . ?
B1 C1 C2 C9 -107.26(18) . . . . ?
B4 C1 C2 C9 107.38(18) . . . . ?
C3 C1 C2 B2 148.18(16) . . . . ?
B5 C1 C2 B2 -67.59(18) . . . . ?
B9 C1 C2 B2 -0.49(19) . . . . ?
B1 C1 C2 B2 38.64(14) . . . . ?
B4 C1 C2 B2 -106.72(16) . . . . ?
C3 C1 C2 B3 -143.70(16) . . . . ?
B5 C1 C2 B3 0.53(19) . . . . ?
B9 C1 C2 B3 67.63(18) . . . . ?
B1 C1 C2 B3 106.77(16) . . . . ?
B4 C1 C2 B3 -38.59(14) . . . . ?
C3 C1 C2 B4 -105.10(17) . . . . ?
B5 C1 C2 B4 39.13(14) . . . . ?
B9 C1 C2 B4 106.23(15) . . . . ?
B1 C1 C2 B4 145.36(14) . . . . ?
C3 C1 C2 B1 109.54(17) . . . . ?
B5 C1 C2 B1 -106.24(15) . . . . ?
B9 C1 C2 B1 -39.13(14) . . . . ?
B4 C1 C2 B1 -145.36(14) . . . . ?
B5 C1 C3 C4 -28.9(2) . . . . ?
C2 C1 C3 C4 110.40(19) . . . . ?
B9 C1 C3 C4 -106.0(2) . . . . ?
B1 C1 C3 C4 179.88(16) . . . . ?
B4 C1 C3 C4 42.5(2) . . . . ?
B5 C1 C3 C8 152.06(18) . . . . ?
C2 C1 C3 C8 -68.6(2) . . . . ?
B9 C1 C3 C8 74.9(2) . . . . ?
B1 C1 C3 C8 0.8(3) . . . . ?
B4 C1 C3 C8 -136.54(17) . . . . ?
C8 C3 C4 C5 0.2(3) . . . . ?
C1 C3 C4 C5 -178.89(18) . . . . ?
C3 C4 C5 C6 0.9(3) . . . . ?
C4 C5 C6 C7 -1.2(3) . . . . ?
C5 C6 C7 C8 0.4(3) . . . . ?
C6 C7 C8 C3 0.6(3) . . . . ?
C4 C3 C8 C7 -0.9(3) . . . . ?
C1 C3 C8 C7 178.12(17) . . . . ?
C16 C11 C12 C13 0.3(3) . . . . ?
C10 C11 C12 C13 178.62(19) . . . . ?
C11 C12 C13 C14 -0.6(3) . . . . ?
C12 C13 C14 C15 0.1(3) . . . . ?
C13 C14 C15 C16 0.6(3) . . . . ?
C14 C15 C16 C11 -0.9(3) . . . . ?
C12 C11 C16 C15 0.4(3) . . . . ?
C10 C11 C16 C15 -177.90(19) . . . . ?
C9 C2 B1 C1 105.30(17) . . . . ?
B2 C2 B1 C1 -138.97(15) . . . . ?
B3 C2 B1 C1 -101.80(16) . . . . ?
B4 C2 B1 C1 -32.71(13) . . . . ?
C9 C2 B1 B8 -155.26(16) . . . . ?
B2 C2 B1 B8 -39.53(14) . . . . ?
B3 C2 B1 B8 -2.4(2) . . . . ?
C1 C2 B1 B8 99.44(15) . . . . ?
B4 C2 B1 B8 66.73(18) . . . . ?
C9 C2 B1 B9 141.94(16) . . . . ?
B2 C2 B1 B9 -102.33(16) . . . . ?
B3 C2 B1 B9 -65.16(19) . . . . ?
C1 C2 B1 B9 36.64(13) . . . . ?
B4 C2 B1 B9 3.93(19) . . . . ?
C9 C2 B1 B2 -115.73(18) . . . . ?
B3 C2 B1 B2 37.17(16) . . . . ?
C1 C2 B1 B2 138.97(15) . . . . ?
B4 C2 B1 B2 106.26(16) . . . . ?
C3 C1 B1 C2 -107.01(16) . . . . ?
B5 C1 B1 C2 99.31(15) . . . . ?
B9 C1 B1 C2 137.45(15) . . . . ?
B4 C1 B1 C2 31.94(13) . . . . ?
C3 C1 B1 B8 155.00(16) . . . . ?
B5 C1 B1 B8 1.3(2) . . . . ?
C2 C1 B1 B8 -98.00(16) . . . . ?
B9 C1 B1 B8 39.45(15) . . . . ?
B4 C1 B1 B8 -66.06(18) . . . . ?
C3 C1 B1 B9 115.55(18) . . . . ?
B5 C1 B1 B9 -38.13(16) . . . . ?
C2 C1 B1 B9 -137.45(15) . . . . ?
B4 C1 B1 B9 -105.51(16) . . . . ?
C3 C1 B1 B2 -142.42(16) . . . . ?
B5 C1 B1 B2 63.90(19) . . . . ?
C2 C1 B1 B2 -35.41(13) . . . . ?
B9 C1 B1 B2 102.03(16) . . . . ?
B4 C1 B1 B2 -3.47(19) . . . . ?
C9 C2 B2 B8 144.04(18) . . . . ?
B3 C2 B2 B8 -102.46(17) . . . . ?
C1 C2 B2 B8 1.5(2) . . . . ?
B4 C2 B2 B8 -65.2(2) . . . . ?
B1 C2 B2 B8 39.37(15) . . . . ?
C9 C2 B2 B7 -153.20(18) . . . . ?
B3 C2 B2 B7 -39.70(15) . . . . ?
C1 C2 B2 B7 64.25(19) . . . . ?
B4 C2 B2 B7 -2.4(2) . . . . ?
B1 C2 B2 B7 102.13(17) . . . . ?
C9 C2 B2 B3 -113.5(2) . . . . ?
C1 C2 B2 B3 103.95(16) . . . . ?
B4 C2 B2 B3 37.30(16) . . . . ?
B1 C2 B2 B3 141.83(16) . . . . ?
C9 C2 B2 B1 104.7(2) . . . . ?
B3 C2 B2 B1 -141.83(16) . . . . ?
C1 C2 B2 B1 -37.88(14) . . . . ?
B4 C2 B2 B1 -104.53(16) . . . . ?
C1 B1 B2 C2 35.86(13) . . . . ?
B8 B1 B2 C2 134.66(16) . . . . ?
B9 B1 B2 C2 97.10(15) . . . . ?
C2 B1 B2 B8 -134.66(16) . . . . ?
C1 B1 B2 B8 -98.79(16) . . . . ?
B9 B1 B2 B8 -37.56(15) . . . . ?
C2 B1 B2 B7 -96.88(17) . . . . ?
C1 B1 B2 B7 -61.02(18) . . . . ?
B8 B1 B2 B7 37.77(15) . . . . ?
B9 B1 B2 B7 0.2(2) . . . . ?
C2 B1 B2 B3 -33.69(14) . . . . ?
C1 B1 B2 B3 2.18(19) . . . . ?
B8 B1 B2 B3 100.97(17) . . . . ?
B9 B1 B2 B3 63.42(19) . . . . ?
C9 C2 B3 B7 153.52(17) . . . . ?
B2 C2 B3 B7 39.77(15) . . . . ?
C1 C2 B3 B7 -63.77(18) . . . . ?
B4 C2 B3 B7 -101.70(17) . . . . ?
B1 C2 B3 B7 2.7(2) . . . . ?
C9 C2 B3 B6 -144.02(18) . . . . ?
B2 C2 B3 B6 102.23(17) . . . . ?
C1 C2 B3 B6 -1.3(2) . . . . ?
B4 C2 B3 B6 -39.24(14) . . . . ?
B1 C2 B3 B6 65.2(2) . . . . ?
C9 C2 B3 B2 113.8(2) . . . . ?
C1 C2 B3 B2 -103.53(16) . . . . ?
B4 C2 B3 B2 -141.47(16) . . . . ?
B1 C2 B3 B2 -37.02(16) . . . . ?
C9 C2 B3 B4 -104.8(2) . . . . ?
B2 C2 B3 B4 141.47(16) . . . . ?
C1 C2 B3 B4 37.93(14) . . . . ?
B1 C2 B3 B4 104.45(16) . . . . ?
B8 B2 B3 C2 96.91(16) . . . . ?
B7 B2 B3 C2 134.36(16) . . . . ?
B1 B2 B3 C2 34.04(14) . . . . ?
C2 B2 B3 B7 -134.36(16) . . . . ?
B8 B2 B3 B7 -37.45(15) . . . . ?
B1 B2 B3 B7 -100.32(17) . . . . ?
C2 B2 B3 B6 -96.97(16) . . . . ?
B8 B2 B3 B6 -0.1(2) . . . . ?
B7 B2 B3 B6 37.39(15) . . . . ?
B1 B2 B3 B6 -62.93(19) . . . . ?
C2 B2 B3 B4 -34.24(14) . . . . ?
B8 B2 B3 B4 62.68(18) . . . . ?
B7 B2 B3 B4 100.12(17) . . . . ?
B1 B2 B3 B4 -0.2(2) . . . . ?
C9 C2 B4 C1 -105.37(17) . . . . ?
B2 C2 B4 C1 101.66(16) . . . . ?
B3 C2 B4 C1 139.11(15) . . . . ?
B1 C2 B4 C1 32.63(13) . . . . ?
C9 C2 B4 B6 155.16(16) . . . . ?
B2 C2 B4 B6 2.2(2) . . . . ?
B3 C2 B4 B6 39.64(15) . . . . ?
