# Electronic Supplementary Material (ESI) for ChemComm.
# This journal is © The Royal Society of Chemistry 2021

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_cu_0825_5_0ma
_database_code_depnum_ccdc_archive 'CCDC 2025268'
loop_
_audit_author_name
_audit_author_address
'Penghui Dong'
;Northwestern Polytechnical University
China
;
_audit_update_record             
;
2020-11-26 deposited with the CCDC.	2021-04-07 downloaded from the CCDC.
;
_audit_creation_date             2020-08-25
_audit_creation_method           
;
Olex2 1.3
(compiled Nov 21 2019 18:26:39 for OlexSys, GUI svn.r6003)
;
_shelx_SHELXL_version_number     2018/3
_chemical_name_common            ?
_chemical_name_systematic        
'ethyl 10-phenylacenaphtho[1,2-c]pyridine-7-carboxylate'
_chemical_formula_moiety         'C24 H17 N O2'
_chemical_formula_sum            'C24 H17 N O2'
_chemical_formula_weight         351.38
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_H-M_alt        'P 1 21/c 1'
_space_group_name_Hall           '-P 2ybc'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'

_cell_length_a                   11.9988(3)
_cell_length_b                   19.1984(5)
_cell_length_c                   7.6672(2)
_cell_angle_alpha                90
_cell_angle_beta                 106.467(2)
_cell_angle_gamma                90
_cell_volume                     1693.75(8)
_cell_formula_units_Z            4
_cell_measurement_reflns_used    5629
_cell_measurement_temperature    150.0
_cell_measurement_theta_max      74.13
_cell_measurement_theta_min      4.48
_shelx_estimated_absorpt_T_max   0.934
_shelx_estimated_absorpt_T_min   0.873
_exptl_absorpt_coefficient_mu    0.697
_exptl_absorpt_correction_T_max  0.7538
_exptl_absorpt_correction_T_min  0.6404
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
;
SADABS-2016/2 (Bruker,2016/2) was used for absorption correction.
wR2(int) was 0.1336 before and 0.0652 after correction.
The Ratio of minimum to maximum transmission is 0.8496.
The λ/2 correction factor is Not present.
;
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            colourless
_exptl_crystal_colour_primary    colourless
_exptl_crystal_density_diffrn    1.378
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       block
_exptl_crystal_F_000             736
_exptl_crystal_size_max          0.2
_exptl_crystal_size_mid          0.15
_exptl_crystal_size_min          0.1
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0650
_diffrn_reflns_av_unetI/netI     0.0353
_diffrn_reflns_Laue_measured_fraction_full 0.997
_diffrn_reflns_Laue_measured_fraction_max 0.993
_diffrn_reflns_limit_h_max       14
_diffrn_reflns_limit_h_min       -14
_diffrn_reflns_limit_k_max       23
_diffrn_reflns_limit_k_min       -23
_diffrn_reflns_limit_l_max       9
_diffrn_reflns_limit_l_min       -9
_diffrn_reflns_number            24320
_diffrn_reflns_point_group_measured_fraction_full 0.997
_diffrn_reflns_point_group_measured_fraction_max 0.993
_diffrn_reflns_theta_full        67.679
_diffrn_reflns_theta_max         74.610
_diffrn_reflns_theta_min         3.841
_diffrn_ambient_temperature      150.0
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 0.997
_diffrn_measured_fraction_theta_max 0.993
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_type           CuK\a
_diffrn_radiation_wavelength     1.54178
_diffrn_source                   ?
_diffrn_source_current           1.0
_diffrn_source_power             0.05
_diffrn_source_voltage           50.0
_diffrn_standards_number         0
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                2744
_reflns_number_total             3446
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       'SAINT v8.37A (Bruker, 2015)'
_computing_data_collection       ?
_computing_data_reduction        'SAINT v8.37A (Bruker, 2015)'
_computing_molecular_graphics    'Olex2 1.3 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 1.3 (Dolomanov et al., 2009)'
_computing_structure_refinement  'SHELXL 2018/3 (Sheldrick, 2015)'
_computing_structure_solution    'SHELXT 2018/2 (Sheldrick, 2018)'
_refine_diff_density_max         0.250
_refine_diff_density_min         -0.307
_refine_diff_density_rms         0.098
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.095
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     245
_refine_ls_number_reflns         3446
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.0586
_refine_ls_R_factor_gt           0.0403
_refine_ls_restrained_S_all      1.095
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0711P)²+0.1971P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1056
_refine_ls_wR_factor_ref         0.1241
_refine_special_details          ?
