# Electronic Supplementary Material (ESI) for Dalton Transactions.
# This journal is © The Royal Society of Chemistry 2023

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
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data_IKmjs_AM17_a
_database_code_depnum_ccdc_archive 'CCDC 2224626'
loop_
_audit_author_name
_audit_author_address
'Burkhard Butschke'
;Albert Ludwigs Universitaet Freiburg
Germany
;
_audit_update_record             
;
2022-12-06 deposited with the CCDC.	2023-03-10 downloaded from the CCDC.
;
_audit_creation_method           
;FinalCif V113 by Daniel Kratzert, Freiburg 2022,
https://dkratzert.de/finalcif.html
;
_shelx_SHELXL_version_number     2018/3
_chemical_name_systematic        ?
_chemical_name_common            ?
_chemical_formula_sum            'C52 H8 Ag Al F64 O4'
_chemical_formula_moiety         'C40 Al F60 O4 1-, C12 H8 Ag F4 1+ '
_chemical_formula_weight         2047.42
_chemical_melting_point          ?
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_H-M_alt        'P 21/n'
_space_group_name_Hall           '-P 2yn'
_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;

loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'

_cell_length_a                   16.213(9)
_cell_length_b                   21.156(11)
_cell_length_c                   17.210(6)
_cell_angle_alpha                90
_cell_angle_beta                 91.208(6)
_cell_angle_gamma                90
_cell_volume                     5902(5)
_cell_formula_units_Z            4
_cell_measurement_temperature    100(2)
_cell_measurement_reflns_used    9546
_cell_measurement_theta_min      2.26
_cell_measurement_theta_max      24.699
_exptl_crystal_description       block
_exptl_crystal_colour            colourless
_exptl_crystal_recrystallization_method 
'Crystals were obtained at room temperature by slow diffusionof pentane into a solution of the compound dissolved in1,2-difluorobenzene by the aid of layering.'
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_density_diffrn    2.304
_exptl_crystal_F_000             3952
_exptl_crystal_size_max          0.240
_exptl_crystal_size_mid          0.140
_vrf_PLAT088_IKmjs_AM17_a        
;
PROBLEM: Poor Data / Parameter Ratio ....................       7.17 Note  
RESPONSE: Major parts of the asymmetric unit had to be descibed by a disorder
model, thus incresing the number of parameters. However, appropriate restraints
have been employed, which can be regarded as additional data.
;
_vrf_PLAT307_IKmjs_AM17_a        
;
PROBLEM: Isolated Metal Atom found in Structure (Unusual)        Ag1 Check 
RESPONSE: The silver atom is not isolated but weakly coordinated by two
molecules of 1,2-difluorobenzene.
;
_exptl_crystal_size_min          0.080
_exptl_absorpt_coefficient_mu    0.611
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_correction_T_min  0.703
_exptl_absorpt_correction_T_max  0.7456
_exptl_absorpt_process_details   
;
SADABS-2016/2 - Bruker AXS area detector scaling and absorption correction:
Krause, L., Herbst-Irmer, R., Sheldrick G.M. & Stalke D., J. Appl. Cryst. 48
(2015) 3-10
;
_exptl_absorpt_special_details   ?
_shelx_estimated_absorpt_T_min   0.867
_shelx_estimated_absorpt_T_max   0.953
_exptl_transmission_factor_min   ?
_exptl_transmission_factor_max   ?
_exptl_special_details           ?
_diffrn_ambient_temperature      100(2)
_diffrn_ambient_environment      N~2~
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_monochromator  'mirror optics'
_olex2_diffrn_ambient_temperature_device 'Oxford Cryostream 800'
_diffrn_measurement_ambient_temperature_device_make ?
_diffrn_radiation_probe          x-ray
_diffrn_source                   'microfocus sealed X-ray tube'
_diffrn_source_type              'Incoatec I\ms'
_diffrn_source_voltage           50.0
_diffrn_source_current           0.6
_diffrn_detector                 CCD
_diffrn_detector_type            'Bruker APEXII'
_diffrn_detector_area_resol_mean 8.3
_diffrn_measurement_device       'three-circle diffractometer'
_diffrn_measurement_device_type  'Bruker APEX2 QUAZAR'
_diffrn_measurement_method       'ω and φ scans'
_diffrn_measurement_specimen_support 'MiTeGen micromount'
_diffrn_reflns_number            225524
_diffrn_reflns_av_unetI/netI     0.0273
_diffrn_reflns_av_R_equivalents  0.0579
_diffrn_reflns_theta_min         1.525
_diffrn_reflns_theta_max         27.931
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_limit_h_min       -21
_diffrn_reflns_limit_h_max       21
_diffrn_reflns_limit_k_min       -27
_diffrn_reflns_limit_k_max       27
_diffrn_reflns_limit_l_min       -22
_diffrn_reflns_limit_l_max       22
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measured_fraction_theta_full 1.000
_diffrn_reflns_Laue_measured_fraction_max 0.999
_diffrn_reflns_Laue_measured_fraction_full 1.000
_diffrn_reflns_point_group_measured_fraction_max 0.999
_diffrn_reflns_point_group_measured_fraction_full 1.000
_reflns_number_total             14129
_reflns_number_gt                10278
_reflns_threshold_expression     'I > 2σ(I)'
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_max     .