C1 C2 B4 B6 -99.47(15) . . . . ?
B1 C2 B4 B6 -66.85(18) . . . . ?
C9 C2 B4 B5 -141.96(16) . . . . ?
B2 C2 B4 B5 65.07(19) . . . . ?
B3 C2 B4 B5 102.52(16) . . . . ?
C1 C2 B4 B5 -36.59(12) . . . . ?
B1 C2 B4 B5 -3.97(19) . . . . ?
C9 C2 B4 B3 115.52(18) . . . . ?
B2 C2 B4 B3 -37.45(16) . . . . ?
C1 C2 B4 B3 -139.11(15) . . . . ?
B1 C2 B4 B3 -106.48(16) . . . . ?
C3 C1 B4 C2 108.49(16) . . . . ?
B5 C1 B4 C2 -137.33(14) . . . . ?
B9 C1 B4 C2 -99.51(15) . . . . ?
B1 C1 B4 C2 -32.03(13) . . . . ?
C3 C1 B4 B6 -153.19(15) . . . . ?
B5 C1 B4 B6 -39.02(14) . . . . ?
C2 C1 B4 B6 98.31(15) . . . . ?
B9 C1 B4 B6 -1.2(2) . . . . ?
B1 C1 B4 B6 66.28(18) . . . . ?
C3 C1 B4 B5 -114.17(17) . . . . ?
C2 C1 B4 B5 137.33(14) . . . . ?
B9 C1 B4 B5 37.83(15) . . . . ?
B1 C1 B4 B5 105.31(15) . . . . ?
C3 C1 B4 B3 143.88(15) . . . . ?
B5 C1 B4 B3 -101.94(15) . . . . ?
C2 C1 B4 B3 35.39(13) . . . . ?
B9 C1 B4 B3 -64.11(18) . . . . ?
B1 C1 B4 B3 3.36(18) . . . . ?
B7 B3 B4 C2 97.12(17) . . . . ?
B6 B3 B4 C2 134.77(16) . . . . ?
B2 B3 B4 C2 33.93(14) . . . . ?
C2 B3 B4 C1 -35.79(13) . . . . ?
B7 B3 B4 C1 61.33(18) . . . . ?
B6 B3 B4 C1 98.98(16) . . . . ?
B2 B3 B4 C1 -1.86(19) . . . . ?
C2 B3 B4 B6 -134.77(16) . . . . ?
B7 B3 B4 B6 -37.66(15) . . . . ?
B2 B3 B4 B6 -100.85(17) . . . . ?
C2 B3 B4 B5 -96.86(16) . . . . ?
B7 B3 B4 B5 0.3(2) . . . . ?
B6 B3 B4 B5 37.92(15) . . . . ?
B2 B3 B4 B5 -62.93(18) . . . . ?
C3 C1 B5 B4 104.07(18) . . . . ?
C2 C1 B5 B4 -38.30(13) . . . . ?
B9 C1 B5 B4 -140.73(16) . . . . ?
B1 C1 B5 B4 -103.08(16) . . . . ?
C3 C1 B5 B10 -154.13(16) . . . . ?
C2 C1 B5 B10 63.49(18) . . . . ?
B9 C1 B5 B10 -38.94(15) . . . . ?
B1 C1 B5 B10 -1.3(2) . . . . ?
B4 C1 B5 B10 101.79(17) . . . . ?
C3 C1 B5 B6 142.87(16) . . . . ?
C2 C1 B5 B6 0.49(19) . . . . ?
B9 C1 B5 B6 -101.94(16) . . . . ?
B1 C1 B5 B6 -64.29(19) . . . . ?
B4 C1 B5 B6 38.79(14) . . . . ?
C3 C1 B5 B9 -115.19(19) . . . . ?
C2 C1 B5 B9 102.43(15) . . . . ?
B1 C1 B5 B9 37.65(15) . . . . ?
B4 C1 B5 B9 140.73(16) . . . . ?
C2 B4 B5 C1 37.05(12) . . . . ?
B6 B4 B5 C1 135.82(16) . . . . ?
B3 B4 B5 C1 98.00(15) . . . . ?
C2 B4 B5 B10 -61.23(18) . . . . ?
C1 B4 B5 B10 -98.28(16) . . . . ?
B6 B4 B5 B10 37.54(15) . . . . ?
B3 B4 B5 B10 -0.3(2) . . . . ?
C2 B4 B5 B6 -98.77(16) . . . . ?
C1 B4 B5 B6 -135.82(16) . . . . ?
B3 B4 B5 B6 -37.82(15) . . . . ?
C2 B4 B5 B9 2.35(19) . . . . ?
C1 B4 B5 B9 -34.70(13) . . . . ?
B6 B4 B5 B9 101.12(16) . . . . ?
B3 B4 B5 B9 63.30(18) . . . . ?
C2 B4 B6 B3 -38.62(15) . . . . ?
C1 B4 B6 B3 -100.07(16) . . . . ?
B5 B4 B6 B3 -137.94(17) . . . . ?
C2 B4 B6 B7 -1.0(2) . . . . ?
C1 B4 B6 B7 -62.46(19) . . . . ?
B5 B4 B6 B7 -100.34(18) . . . . ?
B3 B4 B6 B7 37.60(16) . . . . ?
C2 B4 B6 B5 99.32(16) . . . . ?
C1 B4 B6 B5 37.88(14) . . . . ?
B3 B4 B6 B5 137.94(17) . . . . ?
C2 B4 B6 B10 62.02(19) . . . . ?
C1 B4 B6 B10 0.6(2) . . . . ?
B5 B4 B6 B10 -37.30(15) . . . . ?
B3 B4 B6 B10 100.64(17) . . . . ?
C2 B3 B6 B4 39.20(14) . . . . ?
B7 B3 B6 B4 137.75(17) . . . . ?
B2 B3 B6 B4 100.46(16) . . . . ?
C2 B3 B6 B7 -98.55(17) . . . . ?
B2 B3 B6 B7 -37.29(15) . . . . ?
B4 B3 B6 B7 -137.75(17) . . . . ?
C2 B3 B6 B5 1.6(2) . . . . ?
B7 B3 B6 B5 100.13(17) . . . . ?
B2 B3 B6 B5 62.83(19) . . . . ?
B4 B3 B6 B5 -37.63(15) . . . . ?
C2 B3 B6 B10 -61.56(19) . . . . ?
B7 B3 B6 B10 36.99(15) . . . . ?
B2 B3 B6 B10 -0.3(2) . . . . ?
B4 B3 B6 B10 -100.76(17) . . . . ?
C1 B5 B6 B4 -39.09(14) . . . . ?
B10 B5 B6 B4 -138.07(16) . . . . ?
B9 B5 B6 B4 -100.84(16) . . . . ?
C1 B5 B6 B3 -1.3(2) . . . . ?
B4 B5 B6 B3 37.80(15) . . . . ?
B10 B5 B6 B3 -100.27(17) . . . . ?
B9 B5 B6 B3 -63.04(19) . . . . ?
C1 B5 B6 B7 61.81(18) . . . . ?
B4 B5 B6 B7 100.90(16) . . . . ?
B10 B5 B6 B7 -37.17(14) . . . . ?
B9 B5 B6 B7 0.06(19) . . . . ?
C1 B5 B6 B10 98.98(16) . . . . ?
B4 B5 B6 B10 138.07(16) . . . . ?
B9 B5 B6 B10 37.23(14) . . . . ?
C2 B3 B7 B10 61.7(2) . . . . ?
B6 B3 B7 B10 -37.45(16) . . . . ?
B2 B3 B7 B10 100.82(18) . . . . ?
B4 B3 B7 B10 -0.1(2) . . . . ?
C2 B3 B7 B2 -39.08(14) . . . . ?
B6 B3 B7 B2 -138.27(17) . . . . ?
B4 B3 B7 B2 -100.96(17) . . . . ?
C2 B3 B7 B6 99.19(17) . . . . ?
B2 B3 B7 B6 138.27(17) . . . . ?
B4 B3 B7 B6 37.31(15) . . . . ?
C2 B3 B7 B8 -2.0(2) . . . . ?
B6 B3 B7 B8 -101.16(18) . . . . ?
B2 B3 B7 B8 37.11(16) . . . . ?
B4 B3 B7 B8 -63.9(2) . . . . ?
C2 B2 B7 B3 39.07(15) . . . . ?
B8 B2 B7 B3 138.42(17) . . . . ?
B1 B2 B7 B3 101.11(17) . . . . ?
C2 B2 B7 B10 -62.3(2) . . . . ?
B8 B2 B7 B10 37.10(15) . . . . ?
B3 B2 B7 B10 -101.32(17) . . . . ?
B1 B2 B7 B10 -0.2(2) . . . . ?
C2 B2 B7 B6 1.6(2) . . . . ?
B8 B2 B7 B6 100.96(18) . . . . ?
B3 B2 B7 B6 -37.45(16) . . . . ?
B1 B2 B7 B6 63.7(2) . . . . ?
C2 B2 B7 B8 -99.35(17) . . . . ?
B3 B2 B7 B8 -138.42(17) . . . . ?
B1 B2 B7 B8 -37.31(15) . . . . ?
B4 B6 B7 B3 -37.89(15) . . . . ?
B5 B6 B7 B3 -101.19(16) . . . . ?
B10 B6 B7 B3 -138.39(16) . . . . ?
B4 B6 B7 B10 100.50(17) . . . . ?
B3 B6 B7 B10 138.39(16) . . . . ?
B5 B6 B7 B10 37.20(14) . . . . ?
B4 B6 B7 B2 -0.4(2) . . . . ?
B3 B6 B7 B2 37.52(16) . . . . ?
