# Electronic Supplementary Material (ESI) for Dalton Transactions.
# This journal is © The Royal Society of Chemistry 2021

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
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data_0515003
_database_code_depnum_ccdc_archive 'CCDC 2101157'
_audit_update_record             
;
2021-08-03 deposited with the CCDC.	2021-12-01 downloaded from the CCDC.
;
_audit_creation_date             2021-06-30
_audit_creation_method           
;
Olex2 1.3
(compiled 2020.11.12 svn.r5f609507 for OlexSys, GUI svn.r6272)
;
_shelx_SHELXL_version_number     2018/3
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         'B14 O24 Sr3'
_chemical_formula_sum            'B14 O24 Sr3'
_chemical_formula_weight         798.20
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sr Sr -1.5307 3.2498 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_H-M_alt        'P 1 21/c 1'
_space_group_name_Hall           '-P 2ybc'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'

_cell_length_a                   6.6479(3)
_cell_length_b                   11.6182(5)
_cell_length_c                   21.8990(8)
_cell_angle_alpha                90
_cell_angle_beta                 93.3070(10)
_cell_angle_gamma                90
_cell_volume                     1688.59(12)
_cell_formula_units_Z            4
_cell_measurement_reflns_used    9436
_cell_measurement_temperature    153.0
_cell_measurement_theta_max      27.45
_cell_measurement_theta_min      3.07
_shelx_estimated_absorpt_T_max   0.343
_shelx_estimated_absorpt_T_min   0.258
_exptl_absorpt_coefficient_mu    9.587
_exptl_absorpt_correction_T_max  0.7456
_exptl_absorpt_correction_T_min  0.1643
_exptl_absorpt_correction_type   none
_exptl_absorpt_process_details   
;
SADABS-2016/2 (Bruker,2016/2) was used for absorption correction.
wR2(int) was 0.0816 before and 0.0687 after correction.
The Ratio of minimum to maximum transmission is 0.2204.
The λ/2 correction factor is Not present.
;
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            ?
_exptl_crystal_density_diffrn    3.140
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       ?
_exptl_crystal_F_000             1504
loop_
_exptl_crystal_face_index_h
_exptl_crystal_face_index_k
_exptl_crystal_face_index_l
_exptl_crystal_face_perp_dist
1.00 0.00 1.00 0.0970
-1.00 0.00 -1.00 0.0610
1.00 -1.00 -1.00 0.1010
-1.00 1.00 1.00 0.0960
0.00 0.00 -1.00 0.0130
0.00 0.00 1.00 0.0660
0.00 -1.00 0.00 0.0750
0.00 1.00 0.00 0.0500
-1.00 -1.00 -1.00 0.0750
-1.00 -1.00 1.00 0.0880

_exptl_crystal_size_max          0.194
_exptl_crystal_size_mid          0.144
_exptl_crystal_size_min          0.142
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0988
_diffrn_reflns_av_unetI/netI     0.0707
_diffrn_reflns_Laue_measured_fraction_full 1.000
_diffrn_reflns_Laue_measured_fraction_max 0.995
_diffrn_reflns_limit_h_max       8
_diffrn_reflns_limit_h_min       -8
_diffrn_reflns_limit_k_max       15
_diffrn_reflns_limit_k_min       -15
_diffrn_reflns_limit_l_max       28
_diffrn_reflns_limit_l_min       -22
_diffrn_reflns_number            20175
_diffrn_reflns_point_group_measured_fraction_full 1.000
_diffrn_reflns_point_group_measured_fraction_max 0.995
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         27.511
_diffrn_reflns_theta_min         1.863
_diffrn_ambient_temperature      153.0
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 0.995
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   ?
_diffrn_source_current           1.4
_diffrn_source_power             0.07
_diffrn_source_voltage           50.0
_diffrn_standards_number         0
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                2530
_reflns_number_total             3866
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       'SAINT V8.38A (Bruker, 2018)'
_computing_data_collection       ?
_computing_data_reduction        'SAINT V8.38A (Bruker, 2018)'
_computing_molecular_graphics    'Olex2 1.3 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 1.3 (Dolomanov et al., 2009)'
_computing_structure_refinement  'SHELXL 2018/3 (Sheldrick, 2015)'
_computing_structure_solution    'SHELXT 2014/5 (Sheldrick, 2014)'
_refine_diff_density_max         1.852
_refine_diff_density_min         -0.763
_refine_diff_density_rms         0.188
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.009
_refine_ls_hydrogen_treatment    undef
_refine_ls_matrix_type           full
_refine_ls_number_parameters     370
_refine_ls_number_reflns         3866
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.0881
_refine_ls_R_factor_gt           0.0437
_refine_ls_restrained_S_all      1.009
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0535P)²+0.8174P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0954
_refine_ls_wR_factor_ref         0.1118
_refine_special_details          ?
_olex2_refinement_description    
;
;
_atom_sites_solution_hydrogens   .
_atom_sites_solution_primary     dual
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
B1 B 1.3910(10) 0.3314(6) 0.9300(3) 0.0128(14) Uani 1 1 d . . . . .
B2 B 1.4570(11) 0.7040(6) 0.8132(4) 0.0180(16) Uani 1 1 d . . . . .
B3 B 1.1615(11) 0.5912(6) 0.7925(3) 0.0167(15) Uani 1 1 d . . . . .
B4 B 1.0306(10) 0.2865(5) 0.9055(3) 0.0123(14) Uani 1 1 d . . . . .
B5 B 1.2788(10) 0.1334(6) 0.9321(3) 0.0134(15) Uani 1 1 d . . . . .
B6 B 0.7354(9) 0.4220(5) 0.9143(3) 0.0102(14) Uani 1 1 d . . . . .
B7 B 0.8461(10) 0.4758(6) 0.8116(3) 0.0160(15) Uani 1 1 d . . . . .
B8 B 0.7275(10) 0.4686(6) 0.6949(3) 0.0149(15) Uani 1 1 d . . . . .
B9 B 0.4117(10) 0.5906(6) 0.7177(3) 0.0150(15) Uani 1 1 d . . . . .
B10 B 0.1056(11) 0.6981(6) 0.6931(3) 0.0181(16) Uani 1 1 d . . . . .
B11 B 0.7669(10) 0.4168(5) 0.5836(3) 0.0105(14) Uani 1 1 d . . . . .
B12 B 0.4532(10) 0.2889(6) 0.5851(3) 0.0126(14) Uani 1 1 d . . . . .
B13 B 0.1000(9) 0.3329(6) 0.5572(3) 0.0130(14) Uani 1 1 d . . . . .
B14 B 0.2172(10) 0.1340(6) 0.5589(3) 0.0131(15) Uani 1 1 d . . . . .
O1 O 1.5693(6) 0.7828(3) 0.84777(19) 0.0167(9) Uani 1 1 d . . . . .
O2 O 1.5168(6) 0.6822(3) 0.75637(18) 0.0165(9) Uani 1 1 d . . . . .
O3 O 1.2929(6) 0.6550(3) 0.83709(18) 0.0165(9) Uani 1 1 d . . . . .
O4 O 1.0218(6) 0.5320(4) 0.82980(19) 0.0188(10) Uani 1 1 d . . . . .
O5 O 0.7072(6) 0.4453(3) 0.85011(19) 0.0140(9) Uani 1 1 d . . . . .
