# Electronic Supplementary Material (ESI) for Chemical Science.
# This journal is © The Royal Society of Chemistry 2022

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_1_sq
_database_code_depnum_ccdc_archive 'CCDC 2094270'
loop_
_audit_author_name
_audit_author_address
'Xi Xi Kang'
;Anhui University
China
;
_audit_update_record             
;
2021-07-04 deposited with the CCDC.	2022-04-12 downloaded from the CCDC.
;
_audit_creation_date             2021-03-16
_audit_creation_method           
;
Olex2 1.2
(compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506)
;
_shelx_SHELXL_version_number     2018/3
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         'C280 H420 Ag52 Cl4 S28'
_chemical_formula_sum            'C280 H420 Ag52 Cl4 S28'
_chemical_formula_weight         10434.85
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag 0.1306 4.2820 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.3639 0.7018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.3331 0.5567 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      orthorhombic
_space_group_IT_number           56
_space_group_name_H-M_alt        'P c c n'
_space_group_name_Hall           '-P 2ab 2ac'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, -y+1/2, z'
'-x, y+1/2, -z+1/2'
'x+1/2, -y, -z+1/2'
'-x, -y, -z'
'x-1/2, y-1/2, -z'
'x, -y-1/2, z-1/2'
'-x-1/2, y, z-1/2'

_cell_length_a                   22.7708(5)
_cell_length_b                   37.8932(8)
_cell_length_c                   47.1176(9)
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_volume                     40655.8(15)
_cell_formula_units_Z            4
_cell_measurement_reflns_used    24991
_cell_measurement_temperature    120(2)
_cell_measurement_theta_max      62.499
_cell_measurement_theta_min      2.940
_shelx_estimated_absorpt_T_max   ?
_shelx_estimated_absorpt_T_min   ?
_exptl_absorpt_coefficient_mu    21.409
_exptl_absorpt_correction_T_max  ?
_exptl_absorpt_correction_T_min  ?
_exptl_absorpt_correction_type   ?
_exptl_absorpt_process_details   ?
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            black
_exptl_crystal_colour_primary    ?
_exptl_crystal_density_diffrn    1.705
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       block
_exptl_crystal_F_000             20240
_exptl_crystal_size_max          ?
_exptl_crystal_size_mid          ?
_exptl_crystal_size_min          ?
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0427
_diffrn_reflns_av_unetI/netI     0.0497
_diffrn_reflns_Laue_measured_fraction_full 0.975
_diffrn_reflns_Laue_measured_fraction_max 0.975
_diffrn_reflns_limit_h_max       20
_diffrn_reflns_limit_h_min       -26
_diffrn_reflns_limit_k_max       20
_diffrn_reflns_limit_k_min       -43
_diffrn_reflns_limit_l_max       54
_diffrn_reflns_limit_l_min       -54
_diffrn_reflns_number            151947
_diffrn_reflns_point_group_measured_fraction_full 0.975
_diffrn_reflns_point_group_measured_fraction_max 0.975
_diffrn_reflns_theta_full        62.499
_diffrn_reflns_theta_max         62.499
_diffrn_reflns_theta_min         2.940
_diffrn_ambient_temperature      120(2)
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 0.975
_diffrn_measured_fraction_theta_max 0.975
_diffrn_measurement_device_type  STOE
_diffrn_measurement_method       ?
_diffrn_radiation_type           CuK\a
_diffrn_radiation_wavelength     1.54186
_diffrn_source                   ?
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                24991
_reflns_number_total             31624
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 Structure factors included contributions from the .fab file.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       ?
_computing_data_collection       ?
_computing_data_reduction        ?
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'ShelXL (Sheldrick, 2015)'
_computing_structure_solution    'olex2.solve (Bourhis et al., 2015)'
_refine_diff_density_max         2.887
_refine_diff_density_min         -2.491
_refine_diff_density_rms         0.176
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.047
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1668
_refine_ls_number_reflns         31624
_refine_ls_number_restraints     1430
_refine_ls_R_factor_all          0.0636
_refine_ls_R_factor_gt           0.0514
_refine_ls_restrained_S_all      1.035
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0905P)²] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1371
_refine_ls_wR_factor_ref         0.1423
_refine_special_details          ?
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H) groups, All C(H,H) groups
2. Restrained distances
 C5-C11 = C5-C12 = C7-C21 = C19-C12 = C19-C17 = C17-C16 = C16-C11 = C7-C16 =
 C19-C15 = C5-C14 = C21-C14 = C21-C15
 1.54 with sigma of 0.01
 C04T-C04K = C51-C04T = C51-C134 = C134-C03P = C162-C03P = C20-C162 = C04I-
 C03P = C04K-C04I = C80-C04K = C80-C20 = C57-C20 = C57-C51
 1.54 with sigma of 0.01
3. Restrained planarity
 S0, C12, C7, C16, C21
 with sigma of 0.1
4. Uiso/Uaniso restraints and constraints
C12 \\sim C5 \\sim C14 \\sim C11 \\sim C16 \\sim C7 \\sim C17 \\sim C21 \\sim
C19 \\sim C15: within 3.8A with sigma of 0.01 and sigma for terminal atoms of
0.02
Ag0O \\sim Ag0G \\sim Ag0K \\sim Ag07 \\sim Ag0F \\sim AgB \\sim S0: within
3.8A with sigma of 0.01 and sigma for terminal atoms of 0.02
C03P \\sim C04I \\sim C04K \\sim C04T \\sim C51 \\sim C80 \\sim C162 \\sim C20
\\sim C57 \\sim C134: within 3.8A with sigma of 0.01 and sigma for terminal
atoms of 0.02
C02P \\sim C037 \\sim C04Z \\sim C04G \\sim C04R \\sim C03C \\sim C04L \\sim
C041 \\sim C029: within 3.8A with sigma of 0.01 and sigma for terminal atoms of
0.02
C02W \\sim C031 \\sim C034 \\sim C035 \\sim C03E \\sim C03W \\sim C042 \\sim
C045 \\sim C04C \\sim C04H: within 3.8A with sigma of 0.01 and sigma for
terminal atoms of 0.02
Ag0K \\sim S010 \\sim AgB \\sim S00X \\sim Ag0F: within 3.8A with sigma of 0.01
and sigma for terminal atoms of 0.02
Uanis(C12) \\sim Ueq, Uanis(C19) \\sim Ueq, Uanis(C17) \\sim Ueq, Uanis(C15)
\\sim Ueq, Uanis(C11) \\sim Ueq, Uanis(C5) \\sim Ueq, Uanis(C14) \\sim Ueq,
Uanis(C21) \\sim Ueq, Uanis(C16) \\sim Ueq, Uanis(C7) \\sim Ueq: with sigma of
0.01 and sigma for terminal atoms of 0.02
Uanis(Ag0O) \\sim Ueq, Uanis(Ag0G) \\sim Ueq, Uanis(S0) \\sim Ueq, Uanis(Ag0K)
\\sim Ueq, Uanis(AgB) \\sim Ueq, Uanis(Ag0F) \\sim Ueq, Uanis(Ag07) \\sim Ueq:
with sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(C57) \\sim Ueq, Uanis(C51) \\sim Ueq, Uanis(C134) \\sim Ueq, Uanis(C03P)
\\sim Ueq, Uanis(C162) \\sim Ueq, Uanis(C20) \\sim Ueq, Uanis(C80) \\sim Ueq,
Uanis(C04T) \\sim Ueq, Uanis(C04I) \\sim Ueq, Uanis(C04K) \\sim Ueq: with sigma
of 0.01 and sigma for terminal atoms of 0.02
Uanis(C029) \\sim Ueq, Uanis(C037) \\sim Ueq, Uanis(C03C) \\sim Ueq,
Uanis(C041) \\sim Ueq, Uanis(C04G) \\sim Ueq, Uanis(C04L) \\sim Ueq,
Uanis(C04R) \\sim Ueq, Uanis(C04Y) \\sim Ueq, Uanis(C04Z) \\sim Ueq,
Uanis(C02P) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(C04H) \\sim Ueq, Uanis(C042) \\sim Ueq, Uanis(C03E) \\sim Ueq,
Uanis(C03W) \\sim Ueq, Uanis(C04C) \\sim Ueq, Uanis(C045) \\sim Ueq,
Uanis(C031) \\sim Ueq, Uanis(C02W) \\sim Ueq, Uanis(C034) \\sim Ueq,
Uanis(C035) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(AgB) \\sim Ueq, Uanis(S00X) \\sim Ueq, Uanis(Ag0F) \\sim Ueq, Uanis(S010)
\\sim Ueq, Uanis(Ag0K) \\sim Ueq: with sigma of 0.01 and sigma for terminal
atoms of 0.02
5. Others
 Sof(S0)=1-FVAR(1)
 Sof(S1)=FVAR(1)
 Sof(Ag1B)=1-FVAR(2)
 Sof(Ag1A)=FVAR(2)
 Fixed Sof: AgB(0.5768) AgA(0.4232)
6.a Ternary CH refined with riding coordinates:
 C018(H018), C01A(H01C), C01B(H01D), C01C(H01E), C01D(H01F), C01F(H01I),
 C01H(H01L), C01J(H01O), C01K(H01P), C01L(H01Q), C01M(H01R), C01N(H01S),
 C01P(H01V), C01Q(H01W), C01S(H01Z), C01T(H01), C01U(H0AA), C01V(H1AA),
 C01Z(H5AA), C022(H022), C023(H023), C026(H026), C028(H028), C029(H029),
 C02A(H02K), C02B(H02L), C02C(H02M), C02J(H02X), C02M(H02), C02P(H7AA),
 C02Q(H8AA), C02S(H0BA), C02U(H2BA), C02W(H4BA), C02X(H5BA), C02Y(H6BA),
 C032(H032), C033(H033), C035(H035), C037(H037), C038(H038), C03I(H03Z),
 C03L(H9BA), C03M(H0CA), C03P(H3CA), C03Q(H4CA), C03R(H5CA), C03T(H7CA),
 C03U(H8CA), C03W(H0DA), C03Z(H3DA), C040(H040), C042(H042), C043(H043),
 C044(H044), C045(H045), C047(H047), C048(H048), C04F(H04K), C04K(H04R),
 C04L(H04S), C04R(H04V), C5(H5), C12(H12), C16(H16), C19(H19), C21(H21),
 C51(H51), C20(H20), C134(H134)
6.b Secondary CH2 refined with riding coordinates:
 C019(H01A,H01B), C01E(H01G,H01H), C01G(H01J,H01K), C01I(H01M,H01N), C01O(H01T,
 H01U), C01R(H01X,H01Y), C01W(H2AA,H), C01X(H3AA,HA), C01Y(H4AA,HB), C020(H02A,
 H02B), C021(H02C,H02D), C024(H02E,H02F), C025(H02G,H02H), C027(H02I,H02J),
 C02E(H02N,H02O), C02F(H02P,H02Q), C02G(H02R,H02S), C02H(H02T,H02U), C02I(H02V,
 H02W), C02K(H02Y,HC), C02L(H02Z,HD), C02N(H6AA,HE), C02R(H9AA,HF), C02T(H1BA,
 HG), C02V(H3BA,HH), C02Z(H7BA,HI), C030(H03A,H03B), C031(H03C,H03D), C034(H03E,
 H03F), C036(H03G,H03H), C039(H03I,H03J), C03A(H03K,H03L), C03B(H03M,H03N),
 C03C(H03O,H03P), C03D(H03Q,H03R), C03E(H03S,H03T), C03F(H03U,H03V), C03G(H03W,
 H03X), C03H(H03Y,HJ), C03J(H03,HK), C03K(H8BA,HL), C03N(H1CA,HM), C03O(H2CA,
 HN), C03S(H6CA,HO), C03V(H9CA,HP), C03X(H1DA,HQ), C03Y(H2DA,HR), C041(H04A,
 H04B), C046(H04C,H04D), C04A(H04E,H04F), C04C(H04G,H04H), C04E(H04I,H04J),
 C04G(H04L,H04M), C04H(H04N,H04O), C04I(H04P,H04Q), C04N(H04T,H04U), C04S(H04W,
 H04X), C04T(H04Y,HS), C04W(H04Z,HT), C04Y(H04,HU), C04Z(H4DA,HV), C7(H7A,H7B),
 C11(H11A,H11B), C14(H14A,H14B), C15(H15A,H15B), C17(H17A,H17B), C80(H80A,H80B),
  C162(H16A,H16B), C57(H57A,H57B), C0AA(H0AB,H0AC)
;
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     iterative
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag01 Ag 0.25007(2) 0.28713(2) 0.68757(2) 0.01802(11) Uani 1 1 d . . . . .
Ag02 Ag 0.31221(2) 0.25014(2) 0.64537(2) 0.01978(12) Uani 1 1 d . . . . .
Ag03 Ag 0.32509(2) 0.33664(2) 0.71395(2) 0.02054(12) Uani 1 1 d . . . . .
Ag04 Ag 0.22052(3) 0.31228(2) 0.74259(2) 0.02231(12) Uani 1 1 d . . . . .
Ag05 Ag 0.20919(3) 0.35688(2) 0.69251(2) 0.02376(13) Uani 1 1 d . . . . .
Ag06 Ag 0.40231(3) 0.29488(2) 0.62300(2) 0.02425(13) Uani 1 1 d . . . . .
Ag07 Ag 0.07268(3) 0.27657(2) 0.64172(2) 0.02594(13) Uani 1 1 d . U . . .
Ag08 Ag 0.30876(3) 0.25947(2) 0.73381(2) 0.02866(14) Uani 1 1 d . . . . .
Ag09 Ag 0.31870(3) 0.33188(2) 0.65443(2) 0.02854(14) Uani 1 1 d . . . . .
Ag0A Ag 0.34258(3) 0.31613(2) 0.77180(2) 0.02693(13) Uani 1 1 d . . . . .
Ag0B Ag 0.38648(3) 0.28167(2) 0.68314(2) 0.03114(14) Uani 1 1 d . . . . .
Ag0C Ag 0.30424(3) 0.40308(2) 0.67796(2) 0.03084(14) Uani 1 1 d . . . . .
Ag0D Ag 0.10846(3) 0.34828(2) 0.73774(2) 0.03201(14) Uani 1 1 d . . . . .
Ag0E Ag 0.50926(3) 0.27750(2) 0.66041(2) 0.03253(15) Uani 1 1 d . . . . .
Ag0F Ag 0.14353(3) 0.26778(2) 0.59154(2) 0.03408(15) Uani 1 1 d . U . . .
Ag0G Ag 0.09079(3) 0.33796(2) 0.59562(2) 0.03596(15) Uani 1 1 d . U . . .
Ag0H Ag 0.41925(3) 0.37507(2) 0.63758(2) 0.03787(16) Uani 1 1 d . . . . .
Ag0I Ag 0.13081(3) 0.29929(2) 0.69123(2) 0.04116(18) Uani 1 1 d . . . . .
Ag0J Ag 0.31179(3) 0.23419(2) 0.79111(2) 0.03698(16) Uani 1 1 d . . . . .
Ag0K Ag 0.36506(3) 0.30827(2) 0.56511(2) 0.04233(18) Uani 1 1 d . U . . .
Ag0L Ag 0.44316(3) 0.34618(2) 0.69534(2) 0.04121(18) Uani 1 1 d . . . . .
Ag0M Ag 0.02488(4) 0.33474(2) 0.67748(2) 0.04419(19) Uani 1 1 d . . . . .
Ag0N Ag 0.11858(3) 0.38630(2) 0.65656(2) 0.04561(19) Uani 1 1 d . . . . .
Ag0O Ag 0.17583(4) 0.32201(2) 0.64025(2) 0.0517(2) Uani 1 1 d . U . . .
AgB Ag 0.22490(6) 0.29015(4) 0.53921(3) 0.0412(3) Uani 0.5768 1 d . U P A 2
Cl00 Cl 0.03004(9) 0.24820(5) 0.58909(4) 0.0313(4) Uani 1 1 d . . . . .
Cl1 Cl 0.25506(9) 0.38207(5) 0.74464(4) 0.0288(4) Uani 1 1 d . . . . .
S00T S 0.41525(9) 0.35111(5) 0.74591(4) 0.0224(4) Uani 1 1 d . . . . .
S00U S 0.03969(10) 0.38212(5) 0.71110(4) 0.0277(4) Uani 1 1 d . . . . .
S00V S 0.30741(9) 0.29075(5) 0.81474(4) 0.0263(4) Uani 1 1 d . . . . .
S00W S 0.03687(9) 0.37860(6) 0.62415(4) 0.0297(4) Uani 1 1 d . . . . .
S00X S 0.13186(10) 0.31547(5) 0.55158(4) 0.0297(4) Uani 1 1 d . U . . .
S00Y S -0.03319(9) 0.28531(6) 0.66056(5) 0.0298(4) Uani 1 1 d . . . . .
S00Z S 0.20087(9) 0.42138(5) 0.67457(4) 0.0276(4) Uani 1 1 d . . . . .
S010 S 0.32107(11) 0.28489(6) 0.52344(5) 0.0371(5) Uani 1 1 d . U . . .
S011 S 0.14361(9) 0.32268(5) 0.78202(4) 0.0281(4) Uani 1 1 d . . . . .
S012 S 0.52631(10) 0.33935(5) 0.66358(4) 0.0306(4) Uani 1 1 d . . . . .
S013 S 0.40525(9) 0.41958(6) 0.67368(4) 0.0287(4) Uani 1 1 d . . . . .
S014 S 0.42846(10) 0.34939(6) 0.59114(4) 0.0309(5) Uani 1 1 d . . . . .
S015 S 0.41582(12) 0.24488(8) 0.72625(6) 0.0505(7) Uani 1 1 d . . . . .
S0 S 0.2654(3) 0.34632(19) 0.60674(16) 0.047(2) Uani 0.552(14) 1 d . U P A 2
C018 C 0.3808(4) 0.3989(2) 0.78785(17) 0.0267(18) Uani 1 1 d . . . . .
H018 H 0.347368 0.383095 0.791199 0.032 Uiso 1 1 calc R . . . .
C019 C 0.2471(4) 0.4984(2) 0.6982(2) 0.039(2) Uani 1 1 d . . . . .
H01A H 0.259246 0.489422 0.679895 0.047 Uiso 1 1 calc R . . . .
H01B H 0.279152 0.512231 0.706069 0.047 Uiso 1 1 calc R . . . .
C01A C -0.1036(4) 0.3306(2) 0.6291(2) 0.036(2) Uani 1 1 d . . . . .
H01C H -0.077637 0.349613 0.635496 0.043 Uiso 1 1 calc R . . . .
C01B C 0.2324(4) 0.4678(2) 0.7181(2) 0.034(2) Uani 1 1 d . . . . .
H01D H 0.267112 0.452741 0.720439 0.041 Uiso 1 1 calc R . . . .
C01C C 0.4005(4) 0.3967(2) 0.75637(17) 0.0241(17) Uani 1 1 d . . . . .
H01E H 0.368727 0.405831 0.744438 0.029 Uiso 1 1 calc R . . . .
C01D C 0.4554(4) 0.4201(2) 0.75187(18) 0.032(2) Uani 1 1 d . . . . .
H01F H 0.468730 0.418051 0.732165 0.038 Uiso 1 1 calc R . . . .
C01E C 0.1413(5) 0.4991(2) 0.6825(2) 0.044(2) Uani 1 1 d . . . . .
H01G H 0.106513 0.513563 0.679933 0.053 Uiso 1 1 calc R . . . .
H01H H 0.152913 0.490064 0.664130 0.053 Uiso 1 1 calc R . . . .
C01F C 0.1807(4) 0.4454(2) 0.70713(18) 0.0266(18) Uani 1 1 d . . . . .
H01I H 0.170185 0.428160 0.721760 0.032 Uiso 1 1 calc R . . . .
C01G C -0.1573(4) 0.3265(3) 0.6496(2) 0.044(2) Uani 1 1 d . . . . .
H01J H -0.143520 0.320252 0.668409 0.053 Uiso 1 1 calc R . . . .
H01K H -0.178206 0.348701 0.650880 0.053 Uiso 1 1 calc R . . . .
C01H C -0.0267(4) 0.3824(2) 0.73416(19) 0.0294(19) Uani 1 1 d . . . . .
H01L H -0.021217 0.364616 0.749058 0.035 Uiso 1 1 calc R . . . .
C01I C 0.0862(4) 0.3939(3) 0.8112(2) 0.039(2) Uani 1 1 d . . . . .
H01M H 0.061591 0.377077 0.801255 0.047 Uiso 1 1 calc R . . . .
H01N H 0.069550 0.417265 0.808424 0.047 Uiso 1 1 calc R . . . .
C01J C 0.5051(4) 0.3397(2) 0.58205(18) 0.033(2) Uani 1 1 d . . . . .
H01O H 0.518322 0.319952 0.593885 0.040 Uiso 1 1 calc R . . . .
C01K C 0.1273(4) 0.4692(2) 0.7017(2) 0.038(2) Uani 1 1 d . . . . .
H01P H 0.095038 0.455250 0.693715 0.046 Uiso 1 1 calc R . . . .
C01L C -0.1987(4) 0.2978(3) 0.6386(2) 0.041(2) Uani 1 1 d . . . . .
H01Q H -0.232309 0.295593 0.651447 0.049 Uiso 1 1 calc R . . . .
C01M C 0.1914(4) 0.5221(2) 0.6948(2) 0.042(2) Uani 1 1 d . . . . .
H01R H 0.199918 0.541645 0.681803 0.050 Uiso 1 1 calc R . . . .
C01N C 0.5868(4) 0.3707(3) 0.7098(2) 0.041(2) Uani 1 1 d . . . . .
H01S H 0.552284 0.364531 0.721149 0.049 Uiso 1 1 calc R . . . .
C01O C 0.3626(5) 0.4380(2) 0.7936(2) 0.043(2) Uani 1 1 d . . . . .
H01T H 0.330599 0.444611 0.781140 0.052 Uiso 1 1 calc R . . . .
H01U H 0.349350 0.440471 0.813071 0.052 Uiso 1 1 calc R . . . .
C01P C 0.5440(5) 0.3716(3) 0.5884(2) 0.046(3) Uani 1 1 d . . . . .
H01V H 0.538181 0.379385 0.608078 0.055 Uiso 1 1 calc R . . . .
C01Q C 0.1782(4) 0.3569(2) 0.80367(17) 0.0278(18) Uani 1 1 d . . . . .
H01W H 0.219494 0.358912 0.797962 0.033 Uiso 1 1 calc R . . . .
C01R C -0.0355(5) 0.2956(3) 0.5206(2) 0.051(3) Uani 1 1 d . . . . .
H01X H -0.037519 0.271406 0.527289 0.061 Uiso 1 1 calc R . . . .
H01Y H -0.073108 0.306698 0.524352 0.061 Uiso 1 1 calc R . . . .
C01S C 0.0710(4) 0.2968(3) 0.53045(18) 0.033(2) Uani 1 1 d . . . . .
H01Z H 0.066836 0.271880 0.535614 0.040 Uiso 1 1 calc R . . . .
C01T C -0.0829(4) 0.3736(2) 0.7182(2) 0.042(2) Uani 1 1 d . . . . .
H01 H -0.078483 0.350815 0.708623 0.050 Uiso 1 1 calc R . . . .
C01U C 0.0128(4) 0.3153(3) 0.53688(18) 0.039(2) Uani 1 1 d . . . . .
H0AA H 0.004810 0.314629 0.557311 0.046 Uiso 1 1 calc R . . . .
C01V C 0.1481(4) 0.3929(2) 0.79892(19) 0.034(2) Uani 1 1 d . . . . .
H1AA H 0.147160 0.398564 0.778630 0.040 Uiso 1 1 calc R . . . .
C01W C 0.1860(5) 0.4206(2) 0.81522(19) 0.038(2) Uani 1 1 d . . . . .
H2AA H 0.225617 0.420686 0.807623 0.046 Uiso 1 1 calc R . . . .
H H 0.169475 0.443972 0.812535 0.046 Uiso 1 1 calc R . . . .
C01X C 0.4317(4) 0.3894(3) 0.80767(18) 0.038(2) Uani 1 1 d . . . . .
H3AA H 0.418664 0.391048 0.827218 0.046 Uiso 1 1 calc R . . . .
HA H 0.443689 0.365200 0.804179 0.046 Uiso 1 1 calc R . . . .
C01Y C 0.5795(5) 0.4069(3) 0.6988(2) 0.048(3) Uani 1 1 d . . . . .
H4AA H 0.574537 0.423037 0.714549 0.058 Uiso 1 1 calc R . . . .
HB H 0.544350 0.407980 0.687172 0.058 Uiso 1 1 calc R . . . .
C01Z C 0.1604(4) 0.5059(2) 0.7436(2) 0.042(2) Uani 1 1 d . . . . .
H5AA H 0.149032 0.515442 0.762119 0.050 Uiso 1 1 calc R . . . .
C020 C -0.1645(4) 0.2630(3) 0.6383(2) 0.040(2) Uani 1 1 d . . . . .
H02A H -0.150592 0.257701 0.657268 0.048 Uiso 1 1 calc R . . . .
H02B H -0.190099 0.243989 0.632261 0.048 Uiso 1 1 calc R . . . .
C021 C -0.1334(4) 0.3712(3) 0.7403(3) 0.053(3) Uani 1 1 d . . . . .
H02C H -0.169568 0.364420 0.730862 0.064 Uiso 1 1 calc R . . . .
H02D H -0.124080 0.353407 0.754338 0.064 Uiso 1 1 calc R . . . .
C022 C 0.0847(5) 0.2987(3) 0.49859(19) 0.041(2) Uani 1 1 d . . . . .
H022 H 0.122367 0.287296 0.494493 0.050 Uiso 1 1 calc R . . . .
C023 C 0.0468(5) 0.4531(3) 0.6190(2) 0.043(2) Uani 1 1 d . . . . .
H023 H 0.086258 0.450408 0.627080 0.052 Uiso 1 1 calc R . . . .
C024 C 0.6421(5) 0.3688(3) 0.7287(2) 0.059(3) Uani 1 1 d . . . . .
H02E H 0.646906 0.345122 0.736124 0.070 Uiso 1 1 calc R . . . .
H02F H 0.638072 0.384909 0.744660 0.070 Uiso 1 1 calc R . . . .
C025 C 0.0852(5) 0.3371(3) 0.4883(2) 0.059(3) Uani 1 1 d . . . . .
H02G H 0.092942 0.337632 0.468052 0.071 Uiso 1 1 calc R . . . .
H02H H 0.116409 0.349870 0.497789 0.071 Uiso 1 1 calc R . . . .
C026 C 0.5933(5) 0.3437(3) 0.6854(2) 0.044(2) Uani 1 1 d . . . . .
H026 H 0.602049 0.320588 0.693787 0.052 Uiso 1 1 calc R . . . .
C027 C 0.2141(5) 0.4829(2) 0.7474(2) 0.044(2) Uani 1 1 d . . . . .
H02I H 0.205332 0.463694 0.760330 0.052 Uiso 1 1 calc R . . . .
H02J H 0.245990 0.496644 0.755301 0.052 Uiso 1 1 calc R . . . .
C028 C -0.0703(4) 0.2960(2) 0.62690(19) 0.0301(19) Uani 1 1 d . . . . .
H028 H -0.040235 0.298561 0.612159 0.036 Uiso 1 1 calc R . . . .
C029 C 0.5365(6) 0.2513(4) 0.7332(3) 0.068(2) Uani 1 1 d . U . . .
H029 H 0.538139 0.252012 0.712415 0.082 Uiso 1 1 calc R . . . .
C02A C 0.0311(4) 0.4195(2) 0.6028(2) 0.036(2) Uani 1 1 d . . . . .
H02K H 0.057650 0.417441 0.586517 0.043 Uiso 1 1 calc R . . . .
C02B C 0.5113(5) 0.3290(3) 0.5511(2) 0.046(3) Uani 1 1 d . . . . .
H02L H 0.484147 0.309646 0.546799 0.055 Uiso 1 1 calc R . . . .
C02C C 0.6325(5) 0.4184(3) 0.6810(2) 0.050(3) Uani 1 1 d . . . . .
H02M H 0.626995 0.442658 0.674300 0.060 Uiso 1 1 calc R . . . .
C02E C -0.0970(5) 0.4017(3) 0.6964(3) 0.053(3) Uani 1 1 d . . . . .
H02N H -0.065874 0.402671 0.682332 0.064 Uiso 1 1 calc R . . . .
H02O H -0.133259 0.395700 0.686692 0.064 Uiso 1 1 calc R . . . .
C02F C -0.2207(4) 0.3069(3) 0.6087(2) 0.046(3) Uani 1 1 d . . . . .
H02P H -0.247754 0.288837 0.602200 0.056 Uiso 1 1 calc R . . . .
H02Q H -0.241288 0.329254 0.609051 0.056 Uiso 1 1 calc R . . . .
C02G C 0.0477(5) 0.4842(3) 0.5975(3) 0.056(3) Uani 1 1 d . . . . .
H02R H 0.061140 0.505646 0.606622 0.067 Uiso 1 1 calc R . . . .
H02S H 0.073779 0.478876 0.581782 0.067 Uiso 1 1 calc R . . . .
C02H C 0.1090(4) 0.4841(3) 0.7316(2) 0.047(3) Uani 1 1 d . . . . .
H02T H 0.074422 0.498881 0.729786 0.057 Uiso 1 1 calc R . . . .
H02U H 0.099805 0.464807 0.744381 0.057 Uiso 1 1 calc R . . . .
C02I C 0.5051(4) 0.4100(3) 0.7718(2) 0.046(3) Uani 1 1 d . . . . .
H02V H 0.538524 0.425344 0.768728 0.055 Uiso 1 1 calc R . . . .
H02W H 0.517255 0.385878 0.768141 0.055 Uiso 1 1 calc R . . . .
C02J C 0.3978(5) 0.4624(2) 0.65434(18) 0.037(2) Uani 1 1 d . . . . .
H02X H 0.356956 0.464068 0.647855 0.045 Uiso 1 1 calc R . . . .
C02K C -0.0465(5) 0.4465(2) 0.7267(3) 0.050(3) Uani 1 1 d . . . . .
H02Y H -0.014231 0.448686 0.713335 0.060 Uiso 1 1 calc R . . . .
HC H -0.051267 0.469072 0.736154 0.060 Uiso 1 1 calc R . . . .
C02L C 0.1739(5) 0.5366(2) 0.7235(3) 0.050(3) Uani 1 1 d . . . . .
H02Z H 0.139485 0.551461 0.721550 0.060 Uiso 1 1 calc R . . . .
HD H 0.205565 0.550757 0.731193 0.060 Uiso 1 1 calc R . . . .
C02M C 0.6962(5) 0.3792(3) 0.7105(3) 0.053(3) Uani 1 1 d . . . . .
H02 H 0.732120 0.377891 0.721950 0.064 Uiso 1 1 calc R . . . .
C02N C 0.5761(5) 0.3166(3) 0.5460(3) 0.058(3) Uani 1 1 d . . . . .
H6AA H 0.584438 0.296145 0.557629 0.069 Uiso 1 1 calc R . . . .
HE H 0.580967 0.309905 0.526236 0.069 Uiso 1 1 calc R . . . .
C02P C 0.4784(6) 0.2653(4) 0.7440(3) 0.070(2) Uani 1 1 d . U . . .
H7AA H 0.477301 0.290410 0.739161 0.084 Uiso 1 1 calc R . . . .
C02Q C 0.6467(5) 0.3551(3) 0.6668(2) 0.052(3) Uani 1 1 d . . . . .
H8AA H 0.651084 0.338910 0.650724 0.062 Uiso 1 1 calc R . . . .
C02R C 0.1139(4) 0.3477(2) 0.84705(18) 0.038(2) Uani 1 1 d . . . . .
H9AA H 0.114502 0.341913 0.867097 0.045 Uiso 1 1 calc R . . . .
HF H 0.090013 0.330326 0.837336 0.045 Uiso 1 1 calc R . . . .
C02S C -0.0320(4) 0.4186(2) 0.7483(2) 0.036(2) Uani 1 1 d . . . . .
H0BA H 0.004721 0.424488 0.758068 0.043 Uiso 1 1 calc R . . . .
C02T C -0.1542(5) 0.4353(3) 0.7324(4) 0.079(5) Uani 1 1 d . . . . .
H1BA H -0.158443 0.457907 0.741892 0.095 Uiso 1 1 calc R . . . .
HG H -0.190767 0.430046 0.722766 0.095 Uiso 1 1 calc R . . . .
C02U C 0.1760(4) 0.3470(2) 0.83531(19) 0.033(2) Uani 1 1 d . . . . .
H2BA H 0.193367 0.323559 0.838193 0.040 Uiso 1 1 calc R . . . .
C02V C 0.0149(5) 0.3537(3) 0.5264(2) 0.052(3) Uani 1 1 d . . . . .
H3BA H -0.022028 0.365262 0.530777 0.062 Uiso 1 1 calc R . . . .
HH H 0.045940 0.366245 0.536292 0.062 Uiso 1 1 calc R . . . .
C02W C 0.3856(5) 0.2570(3) 0.8528(2) 0.0495(17) Uani 1 1 d . U . . .
H4BA H 0.389873 0.238104 0.838753 0.059 Uiso 1 1 calc R . . . .
C02X C 0.0871(5) 0.3852(3) 0.8428(2) 0.042(2) Uani 1 1 d . . . . .
H5BA H 0.047147 0.385938 0.850501 0.051 Uiso 1 1 calc R . . . .
C02Y C -0.1681(5) 0.3091(3) 0.5884(2) 0.044(2) Uani 1 1 d . . . . .
H6BA H -0.182175 0.314564 0.569266 0.053 Uiso 1 1 calc R . . . .
C02Z C -0.1272(4) 0.3382(3) 0.5983(2) 0.044(2) Uani 1 1 d . . . . .
H7BA H -0.147942 0.360544 0.598150 0.053 Uiso 1 1 calc R . . . .
HI H -0.094315 0.340011 0.585282 0.053 Uiso 1 1 calc R . . . .
C030 C 0.6884(5) 0.4160(3) 0.6990(3) 0.054(3) Uani 1 1 d . . . . .
H03A H 0.722172 0.422251 0.687489 0.065 Uiso 1 1 calc R . . . .
H03B H 0.686006 0.432614 0.714614 0.065 Uiso 1 1 calc R . . . .
C031 C 0.3346(5) 0.2486(3) 0.8736(2) 0.0515(17) Uani 1 1 d . U . . .
H03C H 0.298460 0.246023 0.862912 0.062 Uiso 1 1 calc R . . . .
H03D H 0.342520 0.226379 0.883056 0.062 Uiso 1 1 calc R . . . .
C032 C 0.4083(4) 0.4937(2) 0.6746(2) 0.039(2) Uani 1 1 d . . . . .
H032 H 0.384137 0.491438 0.691706 0.046 Uiso 1 1 calc R . . . .
C033 C 0.4834(5) 0.4135(3) 0.8033(2) 0.050(3) Uani 1 1 d . . . . .
H033 H 0.515112 0.406805 0.816251 0.060 Uiso 1 1 calc R . . . .
C034 C 0.4439(5) 0.2618(3) 0.8700(2) 0.0538(17) Uani 1 1 d . U . . .
H03E H 0.453979 0.239765 0.879309 0.065 Uiso 1 1 calc R . . . .
H03F H 0.475599 0.267834 0.857111 0.065 Uiso 1 1 calc R . . . .
C035 C 0.3725(5) 0.2923(3) 0.8381(2) 0.0477(17) Uani 1 1 d . U . . .
H035 H 0.406519 0.298178 0.826257 0.057 Uiso 1 1 calc R . . . .
C036 C -0.1348(4) 0.2747(3) 0.58793(19) 0.040(2) Uani 1 1 d . . . . .
H03G H -0.101884 0.276552 0.574949 0.048 Uiso 1 1 calc R . . . .
H03H H -0.160350 0.255983 0.581243 0.048 Uiso 1 1 calc R . . . .
C037 C 0.4768(6) 0.2632(4) 0.7770(3) 0.068(2) Uani 1 1 d . U . . .
H037 H 0.438055 0.270754 0.783677 0.082 Uiso 1 1 calc R . . . .
C038 C -0.1121(4) 0.2657(2) 0.61803(18) 0.0303(19) Uani 1 1 d . . . . .
H038 H -0.090710 0.243247 0.617658 0.036 Uiso 1 1 calc R . . . .
C039 C 0.4993(6) 0.3609(3) 0.5308(2) 0.060(3) Uani 1 1 d . . . . .
H03I H 0.504210 0.353429 0.511264 0.073 Uiso 1 1 calc R . . . .
H03J H 0.459156 0.368890 0.533207 0.073 Uiso 1 1 calc R . . . .
C03A C 0.3930(6) 0.5274(3) 0.6584(3) 0.057(3) Uani 1 1 d . . . . .
H03K H 0.351821 0.526833 0.653165 0.068 Uiso 1 1 calc R . . . .
H03L H 0.399146 0.547612 0.670662 0.068 Uiso 1 1 calc R . . . .
C03B C 0.6374(6) 0.3935(3) 0.6559(2) 0.059(3) Uani 1 1 d . . . . .
H03M H 0.670276 0.400382 0.644003 0.071 Uiso 1 1 calc R . . . .
H03N H 0.601911 0.394680 0.644557 0.071 Uiso 1 1 calc R . . . .
C03C C 0.5933(6) 0.2392(3) 0.7882(3) 0.070(2) Uani 1 1 d . U . . .
H03O H 0.592147 0.238764 0.808783 0.083 Uiso 1 1 calc R . . . .
H03P H 0.632143 0.231590 0.782355 0.083 Uiso 1 1 calc R . . . .
C03D C 0.5329(6) 0.4015(3) 0.5684(2) 0.054(3) Uani 1 1 d . . . . .
H03Q H 0.559448 0.420706 0.572931 0.065 Uiso 1 1 calc R . . . .
H03R H 0.493080 0.409980 0.571189 0.065 Uiso 1 1 calc R . . . .
C03E C 0.3160(5) 0.3123(3) 0.8806(2) 0.0509(17) Uani 1 1 d . U . . .
H03S H 0.311648 0.330933 0.894514 0.061 Uiso 1 1 calc R . . . .
H03T H 0.279431 0.310609 0.870084 0.061 Uiso 1 1 calc R . . . .
C03F C 0.0034(5) 0.4598(3) 0.6432(2) 0.052(3) Uani 1 1 d . . . . .
H03U H 0.003708 0.439996 0.656325 0.063 Uiso 1 1 calc R . . . .
H03V H 0.014513 0.480856 0.653598 0.063 Uiso 1 1 calc R . . . .
C03G C 0.2123(5) 0.3749(3) 0.8509(2) 0.044(2) Uani 1 1 d . . . . .
H03W H 0.213400 0.369219 0.870940 0.053 Uiso 1 1 calc R . . . .
H03X H 0.252334 0.374317 0.843807 0.053 Uiso 1 1 calc R . . . .
C03H C -0.0217(7) 0.3335(4) 0.4786(3) 0.080(4) Uani 1 1 d . . . . .
H03Y H -0.059775 0.344322 0.481607 0.096 Uiso 1 1 calc R . . . .
HJ H -0.013621 0.333922 0.458347 0.096 Uiso 1 1 calc R . . . .
C03I C -0.0234(5) 0.2959(4) 0.4886(2) 0.054(3) Uani 1 1 d . . . . .
H03Z H -0.054380 0.282939 0.478613 0.065 Uiso 1 1 calc R . . . .
C03J C 0.1262(5) 0.4122(3) 0.8581(2) 0.048(3) Uani 1 1 d . . . . .
H03 H 0.109769 0.435573 0.855691 0.058 Uiso 1 1 calc R . . . .
HK H 0.126555 0.406903 0.878287 0.058 Uiso 1 1 calc R . . . .
C03K C -0.0756(5) 0.4313(3) 0.6155(3) 0.052(3) Uani 1 1 d . . . . .
H8BA H -0.114819 0.434063 0.607824 0.062 Uiso 1 1 calc R . . . .
HL H -0.075990 0.411623 0.628700 0.062 Uiso 1 1 calc R . . . .
C03L C 0.5410(7) 0.3912(3) 0.5370(3) 0.069(4) Uani 1 1 d . . . . .
H9BA H 0.533712 0.411275 0.524405 0.083 Uiso 1 1 calc R . . . .
C03M C 0.4369(5) 0.4646(3) 0.6278(2) 0.045(3) Uani 1 1 d . . . . .
H0CA H 0.430128 0.444278 0.615349 0.054 Uiso 1 1 calc R . . . .
C03N C 0.5024(5) 0.4671(3) 0.6361(3) 0.060(3) Uani 1 1 d . . . . .
H1CA H 0.514278 0.445535 0.645499 0.072 Uiso 1 1 calc R . . . .
HM H 0.525995 0.469713 0.619048 0.072 Uiso 1 1 calc R . . . .
C03O C 0.4364(6) 0.4587(2) 0.7579(2) 0.050(3) Uani 1 1 d . . . . .
H2CA H 0.469460 0.474402 0.754858 0.060 Uiso 1 1 calc R . . . .
HN H 0.405281 0.465425 0.744963 0.060 Uiso 1 1 calc R . . . .
C03P C 0.2685(8) 0.3045(4) 0.4720(3) 0.110(3) Uani 1 1 d D U . . .
H3CA H 0.235584 0.288742 0.476255 0.131 Uiso 1 1 calc R . . . .
C03Q C -0.1412(5) 0.4065(3) 0.7545(3) 0.061(3) Uani 1 1 d . . . . .
H4CA H -0.173244 0.405207 0.768342 0.074 Uiso 1 1 calc R . . . .
C03R C -0.1033(5) 0.4373(3) 0.7104(3) 0.059(3) Uani 1 1 d . . . . .
H5CA H -0.111732 0.455496 0.696193 0.071 Uiso 1 1 calc R . . . .
C03S C 0.0340(5) 0.2792(3) 0.4833(2) 0.057(3) Uani 1 1 d . . . . .
H6CA H 0.041625 0.278953 0.463075 0.068 Uiso 1 1 calc R . . . .
HO H 0.032817 0.254889 0.489820 0.068 Uiso 1 1 calc R . . . .
C03T C 0.0260(6) 0.3554(4) 0.4943(2) 0.066(4) Uani 1 1 d . . . . .
H7CA H 0.026411 0.379839 0.487646 0.080 Uiso 1 1 calc R . . . .
C03U C 0.4150(6) 0.4620(3) 0.7885(2) 0.057(3) Uani 1 1 d . . . . .
H8CA H 0.403325 0.486532 0.792026 0.069 Uiso 1 1 calc R . . . .
C03V C 0.4753(5) 0.4950(3) 0.6824(2) 0.054(3) Uani 1 1 d . . . . .
H9CA H 0.482559 0.515032 0.694806 0.065 Uiso 1 1 calc R . . . .
HP H 0.485945 0.473738 0.692643 0.065 Uiso 1 1 calc R . . . .
C03W C 0.3652(5) 0.3222(3) 0.8601(2) 0.0484(17) Uani 1 1 d . U . . .
H0DA H 0.355708 0.344364 0.850438 0.058 Uiso 1 1 calc R . . . .
C03X C -0.0326(6) 0.4551(3) 0.5703(3) 0.062(3) Uani 1 1 d . . . . .
H1DA H -0.071449 0.457764 0.562145 0.074 Uiso 1 1 calc R . . . .
HQ H -0.004902 0.450723 0.555077 0.074 Uiso 1 1 calc R . . . .
C03Y C 0.6998(5) 0.3532(4) 0.6854(3) 0.075(4) Uani 1 1 d . . . . .
H2DA H 0.734407 0.358439 0.674224 0.090 Uiso 1 1 calc R . . . .
HR H 0.703769 0.329381 0.692733 0.090 Uiso 1 1 calc R . . . .
C03Z C -0.0152(5) 0.4888(3) 0.5868(3) 0.057(3) Uani 1 1 d . . . . .
H3DA H -0.016188 0.508798 0.573658 0.068 Uiso 1 1 calc R . . . .
C040 C 0.6183(5) 0.3455(4) 0.5531(3) 0.067(4) Uani 1 1 d . . . . .
H040 H 0.658795 0.337407 0.550500 0.081 Uiso 1 1 calc R . . . .
C041 C 0.5491(7) 0.2164(4) 0.7438(3) 0.074(2) Uani 1 1 d . U . . .
H04A H 0.587880 0.209584 0.737216 0.088 Uiso 1 1 calc R . . . .
H04B H 0.521097 0.200065 0.735614 0.088 Uiso 1 1 calc R . . . .
C042 C 0.3270(5) 0.2777(3) 0.8958(2) 0.0529(17) Uani 1 1 d . U . . .
H042 H 0.294461 0.272079 0.908694 0.063 Uiso 1 1 calc R . . . .
C043 C -0.0576(5) 0.4643(3) 0.6307(3) 0.055(3) Uani 1 1 d . . . . .
H043 H -0.085485 0.468793 0.646096 0.066 Uiso 1 1 calc R . . . .
C044 C -0.0321(4) 0.4240(3) 0.5915(2) 0.043(2) Uani 1 1 d . . . . .
H044 H -0.043821 0.402358 0.581634 0.052 Uiso 1 1 calc R . . . .
C045 C 0.4366(5) 0.2914(3) 0.8925(2) 0.0542(18) Uani 1 1 d . U . . .
H045 H 0.472895 0.293918 0.903497 0.065 Uiso 1 1 calc R . . . .
C046 C 0.4211(6) 0.4999(3) 0.6122(2) 0.058(3) Uani 1 1 d . . . . .
H04C H 0.445569 0.502461 0.595438 0.070 Uiso 1 1 calc R . . . .
H04D H 0.380423 0.499134 0.606021 0.070 Uiso 1 1 calc R . . . .
C047 C 0.5134(6) 0.4983(3) 0.6556(3) 0.059(3) Uani 1 1 d . . . . .
H047 H 0.554990 0.499432 0.660840 0.071 Uiso 1 1 calc R . . . .
C048 C 0.1879(5) 0.4118(3) 0.8472(2) 0.042(2) Uani 1 1 d . . . . .
H048 H 0.212071 0.429056 0.857400 0.051 Uiso 1 1 calc R . . . .
C04A C 0.6059(6) 0.3773(4) 0.5340(3) 0.082(5) Uani 1 1 d . . . . .
H04E H 0.612919 0.370660 0.514367 0.098 Uiso 1 1 calc R . . . .
H04F H 0.632940 0.396137 0.538738 0.098 Uiso 1 1 calc R . . . .
C04C C 0.4230(5) 0.3261(3) 0.8767(2) 0.0552(18) Uani 1 1 d . U . . .
H04G H 0.419667 0.345309 0.890205 0.066 Uiso 1 1 calc R . . . .
H04H H 0.454825 0.331563 0.863713 0.066 Uiso 1 1 calc R . . . .
C04E C -0.0581(6) 0.4958(3) 0.6104(3) 0.069(4) Uani 1 1 d . . . . .
H04I H -0.097248 0.499090 0.602721 0.083 Uiso 1 1 calc R . . . .
H04J H -0.047082 0.517080 0.620538 0.083 Uiso 1 1 calc R . . . .
C04F C 0.4302(6) 0.5316(3) 0.6317(3) 0.059(3) Uani 1 1 d . . . . .
H04K H 0.419652 0.553434 0.621810 0.071 Uiso 1 1 calc R . . . .
C04G C 0.5841(6) 0.2761(4) 0.7467(3) 0.073(2) Uani 1 1 d . U . . .
H04L H 0.622560 0.268847 0.739983 0.088 Uiso 1 1 calc R . . . .
H04M H 0.577385 0.300033 0.740264 0.088 Uiso 1 1 calc R . . . .
C04H C 0.3850(5) 0.2830(3) 0.9126(2) 0.0576(18) Uani 1 1 d . U . . .
H04N H 0.380080 0.302282 0.925979 0.069 Uiso 1 1 calc R . . . .
H04O H 0.393785 0.261825 0.923317 0.069 Uiso 1 1 calc R . . . .
C04I C 0.3172(7) 0.2856(5) 0.4558(4) 0.112(3) Uani 1 1 d D U . . .
H04P H 0.329999 0.265507 0.466949 0.135 Uiso 1 1 calc R . . . .
H04Q H 0.301050 0.276606 0.438185 0.135 Uiso 1 1 calc R . . . .
C04K C 0.3704(8) 0.3081(4) 0.4489(3) 0.108(3) Uani 1 1 d D U . . .
H04R H 0.400646 0.294879 0.438654 0.130 Uiso 1 1 calc R . . . .
C04L C 0.5473(6) 0.2127(4) 0.7766(3) 0.072(2) Uani 1 1 d . U . . .
H04S H 0.555559 0.188472 0.782683 0.086 Uiso 1 1 calc R . . . .
C04N C 0.6085(5) 0.3584(4) 0.5841(3) 0.071(4) Uani 1 1 d . . . . .
H04T H 0.635666 0.377396 0.588351 0.085 Uiso 1 1 calc R . . . .
H04U H 0.616444 0.339148 0.597179 0.085 Uiso 1 1 calc R . . . .
C04R C 0.5840(6) 0.2756(4) 0.7785(3) 0.072(2) Uani 1 1 d . U . . .
H04V H 0.614167 0.291359 0.786174 0.086 Uiso 1 1 calc R . . . .
C04S C 0.4649(5) 0.4518(3) 0.8091(2) 0.057(3) Uani 1 1 d . . . . .
H04W H 0.498164 0.467466 0.806410 0.069 Uiso 1 1 calc R . . . .
H04X H 0.451453 0.454163 0.828539 0.069 Uiso 1 1 calc R . . . .
C04T C 0.3921(8) 0.3212(5) 0.4779(3) 0.110(3) Uani 1 1 d D U . . .
H04Y H 0.401749 0.301018 0.489631 0.132 Uiso 1 1 calc R . . . .
HS H 0.427739 0.334843 0.475193 0.132 Uiso 1 1 calc R . . . .
C04W C -0.0825(5) 0.4170(3) 0.7697(3) 0.061(3) Uani 1 1 d . . . . .
H04Z H -0.087133 0.439801 0.778748 0.073 Uiso 1 1 calc R . . . .
HT H -0.073511 0.399768 0.784335 0.073 Uiso 1 1 calc R . . . .
C04Y C 0.4875(7) 0.2249(4) 0.7863(3) 0.085(4) Uani 1 1 d . U . . .
H04 H 0.484965 0.223250 0.806788 0.102 Uiso 1 1 calc R . . . .
HU H 0.457477 0.209764 0.778200 0.102 Uiso 1 1 calc R . . . .
C04Z C 0.5212(6) 0.2881(4) 0.7873(3) 0.074(2) Uani 1 1 d . U . . .
H4DA H 0.518847 0.289882 0.807773 0.088 Uiso 1 1 calc R . . . .
HV H 0.513760 0.311296 0.779338 0.088 Uiso 1 1 calc R . . . .
C5 C 0.2999(7) 0.4189(4) 0.5967(4) 0.109(3) Uani 1 1 d D U . . .
H5 H 0.328994 0.415096 0.611722 0.130 Uiso 1 1 calc R . . . .
C7 C 0.2426(8) 0.4647(5) 0.5555(4) 0.112(3) Uani 1 1 d D U . . .
H7A H 0.215091 0.470959 0.540617 0.134 Uiso 1 1 calc R . . . .
H7B H 0.263907 0.485928 0.560721 0.134 Uiso 1 1 calc R . . . .
C11 C 0.3279(8) 0.4323(5) 0.5690(3) 0.113(3) Uani 1 1 d D U . . .
H11A H 0.347272 0.454525 0.572912 0.135 Uiso 1 1 calc R . . . .
H11B H 0.357931 0.415559 0.563293 0.135 Uiso 1 1 calc R . . . .
C12 C 0.2664(7) 0.3840(4) 0.5886(4) 0.115(3) Uani 1 1 d D U . . .
H12 H 0.298271 0.370198 0.580114 0.138 Uiso 1 1 calc R . . A 1
C14 C 0.2591(8) 0.4497(5) 0.6032(4) 0.114(3) Uani 1 1 d D U . . .
H14A H 0.281171 0.471593 0.602630 0.137 Uiso 1 1 calc R . . . .
H14B H 0.243235 0.447040 0.622220 0.137 Uiso 1 1 calc R . . . .
C15 C 0.1858(8) 0.4140(4) 0.5782(4) 0.115(3) Uani 1 1 d D U . . .
H15A H 0.149315 0.415221 0.567600 0.138 Uiso 1 1 calc R . . . .
H15B H 0.175935 0.405494 0.597004 0.138 Uiso 1 1 calc R . . . .
C16 C 0.2859(7) 0.4376(4) 0.5440(4) 0.115(3) Uani 1 1 d D U . . .
H16 H 0.306064 0.445838 0.526855 0.138 Uiso 1 1 calc R . . . .
C17 C 0.2531(8) 0.4030(4) 0.5394(4) 0.113(3) Uani 1 1 d D U . . .
H17A H 0.223428 0.407127 0.524990 0.136 Uiso 1 1 calc R . . . .
H17B H 0.280822 0.386189 0.531495 0.136 Uiso 1 1 calc R . . . .
C19 C 0.2234(7) 0.3854(5) 0.5641(3) 0.115(3) Uani 1 1 d D U . . .
H19 H 0.203085 0.363244 0.559849 0.139 Uiso 1 1 calc R . . . .
C21 C 0.2078(8) 0.4516(4) 0.5816(3) 0.113(3) Uani 1 1 d D U . . .
H21 H 0.176816 0.467996 0.587374 0.136 Uiso 1 1 calc R . . . .
C51 C 0.3472(7) 0.3439(4) 0.4933(4) 0.109(3) Uani 1 1 d D U . . .
H51 H 0.363354 0.353700 0.510926 0.131 Uiso 1 1 calc R . . . .
C80 C 0.3426(8) 0.3378(4) 0.4304(4) 0.112(3) Uani 1 1 d D U . . .
H80A H 0.373878 0.352645 0.423118 0.134 Uiso 1 1 calc R . . . .
H80B H 0.323427 0.326924 0.414187 0.134 Uiso 1 1 calc R . . . .
C162 C 0.2499(8) 0.3351(4) 0.4539(4) 0.111(3) Uani 1 1 d D U . . .
H16A H 0.219732 0.348031 0.464027 0.133 Uiso 1 1 calc R . . . .
H16B H 0.232183 0.325809 0.436734 0.133 Uiso 1 1 calc R . . . .
C20 C 0.2983(7) 0.3611(4) 0.4454(3) 0.111(3) Uani 1 1 d D U . . .
H20 H 0.284083 0.380626 0.433608 0.134 Uiso 1 1 calc R . . . .
C57 C 0.3305(9) 0.3733(4) 0.4721(3) 0.112(3) Uani 1 1 d D U . . .
H57A H 0.305872 0.390286 0.481868 0.134 Uiso 1 1 calc R . . . .
H57B H 0.366093 0.385390 0.466408 0.134 Uiso 1 1 calc R . . . .
C134 C 0.2958(8) 0.3201(5) 0.4991(4) 0.110(3) Uani 1 1 d D U . . .
H134 H 0.265623 0.333959 0.508918 0.132 Uiso 1 1 calc R . . . .
C0AA C 0.4947(6) 0.5328(4) 0.6410(3) 0.072(4) Uani 1 1 d . . . . .
H0AB H 0.500344 0.552403 0.653956 0.087 Uiso 1 1 calc R . . . .
H0AC H 0.519343 0.536782 0.624513 0.087 Uiso 1 1 calc R . . . .
AgA Ag 0.22472(8) 0.27754(5) 0.55131(4) 0.0285(4) Uani 0.4232 1 d . . P A 1
S1 S 0.2523(2) 0.35920(15) 0.62032(15) 0.0255(19) Uani 0.448(14) 1 d . . P A 1
Ag1B Ag 0.26390(7) 0.27806(13) 0.59685(7) 0.0252(8) Uani 0.497(10) 1 d . . P A
2
Ag1A Ag 0.26327(7) 0.29375(13) 0.60572(8) 0.0285(9) Uani 0.503(10) 1 d . . P A
1


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag01 Ag01 2.8141(10) 2 ?
Ag01 Ag02 2.8212(7) 2 ?
Ag01 Ag02 2.8144(7) . ?
Ag01 Ag03 2.8254(7) . ?
Ag01 Ag04 2.8431(7) . ?
Ag01 Ag05 2.8117(7) . ?
Ag01 Ag08 3.1080(8) 2 ?
Ag01 Ag08 2.7623(7) . ?
Ag01 Ag09 2.7846(8) . ?
Ag01 Ag0B 3.1200(8) . ?
Ag01 Ag0I 2.7599(9) . ?
Ag01 Ag0O 3.0945(9) . ?
Ag02 Ag02 2.8329(11) 2 ?
Ag02 Ag06 2.8627(8) . ?
Ag02 Ag07 2.8151(8) 2 ?
Ag02 Ag0B 2.7305(8) . ?
Ag02 Ag0F 2.8123(8) 2 ?
Ag02 Ag0O 2.7579(8) 2 ?
Ag02 Ag1B 3.0613(15) 2 ?
Ag02 Ag1B 2.7487(16) . ?
Ag02 Ag1A 3.0348(15) 2 ?
Ag02 Ag1A 2.7319(16) . ?
Ag03 Ag04 2.8888(8) . ?
Ag03 Ag05 2.9280(8) . ?
Ag03 Ag08 3.0928(8) . ?
Ag03 Ag09 2.8136(8) . ?
Ag03 Ag0A 2.8625(8) . ?
Ag03 Ag0B 2.8986(8) . ?
Ag03 Ag0C 3.0724(9) . ?
Ag03 Ag0L 2.8508(9) . ?
Ag03 Cl1 2.7566(19) . ?
Ag03 S00T 2.6043(19) . ?
Ag04 Ag05 2.9141(8) . ?
Ag04 Ag08 2.8299(8) 2 ?
Ag04 Ag08 2.8658(8) . ?
Ag04 Ag0A 3.1049(9) . ?
Ag04 Ag0D 2.9024(8) . ?
Ag04 Ag0I 3.2052(9) . ?
Ag04 Ag0J 2.9777(9) 2 ?
Ag04 Cl1 2.7609(19) . ?
Ag04 S011 2.583(2) . ?
Ag05 Ag09 3.2146(9) . ?
Ag05 Ag0C 2.8671(8) . ?
Ag05 Ag0D 3.1478(9) . ?
Ag05 Ag0I 2.8199(9) . ?
Ag05 Ag0N 2.8928(9) . ?
Ag05 Ag0O 2.8956(9) . ?
Ag05 Cl1 2.835(2) . ?
Ag05 S00Z 2.593(2) . ?
Ag06 Ag07 2.9039(8) 2 ?
Ag06 Ag09 2.7902(8) . ?
Ag06 Ag0B 2.8999(8) . ?
Ag06 Ag0E 3.0775(9) . ?
Ag06 Ag0F 2.9873(8) 2 ?
Ag06 Ag0H 3.1394(9) . ?
Ag06 Ag0K 2.9012(9) . ?
Ag06 Cl00 2.755(2) 2 ?
Ag06 S014 2.622(2) . ?
Ag06 Ag1A 3.2694(16) . ?
Ag07 Ag0B 3.0888(8) 2 ?
Ag07 Ag0E 2.9076(8) 2 ?
Ag07 Ag0F 2.8816(9) . ?
Ag07 Ag0G 3.2096(9) . ?
Ag07 Ag0I 2.8166(9) . ?
Ag07 Ag0M 2.9802(9) . ?
Ag07 Ag0O 2.9132(10) . ?
Ag07 Cl00 2.872(2) . ?
Ag07 S00Y 2.590(2) . ?
Ag08 Ag08 2.7706(13) 2 ?
Ag08 Ag0A 2.8993(8) . ?
Ag08 Ag0B 3.0886(9) . ?
Ag08 Ag0I 3.2980(10) 2 ?
Ag08 Ag0J 2.8655(9) . ?
Ag08 S015 2.525(3) . ?
Ag09 Ag0B 2.7985(9) . ?
Ag09 Ag0C 2.9356(8) . ?
Ag09 Ag0H 2.9245(9) . ?
Ag09 Ag0O 3.3421(12) . ?
Ag09 S0 2.612(5) . ?
Ag09 S1 2.438(5) . ?
Ag09 Ag1A 2.991(5) . ?
Ag0A Ag0J 3.3103(8) . ?
Ag0A S00T 2.446(2) . ?
Ag0A S00V 2.379(2) . ?
Ag0B Ag0E 2.9980(9) . ?
Ag0B Ag0I 3.1162(10) 2 ?
Ag0B Ag0L 2.8237(10) . ?
Ag0B S015 2.553(3) . ?
Ag0C S00Z 2.459(2) . ?
Ag0C S013 2.392(2) . ?
Ag0D Ag0I 2.9170(9) . ?
Ag0D S00U 2.382(2) . ?
Ag0D S011 2.436(2) . ?
Ag0E S00Y 2.442(2) 2 ?
Ag0E S012 2.380(2) . ?
Ag0F Ag0G 2.9241(10) . ?
Ag0F Ag0K 3.1459(10) 2 ?
Ag0F Ag0O 3.1671(10) . ?
Ag0F Cl00 2.691(2) . ?
Ag0F S00X 2.623(2) . ?
Ag0F AgA 2.6737(18) . ?
Ag0F Ag1B 2.780(2) . ?
Ag0F Ag1B 2.743(3) 2 ?
Ag0F Ag1A 2.975(3) . ?
Ag0G Ag0O 2.9221(10) . ?
Ag0G S00W 2.385(2) . ?
Ag0G S00X 2.430(2) . ?
Ag0H Ag0L 2.9836(10) . ?
Ag0H S013 2.416(2) . ?
Ag0H S014 2.404(2) . ?
Ag0I Ag0M 2.8358(11) . ?
Ag0I Ag0O 2.7498(12) . ?
Ag0I S015 2.579(3) 2 ?
Ag0J Ag0J 3.0583(15) 2 ?
Ag0J S00V 2.417(2) . ?
Ag0J S011 2.420(2) 2 ?
Ag0K S010 2.376(2) . ?
Ag0K S014 2.453(2) . ?
Ag0K Ag1B 2.9754(17) . ?
Ag0K Ag1A 3.055(2) . ?
Ag0L S00T 2.473(2) . ?
Ag0L S012 2.428(2) . ?
Ag0M Ag0N 3.0562(12) . ?
Ag0M S00U 2.418(2) . ?
Ag0M S00Y 2.427(2) . ?
Ag0N Ag0O 2.8676(11) . ?
Ag0N S00W 2.425(2) . ?
Ag0N S00Z 2.449(2) . ?
Ag0O S0 2.739(7) . ?
Ag0O S1 2.429(5) . ?
Ag0O Ag1B 3.313(4) . ?
Ag0O Ag1A 2.786(5) . ?
AgB AgB 3.250(3) 2 ?
AgB S00X 2.398(3) . ?
AgB S010 2.321(3) . ?
AgB Ag1B 2.894(3) . ?
S00T C01C 1.827(8) . ?
S00U C01H 1.861(9) . ?
S00V C035 1.848(11) . ?
S00W C02A 1.853(9) . ?
S00X C01S 1.847(9) . ?
S00X AgA 2.557(3) . ?
S00Y C028 1.842(8) . ?
S00Z C01F 1.843(8) . ?
S010 C134 1.851(19) . ?
S010 AgA 2.900(3) 2 ?
S010 AgA 2.572(3) . ?
S011 C01Q 1.828(8) . ?
S012 C026 1.847(11) . ?
S013 C02J 1.870(9) . ?
S014 C01J 1.834(9) . ?
S015 C02P 1.826(14) . ?
S0 C12 1.667(17) . ?
S0 Ag1B 2.628(9) . ?
C018 C01C 1.552(10) . ?
C018 C01O 1.563(10) . ?
C018 C01X 1.533(12) . ?
C019 C01B 1.529(12) . ?
C019 C01M 1.562(13) . ?
C01A C01G 1.565(13) . ?
C01A C028 1.518(12) . ?
C01A C02Z 1.574(13) . ?
C01B C01F 1.542(11) . ?
C01B C027 1.548(12) . ?
C01C C01D 1.547(11) . ?
C01D C02I 1.521(13) . ?
C01D C03O 1.550(12) . ?
C01E C01K 1.484(13) . ?
C01E C01M 1.547(13) . ?
C01F C01K 1.535(12) . ?
C01G C01L 1.530(13) . ?
C01H C01T 1.523(12) . ?
C01H C02S 1.530(11) . ?
C01I C01V 1.524(13) . ?
C01I C02X 1.526(13) . ?
C01J C01P 1.530(12) . ?
C01J C02B 1.519(12) . ?
C01K C02H 1.574(13) . ?
C01L C020 1.530(14) . ?
C01L C02F 1.533(14) . ?
C01M C02L 1.512(14) . ?
C01N C01Y 1.474(14) . ?
C01N C024 1.546(14) . ?
C01N C026 1.544(13) . ?
C01O C03U 1.519(14) . ?
C01P C03D 1.495(15) . ?
C01P C04N 1.566(16) . ?
C01Q C01V 1.545(11) . ?
C01Q C02U 1.538(12) . ?
C01R C01U 1.534(13) . ?
C01R C03I 1.533(13) . ?
C01S C01U 1.529(13) . ?
C01S C022 1.534(11) . ?
C01T C021 1.553(14) . ?
C01T C02E 1.512(14) . ?
C01U C02V 1.538(14) . ?
C01V C01W 1.562(12) . ?
C01W C048 1.543(13) . ?
C01X C033 1.503(14) . ?
C01Y C02C 1.533(15) . ?
C01Z C027 1.512(14) . ?
C01Z C02H 1.539(13) . ?
C01Z C02L 1.531(14) . ?
C020 C038 1.530(12) . ?
C021 C03Q 1.505(14) . ?
C022 C025 1.534(14) . ?
C022 C03S 1.548(13) . ?
C023 C02A 1.528(13) . ?
C023 C02G 1.555(13) . ?
C023 C03F 1.531(15) . ?
C024 C02M 1.554(15) . ?
C025 C03T 1.541(17) . ?
C026 C02Q 1.561(13) . ?
C028 C038 1.550(11) . ?
C029 C02P 1.513(18) . ?
C029 C041 1.442(17) . ?
C029 C04G 1.569(18) . ?
C02A C044 1.543(13) . ?
C02B C02N 1.567(14) . ?
C02B C039 1.568(15) . ?
C02C C030 1.532(15) . ?
C02C C03B 1.518(14) . ?
C02E C03R 1.512(15) . ?
C02F C02Y 1.533(13) . ?
C02G C03Z 1.528(15) . ?
C02I C033 1.568(13) . ?
C02J C032 1.540(12) . ?
C02J C03M 1.539(13) . ?
C02K C02S 1.508(13) . ?
C02K C03R 1.543(13) . ?
C02M C030 1.505(16) . ?
C02M C03Y 1.542(16) . ?
C02N C040 1.493(16) . ?
C02P C037 1.555(18) . ?
C02Q C03B 1.558(16) . ?
C02Q C03Y 1.495(16) . ?
C02R C02U 1.519(13) . ?
C02R C02X 1.558(12) . ?
C02S C04W 1.531(14) . ?
C02T C03Q 1.537(18) . ?
C02T C03R 1.556(18) . ?
C02U C03G 1.531(12) . ?
C02V C03T 1.534(15) . ?
C02W C031 1.551(15) . ?
C02W C034 1.564(15) . ?
C02W C035 1.536(14) . ?
C02X C03J 1.537(14) . ?
C02Y C02Z 1.515(14) . ?
C02Y C036 1.509(14) . ?
C031 C042 1.530(15) . ?
C032 C03A 1.528(13) . ?
C032 C03V 1.569(14) . ?
C033 C04S 1.538(15) . ?
C034 C045 1.555(15) . ?
C035 C03W 1.543(14) . ?
C036 C038 1.547(12) . ?
C037 C04Y 1.535(19) . ?
C037 C04Z 1.466(18) . ?
C039 C03L 1.516(16) . ?
C03A C04F 1.525(16) . ?
C03C C04L 1.552(18) . ?
C03C C04R 1.466(18) . ?
C03D C03L 1.543(15) . ?
C03E C03W 1.525(14) . ?
C03E C042 1.518(14) . ?
C03F C043 1.520(14) . ?
C03G C048 1.516(13) . ?
C03H C03I 1.504(18) . ?
C03H C03T 1.554(18) . ?
C03I C03S 1.475(16) . ?
C03J C048 1.497(15) . ?
C03K C043 1.496(15) . ?
C03K C044 1.529(14) . ?
C03L C04A 1.576(19) . ?
C03M C03N 1.544(14) . ?
C03M C046 1.570(13) . ?
C03N C047 1.520(15) . ?
C03O C03U 1.525(13) . ?
C03P C04I 1.524(9) . ?
C03P C162 1.497(9) . ?
C03P C134 1.541(9) . ?
C03Q C04W 1.568(17) . ?
C03U C04S 1.545(17) . ?
C03V C047 1.537(16) . ?
C03W C04C 1.539(14) . ?
C03X C03Z 1.547(15) . ?
C03X C044 1.545(14) . ?
C03Z C04E 1.505(18) . ?
C040 C04A 1.528(19) . ?
C040 C04N 1.559(16) . ?
C041 C04L 1.553(18) . ?
C042 C04H 1.553(16) . ?
C043 C04E 1.527(17) . ?
C045 C04C 1.543(15) . ?
C045 C04H 1.541(16) . ?
C046 C04F 1.527(15) . ?
C047 C0AA 1.538(16) . ?
C04F C0AA 1.533(17) . ?