B5 B6 B7 B2 -63.7(2) . . . . ?
B10 B6 B7 B2 -100.87(18) . . . . ?
B4 B6 B7 B8 62.9(2) . . . . ?
B3 B6 B7 B8 100.83(17) . . . . ?
B5 B6 B7 B8 -0.4(2) . . . . ?
B10 B6 B7 B8 -37.56(15) . . . . ?
C2 B1 B8 B2 38.57(14) . . . . ?
C1 B1 B8 B2 99.91(16) . . . . ?
B9 B1 B8 B2 138.32(17) . . . . ?
C2 B1 B8 B9 -99.75(16) . . . . ?
C1 B1 B8 B9 -38.41(14) . . . . ?
B2 B1 B8 B9 -138.32(17) . . . . ?
C2 B1 B8 B10 -62.13(19) . . . . ?
C1 B1 B8 B10 -0.8(2) . . . . ?
B9 B1 B8 B10 37.63(16) . . . . ?
B2 B1 B8 B10 -100.69(18) . . . . ?
C2 B1 B8 B7 0.9(2) . . . . ?
C1 B1 B8 B7 62.29(19) . . . . ?
B9 B1 B8 B7 100.70(17) . . . . ?
B2 B1 B8 B7 -37.62(15) . . . . ?
C2 B2 B8 B1 -39.37(14) . . . . ?
B7 B2 B8 B1 -137.85(16) . . . . ?
B3 B2 B8 B1 -100.67(16) . . . . ?
C2 B2 B8 B9 -1.9(2) . . . . ?
B7 B2 B8 B9 -100.39(17) . . . . ?
B3 B2 B8 B9 -63.2(2) . . . . ?
B1 B2 B8 B9 37.46(15) . . . . ?
C2 B2 B8 B10 61.70(19) . . . . ?
B7 B2 B8 B10 -36.78(15) . . . . ?
B3 B2 B8 B10 0.4(2) . . . . ?
B1 B2 B8 B10 101.07(16) . . . . ?
C2 B2 B8 B7 98.48(16) . . . . ?
B3 B2 B8 B7 37.18(15) . . . . ?
B1 B2 B8 B7 137.85(16) . . . . ?
B3 B7 B8 B1 0.6(2) . . . . ?
B10 B7 B8 B1 -100.66(17) . . . . ?
B2 B7 B8 B1 37.98(15) . . . . ?
B6 B7 B8 B1 -63.0(2) . . . . ?
B3 B7 B8 B2 -37.34(15) . . . . ?
B10 B7 B8 B2 -138.64(16) . . . . ?
B6 B7 B8 B2 -101.00(16) . . . . ?
B3 B7 B8 B9 64.2(2) . . . . ?
B10 B7 B8 B9 -37.10(14) . . . . ?
B2 B7 B8 B9 101.53(16) . . . . ?
B6 B7 B8 B9 0.5(2) . . . . ?
B3 B7 B8 B10 101.30(17) . . . . ?
B2 B7 B8 B10 138.64(16) . . . . ?
B6 B7 B8 B10 37.64(14) . . . . ?
C3 C1 B9 B1 -107.76(19) . . . . ?
B5 C1 B9 B1 140.36(16) . . . . ?
C2 C1 B9 B1 38.40(14) . . . . ?
B4 C1 B9 B1 103.02(16) . . . . ?
C3 C1 B9 B8 -146.89(17) . . . . ?
B5 C1 B9 B8 101.23(17) . . . . ?
C2 C1 B9 B8 -0.73(19) . . . . ?
B1 C1 B9 B8 -39.12(15) . . . . ?
B4 C1 B9 B8 63.90(19) . . . . ?
C3 C1 B9 B10 150.50(17) . . . . ?
B5 C1 B9 B10 38.62(14) . . . . ?
C2 C1 B9 B10 -63.34(18) . . . . ?
B1 C1 B9 B10 -101.73(17) . . . . ?
B4 C1 B9 B10 1.3(2) . . . . ?
C3 C1 B9 B5 111.88(19) . . . . ?
C2 C1 B9 B5 -101.96(15) . . . . ?
B1 C1 B9 B5 -140.36(16) . . . . ?
B4 C1 B9 B5 -37.33(15) . . . . ?
C2 B1 B9 C1 -37.00(13) . . . . ?
B8 B1 B9 C1 -135.22(17) . . . . ?
B2 B1 B9 C1 -97.86(16) . . . . ?
C2 B1 B9 B8 98.22(16) . . . . ?
C1 B1 B9 B8 135.22(17) . . . . ?
B2 B1 B9 B8 37.37(15) . . . . ?
C2 B1 B9 B10 60.72(17) . . . . ?
C1 B1 B9 B10 97.72(16) . . . . ?
B8 B1 B9 B10 -37.50(15) . . . . ?
B2 B1 B9 B10 -0.1(2) . . . . ?
C2 B1 B9 B5 -2.23(19) . . . . ?
C1 B1 B9 B5 34.77(13) . . . . ?
B8 B1 B9 B5 -100.45(17) . . . . ?
B2 B1 B9 B5 -63.09(18) . . . . ?
B1 B8 B9 C1 39.33(14) . . . . ?
B2 B8 B9 C1 1.6(2) . . . . ?
B10 B8 B9 C1 -98.61(17) . . . . ?
B7 B8 B9 C1 -61.72(19) . . . . ?
B2 B8 B9 B1 -37.69(15) . . . . ?
B10 B8 B9 B1 -137.95(16) . . . . ?
B7 B8 B9 B1 -101.05(17) . . . . ?
B1 B8 B9 B10 137.95(16) . . . . ?
B2 B8 B9 B10 100.26(18) . . . . ?
B7 B8 B9 B10 36.90(14) . . . . ?
B1 B8 B9 B5 100.55(16) . . . . ?
B2 B8 B9 B5 62.86(19) . . . . ?
B10 B8 B9 B5 -37.40(14) . . . . ?
B7 B8 B9 B5 -0.5(2) . . . . ?
B4 B5 B9 C1 35.35(14) . . . . ?
B10 B5 B9 C1 135.75(16) . . . . ?
B6 B5 B9 C1 98.45(16) . . . . ?
C1 B5 B9 B1 -35.42(14) . . . . ?
B4 B5 B9 B1 -0.1(2) . . . . ?
B10 B5 B9 B1 100.33(17) . . . . ?
B6 B5 B9 B1 63.03(18) . . . . ?
C1 B5 B9 B8 -98.18(16) . . . . ?
B4 B5 B9 B8 -62.83(18) . . . . ?
B10 B5 B9 B8 37.57(14) . . . . ?
B6 B5 B9 B8 0.27(19) . . . . ?
C1 B5 B9 B10 -135.75(16) . . . . ?
B4 B5 B9 B10 -100.40(17) . . . . ?
B6 B5 B9 B10 -37.30(14) . . . . ?
B3 B7 B10 B5 0.0(2) . . . . ?
B2 B7 B10 B5 63.8(2) . . . . ?
B6 B7 B10 B5 -37.40(15) . . . . ?
B8 B7 B10 B5 100.75(17) . . . . ?
B3 B7 B10 B8 -100.77(17) . . . . ?
B2 B7 B10 B8 -36.93(15) . . . . ?
B6 B7 B10 B8 -138.14(15) . . . . ?
B3 B7 B10 B9 -63.7(2) . . . . ?
B2 B7 B10 B9 0.1(2) . . . . ?
B6 B7 B10 B9 -101.08(16) . . . . ?
B8 B7 B10 B9 37.06(15) . . . . ?
B3 B7 B10 B6 37.37(15) . . . . ?
B2 B7 B10 B6 101.22(17) . . . . ?
B8 B7 B10 B6 138.14(15) . . . . ?
C1 B5 B10 B7 -62.9(2) . . . . ?
B4 B5 B10 B7 0.2(2) . . . . ?
B6 B5 B10 B7 37.40(15) . . . . ?
B9 B5 B10 B7 -101.16(17) . . . . ?
C1 B5 B10 B8 0.7(2) . . . . ?
B4 B5 B10 B8 63.8(2) . . . . ?
B6 B5 B10 B8 101.05(17) . . . . ?
B9 B5 B10 B8 -37.51(16) . . . . ?
C1 B5 B10 B9 38.24(14) . . . . ?
B4 B5 B10 B9 101.35(16) . . . . ?
B6 B5 B10 B9 138.56(16) . . . . ?
C1 B5 B10 B6 -100.32(16) . . . . ?
B4 B5 B10 B6 -37.21(15) . . . . ?
B9 B5 B10 B6 -138.56(16) . . . . ?
B1 B8 B10 B7 100.92(18) . . . . ?
B2 B8 B10 B7 36.87(15) . . . . ?
B9 B8 B10 B7 138.55(16) . . . . ?
B1 B8 B10 B5 0.0(2) . . . . ?
B2 B8 B10 B5 -64.0(2) . . . . ?
B9 B8 B10 B5 37.68(15) . . . . ?
B7 B8 B10 B5 -100.87(17) . . . . ?
B1 B8 B10 B9 -37.63(15) . . . . ?
B2 B8 B10 B9 -101.68(16) . . . . ?
B7 B8 B10 B9 -138.55(16) . . . . ?
B1 B8 B10 B6 63.5(2) . . . . ?
B2 B8 B10 B6 -0.6(2) . . . . ?
B9 B8 B10 B6 101.09(16) . . . . ?
B7 B8 B10 B6 -37.45(14) . . . . ?
C1 B9 B10 B7 62.68(19) . . . . ?
B1 B9 B10 B7 0.0(2) . . . . ?
B8 B9 B10 B7 -37.23(15) . . . . ?