O6 O 0.8450(5) 0.3184(3) 0.93117(17) 0.0106(8) Uani 1 1 d . . . . .
O7 O 0.8237(6) 0.4461(4) 0.75044(19) 0.0219(10) Uani 1 1 d . . . . .
O8 O 1.2885(6) 0.5194(3) 0.75600(18) 0.0158(9) Uani 1 1 d . . . . .
O9 O 1.1955(6) 0.3664(3) 0.92260(19) 0.0127(9) Uani 1 1 d . . . . .
O10 O 1.5330(6) 0.4140(3) 0.94063(19) 0.0127(9) Uani 1 1 d . . . . .
O11 O 1.4320(5) 0.2154(3) 0.92951(19) 0.0140(9) Uani 1 1 d . . . . .
O12 O 1.3422(5) 0.0236(3) 0.93941(18) 0.0127(9) Uani 1 1 d . . . . .
O13 O 1.0841(5) 0.1681(3) 0.92949(18) 0.0126(9) Uani 1 1 d . . . . .
O14 O 0.8282(6) 0.4234(3) 0.64793(19) 0.0160(9) Uani 1 1 d . . . . .
O15 O 0.6450(5) 0.3193(3) 0.56445(18) 0.0117(9) Uani 1 1 d . . . . .
O16 O 0.4073(5) 0.1716(3) 0.56041(19) 0.0133(9) Uani 1 1 d . . . . .
O17 O 0.2928(6) 0.3695(3) 0.56280(19) 0.0131(9) Uani 1 1 d . . . . .
O18 O 0.0603(5) 0.2153(3) 0.56201(19) 0.0145(9) Uani 1 1 d . . . . .
O19 O -0.0461(5) 0.4128(3) 0.54916(18) 0.0110(9) Uani 1 1 d . . . . .
O20 O 0.1591(5) 0.0221(3) 0.55215(18) 0.0118(9) Uani 1 1 d . . . . .
O21 O 0.5531(6) 0.5276(4) 0.6840(2) 0.0223(10) Uani 1 1 d . . . . .
O22 O 0.2711(6) 0.6480(3) 0.67040(18) 0.0166(9) Uani 1 1 d . . . . .
O23 O 0.0521(6) 0.6752(3) 0.75135(19) 0.0181(9) Uani 1 1 d . . . . .
O24 O -0.0201(6) 0.7742(3) 0.66195(19) 0.0155(9) Uani 1 1 d . . . . .
Sr1 Sr 1.73376(8) 0.08945(5) 0.94432(3) 0.01263(15) Uani 1 1 d . . . . .
Sr2 Sr 1.17947(10) 0.33077(6) 0.73125(3) 0.02678(19) Uani 1 1 d . . . . .
Sr3 Sr -0.24094(8) 0.08322(4) 0.55607(3) 0.01204(15) Uani 1 1 d . . . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
B1 O9 1.363(7) . ?
B1 O10 1.357(8) . ?
B1 O11 1.376(8) . ?
B1 Sr3 3.112(7) 2_656 ?
B2 O1 1.380(8) . ?
B2 O2 1.352(9) . ?
B2 O3 1.361(8) . ?
B2 Sr2 3.038(7) 2_856 ?
B3 O3 1.473(8) . ?
B3 O4 1.445(8) . ?
B3 O8 1.458(8) . ?
B3 O23 1.489(8) 1_655 ?
B3 Sr2 3.314(7) . ?
B3 Sr3 3.329(7) 2_656 ?
B4 O6 1.434(8) . ?
B4 O9 1.468(7) . ?
B4 O13 1.508(7) . ?
B4 O24 1.481(8) 2_646 ?
B4 Sr1 3.171(7) 1_455 ?
B5 O11 1.398(7) . ?
B5 O12 1.350(8) . ?
B5 O13 1.354(7) . ?
B5 Sr1 3.064(7) . ?
B6 O5 1.434(8) . ?
B6 O6 1.444(7) . ?
B6 O10 1.496(7) 1_455 ?
B6 O20 1.525(7) 2_656 ?
B6 Sr3 3.099(7) 4_666 ?
B7 O4 1.377(8) . ?
B7 O5 1.334(8) . ?
B7 O7 1.383(8) . ?
B7 Sr2 3.361(7) . ?
B8 O7 1.367(8) . ?
B8 O14 1.364(8) . ?
B8 O21 1.356(8) . ?
B8 Sr2 3.457(7) . ?
B9 O2 1.507(8) 1_455 ?
B9 O8 1.463(8) 1_455 ?
B9 O21 1.428(8) . ?
B9 O22 1.509(8) . ?
B9 Sr2 3.411(7) 1_455 ?
B10 O22 1.364(8) . ?
B10 O23 1.370(8) . ?
B10 O24 1.371(8) . ?
B10 Sr2 3.012(8) 2_656 ?
B11 O12 1.509(7) 2_756 ?
B11 O14 1.446(8) . ?
B11 O15 1.441(7) . ?
B11 O19 1.491(7) 1_655 ?
B11 Sr1 3.046(7) 4_465 ?
B12 O1 1.488(8) 2_746 ?
B12 O15 1.422(7) . ?
B12 O16 1.492(7) . ?
B12 O17 1.481(7) . ?
B12 Sr3 3.225(7) 1_655 ?
B13 O17 1.349(7) . ?
B13 O18 1.396(8) . ?
B13 O19 1.348(7) . ?
B13 Sr1 3.180(7) 2_756 ?
B14 O16 1.336(7) . ?
B14 O18 1.412(7) . ?
B14 O20 1.361(7) . ?
B14 Sr3 3.099(6) . ?
O1 Sr2 2.535(4) 2_856 ?
O2 Sr2 2.659(4) 2_856 ?
O3 Sr3 2.526(4) 2_656 ?
O4 Sr3 2.881(4) 2_656 ?
O6 Sr1 2.780(4) 1_455 ?
O6 Sr3 3.049(4) 4_666 ?
O7 Sr2 2.771(4) . ?
O8 Sr2 2.362(4) . ?
O9 Sr3 2.577(4) 2_656 ?
O10 Sr3 2.768(4) 2_656 ?
O10 Sr3 2.866(4) 4_766 ?
O11 Sr1 2.489(4) . ?
O12 Sr1 2.709(4) . ?
O12 Sr1 2.935(4) 3_857 ?
O13 Sr1 2.540(4) 1_455 ?
O14 Sr2 3.074(4) . ?
O15 Sr1 2.928(4) 4_465 ?
O15 Sr3 2.855(4) 1_655 ?
O16 Sr3 2.561(4) 1_655 ?
O17 Sr1 2.565(4) 2_756 ?
O18 Sr3 2.521(4) . ?
O19 Sr1 2.651(4) 4_365 ?
O19 Sr1 2.917(4) 2_756 ?
O20 Sr3 2.749(4) 3_556 ?
O20 Sr3 2.759(4) . ?
O22 Sr1 2.601(4) 2_756 ?
O23 Sr2 2.419(4) 2_656 ?
O24 Sr2 2.704(4) 2_656 ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O9 B1 O11 118.7(6) . . ?
O9 B1 Sr3 54.7(3) . 2_656 ?
O10 B1 O9 117.3(6) . . ?
O10 B1 O11 123.9(5) . . ?