C04G C04R 1.500(18) . ?
C04I C04K 1.517(9) . ?
C04K C04T 1.534(9) . ?
C04K C80 1.560(9) . ?
C04L C04Y 1.508(19) . ?
C04R C04Z 1.562(18) . ?
C04T C51 1.521(9) . ?
C5 C11 1.538(9) . ?
C5 C12 1.573(9) . ?
C5 C14 1.524(9) . ?
C7 C16 1.523(9) . ?
C7 C21 1.543(9) . ?
C11 C16 1.531(9) . ?
C12 C19 1.512(9) . ?
C12 S1 1.797(19) . ?
C14 C21 1.552(9) . ?
C15 C19 1.530(9) . ?
C15 C21 1.519(9) . ?
C16 C17 1.527(9) . ?
C17 C19 1.503(9) . ?
C51 C57 1.544(9) . ?
C51 C134 1.500(9) . ?
C80 C20 1.514(9) . ?
C162 C20 1.533(9) . ?
C20 C57 1.529(9) . ?
AgA AgA 2.384(4) 2 ?
AgA Ag1A 2.778(5) . ?
S1 Ag1A 2.586(8) . ?
Ag1B Ag1B 2.219(10) 2 ?
Ag1A Ag1A 3.371(10) 2 ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Ag01 Ag01 Ag02 60.165(17) 2 . ?
Ag01 Ag01 Ag02 59.925(17) 2 2 ?
Ag01 Ag01 Ag03 131.67(3) 2 . ?
Ag01 Ag01 Ag04 109.568(16) 2 . ?
Ag01 Ag01 Ag08 55.342(16) 2 2 ?
Ag01 Ag01 Ag0B 86.26(3) 2 . ?
Ag01 Ag01 Ag0O 115.24(2) 2 . ?
Ag02 Ag01 Ag02 60.36(2) . 2 ?
Ag02 Ag01 Ag03 109.73(2) . . ?
Ag02 Ag01 Ag03 161.14(3) 2 . ?
Ag02 Ag01 Ag04 158.48(3) . . ?
Ag02 Ag01 Ag04 133.75(3) 2 . ?
Ag02 Ag01 Ag08 89.60(2) 2 2 ?
Ag02 Ag01 Ag08 115.40(2) . 2 ?
Ag02 Ag01 Ag0B 54.494(18) . . ?
Ag02 Ag01 Ag0B 114.84(2) 2 . ?
Ag02 Ag01 Ag0O 88.76(2) . . ?
Ag02 Ag01 Ag0O 55.344(18) 2 . ?
Ag03 Ag01 Ag04 61.276(19) . . ?
Ag03 Ag01 Ag08 109.24(2) . 2 ?
Ag03 Ag01 Ag0B 58.104(19) . . ?
Ag03 Ag01 Ag0O 111.32(2) . . ?
Ag04 Ag01 Ag08 56.575(18) . 2 ?
Ag04 Ag01 Ag0B 108.60(2) . . ?
Ag04 Ag01 Ag0O 112.61(3) . . ?
Ag05 Ag01 Ag01 159.98(3) . 2 ?
Ag05 Ag01 Ag02 111.24(2) . 2 ?
Ag05 Ag01 Ag02 133.88(2) . . ?
Ag05 Ag01 Ag03 62.586(19) . . ?
Ag05 Ag01 Ag04 62.036(19) . . ?
Ag05 Ag01 Ag08 109.47(2) . 2 ?
Ag05 Ag01 Ag0B 113.43(2) . . ?
Ag05 Ag01 Ag0O 58.48(2) . . ?
Ag08 Ag01 Ag01 67.741(18) . 2 ?
Ag08 Ag01 Ag02 127.53(2) . 2 ?
Ag08 Ag01 Ag02 97.19(2) . . ?
Ag08 Ag01 Ag03 67.20(2) . . ?
Ag08 Ag01 Ag04 61.47(2) . . ?
Ag08 Ag01 Ag05 116.84(2) . . ?
Ag08 Ag01 Ag08 55.95(3) . 2 ?
Ag08 Ag01 Ag09 113.69(3) . . ?
Ag08 Ag01 Ag0B 116.00(2) 2 . ?
Ag08 Ag01 Ag0B 63.00(2) . . ?
Ag08 Ag01 Ag0O 174.03(3) . . ?
Ag09 Ag01 Ag01 127.56(3) . 2 ?
Ag09 Ag01 Ag02 101.05(2) . 2 ?
Ag09 Ag01 Ag02 67.98(2) . . ?
Ag09 Ag01 Ag03 60.20(2) . . ?
Ag09 Ag01 Ag04 116.11(2) . . ?
Ag09 Ag01 Ag05 70.11(2) . . ?
Ag09 Ag01 Ag08 168.77(3) . 2 ?
Ag09 Ag01 Ag0B 56.24(2) . . ?
Ag09 Ag01 Ag0O 69.06(2) . . ?
Ag0I Ag01 Ag01 99.54(3) . 2 ?
Ag0I Ag01 Ag02 68.46(2) . 2 ?
Ag0I Ag01 Ag02 128.45(3) . . ?
Ag0I Ag01 Ag03 117.17(2) . . ?
Ag0I Ag01 Ag04 69.77(2) . . ?
Ag0I Ag01 Ag05 60.80(2) . . ?
Ag0I Ag01 Ag08 119.35(3) . . ?
Ag0I Ag01 Ag08 68.09(2) . 2 ?
Ag0I Ag01 Ag09 119.05(3) . . ?
Ag0I Ag01 Ag0B 174.19(3) . . ?
Ag0I Ag01 Ag0O 55.67(3) . . ?
Ag0O Ag01 Ag08 120.81(3) . 2 ?
Ag0O Ag01 Ag0B 121.60(3) . . ?
Ag01 Ag02 Ag01 59.91(2) . 2 ?
Ag01 Ag02 Ag02 59.941(18) . 2 ?
Ag01 Ag02 Ag02 59.704(17) 2 2 ?
Ag01 Ag02 Ag06 108.99(2) . . ?
Ag01 Ag02 Ag06 156.38(3) 2 . ?
Ag01 Ag02 Ag07 133.64(3) . 2 ?
Ag01 Ag02 Ag1B 93.84(9) 2 2 ?
Ag01 Ag02 Ag1B 114.64(3) . 2 ?
Ag01 Ag02 Ag1A 115.04(3) . 2 ?
Ag01 Ag02 Ag1A 82.81(10) 2 2 ?
Ag02 Ag02 Ag06 135.96(3) 2 . ?
Ag02 Ag02 Ag1B 55.43(3) 2 2 ?
Ag02 Ag02 Ag1A 55.37(3) 2 2 ?
Ag06 Ag02 Ag1B 109.73(9) . 2 ?
Ag06 Ag02 Ag1A 120.25(9) . 2 ?
Ag07 Ag02 Ag01 109.33(2) 2 2 ?
Ag07 Ag02 Ag02 158.41(3) 2 2 ?
Ag07 Ag02 Ag06 61.51(2) 2 . ?
Ag07 Ag02 Ag1B 110.87(4) 2 2 ?
Ag07 Ag02 Ag1A 107.03(5) 2 2 ?
Ag0B Ag02 Ag01 68.46(2) . . ?
Ag0B Ag02 Ag01 94.07(2) . 2 ?
Ag0B Ag02 Ag02 128.39(2) . 2 ?
Ag0B Ag02 Ag06 62.41(2) . . ?
Ag0B Ag02 Ag07 67.68(2) . 2 ?
Ag0B Ag02 Ag0F 118.13(3) . 2 ?
Ag0B Ag02 Ag0O 115.43(3) . 2 ?
Ag0B Ag02 Ag1B 171.95(11) . 2 ?
Ag0B Ag02 Ag1B 128.42(11) . . ?
Ag0B Ag02 Ag1A 172.67(11) . 2 ?
Ag0B Ag02 Ag1A 115.70(11) . . ?
Ag0F Ag02 Ag01 159.65(3) 2 . ?
Ag0F Ag02 Ag01 134.02(3) 2 2 ?
Ag0F Ag02 Ag02 110.949(19) 2 2 ?
Ag0F Ag02 Ag06 63.52(2) 2 . ?
Ag0F Ag02 Ag07 61.61(2) 2 2 ?
Ag0F Ag02 Ag1B 56.30(5) 2 2 ?
Ag0F Ag02 Ag1A 61.02(5) 2 2 ?
Ag0O Ag02 Ag01 127.24(3) 2 . ?
Ag0O Ag02 Ag01 67.36(2) 2 2 ?
Ag0O Ag02 Ag02 95.47(3) 2 2 ?
Ag0O Ag02 Ag06 118.95(3) 2 . ?
Ag0O Ag02 Ag07 63.02(3) 2 2 ?
Ag0O Ag02 Ag0F 69.30(2) 2 2 ?
Ag0O Ag02 Ag1B 69.19(10) 2 2 ?
Ag0O Ag02 Ag1A 57.24(11) 2 2 ?
Ag1B Ag02 Ag01 101.23(10) . . ?
Ag1B Ag02 Ag06 75.68(6) . . ?
Ag1B Ag02 Ag1A 58.2(2) . 2 ?
Ag1A Ag02 Ag01 125.44(4) . 2 ?
Ag1A Ag02 Ag01 88.67(12) . . ?
Ag1A Ag02 Ag02 66.07(3) . 2 ?
Ag1A Ag02 Ag06 71.48(4) . . ?
Ag1A Ag02 Ag07 123.75(7) . 2 ?
Ag1A Ag02 Ag0F 71.07(11) . 2 ?
Ag1A Ag02 Ag0O 125.47(13) . 2 ?
Ag1A Ag02 Ag1B 13.69(3) 2 2 ?
Ag1A Ag02 Ag1B 58.0(2) . 2 ?
Ag1A Ag02 Ag1A 71.3(2) . 2 ?
Ag01 Ag03 Ag04 59.664(19) . . ?
Ag01 Ag03 Ag05 58.478(18) . . ?
Ag01 Ag03 Ag08 55.425(17) . . ?
Ag01 Ag03 Ag0A 108.82(2) . . ?
Ag01 Ag03 Ag0B 66.05(2) . . ?
Ag01 Ag03 Ag0C 102.00(2) . . ?
Ag01 Ag03 Ag0L 121.27(3) . . ?
Ag04 Ag03 Ag05 60.125(19) . . ?
Ag04 Ag03 Ag08 57.131(19) . . ?
Ag04 Ag03 Ag0B 113.69(2) . . ?
Ag04 Ag03 Ag0C 113.10(2) . . ?
Ag05 Ag03 Ag08 104.10(2) . . ?
Ag05 Ag03 Ag0C 57.025(19) . . ?
Ag09 Ag03 Ag01 59.181(19) . . ?
Ag09 Ag03 Ag04 113.73(2) . . ?
Ag09 Ag03 Ag05 68.06(2) . . ?
Ag09 Ag03 Ag08 103.57(2) . . ?
Ag09 Ag03 Ag0A 159.85(3) . . ?
Ag09 Ag03 Ag0B 58.65(2) . . ?
Ag09 Ag03 Ag0C 59.640(19) . . ?
Ag09 Ag03 Ag0L 75.55(2) . . ?
Ag0A Ag03 Ag04 65.35(2) . . ?
Ag0A Ag03 Ag05 121.67(3) . . ?
Ag0A Ag03 Ag08 58.114(18) . . ?
Ag0A Ag03 Ag0B 102.39(2) . . ?
Ag0A Ag03 Ag0C 140.33(2) . . ?
Ag0B Ag03 Ag05 116.75(2) . . ?
Ag0B Ag03 Ag08 61.96(2) . . ?
Ag0B Ag03 Ag0C 112.77(2) . . ?
Ag0C Ag03 Ag08 157.40(3) . . ?
Ag0L Ag03 Ag04 164.07(3) . . ?
Ag0L Ag03 Ag05 135.30(3) . . ?
Ag0L Ag03 Ag08 109.05(2) . . ?
Ag0L Ag03 Ag0A 101.31(3) . . ?
Ag0L Ag03 Ag0B 58.82(2) . . ?
Ag0L Ag03 Ag0C 82.65(2) . . ?
Cl1 Ag03 Ag01 107.20(5) . . ?
Cl1 Ag03 Ag04 58.50(4) . . ?
Cl1 Ag03 Ag05 59.74(4) . . ?
Cl1 Ag03 Ag08 111.23(5) . . ?
Cl1 Ag03 Ag09 122.22(5) . . ?
Cl1 Ag03 Ag0A 75.55(5) . . ?
Cl1 Ag03 Ag0B 172.16(5) . . ?
Cl1 Ag03 Ag0C 71.85(5) . . ?
Cl1 Ag03 Ag0L 128.88(5) . . ?
S00T Ag03 Ag01 150.54(5) . . ?
S00T Ag03 Ag04 116.54(5) . . ?
S00T Ag03 Ag05 148.75(5) . . ?
S00T Ag03 Ag08 96.83(5) . . ?
S00T Ag03 Ag09 129.09(5) . . ?
S00T Ag03 Ag0A 52.91(5) . . ?
S00T Ag03 Ag0B 93.48(5) . . ?
S00T Ag03 Ag0C 105.58(5) . . ?
S00T Ag03 Ag0L 53.68(5) . . ?
S00T Ag03 Cl1 91.21(6) . . ?
Ag01 Ag04 Ag03 59.060(18) . . ?
Ag01 Ag04 Ag05 58.453(18) . . ?
Ag01 Ag04 Ag08 57.875(18) . . ?
Ag01 Ag04 Ag0A 102.00(2) . . ?
Ag01 Ag04 Ag0D 107.08(2) . . ?
Ag01 Ag04 Ag0I 53.897(19) . . ?
Ag01 Ag04 Ag0J 124.07(2) . 2 ?
Ag03 Ag04 Ag05 60.606(19) . . ?
Ag03 Ag04 Ag0A 56.918(18) . . ?
Ag03 Ag04 Ag0D 122.52(3) . . ?
Ag03 Ag04 Ag0I 102.80(2) . . ?
Ag03 Ag04 Ag0J 138.71(3) . 2 ?
Ag05 Ag04 Ag0A 114.26(2) . . ?
Ag05 Ag04 Ag0I 54.63(2) . . ?
Ag05 Ag04 Ag0J 160.52(3) . 2 ?
Ag08 Ag04 Ag01 66.442(19) 2 . ?
Ag08 Ag04 Ag03 65.02(2) . . ?
Ag08 Ag04 Ag03 115.65(2) 2 . ?
Ag08 Ag04 Ag05 114.70(2) 2 . ?
Ag08 Ag04 Ag05 110.49(2) . . ?
Ag08 Ag04 Ag08 58.21(2) 2 . ?
Ag08 Ag04 Ag0A 57.937(19) . . ?
Ag08 Ag04 Ag0A 108.71(2) 2 . ?
Ag08 Ag04 Ag0D 158.94(3) . . ?
Ag08 Ag04 Ag0D 103.47(3) 2 . ?
Ag08 Ag04 Ag0I 103.33(2) . . ?
Ag08 Ag04 Ag0I 65.91(2) 2 . ?
Ag08 Ag04 Ag0J 59.06(2) 2 2 ?
Ag08 Ag04 Ag0J 82.60(2) . 2 ?
Ag0A Ag04 Ag0I 155.84(2) . . ?
Ag0D Ag04 Ag05 65.53(2) . . ?
Ag0D Ag04 Ag0A 143.11(3) . . ?
Ag0D Ag04 Ag0I 56.80(2) . . ?
Ag0D Ag04 Ag0J 96.97(3) . 2 ?
Ag0J Ag04 Ag0A 84.76(2) 2 . ?
Ag0J Ag04 Ag0I 109.35(3) 2 . ?
Cl1 Ag04 Ag01 106.59(5) . . ?
Cl1 Ag04 Ag03 58.35(4) . . ?
Cl1 Ag04 Ag05 59.87(4) . . ?
Cl1 Ag04 Ag08 173.02(5) . 2 ?
Cl1 Ag04 Ag08 118.30(5) . . ?
Cl1 Ag04 Ag0A 71.61(5) . . ?
Cl1 Ag04 Ag0D 78.63(5) . . ?
Cl1 Ag04 Ag0I 110.80(5) . . ?
Cl1 Ag04 Ag0J 127.59(5) . 2 ?
S011 Ag04 Ag01 150.16(5) . . ?
S011 Ag04 Ag03 147.79(5) . . ?
S011 Ag04 Ag05 115.72(5) . . ?
S011 Ag04 Ag08 133.29(5) . . ?
S011 Ag04 Ag08 95.28(5) . 2 ?
S011 Ag04 Ag0A 106.31(5) . . ?
S011 Ag04 Ag0D 52.34(5) . . ?
S011 Ag04 Ag0I 97.73(5) . . ?
S011 Ag04 Ag0J 51.00(5) . 2 ?
S011 Ag04 Cl1 91.25(6) . . ?
Ag01 Ag05 Ag03 58.936(18) . . ?
Ag01 Ag05 Ag04 59.510(18) . . ?
Ag01 Ag05 Ag09 54.547(18) . . ?
Ag01 Ag05 Ag0C 107.72(3) . . ?
Ag01 Ag05 Ag0D 101.54(2) . . ?
Ag01 Ag05 Ag0I 58.69(2) . . ?
Ag01 Ag05 Ag0N 123.36(3) . . ?
Ag01 Ag05 Ag0O 65.65(2) . . ?
Ag01 Ag05 Cl1 105.44(4) . . ?
Ag03 Ag05 Ag09 54.280(18) . . ?
Ag03 Ag05 Ag0D 113.33(2) . . ?
Ag04 Ag05 Ag03 59.269(19) . . ?
Ag04 Ag05 Ag09 102.26(2) . . ?
Ag04 Ag05 Ag0D 57.057(19) . . ?
Ag0C Ag05 Ag03 64.02(2) . . ?
Ag0C Ag05 Ag04 118.75(3) . . ?
Ag0C Ag05 Ag09 57.38(2) . . ?
Ag0C Ag05 Ag0D 140.82(3) . . ?
Ag0C Ag05 Ag0N 99.38(3) . . ?
Ag0C Ag05 Ag0O 105.86(3) . . ?
Ag0D Ag05 Ag09 155.86(2) . . ?
Ag0I Ag05 Ag03 112.04(3) . . ?
Ag0I Ag05 Ag04 67.95(2) . . ?
Ag0I Ag05 Ag09 104.53(2) . . ?
Ag0I Ag05 Ag0C 160.96(3) . . ?
Ag0I Ag05 Ag0D 58.21(2) . . ?
Ag0I Ag05 Ag0N 80.46(3) . . ?
Ag0I Ag05 Ag0O 57.50(3) . . ?
Ag0I Ag05 Cl1 120.82(5) . . ?
Ag0N Ag05 Ag03 161.04(3) . . ?
Ag0N Ag05 Ag04 139.53(3) . . ?
Ag0N Ag05 Ag09 109.88(2) . . ?
Ag0N Ag05 Ag0D 85.21(2) . . ?
Ag0N Ag05 Ag0O 59.39(2) . . ?
Ag0O Ag05 Ag03 114.23(3) . . ?
Ag0O Ag05 Ag04 116.57(2) . . ?
Ag0O Ag05 Ag09 66.08(3) . . ?
Ag0O Ag05 Ag0D 109.71(3) . . ?
Cl1 Ag05 Ag03 57.12(4) . . ?
Cl1 Ag05 Ag04 57.38(4) . . ?
Cl1 Ag05 Ag09 107.28(5) . . ?
Cl1 Ag05 Ag0C 73.94(5) . . ?
Cl1 Ag05 Ag0D 73.54(5) . . ?
Cl1 Ag05 Ag0N 129.81(5) . . ?
Cl1 Ag05 Ag0O 170.79(5) . . ?
S00Z Ag05 Ag01 152.02(5) . . ?
S00Z Ag05 Ag03 115.16(5) . . ?
S00Z Ag05 Ag04 144.79(5) . . ?
S00Z Ag05 Ag09 98.77(5) . . ?
S00Z Ag05 Ag0C 53.24(5) . . ?
S00Z Ag05 Ag0D 105.37(5) . . ?
S00Z Ag05 Ag0I 132.55(6) . . ?
S00Z Ag05 Ag0N 52.69(5) . . ?
S00Z Ag05 Ag0O 97.68(5) . . ?
S00Z Ag05 Cl1 89.54(6) . . ?
Ag02 Ag06 Ag07 58.436(19) . 2 ?
Ag02 Ag06 Ag0B 56.562(19) . . ?
Ag02 Ag06 Ag0E 103.28(2) . . ?
Ag02 Ag06 Ag0F 57.419(19) . 2 ?
Ag02 Ag06 Ag0H 125.50(3) . . ?
Ag02 Ag06 Ag0K 103.90(3) . . ?
Ag02 Ag06 Ag1A 52.40(3) . . ?
Ag07 Ag06 Ag0E 58.09(2) 2 . ?
Ag07 Ag06 Ag0F 58.55(2) 2 2 ?
Ag07 Ag06 Ag0H 144.28(3) 2 . ?
Ag07 Ag06 Ag1A 104.68(7) 2 . ?
Ag09 Ag06 Ag02 67.23(2) . . ?
Ag09 Ag06 Ag07 116.17(2) . 2 ?
Ag09 Ag06 Ag0B 58.88(2) . . ?
Ag09 Ag06 Ag0E 110.09(3) . . ?
Ag09 Ag06 Ag0F 115.11(3) . 2 ?
Ag09 Ag06 Ag0H 58.75(2) . . ?
Ag09 Ag06 Ag0K 102.22(3) . . ?
Ag09 Ag06 Ag1A 58.53(11) . . ?
Ag0B Ag06 Ag07 64.31(2) . 2 ?
Ag0B Ag06 Ag0E 60.12(2) . . ?
Ag0B Ag06 Ag0F 107.71(2) . 2 ?
Ag0B Ag06 Ag0H 88.19(2) . . ?
Ag0B Ag06 Ag0K 155.85(3) . . ?
Ag0B Ag06 Ag1A 96.94(6) . . ?
Ag0E Ag06 Ag0H 89.11(2) . . ?
Ag0E Ag06 Ag1A 154.98(3) . . ?
Ag0F Ag06 Ag0E 113.00(3) 2 . ?
Ag0F Ag06 Ag0H 157.05(3) 2 . ?
Ag0F Ag06 Ag1A 61.81(11) 2 . ?
Ag0H Ag06 Ag1A 100.72(10) . . ?
Ag0K Ag06 Ag07 120.41(3) . 2 ?
Ag0K Ag06 Ag0E 143.83(3) . . ?
Ag0K Ag06 Ag0F 64.56(2) . 2 ?
Ag0K Ag06 Ag0H 94.15(3) . . ?
Ag0K Ag06 Ag1A 59.00(5) . . ?
Cl00 Ag06 Ag02 105.27(5) 2 . ?
Cl00 Ag06 Ag07 60.94(5) 2 2 ?
Cl00 Ag06 Ag09 170.80(5) 2 . ?
Cl00 Ag06 Ag0B 122.27(5) 2 . ?
Cl00 Ag06 Ag0E 76.29(5) 2 . ?
Cl00 Ag06 Ag0F 55.72(5) 2 2 ?
Cl00 Ag06 Ag0H 129.18(5) 2 . ?
Cl00 Ag06 Ag0K 73.85(5) 2 . ?
Cl00 Ag06 Ag1A 112.91(12) 2 . ?
S014 Ag06 Ag02 147.15(6) . . ?
S014 Ag06 Ag07 149.76(6) . 2 ?
S014 Ag06 Ag09 93.61(5) . . ?
S014 Ag06 Ag0B 136.35(5) . . ?
S014 Ag06 Ag0E 108.47(5) . . ?
S014 Ag06 Ag0F 114.93(5) . 2 ?
S014 Ag06 Ag0H 48.30(5) . . ?
S014 Ag06 Ag0K 52.43(5) . . ?
S014 Ag06 Cl00 90.44(7) . 2 ?
S014 Ag06 Ag1A 95.02(6) . . ?
Ag02 Ag07 Ag06 60.057(19) 2 2 ?
Ag02 Ag07 Ag0B 54.859(19) 2 2 ?
Ag02 Ag07 Ag0E 109.02(3) 2 2 ?
Ag02 Ag07 Ag0F 59.15(2) 2 . ?
Ag02 Ag07 Ag0G 100.50(2) 2 . ?
Ag02 Ag07 Ag0I 67.78(2) 2 . ?
Ag02 Ag07 Ag0M 124.85(3) 2 . ?
Ag02 Ag07 Ag0O 57.53(2) 2 . ?
Ag02 Ag07 Cl00 103.47(5) 2 . ?
Ag06 Ag07 Ag0B 57.78(2) 2 2 ?
Ag06 Ag07 Ag0E 63.95(2) 2 2 ?
Ag06 Ag07 Ag0G 116.42(3) 2 . ?
Ag06 Ag07 Ag0M 158.90(3) 2 . ?
Ag06 Ag07 Ag0O 112.70(3) 2 . ?
Ag0B Ag07 Ag0G 155.05(3) 2 . ?
Ag0E Ag07 Ag0B 59.91(2) 2 2 ?
Ag0E Ag07 Ag0G 142.95(3) 2 . ?
Ag0E Ag07 Ag0M 96.64(3) 2 . ?
Ag0E Ag07 Ag0O 160.24(3) 2 . ?
Ag0F Ag07 Ag06 62.18(2) . 2 ?
Ag0F Ag07 Ag0B 105.50(2) . 2 ?
Ag0F Ag07 Ag0E 121.76(3) . 2 ?
Ag0F Ag07 Ag0G 57.07(2) . . ?
Ag0F Ag07 Ag0M 138.91(3) . . ?
Ag0F Ag07 Ag0O 66.26(2) . . ?
Ag0I Ag07 Ag06 116.39(3) . 2 ?
Ag0I Ag07 Ag0B 63.50(2) . 2 ?
Ag0I Ag07 Ag0E 105.44(3) . 2 ?
Ag0I Ag07 Ag0F 116.85(3) . . ?
Ag0I Ag07 Ag0G 106.18(3) . . ?
Ag0I Ag07 Ag0M 58.50(2) . . ?
Ag0I Ag07 Ag0O 57.33(2) . . ?
Ag0I Ag07 Cl00 171.24(5) . . ?
Ag0M Ag07 Ag0B 106.33(3) . 2 ?
Ag0M Ag07 Ag0G 83.88(2) . . ?
Ag0O Ag07 Ag0B 101.22(2) . 2 ?
Ag0O Ag07 Ag0G 56.76(2) . . ?
Ag0O Ag07 Ag0M 82.57(3) . . ?
Cl00 Ag07 Ag06 56.97(4) . 2 ?
Cl00 Ag07 Ag0B 112.32(5) . 2 ?
Cl00 Ag07 Ag0E 77.33(4) . 2 ?
Cl00 Ag07 Ag0F 55.78(5) . . ?
Cl00 Ag07 Ag0G 74.35(4) . . ?
Cl00 Ag07 Ag0M 129.90(5) . . ?
Cl00 Ag07 Ag0O 118.25(5) . . ?
S00Y Ag07 Ag02 153.09(5) . 2 ?
S00Y Ag07 Ag06 113.95(5) . 2 ?
S00Y Ag07 Ag0B 98.92(5) . 2 ?
S00Y Ag07 Ag0E 52.35(5) . 2 ?
S00Y Ag07 Ag0F 144.78(5) . . ?
S00Y Ag07 Ag0G 104.99(5) . . ?
S00Y Ag07 Ag0I 96.57(5) . . ?
S00Y Ag07 Ag0M 51.08(5) . . ?
S00Y Ag07 Ag0O 133.07(5) . . ?
S00Y Ag07 Cl00 91.67(7) . . ?
Ag01 Ag08 Ag01 56.92(2) . 2 ?
Ag01 Ag08 Ag03 57.372(18) . . ?
Ag01 Ag08 Ag04 111.47(2) . 2 ?
Ag01 Ag08 Ag04 60.651(19) . . ?
Ag01 Ag08 Ag08 68.35(2) . 2 ?
Ag01 Ag08 Ag0A 109.55(2) . . ?
Ag01 Ag08 Ag0B 64.17(2) . . ?
Ag01 Ag08 Ag0I 88.75(2) . 2 ?
Ag01 Ag08 Ag0I 50.932(18) 2 2 ?
Ag01 Ag08 Ag0J 151.83(3) . . ?
Ag03 Ag08 Ag01 112.15(2) . 2 ?
Ag03 Ag08 Ag0I 113.84(2) . 2 ?
Ag04 Ag08 Ag01 56.983(17) 2 2 ?
Ag04 Ag08 Ag01 101.29(2) . 2 ?
Ag04 Ag08 Ag03 57.850(18) . . ?
Ag04 Ag08 Ag03 168.82(3) 2 . ?
Ag04 Ag08 Ag04 118.98(3) 2 . ?
Ag04 Ag08 Ag0A 133.13(3) 2 . ?
Ag04 Ag08 Ag0A 65.17(2) . . ?
Ag04 Ag08 Ag0B 120.64(3) 2 . ?
Ag04 Ag08 Ag0B 108.87(2) . . ?
Ag04 Ag08 Ag0I 62.52(2) 2 2 ?
Ag04 Ag08 Ag0I 148.41(3) . 2 ?
Ag04 Ag08 Ag0J 63.04(2) 2 . ?
Ag08 Ag08 Ag01 55.700(17) 2 2 ?
Ag08 Ag08 Ag03 111.17(3) 2 . ?
Ag08 Ag08 Ag04 61.54(2) 2 2 ?
Ag08 Ag08 Ag04 60.25(2) 2 . ?
Ag08 Ag08 Ag0A 116.64(3) 2 . ?
Ag08 Ag08 Ag0B 128.610(16) 2 . ?
Ag08 Ag08 Ag0I 103.18(2) 2 2 ?
Ag08 Ag08 Ag0J 86.37(2) 2 . ?
Ag0A Ag08 Ag01 165.47(3) . 2 ?
Ag0A Ag08 Ag03 56.962(18) . . ?
Ag0A Ag08 Ag0B 97.09(2) . . ?
Ag0A Ag08 Ag0I 139.88(3) . 2 ?
Ag0B Ag08 Ag01 81.94(2) . 2 ?
Ag0B Ag08 Ag03 55.928(19) . . ?
Ag0B Ag08 Ag0I 58.30(2) . 2 ?
Ag0J Ag08 Ag01 118.74(2) . 2 ?
Ag0J Ag08 Ag03 126.75(3) . . ?
Ag0J Ag08 Ag04 96.56(3) . . ?
Ag0J Ag08 Ag0A 70.09(2) . . ?
Ag0J Ag08 Ag0B 143.66(3) . . ?
Ag0J Ag08 Ag0I 109.72(2) . 2 ?
S015 Ag08 Ag01 116.03(6) . . ?
S015 Ag08 Ag01 101.12(6) . 2 ?
S015 Ag08 Ag03 92.77(7) . . ?
S015 Ag08 Ag04 148.24(7) . . ?
S015 Ag08 Ag04 92.16(7) . 2 ?
S015 Ag08 Ag08 151.13(7) . 2 ?
S015 Ag08 Ag0A 89.59(7) . . ?
S015 Ag08 Ag0B 52.94(6) . . ?
S015 Ag08 Ag0I 50.47(6) . 2 ?
S015 Ag08 Ag0J 92.09(6) . . ?
Ag01 Ag09 Ag02 56.463(17) . . ?
Ag01 Ag09 Ag03 60.620(19) . . ?
Ag01 Ag09 Ag05 55.339(18) . . ?
Ag01 Ag09 Ag06 112.00(2) . . ?
Ag01 Ag09 Ag0B 67.95(2) . . ?
Ag01 Ag09 Ag0C 106.56(2) . . ?
Ag01 Ag09 Ag0H 158.81(3) . . ?
Ag01 Ag09 Ag0O 59.85(2) . . ?
Ag01 Ag09 Ag1A 84.23(3) . . ?
Ag02 Ag09 Ag05 109.34(2) . . ?
Ag02 Ag09 Ag0O 79.40(2) . . ?
Ag03 Ag09 Ag02 101.66(2) . . ?
Ag03 Ag09 Ag05 57.660(19) . . ?
Ag03 Ag09 Ag0C 64.57(2) . . ?
Ag03 Ag09 Ag0H 101.19(3) . . ?
Ag03 Ag09 Ag0O 104.88(3) . . ?
Ag03 Ag09 Ag1A 144.84(4) . . ?
Ag05 Ag09 Ag0O 52.37(2) . . ?
Ag06 Ag09 Ag02 57.489(18) . . ?
Ag06 Ag09 Ag03 121.74(3) . . ?
Ag06 Ag09 Ag05 166.83(3) . . ?
Ag06 Ag09 Ag0B 62.52(2) . . ?
Ag06 Ag09 Ag0C 137.63(3) . . ?
Ag06 Ag09 Ag0H 66.60(2) . . ?
Ag06 Ag09 Ag0O 120.13(3) . . ?
Ag06 Ag09 Ag1A 68.77(7) . . ?
Ag0B Ag09 Ag02 54.499(19) . . ?
Ag0B Ag09 Ag03 62.19(2) . . ?
Ag0B Ag09 Ag05 111.01(2) . . ?
Ag0B Ag09 Ag0C 120.29(3) . . ?
Ag0B Ag09 Ag0H 94.58(3) . . ?
Ag0B Ag09 Ag0O 123.88(3) . . ?
Ag0B Ag09 Ag1A 105.98(7) . . ?
Ag0C Ag09 Ag02 162.90(3) . . ?
Ag0C Ag09 Ag05 55.349(18) . . ?
Ag0C Ag09 Ag0O 93.96(2) . . ?
Ag0C Ag09 Ag1A 133.33(8) . . ?
Ag0H Ag09 Ag02 123.62(3) . . ?
Ag0H Ag09 Ag05 126.43(2) . . ?
Ag0H Ag09 Ag0C 71.09(2) . . ?
Ag0H Ag09 Ag0O 140.39(3) . . ?
Ag0H Ag09 Ag1A 113.09(4) . . ?
S0 Ag09 Ag01 110.45(12) . . ?
S0 Ag09 Ag02 93.90(17) . . ?
S0 Ag09 Ag03 150.2(2) . . ?
S0 Ag09 Ag05 93.3(2) . . ?
S0 Ag09 Ag06 88.0(2) . . ?
S0 Ag09 Ag0B 144.5(2) . . ?
S0 Ag09 Ag0C 94.6(2) . . ?
S0 Ag09 Ag0H 90.72(12) . . ?
S0 Ag09 Ag0O 53.08(15) . . ?
S1 Ag09 Ag01 106.27(12) . . ?
S1 Ag09 Ag02 107.52(16) . . ?
S1 Ag09 Ag03 131.45(19) . . ?
S1 Ag09 Ag05 76.20(18) . . ?
S1 Ag09 Ag06 106.66(19) . . ?
S1 Ag09 Ag0B 161.73(17) . . ?
S1 Ag09 Ag0C 77.81(18) . . ?
S1 Ag09 Ag0H 93.95(11) . . ?
S1 Ag09 Ag0O 46.51(11) . . ?
S1 Ag09 Ag1A 55.77(18) . . ?
Ag1A Ag09 Ag02 52.95(6) . . ?
Ag1A Ag09 Ag05 104.08(6) . . ?
Ag1A Ag09 Ag0O 51.82(6) . . ?
Ag03 Ag0A Ag04 57.735(18) . . ?
Ag03 Ag0A Ag08 64.92(2) . . ?
Ag03 Ag0A Ag0J 119.14(2) . . ?
Ag04 Ag0A Ag0J 83.58(2) . . ?
Ag08 Ag0A Ag04 56.893(19) . . ?
Ag08 Ag0A Ag0J 54.477(19) . . ?
S00T Ag0A Ag03 58.13(5) . . ?
S00T Ag0A Ag04 114.20(5) . . ?
S00T Ag0A Ag08 105.84(5) . . ?
S00T Ag0A Ag0J 142.05(5) . . ?
S00V Ag0A Ag03 150.79(6) . . ?
S00V Ag0A Ag04 93.25(5) . . ?
S00V Ag0A Ag08 97.84(5) . . ?
S00V Ag0A Ag0J 46.83(5) . . ?
S00V Ag0A S00T 150.57(7) . . ?
Ag02 Ag0B Ag01 57.042(19) . . ?
Ag02 Ag0B Ag03 110.01(3) . . ?
Ag02 Ag0B Ag06 61.03(2) . . ?
Ag02 Ag0B Ag07 57.463(19) . 2 ?
Ag02 Ag0B Ag08 91.70(2) . . ?
Ag02 Ag0B Ag09 68.95(2) . . ?
Ag02 Ag0B Ag0E 108.77(3) . . ?
Ag02 Ag0B Ag0I 64.58(2) . 2 ?
Ag02 Ag0B Ag0L 142.63(3) . . ?
Ag03 Ag0B Ag01 55.850(18) . . ?
Ag03 Ag0B Ag06 115.17(3) . . ?
Ag03 Ag0B Ag07 167.16(3) . 2 ?
Ag03 Ag0B Ag08 62.108(19) . . ?
Ag03 Ag0B Ag0E 131.80(3) . . ?
Ag03 Ag0B Ag0I 125.83(3) . 2 ?
Ag06 Ag0B Ag01 100.24(2) . . ?
Ag06 Ag0B Ag07 57.905(19) . 2 ?
Ag06 Ag0B Ag08 150.87(3) . . ?
Ag06 Ag0B Ag0E 62.88(2) . . ?
Ag06 Ag0B Ag0I 107.77(3) . 2 ?
Ag07 Ag0B Ag01 112.92(2) 2 . ?
Ag07 Ag0B Ag0I 53.99(2) 2 2 ?
Ag08 Ag0B Ag01 52.833(18) . . ?
Ag08 Ag0B Ag07 117.79(3) . 2 ?
Ag08 Ag0B Ag0I 64.22(2) . 2 ?
Ag09 Ag0B Ag01 55.813(19) . . ?
Ag09 Ag0B Ag03 59.16(2) . . ?
Ag09 Ag0B Ag06 58.60(2) . . ?
Ag09 Ag0B Ag07 110.27(2) . 2 ?
Ag09 Ag0B Ag08 104.04(3) . . ?
Ag09 Ag0B Ag0E 112.18(3) . . ?
Ag09 Ag0B Ag0I 131.20(3) . 2 ?
Ag09 Ag0B Ag0L 76.22(3) . . ?
Ag0E Ag0B Ag01 162.90(3) . . ?
Ag0E Ag0B Ag07 57.046(19) . 2 ?
Ag0E Ag0B Ag08 142.76(3) . . ?
Ag0E Ag0B Ag0I 96.30(2) . 2 ?
Ag0I Ag0B Ag01 86.06(2) 2 . ?
Ag0L Ag0B Ag01 112.58(3) . . ?
Ag0L Ag0B Ag03 59.74(2) . . ?
Ag0L Ag0B Ag06 89.59(3) . . ?
Ag0L Ag0B Ag07 127.56(3) . 2 ?
Ag0L Ag0B Ag08 109.89(2) . . ?
Ag0L Ag0B Ag0E 72.07(2) . . ?
Ag0L Ag0B Ag0I 152.27(3) . 2 ?
S015 Ag0B Ag01 104.09(7) . . ?
S015 Ag0B Ag02 116.22(7) . . ?
S015 Ag0B Ag03 96.90(7) . . ?
S015 Ag0B Ag06 147.07(7) . . ?
S015 Ag0B Ag07 91.94(7) . 2 ?
S015 Ag0B Ag08 52.13(7) . . ?
S015 Ag0B Ag09 154.18(7) . . ?
S015 Ag0B Ag0E 90.66(7) . . ?
S015 Ag0B Ag0I 53.00(7) . 2 ?
S015 Ag0B Ag0L 101.02(7) . . ?
Ag05 Ag0C Ag03 58.952(19) . . ?
Ag05 Ag0C Ag09 67.27(2) . . ?
Ag09 Ag0C Ag03 55.794(19) . . ?
S00Z Ag0C Ag03 114.51(5) . . ?
S00Z Ag0C Ag05 57.66(5) . . ?
S00Z Ag0C Ag09 109.99(5) . . ?
S013 Ag0C Ag03 96.44(6) . . ?
S013 Ag0C Ag05 154.91(6) . . ?
S013 Ag0C Ag09 95.77(6) . . ?
S013 Ag0C S00Z 147.28(7) . . ?
Ag04 Ag0D Ag05 57.415(19) . . ?
Ag04 Ag0D Ag0I 66.84(2) . . ?
Ag0I Ag0D Ag05 55.26(2) . . ?
S00U Ag0D Ag04 150.77(6) . . ?
S00U Ag0D Ag05 93.82(6) . . ?
S00U Ag0D Ag0I 93.52(5) . . ?
S00U Ag0D S011 151.86(8) . . ?
S011 Ag0D Ag04 57.08(5) . . ?
S011 Ag0D Ag05 112.44(6) . . ?
S011 Ag0D Ag0I 109.43(5) . . ?
Ag07 Ag0E Ag06 57.96(2) 2 . ?
Ag07 Ag0E Ag0B 63.05(2) 2 . ?
Ag0B Ag0E Ag06 57.00(2) . . ?
S00Y Ag0E Ag06 112.75(6) 2 . ?
S00Y Ag0E Ag07 57.12(5) 2 2 ?
S00Y Ag0E Ag0B 104.97(6) 2 . ?
S012 Ag0E Ag06 87.38(6) . . ?
S012 Ag0E Ag07 144.83(6) . 2 ?
S012 Ag0E Ag0B 94.47(6) . . ?
S012 Ag0E S00Y 157.40(8) . 2 ?
Ag02 Ag0F Ag06 59.065(19) 2 2 ?
Ag02 Ag0F Ag07 59.24(2) 2 . ?
Ag02 Ag0F Ag0G 107.91(3) 2 . ?
Ag02 Ag0F Ag0K 99.10(3) 2 2 ?
Ag02 Ag0F Ag0O 54.544(19) 2 . ?
Ag02 Ag0F Ag1A 63.19(4) 2 . ?
Ag06 Ag0F Ag0K 56.40(2) 2 2 ?
Ag06 Ag0F Ag0O 103.73(2) 2 . ?
Ag07 Ag0F Ag06 59.27(2) . 2 ?
Ag07 Ag0F Ag0G 67.12(2) . . ?
Ag07 Ag0F Ag0K 113.32(3) . 2 ?
Ag07 Ag0F Ag0O 57.35(2) . . ?
Ag07 Ag0F Ag1A 106.90(10) . . ?
Ag0G Ag0F Ag06 123.14(3) . 2 ?
Ag0G Ag0F Ag0K 146.47(3) . 2 ?
Ag0G Ag0F Ag0O 57.17(2) . . ?
Ag0G Ag0F Ag1A 93.49(10) . . ?
Ag0K Ag0F Ag0O 153.61(3) 2 . ?
Cl00 Ag0F Ag02 108.44(5) . 2 ?
Cl00 Ag0F Ag06 57.76(4) . 2 ?
Cl00 Ag0F Ag07 61.93(5) . . ?
Cl00 Ag0F Ag0G 81.91(5) . . ?
Cl00 Ag0F Ag0K 70.77(5) . 2 ?
Cl00 Ag0F Ag0O 115.66(5) . . ?
Cl00 Ag0F Ag1B 171.63(9) . . ?
Cl00 Ag0F Ag1B 124.55(10) . 2 ?
Cl00 Ag0F Ag1A 168.83(11) . . ?
S00X Ag0F Ag02 148.21(5) . 2 ?
S00X Ag0F Ag06 150.25(5) . 2 ?
S00X Ag0F Ag07 116.92(6) . . ?
S00X Ag0F Ag0G 51.62(5) . . ?
S00X Ag0F Ag0K 109.91(5) . 2 ?
S00X Ag0F Ag0O 95.55(5) . . ?
S00X Ag0F Cl00 93.55(7) . . ?
S00X Ag0F AgA 57.71(7) . . ?
S00X Ag0F Ag1B 125.42(11) . 2 ?
S00X Ag0F Ag1B 93.90(6) . . ?
S00X Ag0F Ag1A 91.50(6) . . ?
AgA Ag0F Ag02 115.15(5) . 2 ?
AgA Ag0F Ag06 134.70(5) . 2 ?
AgA Ag0F Ag07 162.35(5) . . ?
AgA Ag0F Ag0G 101.82(5) . . ?
AgA Ag0F Ag0K 83.63(4) . 2 ?
AgA Ag0F Ag0O 105.27(4) . . ?
AgA Ag0F Cl00 132.20(6) . . ?
AgA Ag0F Ag1B 67.72(11) . 2 ?
AgA Ag0F Ag1A 58.64(9) . . ?
Ag1B Ag0F Ag07 117.52(9) . . ?
Ag1B Ag0F Ag07 115.38(9) 2 . ?
Ag1B Ag0F Ag0G 152.33(7) 2 . ?
Ag1B Ag0F Ag0G 105.76(11) . . ?
Ag1B Ag0F Ag0O 99.58(4) 2 . ?
Ag1B Ag0F Ag0O 67.35(12) . . ?
Ag1B Ag0F Ag1B 47.38(18) 2 . ?
Ag1A Ag0F Ag06 118.16(4) . 2 ?
Ag1A Ag0F Ag0K 116.68(11) . 2 ?
Ag1A Ag0F Ag0O 53.83(11) . . ?
Ag0F Ag0G Ag07 55.81(2) . . ?
Ag0O Ag0G Ag07 56.50(2) . . ?
Ag0O Ag0G Ag0F 65.61(2) . . ?
S00W Ag0G Ag07 91.16(6) . . ?
S00W Ag0G Ag0F 146.69(6) . . ?
S00W Ag0G Ag0O 93.95(6) . . ?
S00W Ag0G S00X 154.95(8) . . ?
S00X Ag0G Ag07 111.91(5) . . ?
S00X Ag0G Ag0F 57.79(5) . . ?
S00X Ag0G Ag0O 106.68(6) . . ?
Ag09 Ag0H Ag06 54.65(2) . . ?
Ag09 Ag0H Ag0L 71.93(3) . . ?
Ag0L Ag0H Ag06 82.35(2) . . ?
S013 Ag0H Ag06 144.44(6) . . ?
S013 Ag0H Ag09 95.52(6) . . ?
S013 Ag0H Ag0L 68.79(5) . . ?
S014 Ag0H Ag06 54.52(5) . . ?
S014 Ag0H Ag09 95.10(6) . . ?
S014 Ag0H Ag0L 131.75(6) . . ?
S014 Ag0H S013 159.18(8) . . ?
Ag01 Ag0I Ag02 56.693(19) . 2 ?
Ag01 Ag0I Ag04 56.335(19) . . ?
Ag01 Ag0I Ag05 60.51(2) . . ?
Ag01 Ag0I Ag07 111.08(3) . . ?
Ag01 Ag0I Ag08 60.97(2) . 2 ?
Ag01 Ag0I Ag0B 87.27(2) . 2 ?
Ag01 Ag0I Ag0D 108.95(3) . . ?
Ag01 Ag0I Ag0M 154.39(4) . . ?
Ag02 Ag0I Ag04 110.36(2) 2 . ?
Ag02 Ag0I Ag08 81.00(2) 2 2 ?
Ag04 Ag0I Ag08 51.566(19) . 2 ?
Ag05 Ag0I Ag02 102.40(3) . 2 ?
Ag05 Ag0I Ag04 57.423(19) . . ?
Ag05 Ag0I Ag08 104.20(3) . 2 ?
Ag05 Ag0I Ag0B 147.61(3) . 2 ?
Ag05 Ag0I Ag0D 66.53(2) . . ?
Ag05 Ag0I Ag0M 100.17(3) . . ?
Ag07 Ag0I Ag02 56.086(19) . 2 ?
Ag07 Ag0I Ag04 166.35(3) . . ?
Ag07 Ag0I Ag05 123.48(3) . . ?
Ag07 Ag0I Ag08 119.57(3) . 2 ?
Ag07 Ag0I Ag0B 62.51(2) . 2 ?
Ag07 Ag0I Ag0D 137.28(3) . . ?
Ag07 Ag0I Ag0M 63.64(2) . . ?
Ag0B Ag0I Ag02 51.753(18) 2 2 ?
Ag0B Ag0I Ag04 108.91(3) 2 . ?
Ag0B Ag0I Ag08 57.49(2) 2 2 ?
Ag0D Ag0I Ag02 165.62(3) . 2 ?
Ag0D Ag0I Ag04 56.36(2) . . ?
Ag0D Ag0I Ag08 92.60(3) . 2 ?
Ag0D Ag0I Ag0B 134.14(3) . 2 ?
Ag0M Ag0I Ag02 118.48(3) . 2 ?
Ag0M Ag0I Ag04 129.92(3) . . ?
Ag0M Ag0I Ag08 144.46(3) . 2 ?
Ag0M Ag0I Ag0B 109.32(3) . 2 ?
Ag0M Ag0I Ag0D 73.84(2) . . ?
Ag0O Ag0I Ag01 68.34(3) . . ?
Ag0O Ag0I Ag02 55.36(2) . 2 ?
Ag0O Ag0I Ag04 111.95(3) . . ?
Ag0O Ag0I Ag05 62.64(2) . . ?
Ag0O Ag0I Ag07 63.10(3) . . ?
Ag0O Ag0I Ag08 125.96(3) . 2 ?
Ag0O Ag0I Ag0B 104.39(3) . 2 ?
Ag0O Ag0I Ag0D 121.46(3) . . ?
Ag0O Ag0I Ag0M 88.24(3) . . ?
S015 Ag0I Ag01 109.68(7) 2 . ?
S015 Ag0I Ag02 102.91(7) 2 2 ?
S015 Ag0I Ag04 83.04(7) 2 . ?
S015 Ag0I Ag05 138.51(7) 2 . ?
S015 Ag0I Ag07 97.94(7) 2 . ?
S015 Ag0I Ag08 49.03(7) 2 2 ?
S015 Ag0I Ag0B 52.23(6) 2 2 ?
S015 Ag0I Ag0D 81.98(7) 2 . ?
S015 Ag0I Ag0M 95.94(7) 2 . ?
S015 Ag0I Ag0O 156.29(7) 2 . ?
Ag04 Ag0J Ag0A 113.33(2) 2 . ?
Ag04 Ag0J Ag0J 90.24(3) 2 2 ?
Ag08 Ag0J Ag04 57.90(2) . 2 ?
Ag08 Ag0J Ag0A 55.436(18) . . ?
Ag08 Ag0J Ag0J 81.19(2) . 2 ?
Ag0J Ag0J Ag0A 80.07(3) 2 . ?
S00V Ag0J Ag04 150.20(6) . 2 ?
S00V Ag0J Ag08 97.85(5) . . ?
S00V Ag0J Ag0A 45.87(5) . . ?
S00V Ag0J Ag0J 67.35(5) . 2 ?
S00V Ag0J S011 152.64(8) . 2 ?
S011 Ag0J Ag04 56.04(5) 2 2 ?
S011 Ag0J Ag08 98.12(5) 2 . ?
S011 Ag0J Ag0A 134.24(6) 2 . ?
S011 Ag0J Ag0J 137.29(6) 2 2 ?
Ag06 Ag0K Ag0F 59.05(2) . 2 ?
Ag06 Ag0K Ag1B 71.73(6) . . ?
Ag06 Ag0K Ag1A 66.52(5) . . ?
S010 Ag0K Ag06 146.62(6) . . ?
S010 Ag0K Ag0F 87.66(6) . 2 ?
S010 Ag0K S014 153.95(8) . . ?
S010 Ag0K Ag1B 86.87(11) . . ?
S010 Ag0K Ag1A 97.49(11) . . ?
S014 Ag0K Ag06 57.92(5) . . ?
S014 Ag0K Ag0F 114.87(6) . 2 ?
S014 Ag0K Ag1B 116.66(11) . . ?
S014 Ag0K Ag1A 104.35(11) . . ?
Ag1A Ag0K Ag0F 62.61(9) . 2 ?
Ag03 Ag0L Ag0H 98.91(3) . . ?
Ag0B Ag0L Ag03 61.43(2) . . ?
Ag0B Ag0L Ag0H 92.78(3) . . ?
S00T Ag0L Ag03 58.06(5) . . ?
S00T Ag0L Ag0B 98.29(5) . . ?
S00T Ag0L Ag0H 143.54(5) . . ?
S012 Ag0L Ag03 155.73(6) . . ?
S012 Ag0L Ag0B 97.96(5) . . ?
S012 Ag0L Ag0H 67.60(6) . . ?
S012 Ag0L S00T 143.38(8) . . ?
Ag07 Ag0M Ag0N 92.04(3) . . ?
Ag0I Ag0M Ag07 57.87(2) . . ?
Ag0I Ag0M Ag0N 77.45(3) . . ?
S00U Ag0M Ag07 150.30(6) . . ?
S00U Ag0M Ag0I 94.79(6) . . ?
S00U Ag0M Ag0N 68.86(5) . . ?
S00U Ag0M S00Y 149.77(8) . . ?
S00Y Ag0M Ag07 56.12(5) . . ?
S00Y Ag0M Ag0I 99.95(6) . . ?
S00Y Ag0M Ag0N 140.14(6) . . ?
Ag05 Ag0N Ag0M 93.60(3) . . ?
Ag0O Ag0N Ag05 60.35(2) . . ?
Ag0O Ag0N Ag0M 82.00(3) . . ?
S00W Ag0N Ag05 150.43(6) . . ?
S00W Ag0N Ag0M 65.82(6) . . ?
S00W Ag0N Ag0O 94.47(6) . . ?
S00W Ag0N S00Z 150.53(8) . . ?
S00Z Ag0N Ag05 57.36(5) . . ?
S00Z Ag0N Ag0M 140.30(6) . . ?
S00Z Ag0N Ag0O 101.89(6) . . ?
Ag01 Ag0O Ag0F 111.83(3) . . ?
Ag01 Ag0O Ag1B 84.22(4) . . ?
Ag02 Ag0O Ag01 57.293(19) 2 . ?
Ag02 Ag0O Ag05 110.61(3) 2 . ?
Ag02 Ag0O Ag07 59.44(2) 2 . ?
Ag02 Ag0O Ag0F 56.159(19) 2 . ?
Ag02 Ag0O Ag0G 109.47(3) 2 . ?
Ag02 Ag0O Ag0N 149.71(4) 2 . ?
Ag02 Ag0O Ag1B 59.73(6) 2 . ?
Ag02 Ag0O Ag1A 66.38(7) 2 . ?
Ag05 Ag0O Ag01 55.870(18) . . ?
Ag05 Ag0O Ag07 117.45(4) . . ?
Ag05 Ag0O Ag0F 166.68(3) . . ?
Ag05 Ag0O Ag0G 133.75(3) . . ?
Ag05 Ag0O Ag1B 126.54(7) . . ?
Ag07 Ag0O Ag01 99.84(2) . . ?
Ag07 Ag0O Ag0F 56.39(2) . . ?
Ag07 Ag0O Ag0G 66.74(3) . . ?
Ag07 Ag0O Ag1B 101.86(8) . . ?
Ag0F Ag0O Ag1B 50.74(7) . . ?
Ag0G Ag0O Ag01 165.69(3) . . ?
Ag0G Ag0O Ag0F 57.23(2) . . ?
Ag0G Ag0O Ag1B 93.49(4) . . ?
Ag0I Ag0O Ag01 55.99(2) . . ?
Ag0I Ag0O Ag02 69.52(2) . 2 ?
Ag0I Ag0O Ag05 59.87(2) . . ?
Ag0I Ag0O Ag07 59.57(3) . . ?
Ag0I Ag0O Ag0F 110.07(3) . . ?
Ag0I Ag0O Ag0G 116.51(4) . . ?
Ag0I Ag0O Ag0N 82.10(3) . . ?
Ag0I Ag0O Ag1B 127.40(5) . . ?
Ag0I Ag0O Ag1A 131.02(5) . . ?
Ag0N Ag0O Ag01 114.72(3) . . ?
Ag0N Ag0O Ag05 60.25(2) . . ?
Ag0N Ag0O Ag07 97.43(4) . . ?
Ag0N Ag0O Ag0F 129.77(3) . . ?
Ag0N Ag0O Ag0G 73.50(3) . . ?
Ag0N Ag0O Ag1B 150.17(6) . . ?
S0 Ag0O Ag01 98.74(11) . . ?
S0 Ag0O Ag05 98.12(16) . . ?
S0 Ag0O Ag07 144.39(16) . . ?
S0 Ag0O Ag0F 88.48(17) . . ?
S0 Ag0O Ag0G 90.53(11) . . ?
S0 Ag0O Ag0I 152.43(11) . . ?
S0 Ag0O Ag0N 101.97(18) . . ?
S0 Ag0O Ag1B 50.4(2) . . ?
S1 Ag0O Ag01 97.74(12) . . ?
S1 Ag0O Ag02 122.55(16) . 2 ?
S1 Ag0O Ag05 82.87(18) . . ?
S1 Ag0O Ag07 158.46(16) . . ?
S1 Ag0O Ag0F 105.23(19) . . ?
S1 Ag0O Ag0G 94.41(12) . . ?
S1 Ag0O Ag0I 141.87(17) . . ?
S1 Ag0O Ag0N 86.37(17) . . ?
S1 Ag0O Ag1A 58.99(19) . . ?
Ag1A Ag0O Ag01 82.31(4) . . ?
Ag1A Ag0O Ag05 118.99(9) . . ?
Ag1A Ag0O Ag07 111.28(10) . . ?
Ag1A Ag0O Ag0F 59.55(9) . . ?
Ag1A Ag0O Ag0G 97.63(6) . . ?
Ag1A Ag0O Ag0N 143.90(8) . . ?
Ag0F AgB AgB 87.46(5) . 2 ?
S00X AgB Ag0F 53.62(6) . . ?
S00X AgB AgB 133.27(10) . 2 ?
S00X AgB Ag1B 96.11(9) . . ?
S010 AgB Ag0F 140.41(9) . . ?
S010 AgB AgB 65.65(7) . 2 ?
S010 AgB S00X 161.06(11) . . ?
S010 AgB Ag1B 89.85(8) . . ?
Ag1B AgB Ag0F 54.01(4) . . ?
Ag06 Cl00 Ag07 62.09(4) 2 . ?
Ag0F Cl00 Ag06 66.52(5) . 2 ?
Ag0F Cl00 Ag07 62.29(5) . . ?
Ag03 Cl1 Ag04 63.14(4) . . ?
Ag03 Cl1 Ag05 63.14(4) . . ?
Ag04 Cl1 Ag05 62.75(4) . . ?
Ag0A S00T Ag03 68.97(5) . . ?
Ag0A S00T Ag0L 127.84(8) . . ?
Ag0L S00T Ag03 68.26(5) . . ?
C01C S00T Ag03 102.1(3) . . ?
C01C S00T Ag0A 104.7(3) . . ?
C01C S00T Ag0L 112.2(3) . . ?
Ag0D S00U Ag0M 92.13(7) . . ?
C01H S00U Ag0D 103.2(3) . . ?
C01H S00U Ag0M 105.8(3) . . ?
Ag0A S00V Ag0J 87.29(7) . . ?
C035 S00V Ag0A 102.9(4) . . ?
C035 S00V Ag0J 105.6(3) . . ?
Ag0G S00W Ag0N 92.16(8) . . ?
C02A S00W Ag0G 105.7(3) . . ?
C02A S00W Ag0N 107.2(3) . . ?
Ag0G S00X Ag0F 70.59(6) . . ?
Ag0G S00X AgA 121.30(9) . . ?
AgB S00X Ag0F 79.00(8) . . ?
AgB S00X Ag0G 133.46(10) . . ?
C01S S00X Ag0F 101.5(3) . . ?
C01S S00X Ag0G 107.8(3) . . ?
C01S S00X AgB 112.2(3) . . ?
C01S S00X AgA 113.7(3) . . ?
AgA S00X Ag0F 62.13(7) . . ?
Ag0E S00Y Ag07 70.53(6) 2 . ?
Ag0M S00Y Ag07 72.80(6) . . ?
Ag0M S00Y Ag0E 129.16(9) . 2 ?
C028 S00Y Ag07 99.2(3) . . ?
C028 S00Y Ag0E 108.3(3) . 2 ?
C028 S00Y Ag0M 111.3(3) . . ?
Ag0C S00Z Ag05 69.10(6) . . ?
Ag0N S00Z Ag05 69.95(6) . . ?
Ag0N S00Z Ag0C 127.01(8) . . ?
C01F S00Z Ag05 102.3(3) . . ?
C01F S00Z Ag0C 108.9(3) . . ?
C01F S00Z Ag0N 111.5(3) . . ?
Ag0K S010 AgA 94.69(8) . 2 ?
Ag0K S010 AgA 88.74(8) . . ?
AgB S010 Ag0K 95.81(9) . . ?
C134 S010 Ag0K 111.9(5) . . ?
C134 S010 AgB 81.0(6) . . ?
C134 S010 AgA 97.4(6) . . ?
C134 S010 AgA 139.2(5) . 2 ?
AgA S010 AgA 51.23(9) . 2 ?
Ag0D S011 Ag04 70.58(6) . . ?
Ag0J S011 Ag04 72.96(6) 2 . ?
Ag0J S011 Ag0D 130.07(9) 2 . ?
C01Q S011 Ag04 102.5(3) . . ?
C01Q S011 Ag0D 109.7(3) . . ?
C01Q S011 Ag0J 110.6(3) . 2 ?
Ag0E S012 Ag0L 90.95(7) . . ?
C026 S012 Ag0E 104.9(3) . . ?
C026 S012 Ag0L 106.9(3) . . ?
Ag0C S013 Ag0H 90.22(7) . . ?
C02J S013 Ag0C 100.4(3) . . ?
C02J S013 Ag0H 106.0(3) . . ?
Ag0H S014 Ag06 77.18(6) . . ?
Ag0H S014 Ag0K 131.37(9) . . ?
Ag0K S014 Ag06 69.65(6) . . ?
C01J S014 Ag06 101.0(3) . . ?
C01J S014 Ag0H 112.1(3) . . ?
C01J S014 Ag0K 108.4(3) . . ?
Ag08 S015 Ag0B 74.93(7) . . ?
Ag08 S015 Ag0I 80.49(8) . 2 ?
Ag0B S015 Ag0I 74.78(7) . 2 ?
C02P S015 Ag08 126.6(5) . . ?
C02P S015 Ag0B 109.8(5) . . ?
C02P S015 Ag0I 152.9(5) . 2 ?
Ag09 S0 Ag0O 77.26(17) . . ?
Ag09 S0 Ag1B 87.28(17) . . ?
C12 S0 Ag09 128.0(4) . . ?
C12 S0 Ag0O 126.5(8) . . ?
C12 S0 Ag1B 138.8(7) . . ?
Ag1B S0 Ag0O 76.20(13) . . ?
C01C C018 C01O 107.1(7) . . ?
C01X C018 C01C 110.5(7) . . ?
C01X C018 C01O 108.5(8) . . ?
C01B C019 C01M 108.8(8) . . ?
C01G C01A C02Z 108.7(8) . . ?
C028 C01A C01G 110.2(7) . . ?
C028 C01A C02Z 105.4(8) . . ?
C019 C01B C01F 112.2(8) . . ?
C019 C01B C027 108.9(7) . . ?
C01F C01B C027 107.2(8) . . ?
C018 C01C S00T 111.2(5) . . ?
C01D C01C S00T 110.9(6) . . ?
C01D C01C C018 109.5(7) . . ?
C01C C01D C03O 106.9(8) . . ?
C02I C01D C01C 111.8(7) . . ?
C02I C01D C03O 109.4(8) . . ?
C01K C01E C01M 111.2(9) . . ?
C01B C01F S00Z 111.2(6) . . ?
C01K C01F S00Z 110.5(6) . . ?
C01K C01F C01B 109.8(7) . . ?
C01L C01G C01A 110.1(8) . . ?
C01T C01H S00U 113.1(7) . . ?
C01T C01H C02S 110.1(7) . . ?
C02S C01H S00U 108.9(6) . . ?
C01V C01I C02X 110.6(8) . . ?
C01P C01J S014 110.3(7) . . ?
C02B C01J S014 111.5(7) . . ?
C02B C01J C01P 110.2(7) . . ?
C01E C01K C01F 112.3(8) . . ?
C01E C01K C02H 109.1(8) . . ?
C01F C01K C02H 105.7(8) . . ?
C01G C01L C020 107.5(8) . . ?
C01G C01L C02F 110.6(9) . . ?
C020 C01L C02F 110.6(8) . . ?
C01E C01M C019 108.3(7) . . ?
C02L C01M C019 109.2(9) . . ?
C02L C01M C01E 110.1(9) . . ?
C01Y C01N C024 109.7(9) . . ?
C01Y C01N C026 111.5(9) . . ?
C026 C01N C024 108.8(9) . . ?
C03U C01O C018 109.5(8) . . ?
C01J C01P C04N 105.3(9) . . ?
C03D C01P C01J 112.2(9) . . ?
C03D C01P C04N 108.7(10) . . ?
C01V C01Q S011 110.7(6) . . ?
C02U C01Q S011 110.7(6) . . ?
C02U C01Q C01V 110.0(7) . . ?
C03I C01R C01U 111.0(9) . . ?
C01U C01S S00X 111.6(6) . . ?
C01U C01S C022 110.4(8) . . ?
C022 C01S S00X 110.9(7) . . ?
C01H C01T C021 107.7(9) . . ?
C02E C01T C01H 111.2(8) . . ?
C02E C01T C021 109.9(9) . . ?
C01R C01U C02V 108.8(9) . . ?
C01S C01U C01R 107.5(8) . . ?
C01S C01U C02V 110.1(8) . . ?
C01I C01V C01Q 112.3(8) . . ?
C01I C01V C01W 107.9(7) . . ?
C01Q C01V C01W 106.1(7) . . ?
C048 C01W C01V 110.5(8) . . ?
C033 C01X C018 111.5(8) . . ?
C01N C01Y C02C 111.6(9) . . ?
C027 C01Z C02H 110.4(8) . . ?
C027 C01Z C02L 110.4(8) . . ?
C02L C01Z C02H 109.4(9) . . ?
C038 C020 C01L 110.2(7) . . ?
C03Q C021 C01T 109.5(9) . . ?
C01S C022 C03S 106.3(8) . . ?
C025 C022 C01S 110.8(8) . . ?
C025 C022 C03S 108.2(9) . . ?
C02A C023 C02G 107.9(8) . . ?
C02A C023 C03F 111.0(9) . . ?
C03F C023 C02G 111.7(9) . . ?
C01N C024 C02M 108.3(9) . . ?
C022 C025 C03T 111.2(10) . . ?
C01N C026 S012 113.2(7) . . ?
C01N C026 C02Q 107.9(8) . . ?
C02Q C026 S012 110.8(7) . . ?
C01Z C027 C01B 109.1(9) . . ?
C01A C028 S00Y 111.1(7) . . ?
C01A C028 C038 110.6(7) . . ?
C038 C028 S00Y 110.6(6) . . ?
C02P C029 C04G 105.0(11) . . ?
C041 C029 C02P 112.2(13) . . ?
C041 C029 C04G 105.6(12) . . ?
C023 C02A S00W 114.2(7) . . ?
C023 C02A C044 107.4(8) . . ?
C044 C02A S00W 110.1(7) . . ?
C01J C02B C02N 108.5(9) . . ?
C01J C02B C039 111.3(9) . . ?
C02N C02B C039 107.4(9) . . ?
C030 C02C C01Y 109.6(10) . . ?
C03B C02C C01Y 107.8(9) . . ?
C03B C02C C030 109.5(10) . . ?
C03R C02E C01T 110.5(10) . . ?
C02Y C02F C01L 109.3(8) . . ?
C03Z C02G C023 106.8(9) . . ?
C01Z C02H C01K 108.6(8) . . ?
C01D C02I C033 109.2(8) . . ?
C032 C02J S013 110.6(6) . . ?
C03M C02J S013 112.9(7) . . ?
C03M C02J C032 111.9(8) . . ?
C02S C02K C03R 111.1(8) . . ?
C01M C02L C01Z 109.3(8) . . ?
C030 C02M C024 109.9(10) . . ?
C030 C02M C03Y 108.8(11) . . ?
C03Y C02M C024 107.6(9) . . ?
C040 C02N C02B 110.6(10) . . ?
C029 C02P S015 112.3(10) . . ?
C029 C02P C037 109.9(11) . . ?
C037 C02P S015 114.8(10) . . ?
C03B C02Q C026 109.8(9) . . ?
C03Y C02Q C026 106.7(10) . . ?
C03Y C02Q C03B 110.4(10) . . ?
C02U C02R C02X 109.6(8) . . ?
C01H C02S C04W 108.2(8) . . ?
C02K C02S C01H 110.6(8) . . ?
C02K C02S C04W 108.0(9) . . ?
C03Q C02T C03R 110.0(9) . . ?
C02R C02U C01Q 112.3(7) . . ?
C02R C02U C03G 108.4(8) . . ?
C03G C02U C01Q 106.1(8) . . ?
C03T C02V C01U 111.0(9) . . ?
C031 C02W C034 109.4(9) . . ?
C035 C02W C031 108.5(9) . . ?
C035 C02W C034 107.3(9) . . ?
C01I C02X C02R 109.3(7) . . ?
C01I C02X C03J 108.8(8) . . ?
C03J C02X C02R 108.5(8) . . ?
C02Z C02Y C02F 109.3(9) . . ?
C036 C02Y C02F 110.7(8) . . ?
C036 C02Y C02Z 108.9(8) . . ?
C02Y C02Z C01A 111.1(8) . . ?
C02M C030 C02C 110.7(9) . . ?