B5 B9 B10 B7 100.68(17) . . . . ?
C1 B9 B10 B5 -38.00(14) . . . . ?
B1 B9 B10 B5 -100.67(16) . . . . ?
B8 B9 B10 B5 -137.91(17) . . . . ?
C1 B9 B10 B8 99.91(16) . . . . ?
B1 B9 B10 B8 37.23(14) . . . . ?
B5 B9 B10 B8 137.91(17) . . . . ?
C1 B9 B10 B6 -0.9(2) . . . . ?
B1 B9 B10 B6 -63.54(19) . . . . ?
B8 B9 B10 B6 -100.78(17) . . . . ?
B5 B9 B10 B6 37.13(15) . . . . ?
B4 B6 B10 B7 -100.74(17) . . . . ?
B3 B6 B10 B7 -37.01(15) . . . . ?
B5 B6 B10 B7 -138.14(16) . . . . ?
B4 B6 B10 B5 37.41(15) . . . . ?
B3 B6 B10 B5 101.13(16) . . . . ?
B7 B6 B10 B5 138.14(16) . . . . ?
B4 B6 B10 B8 -63.18(19) . . . . ?
B3 B6 B10 B8 0.5(2) . . . . ?
B7 B6 B10 B8 37.56(14) . . . . ?
B5 B6 B10 B8 -100.58(16) . . . . ?
B4 B6 B10 B9 0.2(2) . . . . ?
B3 B6 B10 B9 63.90(19) . . . . ?
B7 B6 B10 B9 100.91(17) . . . . ?
B5 B6 B10 B9 -37.23(15) . . . . ?

_refine_diff_density_max         0.258
_refine_diff_density_min         -0.221
_refine_diff_density_rms         0.044



####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_shelx_CCDC1
_database_code_depnum_ccdc_archive 'CCDC 1986099'
loop_
_audit_author_name
_audit_author_address
'Won-Sik Han'
;Seoul Womens University
South Korea
;
_audit_update_record             
;
2020-02-25 deposited with the CCDC.	2020-09-10 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-2014/7
_shelx_SHELXL_version_number     2014/7
_chemical_name_systematic        ?
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'C9 H15 B10'
_chemical_formula_weight         231.31

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_H-M_alt        'P 21/n'
_space_group_name_Hall           '-P 2yn'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;

loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'

_cell_length_a                   10.7957(11)
_cell_length_b                   9.7951(9)
_cell_length_c                   13.7818(12)
_cell_angle_alpha                90
_cell_angle_beta                 112.281(3)
_cell_angle_gamma                90
_cell_volume                     1348.5(2)
_cell_formula_units_Z            4
_cell_measurement_temperature    223(2)
_cell_measurement_reflns_used    7946
_cell_measurement_theta_min      2.616
_cell_measurement_theta_max      27.51

_exptl_crystal_description       Block
_exptl_crystal_colour            Colourless
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_density_diffrn    1.139
_exptl_crystal_F_000             476
_exptl_transmission_factor_min   ?
_exptl_transmission_factor_max   ?
_exptl_crystal_size_max          0.210
_exptl_crystal_size_mid          0.140
_exptl_crystal_size_min          0.100
_exptl_absorpt_coefficient_mu    0.053
_shelx_estimated_absorpt_T_min   0.989
_shelx_estimated_absorpt_T_max   0.995
_exptl_absorpt_correction_type   Multi-scan
_exptl_absorpt_correction_T_min  0.959
_exptl_absorpt_correction_T_max  0.995
_exptl_absorpt_process_details   'Bruker SADABS'
_exptl_absorpt_special_details   ?
_diffrn_ambient_temperature      223(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_source                   ?
_diffrn_measurement_device_type  'PHOTON 100 CMOS'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_detector_area_resol_mean ?
_diffrn_reflns_number            43152
_diffrn_reflns_av_unetI/netI     0.0443
_diffrn_reflns_av_R_equivalents  0.1113
_diffrn_reflns_limit_h_min       -14
_diffrn_reflns_limit_h_max       14
_diffrn_reflns_limit_k_min       -13
_diffrn_reflns_limit_k_max       13
_diffrn_reflns_limit_l_min       -18
_diffrn_reflns_limit_l_max       18
_diffrn_reflns_theta_min         2.622
_diffrn_reflns_theta_max         28.515
_diffrn_reflns_theta_full        25.242
_diffrn_measured_fraction_theta_max 0.989
_diffrn_measured_fraction_theta_full 1.000
_diffrn_reflns_Laue_measured_fraction_max 0.989
_diffrn_reflns_Laue_measured_fraction_full 1.000
_diffrn_reflns_point_group_measured_fraction_max 0.989
_diffrn_reflns_point_group_measured_fraction_full 1.000
_reflns_number_total             3392
_reflns_number_gt                2241
_reflns_threshold_expression     'I > 2σ(I)'
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_max     .
_reflns_Friedel_fraction_full    .

_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;

_computing_data_collection       'Bruker APEX2'
_computing_cell_refinement       'Bruker SAINT'
_computing_data_reduction        'Bruker SAINT'
_computing_structure_solution    'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_refine_special_details          ?
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0777P)²+0.6742P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    constr
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       .
_refine_ls_number_reflns         3392
_refine_ls_number_parameters     172
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.1066
_refine_ls_R_factor_gt           0.0625
_refine_ls_wR_factor_ref         0.1749
_refine_ls_wR_factor_gt          0.1487
_refine_ls_goodness_of_fit_ref   1.025
_refine_ls_restrained_S_all      1.025
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
C1 C 0.55999(17) 0.73678(17) 0.16200(12) 0.0255(4) Uani 1 1 d . . . . .
C2 C 0.45393(17) 0.60506(18) 0.10846(13) 0.0277(4) Uani 1 1 d . . . . .
C3 C 0.67486(17) 0.75635(18) 0.12714(13) 0.0285(4) Uani 1 1 d . . . . .
C4 C 0.7984(2) 0.7034(3) 0.18571(18) 0.0508(6) Uani 1 1 d . . . . .
H4 H 0.8114 0.6583 0.2490 0.061 Uiso 1 1 calc R U . . .
C5 C 0.9038(2) 0.7155(3) 0.1528(2) 0.0634(7) Uani 1 1 d . . . . .
H5 H 0.9875 0.6779 0.1936 0.076 Uiso 1 1 calc R U . . .
C6 C 0.8875(2) 0.7818(3) 0.0614(2) 0.0547(6) Uani 1 1 d . . . . .
H6 H 0.9586 0.7879 0.0381 0.066 Uiso 1 1 calc R U . . .
C7 C 0.7665(2) 0.8389(3) 0.00488(19) 0.0598(7) Uani 1 1 d . . . . .
H7 H 0.7552 0.8873 -0.0568 0.072 Uiso 1 1 calc R U . . .
C8 C 0.6604(2) 0.8266(2) 0.03679(16) 0.0467(5) Uani 1 1 d . . . . .
H8 H 0.5775 0.8665 -0.0034 0.056 Uiso 1 1 calc R U . . .
C9 C 0.48440(18) 0.52839(19) 0.03147(13) 0.0321(4) Uani 1 1 d . . . . .
B1 B 0.3978(2) 0.7691(2) 0.07260(15) 0.0310(4) Uani 1 1 d . . . . .
H1 H 0.3747 0.8125 -0.0067 0.037 Uiso 1 1 calc R U . . .
B2 B 0.4724(2) 0.8676(2) 0.18737(16) 0.0330(5) Uani 1 1 d . . . . .
H2 H 0.4972 0.9769 0.1835 0.040 Uiso 1 1 calc R U . . .
B3 B 0.5763(2) 0.7584(2) 0.28849(15) 0.0323(5) Uani 1 1 d . . . . .
H3 H 0.6692 0.7964 0.3510 0.039 Uiso 1 1 calc R U . . .
B4 B 0.5659(2) 0.5907(2) 0.23617(15) 0.0293(4) Uani 1 1 d . . . . .
H4A H 0.6515 0.5185 0.2629 0.035 Uiso 1 1 calc R U . . .
B5 B 0.2942(2) 0.6425(2) 0.09622(17) 0.0356(5) Uani 1 1 d . . . . .
H5A H 0.2026 0.6038 0.0326 0.043 Uiso 1 1 calc R U . . .
B6 B 0.3043(2) 0.8093(3) 0.14903(18) 0.0374(5) Uani 1 1 d . . . . .
H6A H 0.2182 0.8808 0.1206 0.045 Uiso 1 1 calc R U . . .
B7 B 0.4144(2) 0.8032(3) 0.28335(17) 0.0392(5) Uani 1 1 d . . . . .
H7A H 0.4003 0.8706 0.3431 0.047 Uiso 1 1 calc R U . . .
B8 B 0.4731(2) 0.6320(2) 0.31277(16) 0.0367(5) Uani 1 1 d . . . . .
H8A H 0.4979 0.5872 0.3919 0.044 Uiso 1 1 calc R U . . .
B9 B 0.3979(2) 0.5329(2) 0.19724(17) 0.0349(5) Uani 1 1 d . . . . .
H9 H 0.3736 0.4231 0.1994 0.042 Uiso 1 1 calc R U . . .
B10 B 0.3050(2) 0.6642(3) 0.22662(18) 0.0396(5) Uani 1 1 d . . . . .
H10 H 0.2191 0.6407 0.2494 0.048 Uiso 1 1 calc R U . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
C1 C3 1.502(2) . ?
C1 C2 1.697(2) . ?
C1 B3 1.698(2) . ?
C1 B2 1.705(3) . ?
C1 B4 1.745(3) . ?