O10 B1 Sr3 62.8(3) . 2_656 ?
O11 B1 Sr3 170.7(4) . 2_656 ?
O1 B2 Sr2 55.9(3) . 2_856 ?
O2 B2 O1 116.8(6) . . ?
O2 B2 O3 124.1(6) . . ?
O2 B2 Sr2 61.0(3) . 2_856 ?
O3 B2 O1 119.1(6) . . ?
O3 B2 Sr2 174.6(5) . 2_856 ?
O3 B3 O23 108.8(5) . 1_655 ?
O3 B3 Sr2 134.0(4) . . ?
O3 B3 Sr3 45.5(3) . 2_656 ?
O4 B3 O3 103.9(5) . . ?
O4 B3 O8 116.7(5) . . ?
O4 B3 O23 110.3(5) . 1_655 ?
O4 B3 Sr2 80.4(3) . . ?
O4 B3 Sr3 59.6(3) . 2_656 ?
O8 B3 O3 108.1(5) . . ?
O8 B3 O23 108.7(5) . 1_655 ?
O8 B3 Sr2 38.8(3) . . ?
O8 B3 Sr3 117.8(4) . 2_656 ?
O23 B3 Sr2 112.4(4) 1_655 . ?
O23 B3 Sr3 131.7(4) 1_655 2_656 ?
Sr2 B3 Sr3 111.7(2) . 2_656 ?
O6 B4 O9 112.5(5) . . ?
O6 B4 O13 106.8(5) . . ?
O6 B4 O24 115.1(5) . 2_646 ?
O6 B4 Sr1 61.2(3) . 1_455 ?
O9 B4 O13 109.3(5) . . ?
O9 B4 O24 107.9(5) . 2_646 ?
O9 B4 Sr1 148.7(4) . 1_455 ?
O13 B4 Sr1 52.1(2) . 1_455 ?
O24 B4 O13 104.8(5) 2_646 . ?
O24 B4 Sr1 101.7(3) 2_646 1_455 ?
O11 B5 Sr1 53.1(3) . . ?
O12 B5 O11 115.2(5) . . ?
O12 B5 O13 125.3(5) . . ?
O12 B5 Sr1 62.1(3) . . ?
O13 B5 O11 119.5(6) . . ?
O13 B5 Sr1 171.8(4) . . ?
O5 B6 O6 116.3(5) . . ?
O5 B6 O10 108.6(5) . 1_455 ?
O5 B6 O20 111.0(5) . 2_656 ?
O5 B6 Sr3 169.1(4) . 4_666 ?
O6 B6 O10 107.5(5) . 1_455 ?
O6 B6 O20 107.6(4) . 2_656 ?
O6 B6 Sr3 74.5(3) . 4_666 ?
O10 B6 O20 105.1(4) 1_455 2_656 ?
O10 B6 Sr3 66.9(3) 1_455 4_666 ?
O20 B6 Sr3 62.4(3) 2_656 4_666 ?
O4 B7 O7 116.1(6) . . ?
O4 B7 Sr2 79.4(3) . . ?
O5 B7 O4 123.3(6) . . ?
O5 B7 O7 120.4(6) . . ?
O5 B7 Sr2 134.4(4) . . ?
O7 B7 Sr2 53.5(3) . . ?
O7 B8 Sr2 49.5(3) . . ?
O14 B8 O7 111.9(5) . . ?
O14 B8 Sr2 62.4(3) . . ?
O21 B8 O7 127.1(6) . . ?
O21 B8 O14 121.0(6) . . ?
O21 B8 Sr2 175.9(5) . . ?
O2 B9 O22 108.8(5) 1_455 . ?
O2 B9 Sr2 140.6(4) 1_455 1_455 ?
O8 B9 O2 109.4(5) 1_455 1_455 ?
O8 B9 O22 107.3(5) 1_455 . ?
O8 B9 Sr2 34.8(2) 1_455 1_455 ?
O21 B9 O2 110.8(5) . 1_455 ?
O21 B9 O8 114.4(5) . 1_455 ?
O21 B9 O22 105.8(5) . . ?
O21 B9 Sr2 84.6(3) . 1_455 ?
O22 B9 Sr2 100.7(3) . 1_455 ?
O22 B10 O23 121.0(6) . . ?
O22 B10 O24 125.1(6) . . ?
O22 B10 Sr2 164.9(5) . 2_656 ?
O23 B10 O24 113.9(6) . . ?
O23 B10 Sr2 51.8(3) . 2_656 ?
O24 B10 Sr2 63.8(3) . 2_656 ?
O12 B11 Sr1 71.3(3) 2_756 4_465 ?
O14 B11 O12 112.6(5) . 2_756 ?
O14 B11 O19 107.3(5) . 1_655 ?
O14 B11 Sr1 167.7(4) . 4_465 ?
O15 B11 O12 107.3(5) . 2_756 ?
O15 B11 O14 116.6(5) . . ?
O15 B11 O19 107.4(5) . 1_655 ?
O15 B11 Sr1 71.5(3) . 4_465 ?
O19 B11 O12 104.8(5) 1_655 2_756 ?
O19 B11 Sr1 60.5(3) 1_655 4_465 ?
O1 B12 O16 106.5(5) 2_746 . ?
O1 B12 Sr3 105.0(3) 2_746 1_655 ?
O15 B12 O1 118.0(5) . 2_746 ?
O15 B12 O16 106.3(5) . . ?
O15 B12 O17 112.4(5) . . ?
O15 B12 Sr3 62.2(3) . 1_655 ?
O16 B12 Sr3 50.9(2) . 1_655 ?
O17 B12 O1 104.2(5) . 2_746 ?
O17 B12 O16 109.3(5) . . ?
O17 B12 Sr3 148.6(4) . 1_655 ?
O17 B13 O18 119.0(5) . . ?
O17 B13 Sr1 51.4(3) . 2_756 ?
O18 B13 Sr1 170.1(4) . 2_756 ?
O19 B13 O17 117.9(6) . . ?
O19 B13 O18 123.1(5) . . ?
O19 B13 Sr1 66.5(3) . 2_756 ?
O16 B14 O18 118.7(5) . . ?
O16 B14 O20 125.3(5) . . ?
O16 B14 Sr3 171.9(4) . . ?
O18 B14 Sr3 53.2(3) . . ?
O20 B14 O18 116.0(5) . . ?
O20 B14 Sr3 62.9(3) . . ?
B2 O1 B12 119.5(5) . 2_756 ?
B2 O1 Sr2 97.4(4) . 2_856 ?
B12 O1 Sr2 140.5(3) 2_756 2_856 ?
B2 O2 B9 119.9(5) . 1_655 ?
B2 O2 Sr2 92.7(4) . 2_856 ?
B9 O2 Sr2 147.2(4) 1_655 2_856 ?
B2 O3 B3 114.4(5) . . ?
B2 O3 Sr3 130.5(4) . 2_656 ?
B3 O3 Sr3 109.9(4) . 2_656 ?
B3 O4 Sr3 94.8(3) . 2_656 ?
B7 O4 B3 128.6(5) . . ?
B7 O4 Sr3 136.6(4) . 2_656 ?
B7 O5 B6 127.9(5) . . ?
B4 O6 B6 123.2(5) . . ?
B4 O6 Sr1 91.9(3) . 1_455 ?