_reflns_Friedel_fraction_full    .
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_computing_data_collection       
'Bruker BIS 2018.9.0.3/05-Dec-2018 && APEX3_2018.7-2'
_computing_cell_refinement       'SAINT V8.40B'
_computing_data_reduction        'SAINT V8.40B'
_computing_structure_solution    'SHELXT 2018/2 (Sheldrick, 2018)'
_computing_structure_refinement  'SHELXL-2018/3 (Sheldrick, 2018)'
_computing_molecular_graphics    ?
_computing_publication_material  ?
_refine_special_details          ?
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0448P)²+15.2814P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   ?
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    constr
_refine_ls_number_reflns         14129
_refine_ls_number_parameters     1971
_refine_ls_number_restraints     20713
_refine_ls_R_factor_all          0.0800
_refine_ls_R_factor_gt           0.0517
_refine_ls_wR_factor_ref         0.1383
_refine_ls_wR_factor_gt          0.1227
_refine_ls_goodness_of_fit_ref   1.105
_refine_ls_restrained_S_all      0.753
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_diff_density_max         0.873
_refine_diff_density_min         -0.870
_refine_diff_density_rms         0.085
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       .

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Al Al 0.0645 0.0514 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1 Ag 0.76780(9) 0.65969(8) 0.48800(12) 0.0555(5) Uani 0.674(3) 1 d . U P A 3
Ag2 Ag 0.7572(3) 0.6341(3) 0.5083(3) 0.0853(16) Uani 0.232(3) 1 d . U P A 4
Ag3 Ag 0.7532(5) 0.6772(6) 0.4535(7) 0.083(2) Uani 0.094(3) 1 d . U P A 5
C1_1 C 0.5686(4) 0.6917(3) 0.4673(3) 0.0344(11) Uani 0.874(6) 1 d D U P A 1
C2_1 C 0.5577(3) 0.6435(3) 0.5192(3) 0.0391(11) Uani 0.874(6) 1 d D U P A 1
C3_1 C 0.6088(4) 0.6383(3) 0.5836(3) 0.0495(13) Uani 0.874(6) 1 d D U P A 1
H3_1 H 0.602274 0.604490 0.619230 0.059 Uiso 0.874(6) 1 calc R U P A 1
C4_1 C 0.6698(4) 0.6831(3) 0.5956(4) 0.0493(14) Uani 0.874(6) 1 d D U P A 1
H4_1 H 0.704779 0.680217 0.640500 0.059 Uiso 0.874(6) 1 calc R U P A 1
C5_1 C 0.6810(4) 0.7320(3) 0.5434(4) 0.0475(14) Uani 0.874(6) 1 d D U P A 1
H5_1 H 0.723206 0.762398 0.552173 0.057 Uiso 0.874(6) 1 calc R U P A 1
C6_1 C 0.6299(4) 0.7359(3) 0.4786(3) 0.0420(13) Uani 0.874(6) 1 d D U P A 1
H6_1 H 0.637015 0.768868 0.441861 0.050 Uiso 0.874(6) 1 calc R U P A 1
F1_1 F 0.52296(18) 0.69789(16) 0.40395(17) 0.0548(10) Uani 0.874(6) 1 d D U P A
1
F2_1 F 0.4972(4) 0.6022(3) 0.5044(4) 0.080(2) Uani 0.874(6) 1 d D U P A 1
C1_2 C 0.606(2) 0.6299(14) 0.5693(17) 0.048(4) Uani 0.126(6) 1 d D U P A 2