C1 B1 1.746(2) . ?
C2 C9 1.436(2) . ?
C2 B5 1.708(3) . ?
C2 B9 1.710(3) . ?
C2 B4 1.722(3) . ?
C2 B1 1.722(3) . ?
C3 C4 1.372(3) . ?
C3 C8 1.379(3) . ?
C4 C5 1.381(3) . ?
C5 C6 1.367(3) . ?
C6 C7 1.361(3) . ?
C7 C8 1.380(3) . ?
C9 C9 1.182(3) 3_665 ?
B1 B6 1.757(3) . ?
B1 B2 1.765(3) . ?
B1 B5 1.780(3) . ?
B2 B3 1.777(3) . ?
B2 B7 1.780(3) . ?
B2 B6 1.781(3) . ?
B3 B7 1.777(3) . ?
B3 B4 1.780(3) . ?
B3 B8 1.780(3) . ?
B4 B8 1.757(3) . ?
B4 B9 1.778(3) . ?
B5 B10 1.769(3) . ?
B5 B6 1.775(3) . ?
B5 B9 1.778(3) . ?
B6 B10 1.777(3) . ?
B6 B7 1.781(3) . ?
B7 B10 1.777(4) . ?
B7 B8 1.785(3) . ?
B8 B9 1.776(3) . ?
B8 B10 1.780(3) . ?
B9 B10 1.770(3) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C3 C1 C2 117.43(13) . . ?
C3 C1 B3 122.40(14) . . ?
C2 C1 B3 109.34(13) . . ?
C3 C1 B2 123.96(15) . . ?
C2 C1 B2 108.99(13) . . ?
B3 C1 B2 62.96(11) . . ?
C3 C1 B4 116.14(14) . . ?
C2 C1 B4 60.01(11) . . ?
B3 C1 B4 62.24(11) . . ?
B2 C1 B4 113.32(14) . . ?
C3 C1 B1 118.68(14) . . ?
C2 C1 B1 60.01(10) . . ?
B3 C1 B1 112.80(14) . . ?
B2 C1 B1 61.51(11) . . ?
B4 C1 B1 111.47(14) . . ?
C9 C2 C1 114.39(14) . . ?
C9 C2 B5 123.01(15) . . ?
C1 C2 B5 111.67(14) . . ?
C9 C2 B9 123.69(15) . . ?
C1 C2 B9 111.51(13) . . ?
B5 C2 B9 62.71(12) . . ?
C9 C2 B4 116.35(15) . . ?
C1 C2 B4 61.39(10) . . ?
B5 C2 B4 114.20(13) . . ?
B9 C2 B4 62.41(11) . . ?
C9 C2 B1 115.47(15) . . ?
C1 C2 B1 61.41(10) . . ?
B5 C2 B1 62.54(12) . . ?
B9 C2 B1 114.17(14) . . ?
B4 C2 B1 113.81(13) . . ?
C4 C3 C8 118.19(18) . . ?
C4 C3 C1 119.96(16) . . ?
C8 C3 C1 121.85(17) . . ?
C3 C4 C5 120.8(2) . . ?
C6 C5 C4 120.6(2) . . ?
C7 C6 C5 118.9(2) . . ?
C6 C7 C8 120.9(2) . . ?
C3 C8 C7 120.5(2) . . ?
C9 C9 C2 175.7(3) 3_665 . ?
C2 B1 C1 58.58(10) . . ?
C2 B1 B6 104.87(15) . . ?
C1 B1 B6 105.53(14) . . ?
C2 B1 B2 105.15(13) . . ?
C1 B1 B2 58.11(10) . . ?
B6 B1 B2 60.73(13) . . ?
C2 B1 B5 58.33(11) . . ?
C1 B1 B5 106.04(14) . . ?
B6 B1 B5 60.22(13) . . ?
B2 B1 B5 108.77(15) . . ?
C1 B2 B1 60.38(11) . . ?
C1 B2 B3 58.31(11) . . ?
B1 B2 B3 108.15(15) . . ?
C1 B2 B7 105.36(15) . . ?
B1 B2 B7 107.60(16) . . ?
B3 B2 B7 59.95(12) . . ?
C1 B2 B6 106.25(15) . . ?
B1 B2 B6 59.41(12) . . ?
B3 B2 B6 107.96(16) . . ?
B7 B2 B6 60.04(13) . . ?
C1 B3 B2 58.73(11) . . ?
C1 B3 B7 105.81(14) . . ?
B2 B3 B7 60.11(12) . . ?
C1 B3 B4 60.19(10) . . ?
B2 B3 B4 108.28(14) . . ?
B7 B3 B4 107.58(16) . . ?
C1 B3 B8 106.13(14) . . ?
B2 B3 B8 108.21(15) . . ?
B7 B3 B8 60.21(13) . . ?
B4 B3 B8 59.12(12) . . ?
C2 B4 C1 58.60(10) . . ?
C2 B4 B8 104.84(14) . . ?
C1 B4 B8 105.13(14) . . ?
C2 B4 B9 58.47(11) . . ?
C1 B4 B9 106.13(14) . . ?
B8 B4 B9 60.34(12) . . ?
C2 B4 B3 104.52(14) . . ?
C1 B4 B3 57.57(11) . . ?
B8 B4 B3 60.45(13) . . ?
B9 B4 B3 108.44(15) . . ?
C2 B5 B10 104.50(14) . . ?
C2 B5 B6 104.73(15) . . ?
B10 B5 B6 60.18(13) . . ?
C2 B5 B9 58.71(11) . . ?
B10 B5 B9 59.85(12) . . ?
B6 B5 B9 108.18(15) . . ?
C2 B5 B1 59.13(11) . . ?
B10 B5 B1 107.34(15) . . ?
B6 B5 B1 59.24(13) . . ?
B9 B5 B1 108.12(14) . . ?
B1 B6 B5 60.53(12) . . ?
B1 B6 B10 108.02(16) . . ?
B5 B6 B10 59.75(13) . . ?
B1 B6 B2 59.86(12) . . ?
B5 B6 B2 108.32(15) . . ?
B10 B6 B2 107.87(15) . . ?
B1 B6 B7 107.90(15) . . ?
B5 B6 B7 107.96(16) . . ?
B10 B6 B7 59.93(14) . . ?
B2 B6 B7 59.97(13) . . ?
B10 B7 B3 107.92(16) . . ?
B10 B7 B2 107.88(15) . . ?
B3 B7 B2 59.94(12) . . ?
B10 B7 B6 59.91(13) . . ?
B3 B7 B6 107.93(14) . . ?
B2 B7 B6 60.00(12) . . ?
B10 B7 B8 59.96(13) . . ?
B3 B7 B8 59.98(13) . . ?
B2 B7 B8 107.89(15) . . ?
B6 B7 B8 107.88(16) . . ?
B4 B8 B9 60.43(12) . . ?
B4 B8 B10 108.04(15) . . ?
B9 B8 B10 59.69(13) . . ?
B4 B8 B3 60.43(12) . . ?
B9 B8 B3 108.50(14) . . ?
B10 B8 B3 107.67(16) . . ?
B4 B8 B7 108.30(15) . . ?
B9 B8 B7 107.91(15) . . ?
B10 B8 B7 59.82(13) . . ?
B3 B8 B7 59.81(13) . . ?
C2 B9 B10 104.37(15) . . ?
C2 B9 B8 104.48(15) . . ?
B10 B9 B8 60.25(13) . . ?
C2 B9 B4 59.12(11) . . ?
B10 B9 B4 107.53(16) . . ?
B8 B9 B4 59.23(12) . . ?
C2 B9 B5 58.58(11) . . ?
B10 B9 B5 59.81(13) . . ?
B8 B9 B5 108.05(16) . . ?
B4 B9 B5 108.13(15) . . ?
B5 B10 B9 60.33(13) . . ?
B5 B10 B6 60.07(13) . . ?
B9 B10 B6 108.47(15) . . ?
B5 B10 B7 108.41(16) . . ?
B9 B10 B7 108.53(16) . . ?
B6 B10 B7 60.16(13) . . ?
B5 B10 B8 108.31(15) . . ?
B9 B10 B8 60.06(13) . . ?
B6 B10 B8 108.29(16) . . ?
B7 B10 B8 60.22(13) . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
C3 C1 C2 C9 -2.0(2) . . . . ?
B3 C1 C2 C9 -147.34(15) . . . . ?
B2 C1 C2 C9 145.53(16) . . . . ?
B4 C1 C2 C9 -107.92(17) . . . . ?
B1 C1 C2 C9 106.89(17) . . . . ?
C3 C1 C2 B5 -147.53(15) . . . . ?
B3 C1 C2 B5 67.18(17) . . . . ?
B2 C1 C2 B5 0.05(18) . . . . ?
B4 C1 C2 B5 106.60(15) . . . . ?
B1 C1 C2 B5 -38.59(14) . . . . ?
C3 C1 C2 B9 144.41(15) . . . . ?
B3 C1 C2 B9 -0.88(19) . . . . ?
B2 C1 C2 B9 -68.01(17) . . . . ?
B4 C1 C2 B9 38.54(14) . . . . ?
B1 C1 C2 B9 -106.64(15) . . . . ?
C3 C1 C2 B4 105.87(16) . . . . ?
B3 C1 C2 B4 -39.42(13) . . . . ?
B2 C1 C2 B4 -106.55(14) . . . . ?
B1 C1 C2 B4 -145.18(14) . . . . ?
C3 C1 C2 B1 -108.94(16) . . . . ?
B3 C1 C2 B1 105.76(15) . . . . ?
B2 C1 C2 B1 38.64(13) . . . . ?