B4 O6 Sr3 131.2(3) . 4_666 ?
B6 O6 Sr1 133.7(3) . 1_455 ?
B6 O6 Sr3 78.4(3) . 4_666 ?
Sr1 O6 Sr3 101.59(12) 1_455 4_666 ?
B7 O7 Sr2 102.8(3) . . ?
B8 O7 B7 146.5(5) . . ?
B8 O7 Sr2 108.5(4) . . ?
B3 O8 B9 110.7(5) . 1_655 ?
B3 O8 Sr2 118.5(4) . . ?
B9 O8 Sr2 124.6(4) 1_655 . ?
B1 O9 B4 122.3(5) . . ?
B1 O9 Sr3 99.7(4) . 2_656 ?
B4 O9 Sr3 137.9(3) . 2_656 ?
B1 O10 B6 127.6(5) . 1_655 ?
B1 O10 Sr3 91.4(3) . 2_656 ?
B1 O10 Sr3 119.0(4) . 4_766 ?
B6 O10 Sr3 84.3(3) 1_655 4_766 ?
B6 O10 Sr3 127.8(3) 1_655 2_656 ?
Sr3 O10 Sr3 107.57(13) 2_656 4_766 ?
B1 O11 B5 121.5(5) . . ?
B1 O11 Sr1 137.2(4) . . ?
B5 O11 Sr1 100.2(3) . . ?
B5 O12 B11 126.6(5) . 2_746 ?
B5 O12 Sr1 91.8(3) . . ?
B5 O12 Sr1 117.3(4) . 3_857 ?
B11 O12 Sr1 79.5(3) 2_746 3_857 ?
B11 O12 Sr1 133.4(3) 2_746 . ?
Sr1 O12 Sr1 107.76(12) . 3_857 ?
B4 O13 Sr1 100.0(3) . 1_455 ?
B5 O13 B4 119.5(5) . . ?
B5 O13 Sr1 140.3(4) . 1_455 ?
B8 O14 B11 129.2(5) . . ?
B8 O14 Sr2 94.4(4) . . ?
B11 O14 Sr2 136.2(3) . . ?
B11 O15 Sr1 80.7(3) . 4_465 ?
B11 O15 Sr3 128.8(3) . 1_655 ?
B12 O15 B11 127.0(5) . . ?
B12 O15 Sr1 127.3(3) . 4_465 ?
B12 O15 Sr3 91.6(3) . 1_655 ?
Sr3 O15 Sr1 102.83(12) 1_655 4_465 ?
B12 O16 Sr3 102.2(3) . 1_655 ?
B14 O16 B12 118.8(5) . . ?
B14 O16 Sr3 137.1(4) . 1_655 ?
B12 O17 Sr1 134.1(3) . 2_756 ?
B13 O17 B12 119.5(5) . . ?
B13 O17 Sr1 104.3(4) . 2_756 ?
B13 O18 B14 120.5(5) . . ?
B13 O18 Sr3 138.1(3) . . ?
B14 O18 Sr3 100.2(3) . . ?
B11 O19 Sr1 90.2(3) 1_455 4_365 ?
B11 O19 Sr1 124.4(3) 1_455 2_756 ?
B13 O19 B11 124.8(5) . 1_455 ?
B13 O19 Sr1 117.7(4) . 4_365 ?
B13 O19 Sr1 88.4(3) . 2_756 ?
Sr1 O19 Sr1 113.90(13) 4_365 2_756 ?
B6 O20 Sr3 126.8(3) 2_646 . ?
B6 O20 Sr3 88.1(3) 2_646 3_556 ?
B14 O20 B6 123.8(4) . 2_646 ?
B14 O20 Sr3 91.1(3) . . ?
B14 O20 Sr3 116.7(4) . 3_556 ?
Sr3 O20 Sr3 112.36(13) 3_556 . ?
B8 O21 B9 138.6(6) . . ?
B9 O22 Sr1 121.3(3) . 2_756 ?
B10 O22 B9 114.8(5) . . ?
B10 O22 Sr1 119.9(4) . 2_756 ?
B3 O23 Sr2 133.4(4) 1_455 2_656 ?
B10 O23 B3 123.2(5) . 1_455 ?
B10 O23 Sr2 101.7(4) . 2_656 ?
B4 O24 Sr2 147.2(3) 2_656 2_656 ?
B10 O24 B4 123.4(5) . 2_656 ?
B10 O24 Sr2 89.1(4) . 2_656 ?
B11 Sr1 B5 96.07(18) 4_666 . ?
O6 Sr1 B5 95.67(15) 1_655 . ?
O6 Sr1 B11 97.03(14) 1_655 4_666 ?
O6 Sr1 O12 125.33(11) 1_655 3_857 ?
O6 Sr1 O15 79.36(11) 1_655 4_666 ?
O6 Sr1 O19 119.03(11) 1_655 2_746 ?
O11 Sr1 B5 26.68(15) . . ?
O11 Sr1 B11 98.96(15) . 4_666 ?
O11 Sr1 O6 68.99(12) . 1_655 ?
O11 Sr1 O12 52.80(12) . . ?
O11 Sr1 O12 101.44(12) . 3_857 ?
O11 Sr1 O13 120.67(13) . 1_655 ?
O11 Sr1 O15 72.64(12) . 4_666 ?
O11 Sr1 O17 121.69(12) . 2_746 ?
O11 Sr1 O19 170.39(12) . 2_746 ?
O11 Sr1 O19 121.28(12) . 4_766 ?
O11 Sr1 O22 75.85(13) . 2_746 ?
O12 Sr1 B5 26.12(15) . . ?
O12 Sr1 B5 86.10(15) 3_857 . ?
O12 Sr1 B11 29.15(13) 3_857 4_666 ?
O12 Sr1 B11 92.68(15) . 4_666 ?
O12 Sr1 O6 121.78(11) . 1_655 ?
O12 Sr1 O12 72.24(12) . 3_857 ?
O12 Sr1 O15 83.97(11) . 4_666 ?
O12 Sr1 O19 118.88(11) . 2_746 ?
O13 Sr1 B5 146.80(15) 1_655 . ?
O13 Sr1 B11 97.05(15) 1_655 4_666 ?
O13 Sr1 O6 52.50(12) 1_655 1_655 ?
O13 Sr1 O12 169.24(12) 1_655 . ?
O13 Sr1 O12 118.49(11) 1_655 3_857 ?
O13 Sr1 O15 102.62(12) 1_655 4_666 ?
O13 Sr1 O17 114.26(12) 1_655 2_746 ?
O13 Sr1 O19 69.51(12) 1_655 4_766 ?
O13 Sr1 O19 66.67(11) 1_655 2_746 ?
O13 Sr1 O22 75.10(12) 1_655 2_746 ?
O15 Sr1 B5 76.67(15) 4_666 . ?
O15 Sr1 B11 27.83(14) 4_666 4_666 ?
O15 Sr1 O12 47.84(10) 4_666 3_857 ?
O17 Sr1 B5 95.53(15) 2_746 . ?
O17 Sr1 B11 92.16(15) 2_746 4_666 ?
O17 Sr1 O6 164.66(12) 2_746 1_655 ?
O17 Sr1 O12 65.93(12) 2_746 3_857 ?
O17 Sr1 O12 69.75(12) 2_746 . ?