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H) groups, All C(H,H) groups
 At 1.5 times of:
  All C(H,H,H) groups
2.a Secondary CH2 refined with riding coordinates:
 C00K(H00A,H00B)
2.b Aromatic/amide H refined with riding coordinates:
 C004(H004), C00D(H00D), C00F(H00F), C00G(H00G), C00H(H00H), C00J(H00J),
 C00L(H00L), C00M(H00M), C00N(H00N), C00O(H00O), C00P(H00P), C00Q(H00Q)
2.c Idealised Me refined as rotating group:
 C00R(H00C,H00E,H00I)
;
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     dual
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
O001 O 0.22744(9) 0.52101(5) -0.01124(15) 0.0251(3) Uani 1 1 d . . . . .
O002 O 0.11995(9) 0.60769(6) 0.05288(17) 0.0320(3) Uani 1 1 d . . . . .
N003 N 0.40206(11) 0.55699(6) 0.27834(18) 0.0226(3) Uani 1 1 d . . . . .
C004 C 0.73503(13) 0.70702(8) 0.4451(2) 0.0220(3) Uani 1 1 d . . . . .
H004 H 0.698071 0.735887 0.344704 0.026 Uiso 1 1 calc R U . . .
C005 C 0.35175(12) 0.67760(7) 0.2191(2) 0.0185(3) Uani 1 1 d . . . . .
C006 C 0.46355(12) 0.69778(7) 0.33413(19) 0.0182(3) Uani 1 1 d . . . . .
C007 C 0.21324(13) 0.58002(8) 0.0732(2) 0.0219(3) Uani 1 1 d . . . . .
C008 C 0.54473(12) 0.64648(7) 0.41190(19) 0.0187(3) Uani 1 1 d . . . . .
C009 C 0.46742(12) 0.77490(7) 0.3423(2) 0.0191(3) Uani 1 1 d . . . . .
C00A C 0.28696(13) 0.74176(7) 0.1446(2) 0.0195(3) Uani 1 1 d . . . . .
C00B C 0.36054(12) 0.79772(7) 0.2248(2) 0.0194(3) Uani 1 1 d . . . . .
C00C C 0.66931(12) 0.65841(7) 0.5097(2) 0.0200(3) Uani 1 1 d . . . . .
C00D C 0.85396(13) 0.71345(8) 0.5264(2) 0.0260(3) Uani 1 1 d . . . . .
H00D H 0.897612 0.746997 0.482456 0.031 Uiso 1 1 calc R U . . .
C00E C 0.32668(12) 0.60683(7) 0.1941(2) 0.0202(3) Uani 1 1 d . . . . .
C00F C 0.72599(13) 0.61621(8) 0.6578(2) 0.0233(3) Uani 1 1 d . . . . .
H00F H 0.682844 0.583103 0.704103 0.028 Uiso 1 1 calc R U . . .
C00G C 0.90886(13) 0.67088(9) 0.6717(2) 0.0281(4) Uani 1 1 d . . . . .
H00G H 0.990218 0.674856 0.726320 0.034 Uiso 1 1 calc R U . . .
C00H C 0.50577(13) 0.57741(8) 0.3821(2) 0.0222(3) Uani 1 1 d . . . . .
H00H H 0.558176 0.541974 0.441244 0.027 Uiso 1 1 calc R U . . .
C00I C 0.33052(13) 0.86808(8) 0.1924(2) 0.0225(3) Uani 1 1 d . . . . .
C00J C 0.84484(13) 0.62267(9) 0.7367(2) 0.0279(4) Uani 1 1 d . . . . .
H00J H 0.882592 0.593696 0.836368 0.033 Uiso 1 1 calc R U . . .
C00K C 0.12393(13) 0.49503(8) -0.1443(2) 0.0271(4) Uani 1 1 d . . . . .
H00A H 0.092179 0.530880 -0.237978 0.032 Uiso 1 1 calc R U . . .