C042 C031 C02W 111.7(10) . . ?
C02J C032 C03V 108.8(9) . . ?
C03A C032 C02J 107.3(8) . . ?
C03A C032 C03V 108.2(9) . . ?
C01X C033 C02I 109.0(8) . . ?
C01X C033 C04S 109.6(9) . . ?
C04S C033 C02I 109.5(10) . . ?
C045 C034 C02W 110.2(9) . . ?
C02W C035 S00V 113.4(8) . . ?
C02W C035 C03W 110.9(9) . . ?
C03W C035 S00V 109.7(7) . . ?
C02Y C036 C038 110.1(8) . . ?
C04Y C037 C02P 109.2(12) . . ?
C04Z C037 C02P 106.3(12) . . ?
C04Z C037 C04Y 113.9(13) . . ?
C020 C038 C028 111.1(7) . . ?
C020 C038 C036 109.0(8) . . ?
C036 C038 C028 106.8(7) . . ?
C03L C039 C02B 110.9(10) . . ?
C04F C03A C032 111.9(10) . . ?
C02C C03B C02Q 109.4(9) . . ?
C04R C03C C04L 113.6(12) . . ?
C01P C03D C03L 113.1(10) . . ?
C042 C03E C03W 113.0(10) . . ?
C043 C03F C023 108.6(9) . . ?
C048 C03G C02U 112.7(8) . . ?
C03I C03H C03T 111.9(10) . . ?
C03H C03I C01R 108.8(11) . . ?
C03S C03I C01R 108.8(9) . . ?
C03S C03I C03H 109.3(11) . . ?
C048 C03J C02X 112.1(8) . . ?
C043 C03K C044 109.1(9) . . ?
C039 C03L C03D 107.5(9) . . ?
C039 C03L C04A 108.5(11) . . ?
C03D C03L C04A 106.6(12) . . ?
C02J C03M C03N 111.0(9) . . ?
C02J C03M C046 107.1(9) . . ?
C03N C03M C046 106.7(9) . . ?
C047 C03N C03M 111.1(10) . . ?
C03U C03O C01D 109.9(8) . . ?
C04I C03P C134 107.6(15) . . ?
C162 C03P C04I 106.6(15) . . ?
C162 C03P C134 106.8(15) . . ?
C021 C03Q C02T 110.6(12) . . ?
C021 C03Q C04W 109.2(9) . . ?
C02T C03Q C04W 107.0(10) . . ?
C02E C03R C02K 109.8(9) . . ?
C02E C03R C02T 108.6(10) . . ?
C02K C03R C02T 107.8(11) . . ?
C03I C03S C022 112.2(10) . . ?
C025 C03T C03H 106.5(11) . . ?
C02V C03T C025 107.9(9) . . ?
C02V C03T C03H 109.6(11) . . ?
C01O C03U C03O 110.6(9) . . ?
C01O C03U C04S 109.0(9) . . ?
C03O C03U C04S 109.7(10) . . ?
C047 C03V C032 110.9(9) . . ?
C03E C03W C035 108.9(9) . . ?
C03E C03W C04C 109.3(9) . . ?
C04C C03W C035 108.6(9) . . ?
C044 C03X C03Z 107.6(9) . . ?
C02Q C03Y C02M 112.2(10) . . ?
C02G C03Z C03X 108.1(9) . . ?
C04E C03Z C02G 112.7(11) . . ?
C04E C03Z C03X 110.6(11) . . ?
C02N C040 C04A 109.1(11) . . ?
C02N C040 C04N 110.4(9) . . ?
C04A C040 C04N 106.3(12) . . ?
C029 C041 C04L 115.0(12) . . ?
C031 C042 C04H 110.3(10) . . ?
C03E C042 C031 108.5(9) . . ?
C03E C042 C04H 105.5(10) . . ?
C03F C043 C04E 109.8(10) . . ?
C03K C043 C03F 110.0(9) . . ?
C03K C043 C04E 110.7(10) . . ?
C02A C044 C03X 108.3(9) . . ?
C03K C044 C02A 111.7(8) . . ?
C03K C044 C03X 109.6(9) . . ?
C04C C045 C034 107.8(9) . . ?
C04H C045 C034 110.7(10) . . ?
C04H C045 C04C 108.7(10) . . ?
C04F C046 C03M 110.8(9) . . ?
C03N C047 C03V 110.0(9) . . ?
C03N C047 C0AA 110.1(11) . . ?
C03V C047 C0AA 106.4(11) . . ?
C03G C048 C01W 108.8(8) . . ?
C03J C048 C01W 108.0(8) . . ?
C03J C048 C03G 108.2(9) . . ?
C040 C04A C03L 112.5(10) . . ?
C03W C04C C045 109.5(10) . . ?
C03Z C04E C043 108.6(9) . . ?
C03A C04F C046 109.9(9) . . ?
C03A C04F C0AA 107.4(10) . . ?
C046 C04F C0AA 109.1(12) . . ?
C04R C04G C029 113.4(12) . . ?
C045 C04H C042 111.3(9) . . ?
C04K C04I C03P 115.0(16) . . ?
C04I C04K C04T 104.4(15) . . ?
C04I C04K C80 101.6(14) . . ?
C04T C04K C80 113.4(15) . . ?
C03C C04L C041 105.9(12) . . ?
C04Y C04L C03C 107.7(12) . . ?
C04Y C04L C041 107.4(12) . . ?
C040 C04N C01P 110.8(10) . . ?
C03C C04R C04G 108.8(12) . . ?
C03C C04R C04Z 109.7(13) . . ?
C04G C04R C04Z 105.2(12) . . ?
C033 C04S C03U 109.0(8) . . ?
C51 C04T C04K 113.1(15) . . ?
C02S C04W C03Q 110.4(9) . . ?
C04L C04Y C037 110.3(12) . . ?
C037 C04Z C04R 110.4(12) . . ?
C11 C5 C12 105.6(14) . . ?
C14 C5 C11 99.9(14) . . ?
C14 C5 C12 113.4(15) . . ?
C16 C7 C21 113.4(16) . . ?
C16 C11 C5 116.0(16) . . ?
C5 C12 S0 126.9(11) . . ?
C5 C12 S1 108.8(10) . . ?
C19 C12 S0 114.4(10) . . ?
C19 C12 C5 118.1(15) . . ?
C19 C12 S1 122.4(12) . . ?
C5 C14 C21 111.2(15) . . ?
C21 C15 C19 121.6(16) . . ?
C7 C16 C11 102.7(14) . . ?
C7 C16 C17 108.3(15) . . ?
C17 C16 C11 107.5(15) . . ?
C19 C17 C16 119.3(16) . . ?
C12 C19 C15 93.3(14) . . ?
C17 C19 C12 108.3(16) . . ?
C17 C19 C15 105.9(15) . . ?
C7 C21 C14 98.8(14) . . ?
C15 C21 C7 112.9(15) . . ?
C15 C21 C14 105.9(15) . . ?
C04T C51 C57 105.2(15) . . ?
C134 C51 C04T 105.8(15) . . ?
C134 C51 C57 111.0(15) . . ?
C20 C80 C04K 115.4(15) . . ?
C03P C162 C20 116.3(16) . . ?
C80 C20 C162 103.1(15) . . ?
C80 C20 C57 104.0(15) . . ?
C57 C20 C162 108.8(15) . . ?
C20 C57 C51 115.7(15) . . ?
C03P C134 S010 111.2(12) . . ?
C51 C134 S010 107.7(12) . . ?
C51 C134 C03P 113.2(16) . . ?
C04F C0AA C047 111.5(10) . . ?
Ag0F AgA S010 87.68(7) . 2 ?
Ag0F AgA Ag1A 66.10(5) . . ?
S00X AgA Ag0F 60.15(6) . . ?
S00X AgA S010 130.33(10) . . ?
S00X AgA S010 99.40(9) . 2 ?
S00X AgA Ag1A 97.61(11) . . ?
S010 AgA Ag0F 165.20(10) . . ?
S010 AgA S010 99.42(9) . 2 ?
S010 AgA Ag1A 100.24(8) . . ?
AgA AgA Ag0F 102.29(7) 2 . ?
AgA AgA S00X 153.07(12) 2 . ?
AgA AgA S010 71.51(9) 2 . ?
AgA AgA S010 57.26(8) 2 2 ?
AgA AgA Ag1A 92.35(10) 2 . ?
Ag1A AgA S010 135.39(11) . 2 ?
Ag09 S1 Ag1A 73.03(16) . . ?
Ag0O S1 Ag09 86.75(15) . . ?
Ag0O S1 Ag1A 67.41(14) . . ?
C12 S1 Ag09 131.4(6) . . ?
C12 S1 Ag0O 138.9(5) . . ?
C12 S1 Ag1A 105.3(7) . . ?
Ag02 Ag1B Ag02 58.07(4) . 2 ?
Ag02 Ag1B Ag0F 114.55(5) . . ?
Ag02 Ag1B Ag0K 104.85(6) . . ?
Ag02 Ag1B Ag0O 51.08(5) 2 . ?
Ag02 Ag1B Ag0O 85.55(10) . . ?
Ag02 Ag1B AgB 164.6(2) . . ?
Ag0F Ag1B Ag02 61.61(4) 2 . ?
Ag0F Ag1B Ag02 57.32(3) . 2 ?
Ag0F Ag1B Ag02 106.39(8) 2 2 ?
Ag0F Ag1B Ag0F 131.4(2) 2 . ?
Ag0F Ag1B Ag0K 66.60(5) 2 . ?
Ag0F Ag1B Ag0K 140.54(7) . . ?
Ag0F Ag1B Ag0O 61.91(6) . . ?
Ag0F Ag1B Ag0O 147.12(9) 2 . ?
Ag0F Ag1B AgB 104.51(15) 2 . ?
Ag0F Ag1B AgB 68.60(7) . . ?
Ag0K Ag1B Ag02 161.43(13) . 2 ?
Ag0K Ag1B Ag0O 125.83(18) . . ?
AgB Ag1B Ag0K 72.84(5) . . ?
AgB Ag1B Ag0O 108.30(8) . . ?
S0 Ag1B Ag02 103.1(2) . . ?
S0 Ag1B Ag0F 99.61(18) . . ?
S0 Ag1B Ag0K 72.6(2) . . ?
S0 Ag1B Ag0O 53.4(2) . . ?
S0 Ag1B AgB 90.85(15) . . ?
Ag1B Ag1B Ag02 75.24(14) 2 . ?
Ag1B Ag1B Ag0F 65.44(8) 2 . ?
Ag1B Ag1B Ag0K 126.13(17) 2 . ?
Ag1B Ag1B Ag0O 108.00(7) 2 . ?
Ag1B Ag1B AgB 93.67(9) 2 . ?
Ag1B Ag1B S0 161.3(2) 2 . ?
Ag02 Ag1A Ag02 58.57(3) . 2 ?
Ag02 Ag1A Ag06 56.12(3) . . ?
Ag02 Ag1A Ag06 113.72(5) 2 . ?
Ag02 Ag1A Ag09 66.13(7) . . ?
Ag02 Ag1A Ag0F 95.97(11) 2 2 ?
Ag02 Ag1A Ag0F 55.63(7) . 2 ?
Ag02 Ag1A Ag0F 109.10(9) . . ?
Ag02 Ag1A Ag0K 156.03(18) 2 . ?
Ag02 Ag1A Ag0K 103.17(8) . . ?
Ag02 Ag1A Ag0O 97.16(10) . . ?
Ag02 Ag1A AgA 128.8(2) . . ?
Ag02 Ag1A Ag1A 50.16(9) 2 2 ?
Ag02 Ag1A Ag1A 58.53(14) . 2 ?
Ag06 Ag1A Ag1A 100.74(14) . 2 ?
Ag09 Ag1A Ag02 91.78(10) . 2 ?
Ag09 Ag1A Ag06 52.70(5) . . ?
Ag09 Ag1A Ag0F 103.33(4) . 2 ?
Ag09 Ag1A Ag0K 94.22(8) . . ?
Ag09 Ag1A Ag1A 123.42(7) . 2 ?
Ag0F Ag1A Ag02 55.79(3) . 2 ?
Ag0F Ag1A Ag06 161.42(17) . . ?
Ag0F Ag1A Ag06 54.79(5) 2 . ?
Ag0F Ag1A Ag09 135.95(15) . . ?
Ag0F Ag1A Ag0F 108.52(18) . 2 ?
Ag0F Ag1A Ag0K 127.90(16) . . ?
Ag0F Ag1A Ag1A 60.67(6) . 2 ?
Ag0F Ag1A Ag1A 53.58(10) 2 2 ?
Ag0K Ag1A Ag06 54.48(3) . . ?
Ag0K Ag1A Ag0F 60.07(8) . 2 ?
Ag0K Ag1A Ag1A 108.25(15) . 2 ?
Ag0O Ag1A Ag02 56.37(5) . 2 ?
Ag0O Ag1A Ag06 122.80(17) . . ?
Ag0O Ag1A Ag09 70.59(14) . . ?
Ag0O Ag1A Ag0F 66.62(5) . . ?
Ag0O Ag1A Ag0F 150.45(6) . 2 ?
Ag0O Ag1A Ag0K 147.02(18) . . ?
Ag0O Ag1A Ag1A 104.48(7) . 2 ?
AgA Ag1A Ag02 105.54(12) . 2 ?
AgA Ag1A Ag06 122.59(14) . . ?
AgA Ag1A Ag09 161.45(10) . . ?
AgA Ag1A Ag0F 81.77(16) . 2 ?
AgA Ag1A Ag0F 55.26(8) . . ?
AgA Ag1A Ag0K 72.65(10) . . ?
AgA Ag1A Ag0O 113.46(6) . . ?
AgA Ag1A Ag1A 74.09(7) . 2 ?
S1 Ag1A Ag02 107.9(2) . 2 ?
S1 Ag1A Ag02 116.0(2) . . ?
S1 Ag1A Ag06 90.85(16) . . ?
S1 Ag1A Ag09 51.20(16) . . ?
S1 Ag1A Ag0F 144.36(14) . 2 ?
S1 Ag1A Ag0F 106.76(15) . . ?
S1 Ag1A Ag0K 93.86(16) . . ?
S1 Ag1A Ag0O 53.61(17) . . ?
S1 Ag1A AgA 115.28(15) . . ?
S1 Ag1A Ag1A 157.84(16) . 2 ?

_platon_squeeze_details          ?
loop_
_platon_squeeze_void_nr
_platon_squeeze_void_average_x
_platon_squeeze_void_average_y
_platon_squeeze_void_average_z
_platon_squeeze_void_volume
_platon_squeeze_void_count_electrons
_platon_squeeze_void_content
1 0.101 -0.061 0.000 7987 1553 ' '
2 0.325 -0.032 0.500 7971 1553 ' '

_platon_squeeze_void_probe_radius 1.20
_olex2_submission_special_instructions 'No special instructions were received'
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_1_sq_CCDC1
_database_code_depnum_ccdc_archive 'CCDC 2094271'
loop_
_audit_author_name
_audit_author_address
'Xi Xi Kang'
;Anhui University
China
;
_audit_update_record             
;
2021-07-04 deposited with the CCDC.	2022-04-12 downloaded from the CCDC.
;
_audit_creation_date             2021-06-21
_audit_creation_method           
;
Olex2 1.2
(compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506)
;
_shelx_SHELXL_version_number     2018/3
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         'C260 H390 Ag36 S30, 2(F6 Sb)'
_chemical_formula_sum            'C260 H390 Ag36 F12 S30 Sb2'
_chemical_formula_weight         8832.32
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag 0.1306 4.2820 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0727 0.0534 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.3331 0.5567 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sb Sb -0.0562 5.8946 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_H-M_alt        'P 1 21/n 1'
_space_group_name_Hall           '-P 2yn'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'

_cell_length_a                   22.2769(4)
_cell_length_b                   29.4661(4)
_cell_length_c                   24.0645(4)
_cell_angle_alpha                90
_cell_angle_beta                 95.0370(10)
_cell_angle_gamma                90
_cell_volume                     15735.3(4)
_cell_formula_units_Z            2
_cell_measurement_reflns_used    18915
_cell_measurement_temperature    120(2)
_cell_measurement_theta_max      62.499
_cell_measurement_theta_min      3.521
_shelx_estimated_absorpt_T_max   ?
_shelx_estimated_absorpt_T_min   ?
_exptl_absorpt_coefficient_mu    21.085
_exptl_absorpt_correction_T_max  ?
_exptl_absorpt_correction_T_min  ?
_exptl_absorpt_correction_type   ?
_exptl_absorpt_process_details   ?
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            yellow
_exptl_crystal_colour_primary    yellow
_exptl_crystal_density_diffrn    1.864
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       block
_exptl_crystal_F_000             8664
_exptl_crystal_size_max          ?
_exptl_crystal_size_mid          ?
_exptl_crystal_size_min          ?
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0470
_diffrn_reflns_av_unetI/netI     0.0543
_diffrn_reflns_Laue_measured_fraction_full 0.971
_diffrn_reflns_Laue_measured_fraction_max 0.971
_diffrn_reflns_limit_h_max       21
_diffrn_reflns_limit_h_min       -25
_diffrn_reflns_limit_k_max       33
_diffrn_reflns_limit_k_min       -29
_diffrn_reflns_limit_l_max       22
_diffrn_reflns_limit_l_min       -27
_diffrn_reflns_number            49442
_diffrn_reflns_point_group_measured_fraction_full 0.971
_diffrn_reflns_point_group_measured_fraction_max 0.971
_diffrn_reflns_theta_full        62.499
_diffrn_reflns_theta_max         62.499
_diffrn_reflns_theta_min         3.521
_diffrn_ambient_temperature      120(2)
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 0.971
_diffrn_measured_fraction_theta_max 0.971
_diffrn_measurement_device_type  STOE
_diffrn_measurement_method       ?
_diffrn_radiation_type           CuK\a
_diffrn_radiation_wavelength     1.54186
_diffrn_source                   ?
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                18915
_reflns_number_total             24374
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 Structure factors included contributions from the .fab file.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       ?
_computing_data_collection       ?
_computing_data_reduction        ?
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'ShelXL (Sheldrick, 2015)'
_computing_structure_solution    'SHELXT 2018/2 (Sheldrick, 2018)'
_refine_diff_density_max         2.843
_refine_diff_density_min         -4.877
_refine_diff_density_rms         0.282
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.029
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1549
_refine_ls_number_reflns         24374
_refine_ls_number_restraints     2565
_refine_ls_R_factor_all          0.1085
_refine_ls_R_factor_gt           0.0909
_refine_ls_restrained_S_all      0.989
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.1677P)²+221.9751P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.2502
_refine_ls_wR_factor_ref         0.2693
_refine_special_details          ?
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H) groups, All C(H,H) groups
2. Restrained distances
 C03N-C02W = C03Y-C02W = C044-C03Y = C044-C034 = C04S-C03Y = C03N-C02L = C034-
 C02L = C049-C034 = C04V-C049 = C04V-C04H = C04H-C03N = C04V-C04S
 1.54 with sigma of 0.01
 C02W-C044
 2.54 with sigma of 0.01
 C02W-C04H
 2.54 with sigma of 0.01
 C02W-C02L
 2.54 with sigma of 0.01
 C02W-C04S
 2.54 with sigma of 0.01
 C03Y-C034
 2.54 with sigma of 0.01
 C03Y-C03N
 2.54 with sigma of 0.01
 C03Y-C04V
 2.54 with sigma of 0.01
 C044-C049
 2.54 with sigma of 0.01
 C044-C02L
 2.54 with sigma of 0.01
 C044-C04S
 2.54 with sigma of 0.01
 C034-C04V
 2.54 with sigma of 0.01
 C034-C03N
 2.54 with sigma of 0.01
 C049-C04H
 2.54 with sigma of 0.01
 C049-C04S
 2.54 with sigma of 0.01
 C049-C02L
 2.54 with sigma of 0.01
 C04V-C03N
 2.54 with sigma of 0.01
 C04H-C02L
 2.54 with sigma of 0.01
 C03N-C034
 2.54 with sigma of 0.01
 C02W-C034
 2.93 with sigma of 0.01
 C02W-C04V
 2.93 with sigma of 0.01
 C03Y-C02L
 2.93 with sigma of 0.01
 C03Y-C049
 2.93 with sigma of 0.01
 C044-C03N
 2.93 with sigma of 0.01
 C044-C04V
 2.93 with sigma of 0.01
 C034-C04H
 2.93 with sigma of 0.01
 C034-C04S
 2.93 with sigma of 0.01
 C049-C03N
 2.93 with sigma of 0.01
 C049-C03Y
 2.93 with sigma of 0.01
 C04V-C02L
 2.93 with sigma of 0.01
 C04H-C034
 2.93 with sigma of 0.01
 C04T-C04G = C5-C04T = C5-C17 = C18-C17 = C18-C03L = C04G-C03L = C19-C03V =
 C03L-C03G = C17-C12 = C19-C12 = C04T-C03V
 1.54 with sigma of 0.01
 C04G-C03G
 2.54 with sigma of 0.01
 C04G-C5
 2.54 with sigma of 0.01
 C04G-C18
 2.54 with sigma of 0.01
 C04G-C03V
 2.54 with sigma of 0.01
 C03L-C17
 2.54 with sigma of 0.01
 C03L-C04T
 2.54 with sigma of 0.01
 C03L-C19
 2.54 with sigma of 0.01
 C03G-C18
 2.54 with sigma of 0.01
 C03G-C12
 2.54 with sigma of 0.01
 C03G-C03V
 2.54 with sigma of 0.01
 C19-C17
 2.54 with sigma of 0.01
 C19-C04T
 2.54 with sigma of 0.01
 C12-C5
 2.54 with sigma of 0.01
 C12-C18
 2.54 with sigma of 0.01
 C12-C03V
 2.54 with sigma of 0.01
 C17-C04T
 2.54 with sigma of 0.01
 C5-C03V
 2.54 with sigma of 0.01
 C5-C18
 2.54 with sigma of 0.01
 C04G-C19
 2.93 with sigma of 0.01
 C04G-C17
 2.93 with sigma of 0.01
 C03L-C5
 2.93 with sigma of 0.01
 C03L-C03V
 2.93 with sigma of 0.01
 C03L-C12
 2.93 with sigma of 0.01
 C03G-C17
 2.93 with sigma of 0.01
 C03G-C04T
 2.93 with sigma of 0.01
 C19-C5
 2.93 with sigma of 0.01
 C19-C18
 2.93 with sigma of 0.01
 C12-C04T
 2.93 with sigma of 0.01
 C17-C03V
 2.93 with sigma of 0.01
 C04I-C028 = C03P-C028 = C04I-C04D = C04D-C02U = C04R-C02U = C04R-C03P = C04Q-
 C04N = C04Q-C02U = C03U-C03P = C04N-C03U = C04U-C04N
 1.54 with sigma of 0.01
3. Uiso/Uaniso restraints and constraints
C03G \\sim C03L \\sim C03V \\sim C04G \\sim C04T \\sim C5 \\sim C12 \\sim C17
\\sim C18 \\sim C19: within 3.8A with sigma of 0.01 and sigma for terminal
atoms of 0.02
Sb0J \\sim F02X \\sim F045 \\sim F046 \\sim F04F \\sim F04J \\sim F04P: within
3.8A with sigma of 0.01 and sigma for terminal atoms of 0.02
C02L \\sim C02W \\sim C034 \\sim C03N \\sim C03Y \\sim C044 \\sim C049 \\sim
C04H \\sim C04S \\sim C04V: within 3.8A with sigma of 0.01 and sigma for
terminal atoms of 0.02
C028 \\sim C02U \\sim C03P \\sim C03U \\sim C04D \\sim C04I \\sim C04N \\sim
C04Q \\sim C04R \\sim C04U: within 3.8A with sigma of 0.01 and sigma for
terminal atoms of 0.02
C01H \\sim C01R \\sim C01T \\sim C01X \\sim C02E \\sim C02Q \\sim C02Y \\sim
C048 \\sim C04K \\sim C04M: within 3.8A with sigma of 0.01 and sigma for
terminal atoms of 0.02
C01A \\sim C01P \\sim C01Y \\sim C02R \\sim C037 \\sim C03C \\sim C03K \\sim
C03Q \\sim C041 \\sim C043: within 3.8A with sigma of 0.01 and sigma for
terminal atoms of 0.02
C015 \\sim C017 \\sim C01K \\sim C021 \\sim C02I \\sim C02N \\sim C02O \\sim
C02P \\sim C030 \\sim C03O: within 3.8A with sigma of 0.01 and sigma for
terminal atoms of 0.02
C012 \\sim C01O \\sim C02B \\sim C02V \\sim C033 \\sim C038 \\sim C03J \\sim
C03T \\sim C042 \\sim C04E: within 3.8A with sigma of 0.01 and sigma for
terminal atoms of 0.02
Uanis(C03G) \\sim Ueq, Uanis(C03L) \\sim Ueq, Uanis(C03V) \\sim Ueq,
Uanis(C04G) \\sim Ueq, Uanis(C04T) \\sim Ueq, Uanis(C5) \\sim Ueq, Uanis(C12)
\\sim Ueq, Uanis(C17) \\sim Ueq, Uanis(C18) \\sim Ueq, Uanis(C19) \\sim Ueq:
with sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(Sb0J) \\sim Ueq, Uanis(F02X) \\sim Ueq, Uanis(F045) \\sim Ueq,
Uanis(F046) \\sim Ueq, Uanis(F04F) \\sim Ueq, Uanis(F04J) \\sim Ueq,
Uanis(F04P) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(C02L) \\sim Ueq, Uanis(C034) \\sim Ueq, Uanis(C03N) \\sim Ueq,
Uanis(C03Y) \\sim Ueq, Uanis(C044) \\sim Ueq, Uanis(C049) \\sim Ueq,
Uanis(C04H) \\sim Ueq, Uanis(C04S) \\sim Ueq, Uanis(C04V) \\sim Ueq,
Uanis(C02W) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(C028) \\sim Ueq, Uanis(C02U) \\sim Ueq, Uanis(C03P) \\sim Ueq,
Uanis(C03U) \\sim Ueq, Uanis(C04D) \\sim Ueq, Uanis(C04I) \\sim Ueq,
Uanis(C04N) \\sim Ueq, Uanis(C04Q) \\sim Ueq, Uanis(C04R) \\sim Ueq,
Uanis(C04U) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(C01H) \\sim Ueq, Uanis(C01R) \\sim Ueq, Uanis(C01T) \\sim Ueq,
Uanis(C01X) \\sim Ueq, Uanis(C02E) \\sim Ueq, Uanis(C02Q) \\sim Ueq,
Uanis(C02Y) \\sim Ueq, Uanis(C048) \\sim Ueq, Uanis(C04K) \\sim Ueq,
Uanis(C04M) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(C01A) \\sim Ueq, Uanis(C01P) \\sim Ueq, Uanis(C01Y) \\sim Ueq,
Uanis(C02R) \\sim Ueq, Uanis(C037) \\sim Ueq, Uanis(C03C) \\sim Ueq,
Uanis(C03K) \\sim Ueq, Uanis(C03Q) \\sim Ueq, Uanis(C041) \\sim Ueq,
Uanis(C043) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(C017) \\sim Ueq, Uanis(C01K) \\sim Ueq, Uanis(C021) \\sim Ueq,
Uanis(C02I) \\sim Ueq, Uanis(C02N) \\sim Ueq, Uanis(C02O) \\sim Ueq,
Uanis(C02P) \\sim Ueq, Uanis(C030) \\sim Ueq, Uanis(C03O) \\sim Ueq,
Uanis(C015) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(C012) \\sim Ueq, Uanis(C01O) \\sim Ueq, Uanis(C02B) \\sim Ueq,
Uanis(C02V) \\sim Ueq, Uanis(C033) \\sim Ueq, Uanis(C038) \\sim Ueq,
Uanis(C03J) \\sim Ueq, Uanis(C03T) \\sim Ueq, Uanis(C042) \\sim Ueq,
Uanis(C04E) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02
4. Others
 Fixed Sof: Ag0F(0.9) Ag(0.7) Ag1(0.1) Ag2(0.3)
5.a Ternary CH refined with riding coordinates:
 C010(H010), C011(H011), C012(H012), C013(H013), C014(H014), C015(H015),
 C016(H016), C017(H017), C018(H018), C01A(H01C), C01B(H01D), C01D(H01G),
 C01F(H01J), C01G(H01K), C01I(H01N), C01L(H01S), C01P(H01Z), C01Q(H01),
 C01R(H0AA), C01S(H1AA), C01T(H2AA), C01U(H3AA), C01V(H4AA), C01X(H6AA),
 C01Y(H7AA), C01Z(H8AA), C021(H021), C023(H023), C024(H024), C025(H025),
 C028(H028), C029(H029), C02B(H02K), C02E(H02P), C02F(H02Q), C02H(H02T),
 C02J(H02W), C02K(H02X), C02M(H02Z), C02O(H9AA), C02P(H0BA), C02U(H5BA),
 C02W(H7BA), C032(H032), C033(H033), C034(H034), C03C(H03Q), C03D(H03R),
 C03I(H03Z), C03J(H03), C03K(H9BA), C03L(H0CA), C03N(H2CA), C03P(H4CA),
 C03T(H7CA), C03Y(H2DA), C040(H040), C04G(H04Q), C04I(H04T), C04K(H04U),
 C04N(H04X), C04T(H4DA), C04V(H6DA), C17(H17), C19(H19)
5.b Secondary CH2 refined with riding coordinates:
 C019(H01A,H01B), C01C(H01E,H01F), C01E(H01H,H01I), C01H(H01L,H01M), C01J(H01O,
 H01P), C01K(H01Q,H01R), C01M(H01T,H01U), C01N(H01V,H01W), C01O(H01X,H01Y),
 C01W(H5AA,H), C020(H02A,H02B), C022(H02C,H02D), C026(H02E,H02F), C027(H02G,
 H02H), C02A(H02I,H02J), C02C(H02L,H02M), C02D(H02N,H02O), C02G(H02R,H02S),
 C02I(H02U,H02V), C02L(H02Y,HA), C02N(H02,HB), C02Q(H1BA,HC), C02R(H2BA,HD),
 C02S(H3BA,HE), C02T(H4BA,HF), C02V(H6BA,HG), C02Y(H8BA,HH), C030(H03A,H03B),
 C031(H03C,H03D), C035(H03E,H03F), C036(H03G,H03H), C037(H03I,H03J), C038(H03K,
 H03L), C039(H03M,H03N), C03A(H03O,H03P), C03E(H03S,H03T), C03F(H03U,H03V),
 C03G(H03W,H03X), C03H(H03Y,HI), C03M(H1CA,HJ), C03O(H3CA,HK), C03Q(H5CA,HL),
 C03R(H6CA,HM), C03U(H8CA,HN), C03V(H9CA,HO), C03W(H0DA,HP), C03X(H1DA,HQ),
 C03Z(H3DA,HR), C041(H04A,H04B), C042(H04C,H04D), C043(H04E,H04F), C044(H04G,
 H04H), C048(H04I,H04J), C049(H04K,H04L), C04D(H04M,H04N), C04E(H04O,H04P),
 C04H(H04R,H04S), C04M(H04V,H04W), C04Q(H04Y,HS), C04R(H04Z,HT), C04S(H04,HU),
 C04U(H5DA,HV), C5(H5A,H5B), C12(H12A,H12B), C18(H18A,H18B)
;
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag01 Ag 0.59331(4) 0.53057(3) 0.49872(4) 0.0353(2) Uani 1 1 d . . . . .
Ag02 Ag 0.49768(4) 0.51384(3) 0.40408(4) 0.0378(2) Uani 1 1 d . . . . .
Ag03 Ag 0.51126(5) 0.62071(4) 0.42402(4) 0.0422(2) Uani 1 1 d . . . . .
Ag04 Ag 0.51884(5) 0.42357(4) 0.46240(4) 0.0445(3) Uani 1 1 d . . . . .
Ag05 Ag 0.57324(5) 0.66528(4) 0.51948(4) 0.0471(3) Uani 1 1 d . . . . .
Ag06 Ag 0.59248(5) 0.58012(4) 0.34875(4) 0.0486(3) Uani 1 1 d . . . . .
Ag07 Ag 0.60955(6) 0.68763(4) 0.32312(4) 0.0503(3) Uani 1 1 d . . . . .
Ag08 Ag 0.38604(5) 0.46026(4) 0.37100(5) 0.0502(3) Uani 1 1 d . . . . .
Ag09 Ag 0.59052(6) 0.73992(4) 0.42931(4) 0.0515(3) Uani 1 1 d . . . . .
Ag0A Ag 0.72153(5) 0.56418(4) 0.39179(6) 0.0587(3) Uani 1 1 d . . . . .
Ag0B Ag 0.45942(6) 0.59059(4) 0.31272(5) 0.0567(3) Uani 1 1 d . . . . .
Ag0C Ag 0.70291(6) 0.63236(4) 0.54842(5) 0.0566(3) Uani 1 1 d . . . . .
Ag0D Ag 0.43981(6) 0.67536(4) 0.49836(6) 0.0648(4) Uani 1 1 d . . . . .
Ag0E Ag 0.35651(6) 0.55432(4) 0.56584(6) 0.0625(3) Uani 1 1 d . . . . .
Ag0F Ag 0.72515(6) 0.51997(6) 0.52187(7) 0.0603(4) Uani 0.9 1 d . . P . .
Ag0G Ag 0.71268(7) 0.66817(5) 0.42583(7) 0.0751(4) Uani 1 1 d . . . . .
Ag0H Ag 0.31733(7) 0.55053(6) 0.35344(8) 0.0812(4) Uani 1 1 d . . . . .
Ag Ag 0.30856(13) 0.60076(9) 0.46086(10) 0.0704(6) Uani 0.7 1 d . . P A 2
Sb0J Sb 0.98904(10) 0.67985(9) 0.49692(10) 0.1233(7) Uani 1 1 d . U . . .
S00 S 0.61397(15) 0.60073(11) 0.45468(13) 0.0370(7) Uani 1 1 d . . . . .
S1 S 0.58126(15) 0.45845(12) 0.54077(14) 0.0394(7) Uani 1 1 d . . . . .
S00M S 0.41419(15) 0.64665(12) 0.38591(14) 0.0419(7) Uani 1 1 d . . . . .
S00N S 0.54466(17) 0.63210(13) 0.27649(14) 0.0442(8) Uani 1 1 d . . . . .
S00O S 0.58845(15) 0.49448(13) 0.35946(14) 0.0432(8) Uani 1 1 d . . . . .
S00P S 0.44080(16) 0.38823(12) 0.39918(14) 0.0424(7) Uani 1 1 d . . . . .
S00Q S 0.64874(17) 0.75940(12) 0.35466(16) 0.0474(8) Uani 1 1 d . . . . .
S00R S 0.36229(16) 0.63557(13) 0.54258(16) 0.0467(8) Uani 1 1 d . . . . .
S00S S 0.51304(18) 0.73585(12) 0.49139(15) 0.0474(8) Uani 1 1 d . . . . .
S00T S 0.71878(16) 0.56462(14) 0.60227(17) 0.0501(9) Uani 1 1 d . . . . .
S00U S 0.39689(18) 0.52212(13) 0.30273(15) 0.0490(9) Uani 1 1 d . . . . .
S00V S 0.74004(17) 0.49141(14) 0.43287(19) 0.0555(10) Uani 1 1 d . . . . .
S00W S 0.6932(2) 0.70703(15) 0.5097(2) 0.0689(13) Uani 1 1 d . . . . .
S00X S 0.2331(2) 0.57094(16) 0.3999(3) 0.0768(15) Uani 1 1 d . . . . .
S00Z S 0.7200(2) 0.63196(18) 0.3378(2) 0.0702(13) Uani 1 1 d . . . . .
C010 C 0.3196(8) 0.6735(6) 0.5845(7) 0.055(4) Uani 1 1 d . . . . .
H010 H 0.344128 0.676479 0.620164 0.066 Uiso 1 1 calc R . . . .
C011 C 0.6032(7) 0.8005(5) 0.3110(6) 0.042(3) Uani 1 1 d . . . . .
H011 H 0.568297 0.784547 0.292625 0.051 Uiso 1 1 calc R . . . .
C012 C 0.4214(10) 0.7027(7) 0.3522(8) 0.073(2) Uani 1 1 d . U . . .
H012 H 0.463701 0.712035 0.357249 0.088 Uiso 1 1 calc R . . . .
C013 C 0.5801(8) 0.8391(5) 0.3462(7) 0.052(4) Uani 1 1 d . . . . .
H013 H 0.557001 0.826485 0.375313 0.063 Uiso 1 1 calc R . . . .
C014 C 0.6402(8) 0.8192(6) 0.2663(6) 0.053(4) Uani 1 1 d . . . . .
H014 H 0.655212 0.794510 0.243930 0.063 Uiso 1 1 calc R . . . .
C015 C 0.7904(8) 0.5597(7) 0.6455(8) 0.068(2) Uani 1 1 d . U . . .
H015 H 0.787720 0.531658 0.667001 0.081 Uiso 1 1 calc R . . . .
C016 C 0.4465(9) 0.8573(6) 0.5113(7) 0.064(5) Uani 1 1 d . . . . .
H016 H 0.414583 0.871034 0.486109 0.077 Uiso 1 1 calc R . . . .
C017 C 0.8004(9) 0.5976(7) 0.6880(8) 0.068(2) Uani 1 1 d . U . . .
H017 H 0.764412 0.600743 0.708340 0.082 Uiso 1 1 calc R . . . .
C018 C 0.5268(9) 0.7805(6) 0.5464(6) 0.058(4) Uani 1 1 d . . . . .
H018 H 0.557913 0.769957 0.574788 0.070 Uiso 1 1 calc R . . . .
C019 C 0.4243(10) 0.8140(6) 0.5365(8) 0.068(5) Uani 1 1 d . . . . .
H01A H 0.389364 0.820792 0.556436 0.082 Uiso 1 1 calc R . . . .
H01B H 0.411923 0.792839 0.506832 0.082 Uiso 1 1 calc R . . . .
C01A C 0.3782(11) 0.5060(8) 0.2302(9) 0.081(3) Uani 1 1 d . U . . .
H01C H 0.409972 0.485528 0.219630 0.097 Uiso 1 1 calc R . . . .
C01B C 0.5759(8) 0.6197(6) 0.2087(6) 0.055(4) Uani 1 1 d . . . . .
H01D H 0.606370 0.595924 0.215849 0.066 Uiso 1 1 calc R . . . .
C01C C 0.5393(8) 0.8711(6) 0.3081(7) 0.060(4) Uani 1 1 d . . . . .
H01E H 0.526680 0.896781 0.329334 0.072 Uiso 1 1 calc R . . . .
H01F H 0.503680 0.854928 0.292802 0.072 Uiso 1 1 calc R . . . .
C01D C 0.2609(9) 0.6559(6) 0.5992(9) 0.068(5) Uani 1 1 d . . . . .
H01G H 0.265648 0.625123 0.614330 0.082 Uiso 1 1 calc R . . . .
C01E C 0.6329(8) 0.8668(6) 0.3729(8) 0.062(4) Uani 1 1 d . . . . .
H01H H 0.659084 0.847556 0.397052 0.074 Uiso 1 1 calc R . . . .
H01I H 0.618097 0.891086 0.395203 0.074 Uiso 1 1 calc R . . . .
C01F C 0.4621(9) 0.3598(6) 0.3340(7) 0.062(5) Uani 1 1 d . . . . .
H01J H 0.503496 0.368274 0.327601 0.075 Uiso 1 1 calc R . . . .
C01G C 0.4190(10) 0.3743(7) 0.2828(7) 0.072(6) Uani 1 1 d . . . . .
H01K H 0.419650 0.407394 0.279250 0.087 Uiso 1 1 calc R . . . .
C01H C 0.9003(9) 0.4339(8) 0.3953(9) 0.079(2) Uani 1 1 d . U . . .
H01L H 0.915170 0.423881 0.360600 0.094 Uiso 1 1 calc R . . . .
H01M H 0.893813 0.407307 0.417701 0.094 Uiso 1 1 calc R . . . .
C01I C 0.5765(9) 0.8877(7) 0.2600(8) 0.070(6) Uani 1 1 d . . . . .
H01N H 0.551296 0.907297 0.234676 0.084 Uiso 1 1 calc R . . . .
C01J C 0.6399(10) 0.5055(7) 0.2354(7) 0.070(5) Uani 1 1 d . . . . .
H01O H 0.638884 0.522022 0.200441 0.083 Uiso 1 1 calc R . . . .
H01P H 0.652614 0.526355 0.265409 0.083 Uiso 1 1 calc R . . . .
C01K C 0.8130(9) 0.6412(7) 0.6621(8) 0.071(2) Uani 1 1 d . U . . .
H01Q H 0.820996 0.664266 0.690553 0.085 Uiso 1 1 calc R . . . .
H01R H 0.778381 0.650749 0.637541 0.085 Uiso 1 1 calc R . . . .
C01L C 0.5281(10) 0.6009(7) 0.1670(7) 0.071(5) Uani 1 1 d . . . . .
H01S H 0.507864 0.575053 0.182828 0.085 Uiso 1 1 calc R . . . .
C01M C 0.4835(8) 0.6385(6) 0.1517(8) 0.063(4) Uani 1 1 d . . . . .
H01T H 0.465355 0.648181 0.184891 0.075 Uiso 1 1 calc R . . . .
H01U H 0.451734 0.626893 0.125377 0.075 Uiso 1 1 calc R . . . .
C01N C 0.5983(9) 0.8509(7) 0.2296(8) 0.066(5) Uani 1 1 d . . . . .
H01V H 0.620051 0.862741 0.199542 0.079 Uiso 1 1 calc R . . . .
H01W H 0.564302 0.833553 0.213002 0.079 Uiso 1 1 calc R . . . .
C01O C 0.3136(9) 0.7730(7) 0.2764(9) 0.074(2) Uani 1 1 d . U . . .
H01X H 0.289859 0.797544 0.289926 0.089 Uiso 1 1 calc R . . . .
H01Y H 0.304536 0.770625 0.236352 0.089 Uiso 1 1 calc R . . . .
C01P C 0.3757(11) 0.5460(8) 0.1905(9) 0.082(3) Uani 1 1 d . U . . .
H01Z H 0.412032 0.564496 0.198271 0.099 Uiso 1 1 calc R . . . .
C01Q C 0.3154(9) 0.7215(6) 0.5606(9) 0.070(5) Uani 1 1 d . . . . .
H01 H 0.354783 0.732504 0.551017 0.085 Uiso 1 1 calc R . . . .
C01R C 0.9482(10) 0.4657(8) 0.4274(9) 0.078(2) Uani 1 1 d . U . . .
H0AA H 0.986644 0.449695 0.434881 0.093 Uiso 1 1 calc R . . . .
C01S C 0.5129(10) 0.8682(6) 0.5987(9) 0.073(5) Uani 1 1 d . . . . .
H1AA H 0.523948 0.889380 0.629355 0.087 Uiso 1 1 calc R . . . .
C01T C 0.8175(9) 0.4707(8) 0.4366(9) 0.077(2) Uani 1 1 d . U . . .
H2AA H 0.817923 0.442389 0.458094 0.092 Uiso 1 1 calc R . . . .
C01U C 0.5494(8) 0.8249(6) 0.5180(7) 0.057(4) Uani 1 1 d . . . . .
H3AA H 0.584382 0.817934 0.497468 0.068 Uiso 1 1 calc R . . . .
C01V C 0.6683(8) 0.8868(5) 0.3261(9) 0.064(5) Uani 1 1 d . . . . .
H4AA H 0.702897 0.903906 0.343229 0.077 Uiso 1 1 calc R . . . .
C01W C 0.5614(8) 0.6973(6) 0.1672(8) 0.065(5) Uani 1 1 d . . . . .
H5AA H 0.542752 0.708499 0.199474 0.078 Uiso 1 1 calc R . . . .
H H 0.581998 0.722497 0.151254 0.078 Uiso 1 1 calc R . . . .
C01X C 0.8416(9) 0.4590(8) 0.3829(9) 0.077(2) Uani 1 1 d . U . . .
H6AA H 0.812704 0.439888 0.360506 0.093 Uiso 1 1 calc R . . . .
C01Y C 0.3175(11) 0.4798(8) 0.2216(9) 0.084(3) Uani 1 1 d . U . . .
H7AA H 0.316119 0.455330 0.249029 0.100 Uiso 1 1 calc R . . . .
C01Z C 0.4577(11) 0.3079(8) 0.3378(8) 0.085(7) Uani 1 1 d . . . . .
H8AA H 0.483242 0.297323 0.370434 0.102 Uiso 1 1 calc R . . . .
C020 C 0.6839(8) 0.4391(8) 0.2872(7) 0.072(6) Uani 1 1 d . . . . .
H02A H 0.697748 0.457937 0.318781 0.086 Uiso 1 1 calc R . . . .
H02B H 0.712048 0.414098 0.285501 0.086 Uiso 1 1 calc R . . . .
C021 C 0.9099(9) 0.5795(7) 0.6985(8) 0.069(2) Uani 1 1 d . U . . .
H021 H 0.943734 0.571002 0.725323 0.083 Uiso 1 1 calc R . . . .
C022 C 0.5007(9) 0.8457(6) 0.4798(8) 0.066(5) Uani 1 1 d . . . . .
H02C H 0.488604 0.824704 0.449844 0.079 Uiso 1 1 calc R . . . .
H02D H 0.515721 0.873057 0.463348 0.079 Uiso 1 1 calc R . . . .
C023 C 0.6843(9) 0.4666(9) 0.2349(8) 0.080(6) Uani 1 1 d . . . . .
H023 H 0.724919 0.478354 0.231205 0.096 Uiso 1 1 calc R . . . .
C024 C 0.4703(8) 0.7932(7) 0.5744(7) 0.062(4) Uani 1 1 d . . . . .
H024 H 0.453720 0.765871 0.590469 0.074 Uiso 1 1 calc R . . . .
C025 C 0.6077(8) 0.6607(7) 0.1861(6) 0.061(5) Uani 1 1 d . . . . .
H025 H 0.638193 0.672692 0.214028 0.073 Uiso 1 1 calc R . . . .
C026 C 0.4898(13) 0.8260(7) 0.6208(8) 0.088(7) Uani 1 1 d . . . . .
H02E H 0.455770 0.832832 0.641946 0.106 Uiso 1 1 calc R . . . .
H02F H 0.520894 0.812076 0.645941 0.106 Uiso 1 1 calc R . . . .
C027 C 0.3905(9) 0.2914(7) 0.3428(8) 0.066(5) Uani 1 1 d . . . . .
H02G H 0.389559 0.258619 0.346329 0.080 Uiso 1 1 calc R . . . .
H02H H 0.375268 0.304566 0.375681 0.080 Uiso 1 1 calc R . . . .
C028 C 0.7957(13) 0.6362(10) 0.3075(10) 0.122(4) Uani 1 1 d D U . . .
H028 H 0.811660 0.605837 0.300810 0.147 Uiso 1 1 calc R . . . .
C029 C 0.5770(9) 0.4870(7) 0.2437(7) 0.062(4) Uani 1 1 d . . . . .
H029 H 0.548820 0.512365 0.245573 0.074 Uiso 1 1 calc R . . . .
C02A C 0.6643(9) 0.4356(8) 0.1843(8) 0.075(6) Uani 1 1 d . . . . .
H02I H 0.663071 0.453058 0.150010 0.090 Uiso 1 1 calc R . . . .
H02J H 0.693069 0.411107 0.181826 0.090 Uiso 1 1 calc R . . . .
C02B C 0.4019(10) 0.7004(7) 0.2887(9) 0.075(2) Uani 1 1 d . U . . .
H02K H 0.424430 0.676766 0.270919 0.090 Uiso 1 1 calc R . . . .
C02C C 0.4650(12) 0.8890(7) 0.5585(10) 0.090(7) Uani 1 1 d . . . . .
H02L H 0.430134 0.896422 0.578184 0.108 Uiso 1 1 calc R . . . .
H02M H 0.480231 0.916943 0.543698 0.108 Uiso 1 1 calc R . . . .
C02D C 0.6315(9) 0.9170(6) 0.2898(10) 0.079(6) Uani 1 1 d . . . . .
H02N H 0.655270 0.929996 0.261954 0.095 Uiso 1 1 calc R . . . .
H02O H 0.615949 0.941471 0.311340 0.095 Uiso 1 1 calc R . . . .
C02E C 0.8622(9) 0.5030(8) 0.4699(9) 0.078(2) Uani 1 1 d . U . . .
H02P H 0.846807 0.512590 0.504933 0.094 Uiso 1 1 calc R . . . .
C02F C 0.5766(8) 0.4590(6) 0.2953(6) 0.052(4) Uani 1 1 d . . . . .
H02Q H 0.536459 0.445351 0.295089 0.062 Uiso 1 1 calc R . . . .
C02G C 0.6916(8) 0.8477(6) 0.2918(8) 0.065(5) Uani 1 1 d . . . . .
H02R H 0.714022 0.859907 0.262418 0.078 Uiso 1 1 calc R . . . .
H02S H 0.718637 0.828855 0.315629 0.078 Uiso 1 1 calc R . . . .
C02H C 0.5139(10) 0.6800(8) 0.1255(8) 0.075(5) Uani 1 1 d . . . . .
H02T H 0.484054 0.703695 0.115359 0.090 Uiso 1 1 calc R . . . .
C02I C 0.8591(9) 0.5961(7) 0.5872(8) 0.071(2) Uani 1 1 d . U . . .
H02U H 0.825159 0.603170 0.560523 0.085 Uiso 1 1 calc R . . . .
H02V H 0.894223 0.591628 0.566726 0.085 Uiso 1 1 calc R . . . .
C02J C 0.4383(12) 0.3000(8) 0.2344(8) 0.088(7) Uani 1 1 d . . . . .
H02W H 0.453945 0.286462 0.201333 0.106 Uiso 1 1 calc R . . . .
C02K C 0.3509(10) 0.3063(7) 0.2900(8) 0.071(5) Uani 1 1 d . . . . .
H02X H 0.309154 0.296963 0.293384 0.085 Uiso 1 1 calc R . . . .
C02L C 0.0931(7) 0.5871(5) 0.3723(5) 0.101(3) Uani 1 1 d D U . . .
H02Y H 0.111992 0.560732 0.390475 0.122 Uiso 1 1 calc R . . . .
HA H 0.054953 0.592315 0.387742 0.122 Uiso 1 1 calc R . . . .
C02M C 0.2276(9) 0.7351(8) 0.6184(10) 0.081(6) Uani 1 1 d . . . . .
H02Z H 0.212666 0.754568 0.647237 0.097 Uiso 1 1 calc R . . . .
C02N C 0.9230(9) 0.6224(7) 0.6714(8) 0.070(2) Uani 1 1 d . U . . .
H02 H 0.960058 0.619536 0.653255 0.084 Uiso 1 1 calc R . . . .
HB H 0.928566 0.646226 0.699173 0.084 Uiso 1 1 calc R . . . .
C02O C 0.8702(9) 0.6353(7) 0.6273(8) 0.071(2) Uani 1 1 d . U . . .
H9AA H 0.878978 0.663268 0.607606 0.085 Uiso 1 1 calc R . . . .
C02P C 0.8469(9) 0.5557(7) 0.6160(8) 0.070(2) Uani 1 1 d . U . . .
H0BA H 0.841677 0.530910 0.588869 0.083 Uiso 1 1 calc R . . . .
C02Q C 0.9559(10) 0.5062(8) 0.3909(9) 0.079(2) Uani 1 1 d . U . . .
H1BA H 0.967796 0.496512 0.354963 0.095 Uiso 1 1 calc R . . . .
HC H 0.987118 0.525914 0.408103 0.095 Uiso 1 1 calc R . . . .
C02R C 0.2661(11) 0.5277(8) 0.1220(9) 0.084(3) Uani 1 1 d . U . . .
H2BA H 0.229558 0.510643 0.111660 0.101 Uiso 1 1 calc R . . . .
HD H 0.267674 0.552581 0.095782 0.101 Uiso 1 1 calc R . . . .
C02S C 0.6063(12) 0.3892(7) 0.2476(8) 0.084(7) Uani 1 1 d . . . . .
H3BA H 0.567811 0.374765 0.251634 0.100 Uiso 1 1 calc R . . . .
HE H 0.636626 0.365556 0.246978 0.100 Uiso 1 1 calc R . . . .
C02T C 0.5563(10) 0.4563(8) 0.1932(10) 0.084(6) Uani 1 1 d . . . . .
H4BA H 0.554750 0.473648 0.158829 0.101 Uiso 1 1 calc R . . . .
HF H 0.516351 0.444281 0.197328 0.101 Uiso 1 1 calc R . . . .
C02U C 0.9005(13) 0.6809(8) 0.2685(10) 0.123(4) Uani 1 1 d D U . . .
H5BA H 0.939715 0.678542 0.253176 0.147 Uiso 1 1 calc R . . . .
C02V C 0.3174(9) 0.7314(8) 0.3671(9) 0.077(2) Uani 1 1 d . U . . .
H6BA H 0.296636 0.756236 0.383635 0.092 Uiso 1 1 calc R . . . .
HG H 0.306284 0.703436 0.384775 0.092 Uiso 1 1 calc R . . . .
C02W C 0.1954(5) 0.6198(6) 0.3588(6) 0.102(3) Uani 1 1 d D U . . .
H7BA H 0.220787 0.646878 0.364436 0.123 Uiso 1 1 calc R . . . .
F02X F 0.9017(11) 0.6758(8) 0.4940(10) 0.170(5) Uani 1 1 d . U . . .
C02Y C 0.9198(10) 0.4739(8) 0.4807(9) 0.080(2) Uani 1 1 d . U . . .
H8BA H 0.948216 0.489409 0.507012 0.096 Uiso 1 1 calc R . . . .
HH H 0.909598 0.445119 0.496900 0.096 Uiso 1 1 calc R . . . .
C030 C 0.8527(9) 0.5846(8) 0.7283(9) 0.072(2) Uani 1 1 d . U . . .
H03A H 0.843941 0.556217 0.746241 0.087 Uiso 1 1 calc R . . . .
H03B H 0.858851 0.607720 0.756956 0.087 Uiso 1 1 calc R . . . .
C031 C 0.5565(12) 0.5869(8) 0.1151(9) 0.083(6) Uani 1 1 d . . . . .
H03C H 0.586798 0.563798 0.124303 0.100 Uiso 1 1 calc R . . . .
H03D H 0.526086 0.574227 0.088235 0.100 Uiso 1 1 calc R . . . .
C032 C 0.6220(9) 0.4202(6) 0.2963(8) 0.064(5) Uani 1 1 d . . . . .
H032 H 0.623024 0.403518 0.331541 0.077 Uiso 1 1 calc R . . . .
C033 C 0.3806(10) 0.7828(8) 0.2899(9) 0.077(2) Uani 1 1 d . U . . .
H033 H 0.389992 0.812028 0.273306 0.092 Uiso 1 1 calc R . . . .
C034 C 0.0823(6) 0.5785(4) 0.3090(6) 0.102(3) Uani 1 1 d D U . . .
H034 H 0.055733 0.552220 0.302372 0.122 Uiso 1 1 calc R . . . .
C035 C 0.5676(11) 0.8588(8) 0.5664(10) 0.089(7) Uani 1 1 d . . . . .
H03E H 0.599926 0.845934 0.591165 0.107 Uiso 1 1 calc R . . . .
H03F H 0.581960 0.886900 0.551268 0.107 Uiso 1 1 calc R . . . .
C036 C 0.4790(11) 0.2864(8) 0.2859(8) 0.085(7) Uani 1 1 d . . . . .
H03G H 0.478950 0.253660 0.289769 0.101 Uiso 1 1 calc R . . . .
H03H H 0.519995 0.296031 0.281572 0.101 Uiso 1 1 calc R . . . .
C037 C 0.3228(10) 0.5744(8) 0.1930(9) 0.084(3) Uani 1 1 d . U . . .
H03I H 0.323778 0.598348 0.165492 0.100 Uiso 1 1 calc R . . . .
H03J H 0.324205 0.588577 0.229518 0.100 Uiso 1 1 calc R . . . .
C038 C 0.3311(9) 0.6905(7) 0.2802(9) 0.075(2) Uani 1 1 d . U . . .
H03K H 0.318528 0.687237 0.240734 0.091 Uiso 1 1 calc R . . . .
H03L H 0.321945 0.662489 0.298826 0.091 Uiso 1 1 calc R . . . .
C039 C 0.2888(11) 0.7524(8) 0.6031(11) 0.093(7) Uani 1 1 d . . . . .
H03M H 0.284160 0.782797 0.587840 0.111 Uiso 1 1 calc R . . . .
H03N H 0.316442 0.754034 0.636554 0.111 Uiso 1 1 calc R . . . .
C03A C 0.3538(10) 0.3584(7) 0.2866(8) 0.075(6) Uani 1 1 d . . . . .
H03O H 0.328822 0.368832 0.254033 0.090 Uiso 1 1 calc R . . . .
H03P H 0.338234 0.371569 0.319391 0.090 Uiso 1 1 calc R . . . .
C03C C 0.3156(11) 0.4994(8) 0.1169(9) 0.084(3) Uani 1 1 d . U . . .
H03Q H 0.314196 0.487606 0.078766 0.101 Uiso 1 1 calc R . . . .
C03D C 0.6030(10) 0.4164(8) 0.1914(8) 0.079(6) Uani 1 1 d . . . . .
H03R H 0.590739 0.396071 0.160221 0.094 Uiso 1 1 calc R . . . .
C03E C 0.2687(13) 0.7203(9) 0.5086(10) 0.107(10) Uani 1 1 d . . . . .
H03S H 0.264708 0.750618 0.492862 0.129 Uiso 1 1 calc R . . . .
H03T H 0.283741 0.700669 0.480584 0.129 Uiso 1 1 calc R . . . .
C03F C 0.2349(11) 0.6863(8) 0.6401(9) 0.088(7) Uani 1 1 d . . . . .
H03U H 0.260853 0.686318 0.674652 0.105 Uiso 1 1 calc R . . . .
H03V H 0.195807 0.674706 0.648185 0.105 Uiso 1 1 calc R . . . .
C03G C 0.7159(7) 0.8172(6) 0.5167(8) 0.129(4) Uani 1 1 d D U . . .
H03W H 0.688393 0.803425 0.488008 0.155 Uiso 1 1 calc R . . . .
H03X H 0.701194 0.847325 0.524275 0.155 Uiso 1 1 calc R . . . .
C03H C 0.5442(12) 0.6650(9) 0.0749(8) 0.089(7) Uani 1 1 d . . . . .
H03Y H 0.514108 0.655244 0.045793 0.107 Uiso 1 1 calc R . . . .
HI H 0.566478 0.690101 0.060717 0.107 Uiso 1 1 calc R . . . .
C03I C 0.5852(12) 0.6276(8) 0.0904(8) 0.085(7) Uani 1 1 d . . . . .
H03Z H 0.603341 0.617685 0.056783 0.102 Uiso 1 1 calc R . . . .
C03J C 0.2981(10) 0.7291(7) 0.3039(9) 0.076(2) Uani 1 1 d . U . . .
H03 H 0.254585 0.723815 0.298033 0.091 Uiso 1 1 calc R . . . .
C03K C 0.2623(11) 0.5480(8) 0.1824(9) 0.085(3) Uani 1 1 d . U . . .
H9BA H 0.227286 0.567869 0.184240 0.102 Uiso 1 1 calc R . . . .
C03L C 0.7186(6) 0.7880(6) 0.5705(7) 0.128(4) Uani 1 1 d D U . . .
H0CA H 0.678230 0.786043 0.583421 0.154 Uiso 1 1 calc R . . . .
C03M C 0.1870(11) 0.7373(9) 0.5681(10) 0.099(8) Uani 1 1 d . . . . .
H1CA H 0.186211 0.768134 0.553754 0.119 Uiso 1 1 calc R . . . .
HJ H 0.146601 0.729590 0.576807 0.119 Uiso 1 1 calc R . . . .
C03N C 0.1343(7) 0.6290(5) 0.3829(4) 0.103(3) Uani 1 1 d D U . . .
H2CA H 0.140966 0.634673 0.423134 0.123 Uiso 1 1 calc R . . . .
C03O C 0.8982(9) 0.5440(7) 0.6583(8) 0.072(2) Uani 1 1 d . U . . .
H3CA H 0.888736 0.516250 0.677423 0.086 Uiso 1 1 calc R . . . .
HK H 0.934225 0.538550 0.639352 0.086 Uiso 1 1 calc R . . . .
C03P C 0.7910(12) 0.6642(9) 0.2532(11) 0.122(4) Uani 1 1 d D U . . .
H4CA H 0.760204 0.649952 0.227313 0.146 Uiso 1 1 calc R . . . .
C03Q C 0.3751(11) 0.5256(8) 0.1305(9) 0.084(3) Uani 1 1 d . U . . .
H5CA H 0.378394 0.549749 0.103562 0.101 Uiso 1 1 calc R . . . .
HL H 0.409069 0.505249 0.128431 0.101 Uiso 1 1 calc R . . . .
C03R C 0.4419(12) 0.3526(8) 0.2298(8) 0.082(6) Uani 1 1 d . . . . .
H6CA H 0.483179 0.361807 0.226286 0.098 Uiso 1 1 calc R . . . .
HM H 0.417300 0.362851 0.196935 0.098 Uiso 1 1 calc R . . . .
C03T C 0.3839(10) 0.7383(7) 0.3770(9) 0.076(2) Uani 1 1 d . U . . .
H7CA H 0.395035 0.739907 0.417272 0.092 Uiso 1 1 calc R . . . .
C03U C 0.7728(13) 0.7139(9) 0.2605(13) 0.123(4) Uani 1 1 d D U . . .
H8CA H 0.734428 0.715739 0.276527 0.148 Uiso 1 1 calc R . . . .
HN H 0.769146 0.729329 0.224703 0.148 Uiso 1 1 calc R . . . .
C03V C 0.8016(9) 0.7722(7) 0.4832(6) 0.130(4) Uani 1 1 d D U . . .
H9CA H 0.841219 0.773905 0.469597 0.156 Uiso 1 1 calc R . . . .
HO H 0.774218 0.758551 0.454332 0.156 Uiso 1 1 calc R . . . .
C03W C 0.6369(11) 0.6441(10) 0.1337(9) 0.091(7) Uani 1 1 d . . . . .
H0DA H 0.664695 0.619416 0.143433 0.109 Uiso 1 1 calc R . . . .
HP H 0.659119 0.668649 0.118100 0.109 Uiso 1 1 calc R . . . .
C03X C 0.2160(10) 0.6559(8) 0.5459(12) 0.097(8) Uani 1 1 d . . . . .
H1DA H 0.231221 0.636068 0.518084 0.116 Uiso 1 1 calc R . . . .
HQ H 0.177497 0.643991 0.554999 0.116 Uiso 1 1 calc R . . . .
C03Y C 0.1849(5) 0.6102(5) 0.2957(6) 0.102(3) Uani 1 1 d D U . . .
H2DA H 0.223643 0.604092 0.280831 0.123 Uiso 1 1 calc R . . . .
C03Z C 0.3737(11) 0.2841(8) 0.2379(10) 0.086(6) Uani 1 1 d . . . . .
H3DA H 0.372290 0.251328 0.241041 0.103 Uiso 1 1 calc R . . . .
HR H 0.348635 0.293191 0.204783 0.103 Uiso 1 1 calc R . . . .
C040 C 0.2072(10) 0.7037(10) 0.5216(10) 0.095(8) Uani 1 1 d . . . . .
H040 H 0.178450 0.703848 0.488308 0.114 Uiso 1 1 calc R . . . .
C041 C 0.3222(12) 0.4592(8) 0.1590(9) 0.086(3) Uani 1 1 d . U . . .
H04A H 0.360693 0.444240 0.156902 0.103 Uiso 1 1 calc R . . . .
H04B H 0.290400 0.437124 0.150236 0.103 Uiso 1 1 calc R . . . .
C042 C 0.3953(10) 0.7855(7) 0.3505(9) 0.079(2) Uani 1 1 d . U . . .
H04C H 0.370442 0.808307 0.366236 0.095 Uiso 1 1 calc R . . . .
H04D H 0.437216 0.794043 0.358549 0.095 Uiso 1 1 calc R . . . .
C043 C 0.2631(11) 0.5112(8) 0.2237(9) 0.084(3) Uani 1 1 d . U . . .
H04E H 0.226519 0.493454 0.217090 0.101 Uiso 1 1 calc R . . . .
H04F H 0.263576 0.524285 0.260725 0.101 Uiso 1 1 calc R . . . .
C044 C 0.1436(7) 0.5687(4) 0.2856(6) 0.102(3) Uani 1 1 d D U . . .
H04G H 0.162229 0.542323 0.304013 0.123 Uiso 1 1 calc R . . . .
H04H H 0.137365 0.562383 0.245960 0.123 Uiso 1 1 calc R . . . .
F045 F 0.9761(11) 0.7144(9) 0.4324(10) 0.174(5) Uani 1 1 d . U . . .
F046 F 0.9834(11) 0.6253(9) 0.4550(10) 0.175(5) Uani 1 1 d . U . . .
C048 C 0.8531(10) 0.5013(8) 0.3524(9) 0.080(2) Uani 1 1 d . U . . .
H04I H 0.868737 0.493410 0.317245 0.096 Uiso 1 1 calc R . . . .
H04J H 0.815259 0.517112 0.343949 0.096 Uiso 1 1 calc R . . . .
C049 C 0.0529(5) 0.6203(5) 0.2796(6) 0.103(3) Uani 1 1 d D U . . .
H04K H 0.014311 0.626292 0.293932 0.123 Uiso 1 1 calc R . . . .
H04L H 0.046030 0.614543 0.239903 0.123 Uiso 1 1 calc R . . . .
C04D C 0.9022(12) 0.6554(11) 0.3240(11) 0.123(4) Uani 1 1 d D U . . .
H04M H 0.934294 0.667075 0.350019 0.148 Uiso 1 1 calc R . . . .
H04N H 0.908979 0.623316 0.318410 0.148 Uiso 1 1 calc R . . . .
C04E C 0.4151(10) 0.7473(7) 0.2645(9) 0.077(2) Uani 1 1 d . U . . .
H04O H 0.457836 0.753783 0.271220 0.093 Uiso 1 1 calc R . . . .
H04P H 0.404846 0.746999 0.224499 0.093 Uiso 1 1 calc R . . . .
F04F F 1.0757(11) 0.6821(9) 0.4947(10) 0.175(5) Uani 1 1 d . U . . .
C04G C 0.7410(8) 0.7399(5) 0.5580(8) 0.129(4) Uani 1 1 d D U . . .
H04Q H 0.745230 0.723227 0.593355 0.155 Uiso 1 1 calc R . . . .
C04H C 0.1041(8) 0.6707(4) 0.3536(7) 0.104(3) Uani 1 1 d D U . . .
H04R H 0.129416 0.697246 0.360652 0.125 Uiso 1 1 calc R . . . .
H04S H 0.065597 0.676544 0.368193 0.125 Uiso 1 1 calc R . . . .
C04I C 0.8405(11) 0.6633(11) 0.3466(12) 0.124(4) Uani 1 1 d D U . . .
H04T H 0.842056 0.648465 0.383170 0.148 Uiso 1 1 calc R . . . .
F04J F 1.0013(11) 0.6514(9) 0.5635(10) 0.179(5) Uani 1 1 d . U . . .
C04K C 0.8958(10) 0.5318(8) 0.3833(9) 0.081(2) Uani 1 1 d . U . . .
H04U H 0.900603 0.559493 0.361547 0.097 Uiso 1 1 calc R . . . .
C04M C 0.8751(10) 0.5430(8) 0.4345(9) 0.081(2) Uani 1 1 d . U . . .
H04V H 0.838525 0.560763 0.427846 0.097 Uiso 1 1 calc R . . . .
H04W H 0.904990 0.561884 0.455007 0.097 Uiso 1 1 calc R . . . .
C04N C 0.8229(11) 0.7357(11) 0.2997(10) 0.124(4) Uani 1 1 d D U . . .
H04X H 0.813780 0.767781 0.305539 0.148 Uiso 1 1 calc R . . . .
F04P F 0.9973(11) 0.7342(9) 0.5318(10) 0.179(5) Uani 1 1 d . U . . .
C04Q C 0.8834(12) 0.7311(9) 0.2740(13) 0.124(4) Uani 1 1 d D U . . .
H04Y H 0.880357 0.745210 0.237452 0.148 Uiso 1 1 calc R . . . .
HS H 0.914558 0.746638 0.297327 0.148 Uiso 1 1 calc R . . . .
C04R C 0.8523(11) 0.6567(11) 0.2300(12) 0.124(4) Uani 1 1 d D U . . .
H04Z H 0.861170 0.624495 0.228603 0.148 Uiso 1 1 calc R . . . .
HT H 0.851601 0.668859 0.192510 0.148 Uiso 1 1 calc R . . . .
C04S C 0.1552(7) 0.6521(5) 0.2655(7) 0.103(3) Uani 1 1 d D U . . .
H04 H 0.181498 0.678234 0.270954 0.124 Uiso 1 1 calc R . . . .
HU H 0.148400 0.646173 0.225831 0.124 Uiso 1 1 calc R . . . .
C04T C 0.8043(8) 0.7429(5) 0.5365(8) 0.130(4) Uani 1 1 d D U . . .
H4DA H 0.818482 0.712343 0.528263 0.156 Uiso 1 1 calc R . . . .