B4 C1 C2 B1 145.18(14) . . . . ?
C2 C1 C3 C4 -96.2(2) . . . . ?
B3 C1 C3 C4 44.3(3) . . . . ?
B2 C1 C3 C4 121.5(2) . . . . ?
B4 C1 C3 C4 -28.1(2) . . . . ?
B1 C1 C3 C4 -165.24(18) . . . . ?
C2 C1 C3 C8 83.7(2) . . . . ?
B3 C1 C3 C8 -135.8(2) . . . . ?
B2 C1 C3 C8 -58.6(2) . . . . ?
B4 C1 C3 C8 151.80(18) . . . . ?
B1 C1 C3 C8 14.7(3) . . . . ?
C8 C3 C4 C5 -2.5(4) . . . . ?
C1 C3 C4 C5 177.4(2) . . . . ?
C3 C4 C5 C6 0.6(4) . . . . ?
C4 C5 C6 C7 1.8(4) . . . . ?
C5 C6 C7 C8 -2.1(4) . . . . ?
C4 C3 C8 C7 2.1(3) . . . . ?
C1 C3 C8 C7 -177.8(2) . . . . ?
C6 C7 C8 C3 0.2(4) . . . . ?
C9 C2 B1 C1 -105.16(16) . . . . ?
B5 C2 B1 C1 139.21(14) . . . . ?
B9 C2 B1 C1 102.31(15) . . . . ?
B4 C2 B1 C1 33.22(13) . . . . ?
C9 C2 B1 B6 155.50(15) . . . . ?
C1 C2 B1 B6 -99.34(14) . . . . ?
B5 C2 B1 B6 39.87(14) . . . . ?
B9 C2 B1 B6 2.97(19) . . . . ?
B4 C2 B1 B6 -66.12(17) . . . . ?
C9 C2 B1 B2 -141.38(16) . . . . ?
C1 C2 B1 B2 -36.22(13) . . . . ?
B5 C2 B1 B2 102.99(16) . . . . ?
B9 C2 B1 B2 66.09(18) . . . . ?
B4 C2 B1 B2 -3.00(19) . . . . ?
C9 C2 B1 B5 115.63(17) . . . . ?
C1 C2 B1 B5 -139.21(14) . . . . ?
B9 C2 B1 B5 -36.90(14) . . . . ?
B4 C2 B1 B5 -105.99(15) . . . . ?
C3 C1 B1 C2 106.90(16) . . . . ?
B3 C1 B1 C2 -99.92(15) . . . . ?
B2 C1 B1 C2 -137.80(15) . . . . ?
B4 C1 B1 C2 -32.10(13) . . . . ?
C3 C1 B1 B6 -154.92(15) . . . . ?
C2 C1 B1 B6 98.19(15) . . . . ?
B3 C1 B1 B6 -1.7(2) . . . . ?
B2 C1 B1 B6 -39.61(15) . . . . ?
B4 C1 B1 B6 66.09(17) . . . . ?
C3 C1 B1 B2 -115.31(17) . . . . ?
C2 C1 B1 B2 137.80(15) . . . . ?
B3 C1 B1 B2 37.88(15) . . . . ?
B4 C1 B1 B2 105.70(15) . . . . ?
C3 C1 B1 B5 142.24(15) . . . . ?
C2 C1 B1 B5 35.35(13) . . . . ?
B3 C1 B1 B5 -64.57(18) . . . . ?
B2 C1 B1 B5 -102.45(16) . . . . ?
B4 C1 B1 B5 3.25(18) . . . . ?
C3 C1 B2 B1 107.02(17) . . . . ?
C2 C1 B2 B1 -37.97(13) . . . . ?
B3 C1 B2 B1 -140.55(16) . . . . ?
B4 C1 B2 B1 -102.68(15) . . . . ?
C3 C1 B2 B3 -112.43(18) . . . . ?
C2 C1 B2 B3 102.57(15) . . . . ?
B4 C1 B2 B3 37.87(14) . . . . ?
B1 C1 B2 B3 140.55(16) . . . . ?
C3 C1 B2 B7 -151.18(15) . . . . ?
C2 C1 B2 B7 63.83(16) . . . . ?
B3 C1 B2 B7 -38.75(14) . . . . ?
B4 C1 B2 B7 -0.88(19) . . . . ?
B1 C1 B2 B7 101.80(16) . . . . ?
C3 C1 B2 B6 146.17(16) . . . . ?
C2 C1 B2 B6 1.18(18) . . . . ?
B3 C1 B2 B6 -101.40(16) . . . . ?
B4 C1 B2 B6 -63.53(18) . . . . ?
B1 C1 B2 B6 39.15(14) . . . . ?
C2 B1 B2 C1 36.44(13) . . . . ?
B6 B1 B2 C1 135.24(16) . . . . ?
B5 B1 B2 C1 97.59(15) . . . . ?
C2 B1 B2 B3 1.75(19) . . . . ?
C1 B1 B2 B3 -34.68(13) . . . . ?
B6 B1 B2 B3 100.56(17) . . . . ?
B5 B1 B2 B3 62.91(19) . . . . ?
C2 B1 B2 B7 -61.57(17) . . . . ?
C1 B1 B2 B7 -98.01(15) . . . . ?
B6 B1 B2 B7 37.24(15) . . . . ?
B5 B1 B2 B7 -0.41(19) . . . . ?
C2 B1 B2 B6 -98.81(16) . . . . ?
C1 B1 B2 B6 -135.24(16) . . . . ?
B5 B1 B2 B6 -37.65(15) . . . . ?
C3 C1 B3 B2 114.76(18) . . . . ?
C2 C1 B3 B2 -102.00(15) . . . . ?
B4 C1 B3 B2 -140.43(15) . . . . ?
B1 C1 B3 B2 -37.29(15) . . . . ?
C3 C1 B3 B7 153.69(16) . . . . ?
C2 C1 B3 B7 -63.08(18) . . . . ?
B2 C1 B3 B7 38.92(15) . . . . ?
B4 C1 B3 B7 -101.51(17) . . . . ?
B1 C1 B3 B7 1.6(2) . . . . ?
C3 C1 B3 B4 -104.81(17) . . . . ?
C2 C1 B3 B4 38.43(13) . . . . ?
B2 C1 B3 B4 140.43(15) . . . . ?
B1 C1 B3 B4 103.14(15) . . . . ?
C3 C1 B3 B8 -143.42(16) . . . . ?
C2 C1 B3 B8 -0.18(18) . . . . ?
B2 C1 B3 B8 101.82(16) . . . . ?
B4 C1 B3 B8 -38.61(13) . . . . ?
B1 C1 B3 B8 64.53(18) . . . . ?
B1 B2 B3 C1 35.54(14) . . . . ?
B7 B2 B3 C1 135.79(16) . . . . ?
B6 B2 B3 C1 98.37(15) . . . . ?
C1 B2 B3 B7 -135.79(16) . . . . ?
B1 B2 B3 B7 -100.25(17) . . . . ?
B6 B2 B3 B7 -37.42(15) . . . . ?
C1 B2 B3 B4 -35.60(13) . . . . ?
B1 B2 B3 B4 -0.1(2) . . . . ?
B7 B2 B3 B4 100.20(17) . . . . ?
B6 B2 B3 B4 62.78(18) . . . . ?
C1 B2 B3 B8 -98.19(15) . . . . ?
B1 B2 B3 B8 -62.65(18) . . . . ?
B7 B2 B3 B8 37.60(14) . . . . ?
B6 B2 B3 B8 0.18(19) . . . . ?
C9 C2 B4 C1 104.77(16) . . . . ?
B5 C2 B4 C1 -102.48(16) . . . . ?
B9 C2 B4 C1 -139.15(15) . . . . ?
B1 C2 B4 C1 -33.23(13) . . . . ?
C9 C2 B4 B8 -156.34(16) . . . . ?
C1 C2 B4 B8 98.89(15) . . . . ?
B5 C2 B4 B8 -3.6(2) . . . . ?
B9 C2 B4 B8 -40.26(15) . . . . ?
B1 C2 B4 B8 65.66(18) . . . . ?
C9 C2 B4 B9 -116.08(17) . . . . ?
C1 C2 B4 B9 139.15(15) . . . . ?
B5 C2 B4 B9 36.68(16) . . . . ?
B1 C2 B4 B9 105.92(16) . . . . ?
C9 C2 B4 B3 140.95(16) . . . . ?
C1 C2 B4 B3 36.18(13) . . . . ?
B5 C2 B4 B3 -66.29(18) . . . . ?
B9 C2 B4 B3 -102.97(15) . . . . ?
B1 C2 B4 B3 2.95(19) . . . . ?
C3 C1 B4 C2 -108.02(15) . . . . ?
B3 C1 B4 C2 137.38(14) . . . . ?
B2 C1 B4 C2 99.22(15) . . . . ?
B1 C1 B4 C2 32.10(13) . . . . ?
C3 C1 B4 B8 153.60(15) . . . . ?
C2 C1 B4 B8 -98.38(15) . . . . ?
B3 C1 B4 B8 39.00(14) . . . . ?
B2 C1 B4 B8 0.84(19) . . . . ?
B1 C1 B4 B8 -66.28(17) . . . . ?
C3 C1 B4 B9 -143.49(14) . . . . ?
C2 C1 B4 B9 -35.47(13) . . . . ?
B3 C1 B4 B9 101.91(15) . . . . ?
B2 C1 B4 B9 63.75(17) . . . . ?
B1 C1 B4 B9 -3.38(18) . . . . ?
C3 C1 B4 B3 114.60(16) . . . . ?
C2 C1 B4 B3 -137.38(14) . . . . ?