H00B H 0.063501 0.482944 -0.084276 0.032 Uiso 1 1 calc R U . . .
C00L C 0.18097(13) 0.75711(8) 0.0240(2) 0.0247(3) Uani 1 1 d . . . . .
H00L H 0.128693 0.720931 -0.030662 0.030 Uiso 1 1 calc R U . . .
C00M C 0.54495(13) 0.82407(8) 0.4369(2) 0.0220(3) Uani 1 1 d . . . . .
H00M H 0.616656 0.810296 0.519517 0.026 Uiso 1 1 calc R U . . .
C00N C 0.41273(14) 0.91726(8) 0.2899(2) 0.0261(3) Uani 1 1 d . . . . .
H00N H 0.396588 0.965641 0.273101 0.031 Uiso 1 1 calc R U . . .
C00O C 0.15104(14) 0.82808(9) -0.0175(2) 0.0281(4) Uani 1 1 d . . . . .
H00O H 0.079269 0.838564 -0.104697 0.034 Uiso 1 1 calc R U . . .
C00P C 0.51577(14) 0.89559(8) 0.4086(2) 0.0256(3) Uani 1 1 d . . . . .
H00P H 0.569025 0.929577 0.473759 0.031 Uiso 1 1 calc R U . . .
C00Q C 0.22196(14) 0.88196(8) 0.0636(2) 0.0275(4) Uani 1 1 d . . . . .
H00Q H 0.198337 0.928721 0.033474 0.033 Uiso 1 1 calc R U . . .
C00R C 0.15941(16) 0.43143(10) -0.2296(3) 0.0386(4) Uani 1 1 d . . . . .
H00C H 0.093022 0.414334 -0.326727 0.058 Uiso 1 1 calc R U . . .
H00E H 0.185182 0.395102 -0.137125 0.058 Uiso 1 1 calc R U . . .
H00I H 0.223165 0.443363 -0.280628 0.058 Uiso 1 1 calc R U . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
O001 C007 1.3396(18) . ?
O001 C00K 1.4538(17) . ?
O002 C007 1.2085(18) . ?
N003 C00E 1.3488(18) . ?
N003 C00H 1.3318(19) . ?
C004 H004 0.9500 . ?
C004 C00C 1.400(2) . ?
C004 C00D 1.391(2) . ?
C005 C006 1.4342(19) . ?
C005 C00A 1.4818(19) . ?
C005 C00E 1.393(2) . ?
C006 C008 1.3946(19) . ?
C006 C009 1.4822(19) . ?
C007 C00E 1.5039(19) . ?
C008 C00C 1.4879(19) . ?
C008 C00H 1.403(2) . ?
C009 C00B 1.412(2) . ?
C009 C00M 1.378(2) . ?
C00A C00B 1.416(2) . ?
C00A C00L 1.376(2) . ?
C00B C00I 1.402(2) . ?
C00C C00F 1.404(2) . ?
C00D H00D 0.9500 . ?
C00D C00G 1.388(2) . ?
C00F H00F 0.9500 . ?
C00F C00J 1.388(2) . ?
C00G H00G 0.9500 . ?
C00G C00J 1.383(2) . ?
C00H H00H 0.9500 . ?
C00I C00N 1.416(2) . ?
C00I C00Q 1.419(2) . ?
C00J H00J 0.9500 . ?
C00K H00A 0.9900 . ?
C00K H00B 0.9900 . ?
C00K C00R 1.503(2) . ?
C00L H00L 0.9500 . ?
C00L C00O 1.422(2) . ?
C00M H00M 0.9500 . ?
C00M C00P 1.418(2) . ?
C00N H00N 0.9500 . ?
C00N C00P 1.376(2) . ?
C00O H00O 0.9500 . ?
C00O C00Q 1.371(2) . ?
C00P H00P 0.9500 . ?
C00Q H00Q 0.9500 . ?
C00R H00C 0.9800 . ?
C00R H00E 0.9800 . ?
C00R H00I 0.9800 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C007 O001 C00K 115.40(12) . . ?
C00H N003 C00E 117.59(12) . . ?
C00C C004 H004 119.7 . . ?
C00D C004 H004 119.7 . . ?