C04U C 0.8312(15) 0.7110(11) 0.3558(11) 0.124(4) Uani 1 1 d D U . . .
H5DA H 0.865559 0.723476 0.378244 0.149 Uiso 1 1 calc R . . . .
HV H 0.795683 0.715215 0.375924 0.149 Uiso 1 1 calc R . . . .
C04V C 0.0946(7) 0.6616(4) 0.2900(6) 0.103(3) Uani 1 1 d D U . . .
H6DA H 0.075560 0.688197 0.271433 0.124 Uiso 1 1 calc R . . . .
C5 C 0.8480(7) 0.7650(6) 0.5825(8) 0.128(4) Uani 1 1 d D U . . .
H5A H 0.850012 0.746592 0.616021 0.153 Uiso 1 1 calc R . . . .
H5B H 0.888126 0.766796 0.569921 0.153 Uiso 1 1 calc R . . . .
C12 C 0.8232(8) 0.8422(5) 0.5422(8) 0.129(4) Uani 1 1 d D U . . .
H12A H 0.863157 0.844484 0.529405 0.155 Uiso 1 1 calc R . . . .
H12B H 0.809478 0.872581 0.550251 0.155 Uiso 1 1 calc R . . . .
C17 C 0.8253(7) 0.8129(6) 0.5952(6) 0.130(4) Uani 1 1 d D U . . .
H17 H 0.853055 0.826821 0.624188 0.156 Uiso 1 1 calc R . . . .
C18 C 0.7616(9) 0.8104(7) 0.6161(6) 0.130(4) Uani 1 1 d D U . . .
H18A H 0.762762 0.792704 0.650197 0.156 Uiso 1 1 calc R . . . .
H18B H 0.747438 0.840693 0.624036 0.156 Uiso 1 1 calc R . . . .
C19 C 0.7796(9) 0.8202(6) 0.4965(6) 0.130(4) Uani 1 1 d D U . . .
H19 H 0.778075 0.838838 0.462645 0.156 Uiso 1 1 calc R . . . .
Ag1 Ag 0.7475(6) 0.4880(5) 0.5464(4) 0.058(3) Uani 0.1 1 d . . P . .
Ag2 Ag 0.3233(3) 0.6197(3) 0.4403(3) 0.083(2) Uani 0.3 1 d . . P A 1


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag01 Ag02 3.0193(13) . ?
Ag01 Ag04 3.0583(14) 3_666 ?
Ag01 Ag08 3.1401(14) 3_666 ?
Ag01 Ag0E 3.1976(16) 3_666 ?
Ag01 Ag0F 2.9576(16) . ?
Ag01 S00 2.387(3) . ?
Ag01 S1 2.379(3) . ?
Ag02 Ag03 3.1958(15) . ?
Ag02 Ag04 3.0252(14) . ?
Ag02 Ag06 3.2467(15) . ?
Ag02 Ag08 2.9939(15) . ?
Ag02 Ag0B 3.2165(15) . ?
Ag02 S1 2.435(3) 3_666 ?
Ag02 S00O 2.439(4) . ?
Ag03 Ag04 3.1534(15) 3_666 ?
Ag03 Ag05 2.8897(14) . ?
Ag03 Ag06 2.9260(15) . ?
Ag03 Ag0B 2.9585(15) . ?
Ag03 Ag0D 2.9709(17) . ?
Ag03 S00 2.414(3) . ?
Ag03 S00M 2.398(4) . ?
Ag04 Ag05 3.3777(15) 3_666 ?
Ag04 Ag0D 3.1758(16) 3_666 ?
Ag04 Ag0E 2.9881(17) 3_666 ?
Ag04 S1 2.467(4) . ?
Ag04 S00P 2.441(4) . ?
Ag05 Ag09 3.1368(15) . ?
Ag05 Ag0C 3.0686(17) . ?
Ag05 Ag0D 2.9859(18) . ?
Ag05 S00 2.668(3) . ?
Ag05 S00P 2.554(4) 3_666 ?
Ag05 S00S 2.534(4) . ?
Ag06 Ag07 3.2559(16) . ?
Ag06 Ag0A 3.0058(16) . ?
Ag06 Ag0B 3.0303(17) . ?
Ag06 S00 2.623(3) . ?
Ag06 S00N 2.486(4) . ?
Ag06 S00O 2.539(4) . ?
Ag07 Ag09 3.0454(16) . ?
Ag07 Ag0G 3.274(2) . ?
Ag07 S00N 2.396(4) . ?
Ag07 S00Q 2.386(4) . ?
Ag07 S00Z 2.952(5) . ?
Ag08 Ag0H 3.079(2) . ?
Ag08 S00P 2.512(4) . ?
Ag08 S00T 2.582(4) 3_666 ?
Ag08 S00U 2.480(4) . ?
Ag09 S00Q 2.377(4) . ?
Ag09 S00S 2.383(4) . ?
Ag0A Ag0G 3.182(2) . ?
Ag0A S00V 2.382(4) . ?
Ag0A S00Z 2.382(5) . ?
Ag0B S00M 2.675(4) . ?
Ag0B S00N 2.480(4) . ?
Ag0B S00U 2.451(4) . ?
Ag0C Ag0G 3.1585(19) . ?
Ag0C S00T 2.389(4) . ?
Ag0C S00W 2.392(5) . ?
Ag0D S00M 2.845(4) . ?
Ag0D S00R 2.411(4) . ?
Ag0D S00S 2.432(4) . ?
Ag0D Ag2 3.278(6) . ?
Ag0E Ag 2.987(3) . ?
Ag0E S00O 2.533(4) 3_666 ?
Ag0E S00R 2.465(4) . ?
Ag0E S00V 2.540(4) 3_666 ?
Ag0F S00T 2.354(4) . ?
Ag0F S00V 2.352(5) . ?
Ag0F Ag1 1.197(15) . ?
Ag0G S00W 2.392(6) . ?
Ag0G S00Z 2.391(6) . ?
Ag0H Ag 3.000(3) . ?
Ag0H S00U 2.390(4) . ?
Ag0H S00X 2.346(6) . ?
Ag0H Ag1 3.129(12) 3_666 ?
Ag0H Ag2 2.913(6) . ?
Ag S00R 2.437(4) . ?
Ag S00X 2.306(6) . ?
Ag Ag1 2.897(14) 3_666 ?
Sb0J F02X 1.94(2) . ?
Sb0J F045 1.86(2) . ?
Sb0J F046 1.90(2) . ?
Sb0J F04F 1.94(2) . ?
Sb0J F04J 1.81(2) . ?
Sb0J F04P 1.81(3) . ?
S00M C012 1.85(2) . ?
S00M Ag2 2.628(7) . ?
S00N C01B 1.865(15) . ?
S00O C02F 1.865(15) . ?
S00P C01F 1.875(17) . ?
S00Q C011 1.849(14) . ?
S00R C010 1.829(16) . ?
S00R Ag2 2.581(7) . ?
S00S C018 1.873(16) . ?
S00T C015 1.832(19) . ?
S00T Ag1 2.732(15) . ?
S00U C01A 1.82(2) . ?
S00V C01T 1.83(2) . ?
S00V Ag1 2.725(12) . ?
S00W C04G 1.790(17) . ?
S00X C02W 1.900(15) . ?
S00X Ag1 2.185(16) 3_666 ?
S00X Ag2 2.590(7) . ?
S00Z C028 1.90(3) . ?
C010 C01D 1.48(3) . ?
C010 C01Q 1.53(3) . ?
C011 C013 1.53(2) . ?
C011 C014 1.51(2) . ?
C012 C02B 1.55(3) . ?
C012 C03T 1.50(3) . ?
C013 C01C 1.55(2) . ?
C013 C01E 1.52(2) . ?
C014 C01N 1.54(2) . ?
C014 C02G 1.51(3) . ?
C015 C017 1.52(3) . ?
C015 C02P 1.50(3) . ?
C016 C019 1.51(3) . ?
C016 C022 1.52(3) . ?
C016 C02C 1.50(3) . ?
C017 C01K 1.47(3) . ?
C017 C030 1.50(3) . ?
C018 C01U 1.58(2) . ?
C018 C024 1.52(3) . ?
C019 C024 1.45(3) . ?
C01A C01P 1.51(3) . ?
C01A C01Y 1.55(3) . ?
C01B C01L 1.50(3) . ?
C01B C025 1.52(2) . ?
C01C C01I 1.56(2) . ?
C01D C03F 1.49(3) . ?
C01D C03X 1.56(3) . ?
C01E C01V 1.55(3) . ?
C01F C01G 1.55(2) . ?
C01F C01Z 1.54(3) . ?
C01G C03A 1.54(3) . ?
C01G C03R 1.55(3) . ?
C01H C01R 1.57(3) . ?
C01H C01X 1.51(3) . ?
C01I C01N 1.42(3) . ?
C01I C02D 1.61(3) . ?
C01J C023 1.52(3) . ?
C01J C029 1.53(3) . ?
C01K C02O 1.60(3) . ?
C01L C01M 1.51(3) . ?
C01L C031 1.51(3) . ?
C01M C02H 1.56(3) . ?
C01O C033 1.53(3) . ?
C01O C03J 1.51(3) . ?
C01P C037 1.45(3) . ?
C01P C03Q 1.56(3) . ?
C01Q C039 1.53(3) . ?
C01Q C03E 1.56(3) . ?
C01R C02Q 1.50(3) . ?
C01R C02Y 1.50(3) . ?
C01S C026 1.46(3) . ?
C01S C02C 1.51(3) . ?
C01S C035 1.53(3) . ?
C01T C01X 1.48(3) . ?
C01T C02E 1.55(3) . ?
C01U C022 1.49(2) . ?
C01U C035 1.56(2) . ?
C01V C02D 1.45(3) . ?
C01V C02G 1.54(3) . ?
C01W C025 1.53(3) . ?
C01W C02H 1.48(3) . ?
C01X C048 1.48(3) . ?
C01Y C041 1.64(3) . ?
C01Y C043 1.53(3) . ?
C01Z C027 1.59(3) . ?
C01Z C036 1.51(3) . ?
C020 C023 1.50(3) . ?
C020 C032 1.52(3) . ?
C021 C02N 1.46(3) . ?
C021 C030 1.52(3) . ?
C021 C03O 1.43(3) . ?
C023 C02A 1.56(3) . ?
C024 C026 1.51(3) . ?
C025 C03W 1.55(3) . ?
C027 C02K 1.55(3) . ?
C028 C03P 1.539(10) . ?
C028 C04I 1.535(10) . ?
C029 C02F 1.49(2) . ?
C029 C02T 1.55(3) . ?
C02A C03D 1.50(3) . ?
C02B C038 1.60(3) . ?
C02B C04E 1.54(3) . ?
C02E C02Y 1.54(3) . ?
C02E C04M 1.49(3) . ?
C02F C032 1.52(2) . ?
C02H C03H 1.51(3) . ?
C02I C02O 1.51(3) . ?
C02I C02P 1.41(3) . ?
C02J C036 1.52(3) . ?
C02J C03R 1.56(3) . ?
C02J C03Z 1.52(3) . ?
C02K C03A 1.54(3) . ?
C02K C03Z 1.54(3) . ?
C02L C034 1.541(7) . ?
C02L C03N 1.544(8) . ?
C02M C039 1.53(3) . ?
C02M C03F 1.53(3) . ?
C02M C03M 1.45(3) . ?
C02N C02O 1.56(3) . ?
C02P C03O 1.50(3) . ?
C02Q C04K 1.54(3) . ?
C02R C03C 1.40(3) . ?
C02R C03K 1.58(3) . ?
C02S C032 1.50(3) . ?
C02S C03D 1.57(3) . ?
C02T C03D 1.57(3) . ?
C02U C04D 1.530(10) . ?
C02U C04Q 1.534(10) . ?
C02U C04R 1.532(10) . ?
C02V C03J 1.54(3) . ?
C02V C03T 1.49(3) . ?
C02W C03N 1.550(8) . ?
C02W C03Y 1.543(8) . ?
C031 C03I 1.51(3) . ?
C033 C042 1.47(3) . ?
C033 C04E 1.46(3) . ?
C034 C044 1.549(8) . ?
C034 C049 1.536(8) . ?
C037 C03K 1.56(3) . ?
C038 C03J 1.50(3) . ?
C03C C03Q 1.54(3) . ?
C03C C041 1.56(3) . ?
C03E C040 1.51(4) . ?
C03G C03L 1.549(8) . ?
C03G C19 1.543(12) . ?
C03H C03I 1.46(3) . ?
C03I C03W 1.56(3) . ?
C03K C043 1.47(3) . ?
C03L C04G 1.543(8) . ?
C03L C18 1.540(8) . ?
C03M C040 1.59(3) . ?
C03N C04H 1.543(8) . ?
C03P C03U 1.535(10) . ?
C03P C04R 1.536(10) . ?
C03T C042 1.56(3) . ?
C03U C04N 1.537(10) . ?
C03V C04T 1.544(8) . ?
C03V C19 1.540(8) . ?
C03X C040 1.53(4) . ?
C03Y C044 1.537(8) . ?
C03Y C04S 1.549(8) . ?
C048 C04K 1.46(3) . ?
C049 C04V 1.538(8) . ?
C04D C04I 1.538(10) . ?
C04G C04T 1.545(8) . ?
C04H C04V 1.550(9) . ?
C04I C04U 1.44(4) . ?
C04K C04M 1.39(3) . ?
C04N C04Q 1.537(10) . ?
C04N C04U 1.531(10) . ?
C04S C04V 1.546(9) . ?
C04T C5 1.552(8) . ?
C5 C17 1.540(8) . ?
C12 C17 1.537(8) . ?
C12 C19 1.545(8) . ?
C17 C18 1.550(8) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Ag02 Ag01 Ag04 76.21(3) . 3_666 ?
Ag02 Ag01 Ag08 143.04(4) . 3_666 ?
Ag02 Ag01 Ag0E 76.08(4) . 3_666 ?
Ag04 Ag01 Ag08 73.06(4) 3_666 3_666 ?
Ag04 Ag01 Ag0E 145.50(5) 3_666 3_666 ?
Ag08 Ag01 Ag0E 121.71(4) 3_666 3_666 ?
Ag0F Ag01 Ag02 138.42(5) . . ?
Ag0F Ag01 Ag04 144.43(5) . 3_666 ?
Ag0F Ag01 Ag08 76.41(4) . 3_666 ?
Ag0F Ag01 Ag0E 67.98(4) . 3_666 ?
S00 Ag01 Ag02 87.54(8) . . ?
S00 Ag01 Ag04 86.99(9) . 3_666 ?
S00 Ag01 Ag08 110.60(8) . 3_666 ?
S00 Ag01 Ag0E 111.87(9) . 3_666 ?
S00 Ag01 Ag0F 87.02(9) . . ?
S1 Ag01 Ag02 94.40(9) . . ?
S1 Ag01 Ag04 97.99(9) . 3_666 ?
S1 Ag01 Ag08 70.39(9) . 3_666 ?
S1 Ag01 Ag0E 64.23(9) . 3_666 ?
S1 Ag01 Ag0F 88.44(9) . . ?
S1 Ag01 S00 174.95(12) . . ?
Ag01 Ag02 Ag03 71.02(3) . . ?
Ag01 Ag02 Ag04 73.90(3) . . ?
Ag01 Ag02 Ag06 76.70(3) . . ?
Ag01 Ag02 Ag0B 121.87(4) . . ?
Ag03 Ag02 Ag06 54.02(3) . . ?
Ag03 Ag02 Ag0B 54.95(3) . . ?
Ag04 Ag02 Ag03 142.00(4) . . ?
Ag04 Ag02 Ag06 129.70(4) . . ?
Ag04 Ag02 Ag0B 163.04(5) . . ?
Ag08 Ag02 Ag01 143.25(4) . . ?
Ag08 Ag02 Ag03 128.68(4) . . ?
Ag08 Ag02 Ag04 75.62(4) . . ?
Ag08 Ag02 Ag06 139.75(4) . . ?
Ag08 Ag02 Ag0B 91.43(4) . . ?
Ag0B Ag02 Ag06 55.92(3) . . ?
S1 Ag02 Ag01 91.70(9) 3_666 . ?
S1 Ag02 Ag03 69.58(9) 3_666 . ?
S1 Ag02 Ag04 97.62(9) 3_666 . ?
S1 Ag02 Ag06 123.28(9) 3_666 . ?
S1 Ag02 Ag08 72.48(9) 3_666 . ?
S1 Ag02 Ag0B 88.63(9) 3_666 . ?
S1 Ag02 S00O 169.95(13) 3_666 . ?
S00O Ag02 Ag01 79.22(9) . . ?
S00O Ag02 Ag03 103.03(10) . . ?
S00O Ag02 Ag04 84.09(10) . . ?
S00O Ag02 Ag06 50.65(9) . . ?
S00O Ag02 Ag08 117.45(9) . . ?
S00O Ag02 Ag0B 92.51(9) . . ?
Ag04 Ag03 Ag02 72.42(3) 3_666 . ?
Ag05 Ag03 Ag02 126.83(4) . . ?
Ag05 Ag03 Ag04 67.80(4) . 3_666 ?
Ag05 Ag03 Ag06 113.55(5) . . ?
Ag05 Ag03 Ag0B 167.77(5) . . ?
Ag05 Ag03 Ag0D 61.24(4) . . ?
Ag06 Ag03 Ag02 63.88(4) . . ?
Ag06 Ag03 Ag04 123.88(4) . 3_666 ?
Ag06 Ag03 Ag0B 61.99(4) . . ?
Ag06 Ag03 Ag0D 170.91(5) . . ?
Ag0B Ag03 Ag02 62.88(4) . . ?
Ag0B Ag03 Ag04 124.39(5) . 3_666 ?
Ag0B Ag03 Ag0D 121.37(5) . . ?
Ag0D Ag03 Ag02 125.16(5) . . ?
Ag0D Ag03 Ag04 62.39(4) . 3_666 ?
S00 Ag03 Ag02 83.12(8) . . ?
S00 Ag03 Ag04 84.38(8) . 3_666 ?
S00 Ag03 Ag05 59.61(8) . . ?
S00 Ag03 Ag06 57.89(8) . . ?
S00 Ag03 Ag0B 119.18(9) . . ?
S00 Ag03 Ag0D 119.44(9) . . ?
S00M Ag03 Ag02 100.74(9) . . ?
S00M Ag03 Ag04 102.13(9) . 3_666 ?
S00M Ag03 Ag05 120.73(10) . . ?
S00M Ag03 Ag06 118.64(10) . . ?
S00M Ag03 Ag0B 58.82(9) . . ?
S00M Ag03 Ag0D 62.93(10) . . ?
S00M Ag03 S00 173.16(12) . . ?
Ag01 Ag04 Ag03 71.10(3) 3_666 3_666 ?
Ag01 Ag04 Ag05 77.37(4) 3_666 3_666 ?
Ag01 Ag04 Ag0D 122.55(4) 3_666 3_666 ?
Ag02 Ag04 Ag01 69.83(3) . 3_666 ?
Ag02 Ag04 Ag03 136.86(5) . 3_666 ?
Ag02 Ag04 Ag05 132.05(4) . 3_666 ?
Ag02 Ag04 Ag0D 167.01(5) . 3_666 ?
Ag03 Ag04 Ag05 52.38(3) 3_666 3_666 ?
Ag03 Ag04 Ag0D 55.99(4) 3_666 3_666 ?
Ag0D Ag04 Ag05 54.10(3) 3_666 3_666 ?
Ag0E Ag04 Ag01 140.68(5) 3_666 3_666 ?
Ag0E Ag04 Ag02 79.21(4) 3_666 . ?
Ag0E Ag04 Ag03 124.04(5) 3_666 3_666 ?
Ag0E Ag04 Ag05 141.76(5) 3_666 3_666 ?
Ag0E Ag04 Ag0D 90.96(4) 3_666 3_666 ?
S1 Ag04 Ag01 90.16(9) . 3_666 ?
S1 Ag04 Ag02 92.45(9) . . ?
S1 Ag04 Ag03 70.02(8) . 3_666 ?
S1 Ag04 Ag05 122.15(9) . 3_666 ?
S1 Ag04 Ag0D 91.48(9) . 3_666 ?
S1 Ag04 Ag0E 67.06(9) . 3_666 ?
S00P Ag04 Ag01 79.80(9) . 3_666 ?
S00P Ag04 Ag02 90.72(9) . . ?
S00P Ag04 Ag03 99.77(9) . 3_666 ?
S00P Ag04 Ag05 48.88(9) . 3_666 ?
S00P Ag04 Ag0D 88.04(9) . 3_666 ?
S00P Ag04 Ag0E 125.22(10) . 3_666 ?
S00P Ag04 S1 167.72(12) . . ?
Ag03 Ag05 Ag04 59.82(3) . 3_666 ?
Ag03 Ag05 Ag09 81.25(4) . . ?
Ag03 Ag05 Ag0C 114.29(5) . . ?
Ag03 Ag05 Ag0D 60.72(4) . . ?
Ag09 Ag05 Ag04 138.21(4) . 3_666 ?
Ag0C Ag05 Ag04 107.21(4) . 3_666 ?
Ag0C Ag05 Ag09 102.02(5) . . ?
Ag0D Ag05 Ag04 59.50(4) . 3_666 ?
Ag0D Ag05 Ag09 89.61(4) . . ?
Ag0D Ag05 Ag0C 166.71(5) . . ?
S00 Ag05 Ag03 51.31(7) . . ?
S00 Ag05 Ag04 76.38(8) . 3_666 ?
S00 Ag05 Ag09 91.54(8) . . ?
S00 Ag05 Ag0C 62.98(8) . . ?
S00 Ag05 Ag0D 110.85(8) . . ?
S00P Ag05 Ag03 104.28(9) 3_666 . ?
S00P Ag05 Ag04 46.05(8) 3_666 3_666 ?
S00P Ag05 Ag09 173.56(9) 3_666 . ?
S00P Ag05 Ag0C 78.88(9) 3_666 . ?
S00P Ag05 Ag0D 90.28(9) 3_666 . ?
S00P Ag05 S00 94.52(11) 3_666 . ?
S00S Ag05 Ag03 87.49(9) . . ?
S00S Ag05 Ag04 110.94(10) . 3_666 ?
S00S Ag05 Ag09 48.27(9) . . ?
S00S Ag05 Ag0C 141.77(10) . . ?
S00S Ag05 Ag0D 51.49(9) . . ?
S00S Ag05 S00 128.92(12) . . ?
S00S Ag05 S00P 127.84(13) . 3_666 ?
Ag02 Ag06 Ag07 138.93(5) . . ?
Ag03 Ag06 Ag02 62.10(3) . . ?
Ag03 Ag06 Ag07 78.95(4) . . ?
Ag03 Ag06 Ag0A 118.38(5) . . ?
Ag03 Ag06 Ag0B 59.53(4) . . ?
Ag0A Ag06 Ag02 113.67(4) . . ?
Ag0A Ag06 Ag07 95.35(5) . . ?
Ag0A Ag06 Ag0B 175.18(5) . . ?
Ag0B Ag06 Ag02 61.54(3) . . ?
Ag0B Ag06 Ag07 88.53(4) . . ?
S00 Ag06 Ag02 79.08(8) . . ?
S00 Ag06 Ag03 51.23(8) . . ?
S00 Ag06 Ag07 86.82(8) . . ?
S00 Ag06 Ag0A 67.29(8) . . ?
S00 Ag06 Ag0B 110.18(9) . . ?
S00N Ag06 Ag02 113.78(10) . . ?
S00N Ag06 Ag03 86.03(9) . . ?
S00N Ag06 Ag07 47.00(9) . . ?
S00N Ag06 Ag0A 132.50(10) . . ?
S00N Ag06 Ag0B 52.32(9) . . ?
S00N Ag06 S00 124.58(12) . . ?
S00N Ag06 S00O 131.80(12) . . ?
S00O Ag06 Ag02 47.96(8) . . ?
S00O Ag06 Ag03 108.30(9) . . ?
S00O Ag06 Ag07 172.74(9) . . ?
S00O Ag06 Ag0A 81.43(9) . . ?
S00O Ag06 Ag0B 95.04(9) . . ?
S00O Ag06 S00 97.84(11) . . ?
Ag06 Ag07 Ag0G 76.85(4) . . ?
Ag09 Ag07 Ag06 107.82(4) . . ?
Ag09 Ag07 Ag0G 66.12(4) . . ?
S00N Ag07 Ag06 49.36(9) . . ?
S00N Ag07 Ag09 128.01(10) . . ?
S00N Ag07 Ag0G 126.05(10) . . ?
S00N Ag07 S00Z 97.97(15) . . ?
S00Q Ag07 Ag06 147.95(10) . . ?
S00Q Ag07 Ag09 50.11(10) . . ?
S00Q Ag07 Ag0G 72.68(10) . . ?
S00Q Ag07 S00N 160.55(14) . . ?
S00Q Ag07 S00Z 100.18(15) . . ?
S00Z Ag07 Ag06 63.05(10) . . ?
S00Z Ag07 Ag09 110.91(12) . . ?
S00Z Ag07 Ag0G 44.79(12) . . ?
Ag02 Ag08 Ag01 69.13(3) . 3_666 ?
Ag02 Ag08 Ag0H 88.41(5) . . ?
Ag0H Ag08 Ag01 95.17(5) . 3_666 ?
S00P Ag08 Ag01 77.17(8) . 3_666 ?
S00P Ag08 Ag02 90.08(9) . . ?
S00P Ag08 Ag0H 172.22(10) . . ?
S00P Ag08 S00T 96.96(13) . 3_666 ?
S00T Ag08 Ag01 80.34(9) 3_666 3_666 ?
S00T Ag08 Ag02 146.27(10) 3_666 . ?
S00T Ag08 Ag0H 80.21(10) 3_666 . ?
S00U Ag08 Ag01 125.73(10) . 3_666 ?
S00U Ag08 Ag02 70.22(9) . . ?
S00U Ag08 Ag0H 49.49(11) . . ?
S00U Ag08 S00P 136.62(14) . . ?
S00U Ag08 S00T 121.10(14) . 3_666 ?
Ag07 Ag09 Ag05 105.09(4) . . ?
S00Q Ag09 Ag05 143.18(11) . . ?
S00Q Ag09 Ag07 50.39(9) . . ?
S00Q Ag09 S00S 163.62(14) . . ?
S00S Ag09 Ag05 52.52(9) . . ?
S00S Ag09 Ag07 131.49(10) . . ?
Ag06 Ag0A Ag0G 81.91(5) . . ?
S00V Ag0A Ag06 114.15(11) . . ?
S00V Ag0A Ag0G 140.57(13) . . ?
S00Z Ag0A Ag06 73.35(12) . . ?
S00Z Ag0A Ag0G 48.30(14) . . ?
S00Z Ag0A S00V 167.19(16) . . ?
Ag03 Ag0B Ag02 62.17(3) . . ?
Ag03 Ag0B Ag06 58.48(4) . . ?
Ag06 Ag0B Ag02 62.55(4) . . ?
S00M Ag0B Ag02 94.39(8) . . ?
S00M Ag0B Ag03 50.08(8) . . ?
S00M Ag0B Ag06 106.86(8) . . ?
S00N Ag0B Ag02 114.95(10) . . ?
S00N Ag0B Ag03 85.43(9) . . ?
S00N Ag0B Ag06 52.48(9) . . ?
S00N Ag0B S00M 105.73(12) . . ?
S00U Ag0B Ag02 66.58(9) . . ?
S00U Ag0B Ag03 120.59(9) . . ?
S00U Ag0B Ag06 118.51(11) . . ?
S00U Ag0B S00M 109.21(13) . . ?
S00U Ag0B S00N 144.81(14) . . ?
Ag05 Ag0C Ag0G 79.81(4) . . ?
S00T Ag0C Ag05 118.60(10) . . ?
S00T Ag0C Ag0G 140.05(12) . . ?
S00T Ag0C S00W 169.70(15) . . ?
S00W Ag0C Ag05 64.54(13) . . ?
S00W Ag0C Ag0G 48.69(13) . . ?
Ag03 Ag0D Ag04 61.63(4) . 3_666 ?
Ag03 Ag0D Ag05 58.04(4) . . ?
Ag03 Ag0D Ag2 85.28(11) . . ?
Ag04 Ag0D Ag2 82.26(17) 3_666 . ?
Ag05 Ag0D Ag04 66.40(4) . 3_666 ?
Ag05 Ag0D Ag2 139.61(14) . . ?
S00M Ag0D Ag03 48.65(8) . . ?
S00M Ag0D Ag04 92.21(8) . 3_666 ?
S00M Ag0D Ag05 104.24(8) . . ?
S00M Ag0D Ag2 50.22(13) . . ?
S00R Ag0D Ag03 116.39(10) . . ?
S00R Ag0D Ag04 67.83(9) . 3_666 ?
S00R Ag0D Ag05 128.12(11) . . ?
S00R Ag0D S00M 100.57(13) . . ?
S00R Ag0D S00S 153.86(14) . . ?
S00R Ag0D Ag2 51.23(16) . . ?
S00S Ag0D Ag03 87.58(10) . . ?
S00S Ag0D Ag04 120.96(10) . 3_666 ?
S00S Ag0D Ag05 54.62(10) . . ?
S00S Ag0D S00M 103.43(12) . . ?
S00S Ag0D Ag2 148.02(19) . . ?
Ag04 Ag0E Ag01 71.85(4) 3_666 3_666 ?
S00O Ag0E Ag01 74.50(9) 3_666 3_666 ?
S00O Ag0E Ag04 83.31(9) 3_666 3_666 ?
S00O Ag0E Ag 167.22(11) 3_666 . ?
S00O Ag0E S00V 92.75(13) 3_666 3_666 ?
S00R Ag0E Ag01 128.47(10) . 3_666 ?
S00R Ag0E Ag04 70.63(9) . 3_666 ?
S00R Ag0E Ag 52.04(11) . . ?
S00R Ag0E S00O 132.91(14) . 3_666 ?
S00R Ag0E S00V 125.39(14) . 3_666 ?
S00V Ag0E Ag01 85.62(11) 3_666 3_666 ?
S00V Ag0E Ag04 157.39(11) 3_666 3_666 ?
S00V Ag0E Ag 90.75(12) 3_666 . ?
S00T Ag0F Ag01 88.01(10) . . ?
S00V Ag0F Ag01 94.78(11) . . ?
S00V Ag0F S00T 166.40(17) . . ?
Ag1 Ag0F Ag01 122.6(6) . . ?
Ag1 Ag0F S00T 95.0(6) . . ?
Ag1 Ag0F S00V 94.7(6) . . ?
Ag0A Ag0G Ag07 91.69(5) . . ?
Ag0C Ag0G Ag07 131.47(6) . . ?
Ag0C Ag0G Ag0A 85.96(5) . . ?
S00W Ag0G Ag07 112.70(12) . . ?
S00W Ag0G Ag0A 134.25(12) . . ?
S00W Ag0G Ag0C 48.68(11) . . ?
S00Z Ag0G Ag07 60.46(11) . . ?
S00Z Ag0G Ag0A 48.05(12) . . ?
S00Z Ag0G Ag0C 133.97(13) . . ?
S00Z Ag0G S00W 173.04(17) . . ?
Ag08 Ag0H Ag1 80.7(3) . 3_666 ?
Ag Ag0H Ag08 112.15(8) . . ?
Ag Ag0H Ag1 56.4(2) . 3_666 ?
S00U Ag0H Ag08 52.08(10) . . ?
S00U Ag0H Ag 136.06(12) . . ?
S00U Ag0H Ag1 132.8(3) . 3_666 ?
S00U Ag0H Ag2 128.45(15) . . ?
S00X Ag0H Ag08 124.40(14) . . ?
S00X Ag0H Ag 49.27(15) . . ?
S00X Ag0H S00U 173.45(17) . . ?
S00X Ag0H Ag1 44.2(3) . 3_666 ?
S00X Ag0H Ag2 57.80(17) . . ?
Ag2 Ag0H Ag08 120.98(19) . . ?
Ag2 Ag0H Ag1 72.3(3) . 3_666 ?
Ag0E Ag Ag0H 117.21(9) . . ?
S00R Ag Ag0E 52.88(10) . . ?
S00R Ag Ag0H 146.98(15) . . ?
S00R Ag Ag1 127.4(3) . 3_666 ?
S00X Ag Ag0E 123.37(18) . . ?
S00X Ag Ag0H 50.43(16) . . ?
S00X Ag S00R 162.3(2) . . ?
S00X Ag Ag1 48.0(3) . 3_666 ?
Ag1 Ag Ag0E 76.0(3) 3_666 . ?
Ag1 Ag Ag0H 64.1(2) 3_666 . ?
F045 Sb0J F02X 85.5(10) . . ?
F045 Sb0J F046 91.2(11) . . ?
F045 Sb0J F04F 92.3(10) . . ?
F046 Sb0J F02X 84.8(10) . . ?
F046 Sb0J F04F 91.9(11) . . ?
F04F Sb0J F02X 176.0(10) . . ?
F04J Sb0J F02X 94.4(10) . . ?
F04J Sb0J F045 174.4(12) . . ?
F04J Sb0J F046 94.4(11) . . ?
F04J Sb0J F04F 88.2(11) . . ?
F04J Sb0J F04P 89.9(11) . . ?
F04P Sb0J F02X 97.6(11) . . ?
F04P Sb0J F045 84.5(11) . . ?
F04P Sb0J F046 174.9(11) . . ?
F04P Sb0J F04F 85.5(11) . . ?
Ag01 S00 Ag03 97.61(12) . . ?
Ag01 S00 Ag05 105.62(12) . . ?
Ag01 S00 Ag06 101.84(12) . . ?
Ag03 S00 Ag05 69.09(9) . . ?
Ag03 S00 Ag06 70.88(9) . . ?
Ag06 S00 Ag05 133.67(14) . . ?
Ag01 S1 Ag02 92.64(12) . 3_666 ?
Ag01 S1 Ag04 97.12(12) . . ?
Ag02 S1 Ag04 99.83(13) 3_666 . ?
Ag03 S00M Ag0B 71.10(10) . . ?
Ag03 S00M Ag0D 68.42(9) . . ?
Ag03 S00M Ag2 114.9(2) . . ?
Ag0B S00M Ag0D 138.95(14) . . ?
C012 S00M Ag03 110.0(7) . . ?
C012 S00M Ag0B 102.1(7) . . ?
C012 S00M Ag0D 97.7(7) . . ?
C012 S00M Ag2 126.0(7) . . ?
Ag2 S00M Ag0B 119.5(2) . . ?
Ag2 S00M Ag0D 73.47(15) . . ?
Ag07 S00N Ag06 83.64(12) . . ?
Ag07 S00N Ag0B 128.40(15) . . ?
Ag0B S00N Ag06 75.21(10) . . ?
C01B S00N Ag06 108.7(5) . . ?
C01B S00N Ag07 106.7(6) . . ?
C01B S00N Ag0B 124.5(6) . . ?
Ag02 S00O Ag06 81.39(11) . . ?
Ag02 S00O Ag0E 100.88(13) . 3_666 ?
Ag0E S00O Ag06 128.10(15) 3_666 . ?
C02F S00O Ag02 115.7(6) . . ?
C02F S00O Ag06 118.5(6) . . ?
C02F S00O Ag0E 107.1(5) . 3_666 ?
Ag04 S00P Ag05 85.07(11) . 3_666 ?
Ag04 S00P Ag08 96.33(13) . . ?
Ag08 S00P Ag05 129.75(15) . 3_666 ?
C01F S00P Ag04 119.5(6) . . ?
C01F S00P Ag05 115.0(6) . 3_666 ?
C01F S00P Ag08 107.7(5) . . ?
Ag09 S00Q Ag07 79.49(12) . . ?
C011 S00Q Ag07 103.5(5) . . ?
C011 S00Q Ag09 106.2(5) . . ?
Ag0D S00R Ag0E 128.79(15) . . ?
Ag0D S00R Ag 99.71(16) . . ?
Ag0D S00R Ag2 82.01(19) . . ?
Ag0E S00R Ag2 91.2(2) . . ?
Ag S00R Ag0E 75.08(13) . . ?
C010 S00R Ag0D 111.9(6) . . ?
C010 S00R Ag0E 115.4(6) . . ?
C010 S00R Ag 117.4(6) . . ?
C010 S00R Ag2 119.3(6) . . ?
Ag09 S00S Ag05 79.21(12) . . ?
Ag09 S00S Ag0D 127.39(16) . . ?
Ag0D S00S Ag05 73.89(11) . . ?
C018 S00S Ag05 109.8(6) . . ?
C018 S00S Ag09 109.0(6) . . ?
C018 S00S Ag0D 122.4(6) . . ?
Ag08 S00T Ag1 98.3(3) 3_666 . ?
Ag0C S00T Ag08 106.16(14) . 3_666 ?
Ag0C S00T Ag1 117.0(3) . . ?
Ag0F S00T Ag08 99.62(14) . 3_666 ?
Ag0F S00T Ag0C 92.17(15) . . ?
Ag0F S00T Ag1 25.9(3) . . ?
C015 S00T Ag08 126.7(7) . 3_666 ?
C015 S00T Ag0C 117.0(7) . . ?
C015 S00T Ag0F 108.1(7) . . ?
C015 S00T Ag1 89.1(7) . . ?
Ag0B S00U Ag08 128.88(15) . . ?
Ag0H S00U Ag08 78.43(13) . . ?
Ag0H S00U Ag0B 95.87(15) . . ?
C01A S00U Ag08 114.5(7) . . ?
C01A S00U Ag0B 112.9(7) . . ?
C01A S00U Ag0H 117.6(8) . . ?
Ag0A S00V Ag0E 111.51(15) . 3_666 ?
Ag0A S00V Ag1 116.3(4) . . ?
Ag0E S00V Ag1 86.9(3) 3_666 . ?
Ag0F S00V Ag0A 91.30(16) . . ?
Ag0F S00V Ag0E 89.51(14) . 3_666 ?
Ag0F S00V Ag1 26.0(3) . . ?
C01T S00V Ag0A 116.8(8) . . ?
C01T S00V Ag0E 128.3(8) . 3_666 ?
C01T S00V Ag0F 106.5(7) . . ?
C01T S00V Ag1 87.9(8) . . ?
Ag0C S00W Ag0G 82.63(16) . . ?
C04G S00W Ag0C 102.5(6) . . ?
C04G S00W Ag0G 131.7(7) . . ?
Ag0H S00X Ag2 72.14(18) . . ?
Ag S00X Ag0H 80.30(17) . . ?
C02W S00X Ag0H 106.3(5) . . ?
C02W S00X Ag 107.8(5) . . ?
C02W S00X Ag1 165.0(6) . 3_666 ?
C02W S00X Ag2 93.9(5) . . ?
Ag1 S00X Ag0H 87.3(4) 3_666 . ?
Ag1 S00X Ag 80.3(4) 3_666 . ?
Ag1 S00X Ag2 96.4(4) 3_666 . ?
Ag0A S00Z Ag07 120.19(17) . . ?
Ag0A S00Z Ag0G 83.64(16) . . ?
Ag0G S00Z Ag07 74.75(14) . . ?
C028 S00Z Ag07 132.6(9) . . ?
C028 S00Z Ag0A 107.1(9) . . ?
C028 S00Z Ag0G 116.3(8) . . ?
C01D C010 S00R 115.5(13) . . ?
C01D C010 C01Q 113.0(14) . . ?
C01Q C010 S00R 112.0(12) . . ?
C013 C011 S00Q 111.4(10) . . ?
C014 C011 S00Q 109.6(11) . . ?
C014 C011 C013 110.7(12) . . ?
C02B C012 S00M 111.5(15) . . ?
C03T C012 S00M 112.2(15) . . ?
C03T C012 C02B 107.7(16) . . ?
C011 C013 C01C 109.3(13) . . ?
C01E C013 C011 110.3(14) . . ?
C01E C013 C01C 108.3(14) . . ?
C011 C014 C01N 106.6(13) . . ?
C02G C014 C011 110.8(13) . . ?
C02G C014 C01N 107.1(15) . . ?
C017 C015 S00T 113.2(14) . . ?
C02P C015 S00T 117.5(14) . . ?
C02P C015 C017 107.2(16) . . ?
C019 C016 C022 108.2(16) . . ?
C02C C016 C019 107.4(15) . . ?
C02C C016 C022 109.9(18) . . ?
C01K C017 C015 112.3(17) . . ?
C01K C017 C030 109.5(17) . . ?
C030 C017 C015 107.9(17) . . ?
C01U C018 S00S 108.3(11) . . ?
C024 C018 S00S 113.2(13) . . ?
C024 C018 C01U 107.2(14) . . ?
C024 C019 C016 111.8(18) . . ?
C01P C01A S00U 113.2(16) . . ?
C01P C01A C01Y 108.5(18) . . ?
C01Y C01A S00U 112.3(16) . . ?
C01L C01B S00N 111.1(13) . . ?
C01L C01B C025 112.1(13) . . ?
C025 C01B S00N 112.2(12) . . ?
C013 C01C C01I 107.9(13) . . ?
C010 C01D C03F 110.6(18) . . ?
C010 C01D C03X 108.7(16) . . ?
C03F C01D C03X 106.7(17) . . ?
C013 C01E C01V 108.7(15) . . ?
C01G C01F S00P 110.9(12) . . ?
C01Z C01F S00P 111.9(13) . . ?
C01Z C01F C01G 106.3(17) . . ?
C03A C01G C01F 113.1(16) . . ?
C03A C01G C03R 107.7(18) . . ?
C03R C01G C01F 108.3(17) . . ?
C01X C01H C01R 110.2(18) . . ?
C01C C01I C02D 105.6(16) . . ?
C01N C01I C01C 111.8(16) . . ?
C01N C01I C02D 111.0(16) . . ?
C023 C01J C029 109.6(17) . . ?
C017 C01K C02O 108.5(17) . . ?
C01B C01L C01M 107.8(15) . . ?
C01B C01L C031 109.3(19) . . ?
C031 C01L C01M 108.3(16) . . ?
C01L C01M C02H 112.0(16) . . ?
C01I C01N C014 112.7(16) . . ?
C03J C01O C033 109.1(16) . . ?
C01A C01P C03Q 106.3(19) . . ?
C037 C01P C01A 114(2) . . ?
C037 C01P C03Q 108.6(18) . . ?
C010 C01Q C039 108.2(17) . . ?
C010 C01Q C03E 107.2(17) . . ?
C039 C01Q C03E 106.3(18) . . ?
C02Q C01R C01H 107.1(18) . . ?
C02Q C01R C02Y 117(2) . . ?
C02Y C01R C01H 101.4(18) . . ?
C026 C01S C02C 109(2) . . ?
C026 C01S C035 110.7(18) . . ?
C02C C01S C035 107.3(19) . . ?
C01X C01T S00V 116.6(15) . . ?
C01X C01T C02E 109.2(18) . . ?
C02E C01T S00V 112.4(15) . . ?
C022 C01U C018 111.4(15) . . ?
C022 C01U C035 108.9(16) . . ?
C035 C01U C018 106.2(16) . . ?
C02D C01V C01E 112.0(16) . . ?
C02D C01V C02G 109.6(18) . . ?
C02G C01V C01E 108.8(14) . . ?
C02H C01W C025 112.3(17) . . ?
C01T C01X C01H 108.4(18) . . ?
C048 C01X C01H 108.9(19) . . ?
C048 C01X C01T 109.2(19) . . ?
C01A C01Y C041 100.4(18) . . ?
C043 C01Y C01A 112(2) . . ?
C043 C01Y C041 111.7(18) . . ?
C01F C01Z C027 112.0(15) . . ?
C036 C01Z C01F 110.0(18) . . ?
C036 C01Z C027 108(2) . . ?
C023 C020 C032 113.0(15) . . ?
C02N C021 C030 109.3(18) . . ?
C03O C021 C02N 111.2(18) . . ?
C03O C021 C030 106.3(17) . . ?
C01U C022 C016 110.6(15) . . ?
C01J C023 C02A 108.0(16) . . ?
C020 C023 C01J 110.5(15) . . ?
C020 C023 C02A 109(2) . . ?
C019 C024 C018 113.1(16) . . ?
C019 C024 C026 109.6(17) . . ?
C026 C024 C018 106.7(17) . . ?
C01B C025 C01W 110.0(15) . . ?
C01B C025 C03W 106.5(17) . . ?
C01W C025 C03W 107.6(16) . . ?
C01S C026 C024 111.2(17) . . ?
C02K C027 C01Z 109.0(16) . . ?
C03P C028 S00Z 111.3(19) . . ?
C04I C028 S00Z 110.5(19) . . ?
C04I C028 C03P 104(2) . . ?
C01J C029 C02T 108.6(16) . . ?
C02F C029 C01J 112.2(15) . . ?
C02F C029 C02T 107.8(17) . . ?
C03D C02A C023 109.4(16) . . ?
C012 C02B C038 108.8(17) . . ?
C04E C02B C012 106.8(18) . . ?
C04E C02B C038 109.6(16) . . ?
C016 C02C C01S 111.5(17) . . ?
C01V C02D C01I 108.0(15) . . ?
C02Y C02E C01T 103.4(18) . . ?
C04M C02E C01T 109.7(18) . . ?
C04M C02E C02Y 109.6(19) . . ?
C029 C02F S00O 111.6(12) . . ?
C029 C02F C032 112.0(14) . . ?
C032 C02F S00O 111.2(11) . . ?
C014 C02G C01V 111.0(14) . . ?
C01W C02H C01M 107.7(15) . . ?
C01W C02H C03H 107.7(19) . . ?
C03H C02H C01M 109.7(19) . . ?
C02P C02I C02O 110.9(17) . . ?
C036 C02J C03R 107(2) . . ?
C036 C02J C03Z 112(2) . . ?
C03Z C02J C03R 111(2) . . ?
C03A C02K C027 107.7(14) . . ?
C03Z C02K C027 110.0(18) . . ?
C03Z C02K C03A 111.2(18) . . ?
C034 C02L C03N 109.5(4) . . ?
C039 C02M C03F 108.9(18) . . ?
C03M C02M C039 107(2) . . ?
C03M C02M C03F 112(2) . . ?
C021 C02N C02O 110.2(16) . . ?
C02I C02O C01K 109.0(16) . . ?
C02I C02O C02N 108.7(17) . . ?
C02N C02O C01K 105.1(16) . . ?
C015 C02P C03O 108.5(17) . . ?
C02I C02P C015 111.7(18) . . ?
C02I C02P C03O 111.0(17) . . ?
C01R C02Q C04K 108.5(19) . . ?
C03C C02R C03K 114.3(19) . . ?
C032 C02S C03D 110.5(17) . . ?
C029 C02T C03D 107.7(16) . . ?
C04D C02U C04Q 113(2) . . ?
C04D C02U C04R 105(2) . . ?
C04R C02U C04Q 110(2) . . ?
C03T C02V C03J 110.5(19) . . ?
C03N C02W S00X 107.4(9) . . ?
C03Y C02W S00X 113.3(9) . . ?
C03Y C02W C03N 109.8(4) . . ?
C01R C02Y C02E 110.7(18) . . ?
C017 C030 C021 110.9(17) . . ?
C03I C031 C01L 109.4(18) . . ?
C020 C032 C02F 109.4(15) . . ?
C02S C032 C020 105.2(16) . . ?
C02S C032 C02F 109.6(16) . . ?
C042 C033 C01O 110.5(19) . . ?
C04E C033 C01O 108.4(19) . . ?
C04E C033 C042 111.9(18) . . ?
C02L C034 C044 108.9(5) . . ?
C049 C034 C02L 110.3(5) . . ?
C049 C034 C044 109.6(5) . . ?
C01S C035 C01U 109.2(18) . . ?
C01Z C036 C02J 110.8(17) . . ?
C01P C037 C03K 113(2) . . ?
C03J C038 C02B 108.9(18) . . ?
C01Q C039 C02M 111.7(17) . . ?
C01G C03A C02K 110.5(17) . . ?
C02R C03C C03Q 111(2) . . ?
C02R C03C C041 115(2) . . ?
C03Q C03C C041 102.3(18) . . ?
C02A C03D C02S 108.4(18) . . ?
C02A C03D C02T 109(2) . . ?
C02S C03D C02T 109.9(18) . . ?
C040 C03E C01Q 113.3(18) . . ?
C01D C03F C02M 112.0(16) . . ?
C19 C03G C03L 109.0(4) . . ?
C03I C03H C02H 109.3(16) . . ?
C031 C03I C03W 107.3(19) . . ?
C03H C03I C031 115(2) . . ?
C03H C03I C03W 110(2) . . ?
C01O C03J C02V 109.9(18) . . ?
C038 C03J C01O 110.2(19) . . ?
C038 C03J C02V 107.8(17) . . ?
C037 C03K C02R 103.0(19) . . ?
C043 C03K C02R 110(2) . . ?
C043 C03K C037 107.4(18) . . ?
C04G C03L C03G 109.7(5) . . ?
C18 C03L C03G 109.6(6) . . ?
C18 C03L C04G 110.0(6) . . ?
C02M C03M C040 111.5(18) . . ?
C02L C03N C02W 109.1(5) . . ?
C04H C03N C02L 109.4(5) . . ?
C04H C03N C02W 109.2(7) . . ?
C021 C03O C02P 111.8(18) . . ?
C03U C03P C028 114(2) . . ?
C03U C03P C04R 116(2) . . ?
C04R C03P C028 104(2) . . ?
C03C C03Q C01P 109(2) . . ?
C01G C03R C02J 109.2(16) . . ?
C012 C03T C042 110.2(18) . . ?
C02V C03T C012 114.8(19) . . ?
C02V C03T C042 104.6(17) . . ?
C03P C03U C04N 106(2) . . ?
C19 C03V C04T 109.4(4) . . ?
C025 C03W C03I 107.6(17) . . ?
C040 C03X C01D 111.4(18) . . ?
C02W C03Y C04S 109.7(7) . . ?
C044 C03Y C02W 109.8(5) . . ?
C044 C03Y C04S 109.6(5) . . ?
C02J C03Z C02K 107.2(18) . . ?
C03E C040 C03M 105(2) . . ?
C03E C040 C03X 106.7(17) . . ?
C03X C040 C03M 110(2) . . ?
C03C C041 C01Y 107.8(19) . . ?
C033 C042 C03T 109.2(18) . . ?
C03K C043 C01Y 113(2) . . ?
C03Y C044 C034 109.2(4) . . ?
C04K C048 C01X 113.5(19) . . ?
C034 C049 C04V 109.4(4) . . ?
C02U C04D C04I 106(2) . . ?
C033 C04E C02B 111.0(19) . . ?
C03L C04G S00W 116.1(11) . . ?
C03L C04G C04T 109.4(4) . . ?
C04T C04G S00W 108.7(11) . . ?
C03N C04H C04V 109.3(5) . . ?
C028 C04I C04D 105(2) . . ?
C04U C04I C028 120(3) . . ?
C04U C04I C04D 110(3) . . ?
C048 C04K C02Q 106.2(19) . . ?
C04M C04K C02Q 111.3(19) . . ?
C04M C04K C048 110(2) . . ?
C04K C04M C02E 114(2) . . ?
C03U C04N C04Q 109(2) . . ?
C04U C04N C03U 112(2) . . ?
C04U C04N C04Q 106(2) . . ?
C02U C04Q C04N 111(3) . . ?
C02U C04R C03P 108(2) . . ?
C04V C04S C03Y 108.5(5) . . ?
C03V C04T C04G 109.9(5) . . ?
C03V C04T C5 109.5(5) . . ?
C04G C04T C5 108.6(6) . . ?
C04I C04U C04N 110(3) . . ?
C049 C04V C04H 109.0(6) . . ?
C049 C04V C04S 109.2(6) . . ?
C04S C04V C04H 111.1(8) . . ?
C17 C5 C04T 109.3(4) . . ?
C17 C12 C19 109.1(4) . . ?
C5 C17 C18 110.3(6) . . ?
C12 C17 C5 109.7(5) . . ?
C12 C17 C18 109.5(6) . . ?
C03L C18 C17 108.5(4) . . ?
C03G C19 C12 109.8(6) . . ?
C03V C19 C03G 109.3(6) . . ?
C03V C19 C12 110.0(6) . . ?
Ag0F Ag1 Ag0H 117.7(8) . 3_666 ?
Ag0F Ag1 Ag 121.4(7) . 3_666 ?
Ag0F Ag1 S00T 59.2(6) . . ?
Ag0F Ag1 S00V 59.3(5) . . ?
Ag0F Ag1 S00X 165.8(9) . 3_666 ?
S00T Ag1 Ag0H 77.1(3) . 3_666 ?
S00T Ag1 Ag 131.1(5) . 3_666 ?
S00V Ag1 Ag0H 142.5(5) . 3_666 ?
S00V Ag1 Ag 89.1(4) . 3_666 ?
S00V Ag1 S00T 117.8(6) . . ?
S00X Ag1 Ag0H 48.5(3) 3_666 3_666 ?
S00X Ag1 Ag 51.7(3) 3_666 3_666 ?
S00X Ag1 S00T 114.1(5) 3_666 . ?
S00X Ag1 S00V 127.8(6) 3_666 . ?
Ag0H Ag2 Ag0D 129.86(19) . . ?
S00M Ag2 Ag0D 56.31(13) . . ?
S00M Ag2 Ag0H 81.00(17) . . ?
S00R Ag2 Ag0D 46.75(13) . . ?
S00R Ag2 Ag0H 143.3(4) . . ?
S00R Ag2 S00M 102.2(2) . . ?
S00R Ag2 S00X 130.0(3) . . ?
S00X Ag2 Ag0D 175.7(4) . . ?
S00X Ag2 Ag0H 50.05(17) . . ?
S00X Ag2 S00M 126.0(3) . . ?

_olex2_submission_special_instructions 'No special instructions were received'
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_1
_database_code_depnum_ccdc_archive 'CCDC 2094273'
loop_
_audit_author_name
_audit_author_address
'Xi Xi Kang'
;Anhui University
China
;
_audit_update_record             
;
2021-08-12 deposited with the CCDC.	2022-04-12 downloaded from the CCDC.
;
_audit_creation_date             2021-08-12
_audit_creation_method           
;
Olex2 1.2
(compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506)
;
_shelx_SHELXL_version_number     2018/3
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         '1(C261 H348 Ag34 Cl4 P6 S18), 1(F5 Sb1)'
_chemical_formula_sum            'C261 H348 Ag34 Cl4 F5 P6 S18 Sb'
_chemical_formula_weight         8274.49
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag 0.1306 4.2820 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.3639 0.7018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0727 0.0534 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.2955 0.4335 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.3331 0.5567 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sb Sb -0.0562 5.8946 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      trigonal
_space_group_IT_number           148
_space_group_name_H-M_alt        'R -3'
_space_group_name_Hall           '-R 3'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-y, x-y, z'
'-x+y, -x, z'
'x+2/3, y+1/3, z+1/3'
'-y+2/3, x-y+1/3, z+1/3'
'-x+y+2/3, -x+1/3, z+1/3'
'x+1/3, y+2/3, z+2/3'
'-y+1/3, x-y+2/3, z+2/3'
'-x+y+1/3, -x+2/3, z+2/3'
'-x, -y, -z'
'y, -x+y, -z'
'x-y, x, -z'
'-x+2/3, -y+1/3, -z+1/3'
'y+2/3, -x+y+1/3, -z+1/3'
'x-y+2/3, x+1/3, -z+1/3'
'-x+1/3, -y+2/3, -z+2/3'
'y+1/3, -x+y+2/3, -z+2/3'
'x-y+1/3, x+2/3, -z+2/3'

_cell_length_a                   26.59(2)
_cell_length_b                   26.59(2)
_cell_length_c                   87.85(3)
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                120
_cell_volume                     53775(90)
_cell_formula_units_Z            5.99994
_cell_measurement_reflns_used    1635
_cell_measurement_temperature    120(2)
_cell_measurement_theta_max      58.84
_cell_measurement_theta_min      6.84
_shelx_estimated_absorpt_T_max   ?
_shelx_estimated_absorpt_T_min   ?
_exptl_absorpt_coefficient_mu    16.906
_exptl_absorpt_correction_T_max  1.0000
_exptl_absorpt_correction_T_min  0.1920
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
;
STOE LANA, absorption correction by scaling of reflection intensities.
J. Koziskova, F. Hahn, J. Richter, J. Kozisek, "Comparison of different
absorption corrections on the model structure of tetrakis(μ₂-acetato)-
diaqua-di-copper(II)", Acta Chimica Slovaca, vol. 9, no. 2, 2016, pp. 136 - 140.
;
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            black
_exptl_crystal_colour_primary    black
_exptl_crystal_density_diffrn    1.533
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             24324
_exptl_crystal_size_max          ?
_exptl_crystal_size_mid          ?
_exptl_crystal_size_min          ?
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0486
_diffrn_reflns_av_unetI/netI     0.0542
_diffrn_reflns_Laue_measured_fraction_full 0.979
_diffrn_reflns_Laue_measured_fraction_max 0.979
_diffrn_reflns_limit_h_max       24
_diffrn_reflns_limit_h_min       -30
_diffrn_reflns_limit_k_max       30
_diffrn_reflns_limit_k_min       -21
_diffrn_reflns_limit_l_max       101
_diffrn_reflns_limit_l_min       -37
_diffrn_reflns_number            40279
_diffrn_reflns_point_group_measured_fraction_full 0.979
_diffrn_reflns_point_group_measured_fraction_max 0.979
_diffrn_reflns_theta_full        62.497
_diffrn_reflns_theta_max         62.497
_diffrn_reflns_theta_min         6.189
_diffrn_ambient_temperature      120(2)
_diffrn_detector_area_resol_mean 5.81
_diffrn_detector_type            'DECTRIS PILATUS 300K'
_diffrn_measured_fraction_theta_full 0.979
_diffrn_measured_fraction_theta_max 0.979
_diffrn_measurement_details      
;
 629 frames, detector distance = 60 mm
;
_diffrn_measurement_device       'Eulerian 4-circle diffractometer'
_diffrn_measurement_device_type  'STOE STADIVARI'
_diffrn_measurement_method       'rotation method, ω scans'
_diffrn_radiation_type           CuK\a
_diffrn_radiation_wavelength     1.54186
_diffrn_source                   ?
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                12468
_reflns_number_total             18671
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 Structure factors included contributions from the .fab file.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       
;
X-Area Recipe 1.33.0.0 (STOE, 2015)
;
_computing_data_collection       
;
X-Area Pilatus3_SV 1.31.153.0 (STOE, 2018)
;
_computing_data_reduction        
;
X-Area Integrate 1.74.2.0 (STOE, 2018)
X-Area LANA 1.75.3.0 (STOE, 2018)
;
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'ShelXL (Sheldrick, 2015)'
_computing_structure_solution    'SHELXT  (Sheldrick, 2015)'
_refine_diff_density_max         3.738
_refine_diff_density_min         -1.648
_refine_diff_density_rms         0.275
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.281
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     943
_refine_ls_number_reflns         18671
_refine_ls_number_restraints     2733
_refine_ls_R_factor_all          0.1390
_refine_ls_R_factor_gt           0.1066
_refine_ls_restrained_S_all      1.275
_refine_ls_shift/su_max          0.004
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.2100P)²] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.3100
_refine_ls_wR_factor_ref         0.3549
_refine_special_details          ?
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H) groups, All C(H,H) groups
2. Restrained distances
 C70-C14 = C01B-C010 = C36-C010 = C36-C14 = C14-C02Q = C02Q-C021 = C021-C011 =
 C011-C010 = C70-C02L = C02L-C01B = C02L-C01D = C021-C01D
 1.53 with sigma of 0.01
 C36-C02Q
 2.54 with sigma of 0.01
 C36-C01B
 2.54 with sigma of 0.01
 C36-C011
 2.54 with sigma of 0.01
 C36-C70
 2.54 with sigma of 0.01
 C14-C021
 2.54 with sigma of 0.01
 C14-C02L
 2.54 with sigma of 0.01
 C14-C010
 2.54 with sigma of 0.01
 C02Q-C70
 2.54 with sigma of 0.01
 C02Q-C011
 2.54 with sigma of 0.01
 C02Q-C01D
 2.54 with sigma of 0.01
 C021-C010
 2.54 with sigma of 0.01
 C021-C02L
 2.54 with sigma of 0.01
 C01D-C01B
 2.54 with sigma of 0.01
 C01D-C70
 2.54 with sigma of 0.01
 C02L-C010
 2.54 with sigma of 0.01
 C01B-C011
 2.54 with sigma of 0.01
 C01B-C70
 2.54 with sigma of 0.01
 C36-C021
 2.93 with sigma of 0.01
 C36-C02L
 2.93 with sigma of 0.01
 C14-C01B
 2.93 with sigma of 0.01
 C14-C011
 2.93 with sigma of 0.01
 C14-C01D
 2.93 with sigma of 0.01
 C02Q-C02L
 2.93 with sigma of 0.01
 C02Q-C010
 2.93 with sigma of 0.01
 C021-C70
 2.93 with sigma of 0.01
 C021-C01B
 2.93 with sigma of 0.01
 C01D-C010
 2.93 with sigma of 0.01
 C02L-C011
 2.93 with sigma of 0.01
 C01Q-C016 = C01Z-C01Q = C02O-C01Q = C02O-C025 = C188-C025 = C28-C188 = C28-
 C016 = C28-C23 = C23-C020 = C020-C01Z = C02K-C020 = C02K-C025
 1.53 with sigma of 0.01
 C016-C02O
 2.54 with sigma of 0.01
 C016-C01Z
 2.54 with sigma of 0.01
 C016-C188
 2.54 with sigma of 0.01
 C016-C23
 2.54 with sigma of 0.01
 C28-C025
 2.54 with sigma of 0.01
 C28-C01Q
 2.54 with sigma of 0.01
 C28-C020
 2.54 with sigma of 0.01
 C23-C188
 2.54 with sigma of 0.01
 C23-C02K
 2.54 with sigma of 0.01
 C23-C01Z
 2.54 with sigma of 0.01
 C020-C025
 2.54 with sigma of 0.01
 C020-C01Q
 2.54 with sigma of 0.01
 C02K-C02O
 2.54 with sigma of 0.01
 C02K-C188
 2.54 with sigma of 0.01
 C02K-C01Z
 2.54 with sigma of 0.01
 C025-C01Q
 2.54 with sigma of 0.01
 C02O-C01Z
 2.54 with sigma of 0.01
 C01Q-C020
 2.54 with sigma of 0.01
 C016-C025
 2.93 with sigma of 0.01
 C016-C020
 2.93 with sigma of 0.01
 C28-C02O
 2.93 with sigma of 0.01
 C28-C01Z
 2.93 with sigma of 0.01
 C28-C02K
 2.93 with sigma of 0.01
 C23-C025
 2.93 with sigma of 0.01
 C23-C01Q
 2.93 with sigma of 0.01
 C020-C02O
 2.93 with sigma of 0.01
 C020-C188
 2.93 with sigma of 0.01
 C02K-C01Q
 2.93 with sigma of 0.01
 C025-C01Z
 2.93 with sigma of 0.01
 C7AA-C01E = C5AA-C01E = C5AA-C25 = C5AA-C44 = C44-C29 = C79-C25 = C78-C29 =
 C6AA-C29 = C7AA-C19 = C7AA-C6AA = C79-C19 = C79-C78
 1.53 with sigma of 0.01
 C01E-C6AA
 2.54 with sigma of 0.01
 C01E-C25
 2.54 with sigma of 0.01
 C01E-C19
 2.54 with sigma of 0.01
 C01E-C44
 2.54 with sigma of 0.01
 C7AA-C29
 2.54 with sigma of 0.01
 C7AA-C79
 2.54 with sigma of 0.01
 C7AA-C5AA
 2.54 with sigma of 0.01
 C6AA-C78
 2.54 with sigma of 0.01
 C6AA-C44
 2.54 with sigma of 0.01
 C6AA-C19
 2.54 with sigma of 0.01
 C29-C79
 2.54 with sigma of 0.01
 C29-C5AA
 2.54 with sigma of 0.01
 C78-C19
 2.54 with sigma of 0.01
 C78-C25
 2.54 with sigma of 0.01
 C79-C5AA
 2.54 with sigma of 0.01
 C25-C44
 2.54 with sigma of 0.01
 C25-C19
 2.54 with sigma of 0.01
 C5AA-C29
 2.54 with sigma of 0.01
 C01E-C29
 2.93 with sigma of 0.01
 C01E-C79
 2.93 with sigma of 0.01
 C7AA-C25
 2.93 with sigma of 0.01
 C7AA-C44
 2.93 with sigma of 0.01
 C7AA-C78
 2.93 with sigma of 0.01
 C6AA-C79
 2.93 with sigma of 0.01
 C6AA-C5AA
 2.93 with sigma of 0.01
 C29-C19
 2.93 with sigma of 0.01
 C29-C25
 2.93 with sigma of 0.01
 C78-C5AA
 2.93 with sigma of 0.01
 C79-C44
 2.93 with sigma of 0.01
 C92-C87 = C92-C111 = C4AA-C111 = C4AA-C3AA = C20-C111 = C2AA-C20 = C87-C31 =
 C3AA-C31 = C87-C1AA = C2AA-C1AA = C2AA-C151 = C3AA-C151
 1.53 with sigma of 0.01
 C92-C1AA
 2.54 with sigma of 0.01
 C92-C4AA
 2.54 with sigma of 0.01
 C92-C20
 2.54 with sigma of 0.01
 C92-C31
 2.54 with sigma of 0.01
 C111-C3AA
 2.54 with sigma of 0.01
 C111-C87
 2.54 with sigma of 0.01
 C111-C2AA
 2.54 with sigma of 0.01
 C4AA-C151
 2.54 with sigma of 0.01
 C4AA-C31
 2.54 with sigma of 0.01
 C4AA-C20
 2.54 with sigma of 0.01
 C3AA-C87
 2.54 with sigma of 0.01
 C3AA-C2AA
 2.54 with sigma of 0.01
 C151-C1AA
 2.54 with sigma of 0.01
 C151-C20
 2.54 with sigma of 0.01
 C151-C31
 2.54 with sigma of 0.01
 C2AA-C87
 2.54 with sigma of 0.01
 C2AA-C111
 2.54 with sigma of 0.01
 C1AA-C31
 2.54 with sigma of 0.01
 C1AA-C20
 2.54 with sigma of 0.01
 C87-C3AA
 2.54 with sigma of 0.01
 C92-C2AA
 2.93 with sigma of 0.01
 C92-C3AA
 2.93 with sigma of 0.01
 C111-C31
 2.93 with sigma of 0.01
 C111-C1AA
 2.93 with sigma of 0.01
 C111-C151
 2.93 with sigma of 0.01
 C4AA-C2AA
 2.93 with sigma of 0.01
 C4AA-C87
 2.93 with sigma of 0.01
 C3AA-C20
 2.93 with sigma of 0.01
 C3AA-C1AA
 2.93 with sigma of 0.01
 C151-C87
 2.93 with sigma of 0.01
 C151-C111
 2.93 with sigma of 0.01
 C2AA-C31
 2.93 with sigma of 0.01
 C1AA-C111
 2.93 with sigma of 0.01
 Sb0C-F02D = Sb0C-F01V = Sb0C-F34
 1.54 with sigma of 0.01
 F02D-Sb0C = Sb0C-F34
 1.54 with sigma of 0.02
 F34-Sb0C
 1.54 with sigma of 0.02
 F34_$1-Sb0C = Sb0C-F02D
 1.54 with sigma of 0.02
 F34_$1-Sb0C = Sb0C-F01V
 1.54 with sigma of 0.02
 Sb0C-F34 = F34-F01V
 1.54 with sigma of 0.02
 F01V-Sb0C
 1.54 with sigma of 0.02
 F34_$1-Sb0C
 1.54 with sigma of 0.02
 F01V-Sb0C = Sb0C-F34_$1
 1.54 with sigma of 0.02
 F34_$1-Sb0C = Sb0C-F34
 1.54 with sigma of 0.02
 Sb0C-F34_$1
 1.54 with sigma of 0.02
 F02D-Sb0C = Sb0C-F34_$1
 1.54 with sigma of 0.02
 F02D-Sb0C = Sb0C-F01V
 1.54 with sigma of 0.02
 Sb0C-F34
 1.54 with sigma of 0.02
 Sb0C-F02D
 1.54 with sigma of 0.02
 Sb0C-F01V
 1.54 with sigma of 0.02
 F01V-Sb0C = Sb0C-F34
 1.54 with sigma of 0.02
 H01V-H135
 2.11 with sigma of 0.01
 H111-H112
 2.11 with sigma of 0.01
 P00P-C56
 1.88 with sigma of 0.01
 F34_$1-F02D
 2.178 with sigma of 0.04
 F02D-F34
 2.178 with sigma of 0.04
 Sb0C-F01V
 2.178 with sigma of 0.04
 F34_$1-F01V
 2.178 with sigma of 0.04
 F01V-F34_$1
 2.178 with sigma of 0.04
 F34_$1-F34
 2.178 with sigma of 0.04
 F02D-F34_$1
 2.178 with sigma of 0.04
 F02D-F01V
 3.08 with sigma of 0.04
 F01V-F34
 2.178 with sigma of 0.04
3. Uiso/Uaniso restraints and constraints
P00N \\sim P00P \\sim C00R \\sim C00T \\sim C00U \\sim C00V \\sim C00W \\sim
C00X \\sim C01F \\sim C02N \\sim C02P \\sim C01W \\sim C01A \\sim C00Y \\sim
C00Z \\sim C010 \\sim C011 \\sim C013 \\sim C014 \\sim C015 \\sim C016 \\sim
C017 \\sim C018 \\sim C019 \\sim C01B \\sim C01D \\sim C01E \\sim C01G \\sim
C01J \\sim C01K \\sim C01L \\sim C01N \\sim C01O \\sim C01P \\sim C01Q \\sim
C01T \\sim C01Z \\sim C020 \\sim C021 \\sim C023 \\sim C025 \\sim C02K \\sim
C02L \\sim C02O \\sim C02Q \\sim C37 \\sim C110 \\sim C0AA \\sim C76 \\sim C135
\\sim C61 \\sim C92 \\sim C94 \\sim C188 \\sim C115 \\sim C34 \\sim C184 \\sim
C93 \\sim C112 \\sim C01X \\sim C101 \\sim C98 \\sim C174 \\sim C64 \\sim C43
\\sim C56 \\sim C70 \\sim C1AA \\sim C14 \\sim C36 \\sim C28 \\sim C23 \\sim
C19 \\sim C5AA \\sim C25 \\sim C29 \\sim C7AA \\sim C6AA \\sim C44 \\sim C78
\\sim C79 \\sim C3AA \\sim C4AA \\sim C31 \\sim C87 \\sim C111 \\sim C20 \\sim
C2AA \\sim C151 \\sim S00F \\sim S00G \\sim S00I \\sim S00J \\sim S00K \\sim
S00L: within 3.8A with sigma of 0.01 and sigma for terminal atoms of 0.02
Sb0C \\sim F01V \\sim F02D \\sim F34: within 3.8A with sigma of 0.01 and sigma
for terminal atoms of 0.02
Uanis(Sb0C) \\sim Ueq, Uanis(F01V) \\sim Ueq, Uanis(F02D) \\sim Ueq, Uanis(F34)
\\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(Ag) = Uanis(Ag1)
4. Others
 Fixed Sof: Ag(0.85) Ag1(0.15)
5.a Ternary CH refined with riding coordinates:
 C00R(H00R), C00U(H00U), C00W(H00W), C00Y(H00Y), C010(H010), C014(H014),
 C015(H015), C016(H016), C01E(H01P), C01G(H01Q), C01K(H01T), C01L(H01U),
 C01P(H01Z), C01Q(H01), C020(H020), C021(H021), C025(H025), C02L(H02L),
 C92(H92), C14(H14), C36(H36), C28(H28), C5AA(H5AA), C29(H29), C7AA(H7AA),
 C79(H79), C3AA(H3AA), C87(H87), C111(H111), C2AA(H2AA)
5.b Secondary CH2 refined with riding coordinates:
 C00T(H00A,H00B), C00V(H00C,H00D), C00Z(H00E,H00F), C011(H01B,H01C), C013(H01D,
 H01E), C017(H01G,H01F), C018(H01H,H01I), C019(H01J,H01K), C01B(H01L,H01M),
 C01D(H01N,H01O), C01J(H01S,H01R), C01N(H01V,H01X), C01O(H,H01Y), C01T(H0AA,HA),
  C01Z(H1AA,HB), C023(H02A,H02B), C02K(H02C,H02D), C02O(H02E,H02F), C02Q(H02G,
 H02H), C94(H94A,H94B), C188(H18A,H18B), C70(H70A,H70B), C1AA(H1AB,H1AC),
 C23(H23A,H23B), C19(H19A,H19B), C25(H25A,H25B), C6AA(H6AA,H6AB), C44(H44A,
 H44B), C78(H78A,H78B), C4AA(H4AA,H4AB), C31(H31A,H31B), C20(H20A,H20B),
 C151(H15A,H15B)
5.c Aromatic/amide H refined with riding coordinates:
 C00X(H00X), C02N(H02N), C02P(H02P), C01W(H01W), C01A(H01A), C37(H37),
 C110(H110), C0AA(H0AB), C76(H76), C135(H135), C115(H115), C34(H34), C184(H184),
  C93(H93), C112(H112), C101(H101), C98(H98), C174(H174), C64(H64), C43(H43)
5.d Fitted hexagon refined as free rotating group:
 C00X(C01F,C02N,C02P,C01W,C01A), C37(C110,C0AA,C76,C135,C61), C115(C34,C184,
 C93,C112,C01X), C101(C98,C174,C64,C43,C56)
;
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag01 Ag 0.333333 0.666667 0.41591(2) 0.0537(5) Uani 1 3 d S T P . .