B2 C1 B4 B3 -38.16(14) . . . . ?
B1 C1 B4 B3 -105.29(15) . . . . ?
C1 B3 B4 C2 -36.65(12) . . . . ?
B2 B3 B4 C2 -1.67(19) . . . . ?
B7 B3 B4 C2 61.85(17) . . . . ?
B8 B3 B4 C2 99.05(15) . . . . ?
B2 B3 B4 C1 34.99(13) . . . . ?
B7 B3 B4 C1 98.51(15) . . . . ?
B8 B3 B4 C1 135.70(15) . . . . ?
C1 B3 B4 B8 -135.70(15) . . . . ?
B2 B3 B4 B8 -100.71(16) . . . . ?
B7 B3 B4 B8 -37.19(14) . . . . ?
C1 B3 B4 B9 -97.77(14) . . . . ?
B2 B3 B4 B9 -62.78(18) . . . . ?
B7 B3 B4 B9 0.74(18) . . . . ?
B8 B3 B4 B9 37.93(13) . . . . ?
C9 C2 B5 B10 154.32(17) . . . . ?
C1 C2 B5 B10 -63.66(18) . . . . ?
B9 C2 B5 B10 40.17(15) . . . . ?
B4 C2 B5 B10 3.6(2) . . . . ?
B1 C2 B5 B10 -101.78(16) . . . . ?
C9 C2 B5 B6 -143.26(17) . . . . ?
C1 C2 B5 B6 -1.25(18) . . . . ?
B9 C2 B5 B6 102.58(16) . . . . ?
B4 C2 B5 B6 66.02(18) . . . . ?
B1 C2 B5 B6 -39.36(14) . . . . ?
C9 C2 B5 B9 114.15(19) . . . . ?
C1 C2 B5 B9 -103.83(15) . . . . ?
B4 C2 B5 B9 -36.56(15) . . . . ?
B1 C2 B5 B9 -141.95(15) . . . . ?
C9 C2 B5 B1 -103.90(19) . . . . ?
C1 C2 B5 B1 38.11(13) . . . . ?
B9 C2 B5 B1 141.95(15) . . . . ?
B4 C2 B5 B1 105.39(15) . . . . ?
C1 B1 B5 C2 -35.45(12) . . . . ?
B6 B1 B5 C2 -134.45(15) . . . . ?
B2 B1 B5 C2 -96.58(14) . . . . ?
C2 B1 B5 B10 96.83(16) . . . . ?
C1 B1 B5 B10 61.37(18) . . . . ?
B6 B1 B5 B10 -37.63(15) . . . . ?
B2 B1 B5 B10 0.2(2) . . . . ?
C2 B1 B5 B6 134.45(15) . . . . ?
C1 B1 B5 B6 99.00(15) . . . . ?
B2 B1 B5 B6 37.87(14) . . . . ?
C2 B1 B5 B9 33.66(13) . . . . ?
C1 B1 B5 B9 -1.79(19) . . . . ?
B6 B1 B5 B9 -100.79(16) . . . . ?
B2 B1 B5 B9 -62.92(19) . . . . ?
C2 B1 B6 B5 -38.95(13) . . . . ?
C1 B1 B6 B5 -99.87(15) . . . . ?
B2 B1 B6 B5 -138.22(15) . . . . ?
C2 B1 B6 B10 -1.35(19) . . . . ?
C1 B1 B6 B10 -62.27(18) . . . . ?
B2 B1 B6 B10 -100.62(16) . . . . ?
B5 B1 B6 B10 37.60(15) . . . . ?
C2 B1 B6 B2 99.27(14) . . . . ?
C1 B1 B6 B2 38.35(13) . . . . ?
B5 B1 B6 B2 138.22(15) . . . . ?
C2 B1 B6 B7 61.99(19) . . . . ?
C1 B1 B6 B7 1.1(2) . . . . ?
B2 B1 B6 B7 -37.28(15) . . . . ?
B5 B1 B6 B7 100.94(18) . . . . ?
C2 B5 B6 B1 39.31(13) . . . . ?
B10 B5 B6 B1 137.80(15) . . . . ?
B9 B5 B6 B1 100.69(15) . . . . ?
C2 B5 B6 B10 -98.49(15) . . . . ?
B9 B5 B6 B10 -37.11(14) . . . . ?
B1 B5 B6 B10 -137.80(15) . . . . ?
C2 B5 B6 B2 1.94(19) . . . . ?
B10 B5 B6 B2 100.43(16) . . . . ?
B9 B5 B6 B2 63.33(19) . . . . ?
B1 B5 B6 B2 -37.37(14) . . . . ?
C2 B5 B6 B7 -61.52(18) . . . . ?
B10 B5 B6 B7 36.97(15) . . . . ?
B9 B5 B6 B7 -0.1(2) . . . . ?
B1 B5 B6 B7 -100.83(16) . . . . ?
C1 B2 B6 B1 -39.61(13) . . . . ?
B3 B2 B6 B1 -100.88(15) . . . . ?
B7 B2 B6 B1 -138.26(16) . . . . ?
C1 B2 B6 B5 -1.95(19) . . . . ?
B1 B2 B6 B5 37.67(14) . . . . ?
B3 B2 B6 B5 -63.21(18) . . . . ?
B7 B2 B6 B5 -100.59(17) . . . . ?
C1 B2 B6 B10 61.26(18) . . . . ?
B1 B2 B6 B10 100.87(17) . . . . ?
B3 B2 B6 B10 0.0(2) . . . . ?
B7 B2 B6 B10 -37.39(15) . . . . ?
C1 B2 B6 B7 98.65(16) . . . . ?
B1 B2 B6 B7 138.26(16) . . . . ?
B3 B2 B6 B7 37.38(14) . . . . ?
C1 B3 B7 B10 62.43(19) . . . . ?
B2 B3 B7 B10 100.70(16) . . . . ?
B4 B3 B7 B10 -0.69(19) . . . . ?
B8 B3 B7 B10 -37.40(14) . . . . ?
C1 B3 B7 B2 -38.27(14) . . . . ?
B4 B3 B7 B2 -101.39(15) . . . . ?
B8 B3 B7 B2 -138.10(15) . . . . ?
C1 B3 B7 B6 -0.9(2) . . . . ?
B2 B3 B7 B6 37.39(15) . . . . ?
B4 B3 B7 B6 -64.0(2) . . . . ?
B8 B3 B7 B6 -100.71(18) . . . . ?
C1 B3 B7 B8 99.83(16) . . . . ?
B2 B3 B7 B8 138.10(15) . . . . ?
B4 B3 B7 B8 36.71(13) . . . . ?
C1 B2 B7 B10 -62.80(18) . . . . ?
B1 B2 B7 B10 0.4(2) . . . . ?
B3 B2 B7 B10 -100.77(17) . . . . ?
B6 B2 B7 B10 37.38(15) . . . . ?
C1 B2 B7 B3 37.97(13) . . . . ?
B1 B2 B7 B3 101.19(16) . . . . ?
B6 B2 B7 B3 138.15(16) . . . . ?
C1 B2 B7 B6 -100.18(16) . . . . ?
B1 B2 B7 B6 -36.96(14) . . . . ?
B3 B2 B7 B6 -138.15(16) . . . . ?
C1 B2 B7 B8 0.55(19) . . . . ?
B1 B2 B7 B8 63.77(19) . . . . ?
B3 B2 B7 B8 -37.42(14) . . . . ?
B6 B2 B7 B8 100.73(17) . . . . ?
B1 B6 B7 B10 -100.87(18) . . . . ?
B5 B6 B7 B10 -36.90(15) . . . . ?
B2 B6 B7 B10 -138.10(16) . . . . ?
B1 B6 B7 B3 -0.1(2) . . . . ?
B5 B6 B7 B3 63.8(2) . . . . ?
B10 B6 B7 B3 100.73(18) . . . . ?
B2 B6 B7 B3 -37.37(15) . . . . ?
B1 B6 B7 B2 37.23(15) . . . . ?
B5 B6 B7 B2 101.21(16) . . . . ?
B10 B6 B7 B2 138.10(16) . . . . ?
B1 B6 B7 B8 -63.5(2) . . . . ?
B5 B6 B7 B8 0.5(2) . . . . ?
B10 B6 B7 B8 37.36(15) . . . . ?
B2 B6 B7 B8 -100.74(16) . . . . ?
C2 B4 B8 B9 39.34(14) . . . . ?
C1 B4 B8 B9 100.21(15) . . . . ?
B3 B4 B8 B9 137.85(15) . . . . ?
C2 B4 B8 B10 2.0(2) . . . . ?
C1 B4 B8 B10 62.86(19) . . . . ?
B9 B4 B8 B10 -37.35(15) . . . . ?
B3 B4 B8 B10 100.50(17) . . . . ?
C2 B4 B8 B3 -98.51(14) . . . . ?
C1 B4 B8 B3 -37.64(12) . . . . ?
B9 B4 B8 B3 -137.85(15) . . . . ?
C2 B4 B8 B7 -61.32(18) . . . . ?
C1 B4 B8 B7 -0.44(19) . . . . ?
B9 B4 B8 B7 -100.65(17) . . . . ?
B3 B4 B8 B7 37.19(14) . . . . ?
C1 B3 B8 B4 39.11(13) . . . . ?
B2 B3 B8 B4 100.84(15) . . . . ?
B7 B3 B8 B4 138.39(15) . . . . ?
C1 B3 B8 B9 1.12(19) . . . . ?
B2 B3 B8 B9 62.85(18) . . . . ?
B7 B3 B8 B9 100.40(16) . . . . ?
B4 B3 B8 B9 -37.99(14) . . . . ?