C00D C004 C00C 120.64(14) . . ?
C006 C005 C00A 108.03(12) . . ?
C00E C005 C006 118.41(13) . . ?
C00E C005 C00A 133.52(13) . . ?
C005 C006 C009 107.96(12) . . ?
C008 C006 C005 119.37(13) . . ?
C008 C006 C009 132.66(13) . . ?
O001 C007 C00E 111.74(12) . . ?
O002 C007 O001 123.33(14) . . ?
O002 C007 C00E 124.93(14) . . ?
C006 C008 C00C 125.94(13) . . ?
C006 C008 C00H 115.95(13) . . ?
C00H C008 C00C 117.92(13) . . ?
C00B C009 C006 105.73(12) . . ?
C00M C009 C006 135.61(13) . . ?
C00M C009 C00B 118.61(13) . . ?
C00B C00A C005 105.61(12) . . ?
C00L C00A C005 136.14(14) . . ?
C00L C00A C00B 118.24(13) . . ?
C009 C00B C00A 112.55(13) . . ?
C00I C00B C009 123.60(14) . . ?
C00I C00B C00A 123.85(14) . . ?
C004 C00C C008 120.69(13) . . ?
C004 C00C C00F 118.60(13) . . ?
C00F C00C C008 120.40(13) . . ?
C004 C00D H00D 120.0 . . ?
C00G C00D C004 120.03(15) . . ?
C00G C00D H00D 120.0 . . ?
N003 C00E C005 122.47(13) . . ?
N003 C00E C007 114.78(12) . . ?
C005 C00E C007 122.74(13) . . ?
C00C C00F H00F 119.9 . . ?
C00J C00F C00C 120.23(15) . . ?
C00J C00F H00F 119.9 . . ?
C00D C00G H00G 120.1 . . ?
C00J C00G C00D 119.85(14) . . ?
C00J C00G H00G 120.1 . . ?
N003 C00H C008 125.97(14) . . ?
N003 C00H H00H 117.0 . . ?
C008 C00H H00H 117.0 . . ?
C00B C00I C00N 116.32(14) . . ?
C00B C00I C00Q 116.32(14) . . ?
C00N C00I C00Q 127.35(14) . . ?
C00F C00J H00J 119.7 . . ?
C00G C00J C00F 120.65(15) . . ?
C00G C00J H00J 119.7 . . ?
O001 C00K H00A 110.3 . . ?
O001 C00K H00B 110.3 . . ?
O001 C00K C00R 107.05(13) . . ?
H00A C00K H00B 108.6 . . ?
C00R C00K H00A 110.3 . . ?
C00R C00K H00B 110.3 . . ?
C00A C00L H00L 120.6 . . ?
C00A C00L C00O 118.84(15) . . ?
C00O C00L H00L 120.6 . . ?
C009 C00M H00M 120.6 . . ?
C009 C00M C00P 118.81(14) . . ?
C00P C00M H00M 120.6 . . ?
C00I C00N H00N 119.7 . . ?
C00P C00N C00I 120.56(14) . . ?
C00P C00N H00N 119.7 . . ?
C00L C00O H00O 118.8 . . ?
C00Q C00O C00L 122.43(15) . . ?
C00Q C00O H00O 118.8 . . ?
C00M C00P H00P 119.0 . . ?
C00N C00P C00M 122.04(14) . . ?
C00N C00P H00P 119.0 . . ?
C00I C00Q H00Q 119.9 . . ?
C00O C00Q C00I 120.21(14) . . ?
C00O C00Q H00Q 119.9 . . ?
C00K C00R H00C 109.5 . . ?
C00K C00R H00E 109.5 . . ?
C00K C00R H00I 109.5 . . ?
H00C C00R H00E 109.5 . . ?
H00C C00R H00I 109.5 . . ?
H00E C00R H00I 109.5 . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
O001 C007 C00E N003 -35.84(19) . . . . ?
O001 C007 C00E C005 144.84(14) . . . . ?
O002 C007 C00E N003 144.31(16) . . . . ?
O002 C007 C00E C005 -35.0(2) . . . . ?
C004 C00C C00F C00J -0.4(2) . . . . ?
C004 C00D C00G C00J -0.8(2) . . . . ?