Ag02 Ag 0.37968(5) 0.62852(5) 0.43982(2) 0.0584(3) Uani 1 1 d . . . . .
Ag03 Ag 0.45217(5) 0.73333(6) 0.42103(2) 0.0627(3) Uani 1 1 d . . . . .
Ag04 Ag 0.47932(6) 0.75630(5) 0.45349(2) 0.0631(3) Uani 1 1 d . . . . .
Ag05 Ag 0.39257(6) 0.78715(5) 0.40924(2) 0.0637(3) Uani 1 1 d . . . . .
Ag06 Ag 0.40265(6) 0.70298(6) 0.38967(2) 0.0660(4) Uani 1 1 d . . . . .
Ag07 Ag 0.45880(6) 0.57052(7) 0.44850(2) 0.0727(4) Uani 1 1 d . . . . .
Ag08 Ag 0.49220(7) 0.85076(7) 0.42914(2) 0.0785(4) Uani 1 1 d . . . . .
Ag09 Ag 0.51032(7) 0.83086(7) 0.39393(2) 0.0874(5) Uani 1 1 d . . . . .
Ag Ag 0.51077(11) 0.62013(9) 0.42032(2) 0.0805(6) Uani 0.85 1 d . . . A 2
Ag0B Ag 0.55891(7) 0.70984(10) 0.38832(2) 0.0992(6) Uani 1 1 d . . . . .
Sb0C Sb 0.333333 0.666667 0.55026(3) 0.1016(8) Uani 1 3 d DS TU P . .
Ag0D Ag 0.48700(11) 0.50493(10) 0.40369(2) 0.1105(7) Uani 1 1 d . . . . .
Cl00 Cl 0.333333 0.666667 0.46098(6) 0.0576(14) Uani 1 3 d S T P . .
S00F S 0.5024(2) 0.85414(19) 0.45721(5) 0.0680(10) Uani 1 1 d . U . . .
S00G S 0.4689(2) 0.6622(2) 0.45809(5) 0.0687(10) Uani 1 1 d . U . . .
Cl1 Cl 0.4020(2) 0.8634(2) 0.39078(4) 0.0767(12) Uani 1 1 d . . . . .
S00I S 0.5083(3) 0.5365(3) 0.43142(6) 0.0909(14) Uani 1 1 d . U . . .
S00J S 0.5373(2) 0.7222(3) 0.41625(5) 0.0809(12) Uani 1 1 d . U . . .
S00K S 0.4978(3) 0.7530(3) 0.37819(5) 0.0894(13) Uani 1 1 d . U . . .
S00L S 0.5411(3) 0.9176(3) 0.40796(7) 0.1022(17) Uani 1 1 d . U . . .
P00N P 0.6389(3) 0.7178(4) 0.37422(8) 0.1186(18) Uani 1 1 d . U . . .
P00P P 0.5529(4) 0.5033(5) 0.38564(10) 0.137(2) Uani 1 1 d D U . . .
C00R C 0.4386(9) 0.6452(9) 0.4776(2) 0.076(2) Uani 1 1 d . U . . .
H00R H 0.396143 0.623429 0.476872 0.091 Uiso 1 1 calc R . . . .
C00T C 0.5059(9) 0.6724(9) 0.5130(2) 0.077(3) Uani 1 1 d . U . . .
H00A H 0.517018 0.647428 0.518312 0.093 Uiso 1 1 calc R . . . .
H00B H 0.516653 0.705895 0.519495 0.093 Uiso 1 1 calc R . . . .
C00U C 0.4560(9) 0.6967(8) 0.4869(2) 0.073(2) Uani 1 1 d . U . . .
H00U H 0.444497 0.722143 0.481830 0.087 Uiso 1 1 calc R . . . .
C00V C 0.5767(10) 0.8916(9) 0.4875(2) 0.086(3) Uani 1 1 d . U . . .
H00C H 0.589567 0.876010 0.495641 0.103 Uiso 1 1 calc R . . . .
H00D H 0.534699 0.868278 0.486914 0.103 Uiso 1 1 calc R . . . .
C00W C 0.5929(10) 0.9674(10) 0.4630(3) 0.088(3) Uani 1 1 d . U . . .
H00W H 0.577941 0.979214 0.454342 0.106 Uiso 1 1 calc R . . . .
C00X C 0.5615(8) 0.6607(10) 0.35076(19) 0.126(3) Uani 1 1 d . U . . .
H00X H 0.534049 0.660948 0.357290 0.151 Uiso 1 1 calc R . . . .
C01F C 0.6192(8) 0.6860(10) 0.35528(17) 0.128(3) Uani 1 1 d G U . . .
C02N C 0.6601(7) 0.6856(10) 0.3455(2) 0.128(3) Uani 1 1 d G U . . .
H02N H 0.698760 0.702535 0.348540 0.154 Uiso 1 1 calc R . . . .
C02P C 0.6434(8) 0.6599(10) 0.33125(19) 0.131(4) Uani 1 1 d G U . . .
H02P H 0.670808 0.659685 0.324721 0.157 Uiso 1 1 calc R . . . .
C01W C 0.5857(8) 0.6346(10) 0.32673(17) 0.130(4) Uani 1 1 d G U . . .
H01W H 0.574477 0.617467 0.317186 0.156 Uiso 1 1 calc R . . . .
C01A C 0.5447(7) 0.6350(10) 0.3365(2) 0.129(4) Uani 1 1 d G U . . .
H01A H 0.506097 0.618098 0.333470 0.154 Uiso 1 1 calc R . . . .
C00Y C 0.5817(10) 0.9070(10) 0.4608(2) 0.088(3) Uani 1 1 d . U . . .
H00Y H 0.604040 0.906594 0.451934 0.105 Uiso 1 1 calc R . . . .
C00Z C 0.4260(10) 0.6787(9) 0.5021(2) 0.079(3) Uani 1 1 d . U . . .
H00E H 0.384380 0.656954 0.500406 0.095 Uiso 1 1 calc R . . . .
H00F H 0.434778 0.713256 0.507832 0.095 Uiso 1 1 calc R . . . .
C010 C 0.6393(6) 0.8251(6) 0.42456(15) 0.108(3) Uani 1 1 d D U . . .
H010 H 0.619736 0.844149 0.419846 0.130 Uiso 1 1 calc R . . . .
C011 C 0.6801(7) 0.8202(7) 0.41291(12) 0.112(3) Uani 1 1 d D U . . .
H01B H 0.657816 0.798163 0.404131 0.134 Uiso 1 1 calc R . . . .
H01C H 0.708972 0.858631 0.409472 0.134 Uiso 1 1 calc R . . . .
C013 C 0.5193(9) 0.7311(9) 0.4909(2) 0.079(2) Uani 1 1 d . U . . .
H01D H 0.525797 0.762599 0.497642 0.095 Uiso 1 1 calc R . . . .
H01E H 0.541539 0.747931 0.481665 0.095 Uiso 1 1 calc R . . . .
C014 C 0.4593(9) 0.6059(9) 0.4854(2) 0.077(2) Uani 1 1 d . U . . .
H014 H 0.449759 0.571801 0.479138 0.092 Uiso 1 1 calc R . . . .
C015 C 0.5935(10) 0.9533(10) 0.4913(3) 0.092(3) Uani 1 1 d . U . . .
H015 H 0.575532 0.952724 0.501062 0.110 Uiso 1 1 calc R . . . .
C016 C 0.5820(7) 0.5634(7) 0.43797(15) 0.111(3) Uani 1 1 d D U . . .
H016 H 0.607474 0.597568 0.431803 0.134 Uiso 1 1 calc R . . . .
C017 C 0.4263(10) 0.5875(9) 0.5008(2) 0.081(3) Uani 1 1 d . U . . .
H01G H 0.434990 0.560383 0.505965 0.098 Uiso 1 1 calc R . . . .
H01F H 0.384791 0.567835 0.498961 0.098 Uiso 1 1 calc R . . . .
C018 C 0.6742(14) 0.6779(15) 0.3834(3) 0.132(3) Uani 1 1 d . U . . .
H01H H 0.698517 0.673958 0.375829 0.158 Uiso 1 1 calc R . . . .
H01I H 0.699509 0.702229 0.391499 0.158 Uiso 1 1 calc R . . . .
C019 C 0.5619(10) 0.9697(10) 0.4786(2) 0.089(3) Uani 1 1 d . U . . .
H01J H 0.567524 1.008204 0.480304 0.107 Uiso 1 1 calc R . . . .
H01K H 0.520569 0.941881 0.478373 0.107 Uiso 1 1 calc R . . . .
C01B C 0.6758(7) 0.8612(5) 0.43837(17) 0.110(3) Uani 1 1 d D U . . .
H01L H 0.650714 0.864644 0.445808 0.132 Uiso 1 1 calc R . . . .
H01M H 0.704403 0.899996 0.435060 0.132 Uiso 1 1 calc R . . . .
C01D C 0.7466(4) 0.8266(7) 0.43366(17) 0.111(3) Uani 1 1 d D U . . .
H01N H 0.775032 0.865180 0.430191 0.133 Uiso 1 1 calc R . . . .
H01O H 0.767297 0.808786 0.438139 0.133 Uiso 1 1 calc R . . . .
C01E C 0.6180(6) 0.9544(6) 0.41005(17) 0.125(3) Uani 1 1 d D U . . .
H01P H 0.625649 0.939645 0.419468 0.150 Uiso 1 1 calc R . . . .
C01G C 0.5408(10) 0.6932(9) 0.4986(2) 0.078(3) Uani 1 1 d . U . . .
H01Q H 0.582397 0.716132 0.500865 0.094 Uiso 1 1 calc R . . . .
C01J C 0.6682(10) 0.9320(10) 0.4745(3) 0.094(3) Uani 1 1 d . U . . .
H01S H 0.685076 0.921313 0.482829 0.113 Uiso 1 1 calc R . . . .
H01R H 0.685136 0.928158 0.465143 0.113 Uiso 1 1 calc R . . . .
C01K C 0.6000(10) 0.8872(10) 0.4741(2) 0.087(3) Uani 1 1 d . U . . .
H01T H 0.592393 0.847481 0.472639 0.105 Uiso 1 1 calc R . . . .
C01L C 0.6845(10) 0.9926(10) 0.4764(2) 0.091(3) Uani 1 1 d . U . . .
H01U H 0.726697 1.018288 0.476516 0.109 Uiso 1 1 calc R . . . .
C01N C 0.6314(15) 0.6148(14) 0.3904(4) 0.137(3) Uani 1 1 d . U . . .
H01V H 0.653521 0.601522 0.396185 0.164 Uiso 1 1 calc DR . . . .
H01X H 0.603533 0.616703 0.397125 0.164 Uiso 1 1 calc R . . . .
C01O C 0.6572(10) 1.0090(10) 0.4650(3) 0.093(3) Uani 1 1 d . U . . .
H H 0.676572 1.012648 0.455403 0.111 Uiso 1 1 calc R . . . .
H01Y H 0.662855 1.046940 0.467620 0.111 Uiso 1 1 calc R . . . .
C01P C 0.4439(9) 0.6415(9) 0.5114(2) 0.081(3) Uani 1 1 d . U . . .
H01Z H 0.424110 0.630368 0.521265 0.097 Uiso 1 1 calc R . . . .
C01Q C 0.5927(7) 0.5823(6) 0.45484(17) 0.111(3) Uani 1 1 d D U . . .
H01 H 0.581203 0.611525 0.456691 0.134 Uiso 1 1 calc R . . . .
C01T C 0.6547(10) 0.9926(10) 0.4927(3) 0.092(3) Uani 1 1 d . U . . .
H0AA H 0.670721 0.980027 0.500803 0.110 Uiso 1 1 calc R . . . .
HA H 0.662100 1.031355 0.495080 0.110 Uiso 1 1 calc R . . . .
F01V F 0.333333 0.666667 0.56795(8) 0.164(6) Uani 1 3 d DS TU P . .
C01Z C 0.5570(6) 0.5291(8) 0.46507(15) 0.116(3) Uani 1 1 d D U . . .
H1AA H 0.515926 0.512619 0.462891 0.140 Uiso 1 1 calc R . . . .
HB H 0.563402 0.540758 0.475675 0.140 Uiso 1 1 calc R . . . .
C020 C 0.5752(6) 0.4831(6) 0.46215(15) 0.120(3) Uani 1 1 d D U . . .
H020 H 0.552288 0.449261 0.468664 0.144 Uiso 1 1 calc R . . . .
C021 C 0.7102(5) 0.7900(7) 0.42013(14) 0.113(3) Uani 1 1 d D U . . .
H021 H 0.735722 0.786902 0.412607 0.135 Uiso 1 1 calc R . . . .
C023 C 0.5280(9) 0.6423(9) 0.4889(2) 0.078(2) Uani 1 1 d . U . . .
H02A H 0.539842 0.617788 0.494153 0.093 Uiso 1 1 calc R . . . .
H02B H 0.549478 0.655364 0.479473 0.093 Uiso 1 1 calc R . . . .
C025 C 0.6760(5) 0.5625(7) 0.45554(17) 0.118(3) Uani 1 1 d D U . . .
H025 H 0.717341 0.579265 0.457894 0.141 Uiso 1 1 calc R . . . .
F02D F 0.333333 0.666667 0.53287(8) 0.165(6) Uani 1 3 d DS TU P . .
C02K C 0.6402(7) 0.5094(7) 0.46593(16) 0.119(3) Uani 1 1 d D U . . .
H02C H 0.651930 0.480616 0.464303 0.142 Uiso 1 1 calc R . . . .
H02D H 0.647070 0.521203 0.476521 0.142 Uiso 1 1 calc R . . . .
C02L C 0.7068(6) 0.8309(6) 0.44567(13) 0.111(3) Uani 1 1 d D U . . .
H02L H 0.730223 0.854005 0.454320 0.133 Uiso 1 1 calc R . . . .
C02O C 0.6581(6) 0.6084(5) 0.45835(19) 0.118(3) Uani 1 1 d D U . . .
H02E H 0.680762 0.641850 0.451882 0.142 Uiso 1 1 calc R . . . .
H02F H 0.665702 0.621127 0.468866 0.142 Uiso 1 1 calc R . . . .
C02Q C 0.6646(7) 0.7287(5) 0.42561(17) 0.108(3) Uani 1 1 d D U . . .
H02G H 0.641804 0.705559 0.417031 0.130 Uiso 1 1 calc R . . . .
H02H H 0.683893 0.709619 0.430156 0.130 Uiso 1 1 calc R . . . .
C37 C 0.5715(8) 0.4262(11) 0.4012(3) 0.148(3) Uani 1 1 d . U . . .
H37 H 0.531134 0.407140 0.401166 0.177 Uiso 1 1 calc R . . . .
C110 C 0.6003(11) 0.4003(9) 0.4078(3) 0.153(4) Uani 1 1 d G U . . .
H110 H 0.579166 0.363846 0.412302 0.184 Uiso 1 1 calc R . . . .
C0AA C 0.6606(11) 0.4288(11) 0.4078(2) 0.157(4) Uani 1 1 d G U . . .
H0AB H 0.679882 0.411481 0.412271 0.188 Uiso 1 1 calc R . . . .
C76 C 0.6922(8) 0.4833(10) 0.4011(3) 0.157(4) Uani 1 1 d G U . . .
H76 H 0.732566 0.502411 0.401104 0.189 Uiso 1 1 calc R . . . .
C135 C 0.6634(11) 0.5093(8) 0.3944(3) 0.151(4) Uani 1 1 d G U . . .
H135 H 0.684535 0.545707 0.389968 0.182 Uiso 1 1 calc DR . . . .
C61 C 0.6031(11) 0.4807(12) 0.3945(2) 0.147(3) Uani 1 1 d G U . . .
C92 C 0.4731(7) 0.7494(7) 0.35803(17) 0.134(3) Uani 1 1 d D U . . .
H92 H 0.451212 0.708266 0.355149 0.161 Uiso 1 1 calc R . . . .
C94 C 0.6009(15) 0.5743(15) 0.3779(4) 0.139(3) Uani 1 1 d . U . . .
H94A H 0.628805 0.572538 0.371139 0.167 Uiso 1 1 calc R . . . .
H94B H 0.578780 0.587647 0.372095 0.167 Uiso 1 1 calc R . . . .
C188 C 0.6657(6) 0.5439(9) 0.43882(16) 0.119(3) Uani 1 1 d D U . . .
H18A H 0.677515 0.515378 0.436943 0.142 Uiso 1 1 calc R . . . .
H18B H 0.688562 0.577237 0.432326 0.142 Uiso 1 1 calc R . . . .
C115 C 0.7484(10) 0.8286(10) 0.3773(2) 0.136(3) Uani 1 1 d . U . . .
H115 H 0.759130 0.809236 0.384279 0.163 Uiso 1 1 calc R . . . .
C34 C 0.7859(7) 0.8870(10) 0.3742(2) 0.141(4) Uani 1 1 d G U . . .
H34 H 0.821670 0.906772 0.379121 0.169 Uiso 1 1 calc R . . . .
C184 C 0.7699(8) 0.9159(7) 0.3639(2) 0.141(4) Uani 1 1 d G U . . .
H184 H 0.794965 0.955044 0.361783 0.170 Uiso 1 1 calc R . . . .
C93 C 0.7164(8) 0.8864(10) 0.3566(2) 0.143(4) Uani 1 1 d G U . . .
H93 H 0.705719 0.905781 0.349603 0.171 Uiso 1 1 calc R . . . .
C112 C 0.6790(5) 0.8280(10) 0.3596(2) 0.137(3) Uani 1 1 d G U . . .
H112 H 0.643178 0.808246 0.354761 0.165 Uiso 1 1 calc DR . . . .
C01X C 0.6950(8) 0.7991(7) 0.3700(2) 0.132(3) Uani 1 1 d G U . . .
C101 C 0.4932(11) 0.4032(12) 0.3658(2) 0.159(4) Uani 1 1 d . U . . .
H101 H 0.498823 0.382270 0.373454 0.190 Uiso 1 1 calc R . . . .
C98 C 0.4690(11) 0.3768(9) 0.3520(3) 0.165(5) Uani 1 1 d G U . . .
H98 H 0.458368 0.338132 0.350375 0.198 Uiso 1 1 calc R . . . .
C174 C 0.4605(11) 0.4080(12) 0.34059(19) 0.165(5) Uani 1 1 d G U . . .
H174 H 0.444314 0.390345 0.331338 0.198 Uiso 1 1 calc R . . . .
C64 C 0.4763(11) 0.4658(12) 0.3430(2) 0.162(5) Uani 1 1 d G U . . .
H64 H 0.470716 0.486697 0.335379 0.195 Uiso 1 1 calc R . . . .
C43 C 0.5006(11) 0.4922(9) 0.3568(3) 0.157(4) Uani 1 1 d G U . . .
H43 H 0.511171 0.530836 0.358457 0.189 Uiso 1 1 calc R . . . .
C56 C 0.5090(10) 0.4609(12) 0.3682(2) 0.155(4) Uani 1 1 d DG U . . .
C70 C 0.6615(7) 0.7696(7) 0.45124(12) 0.114(3) Uani 1 1 d D U . . .
H70A H 0.636600 0.772258 0.458891 0.137 Uiso 1 1 calc R . . . .
H70B H 0.680895 0.750560 0.455753 0.137 Uiso 1 1 calc R . . . .
C1AA C 0.4716(8) 0.8429(8) 0.35669(17) 0.133(3) Uani 1 1 d D U . . .
H1AB H 0.449184 0.861101 0.353820 0.160 Uiso 1 1 calc R . . . .
H1AC H 0.479354 0.848685 0.367532 0.160 Uiso 1 1 calc R . . . .
C14 C 0.6246(5) 0.7340(5) 0.43741(15) 0.108(3) Uani 1 1 d D U . . .
H14 H 0.595404 0.695128 0.440838 0.130 Uiso 1 1 calc R . . . .
C36 C 0.5939(4) 0.7641(7) 0.43025(17) 0.104(3) Uani 1 1 d D U . . .
H36 H 0.573874 0.770859 0.438689 0.125 Uiso 1 1 calc R . . . .
C28 C 0.6002(7) 0.5175(7) 0.43513(12) 0.119(3) Uani 1 1 d D U . . .
H28 H 0.593401 0.505543 0.424426 0.143 Uiso 1 1 calc R . . . .
C23 C 0.5642(7) 0.4643(5) 0.44535(18) 0.116(3) Uani 1 1 d D U . . .
H23A H 0.523268 0.447522 0.443023 0.139 Uiso 1 1 calc R . . . .
H23B H 0.575176 0.435093 0.443475 0.139 Uiso 1 1 calc R . . . .
C19 C 0.6424(7) 1.0491(7) 0.3971(2) 0.130(3) Uani 1 1 d D U . . .
H19A H 0.602010 1.034355 0.394478 0.156 Uiso 1 1 calc R . . . .
H19B H 0.660950 1.090811 0.398382 0.156 Uiso 1 1 calc R . . . .
C5AA C 0.6489(7) 0.9405(5) 0.39721(18) 0.130(3) Uani 1 1 d D U . . .
H5AA H 0.630740 0.898346 0.395937 0.156 Uiso 1 1 calc R . . . .
C25 C 0.6438(7) 0.9684(7) 0.38225(14) 0.128(3) Uani 1 1 d D U . . .
H25A H 0.662499 0.959601 0.374022 0.154 Uiso 1 1 calc R . . . .
H25B H 0.603208 0.952636 0.379635 0.154 Uiso 1 1 calc R . . . .
C29 C 0.7421(5) 1.0326(7) 0.40348(18) 0.130(4) Uani 1 1 d D U . . .
H29 H 0.783180 1.048733 0.406132 0.156 Uiso 1 1 calc R . . . .
C7AA C 0.6467(7) 1.0206(7) 0.41203(15) 0.130(3) Uani 1 1 d D U . . .
H7AA H 0.626949 1.029059 0.420201 0.156 Uiso 1 1 calc R . . . .
C6AA C 0.7112(7) 1.0457(7) 0.41632(15) 0.132(4) Uani 1 1 d D U . . .
H6AA H 0.729394 1.087365 0.417799 0.159 Uiso 1 1 calc R . . . .
H6AB H 0.714185 1.028439 0.425748 0.159 Uiso 1 1 calc R . . . .
C44 C 0.7139(7) 0.9667(7) 0.4012(2) 0.130(3) Uani 1 1 d D U . . .
H44A H 0.717808 0.948839 0.410404 0.155 Uiso 1 1 calc R . . . .
H44B H 0.733518 0.958710 0.393010 0.155 Uiso 1 1 calc R . . . .
C78 C 0.7375(6) 1.0590(7) 0.38842(17) 0.132(4) Uani 1 1 d D U . . .
H78A H 0.756723 1.049806 0.380414 0.158 Uiso 1 1 calc R . . . .
H78B H 0.756674 1.100965 0.389361 0.158 Uiso 1 1 calc R . . . .
C79 C 0.6729(7) 1.0346(7) 0.38428(14) 0.133(4) Uani 1 1 d D U . . .
H79 H 0.670240 1.052210 0.374739 0.160 Uiso 1 1 calc R . . . .
C3AA C 0.4829(7) 0.7972(8) 0.32711(12) 0.136(4) Uani 1 1 d D U . . .
H3AA H 0.475158 0.791645 0.316153 0.163 Uiso 1 1 calc R . . . .
C4AA C 0.5183(8) 0.7683(8) 0.33195(18) 0.141(4) Uani 1 1 d D U . . .
H4AA H 0.496654 0.727143 0.329638 0.169 Uiso 1 1 calc R . . . .
H4AB H 0.554622 0.785485 0.326387 0.169 Uiso 1 1 calc R . . . .
C31 C 0.4247(6) 0.7687(8) 0.33586(18) 0.141(4) Uani 1 1 d D U . . .
H31A H 0.402790 0.727513 0.333536 0.169 Uiso 1 1 calc R . . . .
H31B H 0.401849 0.786093 0.332727 0.169 Uiso 1 1 calc R . . . .
C87 C 0.4366(6) 0.7774(8) 0.35315(17) 0.135(3) Uani 1 1 d D U . . .
H87 H 0.399808 0.759427 0.358747 0.162 Uiso 1 1 calc R . . . .
C111 C 0.5304(6) 0.7772(7) 0.34915(18) 0.135(3) Uani 1 1 d D U . . .
H111 H 0.552957 0.758948 0.352218 0.162 Uiso 1 1 calc DR . . . .
C20 C 0.5659(6) 0.8432(7) 0.35271(19) 0.136(3) Uani 1 1 d D U . . .
H20A H 0.574496 0.849164 0.363510 0.164 Uiso 1 1 calc R . . . .
H20B H 0.602335 0.860893 0.347170 0.164 Uiso 1 1 calc R . . . .
C2AA C 0.5294(7) 0.8713(5) 0.34787(18) 0.141(4) Uani 1 1 d D U . . .
H2AA H 0.551127 0.912998 0.350126 0.169 Uiso 1 1 calc R . . . .
C151 C 0.5175(8) 0.8624(7) 0.33068(16) 0.141(4) Uani 1 1 d D U . . .
H15A H 0.495531 0.880763 0.327470 0.170 Uiso 1 1 calc R . . . .
H15B H 0.553919 0.880307 0.325148 0.170 Uiso 1 1 calc R . . . .
F34 F 0.2744(6) 0.6158(9) 0.55469(17) 0.216(7) Uani 1 1 d D U . . .
Ag1 Ag 0.5225(8) 0.6457(6) 0.42105(18) 0.0805(6) Uani 0.15 1 d . . . A 1


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag01 Ag02 2.865(2) 3_565 ?
Ag01 Ag02 2.865(2) . ?
Ag01 Ag02 2.865(2) 2_665 ?
Ag01 Ag03 2.780(3) 3_565 ?
Ag01 Ag03 2.780(3) 2_665 ?
Ag01 Ag03 2.780(3) . ?
Ag01 Ag05 2.835(3) . ?
Ag01 Ag05 2.835(3) 2_665 ?
Ag01 Ag05 2.835(3) 3_565 ?
Ag01 Ag06 2.8042(19) . ?
Ag01 Ag06 2.8040(19) 2_665 ?
Ag01 Ag06 2.8040(19) 3_565 ?
Ag02 Ag02 3.375(3) 2_665 ?
Ag02 Ag02 3.375(3) 3_565 ?
Ag02 Ag03 2.927(2) 3_565 ?
Ag02 Ag03 2.972(2) . ?
Ag02 Ag04 3.048(3) 3_565 ?
Ag02 Ag04 3.317(3) . ?
Ag02 Ag05 2.8126(17) 3_565 ?
Ag02 Ag07 3.260(3) . ?
Ag02 Ag08 3.113(3) 3_565 ?
Ag02 Cl00 2.693(4) . ?
Ag02 S00G 2.623(5) . ?
Ag03 Ag04 2.9299(18) . ?
Ag03 Ag05 3.082(3) 3_565 ?
Ag03 Ag05 2.811(3) . ?
Ag03 Ag06 2.9859(19) . ?
Ag03 Ag08 2.840(3) . ?
Ag03 Ag09 3.282(2) . ?
Ag03 S00J 2.462(6) . ?
Ag04 Ag08 3.184(2) . ?
Ag04 S00F 2.378(5) . ?
Ag04 S00G 2.410(5) . ?
Ag05 Ag06 2.939(2) . ?
Ag05 Ag06 2.985(2) 2_665 ?
Ag05 Ag08 2.907(2) . ?
Ag05 Ag09 3.053(3) . ?
Ag05 Ag 3.092(4) 2_665 ?
Ag05 Cl1 2.509(5) . ?
Ag05 Ag1 3.197(18) 2_665 ?
Ag06 Ag06 2.765(3) 2_665 ?
Ag06 Ag06 2.765(3) 3_565 ?
Ag06 Ag09 3.187(3) . ?
Ag06 S00K 2.412(6) . ?
Ag07 Ag08 2.887(3) 3_565 ?
Ag07 Ag 2.821(3) . ?
Ag07 S00F 2.632(5) 3_565 ?
Ag07 S00G 2.463(5) . ?
Ag07 S00I 2.447(5) . ?
Ag07 Ag1 3.049(16) . ?
Ag08 Ag09 3.215(2) . ?
Ag08 S00F 2.478(4) . ?
Ag08 S00L 2.450(6) . ?
Ag09 S00K 2.370(6) . ?
Ag09 S00L 2.371(7) . ?
Ag Ag0D 3.159(3) . ?
Ag Cl1 2.834(5) 3_565 ?
Ag S00I 2.398(7) . ?
Ag S00J 2.464(7) . ?
Ag0B Cl1 2.811(6) 3_565 ?
Ag0B S00J 2.578(5) . ?
Ag0B S00K 2.572(7) . ?
Ag0B P00N 2.377(7) . ?
Ag0B Ag1 3.234(15) . ?
Sb0C F01V 1.554(6) . ?
Sb0C F02D 1.528(7) . ?
Sb0C F34 1.523(5) 3_565 ?
Sb0C F34 1.523(5) . ?
Sb0C F34 1.523(5) 2_665 ?
Ag0D S00I 2.547(5) . ?
Ag0D S00L 2.583(8) 3_565 ?
Ag0D P00P 2.378(8) . ?
S00F C00Y 1.89(2) . ?
S00G C00R 1.85(2) . ?
S00I C016 1.812(15) . ?
S00I Ag1 2.881(16) . ?
S00J C36 1.828(13) . ?
S00J Ag1 1.913(15) . ?
S00K C92 1.874(16) . ?
S00L C01E 1.780(16) . ?
P00N C01F 1.821(15) . ?
P00N C018 1.91(4) . ?
P00N C01X 1.950(18) . ?
P00P C61 1.88(2) . ?
P00P C94 1.80(4) . ?
P00P C56 1.911(9) . ?
C00R C00U 1.46(3) . ?
C00R C014 1.56(3) . ?
C00T C01G 1.50(3) . ?
C00T C01P 1.43(3) . ?
C00U C00Z 1.50(3) . ?
C00U C013 1.50(3) . ?
C00V C015 1.51(3) . ?
C00V C01K 1.36(3) . ?
C00W C00Y 1.49(3) . ?
C00W C019 1.62(3) . ?
C00W C01O 1.51(3) . ?
C00X C01F 1.3900 . ?
C00X C01A 1.3900 . ?
C01F C02N 1.3900 . ?
C02N C02P 1.3900 . ?
C02P C01W 1.3900 . ?
C01W C01A 1.3900 . ?
C00Y C01K 1.47(3) . ?
C00Z C01P 1.53(3) . ?
C010 C011 1.544(8) . ?
C010 C01B 1.550(8) . ?
C010 C36 1.543(8) . ?
C011 C021 1.526(8) . ?
C013 C01G 1.54(3) . ?
C014 C017 1.55(3) . ?
C014 C023 1.61(3) . ?
C015 C019 1.58(3) . ?
C015 C01T 1.43(3) . ?
C016 C01Q 1.545(8) . ?
C016 C28 1.542(8) . ?
C017 C01P 1.57(3) . ?
C018 C01N 1.60(4) . ?
C01B C02L 1.550(8) . ?
C01D C021 1.534(8) . ?
C01D C02L 1.540(8) . ?
C01E C5AA 1.545(8) . ?
C01E C7AA 1.538(8) . ?
C01G C023 1.49(3) . ?
C01J C01K 1.60(3) . ?
C01J C01L 1.45(3) . ?
C01L C01O 1.42(3) . ?
C01L C01T 1.64(3) . ?
C01N C94 1.46(4) . ?
C01Q C01Z 1.539(8) . ?
C01Q C02O 1.547(8) . ?
C01Z C020 1.545(8) . ?
C020 C02K 1.541(8) . ?
C020 C23 1.538(8) . ?
C021 C02Q 1.543(8) . ?
C025 C02K 1.546(8) . ?
C025 C02O 1.534(8) . ?
C025 C188 1.531(9) . ?
C02L C70 1.545(8) . ?
C02Q C14 1.542(8) . ?
C37 C110 1.3900 . ?
C37 C61 1.3900 . ?
C110 C0AA 1.3900 . ?
C0AA C76 1.3900 . ?
C76 C135 1.3900 . ?
C135 C61 1.3900 . ?
C92 C87 1.549(8) . ?
C92 C111 1.533(8) . ?
C188 C28 1.550(8) . ?
C115 C34 1.3900 . ?
C115 C01X 1.3900 . ?
C34 C184 1.3900 . ?
C184 C93 1.3900 . ?
C93 C112 1.3900 . ?
C112 C01X 1.3900 . ?
C101 C98 1.3900 . ?
C101 C56 1.3900 . ?
C98 C174 1.3900 . ?
C174 C64 1.3900 . ?
C64 C43 1.3900 . ?
C43 C56 1.3900 . ?
C70 C14 1.550(8) . ?
C1AA C87 1.543(8) . ?
C1AA C2AA 1.539(8) . ?
C14 C36 1.535(8) . ?
C28 C23 1.540(8) . ?
C19 C7AA 1.548(8) . ?
C19 C79 1.544(8) . ?
C5AA C25 1.549(8) . ?
C5AA C44 1.547(8) . ?
C25 C79 1.537(8) . ?
C29 C6AA 1.535(8) . ?
C29 C44 1.537(8) . ?
C29 C78 1.531(8) . ?
C7AA C6AA 1.543(8) . ?
C78 C79 1.545(8) . ?
C3AA C4AA 1.540(8) . ?
C3AA C31 1.544(8) . ?
C3AA C151 1.536(8) . ?
C4AA C111 1.538(8) . ?
C31 C87 1.546(8) . ?
C111 C20 1.553(8) . ?
C20 C2AA 1.552(8) . ?
C2AA C151 1.537(8) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Ag02 Ag01 Ag02 72.16(6) 2_665 . ?
Ag02 Ag01 Ag02 72.16(6) 2_665 3_565 ?
Ag02 Ag01 Ag02 72.16(6) 3_565 . ?
Ag03 Ag01 Ag02 123.52(7) 3_565 2_665 ?
Ag03 Ag01 Ag02 123.52(7) . 3_565 ?
Ag03 Ag01 Ag02 62.45(4) 3_565 . ?
Ag03 Ag01 Ag02 62.44(4) . 2_665 ?
Ag03 Ag01 Ag02 123.52(7) 2_665 . ?
Ag03 Ag01 Ag02 62.45(4) 2_665 3_565 ?
Ag03 Ag01 Ag02 63.52(4) . . ?
Ag03 Ag01 Ag02 63.52(4) 3_565 3_565 ?
Ag03 Ag01 Ag02 63.52(4) 2_665 2_665 ?
Ag03 Ag01 Ag03 117.43(2) 3_565 . ?
Ag03 Ag01 Ag03 117.43(2) 2_665 . ?
Ag03 Ag01 Ag03 117.43(2) 2_665 3_565 ?
Ag03 Ag01 Ag05 60.06(4) 2_665 2_665 ?
Ag03 Ag01 Ag05 175.71(5) 2_665 3_565 ?
Ag03 Ag01 Ag05 66.56(4) 3_565 2_665 ?
Ag03 Ag01 Ag05 60.06(4) . . ?
Ag03 Ag01 Ag05 175.71(5) . 2_665 ?
Ag03 Ag01 Ag05 60.06(4) 3_565 3_565 ?
Ag03 Ag01 Ag05 66.56(4) 2_665 . ?
Ag03 Ag01 Ag05 175.71(5) 3_565 . ?
Ag03 Ag01 Ag05 66.56(4) . 3_565 ?
Ag03 Ag01 Ag06 113.15(5) 2_665 3_565 ?
Ag03 Ag01 Ag06 113.15(5) 3_565 . ?
Ag03 Ag01 Ag06 64.65(5) 2_665 2_665 ?
Ag03 Ag01 Ag06 64.65(5) 3_565 3_565 ?
Ag03 Ag01 Ag06 64.65(5) . . ?
Ag03 Ag01 Ag06 115.76(5) . 3_565 ?
Ag03 Ag01 Ag06 115.76(5) 3_565 2_665 ?
Ag03 Ag01 Ag06 113.15(5) . 2_665 ?
Ag03 Ag01 Ag06 115.76(5) 2_665 . ?
Ag05 Ag01 Ag02 59.12(5) . 2_665 ?
Ag05 Ag01 Ag02 117.20(4) . . ?
Ag05 Ag01 Ag02 117.20(4) 3_565 3_565 ?
Ag05 Ag01 Ag02 59.12(5) 2_665 3_565 ?
Ag05 Ag01 Ag02 59.12(5) 3_565 . ?
Ag05 Ag01 Ag02 120.69(5) . 3_565 ?
Ag05 Ag01 Ag02 120.69(5) 3_565 2_665 ?
Ag05 Ag01 Ag02 120.69(5) 2_665 . ?
Ag05 Ag01 Ag02 117.20(4) 2_665 2_665 ?
Ag05 Ag01 Ag05 115.85(3) 2_665 . ?
Ag05 Ag01 Ag05 115.85(3) . 3_565 ?
Ag05 Ag01 Ag05 115.85(3) 2_665 3_565 ?
Ag06 Ag01 Ag02 114.75(5) 2_665 3_565 ?
Ag06 Ag01 Ag02 113.56(5) . . ?
Ag06 Ag01 Ag02 171.80(5) 2_665 . ?
Ag06 Ag01 Ag02 113.56(5) 3_565 3_565 ?
Ag06 Ag01 Ag02 171.80(5) . 3_565 ?
Ag06 Ag01 Ag02 114.75(5) 3_565 . ?
Ag06 Ag01 Ag02 114.75(5) . 2_665 ?
Ag06 Ag01 Ag02 171.80(5) 3_565 2_665 ?
Ag06 Ag01 Ag02 113.56(5) 2_665 2_665 ?
Ag06 Ag01 Ag05 63.92(4) . 3_565 ?
Ag06 Ag01 Ag05 62.81(4) 2_665 2_665 ?
Ag06 Ag01 Ag05 112.78(7) 3_565 . ?
Ag06 Ag01 Ag05 62.81(4) . . ?
Ag06 Ag01 Ag05 112.78(7) 2_665 3_565 ?
Ag06 Ag01 Ag05 63.92(4) 2_665 . ?
Ag06 Ag01 Ag05 63.92(4) 3_565 2_665 ?
Ag06 Ag01 Ag05 112.78(7) . 2_665 ?
Ag06 Ag01 Ag05 62.81(4) 3_565 3_565 ?
Ag06 Ag01 Ag06 59.09(7) 2_665 . ?
Ag06 Ag01 Ag06 59.09(7) 2_665 3_565 ?
Ag06 Ag01 Ag06 59.09(7) 3_565 . ?
Ag01 Ag02 Ag02 53.92(3) . 2_665 ?
Ag01 Ag02 Ag02 53.92(3) . 3_565 ?
Ag01 Ag02 Ag03 57.34(4) . 3_565 ?
Ag01 Ag02 Ag03 56.84(4) . . ?
Ag01 Ag02 Ag04 99.64(5) . . ?
Ag01 Ag02 Ag04 106.28(5) . 3_565 ?
Ag01 Ag02 Ag07 146.33(5) . . ?
Ag01 Ag02 Ag08 104.84(5) . 3_565 ?
Ag02 Ag02 Ag02 60.0 2_665 3_565 ?
Ag03 Ag02 Ag02 54.48(4) . 2_665 ?
Ag03 Ag02 Ag02 55.73(5) 3_565 3_565 ?
Ag03 Ag02 Ag02 102.99(4) . 3_565 ?
Ag03 Ag02 Ag02 103.99(4) 3_565 2_665 ?
Ag03 Ag02 Ag03 107.28(7) 3_565 . ?
Ag03 Ag02 Ag04 163.09(5) . 3_565 ?
Ag03 Ag02 Ag04 156.72(5) 3_565 . ?
Ag03 Ag02 Ag04 55.21(5) . . ?
Ag03 Ag02 Ag04 58.69(6) 3_565 3_565 ?
Ag03 Ag02 Ag07 107.70(5) . . ?
Ag03 Ag02 Ag07 109.75(5) 3_565 . ?
Ag03 Ag02 Ag08 55.98(4) 3_565 3_565 ?
Ag03 Ag02 Ag08 119.82(6) . 3_565 ?
Ag04 Ag02 Ag02 54.18(4) . 2_665 ?
Ag04 Ag02 Ag02 109.61(4) . 3_565 ?
Ag04 Ag02 Ag02 61.94(5) 3_565 3_565 ?
Ag04 Ag02 Ag02 116.65(4) 3_565 2_665 ?
Ag04 Ag02 Ag04 134.57(6) 3_565 . ?
Ag04 Ag02 Ag07 87.10(5) 3_565 . ?
Ag04 Ag02 Ag08 62.24(5) 3_565 3_565 ?
Ag05 Ag02 Ag01 59.91(6) 3_565 . ?
Ag05 Ag02 Ag02 106.03(4) 3_565 2_665 ?
Ag05 Ag02 Ag02 103.33(4) 3_565 3_565 ?
Ag05 Ag02 Ag03 58.59(5) 3_565 3_565 ?
Ag05 Ag02 Ag03 64.31(5) 3_565 . ?
Ag05 Ag02 Ag04 109.76(6) 3_565 3_565 ?
Ag05 Ag02 Ag04 115.47(5) 3_565 . ?
Ag05 Ag02 Ag07 86.60(5) 3_565 . ?
Ag05 Ag02 Ag08 58.49(4) 3_565 3_565 ?
Ag07 Ag02 Ag02 149.04(6) . 3_565 ?
Ag07 Ag02 Ag02 145.65(6) . 2_665 ?
Ag07 Ag02 Ag04 91.48(5) . . ?
Ag08 Ag02 Ag02 106.54(6) 3_565 3_565 ?
Ag08 Ag02 Ag02 158.50(4) 3_565 2_665 ?
Ag08 Ag02 Ag04 143.60(6) 3_565 . ?
Ag08 Ag02 Ag07 53.80(4) 3_565 . ?
Cl00 Ag02 Ag01 90.81(11) . . ?
Cl00 Ag02 Ag02 51.20(7) . 3_565 ?
Cl00 Ag02 Ag02 51.21(7) . 2_665 ?
Cl00 Ag02 Ag03 104.78(7) . 3_565 ?
Cl00 Ag02 Ag03 103.57(7) . . ?
Cl00 Ag02 Ag04 69.25(4) . . ?
Cl00 Ag02 Ag04 73.67(5) . 3_565 ?
Cl00 Ag02 Ag05 150.58(10) . 3_565 ?
Cl00 Ag02 Ag07 122.79(10) . . ?
Cl00 Ag02 Ag08 135.69(6) . 3_565 ?
S00G Ag02 Ag01 143.46(11) . . ?
S00G Ag02 Ag02 98.89(11) . 2_665 ?
S00G Ag02 Ag02 138.51(10) . 3_565 ?
S00G Ag02 Ag03 88.17(12) . . ?
S00G Ag02 Ag03 156.96(11) . 3_565 ?
S00G Ag02 Ag04 46.06(10) . . ?
S00G Ag02 Ag04 108.16(12) . 3_565 ?
S00G Ag02 Ag05 117.32(11) . 3_565 ?
S00G Ag02 Ag07 48.00(10) . . ?
S00G Ag02 Ag08 101.67(11) . 3_565 ?
S00G Ag02 Cl00 87.42(13) . . ?
Ag01 Ag03 Ag02 59.65(5) . . ?
Ag01 Ag03 Ag02 60.21(5) . 2_665 ?
Ag01 Ag03 Ag04 111.94(6) . . ?
Ag01 Ag03 Ag05 57.58(3) . 3_565 ?
Ag01 Ag03 Ag05 60.95(4) . . ?
Ag01 Ag03 Ag06 58.07(5) . . ?
Ag01 Ag03 Ag08 115.04(5) . . ?
Ag01 Ag03 Ag09 108.80(6) . . ?
Ag02 Ag03 Ag02 69.79(6) 2_665 . ?
Ag02 Ag03 Ag04 62.71(5) 2_665 . ?
Ag02 Ag03 Ag05 55.33(5) . 3_565 ?
Ag02 Ag03 Ag05 111.05(5) 2_665 3_565 ?
Ag02 Ag03 Ag06 105.52(6) . . ?
Ag02 Ag03 Ag06 107.72(6) 2_665 . ?
Ag02 Ag03 Ag09 166.40(6) . . ?
Ag02 Ag03 Ag09 112.02(6) 2_665 . ?
Ag04 Ag03 Ag02 68.38(5) . . ?
Ag04 Ag03 Ag05 119.37(5) . 3_565 ?
Ag04 Ag03 Ag06 169.70(6) . . ?
Ag04 Ag03 Ag09 124.87(7) . . ?
Ag05 Ag03 Ag02 114.56(5) . . ?
Ag05 Ag03 Ag02 58.67(6) . 2_665 ?
Ag05 Ag03 Ag04 113.30(5) . . ?
Ag05 Ag03 Ag05 109.19(6) . 3_565 ?
Ag05 Ag03 Ag06 60.83(4) . . ?
Ag05 Ag03 Ag08 61.93(5) . . ?
Ag05 Ag03 Ag09 59.54(5) . . ?
Ag05 Ag03 Ag09 113.34(6) 3_565 . ?
Ag06 Ag03 Ag05 58.92(4) . 3_565 ?
Ag06 Ag03 Ag09 60.91(6) . . ?
Ag08 Ag03 Ag02 65.33(5) . 2_665 ?
Ag08 Ag03 Ag02 127.04(6) . . ?
Ag08 Ag03 Ag04 66.98(4) . . ?
Ag08 Ag03 Ag05 171.11(6) . 3_565 ?
Ag08 Ag03 Ag06 113.62(6) . . ?
Ag08 Ag03 Ag09 62.87(6) . . ?
S00J Ag03 Ag01 135.73(14) . . ?
S00J Ag03 Ag02 100.72(14) . . ?
S00J Ag03 Ag02 155.27(12) . 2_665 ?
S00J Ag03 Ag04 92.62(12) . . ?
S00J Ag03 Ag05 141.72(13) . . ?
S00J Ag03 Ag05 78.42(14) . 3_565 ?
S00J Ag03 Ag06 96.77(12) . . ?
S00J Ag03 Ag08 108.28(15) . . ?
S00J Ag03 Ag09 82.72(13) . . ?
Ag02 Ag04 Ag02 63.88(5) 2_665 . ?
Ag02 Ag04 Ag08 59.89(4) 2_665 . ?
Ag03 Ag04 Ag02 56.41(4) . . ?
Ag03 Ag04 Ag02 58.60(4) . 2_665 ?
Ag03 Ag04 Ag08 55.16(5) . . ?
Ag08 Ag04 Ag02 106.28(6) . . ?
S00F Ag04 Ag02 143.83(13) . . ?
S00F Ag04 Ag02 79.95(12) . 2_665 ?
S00F Ag04 Ag03 105.29(11) . . ?
S00F Ag04 Ag08 50.39(11) . . ?
S00F Ag04 S00G 161.03(16) . . ?
S00G Ag04 Ag02 51.60(12) . . ?
S00G Ag04 Ag02 113.72(12) . 2_665 ?
S00G Ag04 Ag03 93.34(11) . . ?
S00G Ag04 Ag08 147.42(11) . . ?
Ag01 Ag05 Ag03 55.85(3) . 2_665 ?
Ag01 Ag05 Ag06 58.08(5) . . ?
Ag01 Ag05 Ag06 57.53(5) . 2_665 ?
Ag01 Ag05 Ag08 111.27(6) . . ?
Ag01 Ag05 Ag09 113.93(6) . . ?
Ag01 Ag05 Ag 133.96(6) . 2_665 ?
Ag01 Ag05 Ag1 124.8(3) . 2_665 ?
Ag02 Ag05 Ag01 60.97(5) 2_665 . ?
Ag02 Ag05 Ag03 60.36(4) 2_665 2_665 ?
Ag02 Ag05 Ag06 109.75(6) 2_665 2_665 ?
Ag02 Ag05 Ag06 112.24(6) 2_665 . ?
Ag02 Ag05 Ag08 65.93(6) 2_665 . ?
Ag02 Ag05 Ag09 122.84(6) 2_665 . ?
Ag02 Ag05 Ag 84.85(6) 2_665 2_665 ?
Ag02 Ag05 Ag1 82.0(3) 2_665 2_665 ?
Ag03 Ag05 Ag01 58.99(4) . . ?
Ag03 Ag05 Ag02 62.74(4) . 2_665 ?
Ag03 Ag05 Ag03 107.39(6) . 2_665 ?
Ag03 Ag05 Ag06 107.00(6) . 2_665 ?
Ag03 Ag05 Ag06 62.53(6) . . ?
Ag03 Ag05 Ag08 59.53(5) . . ?
Ag03 Ag05 Ag09 67.94(6) . . ?
Ag03 Ag05 Ag 132.63(7) . 2_665 ?
Ag03 Ag05 Ag 81.31(6) 2_665 2_665 ?
Ag03 Ag05 Ag1 137.0(3) . 2_665 ?
Ag03 Ag05 Ag1 70.9(3) 2_665 2_665 ?
Ag06 Ag05 Ag03 58.94(5) 2_665 2_665 ?
Ag06 Ag05 Ag03 103.51(5) . 2_665 ?
Ag06 Ag05 Ag06 55.65(6) . 2_665 ?
Ag06 Ag05 Ag09 64.25(5) . . ?
Ag06 Ag05 Ag09 110.73(6) 2_665 . ?
Ag06 Ag05 Ag 162.53(6) . 2_665 ?
Ag06 Ag05 Ag 116.46(6) 2_665 2_665 ?
Ag06 Ag05 Ag1 160.4(3) . 2_665 ?
Ag06 Ag05 Ag1 107.7(3) 2_665 2_665 ?
Ag08 Ag05 Ag03 123.08(6) . 2_665 ?
Ag08 Ag05 Ag06 113.04(6) . . ?
Ag08 Ag05 Ag06 166.52(6) . 2_665 ?
Ag08 Ag05 Ag09 65.23(6) . . ?
Ag08 Ag05 Ag 76.48(6) . 2_665 ?
Ag08 Ag05 Ag1 84.7(3) . 2_665 ?
Ag09 Ag05 Ag03 167.76(6) . 2_665 ?
Ag09 Ag05 Ag 110.33(6) . 2_665 ?
Ag09 Ag05 Ag1 120.5(3) . 2_665 ?
Ag Ag05 Ag1 10.7(2) 2_665 2_665 ?
Cl1 Ag05 Ag01 145.18(12) . . ?
Cl1 Ag05 Ag02 144.56(12) . 2_665 ?
Cl1 Ag05 Ag03 109.49(13) . 2_665 ?
Cl1 Ag05 Ag03 142.72(13) . . ?
Cl1 Ag05 Ag06 103.10(12) . . ?
Cl1 Ag05 Ag06 87.67(12) . 2_665 ?
Cl1 Ag05 Ag08 103.00(13) . . ?
Cl1 Ag05 Ag09 74.84(13) . . ?
Cl1 Ag05 Ag 59.72(12) . 2_665 ?
Cl1 Ag05 Ag1 63.1(3) . 2_665 ?
Ag01 Ag06 Ag03 57.28(6) . . ?
Ag01 Ag06 Ag05 59.12(4) . . ?
Ag01 Ag06 Ag05 58.55(4) . 3_565 ?
Ag01 Ag06 Ag09 110.84(5) . . ?
Ag03 Ag06 Ag09 64.15(5) . . ?
Ag05 Ag06 Ag03 62.14(5) 3_565 . ?
Ag05 Ag06 Ag03 56.63(5) . . ?
Ag05 Ag06 Ag05 108.41(7) . 3_565 ?
Ag05 Ag06 Ag09 118.95(6) 3_565 . ?
Ag05 Ag06 Ag09 59.62(5) . . ?
Ag06 Ag06 Ag01 60.45(3) 2_665 . ?
Ag06 Ag06 Ag01 60.45(3) 3_565 . ?
Ag06 Ag06 Ag03 110.57(4) 3_565 . ?
Ag06 Ag06 Ag03 108.19(4) 2_665 . ?
Ag06 Ag06 Ag05 63.03(6) 2_665 . ?
Ag06 Ag06 Ag05 109.46(5) 2_665 3_565 ?
Ag06 Ag06 Ag05 61.32(5) 3_565 3_565 ?
Ag06 Ag06 Ag05 110.82(5) 3_565 . ?
Ag06 Ag06 Ag06 60.0 2_665 3_565 ?
Ag06 Ag06 Ag09 112.96(8) 2_665 . ?
Ag06 Ag06 Ag09 170.38(6) 3_565 . ?
S00K Ag06 Ag01 149.41(14) . . ?
S00K Ag06 Ag03 92.16(14) . . ?
S00K Ag06 Ag05 108.63(15) . 3_565 ?
S00K Ag06 Ag05 107.12(16) . . ?
S00K Ag06 Ag06 141.78(16) . 2_665 ?
S00K Ag06 Ag06 141.98(16) . 3_565 ?
S00K Ag06 Ag09 47.63(15) . . ?
Ag08 Ag07 Ag02 60.51(5) 3_565 . ?
Ag08 Ag07 Ag1 87.9(3) 3_565 . ?
Ag Ag07 Ag02 81.64(6) . . ?
S00F Ag07 Ag02 72.57(10) 3_565 . ?
S00F Ag07 Ag08 53.13(10) 3_565 3_565 ?
S00F Ag07 Ag 134.12(11) 3_565 . ?
S00F Ag07 Ag1 139.0(4) 3_565 . ?
S00G Ag07 Ag02 52.33(11) . . ?
S00G Ag07 Ag08 112.67(12) . 3_565 ?
S00G Ag07 Ag 92.99(13) . . ?
S00G Ag07 S00F 99.89(16) . 3_565 ?
S00G Ag07 Ag1 82.6(3) . . ?
S00I Ag07 Ag02 128.64(14) . . ?
S00I Ag07 Ag08 86.38(15) . 3_565 ?
S00I Ag07 Ag 53.58(15) . . ?
S00I Ag07 S00F 119.3(2) . 3_565 ?
S00I Ag07 S00G 139.7(2) . . ?
S00I Ag07 Ag1 62.1(3) . . ?
Ag1 Ag07 Ag02 77.5(3) . . ?
Ag02 Ag08 Ag04 57.87(4) 2_665 . ?
Ag02 Ag08 Ag09 109.00(6) 2_665 . ?
Ag03 Ag08 Ag02 58.69(5) . 2_665 ?
Ag03 Ag08 Ag04 57.86(6) . . ?
Ag03 Ag08 Ag05 58.54(5) . . ?
Ag03 Ag08 Ag07 124.34(7) . 2_665 ?
Ag03 Ag08 Ag09 65.32(5) . . ?
Ag04 Ag08 Ag09 118.85(7) . . ?
Ag05 Ag08 Ag02 55.57(5) . 2_665 ?
Ag05 Ag08 Ag04 103.76(7) . . ?
Ag05 Ag08 Ag09 59.57(5) . . ?
Ag07 Ag08 Ag02 65.70(5) 2_665 2_665 ?
Ag07 Ag08 Ag04 91.36(6) 2_665 . ?
Ag07 Ag08 Ag05 92.27(7) 2_665 . ?
Ag07 Ag08 Ag09 141.61(7) 2_665 . ?
S00F Ag08 Ag02 77.20(12) . 2_665 ?
S00F Ag08 Ag03 105.29(12) . . ?
S00F Ag08 Ag04 47.68(11) . . ?
S00F Ag08 Ag05 132.14(13) . . ?
S00F Ag08 Ag07 58.16(12) . 2_665 ?
S00F Ag08 Ag09 160.23(13) . . ?
S00L Ag08 Ag02 142.51(18) . 2_665 ?
S00L Ag08 Ag03 112.23(16) . . ?
S00L Ag08 Ag04 153.03(19) . . ?
S00L Ag08 Ag05 87.94(17) . . ?
S00L Ag08 Ag07 112.68(17) . 2_665 ?
S00L Ag08 Ag09 47.14(15) . . ?
S00L Ag08 S00F 136.1(2) . . ?
Ag05 Ag09 Ag03 52.52(4) . . ?
Ag05 Ag09 Ag06 56.13(4) . . ?
Ag05 Ag09 Ag08 55.20(5) . . ?
Ag06 Ag09 Ag03 54.94(5) . . ?
Ag06 Ag09 Ag08 99.21(5) . . ?
Ag08 Ag09 Ag03 51.82(5) . . ?
S00K Ag09 Ag03 85.89(15) . . ?
S00K Ag09 Ag05 104.77(15) . . ?
S00K Ag09 Ag06 48.77(14) . . ?
S00K Ag09 Ag08 137.55(15) . . ?
S00K Ag09 S00L 169.2(2) . . ?
S00L Ag09 Ag03 100.88(16) . . ?
S00L Ag09 Ag05 86.04(16) . . ?
S00L Ag09 Ag06 141.99(16) . . ?
S00L Ag09 Ag08 49.24(15) . . ?
Ag05 Ag Ag0D 92.52(8) 3_565 . ?
Ag07 Ag Ag05 89.78(8) . 3_565 ?
Ag07 Ag Ag0D 97.98(8) . . ?
Ag07 Ag Cl1 129.73(15) . 3_565 ?
Cl1 Ag Ag05 49.87(10) 3_565 3_565 ?
Cl1 Ag Ag0D 61.83(12) 3_565 . ?
S00I Ag Ag05 117.64(18) . 3_565 ?
S00I Ag Ag07 55.21(13) . . ?
S00I Ag Ag0D 52.41(14) . . ?
S00I Ag Cl1 112.64(18) . 3_565 ?
S00I Ag S00J 160.0(2) . . ?
S00J Ag Ag05 78.20(14) . 3_565 ?
S00J Ag Ag07 116.48(13) . . ?
S00J Ag Ag0D 143.98(14) . . ?
S00J Ag Cl1 86.79(16) . 3_565 ?
Cl1 Ag0B Ag1 60.0(3) 3_565 . ?
S00J Ag0B Cl1 85.14(16) . 3_565 ?
S00J Ag0B Ag1 36.3(3) . . ?
S00K Ag0B Cl1 92.55(18) . 3_565 ?
S00K Ag0B S00J 92.42(17) . . ?
S00K Ag0B Ag1 117.0(3) . . ?
P00N Ag0B Cl1 116.4(3) . 3_565 ?
P00N Ag0B S00J 136.9(2) . . ?
P00N Ag0B S00K 121.1(3) . . ?
P00N Ag0B Ag1 121.9(4) . . ?
F02D Sb0C F01V 180.0 . . ?
F34 Sb0C F01V 75.2(6) 3_565 . ?
F34 Sb0C F01V 75.2(6) . . ?
F34 Sb0C F01V 75.2(6) 2_665 . ?
F34 Sb0C F02D 104.8(6) . . ?
F34 Sb0C F02D 104.8(6) 3_565 . ?
F34 Sb0C F02D 104.8(6) 2_665 . ?
F34 Sb0C F34 113.7(5) . 2_665 ?
F34 Sb0C F34 113.7(5) 3_565 2_665 ?
F34 Sb0C F34 113.7(5) 3_565 . ?
S00I Ag0D Ag 48.24(15) . . ?
S00I Ag0D S00L 91.7(2) . 3_565 ?
S00L Ag0D Ag 91.22(14) 3_565 . ?
P00P Ag0D Ag 122.2(3) . . ?
P00P Ag0D S00I 126.8(3) . . ?
P00P Ag0D S00L 139.6(3) . 3_565 ?
Ag02 Cl00 Ag02 77.59(14) 2_665 . ?
Ag02 Cl00 Ag02 77.59(14) 3_565 . ?
Ag02 Cl00 Ag02 77.59(14) 2_665 3_565 ?
Ag04 S00F Ag07 120.38(18) . 2_665 ?
Ag04 S00F Ag08 81.93(14) . . ?
Ag08 S00F Ag07 68.72(12) . 2_665 ?
C00Y S00F Ag04 114.7(7) . . ?
C00Y S00F Ag07 122.2(8) . 2_665 ?
C00Y S00F Ag08 104.6(7) . . ?
Ag04 S00G Ag02 82.34(14) . . ?
Ag04 S00G Ag07 150.3(2) . . ?
Ag07 S00G Ag02 79.67(14) . . ?
C00R S00G Ag02 105.9(7) . . ?
C00R S00G Ag04 102.6(6) . . ?
C00R S00G Ag07 104.9(6) . . ?
Ag05 Cl1 Ag 70.41(12) . 2_665 ?
Ag05 Cl1 Ag0B 105.58(17) . 2_665 ?
Ag0B Cl1 Ag 76.37(14) 2_665 2_665 ?
Ag07 S00I Ag0D 129.5(2) . . ?
Ag07 S00I Ag1 69.3(4) . . ?
Ag S00I Ag07 71.21(17) . . ?
Ag S00I Ag0D 79.35(18) . . ?
Ag0D S00I Ag1 85.7(4) . . ?
C016 S00I Ag07 109.6(6) . . ?
C016 S00I Ag 103.9(6) . . ?
C016 S00I Ag0D 116.9(5) . . ?
C016 S00I Ag1 97.6(7) . . ?
Ag03 S00J Ag 109.5(2) . . ?
Ag03 S00J Ag0B 117.0(2) . . ?
Ag S00J Ag0B 87.57(18) . . ?
C36 S00J Ag03 109.7(5) . . ?
C36 S00J Ag 105.7(6) . . ?
C36 S00J Ag0B 123.4(5) . . ?
C36 S00J Ag1 99.8(8) . . ?
Ag1 S00J Ag03 112.2(6) . . ?
Ag1 S00J Ag0B 90.9(5) . . ?
Ag06 S00K Ag0B 109.4(2) . . ?
Ag09 S00K Ag06 83.60(17) . . ?
Ag09 S00K Ag0B 110.1(2) . . ?
C92 S00K Ag06 97.0(5) . . ?
C92 S00K Ag09 119.3(6) . . ?
C92 S00K Ag0B 125.9(6) . . ?
Ag08 S00L Ag0D 109.6(2) . 2_665 ?
Ag09 S00L Ag08 83.6(2) . . ?
Ag09 S00L Ag0D 121.5(3) . 2_665 ?
C01E S00L Ag08 111.5(6) . . ?
C01E S00L Ag09 109.3(6) . . ?
C01E S00L Ag0D 116.5(6) . 2_665 ?
C01F P00N Ag0B 113.5(7) . . ?
C01F P00N C018 103.6(12) . . ?
C01F P00N C01X 103.0(10) . . ?
C018 P00N Ag0B 113.3(10) . . ?
C018 P00N C01X 112.2(13) . . ?
C01X P00N Ag0B 110.6(7) . . ?
C61 P00P Ag0D 112.2(8) . . ?
C61 P00P C56 117.5(12) . . ?
C94 P00P Ag0D 112.1(11) . . ?
C94 P00P C61 104.2(16) . . ?
C94 P00P C56 102.7(15) . . ?
C56 P00P Ag0D 107.8(9) . . ?
C00U C00R S00G 113.5(14) . . ?
C00U C00R C014 109.0(15) . . ?
C014 C00R S00G 108.4(14) . . ?
C01P C00T C01G 116.6(17) . . ?
C00R C00U C00Z 109.4(17) . . ?
C00R C00U C013 115.7(17) . . ?
C00Z C00U C013 104.3(16) . . ?
C01K C00V C015 113(2) . . ?
C00Y C00W C019 108.7(18) . . ?
C00Y C00W C01O 110(2) . . ?
C01O C00W C019 106.4(17) . . ?
C01F C00X C01A 120.0 . . ?
C00X C01F P00N 118.5(10) . . ?
C02N C01F P00N 121.5(11) . . ?
C02N C01F C00X 120.0 . . ?
C01F C02N C02P 120.0 . . ?
C01W C02P C02N 120.0 . . ?
C01A C01W C02P 120.0 . . ?
C01W C01A C00X 120.0 . . ?
C00W C00Y S00F 111.7(16) . . ?
C01K C00Y S00F 108.2(16) . . ?
C01K C00Y C00W 110.9(18) . . ?
C00U C00Z C01P 113.1(18) . . ?
C011 C010 C01B 108.8(6) . . ?
C36 C010 C011 109.8(5) . . ?
C36 C010 C01B 108.4(6) . . ?
C021 C011 C010 110.2(4) . . ?
C00U C013 C01G 111.9(17) . . ?
C00R C014 C023 110.7(17) . . ?
C017 C014 C00R 105.3(17) . . ?
C017 C014 C023 108.3(15) . . ?
C00V C015 C019 103.7(17) . . ?
C01T C015 C00V 115(2) . . ?
C01T C015 C019 115(2) . . ?
C01Q C016 S00I 114.8(9) . . ?
C28 C016 S00I 110.0(9) . . ?
C28 C016 C01Q 109.5(4) . . ?
C014 C017 C01P 111.3(17) . . ?
C01N C018 P00N 117(2) . . ?
C015 C019 C00W 103.6(19) . . ?
C010 C01B C02L 109.4(4) . . ?
C021 C01D C02L 109.8(4) . . ?
C5AA C01E S00L 113.3(9) . . ?
C7AA C01E S00L 114.7(10) . . ?
C7AA C01E C5AA 109.7(4) . . ?
C00T C01G C013 104.4(17) . . ?
C023 C01G C00T 109.2(18) . . ?
C023 C01G C013 110.6(16) . . ?
C01L C01J C01K 115(2) . . ?
C00V C01K C00Y 115(2) . . ?
C00V C01K C01J 108.3(19) . . ?
C00Y C01K C01J 101.9(19) . . ?
C01J C01L C01T 102.8(19) . . ?
C01O C01L C01J 110(2) . . ?