C2_2 C 0.560(2) 0.6478(15) 0.5050(18) 0.045(4) Uani 0.126(6) 1 d D U P A 2
C3_2 C 0.579(3) 0.7039(17) 0.469(2) 0.043(4) Uani 0.126(6) 1 d D U P A 2
H3_2 H 0.549270 0.717241 0.424406 0.051 Uiso 0.126(6) 1 calc R U P A 2
C4_2 C 0.642(3) 0.7406(16) 0.499(2) 0.043(4) Uani 0.126(6) 1 d D U P A 2
H4_2 H 0.654570 0.779845 0.475372 0.051 Uiso 0.126(6) 1 calc R U P A 2
C5_2 C 0.688(3) 0.7215(18) 0.564(3) 0.047(4) Uani 0.126(6) 1 d D U P A 2
H5_2 H 0.731676 0.747413 0.583547 0.056 Uiso 0.126(6) 1 calc R U P A 2
C6_2 C 0.671(3) 0.6648(18) 0.599(2) 0.048(4) Uani 0.126(6) 1 d D U P A 2
H6_2 H 0.702785 0.650132 0.641809 0.057 Uiso 0.126(6) 1 calc R U P A 2
F1_2 F 0.5908(17) 0.5778(13) 0.6049(16) 0.085(7) Uani 0.126(6) 1 d D U P A 2
F2_2 F 0.502(2) 0.6091(17) 0.481(2) 0.050(5) Uani 0.126(6) 1 d D U P A 2
C1_3 C 0.6494(4) 0.5758(4) 0.3455(5) 0.0486(17) Uani 0.687(8) 1 d D U P A 1
C2_3 C 0.6794(4) 0.5346(3) 0.4006(5) 0.0404(16) Uani 0.687(8) 1 d D U P A 1
C3_3 C 0.7593(5) 0.5388(4) 0.4296(6) 0.0321(17) Uani 0.687(8) 1 d D U P A 1
H3_3 H 0.778942 0.509802 0.467841 0.039 Uiso 0.687(8) 1 calc R U P A 1
C4_3 C 0.8105(4) 0.5863(3) 0.4022(4) 0.0246(13) Uani 0.687(8) 1 d D U P A 1
H4_3 H 0.865671 0.590059 0.421213 0.029 Uiso 0.687(8) 1 calc R U P A 1
C5_3 C 0.7798(5) 0.6278(3) 0.3468(4) 0.0413(16) Uani 0.687(8) 1 d D U P A 1
H5_3 H 0.814294 0.660465 0.327879 0.050 Uiso 0.687(8) 1 calc R U P A 1
C6_3 C 0.6986(5) 0.6226(5) 0.3180(5) 0.057(2) Uani 0.687(8) 1 d D U P A 1
H6_3 H 0.678112 0.651356 0.279790 0.068 Uiso 0.687(8) 1 calc R U P A 1
F1_3 F 0.5728(3) 0.5678(4) 0.3214(4) 0.098(3) Uani 0.687(8) 1 d D U P A 1
F2_3 F 0.6309(3) 0.4902(2) 0.4277(4) 0.087(2) Uani 0.687(8) 1 d D U P A 1
C1_4 C 0.6585(9) 0.5968(9) 0.3262(9) 0.059(4) Uani 0.313(8) 1 d D U P A 2
C2_4 C 0.6379(9) 0.5494(7) 0.3778(8) 0.061(4) Uani 0.313(8) 1 d D U P A 2
C3_4 C 0.6962(11) 0.5275(8) 0.4290(9) 0.055(5) Uani 0.313(8) 1 d D U P A 2
H3_4 H 0.682240 0.497184 0.467308 0.065 Uiso 0.313(8) 1 calc R U P A 2
C4_4 C 0.7757(11) 0.5497(12) 0.4247(15) 0.055(5) Uani 0.313(8) 1 d D U P A 2
H4_4 H 0.817890 0.530699 0.455882 0.066 Uiso 0.313(8) 1 calc R U P A 2
C5_4 C 0.7954(10) 0.5993(10) 0.3760(11) 0.053(5) Uani 0.313(8) 1 d D U P A 2
H5_4 H 0.849525 0.616575 0.377159 0.064 Uiso 0.313(8) 1 calc R U P A 2
C6_4 C 0.7358(10) 0.6235(10) 0.3256(11) 0.066(5) Uani 0.313(8) 1 d D U P A 2
H6_4 H 0.747888 0.657513 0.291605 0.079 Uiso 0.313(8) 1 calc R U P A 2
F1_4 F 0.5988(9) 0.6147(7) 0.2793(6) 0.100(5) Uani 0.313(8) 1 d D U P A 2
F2_4 F 0.5609(9) 0.5279(8) 0.3778(11) 0.128(6) Uani 0.313(8) 1 d D U P A 2
Al1 Al 0.14620(5) 0.74998(4) 0.45800(5) 0.01075(17) Uani 1 1 d D . . . .