C1 B3 B8 B10 -62.01(18) . . . . ?
B2 B3 B8 B10 -0.28(19) . . . . ?
B7 B3 B8 B10 37.27(14) . . . . ?
B4 B3 B8 B10 -101.12(16) . . . . ?
C1 B3 B8 B7 -99.28(15) . . . . ?
B2 B3 B8 B7 -37.56(14) . . . . ?
B4 B3 B8 B7 -138.39(15) . . . . ?
B10 B7 B8 B4 100.66(16) . . . . ?
B3 B7 B8 B4 -37.46(14) . . . . ?
B2 B7 B8 B4 -0.1(2) . . . . ?
B6 B7 B8 B4 63.3(2) . . . . ?
B10 B7 B8 B9 36.72(14) . . . . ?
B3 B7 B8 B9 -101.40(15) . . . . ?
B2 B7 B8 B9 -64.00(19) . . . . ?
B6 B7 B8 B9 -0.6(2) . . . . ?
B3 B7 B8 B10 -138.12(15) . . . . ?
B2 B7 B8 B10 -100.72(16) . . . . ?
B6 B7 B8 B10 -37.34(15) . . . . ?
B10 B7 B8 B3 138.12(15) . . . . ?
B2 B7 B8 B3 37.40(14) . . . . ?
B6 B7 B8 B3 100.79(16) . . . . ?
C9 C2 B9 B10 -153.25(17) . . . . ?
C1 C2 B9 B10 63.96(17) . . . . ?
B5 C2 B9 B10 -40.12(14) . . . . ?
B4 C2 B9 B10 102.07(16) . . . . ?
B1 C2 B9 B10 -3.29(19) . . . . ?
C9 C2 B9 B8 144.32(17) . . . . ?
C1 C2 B9 B8 1.53(19) . . . . ?
B5 C2 B9 B8 -102.55(16) . . . . ?
B4 C2 B9 B8 39.64(13) . . . . ?
B1 C2 B9 B8 -65.72(18) . . . . ?
C9 C2 B9 B4 104.68(19) . . . . ?
C1 C2 B9 B4 -38.11(13) . . . . ?
B5 C2 B9 B4 -142.19(16) . . . . ?
B1 C2 B9 B4 -105.36(15) . . . . ?
C9 C2 B9 B5 -113.13(19) . . . . ?
C1 C2 B9 B5 104.08(15) . . . . ?
B4 C2 B9 B5 142.19(15) . . . . ?
B1 C2 B9 B5 36.83(14) . . . . ?
B4 B8 B9 C2 -39.59(13) . . . . ?
B10 B8 B9 C2 98.49(16) . . . . ?
B3 B8 B9 C2 -1.60(19) . . . . ?
B7 B8 B9 C2 61.71(18) . . . . ?
B4 B8 B9 B10 -138.07(16) . . . . ?
B3 B8 B9 B10 -100.09(17) . . . . ?
B7 B8 B9 B10 -36.77(15) . . . . ?
B10 B8 B9 B4 138.07(16) . . . . ?
B3 B8 B9 B4 37.99(14) . . . . ?
B7 B8 B9 B4 101.30(16) . . . . ?
B4 B8 B9 B5 -100.77(15) . . . . ?
B10 B8 B9 B5 37.31(15) . . . . ?
B3 B8 B9 B5 -62.78(18) . . . . ?
B7 B8 B9 B5 0.5(2) . . . . ?
C1 B4 B9 C2 35.53(12) . . . . ?
B8 B4 B9 C2 134.04(15) . . . . ?
B3 B4 B9 C2 96.06(14) . . . . ?
C2 B4 B9 B10 -96.57(16) . . . . ?
C1 B4 B9 B10 -61.04(17) . . . . ?
B8 B4 B9 B10 37.47(15) . . . . ?
B3 B4 B9 B10 -0.51(19) . . . . ?
C2 B4 B9 B8 -134.04(15) . . . . ?
C1 B4 B9 B8 -98.51(15) . . . . ?
B3 B4 B9 B8 -37.98(14) . . . . ?
C2 B4 B9 B5 -33.40(13) . . . . ?
C1 B4 B9 B5 2.13(18) . . . . ?
B8 B4 B9 B5 100.64(17) . . . . ?
B3 B4 B9 B5 62.65(17) . . . . ?
B10 B5 B9 C2 -133.77(16) . . . . ?
B6 B5 B9 C2 -96.51(16) . . . . ?
B1 B5 B9 C2 -33.83(13) . . . . ?
C2 B5 B9 B10 133.77(16) . . . . ?
B6 B5 B9 B10 37.25(15) . . . . ?
B1 B5 B9 B10 99.94(17) . . . . ?
C2 B5 B9 B8 96.26(15) . . . . ?
B10 B5 B9 B8 -37.50(15) . . . . ?
B6 B5 B9 B8 -0.2(2) . . . . ?
B1 B5 B9 B8 62.44(18) . . . . ?
C2 B5 B9 B4 33.62(13) . . . . ?
B10 B5 B9 B4 -100.15(17) . . . . ?
B6 B5 B9 B4 -62.90(18) . . . . ?
B1 B5 B9 B4 -0.2(2) . . . . ?
C2 B5 B10 B9 -39.60(14) . . . . ?
B6 B5 B10 B9 -138.48(16) . . . . ?
B1 B5 B10 B9 -101.27(16) . . . . ?
C2 B5 B10 B6 98.88(16) . . . . ?
B9 B5 B10 B6 138.48(16) . . . . ?
B1 B5 B10 B6 37.21(14) . . . . ?
C2 B5 B10 B7 61.70(19) . . . . ?
B6 B5 B10 B7 -37.19(15) . . . . ?
B9 B5 B10 B7 101.30(17) . . . . ?
B1 B5 B10 B7 0.0(2) . . . . ?
C2 B5 B10 B8 -2.1(2) . . . . ?
B6 B5 B10 B8 -101.00(18) . . . . ?
B9 B5 B10 B8 37.48(16) . . . . ?
B1 B5 B10 B8 -63.8(2) . . . . ?
C2 B9 B10 B5 39.51(14) . . . . ?
B8 B9 B10 B5 138.19(16) . . . . ?
B4 B9 B10 B5 101.17(16) . . . . ?
C2 B9 B10 B6 2.2(2) . . . . ?
B8 B9 B10 B6 100.91(18) . . . . ?
B4 B9 B10 B6 63.90(19) . . . . ?
B5 B9 B10 B6 -37.28(15) . . . . ?
C2 B9 B10 B7 -61.58(18) . . . . ?
B8 B9 B10 B7 37.10(15) . . . . ?
B4 B9 B10 B7 0.1(2) . . . . ?
B5 B9 B10 B7 -101.09(17) . . . . ?
C2 B9 B10 B8 -98.68(16) . . . . ?
B4 B9 B10 B8 -37.02(14) . . . . ?
B5 B9 B10 B8 -138.19(16) . . . . ?
B1 B6 B10 B5 -37.95(14) . . . . ?
B2 B6 B10 B5 -101.21(16) . . . . ?
B7 B6 B10 B5 -138.61(16) . . . . ?
B1 B6 B10 B9 -0.6(2) . . . . ?
B5 B6 B10 B9 37.39(15) . . . . ?
B2 B6 B10 B9 -63.8(2) . . . . ?
B7 B6 B10 B9 -101.22(17) . . . . ?
B1 B6 B10 B7 100.67(16) . . . . ?
B5 B6 B10 B7 138.61(16) . . . . ?
B2 B6 B10 B7 37.41(14) . . . . ?
B1 B6 B10 B8 63.1(2) . . . . ?
B5 B6 B10 B8 101.04(16) . . . . ?
B2 B6 B10 B8 -0.2(2) . . . . ?
B7 B6 B10 B8 -37.57(15) . . . . ?
B3 B7 B10 B5 -63.6(2) . . . . ?
B2 B7 B10 B5 -0.3(2) . . . . ?
B6 B7 B10 B5 37.15(15) . . . . ?
B8 B7 B10 B5 -101.01(17) . . . . ?
B3 B7 B10 B9 0.4(2) . . . . ?
B2 B7 B10 B9 63.71(19) . . . . ?
B6 B7 B10 B9 101.13(17) . . . . ?
B8 B7 B10 B9 -37.03(14) . . . . ?
B3 B7 B10 B6 -100.75(16) . . . . ?
B2 B7 B10 B6 -37.42(14) . . . . ?
B8 B7 B10 B6 -138.16(16) . . . . ?
B3 B7 B10 B8 37.40(14) . . . . ?
B2 B7 B10 B8 100.74(16) . . . . ?
B6 B7 B10 B8 138.16(16) . . . . ?
B4 B8 B10 B5 0.1(2) . . . . ?
B9 B8 B10 B5 -37.60(15) . . . . ?
B3 B8 B10 B5 63.9(2) . . . . ?
B7 B8 B10 B5 101.18(18) . . . . ?
B4 B8 B10 B9 37.67(15) . . . . ?
B3 B8 B10 B9 101.51(15) . . . . ?
B7 B8 B10 B9 138.78(15) . . . . ?
B4 B8 B10 B6 -63.6(2) . . . . ?
B9 B8 B10 B6 -101.23(17) . . . . ?
B3 B8 B10 B6 0.3(2) . . . . ?
B7 B8 B10 B6 37.55(15) . . . . ?
B4 B8 B10 B7 -101.11(17) . . . . ?
B9 B8 B10 B7 -138.78(15) . . . . ?
B3 B8 B10 B7 -37.27(14) . . . . ?

_refine_diff_density_max         0.253
_refine_diff_density_min         -0.282
_refine_diff_density_rms         0.047