O17 Sr1 O15 113.49(12) 2_746 4_666 ?
O17 Sr1 O19 49.34(11) 2_746 2_746 ?
O17 Sr1 O19 94.33(12) 2_746 4_766 ?
O17 Sr1 O22 101.81(13) 2_746 2_746 ?
O19 Sr1 B5 144.86(15) 2_746 . ?
O19 Sr1 B5 124.78(15) 4_766 . ?
O19 Sr1 B11 85.65(14) 2_746 4_666 ?
O19 Sr1 B11 29.31(14) 4_766 4_666 ?
O19 Sr1 O6 87.84(11) 4_766 1_655 ?
O19 Sr1 O12 78.48(11) 2_746 3_857 ?
O19 Sr1 O12 120.85(12) 4_766 . ?
O19 Sr1 O12 50.07(11) 4_766 3_857 ?
O19 Sr1 O15 49.83(11) 4_766 4_666 ?
O19 Sr1 O15 112.99(11) 2_746 4_666 ?
O19 Sr1 O19 66.10(13) 4_766 2_746 ?
O22 Sr1 B5 85.11(16) 2_746 . ?
O22 Sr1 B11 165.81(15) 2_746 4_666 ?
O22 Sr1 O6 68.80(12) 2_746 1_655 ?
O22 Sr1 O12 94.42(12) 2_746 . ?
O22 Sr1 O12 164.12(12) 2_746 3_857 ?
O22 Sr1 O15 141.38(12) 2_746 4_666 ?
O22 Sr1 O19 144.55(12) 2_746 4_766 ?
O22 Sr1 O19 101.55(12) 2_746 2_746 ?
B2 Sr2 B3 128.34(19) 2_846 . ?
B2 Sr2 B7 166.30(19) 2_846 . ?
B2 Sr2 B9 91.65(18) 2_846 1_655 ?
B2 Sr2 O14 124.80(17) 2_846 . ?
B3 Sr2 B7 44.79(18) . . ?
B3 Sr2 B9 41.81(18) . 1_655 ?
B7 Sr2 B9 85.27(17) . 1_655 ?
B10 Sr2 B2 117.7(2) 2_646 2_846 ?
B10 Sr2 B3 101.89(19) 2_646 . ?
B10 Sr2 B7 60.91(18) 2_646 . ?
B10 Sr2 B9 143.42(18) 2_646 1_655 ?
B10 Sr2 O14 91.43(15) 2_646 . ?
O1 Sr2 B2 26.77(17) 2_846 2_846 ?
O1 Sr2 B3 121.16(16) 2_846 . ?
O1 Sr2 B7 161.40(16) 2_846 . ?
O1 Sr2 B9 79.37(15) 2_846 1_655 ?
O1 Sr2 B10 136.30(17) 2_846 2_646 ?
O1 Sr2 O2 53.16(13) 2_846 2_846 ?
O1 Sr2 O7 144.23(13) 2_846 . ?
O1 Sr2 O14 100.35(12) 2_846 . ?
O1 Sr2 O24 147.50(13) 2_846 2_646 ?
O2 Sr2 B2 26.39(16) 2_846 2_846 ?
O2 Sr2 B3 126.62(16) 2_846 . ?
O2 Sr2 B7 142.38(15) 2_846 . ?
O2 Sr2 B9 103.80(15) 2_846 1_655 ?
O2 Sr2 B10 96.31(16) 2_846 2_646 ?
O2 Sr2 O7 161.50(13) 2_846 . ?
O2 Sr2 O14 146.55(12) 2_846 . ?
O2 Sr2 O24 95.00(12) 2_846 2_646 ?
O7 Sr2 B2 169.95(17) . 2_846 ?
O7 Sr2 B3 56.37(16) . . ?
O7 Sr2 B7 23.65(15) . . ?
O7 Sr2 B9 88.85(15) . 1_655 ?
O7 Sr2 B10 66.08(16) . 2_646 ?
O7 Sr2 O14 45.17(12) . . ?
O8 Sr2 B2 106.52(17) . 2_846 ?
O8 Sr2 B3 22.74(16) . . ?
O8 Sr2 B7 67.52(16) . . ?
O8 Sr2 B9 20.67(15) . 1_655 ?
O8 Sr2 B10 122.90(17) . 2_646 ?
O8 Sr2 O1 98.92(13) . 2_846 ?
O8 Sr2 O2 110.98(13) . 2_846 ?
O8 Sr2 O7 76.69(14) . . ?
O8 Sr2 O14 91.37(12) . . ?
O8 Sr2 O23 147.91(14) . 2_646 ?
O8 Sr2 O24 99.07(13) . 2_646 ?
O14 Sr2 B3 82.92(14) . . ?
O14 Sr2 B7 68.53(15) . . ?
O14 Sr2 B9 88.32(14) . 1_655 ?
O23 Sr2 B2 102.31(17) 2_646 2_846 ?
O23 Sr2 B3 125.48(17) 2_646 . ?
O23 Sr2 B7 81.22(16) 2_646 . ?
O23 Sr2 B9 166.04(15) 2_646 1_655 ?
O23 Sr2 B10 26.45(17) 2_646 2_646 ?
O23 Sr2 O1 113.17(13) 2_646 2_846 ?
O23 Sr2 O2 89.15(14) 2_646 2_846 ?
O23 Sr2 O7 77.36(14) 2_646 . ?
O23 Sr2 O14 83.49(12) 2_646 . ?
O23 Sr2 O24 52.94(13) 2_646 2_646 ?
O24 Sr2 B2 121.19(17) 2_646 2_846 ?
O24 Sr2 B3 81.19(15) 2_646 . ?
O24 Sr2 B7 50.65(15) 2_646 . ?
O24 Sr2 B9 119.51(15) 2_646 1_655 ?
O24 Sr2 B10 27.07(16) 2_646 2_646 ?
O24 Sr2 O7 66.80(12) 2_646 . ?
O24 Sr2 O14 106.05(12) 2_646 . ?
O3 Sr3 B14 96.07(16) 2_646 . ?
O3 Sr3 O4 49.77(12) 2_646 2_646 ?
O3 Sr3 O6 138.58(12) 2_646 4_465 ?
O3 Sr3 O9 100.13(13) 2_646 2_646 ?
O3 Sr3 O10 94.41(13) 2_646 2_646 ?
O3 Sr3 O10 136.09(12) 2_646 4_365 ?
O3 Sr3 O15 64.67(12) 2_646 1_455 ?
O3 Sr3 O16 70.08(13) 2_646 1_455 ?
O3 Sr3 O20 171.76(12) 2_646 3_556 ?
O3 Sr3 O20 107.30(12) 2_646 . ?
O4 Sr3 B14 64.86(15) 2_646 . ?
O4 Sr3 O6 138.08(11) 2_646 4_465 ?
O6 Sr3 B14 73.23(14) 4_465 . ?
O9 Sr3 B14 94.44(15) 2_646 . ?
O9 Sr3 O4 65.97(12) 2_646 2_646 ?
O9 Sr3 O6 120.20(12) 2_646 4_465 ?
O9 Sr3 O10 51.37(11) 2_646 2_646 ?
O9 Sr3 O10 102.78(11) 2_646 4_365 ?
O9 Sr3 O15 163.06(12) 2_646 1_455 ?