O1_5 O 0.0593(2) 0.77159(15) 0.40228(19) 0.0181(8) Uani 0.648(4) 1 d D U P B 1
C1_5 C 0.0049(3) 0.8170(2) 0.3814(3) 0.0152(8) Uani 0.648(4) 1 d D U P B 1
C2_5 C -0.0713(3) 0.7851(2) 0.3418(3) 0.0218(9) Uani 0.648(4) 1 d D U P B 1
F1_5 F -0.0477(3) 0.75016(16) 0.28081(19) 0.0337(9) Uani 0.648(4) 1 d D U P B 1
F2_5 F -0.1069(2) 0.74381(14) 0.3913(2) 0.0347(9) Uani 0.648(4) 1 d D U P B 1
C3_5 C 0.0413(3) 0.8639(2) 0.3223(3) 0.0192(9) Uani 0.648(4) 1 d D U P B 1
F3_5 F 0.0688(3) 0.8321(2) 0.2595(2) 0.0324(9) Uani 0.648(4) 1 d D U P B 1
F4_5 F 0.10704(18) 0.89373(19) 0.3536(2) 0.0296(8) Uani 0.648(4) 1 d D U P B 1
C4_5 C -0.0273(4) 0.8565(3) 0.4513(4) 0.0192(11) Uani 0.648(4) 1 d D U P B 1
F5_5 F 0.0357(2) 0.8852(2) 0.4885(2) 0.0259(8) Uani 0.648(4) 1 d D U P B 1
F6_5 F -0.0616(4) 0.8181(3) 0.5041(4) 0.0306(12) Uani 0.648(4) 1 d D U P B 1
C5_5 C -0.0917(4) 0.9067(3) 0.4240(5) 0.0216(11) Uani 0.648(4) 1 d D U P B 1
F7_5 F -0.1175(8) 0.9415(7) 0.4855(7) 0.039(2) Uani 0.648(4) 1 d D U P B 1
C6_5 C -0.0528(4) 0.9520(3) 0.3644(4) 0.0235(12) Uani 0.648(4) 1 d D U P B 1
F8_5 F 0.0103(3) 0.98306(19) 0.3983(3) 0.0350(9) Uani 0.648(4) 1 d D U P B 1
F9_5 F -0.1078(3) 0.9962(3) 0.3413(4) 0.0325(11) Uani 0.648(4) 1 d D U P B 1
C7_5 C -0.0234(4) 0.9136(3) 0.2939(4) 0.0212(11) Uani 0.648(4) 1 d D U P B 1
F10_5 F 0.0115(4) 0.9529(4) 0.2422(5) 0.0373(14) Uani 0.648(4) 1 d D U P B 1
C8_5 C -0.0980(5) 0.8794(4) 0.2556(4) 0.0251(13) Uani 0.648(4) 1 d D U P B 1
F11_5 F -0.0749(5) 0.8473(6) 0.1923(5) 0.041(2) Uani 0.648(4) 1 d D U P B 1
F12_5 F -0.1552(7) 0.9212(4) 0.2299(7) 0.034(2) Uani 0.648(4) 1 d D U P B 1
C9_5 C -0.1362(3) 0.8341(3) 0.3147(3) 0.0226(10) Uani 0.648(4) 1 d D U P B 1
F13_5 F -0.2023(3) 0.80298(19) 0.2816(3) 0.0423(11) Uani 0.648(4) 1 d D U P B 1
C10_5 C -0.1658(4) 0.8730(3) 0.3848(4) 0.0226(11) Uani 0.648(4) 1 d D U P B 1
F14_5 F -0.2034(3) 0.8345(2) 0.4362(3) 0.0398(11) Uani 0.648(4) 1 d D U P B 1
F15_5 F -0.2244(3) 0.9145(2) 0.3624(3) 0.0326(11) Uani 0.648(4) 1 d D U P B 1
O1_6 O 0.1008(3) 0.8101(3) 0.4061(3) 0.0165(14) Uani 0.352(4) 1 d D U P B 2
C1_6 C 0.0302(5) 0.8391(4) 0.3816(5) 0.0147(13) Uani 0.352(4) 1 d D U P B 2
C2_6 C -0.0148(6) 0.8726(5) 0.4495(6) 0.0223(19) Uani 0.352(4) 1 d D U P B 2
F1_6 F -0.0358(7) 0.8310(6) 0.5042(7) 0.034(2) Uani 0.352(4) 1 d D U P B 2
F2_6 F 0.0351(5) 0.9150(4) 0.4850(5) 0.039(2) Uani 0.352(4) 1 d D U P B 2
C3_6 C -0.0311(5) 0.7918(3) 0.3431(5) 0.0182(14) Uani 0.352(4) 1 d D U P B 2
F3_6 F -0.0521(4) 0.7461(2) 0.3938(3) 0.0293(14) Uani 0.352(4) 1 d D U P B 2
F4_6 F 0.0043(5) 0.7619(3) 0.2835(3) 0.0320(15) Uani 0.352(4) 1 d D U P B 2