C01O C01L C01T 107(2) . . ?
C94 C01N C018 109(3) . . ?
C01L C01O C00W 115(2) . . ?
C00T C01P C00Z 108.8(18) . . ?
C00T C01P C017 108.4(18) . . ?
C00Z C01P C017 103.1(15) . . ?
C016 C01Q C02O 108.6(6) . . ?
C01Z C01Q C016 109.4(5) . . ?
C01Z C01Q C02O 109.5(5) . . ?
C015 C01T C01L 107.2(18) . . ?
C01Q C01Z C020 109.7(4) . . ?
C02K C020 C01Z 109.3(5) . . ?
C23 C020 C01Z 109.4(5) . . ?
C23 C020 C02K 110.0(5) . . ?
C011 C021 C01D 108.7(7) . . ?
C011 C021 C02Q 110.1(6) . . ?
C01D C021 C02Q 109.9(6) . . ?
C01G C023 C014 109.4(17) . . ?
C02O C025 C02K 109.7(6) . . ?
C188 C025 C02K 110.0(6) . . ?
C188 C025 C02O 109.6(8) . . ?
C020 C02K C025 109.0(4) . . ?
C01D C02L C01B 108.6(6) . . ?
C01D C02L C70 109.9(6) . . ?
C70 C02L C01B 110.1(6) . . ?
C025 C02O C01Q 109.7(4) . . ?
C14 C02Q C021 109.0(4) . . ?
C110 C37 C61 120.0 . . ?
C37 C110 C0AA 120.0 . . ?
C76 C0AA C110 120.0 . . ?
C0AA C76 C135 120.0 . . ?
C61 C135 C76 120.0 . . ?
C37 C61 P00P 110.6(16) . . ?
C135 C61 P00P 129.3(16) . . ?
C135 C61 C37 120.0 . . ?
C87 C92 S00K 121.6(10) . . ?
C111 C92 S00K 102.6(9) . . ?
C111 C92 C87 109.6(4) . . ?
C01N C94 P00P 109(2) . . ?
C025 C188 C28 109.0(5) . . ?
C34 C115 C01X 120.0 . . ?
C184 C34 C115 120.0 . . ?
C34 C184 C93 120.0 . . ?
C112 C93 C184 120.0 . . ?
C93 C112 C01X 120.0 . . ?
C115 C01X P00N 122.5(14) . . ?
C112 C01X P00N 117.4(14) . . ?
C112 C01X C115 120.0 . . ?
C98 C101 C56 120.0 . . ?
C101 C98 C174 120.0 . . ?
C98 C174 C64 120.0 . . ?
C174 C64 C43 120.0 . . ?
C56 C43 C64 120.0 . . ?
C101 C56 P00P 122.2(18) . . ?
C43 C56 P00P 117.2(18) . . ?
C43 C56 C101 120.0 . . ?
C02L C70 C14 108.5(4) . . ?
C2AA C1AA C87 110.0(4) . . ?
C02Q C14 C70 109.2(5) . . ?
C36 C14 C02Q 110.1(5) . . ?
C36 C14 C70 110.0(6) . . ?
C010 C36 S00J 113.3(9) . . ?
C14 C36 S00J 116.6(9) . . ?
C14 C36 C010 109.9(4) . . ?
C016 C28 C188 109.5(6) . . ?
C23 C28 C016 109.6(5) . . ?
C23 C28 C188 109.6(6) . . ?
C020 C23 C28 109.3(4) . . ?
C79 C19 C7AA 108.7(4) . . ?
C01E C5AA C25 108.7(6) . . ?
C01E C5AA C44 109.7(5) . . ?
C44 C5AA C25 108.8(6) . . ?
C79 C25 C5AA 109.6(4) . . ?
C6AA C29 C44 110.1(6) . . ?
C78 C29 C6AA 110.8(6) . . ?
C78 C29 C44 107.7(7) . . ?
C01E C7AA C19 110.3(6) . . ?
C01E C7AA C6AA 109.4(5) . . ?
C6AA C7AA C19 109.4(6) . . ?
C29 C6AA C7AA 109.2(4) . . ?
C29 C44 C5AA 109.9(4) . . ?
C29 C78 C79 109.7(4) . . ?
C19 C79 C78 109.6(6) . . ?
C25 C79 C19 110.1(6) . . ?
C25 C79 C78 109.1(6) . . ?
C4AA C3AA C31 109.2(5) . . ?
C151 C3AA C4AA 109.7(5) . . ?
C151 C3AA C31 109.8(5) . . ?
C111 C4AA C3AA 109.1(4) . . ?
C3AA C31 C87 109.6(4) . . ?
C1AA C87 C92 108.6(6) . . ?
C1AA C87 C31 109.3(5) . . ?
C31 C87 C92 109.3(5) . . ?
C92 C111 C4AA 110.1(5) . . ?
C92 C111 C20 109.8(5) . . ?
C4AA C111 C20 109.5(5) . . ?
C2AA C20 C111 108.4(4) . . ?
C1AA C2AA C20 109.7(5) . . ?
C151 C2AA C1AA 109.9(5) . . ?
C151 C2AA C20 109.0(5) . . ?
C3AA C151 C2AA 109.6(4) . . ?
Ag05 Ag1 Ag0B 82.5(4) 3_565 . ?
Ag07 Ag1 Ag05 83.9(4) . 3_565 ?
Ag07 Ag1 Ag0B 166.0(6) . . ?
S00I Ag1 Ag05 101.5(5) . 3_565 ?
S00I Ag1 Ag07 48.6(3) . . ?
S00I Ag1 Ag0B 131.8(5) . . ?
S00J Ag1 Ag05 83.6(6) . 3_565 ?
S00J Ag1 Ag07 128.5(7) . . ?
S00J Ag1 Ag0B 52.9(4) . . ?
S00J Ag1 S00I 173.3(9) . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Ag02 S00G C00R C00U -114.4(13) . . . . ?
Ag02 S00G C00R C014 124.4(12) . . . . ?
Ag03 S00J C36 C010 -95.2(7) . . . . ?
Ag03 S00J C36 C14 135.7(6) . . . . ?
Ag04 S00F C00Y C00W -180.0(13) . . . . ?
Ag04 S00F C00Y C01K -57.6(16) . . . . ?
Ag04 S00G C00R C00U -28.8(15) . . . . ?
Ag04 S00G C00R C014 -150.1(12) . . . . ?
Ag06 S00K C92 C87 60.3(9) . . . . ?
Ag06 S00K C92 C111 -176.9(6) . . . . ?
Ag07 S00F C00Y C00W 18.5(19) 2_665 . . . ?
Ag07 S00F C00Y C01K 140.9(13) 2_665 . . . ?
Ag07 S00G C00R C00U 162.4(12) . . . . ?
Ag07 S00G C00R C014 41.1(14) . . . . ?
Ag07 S00I C016 C01Q 20.0(9) . . . . ?
Ag07 S00I C016 C28 144.0(6) . . . . ?
Ag08 S00F C00Y C00W 92.3(15) . . . . ?
Ag08 S00F C00Y C01K -145.3(14) . . . . ?
Ag08 S00L C01E C5AA 117.0(7) . . . . ?
Ag08 S00L C01E C7AA -116.0(7) . . . . ?
Ag09 S00K C92 C87 -26.3(11) . . . . ?
Ag09 S00K C92 C111 96.5(8) . . . . ?
Ag09 S00L C01E C5AA 26.3(9) . . . . ?
Ag09 S00L C01E C7AA 153.3(7) . . . . ?
Ag S00I C016 C01Q 94.7(7) . . . . ?
Ag S00I C016 C28 -141.3(6) . . . . ?
Ag S00J C36 C010 146.9(6) . . . . ?
Ag S00J C36 C14 17.8(8) . . . . ?
Ag0B S00J C36 C010 49.3(10) . . . . ?
Ag0B S00J C36 C14 -79.8(9) . . . . ?
Ag0B S00K C92 C87 -179.6(7) . . . . ?
Ag0B S00K C92 C111 -56.7(8) . . . . ?
Ag0B P00N C01F C00X 0.1(15) . . . . ?
Ag0B P00N C01F C02N -178.7(10) . . . . ?
Ag0D S00I C016 C01Q 179.7(6) . . . . ?
Ag0D S00I C016 C28 -56.3(8) . . . . ?
Ag0D S00L C01E C5AA -116.1(8) 2_665 . . . ?
Ag0D S00L C01E C7AA 10.9(10) 2_665 . . . ?
Ag0D P00P C61 C37 57.8(11) . . . . ?
Ag0D P00P C61 C135 -125.0(13) . . . . ?
Ag0D P00P C94 C01N 56(3) . . . . ?
S00F C00Y C01K C00V -69(2) . . . . ?
S00F C00Y C01K C01J 174.5(14) . . . . ?
S00G C00R C00U C00Z 176.0(13) . . . . ?
S00G C00R C00U C013 -66.7(19) . . . . ?
S00G C00R C014 C017 -173.3(13) . . . . ?
S00G C00R C014 C023 69.9(17) . . . . ?
S00I C016 C01Q C01Z 64.7(10) . . . . ?
S00I C016 C01Q C02O -175.7(9) . . . . ?
S00I C016 C28 C188 172.7(8) . . . . ?
S00I C016 C28 C23 -67.0(9) . . . . ?
S00K C92 C87 C1AA 59.2(10) . . . . ?
S00K C92 C87 C31 178.3(10) . . . . ?
S00K C92 C111 C4AA 169.9(9) . . . . ?
S00K C92 C111 C20 -69.4(10) . . . . ?
S00L C01E C5AA C25 69.7(11) . . . . ?
S00L C01E C5AA C44 -171.5(10) . . . . ?
S00L C01E C7AA C19 -68.7(10) . . . . ?
S00L C01E C7AA C6AA 170.8(9) . . . . ?
P00N C01F C02N C02P 178.8(18) . . . . ?
P00N C018 C01N C94 69(3) . . . . ?
C00R C00U C00Z C01P 64(2) . . . . ?
C00R C00U C013 C01G -55(2) . . . . ?
C00R C014 C017 C01P -63(2) . . . . ?
C00R C014 C023 C01G 57(2) . . . . ?
C00T C01G C023 C014 58(2) . . . . ?
C00U C00R C014 C017 63(2) . . . . ?
C00U C00R C014 C023 -54(2) . . . . ?
C00U C00Z C01P C00T 55(2) . . . . ?
C00U C00Z C01P C017 -60(2) . . . . ?
C00U C013 C01G C00T -62(2) . . . . ?
C00U C013 C01G C023 55(2) . . . . ?
C00V C015 C019 C00W -65(2) . . . . ?
C00V C015 C01T C01L 60(3) . . . . ?
C00W C00Y C01K C00V 54(3) . . . . ?
C00W C00Y C01K C01J -63(2) . . . . ?
C00X C01F C02N C02P 0.0 . . . . ?
C01F C00X C01A C01W 0.0 . . . . ?
C01F C02N C02P C01W 0.0 . . . . ?
C02N C02P C01W C01A 0.0 . . . . ?
C02P C01W C01A C00X 0.0 . . . . ?
C01A C00X C01F P00N -178.8(17) . . . . ?
C01A C00X C01F C02N 0.0 . . . . ?
C00Y C00W C019 C015 62(2) . . . . ?
C00Y C00W C01O C01L -52(3) . . . . ?
C00Z C00U C013 C01G 65(2) . . . . ?
C010 C011 C021 C01D -61.0(8) . . . . ?
C010 C011 C021 C02Q 59.4(8) . . . . ?
C010 C01B C02L C01D 59.9(7) . . . . ?
C010 C01B C02L C70 -60.5(7) . . . . ?
C011 C010 C01B C02L -59.3(7) . . . . ?
C011 C010 C36 S00J -74.3(9) . . . . ?
C011 C010 C36 C14 58.1(8) . . . . ?
C011 C021 C02Q C14 -59.7(7) . . . . ?
C013 C00U C00Z C01P -60(2) . . . . ?
C013 C01G C023 C014 -56(2) . . . . ?
C014 C00R C00U C00Z -63(2) . . . . ?
C014 C00R C00U C013 54(2) . . . . ?
C014 C017 C01P C00T -55(2) . . . . ?
C014 C017 C01P C00Z 61(2) . . . . ?
C015 C00V C01K C00Y -61(3) . . . . ?
C015 C00V C01K C01J 52(3) . . . . ?
C016 C01Q C01Z C020 59.6(7) . . . . ?
C016 C01Q C02O C025 -60.4(7) . . . . ?
C016 C28 C23 C020 -60.3(7) . . . . ?
C017 C014 C023 C01G -58(2) . . . . ?
C018 P00N C01F C00X 123.4(15) . . . . ?
C018 P00N C01F C02N -55.4(17) . . . . ?
C018 C01N C94 P00P 180(2) . . . . ?
C019 C00W C00Y S00F 66(2) . . . . ?
C019 C00W C00Y C01K -54(2) . . . . ?
C019 C00W C01O C01L 66(3) . . . . ?
C019 C015 C01T C01L -61(3) . . . . ?
C01B C010 C011 C021 60.1(8) . . . . ?
C01B C010 C36 S00J 166.9(8) . . . . ?
C01B C010 C36 C14 -60.7(7) . . . . ?
C01B C02L C70 C14 59.3(7) . . . . ?
C01D C021 C02Q C14 60.0(7) . . . . ?
C01D C02L C70 C14 -60.3(8) . . . . ?
C01E C5AA C25 C79 60.3(7) . . . . ?
C01E C5AA C44 C29 -58.0(8) . . . . ?
C01E C7AA C6AA C29 60.7(7) . . . . ?
C01G C00T C01P C00Z -54(2) . . . . ?
C01G C00T C01P C017 58(2) . . . . ?
C01J C01L C01O C00W 48(3) . . . . ?
C01J C01L C01T C015 -59(2) . . . . ?
C01K C00V C015 C019 67(2) . . . . ?
C01K C00V C015 C01T -60(3) . . . . ?
C01K C01J C01L C01O -54(3) . . . . ?
C01K C01J C01L C01T 60(2) . . . . ?
C01L C01J C01K C00V -60(3) . . . . ?
C01L C01J C01K C00Y 61(2) . . . . ?
C01O C00W C00Y S00F -177.2(15) . . . . ?
C01O C00W C00Y C01K 62(2) . . . . ?
C01O C00W C019 C015 -57(2) . . . . ?
C01O C01L C01T C015 57(2) . . . . ?
C01P C00T C01G C013 57(2) . . . . ?
C01P C00T C01G C023 -62(2) . . . . ?
C01Q C016 C28 C188 -60.3(7) . . . . ?
C01Q C016 C28 C23 60.0(7) . . . . ?
C01Q C01Z C020 C02K 60.4(7) . . . . ?
C01Q C01Z C020 C23 -60.0(7) . . . . ?
C01T C015 C019 C00W 62(2) . . . . ?
C01T C01L C01O C00W -63(2) . . . . ?
C01Z C01Q C02O C025 59.1(8) . . . . ?
C01Z C020 C02K C025 -60.5(7) . . . . ?
C01Z C020 C23 C28 60.1(7) . . . . ?
C021 C01D C02L C01B -61.1(8) . . . . ?
C021 C01D C02L C70 59.4(8) . . . . ?
C021 C02Q C14 C70 -61.2(7) . . . . ?
C021 C02Q C14 C36 59.7(7) . . . . ?
C023 C014 C017 C01P 55(2) . . . . ?
C025 C188 C28 C016 60.2(8) . . . . ?
C025 C188 C28 C23 -60.1(10) . . . . ?
C02K C020 C23 C28 -59.9(7) . . . . ?
C02K C025 C02O C01Q -59.8(8) . . . . ?
C02K C025 C188 C28 60.3(9) . . . . ?
C02L C01D C021 C011 61.6(8) . . . . ?
C02L C01D C021 C02Q -58.9(8) . . . . ?
C02L C70 C14 C02Q 61.3(7) . . . . ?
C02L C70 C14 C36 -59.6(7) . . . . ?
C02O C01Q C01Z C020 -59.4(7) . . . . ?
C02O C025 C02K C020 60.6(7) . . . . ?
C02O C025 C188 C28 -60.5(9) . . . . ?
C02Q C14 C36 S00J 71.4(9) . . . . ?
C02Q C14 C36 C010 -59.3(7) . . . . ?
C37 C110 C0AA C76 0.0 . . . . ?
C110 C37 C61 P00P 177.5(15) . . . . ?
C110 C37 C61 C135 0.0 . . . . ?
C110 C0AA C76 C135 0.0 . . . . ?
C0AA C76 C135 C61 0.0 . . . . ?
C76 C135 C61 P00P -177.0(18) . . . . ?
C76 C135 C61 C37 0.0 . . . . ?
C61 P00P C94 C01N -66(2) . . . . ?
C61 C37 C110 C0AA 0.0 . . . . ?
C92 C111 C20 C2AA -60.1(7) . . . . ?
C94 P00P C61 C37 179.2(13) . . . . ?
C94 P00P C61 C135 -3.6(19) . . . . ?
C188 C025 C02K C020 -60.1(8) . . . . ?
C188 C025 C02O C01Q 61.1(8) . . . . ?
C188 C28 C23 C020 59.8(8) . . . . ?
C115 C34 C184 C93 0.0 . . . . ?
C34 C115 C01X P00N -177.9(14) . . . . ?
C34 C115 C01X C112 0.0 . . . . ?
C34 C184 C93 C112 0.0 . . . . ?
C184 C93 C112 C01X 0.0 . . . . ?
C93 C112 C01X P00N 178.0(13) . . . . ?
C93 C112 C01X C115 0.0 . . . . ?
C01X P00N C01F C00X -119.5(14) . . . . ?
C01X P00N C01F C02N 61.7(15) . . . . ?
C01X C115 C34 C184 0.0 . . . . ?
C101 C98 C174 C64 0.0 . . . . ?
C98 C101 C56 P00P -170.5(18) . . . . ?
C98 C101 C56 C43 0.0 . . . . ?
C98 C174 C64 C43 0.0 . . . . ?
C174 C64 C43 C56 0.0 . . . . ?
C64 C43 C56 P00P 170.9(17) . . . . ?
C64 C43 C56 C101 0.0 . . . . ?
C56 P00P C61 C37 -68.0(14) . . . . ?
C56 P00P C61 C135 109.2(17) . . . . ?
C56 P00P C94 C01N 171(2) . . . . ?
C56 C101 C98 C174 0.0 . . . . ?
C70 C14 C36 S00J -168.2(8) . . . . ?
C70 C14 C36 C010 61.1(7) . . . . ?
C1AA C2AA C151 C3AA -59.3(7) . . . . ?
C36 C010 C011 C021 -58.4(8) . . . . ?
C36 C010 C01B C02L 60.1(7) . . . . ?
C28 C016 C01Q C01Z -59.6(8) . . . . ?
C28 C016 C01Q C02O 60.0(7) . . . . ?
C23 C020 C02K C025 59.6(7) . . . . ?
C19 C7AA C6AA C29 -60.3(7) . . . . ?
C5AA C01E C7AA C19 60.0(7) . . . . ?
C5AA C01E C7AA C6AA -60.4(7) . . . . ?
C5AA C25 C79 C19 -60.8(7) . . . . ?
C5AA C25 C79 C78 59.4(7) . . . . ?
C25 C5AA C44 C29 60.7(8) . . . . ?
C29 C78 C79 C19 59.0(8) . . . . ?
C29 C78 C79 C25 -61.5(8) . . . . ?
C7AA C01E C5AA C25 -59.8(7) . . . . ?
C7AA C01E C5AA C44 58.9(8) . . . . ?
C7AA C19 C79 C25 59.4(7) . . . . ?
C7AA C19 C79 C78 -60.5(8) . . . . ?
C6AA C29 C44 C5AA 58.9(8) . . . . ?
C6AA C29 C78 C79 -58.4(8) . . . . ?
C44 C5AA C25 C79 -59.1(7) . . . . ?
C44 C29 C6AA C7AA -60.1(7) . . . . ?
C44 C29 C78 C79 62.1(8) . . . . ?
C78 C29 C6AA C7AA 59.0(7) . . . . ?
C78 C29 C44 C5AA -62.0(8) . . . . ?
C79 C19 C7AA C01E -59.1(8) . . . . ?
C79 C19 C7AA C6AA 61.3(8) . . . . ?
C3AA C4AA C111 C92 60.4(7) . . . . ?
C3AA C4AA C111 C20 -60.5(7) . . . . ?
C3AA C31 C87 C92 -59.5(7) . . . . ?
C3AA C31 C87 C1AA 59.2(7) . . . . ?
C4AA C3AA C31 C87 60.5(7) . . . . ?
C4AA C3AA C151 C2AA -60.4(7) . . . . ?
C4AA C111 C20 C2AA 61.0(7) . . . . ?
C31 C3AA C4AA C111 -60.5(7) . . . . ?
C31 C3AA C151 C2AA 59.6(7) . . . . ?
C87 C92 C111 C4AA -59.6(7) . . . . ?
C87 C92 C111 C20 61.1(7) . . . . ?
C87 C1AA C2AA C20 -60.5(7) . . . . ?
C87 C1AA C2AA C151 59.4(7) . . . . ?
C111 C92 C87 C1AA -60.3(7) . . . . ?
C111 C92 C87 C31 58.9(8) . . . . ?
C111 C20 C2AA C1AA 59.6(7) . . . . ?
C111 C20 C2AA C151 -60.9(7) . . . . ?
C20 C2AA C151 C3AA 60.9(7) . . . . ?
C2AA C1AA C87 C92 60.0(7) . . . . ?
C2AA C1AA C87 C31 -59.1(7) . . . . ?
C151 C3AA C4AA C111 59.9(7) . . . . ?
C151 C3AA C31 C87 -59.8(7) . . . . ?
Ag1 S00I C016 C01Q 90.7(8) . . . . ?
Ag1 S00I C016 C28 -145.4(7) . . . . ?
Ag1 S00J C36 C010 146.9(8) . . . . ?
Ag1 S00J C36 C14 17.8(9) . . . . ?

_olex2_submission_special_instructions 'No special instructions were received'
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_1_sq_CCDC2
_database_code_depnum_ccdc_archive 'CCDC 2094276'
loop_
_audit_author_name
_audit_author_address
'Xi Xi Kang'
;Anhui University
China
;
_audit_update_record             
;
2021-07-04 deposited with the CCDC.	2022-04-12 downloaded from the CCDC.
;
_audit_creation_date             2021-01-06
_audit_creation_method           
;
Olex2 1.2
(compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506)
;
_shelx_SHELXL_version_number     2016/4
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         'C280 H420 Ag52 Cl4 S28'
_chemical_formula_sum            'C280 H420 Ag52 Cl4 S28'
_chemical_formula_weight         10434.85
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag 0.1306 4.2820 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.3639 0.7018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.3331 0.5567 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      orthorhombic
_space_group_IT_number           56
_space_group_name_H-M_alt        'P c c n'
_space_group_name_Hall           '-P 2ab 2ac'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, -y+1/2, z'
'x+1/2, -y, -z+1/2'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, y-1/2, -z'
'-x-1/2, y, z-1/2'
'x, -y-1/2, z-1/2'

_cell_length_a                   22.5930(2)
_cell_length_b                   38.2448(3)
_cell_length_c                   47.1063(2)
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_volume                     40702.9(5)
_cell_formula_units_Z            4
_cell_measurement_reflns_used    12911
_cell_measurement_temperature    120(2)
_cell_measurement_theta_max      68.788
_cell_measurement_theta_min      3.982
_shelx_estimated_absorpt_T_max   ?
_shelx_estimated_absorpt_T_min   ?
_exptl_absorpt_coefficient_mu    21.384
_exptl_absorpt_correction_T_max  ?
_exptl_absorpt_correction_T_min  ?
_exptl_absorpt_correction_type   ?
_exptl_absorpt_process_details   ?
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            pink
_exptl_crystal_density_diffrn    1.703
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       block
_exptl_crystal_F_000             20240
_exptl_crystal_size_max          ?
_exptl_crystal_size_mid          ?
_exptl_crystal_size_min          ?
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.1507
_diffrn_reflns_av_unetI/netI     0.2173
_diffrn_reflns_Laue_measured_fraction_full 0.957
_diffrn_reflns_Laue_measured_fraction_max 0.943
_diffrn_reflns_limit_h_max       27
_diffrn_reflns_limit_h_min       -22
_diffrn_reflns_limit_k_max       46
_diffrn_reflns_limit_k_min       -17
_diffrn_reflns_limit_l_max       52
_diffrn_reflns_limit_l_min       -56
_diffrn_reflns_number            123849
_diffrn_reflns_point_group_measured_fraction_full 0.957
_diffrn_reflns_point_group_measured_fraction_max 0.943
_diffrn_reflns_theta_full        67.686
_diffrn_reflns_theta_max         68.788
_diffrn_reflns_theta_min         3.982
_diffrn_ambient_temperature      120(2)
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 0.957
_diffrn_measured_fraction_theta_max 0.943
_diffrn_measurement_device_type  STOE
_diffrn_measurement_method       ?
_diffrn_radiation_type           CuK\a
_diffrn_radiation_wavelength     1.54186
_diffrn_source                   ?
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                12911
_reflns_number_total             35549
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 Structure factors included contributions from the .fab file.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       ?
_computing_data_collection       ?
_computing_data_reduction        ?
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'ShelXL (Sheldrick, 2015)'
_computing_structure_solution    'SHELXT 2014/5 (Sheldrick, 2014)'
_refine_diff_density_max         1.777
_refine_diff_density_min         -2.259
_refine_diff_density_rms         0.190
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.801
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1543
_refine_ls_number_reflns         35549
_refine_ls_number_restraints     4039
_refine_ls_R_factor_all          0.1631
_refine_ls_R_factor_gt           0.0690
_refine_ls_restrained_S_all      0.771
_refine_ls_shift/su_max          0.004
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0831P)²] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1591
_refine_ls_wR_factor_ref         0.1977
_refine_special_details          ?
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H) groups, All C(H,H) groups
2. Restrained distances
 C61-C53 = C7BA-C53 = C7BA-C136 = C6BA-C61 = C61-C174 = C68-C174 = C8BA-C68 =
 C9BA-C68 = C8BA-C5BA = C5BA-C136 = C6BA-C5BA = C9BA-C7BA
 1.56 with sigma of 0.01
 C7BA-C61
 2.56 with sigma of 0.01
 C9BA-C61
 2.93 with sigma of 0.01
 C67-C0CA = C1CA-C0CA = C3CA-C1CA = C99-C3CA = C3CA-C166 = C2CA-C166 = C2CA-
 C110 = C110-C0CA = C82-C80 = C99-C82 = C82-C67 = C80-C2CA
 1.56 with sigma of 0.01
 S25-C95
 1.8 with sigma of 0.01
 C95-C151 = C151-C112 = C112-C107 = C107-C106 = C83-C106 = C83-C122 = C151-
 C118 = C118-C104 = C122-C104 = C104-C100 = C107-C100 = C95-C83
 1.56 with sigma of 0.01
 C95-C106
 2.56 with sigma of 0.01
 C95-C118
 2.56 with sigma of 0.01
 C95-C112
 2.56 with sigma of 0.01
 C95-C122
 2.56 with sigma of 0.01
 C151-C104
 2.56 with sigma of 0.01
 C151-C83
 2.56 with sigma of 0.01
 C151-C107
 2.56 with sigma of 0.01
 C112-C106
 2.56 with sigma of 0.01
 C112-C100
 2.56 with sigma of 0.01
 C112-C118
 2.56 with sigma of 0.01
 C107-C104
 2.56 with sigma of 0.01
 C107-C83
 2.56 with sigma of 0.01
 C100-C122
 2.56 with sigma of 0.01
 C100-C118
 2.56 with sigma of 0.01
 C104-C83
 2.56 with sigma of 0.01
 C104-C151
 2.56 with sigma of 0.01
 C122-C106
 2.56 with sigma of 0.01
 C83-C100
 2.93 with sigma of 0.01
 C95-C107
 2.93 with sigma of 0.01
 C151-C106
 2.93 with sigma of 0.01
 C151-C100
 2.93 with sigma of 0.01
 C151-C122
 2.93 with sigma of 0.01
 C112-C104
 2.93 with sigma of 0.01
 C106-C104
 2.93 with sigma of 0.01
 C100-C83
 2.93 with sigma of 0.01
 C107-C122
 2.93 with sigma of 0.01
 C82-C67 = C67-C0CA = C80-C2CA = C82-C80 = C2CA-C110 = C99-C82 = C99-C3CA =
 C2CA-C166 = C3CA-C166 = C3CA-C1CA = C1CA-C0CA
 1.56 with sigma of 0.01
 C67-C2CA
 2.93 with sigma of 0.01
 C80-C0CA
 2.93 with sigma of 0.01
 C82-C110
 2.93 with sigma of 0.01
 C166-C0CA
 2.93 with sigma of 0.01
 C2CA-C1CA
 2.93 with sigma of 0.01
 C3CA-C110
 2.93 with sigma of 0.01
 C67-C0CA = C82-C67 = C99-C82 = C82-C80 = C80-C2CA = C2CA-C110 = C110-C0CA =
 C1CA-C0CA = C3CA-C1CA = C99-C3CA = C3CA-C166 = C2CA-C166
 1.56 with sigma of 0.01
 C67-C110
 2.56 with sigma of 0.01
 C67-C80
 2.56 with sigma of 0.01
 C67-C1CA
 2.56 with sigma of 0.01
 C0CA-C2CA
 2.56 with sigma of 0.01
 C0CA-C3CA
 2.56 with sigma of 0.01
 C0CA-C82
 2.56 with sigma of 0.01
 C1CA-C166
 2.56 with sigma of 0.01
 C1CA-C110
 2.56 with sigma of 0.01
 C166-C80
 2.56 with sigma of 0.01
 C71-C16 = C71-C4CA = C4CA-C129 = C130-C129 = C7DA-C130 = C84-C7DA = C7DA-C102
 = C71-C102 = C51-C16 = C84-C51 = C70-C51 = C70-C129
 1.56 with sigma of 0.01
 C16-C4CA
 2.56 with sigma of 0.01
 C16-C102
 2.56 with sigma of 0.01
 C16-C70
 2.56 with sigma of 0.01
 C51-C129
 2.56 with sigma of 0.01
 C51-C71
 2.56 with sigma of 0.01
 C70-C4CA
 2.56 with sigma of 0.01
 C70-C84
 2.56 with sigma of 0.01
 C70-C130
 2.56 with sigma of 0.01
 C129-C71
 2.56 with sigma of 0.01
 C129-C7DA
 2.56 with sigma of 0.01
 C130-C102
 2.56 with sigma of 0.01
 C7DA-C71
 2.56 with sigma of 0.01
 C16-C129
 2.93 with sigma of 0.01
 C16-C7DA
 2.93 with sigma of 0.01
 C51-C4CA
 2.93 with sigma of 0.01
 C51-C130
 2.93 with sigma of 0.01
 C51-C102
 2.93 with sigma of 0.01
 C70-C71
 2.93 with sigma of 0.01
 C70-C7DA
 2.93 with sigma of 0.01
 C129-C102
 2.93 with sigma of 0.01
 C4CA-C7DA
 2.93 with sigma of 0.01
 C71-C130
 2.93 with sigma of 0.01
 C84-C129
 2.93 with sigma of 0.01
 C84-C71
 2.93 with sigma of 0.01
 C7CA-C4DA = C7CA-C0DA = C8CA-C0DA = C160-C0DA = C8CA-C5DA = C5DA-C1DA = C5DA-
 C156 = C2DA-C160 = C2DA-C156 = C3DA-C2DA = C4DA-C1DA = C4DA-C3DA
 1.56 with sigma of 0.01
 C7CA-C160
 2.56 with sigma of 0.01
 C7CA-C3DA
 2.56 with sigma of 0.01
 C7CA-C8CA
 2.56 with sigma of 0.01
 C4DA-C0DA
 2.56 with sigma of 0.01
 C4DA-C2DA
 2.56 with sigma of 0.01
 C4DA-C5DA
 2.56 with sigma of 0.01
 C3DA-C160
 2.56 with sigma of 0.01
 C3DA-C1DA
 2.56 with sigma of 0.01
 C3DA-C156
 2.56 with sigma of 0.01
 C0DA-C5DA
 2.56 with sigma of 0.01
 C0DA-C2DA
 2.56 with sigma of 0.01
 C160-C8CA
 2.56 with sigma of 0.01
 C160-C156
 2.56 with sigma of 0.01
 C2DA-C5DA
 2.56 with sigma of 0.01
 C156-C8CA
 2.56 with sigma of 0.01
 C5DA-C0DA
 2.56 with sigma of 0.01
 C4DA-C160
 2.93 with sigma of 0.01
 C4DA-C8CA
 2.93 with sigma of 0.01
 C4DA-C156
 2.93 with sigma of 0.01
 C3DA-C0DA
 2.93 with sigma of 0.01
 C5DA-C3DA
 2.93 with sigma of 0.01
 C7CA-C2DA
 2.93 with sigma of 0.01
 C7CA-C5DA
 2.93 with sigma of 0.01
 C2DA-C8CA
 2.93 with sigma of 0.01
 C0DA-C156
 2.93 with sigma of 0.01
 C160-C5DA
 2.93 with sigma of 0.01
 C1DA-C2DA
 2.93 with sigma of 0.01
 C1DA-C0DA
 2.93 with sigma of 0.01
 C63-C55
 1.56 with sigma of 0.01
 S2A-C7CA
 1.76 with sigma of 0.01
3. Uiso/Uaniso restraints and constraints
C7 \\sim C9 \\sim C10 \\sim C12 \\sim C15 \\sim C17 \\sim C24 \\sim C32 \\sim
C34 \\sim C35 \\sim C37 \\sim C39 \\sim C47 \\sim C50 \\sim C54 \\sim C55 \\sim
C62 \\sim C63 \\sim C65 \\sim C66 \\sim C69 \\sim C74 \\sim C78 \\sim C83 \\sim
C85 \\sim C86 \\sim C87 \\sim C90 \\sim C93 \\sim C94 \\sim C95 \\sim C100
\\sim C103 \\sim C104 \\sim C106 \\sim C107 \\sim C112 \\sim C118 \\sim C122
\\sim C151 \\sim C1 \\sim C2 \\sim C3 \\sim C4 \\sim C5 \\sim C6 \\sim C5AA
\\sim C8 \\sim C2BA \\sim C6AA \\sim C11 \\sim C9AA \\sim C13 \\sim C14 \\sim
C2AA \\sim C16 \\sim C0BA \\sim C18 \\sim C19 \\sim C20 \\sim C21 \\sim C22
\\sim C23 \\sim C4AA \\sim C25 \\sim C26 \\sim C27 \\sim C28 \\sim C29 \\sim
C30 \\sim C31 \\sim C1BA \\sim C33 \\sim C0AA \\sim C3BA \\sim C36 \\sim C7AA
\\sim C38 \\sim C8AA \\sim C40 \\sim C41 \\sim C42 \\sim C43 \\sim C44 \\sim
C45 \\sim C46 \\sim C3AA \\sim C48 \\sim C49 \\sim C4BA \\sim C51 \\sim C52
\\sim C53 \\sim C5BA \\sim C1AA \\sim C56 \\sim C57 \\sim C58 \\sim C59 \\sim
C60 \\sim C61 \\sim C0CA \\sim C6BA \\sim C64 \\sim C1CA \\sim C67 \\sim C68
\\sim C70 \\sim C71 \\sim C4CA \\sim C76 \\sim C77 \\sim C2CA \\sim C80 \\sim
C82 \\sim C7BA \\sim C84 \\sim C8BA \\sim C88 \\sim C3CA \\sim C99 \\sim C9BA
\\sim C102 \\sim C110 \\sim C129 \\sim C130 \\sim C136 \\sim C166 \\sim C174
\\sim C2DA \\sim C4DA \\sim C8CA \\sim C1DA \\sim C0DA \\sim C3DA \\sim C7CA
\\sim C5DA \\sim C156 \\sim C160: within 3.8A with sigma of 0.01 and sigma for
terminal atoms of 0.02
C16 \\sim C71 \\sim C102 \\sim C4CA \\sim C129 \\sim C130 \\sim C84 \\sim C51
\\sim C7DA: within 1.7A with sigma of 0.04 and sigma for terminal atoms of 0.08
S4# \\sim C1 \\sim C22 \\sim C11 \\sim C42 \\sim C14 \\sim C2AA \\sim C3AA
\\sim C60 \\sim C36 \\sim C27: within 1.7A with sigma of 0.04 and sigma for
terminal atoms of 0.08
S4# \\sim C1 \\sim C14 \\sim C27 \\sim C3AA \\sim C36 \\sim C60 \\sim C2AA
\\sim C42 \\sim C11 \\sim C22: within 1.7A with sigma of 0.04 and sigma for
terminal atoms of 0.08
Uanis(S4#) \\sim Ueq, Uanis(C1) \\sim Ueq, Uanis(C11) \\sim Ueq, Uanis(C22)
\\sim Ueq, Uanis(C42) \\sim Ueq, Uanis(C2AA) \\sim Ueq, Uanis(C27) \\sim Ueq,
Uanis(C14) \\sim Ueq, Uanis(C3AA) \\sim Ueq, Uanis(C60) \\sim Ueq, Uanis(C36)
\\sim Ueq: with sigma of 0.1 and sigma for terminal atoms of 0.2
Uanis(C102) = Uanis(C130) = Uanis(C129) = Uanis(C4CA) = Uanis(C71) = Uanis(C84)
= Uanis(C51)
Uanis(C25) = Uanis(C6AA) = Uanis(C31) = Uanis(C49) = Uanis(C7AA) = Uanis(C8AA)
= Uanis(C58) = Uanis(C88) = Uanis(C56) = Uanis(C76) = Uanis(S6)
4.a Ternary CH refined with riding coordinates:
 C7(H7), C9(H9), C10(H10), C12(H12), C15(H15), C17(H17), C34(H34), C35(H35),
 C55(H55), C62(H62), C65(H65), C66(H66), C74(H74), C83(H83), C86(H86), C93(H93),
  C95(H95), C104(H104), C107(H107), C151(H151), C1(H1), C2(H2), C4(H4), C5(H5),
 C8(H8), C2BA(H2BA), C6AA(H6AA), C11(H11), C9AA(H9AA), C13(H13), C14(H14),
 C16(H16), C0BA(H0BA), C23(H23), C4AA(H4AA), C25(H25), C26(H26), C28(H28),
 C29(H29), C0AA(H0AA), C36(H36), C8AA(H8AA), C41(H41), C42(H42), C43(H43),
 C46(H46), C4BA(H4BA), C51(H51), C52(H52), C5BA(H5BA), C57(H57), C58(H58),
 C61(H61), C0CA(H0CA), C67(H67), C68(H68), C71(H71), C2CA(H2CA), C82(H82),
 C7BA(H7BA), C8BA(H8BA), C88(H88), C3CA(H3CA), C129(H129), C2DA(H2DA),
 C4DA(H4DA), C0DA(H0DA), C7CA(H7CA), C5DA(H5DA), C7DA(H7DA)
4.b Secondary CH2 refined with riding coordinates:
 C24(H24A,H24B), C32(H32A,H32B), C37(H37A,H37B), C39(H39A,H39B), C47(H47A,
 H47B), C50(H50A,H50B), C54(H54A,H54B), C63(H63A,H63B), C69(H69A,H69B),
 C78(H78A,H78B), C85(H85A,H85B), C87(H87A,H87B), C90(H90A,H90B), C94(H94A,H94B),
  C100(H10A,H10B), C103(H10C,H10D), C106(H10E,H10F), C112(H11A,H11B), C118(H11C,
 H11D), C122(H12A,H12B), C3(H3A,H3B), C6(H6A,H6B), C5AA(H5AA,H5AB), C2AA(H2AA,
 H2AB), C18(H18A,H18B), C19(H19A,H19B), C20(H20A,H20B), C21(H21A,H21B),
 C22(H22A,H22B), C27(H27A,H27B), C30(H30A,H30B), C31(H31A,H31B), C1BA(H1BA,
 H1BB), C33(H33A,H33B), C3BA(H3BA,H3BB), C7AA(H7AA,H7AB), C38(H38A,H38B),
 C40(H40A,H40B), C44(H44A,H44B), C45(H45A,H45B), C3AA(H3AA,H3AB), C48(H48A,
 H48B), C49(H49A,H49B), C53(H53A,H53B), C1AA(H1AA,H1AB), C56(H56A,H56B),
 C59(H59A,H59B), C60(H60A,H60B), C6BA(H6BA,H6BB), C64(H64A,H64B), C1CA(H1CA,
 H1CB), C70(H70A,H70B), C4CA(H4CA,H4CB), C76(H76A,H76B), C77(H77A,H77B),
 C80(H80A,H80B), C84(H84A,H84B), C99(H99A,H99B), C9BA(H9BA,H9BB), C102(H10G,
 H10H), C110(H11E,H11F), C130(H13A,H13B), C136(H13C,H13D), C166(H16A,H16B),
 C174(H17A,H17B), C8CA(H8CA,H8CB), C1DA(H1DA,H1DB), C3DA(H3DA,H3DB), C156(H15A,
 H15B), C160(H16C,H16D)
;
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1 Ag 0.24885(5) 0.71306(3) 0.30810(2) 0.0372(3) Uani 1 1 d . . . . .
Ag01 Ag 0.27839(6) 0.68788(3) 0.25287(3) 0.0452(3) Uani 1 1 d . . . . .
Ag1A Ag 0.23271(7) 0.71538(5) 0.39612(4) 0.0767(5) Uani 1 1 d . . . . .
Ag1B Ag 0.07932(7) 0.63115(5) 0.35804(4) 0.0920(7) Uani 1 1 d . . . . .
Ag1D Ag 0.27707(8) 0.71558(5) 0.45224(5) 0.1004(7) Uani 1 1 d . . . . .
Ag1E Ag 0.04941(10) 0.65358(4) 0.29855(4) 0.1005(7) Uani 1 1 d . . . . .
Ag2 Ag 0.18806(5) 0.75038(3) 0.35011(3) 0.0385(3) Uani 1 1 d . . . . .
Ag02 Ag 0.07347(5) 0.77642(3) 0.35357(3) 0.0444(3) Uani 1 1 d . . . . .
Ag5 Ag 0.29144(6) 0.64300(3) 0.30288(3) 0.0434(3) Uani 1 1 d . . . . .
Ag05 Ag 0.19408(6) 0.59716(3) 0.31935(3) 0.0517(4) Uani 1 1 d . . . . .
Ag7 Ag 0.09920(6) 0.70697(3) 0.37402(3) 0.0447(3) Uani 1 1 d . . . . .
Ag8 Ag 0.32535(6) 0.83688(3) 0.28244(3) 0.0429(3) Uani 1 1 d . . . . .
Ag10 Ag 0.30995(7) 0.75907(3) 0.26230(3) 0.0631(4) Uani 1 1 d . . . . .
Ag11 Ag 0.13224(7) 0.69287(4) 0.43223(3) 0.0652(4) Uani 1 1 d . . . . .
Ag12 Ag 0.32661(7) 0.67769(3) 0.35310(4) 0.0687(5) Uani 1 1 d . . . . .
Ag13 Ag 0.36830(6) 0.70326(4) 0.30179(4) 0.0678(5) Uani 1 1 d . . . . .
Ag15 Ag 0.31285(7) 0.73445(4) 0.20433(4) 0.0654(4) Uani 1 1 d . . . . .
Ag16 Ag 0.03124(8) 0.83489(4) 0.31904(3) 0.0688(5) Uani 1 1 d . . . . .
Ag17 Ag 0.14379(6) 0.76838(3) 0.40370(3) 0.0506(4) Uani 1 1 d . . . . .
Ag18 Ag 0.34428(7) 0.81540(3) 0.22451(3) 0.0520(4) Uani 1 1 d . . . . .
Ag19 Ag 0.39058(6) 0.65120(4) 0.25735(3) 0.0541(4) Uani 1 1 d . . . . .
Ag20 Ag 0.18703(7) 0.66838(3) 0.34318(3) 0.0527(4) Uani 1 1 d . . . . .
Ag21 Ag -0.01081(6) 0.72430(3) 0.33431(3) 0.0536(4) Uani 1 1 d . . . . .
Ag25 Ag 0.38671(6) 0.78571(4) 0.31440(3) 0.0567(4) Uani 1 1 d . . . . .
Ag29 Ag 0.40975(6) 0.66268(4) 0.39881(3) 0.0568(4) Uani 1 1 d . . . . .
Ag32 Ag 0.38234(7) 0.61121(4) 0.34107(3) 0.0614(4) Uani 1 1 d . . . . .
S1A S 0.4210(3) 0.74832(19) 0.27196(15) 0.102(2) Uani 1 1 d . . . . .
S1 S 0.2979(2) 0.57975(10) 0.32239(10) 0.0465(11) Uani 1 1 d . . . . .
S2A S 0.2482(4) 0.65047(17) 0.38575(17) 0.121(3) Uani 1 1 d D . . . .
S2 S 0.0444(2) 0.88216(11) 0.28589(10) 0.0469(11) Uani 1 1 d . . . . .
S3 S -0.0323(2) 0.78618(12) 0.33537(10) 0.0491(11) Uani 1 1 d . . . . .
S4 S 0.4655(2) 0.62089(12) 0.37278(10) 0.0491(11) Uani 1 1 d . U . . .
Cl4 Cl 0.0293(3) 0.7494(2) 0.40791(18) 0.129(3) Uani 1 1 d . . . . .
S6 S 0.0842(2) 0.64879(13) 0.25015(11) 0.0614(7) Uani 1 1 d . . . . .
S7 S 0.3078(2) 0.79072(11) 0.18180(10) 0.0485(11) Uani 1 1 d . . . . .
Cl8 Cl 0.2472(2) 0.61854(10) 0.25170(10) 0.0579(12) Uani 1 1 d . . . . .
S10 S 0.3575(2) 0.67789(11) 0.21336(10) 0.0500(12) Uani 1 1 d . . . . .
S16 S 0.0919(2) 0.58412(13) 0.32348(12) 0.0603(14) Uani 1 1 d . . . . .
S18 S 0.3710(2) 0.68631(13) 0.44335(11) 0.0560(13) Uani 1 1 d . . . . .
S19 S 0.1788(2) 0.71576(12) 0.47305(11) 0.0571(13) Uani 1 1 d . . . . .
S20 S 0.0672(2) 0.65457(13) 0.40553(11) 0.0603(14) Uani 1 1 d . . . . .
S25 S -0.0299(2) 0.66361(13) 0.33180(13) 0.0723(17) Uani 1 1 d D . . . .
C7 C -0.1060(8) 0.8300(5) 0.3649(4) 0.061(2) Uani 1 1 d . U . . .
H7 H -0.081709 0.848771 0.356958 0.074 Uiso 1 1 calc R . . . .
C9 C -0.1977(8) 0.7942(5) 0.3574(4) 0.064(2) Uani 1 1 d . U . . .
H9 H -0.230914 0.790486 0.344344 0.077 Uiso 1 1 calc R . . . .
C10 C -0.1700(8) 0.8098(5) 0.4074(5) 0.063(2) Uani 1 1 d . U . . .
H10 H -0.183531 0.815717 0.426527 0.076 Uiso 1 1 calc R . . . .
C12 C -0.0284(9) 0.9212(5) 0.2504(5) 0.072(3) Uani 1 1 d . U . . .
H12 H 0.007936 0.926674 0.239968 0.086 Uiso 1 1 calc R . . . .
C15 C -0.0812(9) 0.8750(5) 0.2800(5) 0.070(3) Uani 1 1 d . U . . .
H15 H -0.078459 0.852092 0.289209 0.084 Uiso 1 1 calc R . . . .
C17 C -0.0688(8) 0.7979(5) 0.3681(4) 0.062(2) Uani 1 1 d . U . . .
H17 H -0.038324 0.802638 0.382368 0.075 Uiso 1 1 calc R . . . .
C24 C -0.0910(9) 0.9047(5) 0.3031(5) 0.073(3) Uani 1 1 d . U . . .
H24A H -0.126163 0.899731 0.314159 0.088 Uiso 1 1 calc R . . . .
H24B H -0.057338 0.905748 0.315814 0.088 Uiso 1 1 calc R . . . .
C32 C -0.1306(8) 0.7775(5) 0.4080(4) 0.063(2) Uani 1 1 d . U . . .
H32A H -0.097310 0.781756 0.420519 0.076 Uiso 1 1 calc R . . . .
H32B H -0.152885 0.757947 0.415558 0.076 Uiso 1 1 calc R . . . .
C34 C -0.1079(8) 0.7682(5) 0.3790(4) 0.061(2) Uani 1 1 d . U . . .
H34 H -0.084616 0.746630 0.380199 0.073 Uiso 1 1 calc R . . . .
C35 C -0.0251(8) 0.8825(5) 0.2631(5) 0.072(3) Uani 1 1 d . U . . .
H35 H -0.021203 0.865542 0.247617 0.086 Uiso 1 1 calc R . . . .
C37 C -0.1573(8) 0.8237(5) 0.3460(4) 0.063(2) Uani 1 1 d . U . . .
H37A H -0.143115 0.817447 0.327202 0.076 Uiso 1 1 calc R . . . .
H37B H -0.180129 0.845101 0.344238 0.076 Uiso 1 1 calc R . . . .
C39 C -0.2217(8) 0.8057(5) 0.3877(4) 0.065(2) Uani 1 1 d . U . . .
H39A H -0.242896 0.827712 0.386123 0.078 Uiso 1 1 calc R . . . .
H39B H -0.248662 0.788203 0.394983 0.078 Uiso 1 1 calc R . . . .
C47 C -0.1278(8) 0.8410(5) 0.3946(4) 0.064(2) Uani 1 1 d . U . . .
H47A H -0.150081 0.862616 0.393283 0.077 Uiso 1 1 calc R . . . .
H47B H -0.094284 0.844824 0.407075 0.077 Uiso 1 1 calc R . . . .
C50 C -0.1599(8) 0.7629(5) 0.3581(4) 0.064(2) Uani 1 1 d . U . . .
H50A H -0.144415 0.758314 0.339222 0.077 Uiso 1 1 calc R . . . .
H50B H -0.183179 0.742837 0.363884 0.077 Uiso 1 1 calc R . . . .
C54 C -0.1324(9) 0.8759(5) 0.2599(5) 0.072(3) Uani 1 1 d . U . . .
H54A H -0.127678 0.857236 0.246089 0.087 Uiso 1 1 calc R . . . .
H54B H -0.168544 0.871474 0.270345 0.087 Uiso 1 1 calc R . . . .
C55 C -0.1382(9) 0.9095(5) 0.2446(4) 0.074(3) Uani 1 1 d D U . . .
H55 H -0.171553 0.909176 0.231266 0.089 Uiso 1 1 calc R . . . .
C62 C -0.0481(11) 0.6149(7) 0.4587(6) 0.099(3) Uani 1 1 d . U . . .
H62 H -0.040619 0.595641 0.471925 0.119 Uiso 1 1 calc R . . . .
C63 C -0.1472(9) 0.9368(5) 0.2684(4) 0.076(3) Uani 1 1 d D U . . .
H63A H -0.152185 0.959708 0.259873 0.091 Uiso 1 1 calc R . . . .
H63B H -0.183150 0.931290 0.278714 0.091 Uiso 1 1 calc R . . . .
C65 C -0.0505(11) 0.6338(7) 0.4065(6) 0.099(3) Uani 1 1 d . U . . .
H65 H -0.046759 0.625748 0.386820 0.119 Uiso 1 1 calc R . . . .
C66 C -0.0977(9) 0.9379(5) 0.2882(5) 0.075(3) Uani 1 1 d . U . . .
H66 H -0.106449 0.955874 0.302361 0.090 Uiso 1 1 calc R . . . .
C69 C -0.0403(9) 0.9487(5) 0.2727(5) 0.074(3) Uani 1 1 d . U . . .
H69A H -0.045207 0.971405 0.263814 0.089 Uiso 1 1 calc R . . . .
H69B H -0.007658 0.949976 0.285974 0.089 Uiso 1 1 calc R . . . .
C74 C -0.0081(11) 0.6649(6) 0.4135(5) 0.098(3) Uani 1 1 d . U . . .
H74 H -0.019486 0.684466 0.401204 0.117 Uiso 1 1 calc R . . . .
C78 C -0.0820(8) 0.9223(5) 0.2306(5) 0.075(3) Uani 1 1 d . U . . .
H78A H -0.087851 0.946173 0.224256 0.089 Uiso 1 1 calc R . . . .
H78B H -0.073863 0.908047 0.214074 0.089 Uiso 1 1 calc R . . . .
C83 C -0.0904(6) 0.6335(5) 0.2843(4) 0.181(6) Uani 1 1 d D U . . .
H83 H -0.052041 0.635111 0.274702 0.218 Uiso 1 1 calc R . . . .
C85 C -0.1170(11) 0.6502(6) 0.4136(5) 0.099(3) Uani 1 1 d . U . . .
H85A H -0.123748 0.670506 0.401681 0.118 Uiso 1 1 calc R . . . .
H85B H -0.146956 0.632909 0.408938 0.118 Uiso 1 1 calc R . . . .
C86 C -0.0178(11) 0.6779(7) 0.4467(5) 0.100(3) Uani 1 1 d . U . . .
H86 H 0.009924 0.696513 0.451952 0.120 Uiso 1 1 calc R . . . .
C87 C -0.0827(10) 0.6907(6) 0.4469(6) 0.099(3) Uani 1 1 d . U . . .
H87A H -0.091901 0.701248 0.465096 0.119 Uiso 1 1 calc R . . . .
H87B H -0.088604 0.708084 0.432211 0.119 Uiso 1 1 calc R . . . .
C90 C -0.0389(11) 0.6048(6) 0.4280(5) 0.099(3) Uani 1 1 d . U . . .
H90A H -0.064711 0.585269 0.423586 0.119 Uiso 1 1 calc R . . . .
H90B H 0.001559 0.596846 0.425661 0.119 Uiso 1 1 calc R . . . .
C93 C -0.1229(12) 0.6597(7) 0.4417(6) 0.099(3) Uani 1 1 d . U . . .
H93 H -0.163777 0.667541 0.444609 0.119 Uiso 1 1 calc R . . . .
C94 C -0.0085(11) 0.6461(6) 0.4635(5) 0.099(3) Uani 1 1 d . U . . .
H94A H -0.011866 0.652561 0.483342 0.119 Uiso 1 1 calc R . . . .
H94B H 0.031939 0.638571 0.460424 0.119 Uiso 1 1 calc R . . . .
C95 C -0.0946(6) 0.6621(4) 0.3084(4) 0.182(6) Uani 1 1 d D U . . .
H95 H -0.094230 0.684548 0.298361 0.219 Uiso 1 1 calc R . . . .
C100 C -0.2045(8) 0.5974(4) 0.2916(4) 0.183(6) Uani 1 1 d D U . . .
H10A H -0.199344 0.579171 0.277491 0.220 Uiso 1 1 calc R . . . .
H10B H -0.242943 0.594218 0.300375 0.220 Uiso 1 1 calc R . . . .
C103 C -0.1117(11) 0.6310(6) 0.4617(6) 0.101(3) Uani 1 1 d . U . . .
H10C H -0.140814 0.612793 0.458654 0.121 Uiso 1 1 calc R . . . .
H10D H -0.116595 0.639651 0.480928 0.121 Uiso 1 1 calc R . . . .
C104 C -0.2024(7) 0.6331(5) 0.2770(4) 0.182(6) Uani 1 1 d D U . . .
H104 H -0.234129 0.634979 0.262911 0.219 Uiso 1 1 calc R . . . .
C106 C -0.0968(8) 0.5970(4) 0.2990(5) 0.182(6) Uani 1 1 d D U . . .
H10E H -0.094031 0.578733 0.284800 0.219 Uiso 1 1 calc R . . . .
H10F H -0.064786 0.593785 0.312454 0.219 Uiso 1 1 calc R . . . .
C107 C -0.1557(9) 0.5942(4) 0.3144(4) 0.185(6) Uani 1 1 d D U . . .
H107 H -0.158599 0.571271 0.323594 0.222 Uiso 1 1 calc R . . . .
C112 C -0.1651(9) 0.6235(5) 0.3368(3) 0.183(6) Uani 1 1 d D U . . .
H11A H -0.136374 0.621056 0.351959 0.220 Uiso 1 1 calc R . . . .
H11B H -0.204418 0.621662 0.344907 0.220 Uiso 1 1 calc R . . . .
C118 C -0.2055(7) 0.6642(4) 0.2983(5) 0.182(6) Uani 1 1 d D U . . .
H11C H -0.244472 0.665083 0.306929 0.219 Uiso 1 1 calc R . . . .
H11D H -0.199046 0.686025 0.288255 0.219 Uiso 1 1 calc R . . . .
C122 C -0.1412(9) 0.6385(5) 0.2627(3) 0.183(6) Uani 1 1 d D U . . .
H12A H -0.136584 0.621954 0.247312 0.220 Uiso 1 1 calc R . . . .
H12B H -0.139131 0.661914 0.254823 0.220 Uiso 1 1 calc R . . . .
C151 C -0.1575(8) 0.6597(4) 0.3219(3) 0.183(6) Uani 1 1 d D U . . .
H151 H -0.162032 0.678349 0.335981 0.220 Uiso 1 1 calc R . . . .
C1 C 0.4689(10) 0.5825(5) 0.3958(5) 0.080(3) Uani 1 1 d . U . . .
H1 H 0.441930 0.585895 0.411839 0.096 Uiso 1 1 calc R . . . .
C2 C 0.3689(8) 0.5300(4) 0.2952(4) 0.055(2) Uani 1 1 d . U . . .
H2 H 0.402844 0.543157 0.302558 0.066 Uiso 1 1 calc R . . . .
C3 C 0.2808(8) 0.5176(4) 0.2506(4) 0.057(2) Uani 1 1 d . U . . .
H3A H 0.293228 0.536400 0.238101 0.069 Uiso 1 1 calc R . . . .
H3B H 0.247503 0.505593 0.241961 0.069 Uiso 1 1 calc R . . . .
C4 C 0.2637(8) 0.5321(4) 0.2804(4) 0.055(2) Uani 1 1 d . U . . .
H4 H 0.228346 0.546783 0.278552 0.066 Uiso 1 1 calc R . . . .
C5 C 0.3256(9) 0.6544(5) 0.1594(4) 0.067(3) Uani 1 1 d . U . . .
H5 H 0.308110 0.677408 0.155935 0.081 Uiso 1 1 calc R . . . .
C6 C 0.2508(8) 0.5024(4) 0.3019(4) 0.058(2) Uani 1 1 d . U . . .
H6A H 0.240025 0.512597 0.320017 0.069 Uiso 1 1 calc R . . . .
H6B H 0.217175 0.488886 0.295190 0.069 Uiso 1 1 calc R . . . .
C5AA C 0.3520(8) 0.5009(4) 0.3174(4) 0.058(2) Uani 1 1 d . U . . .
H5AA H 0.386092 0.486181 0.321071 0.070 Uiso 1 1 calc R . . . .
H5AB H 0.340244 0.511752 0.335136 0.070 Uiso 1 1 calc R . . . .
C8 C 0.3164(8) 0.5553(5) 0.2917(4) 0.058(2) Uani 1 1 d . U . . .
H8 H 0.326781 0.571937 0.276642 0.069 Uiso 1 1 calc R . . . .
C2BA C 0.3759(12) 0.7927(6) 0.1576(5) 0.094(3) Uani 1 1 d . U . . .
H2BA H 0.410315 0.797638 0.169676 0.113 Uiso 1 1 calc R . . . .
C6AA C 0.0988(9) 0.6050(5) 0.2398(4) 0.0614(7) Uani 1 1 d . U . . .
H6AA H 0.131480 0.596536 0.251608 0.074 Uiso 1 1 calc R . . . .
C11 C 0.4525(10) 0.5462(5) 0.3800(5) 0.075(3) Uani 1 1 d . U . . .
H11 H 0.412985 0.548452 0.371613 0.089 Uiso 1 1 calc R . . . .
C9AA C 0.3228(10) 0.6449(5) 0.1915(4) 0.067(3) Uani 1 1 d . U . . .
H9AA H 0.281154 0.642907 0.197096 0.080 Uiso 1 1 calc R . . . .
C13 C 0.3362(8) 0.4900(5) 0.2565(4) 0.059(2) Uani 1 1 d . U . . .
H13 H 0.347881 0.479048 0.238508 0.070 Uiso 1 1 calc R . . . .
C14 C 0.5306(10) 0.5763(5) 0.4071(5) 0.075(3) Uani 1 1 d . U . . .
H14 H 0.542738 0.598063 0.416392 0.090 Uiso 1 1 calc R . . . .
C2AA C 0.5776(10) 0.5689(5) 0.3838(5) 0.076(3) Uani 1 1 d . U . . .
H2AA H 0.578643 0.587671 0.370027 0.091 Uiso 1 1 calc R . . . .
H2AB H 0.616593 0.566307 0.392157 0.091 Uiso 1 1 calc R . . . .
C16 C 0.0993(8) 0.5410(5) 0.3434(4) 0.156(2) Uani 1 1 d D U . . .
H16 H 0.140638 0.538328 0.349368 0.187 Uiso 1 1 calc R . . . .
C0BA C 0.3163(10) 0.5897(5) 0.1496(4) 0.069(3) Uani 1 1 d . U . . .
H0BA H 0.293416 0.572133 0.139217 0.083 Uiso 1 1 calc R . . . .
C18 C 0.3852(8) 0.5152(4) 0.2662(4) 0.057(2) Uani 1 1 d . U . . .
H18A H 0.422617 0.502916 0.267312 0.069 Uiso 1 1 calc R . . . .
H18B H 0.389312 0.534115 0.252566 0.069 Uiso 1 1 calc R . . . .
C19 C 0.2884(9) 0.6252(5) 0.1449(4) 0.069(3) Uani 1 1 d . U . . .
H19A H 0.248591 0.625281 0.152666 0.082 Uiso 1 1 calc R . . . .
H19B H 0.285655 0.629828 0.124710 0.082 Uiso 1 1 calc R . . . .
C20 C 0.3159(9) 0.5805(5) 0.1804(4) 0.068(3) Uani 1 1 d . U . . .
H20A H 0.333553 0.557668 0.183320 0.082 Uiso 1 1 calc R . . . .
H20B H 0.275609 0.579977 0.187528 0.082 Uiso 1 1 calc R . . . .
C21 C 0.3904(9) 0.6533(5) 0.1491(4) 0.067(3) Uani 1 1 d . U . . .
H21A H 0.414100 0.669745 0.159868 0.081 Uiso 1 1 calc R . . . .
H21B H 0.392349 0.659853 0.129185 0.081 Uiso 1 1 calc R . . . .
C22 C 0.4954(9) 0.5380(5) 0.3570(5) 0.074(3) Uani 1 1 d . U . . .
H22A H 0.495138 0.556529 0.342991 0.089 Uiso 1 1 calc R . . . .
H22B H 0.484239 0.516349 0.347720 0.089 Uiso 1 1 calc R . . . .
C23 C 0.4177(10) 0.7022(6) 0.4979(5) 0.078(3) Uani 1 1 d . U . . .
H23 H 0.380271 0.714213 0.501842 0.094 Uiso 1 1 calc R . . . .
C4AA C 0.3014(8) 0.4788(5) 0.3060(4) 0.058(2) Uani 1 1 d . U . . .
H4AA H 0.291384 0.460133 0.319466 0.070 Uiso 1 1 calc R . . . .
C25 C 0.1185(9) 0.6007(5) 0.2077(4) 0.0614(7) Uani 1 1 d . U . . .
H25 H 0.151414 0.616711 0.203810 0.074 Uiso 1 1 calc R . . . .
C26 C 0.3531(9) 0.6097(5) 0.1964(5) 0.067(3) Uani 1 1 d . U . . .
H26 H 0.352736 0.604553 0.216774 0.081 Uiso 1 1 calc R . . . .
C27 C 0.4508(9) 0.5170(5) 0.4019(5) 0.075(3) Uani 1 1 d . U . . .
H27A H 0.438872 0.495287 0.392925 0.090 Uiso 1 1 calc R . . . .
H27B H 0.422003 0.522536 0.416543 0.090 Uiso 1 1 calc R . . . .
C28 C 0.3658(12) 0.8261(6) 0.1375(5) 0.094(3) Uani 1 1 d . U . . .
H28 H 0.354953 0.847637 0.147481 0.113 Uiso 1 1 calc R . . . .
C29 C 0.4904(10) 0.6848(6) 0.4595(5) 0.078(3) Uani 1 1 d . U . . .
H29 H 0.499334 0.685591 0.439148 0.094 Uiso 1 1 calc R . . . .
C30 C 0.4125(9) 0.6621(5) 0.5070(5) 0.078(3) Uani 1 1 d . U . . .
H30A H 0.402175 0.660327 0.526927 0.094 Uiso 1 1 calc R . . . .
H30B H 0.381812 0.650645 0.495976 0.094 Uiso 1 1 calc R . . . .
C31 C 0.1397(8) 0.5633(4) 0.2031(4) 0.0614(7) Uani 1 1 d . U . . .
H31A H 0.172258 0.558024 0.215836 0.074 Uiso 1 1 calc R . . . .
H31B H 0.153446 0.560259 0.183719 0.074 Uiso 1 1 calc R . . . .
C1BA C 0.3791(9) 0.5912(5) 0.1372(4) 0.070(3) Uani 1 1 d . U . . .
H1BA H 0.396617 0.568035 0.137601 0.085 Uiso 1 1 calc R . . . .
H1BB H 0.377219 0.598772 0.117537 0.085 Uiso 1 1 calc R . . . .
C33 C 0.4661(9) 0.7202(6) 0.5125(5) 0.079(3) Uani 1 1 d . U . . .
H33A H 0.458350 0.720755 0.532736 0.095 Uiso 1 1 calc R . . . .
H33B H 0.468675 0.744148 0.505779 0.095 Uiso 1 1 calc R . . . .
C0AA C 0.4307(9) 0.7029(6) 0.4649(4) 0.077(3) Uani 1 1 d . U . . .
H0AA H 0.435864 0.727558 0.459637 0.092 Uiso 1 1 calc R . . . .
C3BA C 0.3349(11) 0.7493(6) 0.1213(5) 0.095(3) Uani 1 1 d . U . . .
H3BA H 0.344383 0.727984 0.111101 0.114 Uiso 1 1 calc R . . . .
H3BB H 0.299080 0.745106 0.132157 0.114 Uiso 1 1 calc R . . . .
C36 C 0.5133(10) 0.5124(5) 0.4157(5) 0.075(3) Uani 1 1 d . U . . .
H36 H 0.512981 0.493538 0.429726 0.090 Uiso 1 1 calc R . . . .
C7AA C 0.0633(9) 0.5417(5) 0.2397(4) 0.0614(7) Uani 1 1 d . U . . .
H7AA H 0.094390 0.535348 0.252935 0.074 Uiso 1 1 calc R . . . .
H7AB H 0.030134 0.525997 0.242655 0.074 Uiso 1 1 calc R . . . .
C38 C 0.4188(9) 0.6084(5) 0.1856(4) 0.068(3) Uani 1 1 d . U . . .
H38A H 0.442405 0.626290 0.194757 0.082 Uiso 1 1 calc R . . . .
H38B H 0.436323 0.585725 0.189469 0.082 Uiso 1 1 calc R . . . .
C8AA C 0.0437(8) 0.5797(5) 0.2450(4) 0.0614(7) Uani 1 1 d . U . . .
H8AA H 0.029470 0.582271 0.264581 0.074 Uiso 1 1 calc R . . . .
C40 C 0.5395(10) 0.7037(6) 0.4759(4) 0.079(3) Uani 1 1 d . U . . .
H40A H 0.577439 0.692877 0.471942 0.095 Uiso 1 1 calc R . . . .
H40B H 0.541411 0.728022 0.470120 0.095 Uiso 1 1 calc R . . . .
C41 C 0.3875(11) 0.7583(6) 0.1425(5) 0.094(3) Uani 1 1 d . U . . .
H41 H 0.392645 0.739403 0.156346 0.113 Uiso 1 1 calc R . . . .
C42 C 0.5575(10) 0.5344(5) 0.3698(5) 0.074(3) Uani 1 1 d . U . . .
H42 H 0.585345 0.528412 0.354646 0.089 Uiso 1 1 calc R . . . .
C43 C 0.4152(10) 0.6150(5) 0.1532(4) 0.069(3) Uani 1 1 d . U . . .
H43 H 0.455429 0.614172 0.145436 0.082 Uiso 1 1 calc R . . . .
C44 C 0.3187(12) 0.8121(6) 0.1166(5) 0.096(3) Uani 1 1 d . U . . .
H44A H 0.282110 0.810476 0.127331 0.115 Uiso 1 1 calc R . . . .
H44B H 0.312723 0.830468 0.102679 0.115 Uiso 1 1 calc R . . . .
C45 C 0.5210(10) 0.6649(6) 0.5175(5) 0.080(3) Uani 1 1 d . U . . .
H45A H 0.512630 0.665298 0.537734 0.096 Uiso 1 1 calc R . . . .
H45B H 0.558383 0.652954 0.514732 0.096 Uiso 1 1 calc R . . . .
C46 C 0.5256(10) 0.7012(6) 0.5068(5) 0.078(3) Uani 1 1 d . U . . .
H46 H 0.556906 0.713192 0.517460 0.094 Uiso 1 1 calc R . . . .
C3AA C 0.5269(10) 0.5487(5) 0.4303(5) 0.075(3) Uani 1 1 d . U . . .