O9 Sr3 O20 72.18(12) 2_646 3_556 ?
O9 Sr3 O20 69.57(11) 2_646 . ?
O10 Sr3 B14 145.57(14) 2_646 . ?
O10 Sr3 B14 118.68(15) 4_365 . ?
O10 Sr3 O4 98.69(12) 2_646 2_646 ?
O10 Sr3 O4 168.73(11) 4_365 2_646 ?
O10 Sr3 O6 47.16(10) 4_365 4_465 ?
O10 Sr3 O6 117.25(11) 2_646 4_465 ?
O10 Sr3 O10 72.43(13) 2_646 4_365 ?
O10 Sr3 O15 119.46(11) 2_646 1_455 ?
O15 Sr3 B14 94.61(14) 1_455 . ?
O15 Sr3 O4 105.39(11) 1_455 2_646 ?
O15 Sr3 O6 76.21(11) 1_455 4_465 ?
O15 Sr3 O10 85.30(11) 1_455 4_365 ?
O16 Sr3 B14 145.24(15) 1_455 . ?
O16 Sr3 O4 117.88(13) 1_455 2_646 ?
O16 Sr3 O6 95.84(11) 1_455 4_465 ?
O16 Sr3 O9 118.89(12) 1_455 2_646 ?
O16 Sr3 O10 66.08(12) 1_455 4_365 ?
O16 Sr3 O10 68.92(11) 1_455 2_646 ?
O16 Sr3 O15 50.65(11) 1_455 1_455 ?
O16 Sr3 O20 171.26(12) 1_455 . ?
O16 Sr3 O20 115.91(12) 1_455 3_556 ?
O18 Sr3 B14 26.64(15) . . ?
O18 Sr3 O3 84.37(13) . 2_646 ?
O18 Sr3 O4 73.77(13) . 2_646 ?
O18 Sr3 O6 68.20(12) . 4_465 ?
O18 Sr3 O9 120.08(12) . 2_646 ?
O18 Sr3 O10 114.41(12) . 4_365 ?
O18 Sr3 O10 171.08(12) . 2_646 ?
O18 Sr3 O15 67.97(11) . 1_455 ?
O18 Sr3 O16 118.60(12) . 1_455 ?
O18 Sr3 O20 52.67(11) . . ?
O18 Sr3 O20 96.85(12) . 3_556 ?
O20 Sr3 B14 81.87(15) 3_556 . ?
O20 Sr3 B14 26.04(14) . . ?
O20 Sr3 O4 122.72(11) 3_556 2_646 ?
O20 Sr3 O4 62.22(12) . 2_646 ?
O20 Sr3 O6 80.65(10) . 4_465 ?
O20 Sr3 O6 48.46(10) 3_556 4_465 ?
O20 Sr3 O10 83.12(12) 3_556 2_646 ?
O20 Sr3 O10 119.81(11) . 2_646 ?
O20 Sr3 O10 50.54(11) 3_556 4_365 ?
O20 Sr3 O10 115.65(11) . 4_365 ?
O20 Sr3 O15 120.62(11) . 1_455 ?
O20 Sr3 O15 123.35(11) 3_556 1_455 ?
O20 Sr3 O20 67.64(13) 3_556 . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
O1 B2 O2 B9 175.3(5) . . . 1_655 ?
O1 B2 O2 Sr2 -0.8(6) . . . 2_856 ?
O1 B2 O3 B3 168.1(5) . . . . ?
O1 B2 O3 Sr3 -40.4(8) . . . 2_656 ?
O1 B12 O15 B11 -50.8(8) 2_746 . . . ?
O1 B12 O15 Sr1 -159.5(3) 2_746 . . 4_465 ?
O1 B12 O15 Sr3 93.0(5) 2_746 . . 1_655 ?
O1 B12 O16 B14 70.8(6) 2_746 . . . ?
O1 B12 O16 Sr3 -96.2(4) 2_746 . . 1_655 ?
O1 B12 O17 B13 -76.6(6) 2_746 . . . ?
O1 B12 O17 Sr1 84.0(6) 2_746 . . 2_756 ?
O2 B2 O1 B12 -164.3(5) . . . 2_756 ?
O2 B2 O1 Sr2 0.8(6) . . . 2_856 ?
O2 B2 O3 B3 -10.5(9) . . . . ?
O2 B2 O3 Sr3 141.1(5) . . . 2_656 ?
O2 B9 O21 B8 53.1(10) 1_455 . . . ?
O2 B9 O22 B10 -70.6(6) 1_455 . . . ?
O2 B9 O22 Sr1 131.9(4) 1_455 . . 2_756 ?
O3 B2 O1 B12 17.0(8) . . . 2_756 ?
O3 B2 O1 Sr2 -177.9(5) . . . 2_856 ?
O3 B2 O2 B9 -6.1(9) . . . 1_655 ?
O3 B2 O2 Sr2 177.8(6) . . . 2_856 ?
O3 B3 O4 B7 167.9(5) . . . . ?
O3 B3 O4 Sr3 -10.8(4) . . . 2_656 ?
O3 B3 O8 B9 -67.2(6) . . . 1_655 ?
O3 B3 O8 Sr2 139.3(4) . . . . ?
O4 B3 O3 B2 170.5(5) . . . . ?
O4 B3 O3 Sr3 13.1(5) . . . 2_656 ?
O4 B3 O8 B9 176.2(5) . . . 1_655 ?
O4 B3 O8 Sr2 22.7(7) . . . . ?
O4 B7 O5 B6 -26.0(9) . . . . ?
O4 B7 O7 B8 -107.0(10) . . . . ?
O4 B7 O7 Sr2 51.8(6) . . . . ?
O5 B6 O6 B4 46.9(7) . . . . ?
O5 B6 O6 Sr1 -86.1(6) . . . 1_455 ?
O5 B6 O6 Sr3 178.9(5) . . . 4_666 ?
O5 B7 O4 B3 -165.2(6) . . . . ?
O5 B7 O4 Sr3 12.9(9) . . . 2_656 ?
O5 B7 O7 B8 76.1(12) . . . . ?
O5 B7 O7 Sr2 -125.1(5) . . . . ?
O6 B4 O9 B1 148.0(5) . . . . ?
O6 B4 O9 Sr3 -34.0(8) . . . 2_656 ?
O6 B4 O13 B5 -155.8(5) . . . . ?
O6 B4 O13 Sr1 29.1(5) . . . 1_455 ?
O6 B6 O5 B7 -69.5(8) . . . . ?
O7 B7 O4 B3 18.0(9) . . . . ?
O7 B7 O4 Sr3 -163.8(4) . . . 2_656 ?
O7 B7 O5 B6 150.5(6) . . . . ?
O7 B8 O14 B11 172.5(5) . . . . ?
O7 B8 O14 Sr2 -2.6(5) . . . . ?
O7 B8 O21 B9 3.9(12) . . . . ?
O8 B3 O3 B2 45.8(7) . . . . ?
O8 B3 O3 Sr3 -111.5(4) . . . 2_656 ?
O8 B3 O4 B7 -73.2(8) . . . . ?
O8 B3 O4 Sr3 108.1(5) . . . 2_656 ?
O8 B9 O21 B8 -71.2(9) 1_455 . . . ?
O8 B9 O22 B10 47.7(6) 1_455 . . . ?