C4_6 C 0.0509(5) 0.8902(4) 0.3208(5) 0.0195(15) Uani 0.352(4) 1 d D U P B 2
F5_6 F 0.0905(4) 0.8642(4) 0.2615(4) 0.0305(15) Uani 0.352(4) 1 d D U P B 2
F6_6 F 0.1031(3) 0.9331(3) 0.3528(4) 0.0326(15) Uani 0.352(4) 1 d D U P B 2
C5_6 C -0.0283(7) 0.9244(5) 0.2908(7) 0.0209(16) Uani 0.352(4) 1 d D U P B 2
F7_6 F -0.0071(8) 0.9674(6) 0.2365(9) 0.037(3) Uani 0.352(4) 1 d D U P B 2
C6_6 C -0.0867(8) 0.8756(6) 0.2522(7) 0.0207(18) Uani 0.352(4) 1 d D U P B 2
F8_6 F -0.0509(9) 0.8486(10) 0.1908(9) 0.032(3) Uani 0.352(4) 1 d D U P B 2
F9_6 F -0.1541(11) 0.9052(8) 0.2227(12) 0.029(3) Uani 0.352(4) 1 d D U P B 2
C7_6 C -0.1102(5) 0.8254(4) 0.3130(6) 0.0194(15) Uani 0.352(4) 1 d D U P B 2
F10_6 F -0.1640(5) 0.7835(3) 0.2794(4) 0.0359(17) Uani 0.352(4) 1 d D U P B 2
C8_6 C -0.1533(6) 0.8579(5) 0.3808(6) 0.0223(17) Uani 0.352(4) 1 d D U P B 2
F11_6 F -0.1777(5) 0.8149(5) 0.4338(6) 0.040(2) Uani 0.352(4) 1 d D U P B 2
F12_6 F -0.2232(5) 0.8875(4) 0.3562(6) 0.0307(19) Uani 0.352(4) 1 d D U P B 2
C9_6 C -0.0945(7) 0.9066(6) 0.4199(8) 0.0234(16) Uani 0.352(4) 1 d D U P B 2
F13_6 F -0.1334(14) 0.9332(12) 0.4811(11) 0.034(3) Uani 0.352(4) 1 d D U P B 2
C10_6 C -0.0709(7) 0.9569(5) 0.3596(7) 0.0234(18) Uani 0.352(4) 1 d D U P B 2
F14_6 F -0.0214(5) 1.0015(3) 0.3907(6) 0.044(2) Uani 0.352(4) 1 d D U P B 2
F15_6 F -0.1379(5) 0.9881(5) 0.3326(7) 0.034(2) Uani 0.352(4) 1 d D U P B 2
O1_7 O 0.2119(2) 0.81166(16) 0.46375(18) 0.0159(8) Uani 0.631(5) 1 d D U P B 1
C1_7 C 0.2756(3) 0.8415(2) 0.5008(3) 0.0122(8) Uani 0.631(5) 1 d D U P B 1
C2_7 C 0.3429(3) 0.7948(2) 0.5315(3) 0.0137(9) Uani 0.631(5) 1 d D U P B 1
F1_7 F 0.3099(2) 0.75332(13) 0.58171(19) 0.0224(8) Uani 0.631(5) 1 d D U P B 1
F2_7 F 0.3719(2) 0.75932(14) 0.4733(2) 0.0220(7) Uani 0.631(5) 1 d D U P B 1
C3_7 C 0.2453(4) 0.8815(2) 0.5708(3) 0.0137(10) Uani 0.631(5) 1 d D U P B 1
F3_7 F 0.2084(2) 0.8440(2) 0.6225(2) 0.0219(8) Uani 0.631(5) 1 d D U P B 1
F4_7 F 0.1879(2) 0.92307(19) 0.5466(2) 0.0217(8) Uani 0.631(5) 1 d D U P B 1
C4_7 C 0.3179(3) 0.8872(2) 0.4429(3) 0.0145(10) Uani 0.631(5) 1 d D U P B 1
F5_7 F 0.26292(19) 0.9292(2) 0.41420(18) 0.0221(7) Uani 0.631(5) 1 d D U P B 1
F6_7 F 0.3454(3) 0.8548(2) 0.3813(2) 0.0218(9) Uani 0.631(5) 1 d D U P B 1
C5_7 C 0.3907(4) 0.9230(3) 0.4824(4) 0.0159(11) Uani 0.631(5) 1 d D U P B 1
F7_7 F 0.4247(7) 0.9628(5) 0.4297(5) 0.0277(17) Uani 0.631(5) 1 d D U P B 1
C6_7 C 0.3581(4) 0.9620(3) 0.5515(4) 0.0159(12) Uani 0.631(5) 1 d D U P B 1
F8_7 F 0.3038(3) 1.00567(19) 0.5258(3) 0.0249(9) Uani 0.631(5) 1 d D U P B 1