H3AA H 0.495654 0.554598 0.443625 0.090 Uiso 1 1 calc R . . . .
H3AB H 0.564002 0.547516 0.440630 0.090 Uiso 1 1 calc R . . . .
C48 C 0.3193(9) 0.4630(5) 0.2767(4) 0.060(2) Uani 1 1 d . U . . .
H48A H 0.352206 0.447031 0.279300 0.071 Uiso 1 1 calc R . . . .
H48B H 0.286292 0.449786 0.269079 0.071 Uiso 1 1 calc R . . . .
C49 C 0.0678(8) 0.6101(5) 0.1890(4) 0.0614(7) Uani 1 1 d . U . . .
H49A H 0.080442 0.609178 0.169290 0.074 Uiso 1 1 calc R . . . .
H49B H 0.055426 0.633825 0.193061 0.074 Uiso 1 1 calc R . . . .
C4BA C 0.3238(12) 0.7786(6) 0.1001(5) 0.096(3) Uani 1 1 d . U . . .
H4BA H 0.290107 0.774162 0.087561 0.115 Uiso 1 1 calc R . . . .
C51 C 0.0837(7) 0.5106(5) 0.3234(3) 0.1576(12) Uani 1 1 d D U . . .
H51 H 0.108907 0.511698 0.306526 0.189 Uiso 1 1 calc R . . . .
C52 C 0.4359(12) 0.7943(6) 0.1040(5) 0.096(3) Uani 1 1 d . U . . .
H52 H 0.472163 0.797250 0.092809 0.115 Uiso 1 1 calc R . . . .
C53 C 0.6137(10) 0.7503(8) 0.2159(6) 0.160(5) Uani 1 1 d D U . . .
H53A H 0.627162 0.769733 0.204303 0.192 Uiso 1 1 calc R . . . .
H53B H 0.646896 0.734591 0.218607 0.192 Uiso 1 1 calc R . . . .
C5BA C 0.5235(12) 0.7124(8) 0.2492(6) 0.160(5) Uani 1 1 d D U . . .
H5BA H 0.511803 0.692175 0.260685 0.191 Uiso 1 1 calc R . . . .
C1AA C 0.4838(10) 0.6449(6) 0.4693(4) 0.078(3) Uani 1 1 d . U . . .
H1AA H 0.451634 0.633722 0.459102 0.094 Uiso 1 1 calc R . . . .
H1AB H 0.520010 0.632133 0.465385 0.094 Uiso 1 1 calc R . . . .
C56 C 0.0393(8) 0.5484(5) 0.1883(4) 0.0614(7) Uani 1 1 d . U . . .
H56A H 0.006392 0.532223 0.189648 0.074 Uiso 1 1 calc R . . . .
H56B H 0.055339 0.546710 0.169204 0.074 Uiso 1 1 calc R . . . .
C57 C 0.4708(10) 0.6447(6) 0.5017(5) 0.079(3) Uani 1 1 d . U . . .
H57 H 0.469365 0.620512 0.508619 0.095 Uiso 1 1 calc R . . . .
C58 C 0.0861(8) 0.5380(5) 0.2092(4) 0.0614(7) Uani 1 1 d . U . . .
H58 H 0.098081 0.513753 0.205662 0.074 Uiso 1 1 calc R . . . .
C59 C 0.3842(11) 0.7846(6) 0.0837(5) 0.096(3) Uani 1 1 d . U . . .
H59A H 0.394446 0.763503 0.073399 0.116 Uiso 1 1 calc R . . . .
H59B H 0.378936 0.803240 0.069948 0.116 Uiso 1 1 calc R . . . .
C60 C 0.5546(10) 0.5036(5) 0.3911(5) 0.076(3) Uani 1 1 d . U . . .
H60A H 0.540447 0.482799 0.381499 0.091 Uiso 1 1 calc R . . . .
H60B H 0.593926 0.498785 0.398390 0.091 Uiso 1 1 calc R . . . .
C61 C 0.5641(12) 0.7308(6) 0.2001(5) 0.160(5) Uani 1 1 d D U . . .
H61 H 0.577251 0.722224 0.181500 0.192 Uiso 1 1 calc R . . . .
C0CA C 0.1435(8) 0.6565(5) 0.5047(3) 0.154(3) Uani 1 1 d D U . . .
H0CA H 0.125835 0.647256 0.487241 0.185 Uiso 1 1 calc R . . . .
C6BA C 0.5348(14) 0.7015(7) 0.2181(6) 0.160(5) Uani 1 1 d D U . . .
H6BA H 0.497467 0.695043 0.209384 0.192 Uiso 1 1 calc R . . . .
H6BB H 0.560224 0.681068 0.217858 0.192 Uiso 1 1 calc R . . . .
C64 C 0.4430(11) 0.7616(6) 0.1236(5) 0.096(3) Uani 1 1 d . U . . .
H64A H 0.447426 0.740687 0.112061 0.116 Uiso 1 1 calc R . . . .
H64B H 0.477990 0.764022 0.135316 0.116 Uiso 1 1 calc R . . . .
C1CA C 0.0975(7) 0.6801(6) 0.5203(4) 0.154(4) Uani 1 1 d D U . . .
H1CA H 0.085880 0.699339 0.508154 0.185 Uiso 1 1 calc R . . . .
H1CB H 0.062409 0.666524 0.524816 0.185 Uiso 1 1 calc R . . . .
C67 C 0.1991(9) 0.6788(6) 0.4972(4) 0.154(3) Uani 1 1 d D U . . .
H67 H 0.227876 0.663790 0.487485 0.185 Uiso 1 1 calc R . . . .
C68 C 0.4845(12) 0.7696(7) 0.2256(6) 0.160(5) Uani 1 1 d D U . . .
H68 H 0.450510 0.785238 0.223106 0.192 Uiso 1 1 calc R . . . .
C70 C 0.0177(9) 0.5133(5) 0.3143(3) 0.158(2) Uani 1 1 d D U . . .
H70A H 0.010738 0.535262 0.304626 0.189 Uiso 1 1 calc R . . . .
H70B H 0.007922 0.494359 0.301384 0.189 Uiso 1 1 calc R . . . .
C71 C 0.0595(8) 0.5395(4) 0.3702(3) 0.1576(12) Uani 1 1 d D U . . .
H71 H 0.068832 0.559043 0.382905 0.189 Uiso 1 1 calc R . . . .
C4CA C -0.0066(8) 0.5405(5) 0.3621(4) 0.1576(12) Uani 1 1 d D U . . .
H4CA H -0.030661 0.538170 0.379033 0.189 Uiso 1 1 calc R . . . .
H4CB H -0.015767 0.562867 0.353382 0.189 Uiso 1 1 calc R . . . .
C76 C -0.0032(8) 0.5879(5) 0.2253(4) 0.0614(7) Uani 1 1 d . U . . .
H76A H -0.017453 0.611354 0.229227 0.074 Uiso 1 1 calc R . . . .
H76B H -0.035746 0.571859 0.228397 0.074 Uiso 1 1 calc R . . . .
C77 C 0.4230(11) 0.8284(6) 0.1196(5) 0.096(3) Uani 1 1 d . U . . .
H77A H 0.419030 0.847150 0.105907 0.115 Uiso 1 1 calc R . . . .
H77B H 0.456042 0.833943 0.131956 0.115 Uiso 1 1 calc R . . . .
C2CA C 0.1899(9) 0.6405(4) 0.5518(3) 0.153(4) Uani 1 1 d D U . . .
H2CA H 0.200965 0.620841 0.564065 0.184 Uiso 1 1 calc R . . . .
C80 C 0.2465(7) 0.6607(6) 0.5434(4) 0.154(4) Uani 1 1 d D U . . .
H80A H 0.272812 0.645733 0.532572 0.185 Uiso 1 1 calc R . . . .
H80B H 0.267318 0.668451 0.560318 0.185 Uiso 1 1 calc R . . . .
C82 C 0.2272(9) 0.6927(4) 0.5253(5) 0.153(4) Uani 1 1 d D U . . .
H82 H 0.262282 0.706681 0.520630 0.184 Uiso 1 1 calc R . . . .
C7BA C 0.5930(11) 0.7644(6) 0.2452(5) 0.160(5) Uani 1 1 d D U . . .
H7BA H 0.624665 0.777603 0.254590 0.192 Uiso 1 1 calc R . . . .
C84 C 0.0954(8) 0.4762(5) 0.3392(4) 0.1576(12) Uani 1 1 d D U . . .
H84A H 0.087600 0.456618 0.326573 0.189 Uiso 1 1 calc R . . . .
H84B H 0.136584 0.475109 0.344862 0.189 Uiso 1 1 calc R . . . .
C8BA C 0.4706(13) 0.7372(7) 0.2443(7) 0.160(5) Uani 1 1 d D U . . .
H8BA H 0.445342 0.723292 0.231750 0.193 Uiso 1 1 calc R . . . .
C88 C 0.0164(9) 0.5858(5) 0.1931(4) 0.0614(7) Uani 1 1 d . U . . .
H88 H -0.016347 0.591453 0.180299 0.074 Uiso 1 1 calc R . . . .
C3CA C 0.1258(10) 0.6944(4) 0.5481(5) 0.153(4) Uani 1 1 d D U . . .
H3CA H 0.097052 0.709108 0.558133 0.184 Uiso 1 1 calc R . . . .
C99 C 0.1834(11) 0.7156(6) 0.5427(6) 0.154(4) Uani 1 1 d D U . . .
H99A H 0.201235 0.722090 0.560670 0.184 Uiso 1 1 calc R . . . .
H99B H 0.174198 0.736779 0.532320 0.184 Uiso 1 1 calc R . . . .
C9BA C 0.5388(12) 0.7879(6) 0.2395(6) 0.160(5) Uani 1 1 d D U . . .
H9BA H 0.551079 0.806931 0.227284 0.192 Uiso 1 1 calc R . . . .
H9BB H 0.526168 0.797998 0.257385 0.192 Uiso 1 1 calc R . . . .
C102 C 0.0713(9) 0.5041(5) 0.3857(3) 0.1576(12) Uani 1 1 d D U . . .
H10G H 0.112588 0.502677 0.391211 0.189 Uiso 1 1 calc R . . . .
H10H H 0.047244 0.502644 0.402694 0.189 Uiso 1 1 calc R . . . .
C110 C 0.1615(9) 0.6259(3) 0.5244(4) 0.154(3) Uani 1 1 d D U . . .
H11E H 0.126857 0.612086 0.529167 0.185 Uiso 1 1 calc R . . . .
H11F H 0.189468 0.610807 0.514664 0.185 Uiso 1 1 calc R . . . .
C129 C -0.0217(6) 0.5109(5) 0.3413(4) 0.1576(12) Uani 1 1 d D U . . .
H129 H -0.063487 0.512410 0.335923 0.189 Uiso 1 1 calc R . . . .
C130 C -0.0101(8) 0.4762(5) 0.3569(4) 0.1576(12) Uani 1 1 d D U . . .
H13A H -0.020487 0.456811 0.344591 0.189 Uiso 1 1 calc R . . . .
H13B H -0.034597 0.474969 0.373726 0.189 Uiso 1 1 calc R . . . .
C136 C 0.5792(13) 0.7302(7) 0.2616(7) 0.160(5) Uani 1 1 d D U . . .
H13C H 0.612662 0.714407 0.260213 0.192 Uiso 1 1 calc R . . . .
H13D H 0.572737 0.735465 0.281491 0.192 Uiso 1 1 calc R . . . .
C166 C 0.1445(9) 0.6635(6) 0.5675(3) 0.155(4) Uani 1 1 d D U . . .
H16A H 0.161832 0.672371 0.584882 0.186 Uiso 1 1 calc R . . . .
H16B H 0.110056 0.649611 0.572424 0.186 Uiso 1 1 calc R . . . .
C174 C 0.5131(12) 0.7582(7) 0.1973(6) 0.161(5) Uani 1 1 d D U . . .
H17A H 0.528622 0.778803 0.187828 0.193 Uiso 1 1 calc R . . . .
H17B H 0.482531 0.748446 0.185193 0.193 Uiso 1 1 calc R . . . .
C2DA C 0.2077(8) 0.5649(4) 0.4528(3) 0.161(3) Uani 1 1 d D U . . .
H2DA H 0.185857 0.557431 0.469755 0.193 Uiso 1 1 calc R . . . .
C4DA C 0.2009(8) 0.5750(4) 0.3998(3) 0.158(3) Uani 1 1 d D U . . .
H4DA H 0.175381 0.573704 0.383030 0.190 Uiso 1 1 calc R . . . .
C8CA C 0.3179(6) 0.5899(5) 0.4254(4) 0.153(3) Uani 1 1 d D U . . .
H8CA H 0.339115 0.597300 0.408485 0.183 Uiso 1 1 calc R . . . .
H8CB H 0.344847 0.591229 0.441363 0.183 Uiso 1 1 calc R . . . .
C1DA C 0.2559(9) 0.5510(5) 0.3958(3) 0.161(3) Uani 1 1 d D U . . .
H1DA H 0.242812 0.527150 0.392561 0.193 Uiso 1 1 calc R . . . .
H1DB H 0.277846 0.558518 0.379172 0.193 Uiso 1 1 calc R . . . .
C0DA C 0.2640(8) 0.6147(3) 0.4305(4) 0.160(3) Uani 1 1 d D U . . .
H0DA H 0.277951 0.638754 0.433175 0.192 Uiso 1 1 calc R . . . .
C3DA C 0.1660(6) 0.5634(4) 0.4264(4) 0.160(3) Uani 1 1 d D U . . .
H3DA H 0.151508 0.539709 0.423804 0.191 Uiso 1 1 calc R . . . .
H3DB H 0.132282 0.578641 0.429276 0.191 Uiso 1 1 calc R . . . .
C7CA C 0.2237(8) 0.6126(4) 0.4036(4) 0.159(3) Uani 1 1 d D U . . .
H7CA H 0.187799 0.622602 0.412018 0.191 Uiso 1 1 calc R . . . .
C5DA C 0.2961(7) 0.5521(4) 0.4216(4) 0.159(3) Uani 1 1 d D U . . .
H5DA H 0.329951 0.536488 0.418699 0.191 Uiso 1 1 calc R . . . .
C156 C 0.2606(9) 0.5400(4) 0.4478(4) 0.159(3) Uani 1 1 d D U . . .
H15A H 0.286023 0.539928 0.464373 0.190 Uiso 1 1 calc R . . . .
H15B H 0.246196 0.516405 0.444804 0.190 Uiso 1 1 calc R . . . .
C160 C 0.2296(9) 0.6029(5) 0.4569(3) 0.158(3) Uani 1 1 d D U . . .
H16C H 0.196009 0.618223 0.459939 0.189 Uiso 1 1 calc R . . . .
H16D H 0.254946 0.604157 0.473476 0.189 Uiso 1 1 calc R . . . .
C7DA C 0.0558(9) 0.4735(4) 0.3653(4) 0.180(10) Uani 1 1 d D U . . .
H7DA H 0.062880 0.451130 0.374929 0.216 Uiso 1 1 calc R . . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag1 Ag1 2.826(2) 2_565 ?
Ag1 Ag01 2.8532(17) . ?
Ag1 Ag2 2.7998(17) . ?
Ag1 Ag2 2.8114(17) 2_565 ?
Ag1 Ag5 2.8573(16) . ?
Ag1 Ag8 2.8141(17) 2_565 ?
Ag1 Ag10 2.7488(18) 2_565 ?
Ag1 Ag10 3.1075(18) . ?
Ag1 Ag12 3.0674(19) . ?
Ag1 Ag13 2.7407(19) . ?
Ag1 Ag20 2.7568(18) . ?
Ag1 Ag25 3.0774(19) 2_565 ?
Ag01 Ag5 2.9296(18) . ?
Ag01 Ag8 2.8861(18) 2_565 ?
Ag01 Ag10 2.8492(18) . ?
Ag01 Ag10 2.880(2) 2_565 ?
Ag01 Ag13 3.128(2) . ?
Ag01 Ag15 3.001(2) . ?
Ag01 Ag18 3.079(2) 2_565 ?
Ag01 Ag19 2.9048(19) . ?
Ag01 Cl8 2.745(4) . ?
Ag01 S10 2.609(5) . ?
Ag1A Ag1A 2.761(4) 2_565 ?
Ag1A Ag1D 2.827(3) . ?
Ag1A Ag2 2.7398(19) . ?
Ag1A Ag2 3.1010(19) 2_565 ?
Ag1A Ag7 3.207(2) . ?
Ag1A Ag11 2.964(2) . ?
Ag1A Ag12 3.269(3) . ?
Ag1A Ag17 2.876(2) . ?
Ag1A Ag17 2.881(2) 2_565 ?
Ag1A Ag20 3.243(2) . ?
Ag1A S2A 2.554(8) . ?
Ag1B Ag1E 3.008(3) . ?
Ag1B Ag7 3.029(2) . ?
Ag1B Ag20 2.905(2) . ?
Ag1B S16 2.443(5) . ?
Ag1B S20 2.426(6) . ?
Ag1D Ag1D 2.903(4) 2_565 ?
Ag1D Ag17 2.967(3) 2_565 ?
Ag1D S18 2.436(5) . ?
Ag1D S19 2.428(5) . ?
Ag1E Ag8 2.952(2) 2_565 ?
Ag1E Ag25 2.834(2) 2_565 ?
Ag1E S6 2.419(6) . ?
Ag1E S25 2.411(5) . ?
Ag2 Ag1 2.8114(17) 2_565 ?
Ag2 Ag1A 3.1011(19) 2_565 ?
Ag2 Ag2 2.799(2) 2_565 ?
Ag2 Ag02 2.7788(17) . ?
Ag2 Ag7 2.8381(18) . ?
Ag2 Ag12 2.7745(17) 2_565 ?
Ag2 Ag13 3.1535(19) 2_565 ?
Ag2 Ag17 2.8016(18) . ?
Ag2 Ag20 3.1528(17) . ?
Ag2 Ag25 2.7545(18) 2_565 ?
Ag02 Ag7 2.8844(17) . ?
Ag02 Ag12 2.860(2) 2_565 ?
Ag02 Ag13 2.878(2) 2_565 ?
Ag02 Ag16 2.925(2) . ?
Ag02 Ag17 2.863(2) . ?
Ag02 Ag21 2.9021(18) . ?
Ag02 Ag25 3.1400(19) 2_565 ?
Ag02 Ag29 3.180(2) 2_565 ?
Ag02 S3 2.565(5) . ?
Ag5 Ag05 2.9178(18) . ?
Ag5 Ag8 2.9121(18) 2_565 ?
Ag5 Ag12 2.826(2) . ?
Ag5 Ag13 2.8861(19) . ?
Ag5 Ag19 3.117(2) . ?
Ag5 Ag20 3.1795(19) . ?
Ag5 Ag32 2.989(2) . ?
Ag5 S1 2.592(4) . ?
Ag5 Cl8 2.773(5) . ?
Ag05 Ag8 3.0948(18) 2_565 ?
Ag05 Ag20 2.9504(18) . ?
Ag05 S1 2.442(5) . ?
Ag05 S16 2.370(5) . ?
Ag7 Ag11 2.893(2) . ?
Ag7 Ag17 2.9132(18) . ?
Ag7 Ag20 2.8682(19) . ?
Ag7 Ag21 3.180(2) . ?
Ag7 Ag25 2.840(2) 2_565 ?
Ag7 Cl4 2.769(8) . ?
Ag7 S20 2.597(5) . ?
Ag8 Ag1 2.8139(17) 2_565 ?
Ag8 Ag01 2.8861(18) 2_565 ?
Ag8 Ag1E 2.952(2) 2_565 ?
Ag8 Ag5 2.9122(18) 2_565 ?
Ag8 Ag05 3.0949(18) 2_565 ?
Ag8 Ag10 3.1428(18) . ?
Ag8 Ag18 2.8819(19) . ?
Ag8 Ag20 2.8819(19) 2_565 ?
Ag8 Ag25 2.8318(19) . ?
Ag8 S6 2.606(5) 2_565 ?
Ag8 Cl8 2.773(5) 2_565 ?
Ag10 Ag1 2.7487(18) 2_565 ?
Ag10 Ag01 2.880(2) 2_565 ?
Ag10 Ag10 2.796(3) 2_565 ?
Ag10 Ag13 3.123(2) . ?
Ag10 Ag15 2.889(2) . ?
Ag10 Ag18 2.9005(19) . ?
Ag10 Ag25 3.173(2) . ?
Ag10 S1A 2.583(7) . ?
Ag11 Ag17 3.196(2) . ?
Ag11 S19 2.360(5) . ?
Ag11 S20 2.427(5) . ?
Ag12 Ag2 2.7744(17) 2_565 ?
Ag12 Ag02 2.860(2) 2_565 ?
Ag12 Ag13 2.772(3) . ?
Ag12 Ag17 3.222(2) 2_565 ?
Ag12 Ag20 3.208(2) . ?
Ag12 Ag29 2.915(2) . ?
Ag12 Ag32 2.893(2) . ?
Ag12 S2A 2.566(8) . ?
Ag13 Ag2 3.1535(19) 2_565 ?
Ag13 Ag02 2.878(2) 2_565 ?
Ag13 Ag16 2.818(2) 2_565 ?
Ag13 Ag19 2.933(2) . ?
Ag13 Ag25 3.236(2) . ?
Ag13 S1A 2.522(7) . ?
Ag15 Ag15 3.079(3) 2_565 ?
Ag15 Ag18 3.3157(19) . ?
Ag15 S7 2.402(4) . ?
Ag15 S10 2.425(5) . ?
Ag16 Ag13 2.818(2) 2_565 ?
Ag16 Ag32 3.023(2) 2_565 ?
Ag16 S2 2.407(5) . ?
Ag16 S3 2.474(5) . ?
Ag17 Ag1A 2.881(2) 2_565 ?
Ag17 Ag1D 2.967(3) 2_565 ?
Ag17 Ag12 3.222(2) 2_565 ?
Ag17 Ag29 2.9097(19) 2_565 ?
Ag17 Cl4 2.694(8) . ?
Ag17 S18 2.570(5) 2_565 ?
Ag18 Ag01 3.079(2) 2_565 ?
Ag18 S6 2.438(5) 2_565 ?
Ag18 S7 2.371(5) . ?
Ag19 S2 2.365(5) 2_565 ?
Ag19 S10 2.428(5) . ?
Ag20 Ag8 2.8820(19) 2_565 ?
Ag20 Ag25 2.774(2) 2_565 ?
Ag20 S2A 2.530(7) . ?
Ag21 Ag25 2.981(2) 2_565 ?
Ag21 S3 2.416(5) . ?
Ag21 S25 2.364(5) . ?
Ag25 Ag1 3.0774(19) 2_565 ?
Ag25 Ag1E 2.834(2) 2_565 ?
Ag25 Ag2 2.7546(18) 2_565 ?
Ag25 Ag02 3.1400(19) 2_565 ?
Ag25 Ag7 2.840(2) 2_565 ?
Ag25 Ag20 2.774(2) 2_565 ?
Ag25 Ag21 2.981(2) 2_565 ?
Ag25 S1A 2.577(6) . ?
Ag29 Ag02 3.180(2) 2_565 ?
Ag29 Ag17 2.9098(19) 2_565 ?
Ag29 S4 2.375(5) . ?
Ag29 S18 2.446(5) . ?
Ag32 Ag16 3.023(2) 2_565 ?
Ag32 S1 2.422(5) . ?
Ag32 S4 2.428(5) . ?
S1A C8BA 1.77(3) . ?
S1 C8 1.774(18) . ?
S2A C7CA 1.764(9) . ?
S2 Ag19 2.365(5) 2_565 ?
S2 C35 1.90(2) . ?
S3 C17 1.80(2) . ?
S4 C1 1.83(2) . ?
S6 Ag8 2.606(5) 2_565 ?
S6 Ag18 2.438(5) 2_565 ?
S6 C6AA 1.774(18) . ?
S7 C2BA 1.92(2) . ?
Cl8 Ag8 2.773(5) 2_565 ?
S10 C9AA 1.806(19) . ?
S16 C16 1.905(19) . ?
S18 Ag17 2.570(5) 2_565 ?
S18 C0AA 1.80(2) . ?
S19 C67 1.871(18) . ?
S20 C74 1.79(2) . ?
S25 C95 1.831(9) . ?
C7 C17 1.49(2) . ?
C7 C37 1.48(2) . ?
C7 C47 1.54(3) . ?
C9 C37 1.55(2) . ?
C9 C39 1.59(3) . ?
C9 C50 1.47(2) . ?
C10 C32 1.52(2) . ?
C10 C39 1.50(2) . ?
C10 C47 1.64(2) . ?
C12 C35 1.59(3) . ?
C12 C69 1.51(3) . ?
C12 C78 1.53(3) . ?
C15 C24 1.58(3) . ?
C15 C35 1.52(3) . ?
C15 C54 1.50(3) . ?
C17 C34 1.53(2) . ?
C24 C66 1.46(3) . ?
C32 C34 1.50(2) . ?
C34 C50 1.55(2) . ?
C54 C55 1.48(2) . ?
C55 C63 1.545(10) . ?
C55 C78 1.51(3) . ?
C62 C90 1.51(3) . ?
C62 C94 1.51(3) . ?
C62 C103 1.57(3) . ?
C63 C66 1.46(3) . ?
C65 C74 1.56(3) . ?
C65 C85 1.66(3) . ?
C65 C90 1.52(3) . ?
C66 C69 1.54(3) . ?
C74 C86 1.65(3) . ?
C83 C95 1.580(8) . ?
C83 C106 1.563(8) . ?
C83 C122 1.546(8) . ?
C85 C93 1.38(3) . ?
C86 C87 1.55(3) . ?
C86 C94 1.47(3) . ?
C87 C93 1.51(3) . ?
C93 C103 1.47(3) . ?
C95 C151 1.557(8) . ?
C100 C104 1.528(8) . ?
C100 C107 1.543(8) . ?
C104 C118 1.557(9) . ?
C104 C122 1.553(8) . ?
C106 C107 1.519(8) . ?
C107 C112 1.554(8) . ?
C112 C151 1.564(8) . ?
C118 C151 1.563(8) . ?
C1 C11 1.62(3) . ?
C1 C14 1.51(3) . ?
C2 C5AA 1.57(2) . ?
C2 C8 1.54(2) . ?
C2 C18 1.53(2) . ?
C3 C4 1.56(2) . ?
C3 C13 1.66(2) . ?
C4 C6 1.55(2) . ?
C4 C8 1.58(2) . ?
C5 C9AA 1.56(3) . ?
C5 C19 1.55(2) . ?
C5 C21 1.54(3) . ?
C6 C4AA 1.47(2) . ?
C5AA C4AA 1.52(2) . ?
C2BA C28 1.61(3) . ?
C2BA C41 1.52(3) . ?
C6AA C25 1.59(2) . ?
C6AA C8AA 1.60(2) . ?
C11 C22 1.49(3) . ?
C11 C27 1.52(3) . ?
C9AA C26 1.53(2) . ?
C13 C18 1.54(2) . ?
C13 C48 1.46(2) . ?
C14 C2AA 1.55(3) . ?
C14 C3AA 1.52(3) . ?
C2AA C42 1.54(2) . ?
C16 C51 1.538(8) . ?
C16 C71 1.553(8) . ?
C0BA C19 1.51(2) . ?
C0BA C20 1.49(3) . ?
C0BA C1BA 1.54(3) . ?
C20 C26 1.59(2) . ?
C21 C43 1.58(2) . ?
C22 C42 1.53(3) . ?
C23 C30 1.60(3) . ?
C23 C33 1.46(3) . ?
C23 C0AA 1.58(3) . ?
C4AA C48 1.56(2) . ?
C25 C31 1.52(2) . ?
C25 C49 1.49(2) . ?
C26 C38 1.57(3) . ?
C27 C36 1.56(3) . ?
C28 C44 1.55(3) . ?
C28 C77 1.55(3) . ?
C29 C0AA 1.54(3) . ?
C29 C40 1.53(3) . ?
C29 C1AA 1.60(3) . ?
C30 C57 1.50(3) . ?
C31 C58 1.58(2) . ?
C1BA C43 1.44(2) . ?
C33 C46 1.55(3) . ?
C3BA C41 1.59(3) . ?
C3BA C4BA 1.52(3) . ?
C36 C3AA 1.58(3) . ?
C36 C60 1.52(3) . ?
C7AA C8AA 1.54(2) . ?
C7AA C58 1.53(2) . ?
C38 C43 1.55(3) . ?
C8AA C76 1.44(2) . ?
C40 C46 1.50(3) . ?
C41 C64 1.54(3) . ?
C42 C60 1.55(3) . ?
C44 C4BA 1.51(3) . ?
C45 C46 1.48(3) . ?
C45 C57 1.56(3) . ?
C49 C88 1.50(2) . ?
C4BA C59 1.59(3) . ?
C51 C70 1.556(8) . ?
C51 C84 1.533(9) . ?
C52 C59 1.56(3) . ?
C52 C64 1.56(3) . ?
C52 C77 1.52(3) . ?
C53 C61 1.538(10) . ?
C53 C7BA 1.557(10) . ?
C5BA C6BA 1.545(10) . ?
C5BA C8BA 1.543(10) . ?
C5BA C136 1.546(10) . ?
C1AA C57 1.56(3) . ?
C56 C58 1.50(2) . ?
C56 C88 1.54(2) . ?
C61 C6BA 1.554(10) . ?
C61 C174 1.562(10) . ?
C0CA C1CA 1.559(5) . ?
C0CA C67 1.558(5) . ?
C0CA C110 1.550(6) . ?
C1CA C3CA 1.557(6) . ?
C67 C82 1.563(6) . ?
C68 C8BA 1.555(10) . ?
C68 C9BA 1.554(10) . ?
C68 C174 1.547(10) . ?
C70 C129 1.554(8) . ?
C71 C4CA 1.543(8) . ?
C71 C102 1.559(8) . ?
C4CA C129 1.533(8) . ?
C76 C88 1.58(2) . ?
C2CA C80 1.546(6) . ?
C2CA C110 1.545(6) . ?
C2CA C166 1.541(6) . ?
C80 C82 1.556(6) . ?
C82 C99 1.556(6) . ?
C7BA C9BA 1.543(10) . ?
C7BA C136 1.550(10) . ?
C84 C7DA 1.527(9) . ?
C3CA C99 1.553(6) . ?
C3CA C166 1.553(6) . ?
C102 C7DA 1.554(8) . ?
C129 C130 1.539(8) . ?
C130 C7DA 1.544(9) . ?
C2DA C3DA 1.562(8) . ?
C2DA C156 1.546(8) . ?
C2DA C160 1.545(8) . ?
C4DA C1DA 1.557(8) . ?
C4DA C3DA 1.545(8) . ?
C4DA C7CA 1.537(8) . ?
C8CA C0DA 1.562(8) . ?
C8CA C5DA 1.541(8) . ?
C1DA C5DA 1.520(9) . ?
C0DA C7CA 1.564(8) . ?
C0DA C160 1.534(8) . ?
C5DA C156 1.541(8) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Ag1 Ag1 Ag01 109.45(4) 2_565 . ?
Ag1 Ag1 Ag5 158.64(8) 2_565 . ?
Ag1 Ag1 Ag10 54.94(4) 2_565 . ?
Ag1 Ag1 Ag12 115.49(5) 2_565 . ?
Ag1 Ag1 Ag25 90.18(6) 2_565 2_565 ?
Ag01 Ag1 Ag5 61.73(4) . . ?
Ag01 Ag1 Ag10 56.92(4) . . ?
Ag01 Ag1 Ag12 110.32(6) . . ?
Ag01 Ag1 Ag25 109.02(5) . 2_565 ?
Ag2 Ag1 Ag1 59.96(4) . 2_565 ?
Ag2 Ag1 Ag1 59.56(4) 2_565 2_565 ?
Ag2 Ag1 Ag01 133.72(6) 2_565 . ?
Ag2 Ag1 Ag01 158.62(6) . . ?
Ag2 Ag1 Ag2 59.84(5) . 2_565 ?
Ag2 Ag1 Ag5 134.75(6) . . ?
Ag2 Ag1 Ag5 110.87(5) 2_565 . ?
Ag2 Ag1 Ag8 110.94(5) . 2_565 ?
Ag2 Ag1 Ag8 160.39(6) 2_565 2_565 ?
Ag2 Ag1 Ag10 114.83(5) . . ?
Ag2 Ag1 Ag10 88.96(5) 2_565 . ?
Ag2 Ag1 Ag12 56.12(4) 2_565 . ?
Ag2 Ag1 Ag12 90.99(5) . . ?
Ag2 Ag1 Ag25 115.41(5) 2_565 2_565 ?
Ag2 Ag1 Ag25 55.66(4) . 2_565 ?
Ag5 Ag1 Ag10 108.76(5) . . ?
Ag5 Ag1 Ag12 56.85(4) . . ?
Ag5 Ag1 Ag25 110.96(5) . 2_565 ?
Ag8 Ag1 Ag1 133.60(6) 2_565 2_565 ?
Ag8 Ag1 Ag01 61.22(4) 2_565 . ?
Ag8 Ag1 Ag5 61.79(4) 2_565 . ?
Ag8 Ag1 Ag10 110.53(5) 2_565 . ?
Ag8 Ag1 Ag12 109.80(5) 2_565 . ?
Ag8 Ag1 Ag25 57.25(4) 2_565 2_565 ?
Ag10 Ag1 Ag1 67.74(4) 2_565 2_565 ?
Ag10 Ag1 Ag01 61.85(5) 2_565 . ?
Ag10 Ag1 Ag2 127.20(5) 2_565 2_565 ?
Ag10 Ag1 Ag2 96.89(5) 2_565 . ?
Ag10 Ag1 Ag5 117.32(5) 2_565 . ?
Ag10 Ag1 Ag8 68.79(5) 2_565 2_565 ?
Ag10 Ag1 Ag10 56.64(7) 2_565 . ?
Ag10 Ag1 Ag12 171.96(7) 2_565 . ?
Ag10 Ag1 Ag20 117.78(6) 2_565 . ?
Ag10 Ag1 Ag25 65.72(5) 2_565 2_565 ?
Ag12 Ag1 Ag10 118.36(6) . . ?
Ag12 Ag1 Ag25 120.67(6) . 2_565 ?
Ag13 Ag1 Ag1 96.80(7) . 2_565 ?
Ag13 Ag1 Ag01 67.96(5) . . ?
Ag13 Ag1 Ag2 69.20(5) . 2_565 ?
Ag13 Ag1 Ag2 128.99(6) . . ?
Ag13 Ag1 Ag5 62.03(5) . . ?
Ag13 Ag1 Ag8 116.57(6) . 2_565 ?
Ag13 Ag1 Ag10 116.35(7) . 2_565 ?
Ag13 Ag1 Ag10 64.20(6) . . ?
Ag13 Ag1 Ag12 56.68(6) . . ?
Ag13 Ag1 Ag20 118.63(6) . . ?
Ag13 Ag1 Ag25 172.98(6) . 2_565 ?
Ag20 Ag1 Ag1 128.98(5) . 2_565 ?
Ag20 Ag1 Ag01 117.12(5) . . ?
Ag20 Ag1 Ag2 98.23(5) . 2_565 ?
Ag20 Ag1 Ag2 69.13(5) . . ?
Ag20 Ag1 Ag5 68.96(5) . . ?
Ag20 Ag1 Ag8 62.30(5) . 2_565 ?
Ag20 Ag1 Ag10 172.81(6) . . ?
Ag20 Ag1 Ag12 66.59(5) . . ?
Ag20 Ag1 Ag25 56.46(5) . 2_565 ?
Ag25 Ag1 Ag10 120.03(6) 2_565 . ?
Ag1 Ag01 Ag5 59.20(4) . . ?
Ag1 Ag01 Ag8 58.72(4) . 2_565 ?
Ag1 Ag01 Ag10 57.29(4) . 2_565 ?
Ag1 Ag01 Ag13 54.31(4) . . ?
Ag1 Ag01 Ag15 123.72(5) . . ?
Ag1 Ag01 Ag18 101.47(5) . 2_565 ?
Ag1 Ag01 Ag19 107.51(6) . . ?
Ag5 Ag01 Ag13 56.79(5) . . ?
Ag5 Ag01 Ag15 159.11(6) . . ?
Ag5 Ag01 Ag18 114.56(5) . 2_565 ?
Ag8 Ag01 Ag5 60.09(4) 2_565 . ?
Ag8 Ag01 Ag13 103.51(6) 2_565 . ?
Ag8 Ag01 Ag15 140.63(6) 2_565 . ?
Ag8 Ag01 Ag18 57.67(4) 2_565 2_565 ?
Ag8 Ag01 Ag19 121.00(6) 2_565 . ?
Ag10 Ag01 Ag1 66.04(4) . . ?
Ag10 Ag01 Ag5 111.00(6) 2_565 . ?
Ag10 Ag01 Ag5 114.16(6) . . ?
Ag10 Ag01 Ag8 66.05(5) 2_565 2_565 ?
Ag10 Ag01 Ag8 116.21(6) . 2_565 ?
Ag10 Ag01 Ag10 58.42(6) . 2_565 ?
Ag10 Ag01 Ag13 62.80(5) . . ?
Ag10 Ag01 Ag13 101.77(5) 2_565 . ?
Ag10 Ag01 Ag15 59.12(5) . . ?
Ag10 Ag01 Ag15 83.06(5) 2_565 . ?
Ag10 Ag01 Ag18 109.38(6) . 2_565 ?
Ag10 Ag01 Ag18 58.13(5) 2_565 2_565 ?
Ag10 Ag01 Ag19 159.01(6) 2_565 . ?
Ag10 Ag01 Ag19 103.40(6) . . ?
Ag15 Ag01 Ag13 106.34(6) . . ?
Ag15 Ag01 Ag18 85.82(5) . 2_565 ?
Ag18 Ag01 Ag13 155.77(6) 2_565 . ?
Ag19 Ag01 Ag5 64.59(5) . . ?
Ag19 Ag01 Ag13 58.04(5) . . ?
Ag19 Ag01 Ag15 96.64(6) . . ?
Ag19 Ag01 Ag18 142.86(6) . 2_565 ?
Cl8 Ag01 Ag1 106.52(11) . . ?
Cl8 Ag01 Ag5 58.40(11) . . ?
Cl8 Ag01 Ag8 58.94(11) . 2_565 ?
Cl8 Ag01 Ag10 120.38(12) . 2_565 ?
Cl8 Ag01 Ag10 172.19(12) . . ?
Cl8 Ag01 Ag13 111.31(11) . . ?
Cl8 Ag01 Ag15 128.65(12) . . ?
Cl8 Ag01 Ag18 73.78(11) . 2_565 ?
Cl8 Ag01 Ag19 76.05(11) . . ?
S10 Ag01 Ag1 149.34(12) . . ?
S10 Ag01 Ag5 114.76(11) . . ?
S10 Ag01 Ag8 148.50(12) . 2_565 ?
S10 Ag01 Ag10 133.47(11) . 2_565 ?
S10 Ag01 Ag10 94.57(11) . . ?
S10 Ag01 Ag13 96.21(12) . . ?
S10 Ag01 Ag15 50.62(10) . . ?
S10 Ag01 Ag18 107.53(12) . 2_565 ?
S10 Ag01 Ag19 51.91(11) . . ?
S10 Ag01 Cl8 91.15(15) . . ?
Ag1A Ag1A Ag1D 84.09(6) 2_565 . ?
Ag1A Ag1A Ag2 55.36(5) 2_565 2_565 ?
Ag1A Ag1A Ag7 111.24(8) 2_565 . ?
Ag1A Ag1A Ag11 119.68(8) 2_565 . ?
Ag1A Ag1A Ag12 103.84(6) 2_565 . ?
Ag1A Ag1A Ag17 61.42(6) 2_565 . ?
Ag1A Ag1A Ag17 61.26(6) 2_565 2_565 ?
Ag1A Ag1A Ag20 128.44(4) 2_565 . ?
Ag1D Ag1A Ag2 116.60(7) . 2_565 ?
Ag1D Ag1A Ag7 129.58(7) . . ?
Ag1D Ag1A Ag11 74.67(6) . . ?
Ag1D Ag1A Ag12 110.54(6) . . ?
Ag1D Ag1A Ag17 97.44(7) . . ?
Ag1D Ag1A Ag17 62.62(6) . 2_565 ?
Ag1D Ag1A Ag20 146.45(8) . . ?
Ag2 Ag1A Ag1A 68.63(5) . 2_565 ?
Ag2 Ag1A Ag1D 150.33(9) . . ?
Ag2 Ag1A Ag2 56.86(5) . 2_565 ?
Ag2 Ag1A Ag7 56.35(4) . . ?
Ag2 Ag1A Ag7 111.00(6) 2_565 . ?
Ag2 Ag1A Ag11 108.29(6) . . ?
Ag2 Ag1A Ag12 87.93(6) . . ?
Ag2 Ag1A Ag12 51.56(4) 2_565 . ?
Ag2 Ag1A Ag17 59.79(5) . . ?
Ag2 Ag1A Ag17 110.46(6) . 2_565 ?
Ag2 Ag1A Ag20 83.13(5) 2_565 . ?
Ag2 Ag1A Ag20 62.95(5) . . ?
Ag7 Ag1A Ag12 111.40(7) . . ?
Ag7 Ag1A Ag20 52.80(4) . . ?
Ag11 Ag1A Ag2 164.95(7) . 2_565 ?
Ag11 Ag1A Ag7 55.73(5) . . ?
Ag11 Ag1A Ag12 136.45(7) . . ?
Ag11 Ag1A Ag20 92.10(6) . . ?
Ag17 Ag1A Ag2 55.71(4) 2_565 2_565 ?
Ag17 Ag1A Ag2 101.09(6) . 2_565 ?
Ag17 Ag1A Ag7 166.62(7) 2_565 . ?
Ag17 Ag1A Ag7 56.91(4) . . ?
Ag17 Ag1A Ag11 66.33(5) . . ?
Ag17 Ag1A Ag11 137.15(7) 2_565 . ?
Ag17 Ag1A Ag12 62.83(5) 2_565 . ?
Ag17 Ag1A Ag12 147.25(7) . . ?
Ag17 Ag1A Ag17 120.61(7) . 2_565 ?
Ag17 Ag1A Ag20 121.54(7) 2_565 . ?
Ag17 Ag1A Ag20 105.30(6) . . ?
Ag20 Ag1A Ag12 59.03(5) . . ?
S2A Ag1A Ag1A 153.3(2) . 2_565 ?
S2A Ag1A Ag1D 97.64(17) . . ?
S2A Ag1A Ag2 111.96(18) . . ?
S2A Ag1A Ag2 101.39(19) . 2_565 ?
S2A Ag1A Ag7 88.3(2) . . ?
S2A Ag1A Ag11 86.1(2) . . ?
S2A Ag1A Ag12 50.49(19) . . ?
S2A Ag1A Ag17 95.8(2) . 2_565 ?
S2A Ag1A Ag17 143.6(2) . . ?
S2A Ag1A Ag20 50.05(17) . . ?
Ag1E Ag1B Ag7 89.53(7) . . ?
Ag20 Ag1B Ag1E 79.86(7) . . ?
Ag20 Ag1B Ag7 57.76(5) . . ?
S16 Ag1B Ag1E 67.37(14) . . ?
S16 Ag1B Ag7 148.56(15) . . ?
S16 Ag1B Ag20 95.90(13) . . ?
S20 Ag1B Ag1E 136.78(15) . . ?
S20 Ag1B Ag7 55.54(13) . . ?
S20 Ag1B Ag20 97.83(13) . . ?
S20 Ag1B S16 154.1(2) . . ?
Ag1A Ag1D Ag1D 81.56(6) . 2_565 ?
Ag1A Ag1D Ag17 59.57(6) . 2_565 ?
Ag1D Ag1D Ag17 93.81(7) 2_565 2_565 ?
S18 Ag1D Ag1A 98.44(14) . . ?
S18 Ag1D Ag1D 141.62(16) . 2_565 ?
S18 Ag1D Ag17 55.76(13) . 2_565 ?
S19 Ag1D Ag1A 93.06(14) . . ?
S19 Ag1D Ag1D 67.17(13) . 2_565 ?
S19 Ag1D Ag17 149.55(15) . 2_565 ?
S19 Ag1D S18 150.21(19) . . ?
Ag8 Ag1E Ag1B 93.40(8) 2_565 . ?
Ag25 Ag1E Ag1B 82.74(8) 2_565 . ?
Ag25 Ag1E Ag8 58.56(5) 2_565 2_565 ?
S6 Ag1E Ag1B 141.60(16) . . ?
S6 Ag1E Ag8 57.01(13) . 2_565 ?
S6 Ag1E Ag25 98.34(13) . 2_565 ?
S25 Ag1E Ag1B 66.86(16) . . ?
S25 Ag1E Ag8 149.30(16) . 2_565 ?
S25 Ag1E Ag25 94.41(13) . 2_565 ?
S25 Ag1E S6 150.0(2) . . ?
Ag1 Ag2 Ag1 60.49(5) . 2_565 ?
Ag1 Ag2 Ag1A 115.22(5) . 2_565 ?
Ag1 Ag2 Ag1A 89.38(5) 2_565 2_565 ?
Ag1 Ag2 Ag7 158.28(6) 2_565 . ?
Ag1 Ag2 Ag7 109.23(5) . . ?
Ag1 Ag2 Ag13 88.55(5) . 2_565 ?
Ag1 Ag2 Ag13 54.34(4) 2_565 2_565 ?
Ag1 Ag2 Ag17 159.61(6) . . ?
Ag1 Ag2 Ag20 115.19(5) 2_565 . ?
Ag1 Ag2 Ag20 54.79(4) . . ?
Ag1A Ag2 Ag1 127.82(6) . 2_565 ?
Ag1A Ag2 Ag1 97.44(6) . . ?
Ag1A Ag2 Ag1A 56.01(8) . 2_565 ?
Ag1A Ag2 Ag2 68.08(5) . 2_565 ?
Ag1A Ag2 Ag02 118.14(6) . . ?
Ag1A Ag2 Ag7 70.17(5) . . ?
Ag1A Ag2 Ag12 119.22(7) . 2_565 ?
Ag1A Ag2 Ag13 173.85(7) . 2_565 ?
Ag1A Ag2 Ag13 120.00(6) 2_565 2_565 ?
Ag1A Ag2 Ag17 62.53(6) . . ?
Ag1A Ag2 Ag20 119.78(6) 2_565 . ?
Ag1A Ag2 Ag20 66.34(5) . . ?
Ag1A Ag2 Ag25 117.65(6) . 2_565 ?
Ag2 Ag2 Ag1 60.28(4) 2_565 . ?
Ag2 Ag2 Ag1 59.88(4) 2_565 2_565 ?
Ag2 Ag2 Ag1A 55.05(4) 2_565 2_565 ?
Ag2 Ag2 Ag7 134.53(6) 2_565 . ?
Ag2 Ag2 Ag13 114.18(5) 2_565 2_565 ?
Ag2 Ag2 Ag17 111.07(4) 2_565 . ?
Ag2 Ag2 Ag20 89.83(6) 2_565 . ?
Ag02 Ag2 Ag1 132.94(6) . . ?
Ag02 Ag2 Ag1 109.60(5) . 2_565 ?
Ag02 Ag2 Ag1A 110.21(5) . 2_565 ?
Ag02 Ag2 Ag2 159.29(7) . 2_565 ?
Ag02 Ag2 Ag7 61.79(4) . . ?
Ag02 Ag2 Ag13 57.63(5) . 2_565 ?
Ag02 Ag2 Ag17 61.73(5) . . ?
Ag02 Ag2 Ag20 110.84(5) . . ?
Ag7 Ag2 Ag1A 112.21(6) . 2_565 ?
Ag7 Ag2 Ag13 109.25(5) . 2_565 ?
Ag7 Ag2 Ag20 56.92(4) . . ?
Ag12 Ag2 Ag1 126.87(6) 2_565 . ?
Ag12 Ag2 Ag1 66.61(5) 2_565 2_565 ?
Ag12 Ag2 Ag1A 67.34(6) 2_565 2_565 ?
Ag12 Ag2 Ag2 97.45(7) 2_565 2_565 ?
Ag12 Ag2 Ag02 61.99(5) 2_565 . ?
Ag12 Ag2 Ag7 118.38(6) 2_565 . ?
Ag12 Ag2 Ag13 55.32(5) 2_565 2_565 ?
Ag12 Ag2 Ag17 70.60(5) 2_565 . ?
Ag12 Ag2 Ag20 172.12(7) 2_565 . ?
Ag17 Ag2 Ag1 133.87(6) . 2_565 ?
Ag17 Ag2 Ag1A 58.16(5) . 2_565 ?
Ag17 Ag2 Ag7 62.20(4) . . ?
Ag17 Ag2 Ag13 111.59(6) . 2_565 ?
Ag17 Ag2 Ag20 109.58(5) . . ?
Ag20 Ag2 Ag13 118.79(6) . 2_565 ?
Ag25 Ag2 Ag1 97.50(5) 2_565 2_565 ?
Ag25 Ag2 Ag1 67.29(5) 2_565 . ?
Ag25 Ag2 Ag1A 172.91(7) 2_565 2_565 ?
Ag25 Ag2 Ag2 127.45(5) 2_565 2_565 ?
Ag25 Ag2 Ag02 69.15(5) 2_565 . ?
Ag25 Ag2 Ag7 61.01(5) 2_565 . ?
Ag25 Ag2 Ag12 117.04(7) 2_565 2_565 ?
Ag25 Ag2 Ag13 66.01(5) 2_565 2_565 ?
Ag25 Ag2 Ag17 117.03(6) 2_565 . ?
Ag25 Ag2 Ag20 55.52(5) 2_565 . ?
Ag2 Ag02 Ag7 60.12(4) . . ?
Ag2 Ag02 Ag12 58.93(5) . 2_565 ?
Ag2 Ag02 Ag13 67.73(5) . 2_565 ?
Ag2 Ag02 Ag16 123.04(6) . . ?
Ag2 Ag02 Ag17 59.53(4) . . ?
Ag2 Ag02 Ag21 110.29(5) . . ?
Ag2 Ag02 Ag25 55.06(4) . 2_565 ?
Ag2 Ag02 Ag29 101.00(5) . 2_565 ?
Ag7 Ag02 Ag16 162.82(7) . . ?
Ag7 Ag02 Ag21 66.68(5) . . ?
Ag7 Ag02 Ag25 56.06(4) . 2_565 ?
Ag7 Ag02 Ag29 115.25(6) . 2_565 ?
Ag12 Ag02 Ag7 114.12(6) 2_565 . ?
Ag12 Ag02 Ag13 57.78(5) 2_565 2_565 ?
Ag12 Ag02 Ag16 77.52(6) 2_565 . ?
Ag12 Ag02 Ag17 68.54(5) 2_565 . ?
Ag12 Ag02 Ag21 159.57(7) 2_565 . ?
Ag12 Ag02 Ag25 103.51(5) 2_565 2_565 ?
Ag12 Ag02 Ag29 57.42(5) 2_565 2_565 ?
Ag13 Ag02 Ag7 116.07(6) 2_565 . ?
Ag13 Ag02 Ag16 58.09(5) 2_565 . ?
Ag13 Ag02 Ag21 102.73(6) 2_565 . ?
Ag13 Ag02 Ag25 64.88(5) 2_565 2_565 ?
Ag13 Ag02 Ag29 108.40(6) 2_565 2_565 ?
Ag16 Ag02 Ag25 110.20(6) . 2_565 ?
Ag16 Ag02 Ag29 81.47(5) . 2_565 ?
Ag17 Ag02 Ag7 60.91(5) . . ?
Ag17 Ag02 Ag13 118.31(6) . 2_565 ?
Ag17 Ag02 Ag16 136.20(6) . . ?
Ag17 Ag02 Ag21 123.25(6) . . ?
Ag17 Ag02 Ag25 104.15(5) . 2_565 ?
Ag17 Ag02 Ag29 57.28(4) . 2_565 ?
Ag21 Ag02 Ag16 97.89(6) . . ?
Ag21 Ag02 Ag25 58.97(4) . 2_565 ?
Ag21 Ag02 Ag29 142.27(6) . 2_565 ?
Ag25 Ag02 Ag29 156.06(6) 2_565 2_565 ?
S3 Ag02 Ag2 154.18(12) . . ?
S3 Ag02 Ag7 115.68(11) . . ?
S3 Ag02 Ag12 130.04(12) . 2_565 ?
S3 Ag02 Ag13 95.93(12) . 2_565 ?
S3 Ag02 Ag16 53.08(11) . . ?
S3 Ag02 Ag17 143.91(12) . . ?
S3 Ag02 Ag21 52.01(10) . . ?
S3 Ag02 Ag25 100.41(11) . 2_565 ?
S3 Ag02 Ag29 103.20(11) . 2_565 ?
Ag1 Ag5 Ag01 59.06(4) . . ?
Ag1 Ag5 Ag05 106.66(5) . . ?
Ag1 Ag5 Ag8 58.38(4) . 2_565 ?
Ag1 Ag5 Ag13 57.00(4) . . ?
Ag1 Ag5 Ag19 101.94(5) . . ?
Ag1 Ag5 Ag20 54.03(4) . . ?
Ag1 Ag5 Ag32 124.13(6) . . ?
Ag01 Ag5 Ag19 57.32(4) . . ?
Ag01 Ag5 Ag20 103.10(5) . . ?
Ag01 Ag5 Ag32 142.32(6) . . ?
Ag05 Ag5 Ag01 119.33(6) . . ?
Ag05 Ag5 Ag19 141.72(6) . . ?
Ag05 Ag5 Ag20 57.69(4) . . ?
Ag05 Ag5 Ag32 96.52(5) . . ?
Ag8 Ag5 Ag01 59.21(4) 2_565 . ?
Ag8 Ag5 Ag05 64.12(5) 2_565 . ?
Ag8 Ag5 Ag19 113.39(6) 2_565 . ?
Ag8 Ag5 Ag20 56.27(4) 2_565 . ?
Ag8 Ag5 Ag32 158.30(6) 2_565 . ?
Ag12 Ag5 Ag1 65.32(4) . . ?
Ag12 Ag5 Ag01 115.23(5) . . ?
Ag12 Ag5 Ag05 105.76(6) . . ?
Ag12 Ag5 Ag8 114.05(6) . 2_565 ?
Ag12 Ag5 Ag13 58.05(5) . . ?
Ag12 Ag5 Ag19 109.07(6) . . ?
Ag12 Ag5 Ag20 64.25(5) . . ?
Ag12 Ag5 Ag32 59.60(5) . . ?
Ag13 Ag5 Ag01 65.07(5) . . ?
Ag13 Ag5 Ag05 159.74(7) . . ?
Ag13 Ag5 Ag8 109.17(6) . 2_565 ?
Ag13 Ag5 Ag19 58.34(5) . . ?
Ag13 Ag5 Ag20 102.31(5) . . ?
Ag13 Ag5 Ag32 85.53(6) . . ?
Ag19 Ag5 Ag20 155.96(5) . . ?
Ag32 Ag5 Ag19 87.78(5) . . ?
Ag32 Ag5 Ag20 105.94(6) . . ?
S1 Ag5 Ag1 149.72(12) . . ?
S1 Ag5 Ag01 146.88(12) . . ?
S1 Ag5 Ag05 52.20(11) . . ?
S1 Ag5 Ag8 114.49(11) . 2_565 ?
S1 Ag5 Ag12 97.22(11) . . ?
S1 Ag5 Ag13 135.89(12) . . ?
S1 Ag5 Ag19 107.31(11) . . ?
S1 Ag5 Ag20 96.59(11) . . ?
S1 Ag5 Ag32 50.84(11) . . ?
S1 Ag5 Cl8 90.77(14) . . ?
Cl8 Ag5 Ag1 105.65(10) . . ?
Cl8 Ag5 Ag01 57.46(9) . . ?
Cl8 Ag5 Ag05 75.91(11) . . ?
Cl8 Ag5 Ag8 58.32(11) . 2_565 ?
Cl8 Ag5 Ag12 170.97(10) . . ?
Cl8 Ag5 Ag13 118.10(11) . . ?
Cl8 Ag5 Ag19 72.22(11) . . ?
Cl8 Ag5 Ag20 110.77(12) . . ?
Cl8 Ag5 Ag32 129.34(10) . . ?
Ag5 Ag05 Ag8 57.85(4) . 2_565 ?
Ag5 Ag05 Ag20 65.61(5) . . ?
Ag20 Ag05 Ag8 56.88(4) . 2_565 ?
S1 Ag05 Ag5 57.01(10) . . ?
S1 Ag05 Ag8 113.04(11) . 2_565 ?
S1 Ag05 Ag20 106.34(11) . . ?
S16 Ag05 Ag5 151.97(15) . . ?
S16 Ag05 Ag8 94.56(14) . 2_565 ?
S16 Ag05 Ag20 96.35(13) . . ?
S16 Ag05 S1 150.84(17) . . ?
Ag1B Ag7 Ag1A 108.43(6) . . ?
Ag1B Ag7 Ag21 86.41(5) . . ?
Ag2 Ag7 Ag1A 53.48(4) . . ?
Ag2 Ag7 Ag1B 124.48(6) . . ?
Ag2 Ag7 Ag02 58.09(4) . . ?
Ag2 Ag7 Ag11 107.62(6) . . ?
Ag2 Ag7 Ag17 58.29(4) . . ?
Ag2 Ag7 Ag20 67.08(5) . . ?
Ag2 Ag7 Ag21 101.39(5) . . ?
Ag2 Ag7 Ag25 58.04(5) . 2_565 ?
Ag02 Ag7 Ag1A 101.87(5) . . ?
Ag02 Ag7 Ag1B 140.22(7) . . ?
Ag02 Ag7 Ag11 122.70(6) . . ?
Ag02 Ag7 Ag17 59.18(5) . . ?
Ag02 Ag7 Ag21 56.92(4) . . ?
Ag11 Ag7 Ag1A 57.88(5) . . ?
Ag11 Ag7 Ag1B 95.48(6) . . ?
Ag11 Ag7 Ag17 66.80(5) . . ?
Ag11 Ag7 Ag21 142.95(6) . . ?
Ag17 Ag7 Ag1A 55.81(5) . . ?
Ag17 Ag7 Ag1B 160.44(7) . . ?
Ag17 Ag7 Ag21 112.62(5) . . ?
Ag20 Ag7 Ag1A 64.23(5) . . ?
Ag20 Ag7 Ag1B 58.95(5) . . ?
Ag20 Ag7 Ag02 116.37(6) . . ?
Ag20 Ag7 Ag11 101.87(6) . . ?
Ag20 Ag7 Ag17 114.75(6) . . ?
Ag20 Ag7 Ag21 110.49(6) . . ?
Ag21 Ag7 Ag1A 154.82(6) . . ?
Ag25 Ag7 Ag1A 101.87(6) 2_565 . ?
Ag25 Ag7 Ag1B 82.25(6) 2_565 . ?
Ag25 Ag7 Ag02 66.53(5) 2_565 . ?
Ag25 Ag7 Ag11 157.94(7) 2_565 . ?
Ag25 Ag7 Ag17 110.88(6) 2_565 . ?
Ag25 Ag7 Ag20 58.15(5) 2_565 . ?
Ag25 Ag7 Ag21 59.03(5) 2_565 . ?
Cl4 Ag7 Ag1A 106.87(18) . . ?
Cl4 Ag7 Ag1B 128.25(18) . . ?
Cl4 Ag7 Ag2 106.84(17) . . ?
Cl4 Ag7 Ag02 62.53(17) . . ?
Cl4 Ag7 Ag11 73.12(18) . . ?
Cl4 Ag7 Ag17 56.53(17) . . ?
Cl4 Ag7 Ag20 170.97(18) . . ?
Cl4 Ag7 Ag21 76.81(18) . . ?
Cl4 Ag7 Ag25 125.20(18) . 2_565 ?
S20 Ag7 Ag1A 98.86(12) . . ?
S20 Ag7 Ag1B 50.36(12) . . ?
S20 Ag7 Ag2 151.09(13) . . ?
S20 Ag7 Ag02 147.70(13) . . ?
S20 Ag7 Ag11 52.13(12) . . ?
S20 Ag7 Ag17 116.37(13) . . ?
S20 Ag7 Ag20 94.90(12) . . ?
S20 Ag7 Ag21 106.21(12) . . ?
S20 Ag7 Ag25 132.26(13) . 2_565 ?
S20 Ag7 Cl4 87.9(2) . . ?
Ag1 Ag8 Ag01 60.06(4) 2_565 2_565 ?
Ag1 Ag8 Ag1E 122.98(6) 2_565 2_565 ?
Ag1 Ag8 Ag5 59.84(4) 2_565 2_565 ?
Ag1 Ag8 Ag05 103.15(5) 2_565 2_565 ?
Ag1 Ag8 Ag10 54.62(4) 2_565 . ?
Ag1 Ag8 Ag18 107.56(5) 2_565 . ?
Ag1 Ag8 Ag20 57.88(4) 2_565 2_565 ?
Ag1 Ag8 Ag25 66.06(5) 2_565 . ?
Ag01 Ag8 Ag1E 160.55(7) 2_565 2_565 ?
Ag01 Ag8 Ag5 60.70(4) 2_565 2_565 ?
Ag01 Ag8 Ag05 115.05(5) 2_565 2_565 ?
Ag01 Ag8 Ag10 56.89(5) 2_565 . ?
Ag1E Ag8 Ag05 83.73(6) 2_565 2_565 ?
Ag1E Ag8 Ag10 107.50(6) 2_565 . ?
Ag5 Ag8 Ag1E 138.65(7) 2_565 2_565 ?
Ag5 Ag8 Ag05 58.03(4) 2_565 2_565 ?
Ag5 Ag8 Ag10 104.46(5) 2_565 . ?
Ag05 Ag8 Ag10 157.77(6) 2_565 . ?
Ag18 Ag8 Ag01 64.53(5) . 2_565 ?
Ag18 Ag8 Ag1E 97.84(7) . 2_565 ?
Ag18 Ag8 Ag5 121.53(6) . 2_565 ?
Ag18 Ag8 Ag05 141.75(6) . 2_565 ?
Ag18 Ag8 Ag10 57.36(4) . . ?
Ag18 Ag8 Ag20 159.17(6) . 2_565 ?
Ag20 Ag8 Ag01 112.17(6) 2_565 2_565 ?
Ag20 Ag8 Ag1E 81.17(6) 2_565 2_565 ?
Ag20 Ag8 Ag5 66.56(5) 2_565 2_565 ?
Ag20 Ag8 Ag05 59.03(4) 2_565 2_565 ?
Ag20 Ag8 Ag10 102.87(5) 2_565 . ?
Ag25 Ag8 Ag01 115.30(6) . 2_565 ?
Ag25 Ag8 Ag1E 58.63(5) . 2_565 ?
Ag25 Ag8 Ag5 116.76(6) . 2_565 ?
Ag25 Ag8 Ag05 109.51(6) . 2_565 ?
Ag25 Ag8 Ag10 63.92(5) . . ?
Ag25 Ag8 Ag18 103.52(6) . . ?
Ag25 Ag8 Ag20 58.08(5) . 2_565 ?
S6 Ag8 Ag1 149.39(13) 2_565 2_565 ?
S6 Ag8 Ag01 115.10(13) 2_565 2_565 ?
S6 Ag8 Ag1E 51.13(13) 2_565 2_565 ?
S6 Ag8 Ag5 147.99(12) 2_565 2_565 ?
S6 Ag8 Ag05 105.52(13) 2_565 2_565 ?
S6 Ag8 Ag10 96.30(12) 2_565 . ?
S6 Ag8 Ag18 52.47(12) 2_565 . ?
S6 Ag8 Ag20 132.10(13) 2_565 2_565 ?
S6 Ag8 Ag25 94.12(12) 2_565 . ?
S6 Ag8 Cl8 91.67(16) 2_565 2_565 ?
Cl8 Ag8 Ag1 106.84(11) 2_565 2_565 ?
Cl8 Ag8 Ag01 57.99(10) 2_565 2_565 ?
Cl8 Ag8 Ag1E 128.66(11) 2_565 2_565 ?
Cl8 Ag8 Ag5 58.33(11) 2_565 2_565 ?
Cl8 Ag8 Ag05 73.05(10) 2_565 2_565 ?
Cl8 Ag8 Ag10 111.05(11) 2_565 . ?
Cl8 Ag8 Ag18 76.61(11) 2_565 . ?
Cl8 Ag8 Ag20 120.27(11) 2_565 2_565 ?
Cl8 Ag8 Ag25 172.71(11) 2_565 . ?
Ag1 Ag10 Ag1 57.32(5) 2_565 . ?
Ag1 Ag10 Ag01 111.84(6) 2_565 . ?
Ag1 Ag10 Ag01 60.86(5) 2_565 2_565 ?
Ag1 Ag10 Ag8 112.08(5) . . ?
Ag1 Ag10 Ag8 56.58(4) 2_565 . ?
Ag1 Ag10 Ag10 68.17(5) 2_565 2_565 ?
Ag1 Ag10 Ag13 90.09(6) 2_565 . ?
Ag1 Ag10 Ag13 52.19(4) . . ?
Ag1 Ag10 Ag15 151.54(8) 2_565 . ?
Ag1 Ag10 Ag18 108.84(5) 2_565 . ?
Ag1 Ag10 Ag25 83.55(5) . . ?
Ag1 Ag10 Ag25 62.13(5) 2_565 . ?
Ag01 Ag10 Ag1 57.04(4) . . ?
Ag01 Ag10 Ag1 101.43(6) 2_565 . ?
Ag01 Ag10 Ag01 118.40(7) . 2_565 ?
Ag01 Ag10 Ag8 57.06(4) 2_565 . ?
Ag01 Ag10 Ag8 168.40(6) . . ?
Ag01 Ag10 Ag13 149.96(6) 2_565 . ?
Ag01 Ag10 Ag13 62.97(5) . . ?
Ag01 Ag10 Ag15 95.71(6) 2_565 . ?
Ag01 Ag10 Ag15 63.06(5) . . ?
Ag01 Ag10 Ag18 64.37(5) 2_565 . ?
Ag01 Ag10 Ag18 132.92(7) . . ?
Ag01 Ag10 Ag25 124.35(6) . . ?
Ag01 Ag10 Ag25 105.77(5) 2_565 . ?
Ag8 Ag10 Ag25 53.27(4) . . ?
Ag10 Ag10 Ag1 55.19(4) 2_565 . ?
Ag10 Ag10 Ag01 61.35(5) 2_565 . ?
Ag10 Ag10 Ag01 60.23(6) 2_565 2_565 ?
Ag10 Ag10 Ag8 110.01(7) 2_565 . ?
Ag10 Ag10 Ag13 103.85(6) 2_565 . ?
Ag10 Ag10 Ag15 86.62(5) 2_565 . ?
Ag10 Ag10 Ag18 116.32(7) 2_565 . ?
Ag10 Ag10 Ag25 127.53(4) 2_565 . ?
Ag13 Ag10 Ag8 114.87(6) . . ?
Ag13 Ag10 Ag25 61.84(5) . . ?
Ag15 Ag10 Ag1 118.80(6) . . ?
Ag15 Ag10 Ag8 126.25(6) . . ?
Ag15 Ag10 Ag13 109.31(6) . . ?
Ag15 Ag10 Ag18 69.87(5) . . ?
Ag15 Ag10 Ag25 145.41(7) . . ?
Ag18 Ag10 Ag1 164.92(6) . . ?
Ag18 Ag10 Ag8 56.79(4) . . ?
Ag18 Ag10 Ag13 139.49(7) . . ?
Ag18 Ag10 Ag25 95.17(6) . . ?
S1A Ag10 Ag1 102.65(17) . . ?
S1A Ag10 Ag1 113.13(16) . 2_565 ?
S1A Ag10 Ag01 144.32(17) . 2_565 ?
S1A Ag10 Ag01 96.81(17) . . ?
S1A Ag10 Ag8 89.43(16) . . ?
S1A Ag10 Ag10 154.36(18) . 2_565 ?
S1A Ag10 Ag13 51.41(17) . . ?
S1A Ag10 Ag15 95.32(15) . . ?
S1A Ag10 Ag18 88.08(17) . . ?
S1A Ag10 Ag25 51.97(15) . . ?
Ag1A Ag11 Ag17 55.52(5) . . ?
Ag7 Ag11 Ag1A 66.39(5) . . ?
Ag7 Ag11 Ag17 56.91(4) . . ?
S19 Ag11 Ag1A 91.09(14) . . ?
S19 Ag11 Ag7 144.92(14) . . ?
S19 Ag11 Ag17 88.35(13) . . ?
S19 Ag11 S20 156.34(19) . . ?
S20 Ag11 Ag1A 109.99(13) . . ?
S20 Ag11 Ag7 57.65(13) . . ?
S20 Ag11 Ag17 112.15(14) . . ?
Ag1 Ag12 Ag1A 82.08(5) . . ?
Ag1 Ag12 Ag17 110.36(5) . 2_565 ?
Ag1 Ag12 Ag20 52.06(4) . . ?
Ag2 Ag12 Ag1 57.27(4) 2_565 . ?
Ag2 Ag12 Ag1A 61.10(5) 2_565 . ?
Ag2 Ag12 Ag02 59.08(4) 2_565 2_565 ?
Ag2 Ag12 Ag5 112.92(6) 2_565 . ?
Ag2 Ag12 Ag17 55.09(4) 2_565 2_565 ?
Ag2 Ag12 Ag20 89.15(5) 2_565 . ?
Ag2 Ag12 Ag29 108.05(6) 2_565 . ?