O8 B9 O22 Sr1 -109.8(4) 1_455 . . 2_756 ?
O9 B1 O10 B6 -138.6(6) . . . 1_655 ?
O9 B1 O10 Sr3 114.9(5) . . . 4_766 ?
O9 B1 O10 Sr3 3.9(5) . . . 2_656 ?
O9 B1 O11 B5 -11.0(9) . . . . ?
O9 B1 O11 Sr1 -176.5(3) . . . . ?
O9 B4 O6 B6 66.1(7) . . . . ?
O9 B4 O6 Sr1 -145.9(4) . . . 1_455 ?
O9 B4 O6 Sr3 -38.6(7) . . . 4_666 ?
O9 B4 O13 B5 -33.8(7) . . . . ?
O9 B4 O13 Sr1 151.1(4) . . . 1_455 ?
O10 B1 O9 B4 174.4(5) . . . . ?
O10 B1 O9 Sr3 -4.2(6) . . . 2_656 ?
O10 B1 O11 B5 165.4(6) . . . . ?
O10 B1 O11 Sr1 -0.1(10) . . . . ?
O10 B6 O5 B7 169.0(5) 1_455 . . . ?
O10 B6 O6 B4 168.9(5) 1_455 . . . ?
O10 B6 O6 Sr1 36.0(7) 1_455 . . 1_455 ?
O10 B6 O6 Sr3 -59.0(4) 1_455 . . 4_666 ?
O11 B1 O9 B4 -9.0(9) . . . . ?
O11 B1 O9 Sr3 172.4(5) . . . 2_656 ?
O11 B1 O10 B6 45.0(9) . . . 1_655 ?
O11 B1 O10 Sr3 -172.5(6) . . . 2_656 ?
O11 B1 O10 Sr3 -61.5(7) . . . 4_766 ?
O11 B5 O12 B11 -150.2(5) . . . 2_746 ?
O11 B5 O12 Sr1 112.5(5) . . . 3_857 ?
O11 B5 O12 Sr1 1.4(5) . . . . ?
O11 B5 O13 B4 18.1(9) . . . . ?
O11 B5 O13 Sr1 -169.5(3) . . . 1_455 ?
O12 B5 O11 B1 -171.6(5) . . . . ?
O12 B5 O11 Sr1 -1.6(6) . . . . ?
O12 B5 O13 B4 -164.6(6) . . . . ?
O12 B5 O13 Sr1 7.8(11) . . . 1_455 ?
O12 B11 O14 B8 39.1(8) 2_756 . . . ?
O12 B11 O14 Sr2 -148.1(3) 2_756 . . . ?
O12 B11 O15 B12 -67.5(7) 2_756 . . . ?
O12 B11 O15 Sr1 62.7(4) 2_756 . . 4_465 ?
O12 B11 O15 Sr3 161.8(3) 2_756 . . 1_655 ?
O13 B4 O6 B6 -174.0(4) . . . . ?
O13 B4 O6 Sr1 -26.0(4) . . . 1_455 ?
O13 B4 O6 Sr3 81.3(5) . . . 4_666 ?
O13 B4 O9 B1 29.5(8) . . . . ?
O13 B4 O9 Sr3 -152.5(4) . . . 2_656 ?
O13 B5 O11 B1 6.0(9) . . . . ?
O13 B5 O11 Sr1 176.0(5) . . . . ?
O13 B5 O12 B11 32.4(10) . . . 2_746 ?
O13 B5 O12 Sr1 -176.0(6) . . . . ?
O13 B5 O12 Sr1 -64.9(7) . . . 3_857 ?
O14 B8 O7 B7 161.2(8) . . . . ?
O14 B8 O7 Sr2 3.0(6) . . . . ?
O14 B8 O21 B9 -176.2(6) . . . . ?
O14 B11 O15 B12 59.9(7) . . . . ?
O14 B11 O15 Sr1 -169.9(5) . . . 4_465 ?
O14 B11 O15 Sr3 -70.9(6) . . . 1_655 ?
O15 B11 O14 B8 -85.6(7) . . . . ?
O15 B11 O14 Sr2 87.2(6) . . . . ?
O15 B12 O16 B14 -162.6(5) . . . . ?
O15 B12 O16 Sr3 30.4(5) . . . 1_655 ?
O15 B12 O17 B13 154.5(5) . . . . ?
O15 B12 O17 Sr1 -44.8(8) . . . 2_756 ?
O16 B12 O15 B11 -170.2(5) . . . . ?
O16 B12 O15 Sr1 81.2(5) . . . 4_465 ?
O16 B12 O15 Sr3 -26.3(4) . . . 1_655 ?
O16 B12 O17 B13 36.9(8) . . . . ?
O16 B12 O17 Sr1 -162.5(3) . . . 2_756 ?
O16 B14 O18 B13 9.9(9) . . . . ?
O16 B14 O18 Sr3 179.7(5) . . . . ?
O16 B14 O20 B6 43.5(9) . . . 2_646 ?
O16 B14 O20 Sr3 -179.3(6) . . . . ?
O16 B14 O20 Sr3 -63.5(7) . . . 3_556 ?
O17 B12 O15 B11 70.4(7) . . . . ?
O17 B12 O15 Sr1 -38.3(7) . . . 4_465 ?
O17 B12 O15 Sr3 -145.8(4) . . . 1_655 ?
O17 B12 O16 B14 -41.2(7) . . . . ?
O17 B12 O16 Sr3 151.8(4) . . . 1_655 ?
O17 B13 O18 B14 -14.2(9) . . . . ?
O17 B13 O18 Sr3 -179.1(4) . . . . ?
O17 B13 O19 B11 -132.7(6) . . . 1_455 ?
O17 B13 O19 Sr1 -0.7(6) . . . 2_756 ?
O17 B13 O19 Sr1 115.6(5) . . . 4_365 ?
O18 B13 O17 B12 -11.3(9) . . . . ?
O18 B13 O17 Sr1 -177.1(5) . . . 2_756 ?
O18 B13 O19 B11 45.1(9) . . . 1_455 ?
O18 B13 O19 Sr1 177.1(6) . . . 2_756 ?
O18 B13 O19 Sr1 -66.6(7) . . . 4_365 ?
O18 B14 O16 B12 19.5(8) . . . . ?
O18 B14 O16 Sr3 -179.3(3) . . . 1_655 ?
O18 B14 O20 B6 -139.0(5) . . . 2_646 ?
O18 B14 O20 Sr3 -1.8(5) . . . . ?
O18 B14 O20 Sr3 114.0(5) . . . 3_556 ?
O19 B11 O14 B8 153.9(5) 1_655 . . . ?
O19 B11 O14 Sr2 -33.2(7) 1_655 . . . ?
O19 B11 O15 B12 -179.7(5) 1_655 . . . ?
O19 B11 O15 Sr1 -49.5(4) 1_655 . . 4_465 ?
O19 B11 O15 Sr3 49.5(6) 1_655 . . 1_655 ?
O19 B13 O17 B12 166.6(5) . . . . ?
O19 B13 O17 Sr1 0.8(6) . . . 2_756 ?
O19 B13 O18 B14 168.0(6) . . . . ?
O19 B13 O18 Sr3 3.2(10) . . . . ?
O20 B6 O5 B7 53.9(7) 2_656 . . . ?