F9_7 F 0.4201(3) 0.9943(3) 0.5862(4) 0.0246(11) Uani 0.631(5) 1 d D U P B 1
C7_7 C 0.3183(4) 0.9173(3) 0.6107(5) 0.0153(11) Uani 0.631(5) 1 d D U P B 1
F10_7 F 0.2913(11) 0.9516(8) 0.6721(8) 0.026(2) Uani 0.631(5) 1 d D U P B 1
C8_7 C 0.3831(4) 0.8688(3) 0.6404(4) 0.0187(11) Uani 0.631(5) 1 d D U P B 1
F11_7 F 0.3499(3) 0.8300(2) 0.6930(2) 0.0261(9) Uani 0.631(5) 1 d D U P B 1
F12_7 F 0.4456(3) 0.8987(2) 0.6781(3) 0.0267(10) Uani 0.631(5) 1 d D U P B 1
C9_7 C 0.4153(3) 0.8301(2) 0.5718(3) 0.0156(10) Uani 0.631(5) 1 d D U P B 1
F13_7 F 0.4735(2) 0.78821(18) 0.5984(2) 0.0274(8) Uani 0.631(5) 1 d D U P B 1
C10_7 C 0.4554(4) 0.8749(4) 0.5126(5) 0.0179(12) Uani 0.631(5) 1 d D U P B 1
F14_7 F 0.4860(6) 0.8413(6) 0.4530(7) 0.0247(17) Uani 0.631(5) 1 d D U P B 1
F15_7 F 0.5203(4) 0.9051(3) 0.5457(5) 0.0253(13) Uani 0.631(5) 1 d D U P B 1
O1_8 O 0.2454(3) 0.7754(3) 0.4891(3) 0.0186(14) Uani 0.369(5) 1 d D U P B 2
C1_8 C 0.2977(5) 0.8213(4) 0.5159(4) 0.0112(12) Uani 0.369(5) 1 d D U P B 2
C2_8 C 0.3758(5) 0.7900(3) 0.5521(4) 0.0139(13) Uani 0.369(5) 1 d D U P B 2
F1_8 F 0.3563(4) 0.7512(2) 0.6106(3) 0.0249(13) Uani 0.369(5) 1 d D U P B 2
F2_8 F 0.4124(4) 0.7527(2) 0.4992(4) 0.0225(12) Uani 0.369(5) 1 d D U P B 2
C3_8 C 0.2589(5) 0.8632(4) 0.5797(5) 0.0153(15) Uani 0.369(5) 1 d D U P B 2
F3_8 F 0.2352(4) 0.8277(4) 0.6403(4) 0.0243(15) Uani 0.369(5) 1 d D U P B 2
F4_8 F 0.1900(4) 0.8920(4) 0.5529(4) 0.0222(13) Uani 0.369(5) 1 d D U P B 2
C4_8 C 0.3238(5) 0.8658(4) 0.4492(5) 0.0139(15) Uani 0.369(5) 1 d D U P B 2
F5_8 F 0.2586(3) 0.8942(3) 0.4157(3) 0.0213(12) Uani 0.369(5) 1 d D U P B 2
F6_8 F 0.3595(6) 0.8314(4) 0.3924(5) 0.0255(17) Uani 0.369(5) 1 d D U P B 2
C5_8 C 0.3868(7) 0.9159(5) 0.4783(7) 0.0144(15) Uani 0.369(5) 1 d D U P B 2
F7_8 F 0.4113(11) 0.9531(7) 0.4184(9) 0.024(3) Uani 0.369(5) 1 d D U P B 2
C6_8 C 0.3467(7) 0.9569(5) 0.5415(7) 0.0160(17) Uani 0.369(5) 1 d D U P B 2
F8_8 F 0.2805(5) 0.9876(3) 0.5115(5) 0.0254(15) Uani 0.369(5) 1 d D U P B 2
F9_8 F 0.3988(6) 1.0021(5) 0.5668(7) 0.0261(19) Uani 0.369(5) 1 d D U P B 2
C7_8 C 0.3211(7) 0.9142(5) 0.6098(7) 0.0159(16) Uani 0.369(5) 1 d D U P B 2
F10_8 F 0.2854(18) 0.9498(13) 0.6656(14) 0.025(3) Uani 0.369(5) 1 d D U P B 2
C8_8 C 0.3988(6) 0.8811(5) 0.6441(6) 0.0162(16) Uani 0.369(5) 1 d D U P B 2
F11_8 F 0.3796(5) 0.8456(4) 0.7059(4) 0.0283(16) Uani 0.369(5) 1 d D U P B 2
F12_8 F 0.4530(5) 0.9242(4) 0.6718(5) 0.0250(17) Uani 0.369(5) 1 d D U P B 2
C9_8 C 0.4384(5) 0.8401(4) 0.5812(5) 0.0153(14) Uani 0.369(5) 1 d D U P B 2
F13_8 F 0.5067(4) 0.8104(3) 0.6118(4) 0.0251(13) Uani 0.369(5) 1 d D U P B 2