C005 C006 C008 C00C 169.90(14) . . . . ?
C005 C006 C008 C00H -5.1(2) . . . . ?
C005 C006 C009 C00B -2.94(16) . . . . ?
C005 C006 C009 C00M 174.51(17) . . . . ?
C005 C00A C00B C009 0.79(17) . . . . ?
C005 C00A C00B C00I -178.81(14) . . . . ?
C005 C00A C00L C00O -177.89(16) . . . . ?
C006 C005 C00A C00B -2.65(16) . . . . ?
C006 C005 C00A C00L 176.56(17) . . . . ?
C006 C005 C00E N003 2.1(2) . . . . ?
C006 C005 C00E C007 -178.64(13) . . . . ?
C006 C008 C00C C004 -40.9(2) . . . . ?
C006 C008 C00C C00F 145.58(15) . . . . ?
C006 C008 C00H N003 4.4(2) . . . . ?
C006 C009 C00B C00A 1.30(17) . . . . ?
C006 C009 C00B C00I -179.10(14) . . . . ?
C006 C009 C00M C00P -178.97(16) . . . . ?
C007 O001 C00K C00R 177.04(14) . . . . ?
C008 C006 C009 C00B 176.19(15) . . . . ?
C008 C006 C009 C00M -6.4(3) . . . . ?
C008 C00C C00F C00J 173.31(14) . . . . ?
C009 C006 C008 C00C -9.2(3) . . . . ?
C009 C006 C008 C00H 175.84(15) . . . . ?
C009 C00B C00I C00N -2.1(2) . . . . ?
C009 C00B C00I C00Q 177.01(14) . . . . ?
C009 C00M C00P C00N -0.1(2) . . . . ?
C00A C005 C006 C008 -175.80(13) . . . . ?
C00A C005 C006 C009 3.47(16) . . . . ?
C00A C005 C00E N003 179.50(15) . . . . ?
C00A C005 C00E C007 -1.2(3) . . . . ?
C00A C00B C00I C00N 177.49(14) . . . . ?
C00A C00B C00I C00Q -3.4(2) . . . . ?
C00A C00L C00O C00Q -2.6(3) . . . . ?
C00B C009 C00M C00P -1.8(2) . . . . ?
C00B C00A C00L C00O 1.2(2) . . . . ?
C00B C00I C00N C00P 0.1(2) . . . . ?
C00B C00I C00Q C00O 2.0(2) . . . . ?
C00C C004 C00D C00G 0.8(2) . . . . ?
C00C C008 C00H N003 -171.06(14) . . . . ?
C00C C00F C00J C00G 0.4(2) . . . . ?
C00D C004 C00C C008 -173.87(14) . . . . ?
C00D C004 C00C C00F -0.2(2) . . . . ?
C00D C00G C00J C00F 0.2(2) . . . . ?
C00E N003 C00H C008 -0.3(2) . . . . ?
C00E C005 C006 C008 2.2(2) . . . . ?
C00E C005 C006 C009 -178.51(13) . . . . ?
C00E C005 C00A C00B 179.75(16) . . . . ?
C00E C005 C00A C00L -1.0(3) . . . . ?
C00H N003 C00E C005 -3.1(2) . . . . ?
C00H N003 C00E C007 177.59(13) . . . . ?
C00H C008 C00C C004 134.05(15) . . . . ?
C00H C008 C00C C00F -39.5(2) . . . . ?
C00I C00N C00P C00M 0.9(2) . . . . ?
C00K O001 C007 O002 5.5(2) . . . . ?
C00K O001 C007 C00E -174.32(12) . . . . ?
C00L C00A C00B C009 -178.59(13) . . . . ?
C00L C00A C00B C00I 1.8(2) . . . . ?
C00L C00O C00Q C00I 0.9(3) . . . . ?
C00M C009 C00B C00A -176.67(13) . . . . ?
C00M C009 C00B C00I 2.9(2) . . . . ?
C00N C00I C00Q C00O -179.03(16) . . . . ?
C00Q C00I C00N C00P -178.83(15) . . . . ?

_olex2_submission_special_instructions 'No special instructions were received'
_exptl_crystal_recrystallization_method 
'Re-crystallisation from solvent: petroleum ether/dichloromethane'