O20 B6 O6 B4 -78.3(6) 2_656 . . . ?
O20 B6 O6 Sr1 148.8(3) 2_656 . . 1_455 ?
O20 B6 O6 Sr3 53.7(4) 2_656 . . 4_666 ?
O20 B14 O16 B12 -163.0(6) . . . . ?
O20 B14 O16 Sr3 -1.9(10) . . . 1_655 ?
O20 B14 O18 B13 -167.8(5) . . . . ?
O20 B14 O18 Sr3 2.0(6) . . . . ?
O21 B8 O7 B7 -18.9(14) . . . . ?
O21 B8 O7 Sr2 -177.1(5) . . . . ?
O21 B8 O14 B11 -7.4(9) . . . . ?
O21 B8 O14 Sr2 177.5(5) . . . . ?
O21 B9 O22 B10 170.3(5) . . . . ?
O21 B9 O22 Sr1 12.8(6) . . . 2_756 ?
O22 B9 O21 B8 170.9(6) . . . . ?
O22 B10 O23 B3 -3.1(9) . . . 1_455 ?
O22 B10 O23 Sr2 163.8(5) . . . 2_656 ?
O22 B10 O24 B4 18.7(9) . . . 2_656 ?
O22 B10 O24 Sr2 -165.8(6) . . . 2_656 ?
O23 B3 O3 B2 -72.1(7) 1_655 . . . ?
O23 B3 O3 Sr3 130.6(4) 1_655 . . 2_656 ?
O23 B3 O4 B7 51.5(8) 1_655 . . . ?
O23 B3 O4 Sr3 -127.2(4) 1_655 . . 2_656 ?
O23 B3 O8 B9 50.7(6) 1_655 . . 1_655 ?
O23 B3 O8 Sr2 -102.7(5) 1_655 . . . ?
O23 B10 O22 B9 -13.7(8) . . . . ?
O23 B10 O22 Sr1 144.1(5) . . . 2_756 ?
O23 B10 O24 B4 -161.6(5) . . . 2_656 ?
O23 B10 O24 Sr2 13.9(5) . . . 2_656 ?
O24 B4 O6 B6 -58.1(7) 2_646 . . . ?
O24 B4 O6 Sr1 89.9(4) 2_646 . . 1_455 ?
O24 B4 O6 Sr3 -162.8(3) 2_646 . . 4_666 ?
O24 B4 O9 B1 -83.9(6) 2_646 . . . ?
O24 B4 O9 Sr3 94.1(6) 2_646 . . 2_656 ?
O24 B4 O13 B5 81.6(6) 2_646 . . . ?
O24 B4 O13 Sr1 -93.5(4) 2_646 . . 1_455 ?
O24 B10 O22 B9 166.0(6) . . . . ?
O24 B10 O22 Sr1 -36.2(8) . . . 2_756 ?
O24 B10 O23 B3 177.2(5) . . . 1_455 ?
O24 B10 O23 Sr2 -15.9(6) . . . 2_656 ?
Sr1 B4 O6 B6 -148.0(5) 1_455 . . . ?
Sr1 B4 O6 Sr3 107.3(3) 1_455 . . 4_666 ?
Sr1 B4 O9 B1 76.8(9) 1_455 . . . ?
Sr1 B4 O9 Sr3 -105.2(7) 1_455 . . 2_656 ?
Sr1 B4 O13 B5 175.0(6) 1_455 . . . ?
Sr1 B5 O11 B1 -170.1(6) . . . . ?
Sr1 B5 O12 B11 -151.6(6) . . . 2_746 ?
Sr1 B5 O12 Sr1 111.1(3) . . . 3_857 ?
Sr1 B11 O14 B8 145.5(16) 4_465 . . . ?
Sr1 B11 O14 Sr2 -42(2) 4_465 . . . ?
Sr1 B11 O15 B12 -130.2(5) 4_465 . . . ?
Sr1 B11 O15 Sr3 99.0(3) 4_465 . . 1_655 ?
Sr1 B13 O17 B12 165.8(6) 2_756 . . . ?
Sr1 B13 O19 B11 -132.0(5) 2_756 . . 1_455 ?
Sr1 B13 O19 Sr1 116.3(3) 2_756 . . 4_365 ?
Sr2 B2 O1 B12 -165.1(5) 2_856 . . 2_756 ?
Sr2 B2 O2 B9 176.1(5) 2_856 . . 1_655 ?
Sr2 B3 O3 B2 80.4(7) . . . . ?
Sr2 B3 O3 Sr3 -76.9(6) . . . 2_656 ?
Sr2 B3 O4 B7 -59.0(6) . . . . ?
Sr2 B3 O4 Sr3 122.29(14) . . . 2_656 ?
Sr2 B3 O8 B9 153.4(6) . . . 1_655 ?
Sr2 B7 O4 B3 58.0(6) . . . . ?
Sr2 B7 O4 Sr3 -123.9(4) . . . 2_656 ?
Sr2 B7 O5 B6 83.5(8) . . . . ?
Sr2 B7 O7 B8 -158.8(11) . . . . ?
Sr2 B8 O7 B7 158.2(11) . . . . ?
Sr2 B8 O14 B11 175.0(6) . . . . ?
Sr2 B9 O21 B8 -89.5(7) 1_455 . . . ?
Sr2 B9 O22 B10 82.9(5) 1_455 . . . ?
Sr2 B9 O22 Sr1 -74.6(4) 1_455 . . 2_756 ?
Sr2 B10 O22 B9 44(2) 2_656 . . . ?
Sr2 B10 O22 Sr1 -158.7(16) 2_656 . . 2_756 ?
Sr2 B10 O23 B3 -166.9(6) 2_656 . . 1_455 ?
Sr2 B10 O24 B4 -175.5(5) 2_656 . . 2_656 ?
Sr3 B1 O9 B4 178.6(6) 2_656 . . . ?
Sr3 B1 O10 B6 -142.5(6) 2_656 . . 1_655 ?
Sr3 B1 O10 Sr3 111.0(3) 2_656 . . 4_766 ?
Sr3 B3 O3 B2 157.3(6) 2_656 . . . ?
Sr3 B3 O4 B7 178.7(6) 2_656 . . . ?
Sr3 B3 O8 B9 -115.9(4) 2_656 . . 1_655 ?
Sr3 B3 O8 Sr2 90.7(4) 2_656 . . . ?
Sr3 B6 O5 B7 105(2) 4_666 . . . ?
Sr3 B6 O6 B4 -132.0(5) 4_666 . . . ?
Sr3 B6 O6 Sr1 95.0(4) 4_666 . . 1_455 ?
Sr3 B12 O15 B11 -143.8(5) 1_655 . . . ?
Sr3 B12 O15 Sr1 107.5(3) 1_655 . . 4_465 ?
Sr3 B12 O16 B14 167.0(6) 1_655 . . . ?
Sr3 B12 O17 B13 81.6(9) 1_655 . . . ?
Sr3 B12 O17 Sr1 -117.8(6) 1_655 . . 2_756 ?
Sr3 B14 O18 B13 -169.8(6) . . . . ?
Sr3 B14 O20 B6 -137.2(5) . . . 2_646 ?
Sr3 B14 O20 Sr3 115.8(2) . . . 3_556 ?

_olex2_submission_special_instructions 'No special instructions were received'