C10_8 C 0.4640(7) 0.8833(6) 0.5136(7) 0.0155(16) Uani 0.369(5) 1 d D U P B 2
F14_8 F 0.5021(11) 0.8498(10) 0.4584(11) 0.023(3) Uani 0.369(5) 1 d D U P B 2
F15_8 F 0.5206(8) 0.9251(4) 0.5392(9) 0.0211(19) Uani 0.369(5) 1 d D U P B 2
O1_9 O 0.1926(6) 0.6840(5) 0.4206(5) 0.0126(15) Uani 0.405(16) 1 d D U P B 1
C1_9 C 0.2158(6) 0.6524(5) 0.3570(6) 0.0144(10) Uani 0.405(16) 1 d D U P B 1
C2_9 C 0.2863(7) 0.6049(5) 0.3798(7) 0.0170(12) Uani 0.405(16) 1 d D U P B 1
F1_9 F 0.3498(7) 0.6360(4) 0.4136(7) 0.0201(16) Uani 0.405(16) 1 d D U P B 1
F2_9 F 0.2578(12) 0.5636(7) 0.4328(9) 0.021(2) Uani 0.405(16) 1 d D U P B 1
C3_9 C 0.2499(7) 0.6968(5) 0.2930(6) 0.0155(12) Uani 0.405(16) 1 d D U P B 1
F3_9 F 0.3139(7) 0.7310(6) 0.3221(8) 0.0169(15) Uani 0.405(16) 1 d D U P B 1
F4_9 F 0.1921(6) 0.7388(5) 0.2700(6) 0.0191(15) Uani 0.405(16) 1 d D U P B 1
C4_9 C 0.1440(6) 0.6134(5) 0.3187(6) 0.0170(12) Uani 0.405(16) 1 d D U P B 1
F5_9 F 0.0810(5) 0.6510(5) 0.2971(6) 0.0215(15) Uani 0.405(16) 1 d D U P B 1
F6_9 F 0.1110(12) 0.5737(7) 0.3712(10) 0.023(2) Uani 0.405(16) 1 d D U P B 1
C5_9 C 0.1738(7) 0.5748(5) 0.2482(6) 0.0210(12) Uani 0.405(16) 1 d D U P B 1
F7_9 F 0.1104(6) 0.5404(5) 0.2164(5) 0.0297(18) Uani 0.405(16) 1 d D U P B 1
C6_9 C 0.2075(7) 0.6200(5) 0.1864(6) 0.0228(14) Uani 0.405(16) 1 d D U P B 1
F8_9 F 0.1459(6) 0.6589(5) 0.1619(5) 0.0273(16) Uani 0.405(16) 1 d D U P B 1
F9_9 F 0.2304(8) 0.5889(6) 0.1223(5) 0.034(2) Uani 0.405(16) 1 d D U P B 1
C7_9 C 0.2797(7) 0.6590(6) 0.2217(7) 0.0200(11) Uani 0.405(16) 1 d D U P B 1
F10_9 F 0.3056(15) 0.6999(10) 0.1662(12) 0.026(2) Uani 0.405(16) 1 d D U P B 1
C8_9 C 0.3496(7) 0.6138(6) 0.2470(7) 0.0212(14) Uani 0.405(16) 1 d D U P B 1
F11_9 F 0.4157(9) 0.6453(6) 0.2759(10) 0.0243(19) Uani 0.405(16) 1 d D U P B 1
F12_9 F 0.3771(8) 0.5805(6) 0.1855(7) 0.028(2) Uani 0.405(16) 1 d D U P B 1
C9_9 C 0.3169(7) 0.5673(5) 0.3091(7) 0.0211(12) Uani 0.405(16) 1 d D U P B 1
F13_9 F 0.3778(7) 0.5274(5) 0.3321(8) 0.0337(19) Uani 0.405(16) 1 d D U P B 1
C10_9 C 0.2433(7) 0.5295(5) 0.2737(6) 0.0235(13) Uani 0.405(16) 1 d D U P B 1
F14_9 F 0.2161(8) 0.4874(6) 0.3269(8) 0.030(2) Uani 0.405(16) 1 d D U P B 1
F15_9 F 0.2693(8) 0.4948(5) 0.2132(6) 0.035(2) Uani 0.405(16) 1 d D U P B 1
O1_10 O 0.1702(6) 0.6840(3) 0.4051(5) 0.0263(16) Uani 0.595(16) 1 d D U P B 2
C1_10 C 0.2091(5) 0.6517(4) 0.3492(5) 0.0176(9) Uani 0.595(16) 1 d D U P B 2
C2_10 C 0.1487(4) 0.6027(3) 0.3113(4) 0.0168(9) Uani 0.595(16) 1 d D U P B 2
F1_10 F 0.1212(8) 0.5634(5) 0.3675(6) 0.0200(15) Uani 0.595(16) 1 d D U P B 2
F2_10 F 0.0819(4) 0.6328(4) 0.2811(5) 0.0275(13) Uani 0.595(16) 1 d D U P B 2