Ag2 Ag12 Ag32 155.98(8) 2_565 . ?
Ag02 Ag12 Ag1 100.78(5) 2_565 . ?
Ag02 Ag12 Ag1A 103.71(6) 2_565 . ?
Ag02 Ag12 Ag17 55.78(4) 2_565 2_565 ?
Ag02 Ag12 Ag20 147.71(6) 2_565 . ?
Ag02 Ag12 Ag29 66.82(5) 2_565 . ?
Ag02 Ag12 Ag32 101.38(7) 2_565 . ?
Ag5 Ag12 Ag1 57.83(4) . . ?
Ag5 Ag12 Ag1A 122.91(7) . . ?
Ag5 Ag12 Ag02 121.11(8) . 2_565 ?
Ag5 Ag12 Ag17 167.97(6) . 2_565 ?
Ag5 Ag12 Ag20 63.23(5) . . ?
Ag5 Ag12 Ag29 135.00(7) . . ?
Ag5 Ag12 Ag32 62.99(5) . . ?
Ag13 Ag12 Ag1 55.71(5) . . ?
Ag13 Ag12 Ag1A 127.26(6) . . ?
Ag13 Ag12 Ag2 69.30(5) . 2_565 ?
Ag13 Ag12 Ag02 61.45(5) . 2_565 ?
Ag13 Ag12 Ag5 62.06(5) . . ?
Ag13 Ag12 Ag17 110.41(6) . 2_565 ?
Ag13 Ag12 Ag20 104.25(6) . . ?
Ag13 Ag12 Ag29 119.65(7) . . ?
Ag13 Ag12 Ag32 89.51(7) . . ?
Ag17 Ag12 Ag1A 52.69(5) 2_565 . ?
Ag20 Ag12 Ag1A 60.08(5) . . ?
Ag20 Ag12 Ag17 112.51(6) . 2_565 ?
Ag29 Ag12 Ag1 165.14(6) . . ?
Ag29 Ag12 Ag1A 92.70(6) . . ?
Ag29 Ag12 Ag17 56.34(5) . 2_565 ?
Ag29 Ag12 Ag20 136.00(7) . . ?
Ag32 Ag12 Ag1 120.09(7) . . ?
Ag32 Ag12 Ag1A 142.31(7) . . ?
Ag32 Ag12 Ag17 128.10(6) . 2_565 ?
Ag32 Ag12 Ag20 107.56(5) . . ?
Ag32 Ag12 Ag29 72.01(5) . . ?
S2A Ag12 Ag1 101.41(17) . . ?
S2A Ag12 Ag1A 50.17(18) . . ?
S2A Ag12 Ag2 110.50(19) . 2_565 ?
S2A Ag12 Ag02 142.1(2) . 2_565 ?
S2A Ag12 Ag5 96.73(19) . . ?
S2A Ag12 Ag13 154.17(18) . . ?
S2A Ag12 Ag17 87.7(2) . 2_565 ?
S2A Ag12 Ag20 50.50(17) . . ?
S2A Ag12 Ag29 85.53(17) . . ?
S2A Ag12 Ag32 93.50(18) . . ?
Ag1 Ag13 Ag01 57.73(4) . . ?
Ag1 Ag13 Ag2 56.45(4) . 2_565 ?
Ag1 Ag13 Ag02 108.75(6) . 2_565 ?
Ag1 Ag13 Ag5 60.97(4) . . ?
Ag1 Ag13 Ag10 63.61(5) . . ?
Ag1 Ag13 Ag12 67.62(5) . . ?
Ag1 Ag13 Ag16 146.37(8) . 2_565 ?
Ag1 Ag13 Ag19 109.82(6) . . ?
Ag1 Ag13 Ag25 88.48(5) . . ?
Ag01 Ag13 Ag2 112.04(5) . 2_565 ?
Ag01 Ag13 Ag25 113.71(6) . . ?
Ag2 Ag13 Ag25 51.06(4) 2_565 . ?
Ag02 Ag13 Ag01 166.42(6) 2_565 . ?
Ag02 Ag13 Ag2 54.63(4) 2_565 2_565 ?
Ag02 Ag13 Ag5 118.40(7) 2_565 . ?
Ag02 Ag13 Ag10 120.88(6) 2_565 . ?
Ag02 Ag13 Ag19 135.22(7) 2_565 . ?
Ag02 Ag13 Ag25 61.48(4) 2_565 . ?
Ag5 Ag13 Ag01 58.14(4) . . ?
Ag5 Ag13 Ag2 101.14(6) . 2_565 ?
Ag5 Ag13 Ag10 107.59(6) . . ?
Ag5 Ag13 Ag19 64.77(5) . . ?
Ag5 Ag13 Ag25 148.47(6) . . ?
Ag10 Ag13 Ag01 54.23(5) . . ?
Ag10 Ag13 Ag2 82.84(5) . 2_565 ?
Ag10 Ag13 Ag25 59.85(5) . . ?
Ag12 Ag13 Ag01 110.81(6) . . ?
Ag12 Ag13 Ag2 55.39(5) . 2_565 ?
Ag12 Ag13 Ag02 60.78(5) . 2_565 ?
Ag12 Ag13 Ag5 59.89(5) . . ?
Ag12 Ag13 Ag10 128.10(6) . . ?
Ag12 Ag13 Ag16 80.77(7) . 2_565 ?
Ag12 Ag13 Ag19 116.18(7) . . ?
Ag12 Ag13 Ag25 103.15(6) . . ?
Ag16 Ag13 Ag01 129.65(6) 2_565 . ?
Ag16 Ag13 Ag2 114.10(7) 2_565 2_565 ?
Ag16 Ag13 Ag02 61.79(5) 2_565 2_565 ?
Ag16 Ag13 Ag5 93.78(6) 2_565 . ?
Ag16 Ag13 Ag10 149.95(7) 2_565 . ?
Ag16 Ag13 Ag19 73.50(5) 2_565 . ?
Ag16 Ag13 Ag25 110.38(6) 2_565 . ?
Ag19 Ag13 Ag01 57.17(5) . . ?
Ag19 Ag13 Ag2 165.07(6) . 2_565 ?
Ag19 Ag13 Ag10 96.38(6) . . ?
Ag19 Ag13 Ag25 140.41(7) . . ?
S1A Ag13 Ag1 115.58(18) . . ?
S1A Ag13 Ag01 91.40(18) . . ?
S1A Ag13 Ag2 102.04(15) . 2_565 ?
S1A Ag13 Ag02 94.12(17) . 2_565 ?
S1A Ag13 Ag5 147.08(18) . . ?
S1A Ag13 Ag10 53.16(18) . . ?
S1A Ag13 Ag12 152.52(17) . . ?
S1A Ag13 Ag16 97.71(18) . 2_565 ?
S1A Ag13 Ag19 89.14(15) . . ?
S1A Ag13 Ag25 51.38(15) . . ?
Ag01 Ag15 Ag15 89.43(5) . 2_565 ?
Ag01 Ag15 Ag18 113.03(6) . . ?
Ag10 Ag15 Ag01 57.82(5) . . ?
Ag10 Ag15 Ag15 81.56(5) . 2_565 ?
Ag10 Ag15 Ag18 55.22(4) . . ?
Ag15 Ag15 Ag18 80.61(6) 2_565 . ?
S7 Ag15 Ag01 148.85(13) . . ?
S7 Ag15 Ag10 97.15(12) . . ?
S7 Ag15 Ag15 67.03(12) . 2_565 ?
S7 Ag15 Ag18 45.60(12) . . ?
S7 Ag15 S10 153.72(18) . . ?
S10 Ag15 Ag01 56.28(12) . . ?
S10 Ag15 Ag10 97.72(12) . . ?
S10 Ag15 Ag15 136.77(14) . 2_565 ?
S10 Ag15 Ag18 133.91(13) . . ?
Ag02 Ag16 Ag32 96.88(6) . 2_565 ?
Ag13 Ag16 Ag02 60.12(5) 2_565 . ?
Ag13 Ag16 Ag32 86.09(7) 2_565 2_565 ?
S2 Ag16 Ag02 153.45(13) . . ?
S2 Ag16 Ag13 95.88(12) . 2_565 ?
S2 Ag16 Ag32 68.34(12) . 2_565 ?
S2 Ag16 S3 147.01(17) . . ?
S3 Ag16 Ag02 55.98(11) . . ?
S3 Ag16 Ag13 99.60(12) . 2_565 ?
S3 Ag16 Ag32 141.37(13) . 2_565 ?
Ag1A Ag17 Ag1A 57.31(7) . 2_565 ?
Ag1A Ag17 Ag1D 79.65(6) . 2_565 ?
Ag1A Ag17 Ag1D 57.81(6) 2_565 2_565 ?
Ag1A Ag17 Ag7 67.28(5) . . ?
Ag1A Ag17 Ag7 116.69(6) 2_565 . ?
Ag1A Ag17 Ag11 109.03(6) 2_565 . ?
Ag1A Ag17 Ag11 58.16(5) . . ?
Ag1A Ag17 Ag12 64.48(6) 2_565 2_565 ?
Ag1A Ag17 Ag12 102.37(6) . 2_565 ?
Ag1A Ag17 Ag29 101.39(6) 2_565 2_565 ?
Ag1A Ag17 Ag29 156.79(7) . 2_565 ?
Ag1D Ag17 Ag11 84.94(6) 2_565 . ?
Ag1D Ag17 Ag12 108.23(6) 2_565 2_565 ?
Ag2 Ag17 Ag1A 57.69(5) . . ?
Ag2 Ag17 Ag1A 66.13(5) . 2_565 ?
Ag2 Ag17 Ag1D 122.02(6) . 2_565 ?
Ag2 Ag17 Ag02 58.74(5) . . ?
Ag2 Ag17 Ag7 59.52(4) . . ?
Ag2 Ag17 Ag11 100.71(5) . . ?
Ag2 Ag17 Ag12 54.31(4) . 2_565 ?
Ag2 Ag17 Ag29 107.44(6) . 2_565 ?
Ag02 Ag17 Ag1A 111.15(6) . . ?
Ag02 Ag17 Ag1A 114.34(7) . 2_565 ?
Ag02 Ag17 Ag1D 161.46(7) . 2_565 ?
Ag02 Ag17 Ag7 59.91(4) . . ?
Ag02 Ag17 Ag11 113.48(5) . . ?
Ag02 Ag17 Ag12 55.69(5) . 2_565 ?
Ag02 Ag17 Ag29 66.84(5) . 2_565 ?
Ag7 Ag17 Ag1D 138.16(7) . 2_565 ?
Ag7 Ag17 Ag11 56.29(4) . . ?
Ag7 Ag17 Ag12 103.46(6) . 2_565 ?
Ag11 Ag17 Ag12 155.00(6) . 2_565 ?
Ag29 Ag17 Ag1D 97.15(6) 2_565 2_565 ?
Ag29 Ag17 Ag7 123.28(6) 2_565 . ?
Ag29 Ag17 Ag11 144.89(6) 2_565 . ?
Ag29 Ag17 Ag12 56.48(5) 2_565 2_565 ?
Cl4 Ag17 Ag1A 175.71(18) . 2_565 ?
Cl4 Ag17 Ag1A 119.29(17) . . ?
Cl4 Ag17 Ag1D 125.29(19) . 2_565 ?
Cl4 Ag17 Ag2 110.04(19) . . ?
Cl4 Ag17 Ag02 63.70(19) . . ?
Cl4 Ag17 Ag7 59.04(17) . . ?
Cl4 Ag17 Ag11 69.30(17) . . ?
Cl4 Ag17 Ag12 115.26(19) . 2_565 ?
Cl4 Ag17 Ag29 81.46(17) . 2_565 ?
S18 Ag17 Ag1A 94.07(12) 2_565 2_565 ?
S18 Ag17 Ag1A 131.03(13) 2_565 . ?
S18 Ag17 Ag1D 51.61(12) 2_565 2_565 ?
S18 Ag17 Ag2 150.14(12) 2_565 . ?
S18 Ag17 Ag02 117.06(12) 2_565 . ?
S18 Ag17 Ag7 147.95(13) 2_565 . ?
S18 Ag17 Ag11 107.04(12) 2_565 . ?
S18 Ag17 Ag12 97.65(12) 2_565 2_565 ?
S18 Ag17 Ag29 52.59(12) 2_565 2_565 ?
S18 Ag17 Cl4 90.2(2) 2_565 . ?
Ag01 Ag18 Ag15 83.89(5) 2_565 . ?
Ag8 Ag18 Ag01 57.80(4) . 2_565 ?
Ag8 Ag18 Ag10 65.85(5) . . ?
Ag8 Ag18 Ag15 120.39(6) . . ?
Ag10 Ag18 Ag01 57.50(5) . 2_565 ?
Ag10 Ag18 Ag15 54.91(5) . . ?
S6 Ag18 Ag01 113.85(14) 2_565 2_565 ?
S6 Ag18 Ag8 57.93(13) 2_565 . ?
S6 Ag18 Ag10 106.88(13) 2_565 . ?
S6 Ag18 Ag15 143.95(14) 2_565 . ?
S7 Ag18 Ag01 92.22(12) . 2_565 ?
S7 Ag18 Ag8 149.94(13) . . ?
S7 Ag18 Ag10 97.59(12) . . ?
S7 Ag18 Ag15 46.39(11) . . ?
S7 Ag18 S6 151.01(18) . 2_565 ?
Ag01 Ag19 Ag5 58.09(4) . . ?
Ag01 Ag19 Ag13 64.79(5) . . ?
Ag13 Ag19 Ag5 56.89(5) . . ?
S2 Ag19 Ag01 147.56(13) 2_565 . ?
S2 Ag19 Ag5 90.06(12) 2_565 . ?
S2 Ag19 Ag13 93.85(12) 2_565 . ?
S2 Ag19 S10 154.57(17) 2_565 . ?
S10 Ag19 Ag01 57.76(12) . . ?
S10 Ag19 Ag5 114.11(13) . . ?
S10 Ag19 Ag13 105.73(12) . . ?
Ag1 Ag20 Ag1A 87.49(5) . . ?
Ag1 Ag20 Ag1B 150.75(8) . . ?
Ag1 Ag20 Ag2 56.08(4) . . ?
Ag1 Ag20 Ag5 57.01(4) . . ?
Ag1 Ag20 Ag05 108.47(6) . . ?
Ag1 Ag20 Ag7 109.59(5) . . ?
Ag1 Ag20 Ag8 59.83(4) . 2_565 ?
Ag1 Ag20 Ag12 61.35(5) . . ?
Ag1 Ag20 Ag25 67.62(5) . 2_565 ?
Ag1B Ag20 Ag1A 110.67(6) . . ?
Ag1B Ag20 Ag2 117.95(6) . . ?
Ag1B Ag20 Ag5 128.00(6) . . ?
Ag1B Ag20 Ag05 71.60(5) . . ?
Ag1B Ag20 Ag12 147.44(7) . . ?
Ag2 Ag20 Ag1A 50.71(4) . . ?
Ag2 Ag20 Ag5 111.10(5) . . ?
Ag2 Ag20 Ag12 82.37(5) . . ?
Ag5 Ag20 Ag1A 113.10(6) . . ?
Ag5 Ag20 Ag12 52.52(5) . . ?
Ag05 Ag20 Ag1A 141.93(6) . . ?
Ag05 Ag20 Ag2 163.18(6) . . ?
Ag05 Ag20 Ag5 56.70(4) . . ?
Ag05 Ag20 Ag12 96.02(5) . . ?
Ag7 Ag20 Ag1A 62.96(5) . . ?
Ag7 Ag20 Ag1B 63.29(5) . . ?
Ag7 Ag20 Ag2 56.01(4) . . ?
Ag7 Ag20 Ag5 166.60(6) . . ?
Ag7 Ag20 Ag05 134.83(6) . . ?
Ag7 Ag20 Ag8 118.14(6) . 2_565 ?
Ag7 Ag20 Ag12 123.32(6) . . ?
Ag8 Ag20 Ag1A 146.42(6) 2_565 . ?
Ag8 Ag20 Ag1B 97.10(6) 2_565 . ?
Ag8 Ag20 Ag2 99.96(5) 2_565 . ?
Ag8 Ag20 Ag5 57.17(4) 2_565 . ?
Ag8 Ag20 Ag05 64.08(5) 2_565 . ?
Ag8 Ag20 Ag12 104.34(6) 2_565 . ?
Ag12 Ag20 Ag1A 60.89(5) . . ?
Ag25 Ag20 Ag1A 102.48(5) 2_565 . ?
Ag25 Ag20 Ag1B 85.68(7) 2_565 . ?
Ag25 Ag20 Ag2 54.94(4) 2_565 . ?
Ag25 Ag20 Ag5 110.31(6) 2_565 . ?
Ag25 Ag20 Ag05 115.51(6) 2_565 . ?
Ag25 Ag20 Ag7 60.42(5) 2_565 . ?
Ag25 Ag20 Ag8 60.05(5) 2_565 2_565 ?
Ag25 Ag20 Ag12 126.25(6) 2_565 . ?
S2A Ag20 Ag1 111.47(18) . . ?
S2A Ag20 Ag1A 50.70(18) . . ?
S2A Ag20 Ag1B 97.71(18) . . ?
S2A Ag20 Ag2 100.56(18) . . ?
S2A Ag20 Ag5 89.1(2) . . ?
S2A Ag20 Ag05 91.27(19) . . ?
S2A Ag20 Ag7 96.7(2) . . ?
S2A Ag20 Ag8 145.2(2) . 2_565 ?
S2A Ag20 Ag12 51.49(19) . . ?
S2A Ag20 Ag25 152.5(2) . 2_565 ?
Ag02 Ag21 Ag7 56.39(4) . . ?
Ag02 Ag21 Ag25 64.50(5) . 2_565 ?
Ag25 Ag21 Ag7 54.78(4) 2_565 . ?
S3 Ag21 Ag02 56.79(11) . . ?
S3 Ag21 Ag7 110.40(12) . . ?
S3 Ag21 Ag25 108.72(12) . 2_565 ?
S25 Ag21 Ag02 144.08(17) . . ?
S25 Ag21 Ag7 88.14(16) . . ?
S25 Ag21 Ag25 91.71(14) . 2_565 ?
S25 Ag21 S3 157.85(19) . . ?
Ag1 Ag25 Ag02 110.70(5) 2_565 2_565 ?
Ag1 Ag25 Ag10 52.15(4) 2_565 . ?
Ag1 Ag25 Ag13 82.49(5) 2_565 . ?
Ag1E Ag25 Ag1 117.96(6) 2_565 2_565 ?
Ag1E Ag25 Ag02 128.97(6) 2_565 2_565 ?
Ag1E Ag25 Ag7 97.05(7) 2_565 2_565 ?
Ag1E Ag25 Ag10 109.73(6) 2_565 . ?
Ag1E Ag25 Ag13 144.64(8) 2_565 . ?
Ag1E Ag25 Ag21 73.08(5) 2_565 2_565 ?
Ag2 Ag25 Ag1 57.06(4) 2_565 2_565 ?
Ag2 Ag25 Ag1E 152.10(8) 2_565 2_565 ?
Ag2 Ag25 Ag02 55.79(4) 2_565 2_565 ?
Ag2 Ag25 Ag7 60.94(5) 2_565 2_565 ?
Ag2 Ag25 Ag8 111.76(6) 2_565 . ?
Ag2 Ag25 Ag10 88.64(5) 2_565 . ?
Ag2 Ag25 Ag13 62.93(5) 2_565 . ?
Ag2 Ag25 Ag20 69.54(5) 2_565 2_565 ?
Ag2 Ag25 Ag21 108.69(6) 2_565 2_565 ?
Ag02 Ag25 Ag10 111.59(6) 2_565 . ?
Ag02 Ag25 Ag13 53.64(5) 2_565 . ?
Ag7 Ag25 Ag1 101.86(5) 2_565 2_565 ?
Ag7 Ag25 Ag02 57.41(4) 2_565 2_565 ?
Ag7 Ag25 Ag10 149.06(6) 2_565 . ?
Ag7 Ag25 Ag13 106.97(6) 2_565 . ?
Ag7 Ag25 Ag21 66.18(5) 2_565 2_565 ?
Ag8 Ag25 Ag1 56.69(4) . 2_565 ?
Ag8 Ag25 Ag1E 62.81(5) . 2_565 ?
Ag8 Ag25 Ag02 167.33(6) . 2_565 ?
Ag8 Ag25 Ag7 120.84(6) . 2_565 ?
Ag8 Ag25 Ag10 62.81(5) . . ?
Ag8 Ag25 Ag13 120.86(6) . . ?
Ag8 Ag25 Ag21 135.76(6) . 2_565 ?
Ag10 Ag25 Ag13 58.32(5) . . ?
Ag20 Ag25 Ag1 55.92(4) 2_565 2_565 ?
Ag20 Ag25 Ag1E 85.19(7) 2_565 2_565 ?
Ag20 Ag25 Ag02 111.34(6) 2_565 2_565 ?
Ag20 Ag25 Ag7 61.44(5) 2_565 2_565 ?
Ag20 Ag25 Ag8 61.86(5) 2_565 . ?
Ag20 Ag25 Ag10 104.65(6) 2_565 . ?
Ag20 Ag25 Ag13 128.99(6) 2_565 . ?
Ag20 Ag25 Ag21 119.51(7) 2_565 2_565 ?
Ag21 Ag25 Ag1 165.55(6) 2_565 2_565 ?
Ag21 Ag25 Ag02 56.53(4) 2_565 2_565 ?
Ag21 Ag25 Ag10 135.73(6) 2_565 . ?
Ag21 Ag25 Ag13 93.07(5) 2_565 . ?
S1A Ag25 Ag1 103.45(16) . 2_565 ?
S1A Ag25 Ag1E 95.57(17) . 2_565 ?
S1A Ag25 Ag2 112.33(16) . 2_565 ?
S1A Ag25 Ag02 87.12(19) . 2_565 ?
S1A Ag25 Ag7 142.00(19) . 2_565 ?
S1A Ag25 Ag8 96.78(19) . . ?
S1A Ag25 Ag10 52.12(17) . . ?
S1A Ag25 Ag13 49.87(16) . . ?
S1A Ag25 Ag20 155.60(18) . 2_565 ?
S1A Ag25 Ag21 83.69(17) . 2_565 ?
Ag12 Ag29 Ag02 55.76(5) . 2_565 ?
Ag17 Ag29 Ag02 55.88(4) 2_565 2_565 ?
Ag17 Ag29 Ag12 67.18(5) 2_565 . ?
S4 Ag29 Ag02 94.80(12) . 2_565 ?
S4 Ag29 Ag12 95.32(12) . . ?
S4 Ag29 Ag17 150.56(13) . 2_565 ?
S4 Ag29 S18 151.73(17) . . ?
S18 Ag29 Ag02 110.30(13) . 2_565 ?
S18 Ag29 Ag12 109.30(13) . . ?
S18 Ag29 Ag17 56.54(12) . 2_565 ?
Ag5 Ag32 Ag16 87.70(6) . 2_565 ?
Ag12 Ag32 Ag5 57.40(5) . . ?
Ag12 Ag32 Ag16 75.47(6) . 2_565 ?
S1 Ag32 Ag5 56.07(11) . . ?
S1 Ag32 Ag12 99.49(11) . . ?
S1 Ag32 Ag16 136.31(13) . 2_565 ?
S1 Ag32 S4 155.35(17) . . ?
S4 Ag32 Ag5 147.12(13) . . ?
S4 Ag32 Ag12 94.71(12) . . ?
S4 Ag32 Ag16 66.90(12) . 2_565 ?
Ag13 S1A Ag10 75.43(17) . . ?
Ag13 S1A Ag25 78.76(18) . . ?
Ag25 S1A Ag10 75.91(17) . . ?
C8BA S1A Ag10 121.6(12) . . ?
C8BA S1A Ag13 123.0(10) . . ?
C8BA S1A Ag25 153.4(12) . . ?
Ag05 S1 Ag5 70.78(12) . . ?
Ag32 S1 Ag5 73.09(12) . . ?
Ag32 S1 Ag05 129.99(18) . . ?
C8 S1 Ag5 102.5(7) . . ?
C8 S1 Ag05 108.9(7) . . ?
C8 S1 Ag32 111.8(6) . . ?
Ag1A S2A Ag12 79.34(18) . . ?
Ag20 S2A Ag1A 79.25(19) . . ?
Ag20 S2A Ag12 78.01(19) . . ?
C7CA S2A Ag1A 131.6(8) . . ?
C7CA S2A Ag12 146.7(8) . . ?
C7CA S2A Ag20 115.4(7) . . ?
Ag19 S2 Ag16 92.31(16) 2_565 . ?
C35 S2 Ag16 105.6(6) . . ?
C35 S2 Ag19 101.3(7) . 2_565 ?
Ag16 S3 Ag02 70.95(13) . . ?
Ag21 S3 Ag02 71.20(13) . . ?
Ag21 S3 Ag16 127.9(2) . . ?
C17 S3 Ag02 100.2(7) . . ?
C17 S3 Ag16 110.1(6) . . ?
C17 S3 Ag21 110.7(7) . . ?
Ag29 S4 Ag32 90.58(16) . . ?
C1 S4 Ag29 104.9(8) . . ?
C1 S4 Ag32 106.0(7) . . ?
Ag17 Cl4 Ag7 64.44(17) . . ?
Ag1E S6 Ag8 71.86(15) . 2_565 ?
Ag1E S6 Ag18 129.8(2) . 2_565 ?
Ag18 S6 Ag8 69.60(13) 2_565 2_565 ?
C6AA S6 Ag1E 113.1(7) . . ?
C6AA S6 Ag8 102.3(7) . 2_565 ?
C6AA S6 Ag18 105.6(7) . 2_565 ?
Ag18 S7 Ag15 88.00(16) . . ?
C2BA S7 Ag15 105.1(7) . . ?
C2BA S7 Ag18 102.0(8) . . ?
Ag01 Cl8 Ag5 64.14(10) . . ?
Ag01 Cl8 Ag8 63.08(10) . 2_565 ?
Ag5 Cl8 Ag8 63.35(11) . 2_565 ?
Ag15 S10 Ag01 73.10(13) . . ?
Ag15 S10 Ag19 130.8(2) . . ?
Ag19 S10 Ag01 70.34(13) . . ?
C9AA S10 Ag01 102.2(7) . . ?
C9AA S10 Ag15 110.0(6) . . ?
C9AA S10 Ag19 109.1(6) . . ?
Ag05 S16 Ag1B 90.75(17) . . ?
C16 S16 Ag1B 108.6(6) . . ?
C16 S16 Ag05 97.9(5) . . ?
Ag1D S18 Ag17 72.63(15) . 2_565 ?
Ag1D S18 Ag29 129.0(2) . . ?
Ag29 S18 Ag17 70.87(14) . 2_565 ?
C0AA S18 Ag1D 113.1(7) . . ?
C0AA S18 Ag17 105.5(8) . 2_565 ?
C0AA S18 Ag29 110.2(7) . . ?
Ag11 S19 Ag1D 94.43(18) . . ?
C67 S19 Ag1D 91.1(6) . . ?
C67 S19 Ag11 108.9(7) . . ?
Ag1B S20 Ag7 74.10(16) . . ?
Ag1B S20 Ag11 129.2(2) . . ?
Ag11 S20 Ag7 70.21(14) . . ?
C74 S20 Ag1B 112.6(9) . . ?
C74 S20 Ag7 102.4(9) . . ?
C74 S20 Ag11 109.5(8) . . ?
Ag21 S25 Ag1E 93.04(18) . . ?
C95 S25 Ag1E 101.4(7) . . ?
C95 S25 Ag21 101.9(5) . . ?
C17 C7 C47 108.3(17) . . ?
C37 C7 C17 111.6(16) . . ?
C37 C7 C47 109.9(16) . . ?
C37 C9 C39 108.1(16) . . ?
C50 C9 C37 105.0(15) . . ?
C50 C9 C39 113.8(18) . . ?
C32 C10 C47 104.9(15) . . ?
C39 C10 C32 112.5(17) . . ?
C39 C10 C47 107.5(17) . . ?
C69 C12 C35 113.3(19) . . ?
C69 C12 C78 105.1(17) . . ?
C78 C12 C35 106.9(17) . . ?
C35 C15 C24 109.9(17) . . ?
C54 C15 C24 108.1(17) . . ?
C54 C15 C35 107.8(19) . . ?
C7 C17 S3 112.1(15) . . ?
C7 C17 C34 108.5(16) . . ?
C34 C17 S3 111.6(13) . . ?
C66 C24 C15 107.9(19) . . ?
C34 C32 C10 112.0(18) . . ?
C17 C34 C50 108.7(17) . . ?
C32 C34 C17 109.2(16) . . ?
C32 C34 C50 110.6(16) . . ?
C12 C35 S2 104.8(14) . . ?
C15 C35 S2 112.9(16) . . ?
C15 C35 C12 109.4(17) . . ?
C7 C37 C9 111.6(17) . . ?
C10 C39 C9 108.6(16) . . ?
C7 C47 C10 108.6(15) . . ?
C9 C50 C34 110.4(16) . . ?
C55 C54 C15 113.4(18) . . ?
C54 C55 C63 104.3(17) . . ?
C54 C55 C78 114.7(18) . . ?
C78 C55 C63 101.8(17) . . ?
C90 C62 C103 108(2) . . ?
C94 C62 C90 105(2) . . ?
C94 C62 C103 102(2) . . ?
C66 C63 C55 112.5(18) . . ?
C74 C65 C85 102.9(18) . . ?
C90 C65 C74 108(2) . . ?
C90 C65 C85 107(2) . . ?
C24 C66 C69 111.9(18) . . ?
C63 C66 C24 111.3(19) . . ?
C63 C66 C69 110.5(19) . . ?
C12 C69 C66 107.0(18) . . ?
C65 C74 S20 111.7(16) . . ?
C65 C74 C86 110(2) . . ?
C86 C74 S20 113.0(18) . . ?
C55 C78 C12 113.0(19) . . ?
C106 C83 C95 107.2(6) . . ?
C122 C83 C95 110.0(6) . . ?
C122 C83 C106 109.4(6) . . ?
C93 C85 C65 112(2) . . ?
C87 C86 C74 103(2) . . ?
C94 C86 C74 104(2) . . ?
C94 C86 C87 113(2) . . ?
C93 C87 C86 109(2) . . ?
C62 C90 C65 115(2) . . ?
C85 C93 C87 108(2) . . ?
C85 C93 C103 114(2) . . ?
C103 C93 C87 112(2) . . ?
C86 C94 C62 119(2) . . ?
C83 C95 S25 113.9(11) . . ?
C151 C95 S25 119.1(11) . . ?
C151 C95 C83 107.8(5) . . ?
C104 C100 C107 111.2(4) . . ?
C93 C103 C62 113(2) . . ?
C100 C104 C118 113.1(6) . . ?
C100 C104 C122 110.0(6) . . ?
C122 C104 C118 102.5(9) . . ?
C107 C106 C83 110.9(5) . . ?
C100 C107 C112 108.5(6) . . ?
C106 C107 C100 106.8(7) . . ?
C106 C107 C112 113.0(6) . . ?
C107 C112 C151 108.6(4) . . ?
C104 C118 C151 110.0(6) . . ?
C83 C122 C104 111.1(4) . . ?
C95 C151 C112 109.6(6) . . ?
C95 C151 C118 109.8(6) . . ?
C118 C151 C112 109.9(6) . . ?
C11 C1 S4 114.1(15) . . ?
C14 C1 S4 112.0(16) . . ?
C14 C1 C11 103.8(17) . . ?
C8 C2 C5AA 109.2(15) . . ?
C18 C2 C5AA 113.1(14) . . ?
C18 C2 C8 108.7(16) . . ?
C4 C3 C13 105.2(15) . . ?
C3 C4 C8 108.4(15) . . ?
C6 C4 C3 111.9(14) . . ?
C6 C4 C8 109.6(16) . . ?
C19 C5 C9AA 103.8(16) . . ?
C21 C5 C9AA 109.9(17) . . ?
C21 C5 C19 110.9(17) . . ?
C4AA C6 C4 112.9(16) . . ?
C4AA C5AA C2 110.0(16) . . ?
C2 C8 S1 115.1(14) . . ?
C2 C8 C4 105.4(14) . . ?
C4 C8 S1 113.1(12) . . ?
C28 C2BA S7 105.5(16) . . ?
C41 C2BA S7 112.5(18) . . ?
C41 C2BA C28 115.8(19) . . ?
C25 C6AA S6 114.5(14) . . ?
C25 C6AA C8AA 107.6(15) . . ?
C8AA C6AA S6 112.6(13) . . ?
C22 C11 C1 111.4(19) . . ?
C22 C11 C27 110.9(18) . . ?
C27 C11 C1 108.9(18) . . ?
C5 C9AA S10 112.0(14) . . ?
C26 C9AA S10 109.5(14) . . ?
C26 C9AA C5 109.4(17) . . ?
C18 C13 C3 101.2(13) . . ?
C48 C13 C3 111.3(15) . . ?
C48 C13 C18 116.0(18) . . ?
C1 C14 C2AA 114.3(19) . . ?
C1 C14 C3AA 108.1(19) . . ?
C3AA C14 C2AA 114.8(18) . . ?
C42 C2AA C14 104.9(18) . . ?
C51 C16 S16 109.5(10) . . ?
C51 C16 C71 109.7(4) . . ?
C71 C16 S16 112.5(11) . . ?
C19 C0BA C1BA 107.2(18) . . ?
C20 C0BA C19 110.6(17) . . ?
C20 C0BA C1BA 112.7(18) . . ?
C2 C18 C13 109.0(15) . . ?
C0BA C19 C5 110.7(16) . . ?
C0BA C20 C26 107.0(17) . . ?
C5 C21 C43 108.7(17) . . ?
C11 C22 C42 109.2(19) . . ?
C33 C23 C30 112.4(19) . . ?
C33 C23 C0AA 108.3(19) . . ?
C0AA C23 C30 107.1(18) . . ?
C6 C4AA C5AA 106.8(14) . . ?
C6 C4AA C48 108.7(17) . . ?
C5AA C4AA C48 109.4(15) . . ?
C31 C25 C6AA 108.8(16) . . ?
C49 C25 C6AA 108.8(17) . . ?
C49 C25 C31 112.6(16) . . ?
C9AA C26 C20 108.1(16) . . ?
C9AA C26 C38 113.7(18) . . ?
C38 C26 C20 109.0(16) . . ?
C11 C27 C36 109.9(19) . . ?
C44 C28 C2BA 102(2) . . ?
C77 C28 C2BA 104(2) . . ?
C77 C28 C44 104.3(19) . . ?
C0AA C29 C1AA 107.5(19) . . ?
C40 C29 C0AA 109.9(18) . . ?
C40 C29 C1AA 111.7(18) . . ?
C57 C30 C23 108.5(19) . . ?
C25 C31 C58 107.9(16) . . ?
C43 C1BA C0BA 110.3(18) . . ?
C23 C33 C46 110.3(18) . . ?
C23 C0AA S18 114.1(16) . . ?
C29 C0AA S18 113.8(15) . . ?
C29 C0AA C23 108.4(18) . . ?
C4BA C3BA C41 112(2) . . ?
C27 C36 C3AA 105.0(17) . . ?
C60 C36 C27 105.3(18) . . ?
C60 C36 C3AA 114.0(19) . . ?
C58 C7AA C8AA 109.6(17) . . ?
C43 C38 C26 105.4(17) . . ?
C7AA C8AA C6AA 108.8(16) . . ?
C76 C8AA C6AA 109.9(17) . . ?
C76 C8AA C7AA 108.1(16) . . ?
C46 C40 C29 108.0(19) . . ?
C2BA C41 C3BA 111(2) . . ?
C2BA C41 C64 110(2) . . ?
C64 C41 C3BA 105.2(18) . . ?
C2AA C42 C60 112.7(18) . . ?
C22 C42 C2AA 111.2(17) . . ?
C22 C42 C60 106.5(18) . . ?
C1BA C43 C21 108.8(17) . . ?
C1BA C43 C38 116.4(19) . . ?
C38 C43 C21 106.9(16) . . ?
C4BA C44 C28 125(2) . . ?
C46 C45 C57 110.7(19) . . ?
C40 C46 C33 108.6(18) . . ?
C45 C46 C33 109(2) . . ?
C45 C46 C40 114(2) . . ?
C14 C3AA C36 107.8(18) . . ?
C13 C48 C4AA 111.9(15) . . ?
C25 C49 C88 111.7(17) . . ?
C3BA C4BA C59 107(2) . . ?
C44 C4BA C3BA 108(2) . . ?
C44 C4BA C59 101(2) . . ?
C16 C51 C70 109.8(6) . . ?
C84 C51 C16 108.3(8) . . ?
C84 C51 C70 110.8(6) . . ?
C59 C52 C64 104(2) . . ?
C77 C52 C59 111(2) . . ?
C77 C52 C64 114.8(19) . . ?
C61 C53 C7BA 112.3(10) . . ?
C6BA C5BA C136 110(3) . . ?
C8BA C5BA C6BA 99(2) . . ?
C8BA C5BA C136 115(3) . . ?
C57 C1AA C29 107.8(18) . . ?
C58 C56 C88 112.7(16) . . ?
C30 C57 C45 109.9(18) . . ?
C30 C57 C1AA 109.0(18) . . ?
C1AA C57 C45 109.2(19) . . ?
C7AA C58 C31 111.8(15) . . ?
C56 C58 C31 105.1(16) . . ?
C56 C58 C7AA 110.8(17) . . ?
C52 C59 C4BA 112.4(19) . . ?
C36 C60 C42 110.4(17) . . ?
C53 C61 C6BA 113(2) . . ?
C53 C61 C174 104.7(19) . . ?
C6BA C61 C174 102(2) . . ?
C67 C0CA C1CA 109.3(6) . . ?
C110 C0CA C1CA 109.2(6) . . ?
C110 C0CA C67 109.7(5) . . ?
C5BA C6BA C61 113(2) . . ?
C41 C64 C52 109(2) . . ?
C3CA C1CA C0CA 109.1(6) . . ?
C0CA C67 S19 110.7(11) . . ?
C0CA C67 C82 108.8(6) . . ?
C82 C67 S19 110.9(14) . . ?
C9BA C68 C8BA 106(3) . . ?
C174 C68 C8BA 110(2) . . ?
C174 C68 C9BA 99(2) . . ?
C129 C70 C51 108.6(4) . . ?
C16 C71 C102 108.2(6) . . ?
C4CA C71 C16 110.9(6) . . ?
C4CA C71 C102 107.7(7) . . ?
C129 C4CA C71 110.8(5) . . ?
C8AA C76 C88 113.6(17) . . ?
C52 C77 C28 112(2) . . ?
C110 C2CA C80 108.2(8) . . ?
C166 C2CA C80 112.8(7) . . ?
C166 C2CA C110 109.3(8) . . ?
C2CA C80 C82 107.6(8) . . ?
C80 C82 C67 108.2(6) . . ?
C99 C82 C67 112.3(18) . . ?
C99 C82 C80 109.3(19) . . ?
C9BA C7BA C53 106.5(16) . . ?
C9BA C7BA C136 115(2) . . ?
C136 C7BA C53 102(2) . . ?
C7DA C84 C51 110.3(5) . . ?
C5BA C8BA S1A 122(2) . . ?
C5BA C8BA C68 115(2) . . ?
C68 C8BA S1A 110.7(18) . . ?
C49 C88 C56 107.2(16) . . ?
C49 C88 C76 108.0(15) . . ?
C56 C88 C76 106.6(16) . . ?
C99 C3CA C1CA 112.9(18) . . ?
C99 C3CA C166 105(2) . . ?
C166 C3CA C1CA 109.7(6) . . ?
C3CA C99 C82 109.1(17) . . ?
C7BA C9BA C68 116.1(18) . . ?
C7DA C102 C71 109.1(5) . . ?
C2CA C110 C0CA 109.6(5) . . ?
C4CA C129 C70 110.7(6) . . ?
C4CA C129 C130 107.1(7) . . ?
C130 C129 C70 110.0(6) . . ?
C129 C130 C7DA 110.2(5) . . ?
C5BA C136 C7BA 110(2) . . ?
C2CA C166 C3CA 109.5(8) . . ?
C68 C174 C61 115(2) . . ?
C156 C2DA C3DA 108.7(6) . . ?
C160 C2DA C3DA 109.1(5) . . ?
C160 C2DA C156 110.5(6) . . ?
C3DA C4DA C1DA 109.6(6) . . ?
C7CA C4DA C1DA 107.4(7) . . ?
C7CA C4DA C3DA 110.3(6) . . ?
C5DA C8CA C0DA 109.8(4) . . ?
C5DA C1DA C4DA 111.2(5) . . ?
C8CA C0DA C7CA 107.2(6) . . ?
C160 C0DA C8CA 110.0(5) . . ?
C160 C0DA C7CA 110.3(5) . . ?
C4DA C3DA C2DA 109.1(4) . . ?
C4DA C7CA S2A 144.8(12) . . ?
C4DA C7CA C0DA 109.7(4) . . ?
C0DA C7CA S2A 99.3(10) . . ?
C8CA C5DA C156 110.9(6) . . ?
C1DA C5DA C8CA 108.0(7) . . ?
C1DA C5DA C156 108.8(7) . . ?
C5DA C156 C2DA 109.9(4) . . ?
C0DA C160 C2DA 109.8(4) . . ?
C84 C7DA C102 108.4(8) . . ?
C84 C7DA C130 110.6(8) . . ?
C130 C7DA C102 109.0(7) . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Ag01 S10 C9AA C5 132.2(13) . . . . ?
Ag01 S10 C9AA C26 -106.3(15) . . . . ?
Ag1A S2A C7CA C4DA 142.7(14) . . . . ?
Ag1A S2A C7CA C0DA -71.7(10) . . . . ?
Ag1B S20 C74 C65 50(2) . . . . ?
Ag1B S20 C74 C86 175.4(14) . . . . ?
Ag1D S18 C0AA C23 55.0(18) . . . . ?
Ag1D S18 C0AA C29 -179.8(14) . . . . ?
Ag1D S19 C67 C0CA -151.4(10) . . . . ?
Ag1D S19 C67 C82 87.8(11) . . . . ?
Ag1E S6 C6AA C25 176.9(12) . . . . ?
Ag1E S6 C6AA C8AA 53.6(15) . . . . ?
Ag1E S25 C95 C83 38.4(9) . . . . ?
Ag1E S25 C95 C151 167.4(8) . . . . ?
Ag02 S3 C17 C7 132.0(12) . . . . ?
Ag02 S3 C17 C34 -106.0(13) . . . . ?
Ag5 S1 C8 C2 130.7(12) . . . . ?
Ag5 S1 C8 C4 -108.1(13) . . . . ?
Ag05 S1 C8 C2 -155.6(11) . . . . ?
Ag05 S1 C8 C4 -34.4(15) . . . . ?
Ag7 S20 C74 C65 128.0(18) . . . . ?
Ag7 S20 C74 C86 -106.9(17) . . . . ?
Ag8 S6 C6AA C25 -107.7(14) 2_565 . . . ?
Ag8 S6 C6AA C8AA 128.9(13) 2_565 . . . ?
Ag10 S1A C8BA C5BA -146(2) . . . . ?
Ag10 S1A C8BA C68 74(3) . . . . ?
Ag11 S19 C67 C0CA -56.4(11) . . . . ?
Ag11 S19 C67 C82 -177.2(9) . . . . ?
Ag11 S20 C74 C65 -158.9(16) . . . . ?
Ag11 S20 C74 C86 -34(2) . . . . ?
Ag12 S2A C7CA C4DA -63(2) . . . . ?
Ag12 S2A C7CA C0DA 82.4(16) . . . . ?
Ag13 S1A C8BA C5BA -53(3) . . . . ?
Ag13 S1A C8BA C68 167.0(17) . . . . ?
Ag15 S10 C9AA C5 56.0(16) . . . . ?
Ag15 S10 C9AA C26 177.5(13) . . . . ?
Ag16 S3 C17 C7 58.7(14) . . . . ?
Ag16 S3 C17 C34 -179.3(12) . . . . ?
Ag17 S18 C0AA C23 132.4(15) 2_565 . . . ?
Ag17 S18 C0AA C29 -102.4(17) 2_565 . . . ?
Ag18 S6 C6AA C25 -35.8(15) 2_565 . . . ?
Ag18 S6 C6AA C8AA -159.1(12) 2_565 . . . ?
Ag19 S10 C9AA C5 -154.6(12) . . . . ?
Ag19 S10 C9AA C26 -33.1(17) . . . . ?
Ag20 S2A C7CA C4DA 44(2) . . . . ?
Ag20 S2A C7CA C0DA -170.0(6) . . . . ?
Ag21 S3 C17 C7 -154.4(11) . . . . ?
Ag21 S3 C17 C34 -32.4(15) . . . . ?
Ag21 S25 C95 C83 134.0(7) . . . . ?
Ag21 S25 C95 C151 -97.0(8) . . . . ?
Ag25 S1A C8BA C5BA 88(3) . . . . ?
Ag25 S1A C8BA C68 -52(4) . . . . ?
Ag29 S4 C1 C11 131.7(15) . . . . ?
Ag29 S4 C1 C14 -110.7(15) . . . . ?
Ag29 S18 C0AA C23 -152.7(14) . . . . ?
Ag29 S18 C0AA C29 -27.5(19) . . . . ?
Ag32 S1 C8 C2 54.1(14) . . . . ?
Ag32 S1 C8 C4 175.4(11) . . . . ?
Ag32 S4 C1 C11 36.7(18) . . . . ?
Ag32 S4 C1 C14 154.3(14) . . . . ?
S3 C17 C34 C32 172.6(13) . . . . ?
S3 C17 C34 C50 -66.7(18) . . . . ?
S4 C1 C11 C22 63(2) . . . . ?
S4 C1 C11 C27 -174.2(15) . . . . ?
S4 C1 C14 C2AA -62(2) . . . . ?
S4 C1 C14 C3AA 168.9(14) . . . . ?
S6 C6AA C25 C31 170.3(13) . . . . ?
S6 C6AA C25 C49 -66.6(18) . . . . ?
S6 C6AA C8AA C7AA -171.7(14) . . . . ?
S6 C6AA C8AA C76 70.1(19) . . . . ?
S7 C2BA C28 C44 -75.1(19) . . . . ?
S7 C2BA C28 C77 176.6(16) . . . . ?
S7 C2BA C41 C3BA 65(2) . . . . ?
S7 C2BA C41 C64 -179.7(16) . . . . ?
S10 C9AA C26 C20 171.9(14) . . . . ?
S10 C9AA C26 C38 -67(2) . . . . ?
S16 C16 C51 C70 -63.9(12) . . . . ?
S16 C16 C51 C84 175.0(11) . . . . ?
S16 C16 C71 C4CA 64.8(12) . . . . ?
S16 C16 C71 C102 -177.2(10) . . . . ?
S19 C67 C82 C80 -176.5(13) . . . . ?
S19 C67 C82 C99 62.8(18) . . . . ?
S20 C74 C86 C87 171.4(16) . . . . ?
S20 C74 C86 C94 -70(2) . . . . ?
S25 C95 C151 C112 -67.3(11) . . . . ?
S25 C95 C151 C118 171.9(10) . . . . ?
C7 C17 C34 C32 -63(2) . . . . ?
C7 C17 C34 C50 57(2) . . . . ?
C10 C32 C34 C17 63(2) . . . . ?
C10 C32 C34 C50 -56(2) . . . . ?
C15 C24 C66 C63 59(2) . . . . ?
C15 C24 C66 C69 -66(2) . . . . ?
C15 C54 C55 C63 -60(2) . . . . ?
C15 C54 C55 C78 50(3) . . . . ?
C17 C7 C37 C9 60(2) . . . . ?
C17 C7 C47 C10 -63.2(19) . . . . ?
C17 C34 C50 C9 -64(2) . . . . ?
C24 C15 C35 S2 62.7(19) . . . . ?
C24 C15 C35 C12 -54(2) . . . . ?
C24 C15 C54 C55 61(2) . . . . ?
C24 C66 C69 C12 63(2) . . . . ?
C32 C10 C39 C9 -53(2) . . . . ?
C32 C10 C47 C7 59(2) . . . . ?
C32 C34 C50 C9 56(2) . . . . ?
C35 C12 C69 C66 -55(2) . . . . ?
C35 C12 C78 C55 52(2) . . . . ?
C35 C15 C24 C66 61(2) . . . . ?
C35 C15 C54 C55 -58(2) . . . . ?
C37 C7 C17 S3 67.1(19) . . . . ?
C37 C7 C17 C34 -57(2) . . . . ?
C37 C7 C47 C10 59(2) . . . . ?
C37 C9 C39 C10 -62(2) . . . . ?
C37 C9 C50 C34 63(2) . . . . ?
C39 C9 C37 C7 61(2) . . . . ?
C39 C9 C50 C34 -55(2) . . . . ?
C39 C10 C32 C34 57(2) . . . . ?
C39 C10 C47 C7 -61(2) . . . . ?
C47 C7 C17 S3 -171.8(13) . . . . ?
C47 C7 C17 C34 64(2) . . . . ?
C47 C7 C37 C9 -61(2) . . . . ?
C47 C10 C32 C34 -59(2) . . . . ?
C47 C10 C39 C9 62(2) . . . . ?
C50 C9 C37 C7 -61(2) . . . . ?
C50 C9 C39 C10 54(2) . . . . ?
C54 C15 C24 C66 -56(2) . . . . ?
C54 C15 C35 S2 -179.8(13) . . . . ?
C54 C15 C35 C12 64(2) . . . . ?
C54 C55 C63 C66 60(2) . . . . ?
C54 C55 C78 C12 -48(2) . . . . ?
C55 C63 C66 C24 -63(2) . . . . ?
C55 C63 C66 C69 62(2) . . . . ?
C63 C55 C78 C12 64(2) . . . . ?
C63 C66 C69 C12 -61(2) . . . . ?
C65 C74 C86 C87 -63(3) . . . . ?
C65 C74 C86 C94 56(3) . . . . ?
C65 C85 C93 C87 68(3) . . . . ?
C65 C85 C93 C103 -57(3) . . . . ?
C69 C12 C35 S2 -68(2) . . . . ?
C69 C12 C35 C15 54(2) . . . . ?
C69 C12 C78 C55 -68(2) . . . . ?
C74 C65 C85 C93 -62(3) . . . . ?
C74 C65 C90 C62 59(3) . . . . ?
C74 C86 C87 C93 66(3) . . . . ?
C74 C86 C94 C62 -60(3) . . . . ?
C78 C12 C35 S2 177.2(14) . . . . ?
C78 C12 C35 C15 -62(2) . . . . ?
C78 C12 C69 C66 61(2) . . . . ?
C78 C55 C63 C66 -60(2) . . . . ?
C83 C95 C151 C112 64.4(8) . . . . ?
C83 C95 C151 C118 -56.4(8) . . . . ?
C83 C106 C107 C100 62.3(8) . . . . ?
C83 C106 C107 C112 -56.9(9) . . . . ?
C85 C65 C74 S20 -176.6(17) . . . . ?
C85 C65 C74 C86 57(3) . . . . ?
C85 C65 C90 C62 -51(3) . . . . ?
C85 C93 C103 C62 59(3) . . . . ?
C86 C87 C93 C85 -72(3) . . . . ?
C86 C87 C93 C103 54(3) . . . . ?
C87 C86 C94 C62 51(3) . . . . ?
C87 C93 C103 C62 -64(3) . . . . ?
C90 C62 C94 C86 60(3) . . . . ?
C90 C62 C103 C93 -53(3) . . . . ?
C90 C65 C74 S20 70(2) . . . . ?
C90 C65 C74 C86 -56(3) . . . . ?
C90 C65 C85 C93 52(3) . . . . ?
C94 C62 C90 C65 -56(3) . . . . ?
C94 C62 C103 C93 58(3) . . . . ?
C94 C86 C87 C93 -46(3) . . . . ?
C95 C83 C106 C107 59.7(8) . . . . ?
C95 C83 C122 C104 -63.2(8) . . . . ?
C100 C104 C118 C151 52.2(12) . . . . ?
C100 C104 C122 C83 -54.7(9) . . . . ?
C100 C107 C112 C151 -63.1(7) . . . . ?
C103 C62 C90 C65 53(3) . . . . ?
C103 C62 C94 C86 -53(3) . . . . ?
C104 C100 C107 C106 -62.7(8) . . . . ?
C104 C100 C107 C112 59.4(8) . . . . ?
C104 C118 C151 C95 65.1(10) . . . . ?
C104 C118 C151 C112 -55.6(11) . . . . ?
C106 C83 C95 S25 71.1(11) . . . . ?
C106 C83 C95 C151 -63.4(8) . . . . ?
C106 C83 C122 C104 54.3(9) . . . . ?
C106 C107 C112 C151 55.1(8) . . . . ?
C107 C100 C104 C118 -54.7(10) . . . . ?
C107 C100 C104 C122 59.3(8) . . . . ?
C107 C112 C151 C95 -58.7(8) . . . . ?
C107 C112 C151 C118 62.1(9) . . . . ?
C118 C104 C122 C83 65.8(8) . . . . ?
C122 C83 C95 S25 -170.0(10) . . . . ?
C122 C83 C95 C151 55.5(8) . . . . ?
C122 C83 C106 C107 -59.6(8) . . . . ?
C122 C104 C118 C151 -66.2(10) . . . . ?
C1 C11 C22 C42 60(2) . . . . ?
C1 C11 C27 C36 -62(2) . . . . ?
C1 C14 C2AA C42 -63(2) . . . . ?
C1 C14 C3AA C36 71(2) . . . . ?
C2 C5AA C4AA C6 -61.3(19) . . . . ?
C2 C5AA C4AA C48 56.3(19) . . . . ?
C3 C4 C6 C4AA 59(2) . . . . ?
C3 C4 C8 S1 169.3(12) . . . . ?
C3 C4 C8 C2 -64.1(19) . . . . ?
C3 C13 C18 C2 69.1(18) . . . . ?
C3 C13 C48 C4AA -60(2) . . . . ?
C4 C3 C13 C18 -67.4(17) . . . . ?
C4 C3 C13 C48 56.4(19) . . . . ?
C4 C6 C4AA C5AA 61(2) . . . . ?
C4 C6 C4AA C48 -57.5(19) . . . . ?
C5 C9AA C26 C20 -65(2) . . . . ?
C5 C9AA C26 C38 56(2) . . . . ?
C5 C21 C43 C1BA 59(2) . . . . ?
C5 C21 C43 C38 -67(2) . . . . ?
C6 C4 C8 S1 -68.2(17) . . . . ?
C6 C4 C8 C2 58.4(18) . . . . ?
C6 C4AA C48 C13 60(2) . . . . ?
C5AA C2 C8 S1 64.6(17) . . . . ?
C5AA C2 C8 C4 -60.7(19) . . . . ?
C5AA C2 C18 C13 51(2) . . . . ?
C5AA C4AA C48 C13 -56(2) . . . . ?
C8 C2 C5AA C4AA 64.6(18) . . . . ?
C8 C2 C18 C13 -70.6(18) . . . . ?
C8 C4 C6 C4AA -61.1(19) . . . . ?
C2BA C28 C44 C4BA -52(3) . . . . ?
C2BA C28 C77 C52 55(3) . . . . ?
C2BA C41 C64 C52 -52(3) . . . . ?
C6AA C25 C31 C58 62(2) . . . . ?
C6AA C25 C49 C88 -63(2) . . . . ?
C6AA C8AA C76 C88 57(2) . . . . ?
C11 C1 C14 C2AA 61(2) . . . . ?
C11 C1 C14 C3AA -68(2) . . . . ?
C11 C22 C42 C2AA -62(2) . . . . ?
C11 C22 C42 C60 61(2) . . . . ?
C11 C27 C36 C3AA 61(2) . . . . ?
C11 C27 C36 C60 -60(2) . . . . ?
C9AA C5 C19 C0BA -63(2) . . . . ?
C9AA C5 C21 C43 61(2) . . . . ?
C9AA C26 C38 C43 -61(2) . . . . ?
C13 C3 C4 C6 -53.6(19) . . . . ?
C13 C3 C4 C8 67.4(17) . . . . ?
C14 C1 C11 C22 -59(2) . . . . ?
C14 C1 C11 C27 64(2) . . . . ?
C14 C2AA C42 C22 59(2) . . . . ?
C14 C2AA C42 C60 -60(2) . . . . ?
C2AA C14 C3AA C36 -57(2) . . . . ?
C2AA C42 C60 C36 57(3) . . . . ?
C16 C51 C70 C129 -60.8(8) . . . . ?
C16 C51 C84 C7DA 62.0(10) . . . . ?
C16 C71 C4CA C129 55.9(10) . . . . ?
C16 C71 C102 C7DA -60.2(9) . . . . ?
C0BA C20 C26 C9AA 61(2) . . . . ?
C0BA C20 C26 C38 -63(2) . . . . ?
C0BA C1BA C43 C21 -66(2) . . . . ?
C0BA C1BA C43 C38 54(2) . . . . ?
C18 C2 C5AA C4AA -57(2) . . . . ?
C18 C2 C8 S1 -171.6(12) . . . . ?
C18 C2 C8 C4 63.1(18) . . . . ?
C18 C13 C48 C4AA 55(2) . . . . ?
C19 C5 C9AA S10 -174.4(13) . . . . ?
C19 C5 C9AA C26 64(2) . . . . ?
C19 C5 C21 C43 -53(2) . . . . ?
C19 C0BA C20 C26 -60(2) . . . . ?
C19 C0BA C1BA C43 67(2) . . . . ?
C20 C0BA C19 C5 64(2) . . . . ?
C20 C0BA C1BA C43 -55(2) . . . . ?
C20 C26 C38 C43 59.2(19) . . . . ?
C21 C5 C9AA S10 66.9(18) . . . . ?
C21 C5 C9AA C26 -55(2) . . . . ?
C21 C5 C19 C0BA 55(2) . . . . ?
C22 C11 C27 C36 61(2) . . . . ?
C22 C42 C60 C36 -65(2) . . . . ?
C23 C30 C57 C45 55(2) . . . . ?
C23 C30 C57 C1AA -65(2) . . . . ?
C23 C33 C46 C40 65(3) . . . . ?
C23 C33 C46 C45 -60(2) . . . . ?
C25 C6AA C8AA C7AA 61(2) . . . . ?
C25 C6AA C8AA C76 -57(2) . . . . ?
C25 C31 C58 C7AA -60(2) . . . . ?
C25 C31 C58 C56 60(2) . . . . ?
C25 C49 C88 C56 -55(2) . . . . ?
C25 C49 C88 C76 59(2) . . . . ?
C26 C38 C43 C21 64(2) . . . . ?
C26 C38 C43 C1BA -58(2) . . . . ?
C27 C11 C22 C42 -61(2) . . . . ?
C27 C36 C3AA C14 -64(2) . . . . ?
C27 C36 C60 C42 63(2) . . . . ?
C28 C2BA C41 C3BA -57(3) . . . . ?
C28 C2BA C41 C64 59(3) . . . . ?
C28 C44 C4BA C3BA 55(3) . . . . ?
C28 C44 C4BA C59 -57(3) . . . . ?
C29 C40 C46 C33 -62(2) . . . . ?
C29 C40 C46 C45 59(3) . . . . ?
C29 C1AA C57 C30 64(2) . . . . ?
C29 C1AA C57 C45 -56(2) . . . . ?
C30 C23 C33 C46 57(3) . . . . ?
C30 C23 C0AA S18 65(2) . . . . ?
C30 C23 C0AA C29 -63(2) . . . . ?
C31 C25 C49 C88 57(2) . . . . ?
C1BA C0BA C19 C5 -59(2) . . . . ?
C1BA C0BA C20 C26 60(2) . . . . ?
C33 C23 C30 C57 -56(2) . . . . ?
C33 C23 C0AA S18 -173.1(15) . . . . ?
C33 C23 C0AA C29 59(2) . . . . ?
C0AA C23 C30 C57 63(2) . . . . ?
C0AA C23 C33 C46 -61(2) . . . . ?
C0AA C29 C40 C46 62(2) . . . . ?
C0AA C29 C1AA C57 -63(2) . . . . ?
C3BA C41 C64 C52 67(2) . . . . ?
C3BA C4BA C59 C52 -59(3) . . . . ?
C7AA C8AA C76 C88 -62(2) . . . . ?
C8AA C6AA C25 C31 -64(2) . . . . ?
C8AA C6AA C25 C49 59(2) . . . . ?
C8AA C7AA C58 C31 59(2) . . . . ?
C8AA C7AA C58 C56 -58(2) . . . . ?
C8AA C76 C88 C49 -57(2) . . . . ?
C8AA C76 C88 C56 58(2) . . . . ?
C40 C29 C0AA S18 172.9(15) . . . . ?
C40 C29 C0AA C23 -59(2) . . . . ?
C40 C29 C1AA C57 58(2) . . . . ?
C41 C2BA C28 C44 50(3) . . . . ?
C41 C2BA C28 C77 -58(3) . . . . ?
C41 C3BA C4BA C44 -50(3) . . . . ?
C41 C3BA C4BA C59 58(2) . . . . ?
C44 C28 C77 C52 -51(3) . . . . ?
C44 C4BA C59 C52 54(3) . . . . ?
C46 C45 C57 C30 -62(3) . . . . ?
C46 C45 C57 C1AA 58(2) . . . . ?
C3AA C14 C2AA C42 62(2) . . . . ?
C3AA C36 C60 C42 -51(2) . . . . ?
C48 C13 C18 C2 -51(2) . . . . ?
C49 C25 C31 C58 -59(2) . . . . ?
C4BA C3BA C41 C2BA 55(3) . . . . ?
C4BA C3BA C41 C64 -63(2) . . . . ?
C51 C16 C71 C4CA -57.2(9) . . . . ?
C51 C16 C71 C102 60.8(8) . . . . ?
C51 C70 C129 C4CA 59.3(8) . . . . ?
C51 C70 C129 C130 -58.9(8) . . . . ?
C51 C84 C7DA C102 -61.8(10) . . . . ?
C51 C84 C7DA C130 57.5(11) . . . . ?
C53 C61 C6BA C5BA 42(3) . . . . ?
C53 C61 C174 C68 -66(3) . . . . ?
C53 C7BA C9BA C68 61(3) . . . . ?
C53 C7BA C136 C5BA -70(2) . . . . ?
C1AA C29 C0AA S18 -65(2) . . . . ?
C1AA C29 C0AA C23 63(2) . . . . ?
C1AA C29 C40 C46 -57(2) . . . . ?
C57 C45 C46 C33 61(2) . . . . ?
C57 C45 C46 C40 -60(3) . . . . ?
C58 C7AA C8AA C6AA -59(2) . . . . ?
C58 C7AA C8AA C76 60(2) . . . . ?
C58 C56 C88 C49 62(2) . . . . ?
C58 C56 C88 C76 -53(2) . . . . ?
C59 C52 C64 C41 -67(2) . . . . ?
C59 C52 C77 C28 59(3) . . . . ?
C60 C36 C3AA C14 51(3) . . . . ?
C61 C53 C7BA C9BA -57(3) . . . . ?
C61 C53 C7BA C136 64(3) . . . . ?
C0CA C1CA C3CA C99 57.9(17) . . . . ?
C0CA C1CA C3CA C166 -59.3(14) . . . . ?
C0CA C67 C82 C80 61.5(13) . . . . ?
C0CA C67 C82 C99 -59.2(17) . . . . ?
C6BA C5BA C8BA S1A 160(2) . . . . ?
C6BA C5BA C8BA C68 -62(3) . . . . ?
C6BA C5BA C136 C7BA 63(3) . . . . ?
C6BA C61 C174 C68 53(3) . . . . ?
C64 C52 C59 C4BA 63(2) . . . . ?
C64 C52 C77 C28 -58(3) . . . . ?
C1CA C0CA C67 S19 -60.9(13) . . . . ?
C1CA C0CA C67 C82 61.1(11) . . . . ?
C1CA C0CA C110 C2CA -60.6(10) . . . . ?
C1CA C3CA C99 C82 -54(3) . . . . ?
C1CA C3CA C166 C2CA 59.9(15) . . . . ?
C67 C0CA C1CA C3CA -60.5(11) . . . . ?
C67 C0CA C110 C2CA 59.1(10) . . . . ?
C67 C82 C99 C3CA 55(3) . . . . ?
C70 C51 C84 C7DA -58.5(10) . . . . ?
C70 C129 C130 C7DA 59.0(9) . . . . ?
C71 C16 C51 C70 60.0(9) . . . . ?
C71 C16 C51 C84 -61.2(9) . . . . ?
C71 C4CA C129 C70 -57.2(10) . . . . ?
C71 C4CA C129 C130 62.7(9) . . . . ?
C71 C102 C7DA C84 60.7(9) . . . . ?
C71 C102 C7DA C130 -59.6(9) . . . . ?
C4CA C71 C102 C7DA 59.8(9) . . . . ?
C4CA C129 C130 C7DA -61.4(10) . . . . ?
C77 C28 C44 C4BA 57(3) . . . . ?
C77 C52 C59 C4BA -62(3) . . . . ?
C77 C52 C64 C41 54(3) . . . . ?
C2CA C80 C82 C67 -64.7(14) . . . . ?
C2CA C80 C82 C99 57.8(16) . . . . ?
C80 C2CA C110 C0CA -62.1(11) . . . . ?
C80 C2CA C166 C3CA 60.0(13) . . . . ?
C80 C82 C99 C3CA -65(3) . . . . ?
C7BA C53 C61 C6BA -53(3) . . . . ?
C7BA C53 C61 C174 58(3) . . . . ?
C84 C51 C70 C129 58.8(8) . . . . ?
C8BA C5BA C6BA C61 74(3) . . . . ?
C8BA C5BA C136 C7BA -47(3) . . . . ?
C8BA C68 C9BA C7BA 52(3) . . . . ?
C8BA C68 C174 C61 -47(3) . . . . ?
C88 C56 C58 C31 -64(2) . . . . ?
C88 C56 C58 C7AA 57(2) . . . . ?
C99 C3CA C166 C2CA -61.9(16) . . . . ?
C9BA C68 C8BA S1A 89(2) . . . . ?
C9BA C68 C8BA C5BA -54(3) . . . . ?
C9BA C68 C174 C61 65(3) . . . . ?
C9BA C7BA C136 C5BA 45(3) . . . . ?
C102 C71 C4CA C129 -62.4(10) . . . . ?
C110 C0CA C1CA C3CA 59.6(12) . . . . ?
C110 C0CA C67 S19 179.4(12) . . . . ?
C110 C0CA C67 C82 -58.6(12) . . . . ?
C110 C2CA C80 C82 64.8(13) . . . . ?
C110 C2CA C166 C3CA -60.4(14) . . . . ?
C129 C130 C7DA C84 -58.1(10) . . . . ?
C129 C130 C7DA C102 60.9(9) . . . . ?
C136 C5BA C6BA C61 -47(3) . . . . ?
C136 C5BA C8BA S1A -83(3) . . . . ?
C136 C5BA C8BA C68 55(4) . . . . ?
C136 C7BA C9BA C68 -51(3) . . . . ?
C166 C2CA C80 C82 -56.2(12) . . . . ?
C166 C2CA C110 C0CA 61.0(11) . . . . ?
C166 C3CA C99 C82 65(2) . . . . ?
C174 C61 C6BA C5BA -70(3) . . . . ?
C174 C68 C8BA S1A -164(2) . . . . ?
C174 C68 C8BA C5BA 53(4) . . . . ?
C174 C68 C9BA C7BA -62(3) . . . . ?
C4DA C1DA C5DA C8CA -61.3(10) . . . . ?
C4DA C1DA C5DA C156 59.1(10) . . . . ?
C8CA C0DA C7CA S2A -97.9(12) . . . . ?
C8CA C0DA C7CA C4DA 61.9(8) . . . . ?
C8CA C0DA C160 C2DA -59.0(8) . . . . ?
C8CA C5DA C156 C2DA 57.6(8) . . . . ?
C1DA C4DA C3DA C2DA 58.1(8) . . . . ?
C1DA C4DA C7CA S2A 82.8(19) . . . . ?
C1DA C4DA C7CA C0DA -61.0(8) . . . . ?
C1DA C5DA C156 C2DA -61.0(9) . . . . ?
C0DA C8CA C5DA C1DA 61.4(8) . . . . ?
C0DA C8CA C5DA C156 -57.7(8) . . . . ?
C3DA C2DA C156 C5DA 61.7(8) . . . . ?
C3DA C2DA C160 C0DA -60.3(7) . . . . ?
C3DA C4DA C1DA C5DA -58.5(10) . . . . ?
C3DA C4DA C7CA S2A -157.8(19) . . . . ?
C3DA C4DA C7CA C0DA 58.4(8) . . . . ?
C7CA C4DA C1DA C5DA 61.3(10) . . . . ?
C7CA C4DA C3DA C2DA -60.0(7) . . . . ?
C7CA C0DA C160 C2DA 59.1(7) . . . . ?
C5DA C8CA C0DA C7CA -61.6(8) . . . . ?
C5DA C8CA C0DA C160 58.4(8) . . . . ?
C156 C2DA C3DA C4DA -60.2(7) . . . . ?
C156 C2DA C160 C0DA 59.0(8) . . . . ?
C160 C2DA C3DA C4DA 60.4(7) . . . . ?
C160 C2DA C156 C5DA -57.9(8) . . . . ?
C160 C0DA C7CA S2A 142.3(12) . . . . ?
C160 C0DA C7CA C4DA -57.9(8) . . . . ?