C3_10 C 0.2842(5) 0.6142(4) 0.3828(5) 0.0182(10) Uani 0.595(16) 1 d D U P B 2
F3_10 F 0.2620(8) 0.5754(5) 0.4416(6) 0.0223(16) Uani 0.595(16) 1 d D U P B 2
F4_10 F 0.3401(5) 0.6539(4) 0.4150(5) 0.0292(16) Uani 0.595(16) 1 d D U P B 2
C4_10 C 0.2421(6) 0.6943(4) 0.2823(5) 0.0198(11) Uani 0.595(16) 1 d D U P B 2
F5_10 F 0.2952(6) 0.7376(4) 0.3109(6) 0.0275(15) Uani 0.595(16) 1 d D U P B 2
F6_10 F 0.1793(5) 0.7279(3) 0.2497(5) 0.0296(14) Uani 0.595(16) 1 d D U P B 2
C5_10 C 0.2846(5) 0.6543(4) 0.2190(5) 0.0168(8) Uani 0.595(16) 1 d D U P B 2
F7_10 F 0.3136(10) 0.6926(6) 0.1618(8) 0.0237(17) Uani 0.595(16) 1 d D U P B 2
C6_10 C 0.3586(5) 0.6178(4) 0.2555(5) 0.0184(10) Uani 0.595(16) 1 d D U P B 2
F8_10 F 0.4138(6) 0.6589(5) 0.2848(6) 0.0264(15) Uani 0.595(16) 1 d D U P B 2
F9_10 F 0.3973(5) 0.5849(4) 0.2004(4) 0.0250(13) Uani 0.595(16) 1 d D U P B 2
C7_10 C 0.3265(4) 0.5740(4) 0.3198(4) 0.0171(9) Uani 0.595(16) 1 d D U P B 2
F10_10 F 0.3906(4) 0.5405(4) 0.3519(4) 0.0305(14) Uani 0.595(16) 1 d D U P B 2
C8_10 C 0.2639(4) 0.5266(3) 0.2845(4) 0.0170(9) Uani 0.595(16) 1 d D U P B 2
F11_10 F 0.2383(5) 0.4859(4) 0.3392(5) 0.0243(13) Uani 0.595(16) 1 d D U P B 2
F12_10 F 0.2991(5) 0.4901(3) 0.2306(3) 0.0271(12) Uani 0.595(16) 1 d D U P B 2
C9_10 C 0.1900(4) 0.5630(3) 0.2479(4) 0.0161(9) Uani 0.595(16) 1 d D U P B 2
F13_10 F 0.1349(4) 0.5219(3) 0.2158(4) 0.0264(12) Uani 0.595(16) 1 d D U P B 2
C10_10 C 0.2215(4) 0.6070(3) 0.1835(4) 0.0179(10) Uani 0.595(16) 1 d D U P B 2
F14_10 F 0.1587(4) 0.6385(4) 0.1490(4) 0.0290(13) Uani 0.595(16) 1 d D U P B 2
F15_10 F 0.2562(5) 0.5735(3) 0.1268(3) 0.0237(11) Uani 0.595(16) 1 d D U P B 2
O1_11 O 0.10441(17) 0.73186(11) 0.54586(15) 0.0334(6) Uani 1 1 d D U . . .
C1_11 C 0.07346(18) 0.68953(14) 0.59563(17) 0.0190(6) Uani 1 1 d D U . . .
C2_11 C 0.03889(18) 0.72444(14) 0.66791(18) 0.0201(6) Uani 1 1 d D U . . .
F1_11 F 0.09906(13) 0.75886(9) 0.70299(12) 0.0334(5) Uani 1 1 d D U . . .
F2_11 F -0.02025(13) 0.76559(8) 0.64622(11) 0.0282(4) Uani 1 1 d D U . . .
C3_11 C 0.14033(18) 0.64182(15) 0.62525(19) 0.0236(7) Uani 1 1 d D U . . .
F3_11 F 0.20404(12) 0.67317(11) 0.65831(13) 0.0375(5) Uani 1 1 d D U . . .
F4_11 F 0.17164(12) 0.60978(9) 0.56514(12) 0.0309(5) Uani 1 1 d D U . . .
C4_11 C 0.00115(18) 0.65016(14) 0.55946(17) 0.0183(6) Uani 1 1 d D U . . .
F5_11 F 0.02638(12) 0.61885(9) 0.49591(10) 0.0265(4) Uani 1 1 d D U . . .
F6_11 F -0.06072(12) 0.68832(9) 0.53391(11) 0.0282(4) Uani 1 1 d D U . . .
C5_11 C -0.03410(17) 0.60271(13) 0.61871(16) 0.0159(6) Uani 1 1 d D U . . .
F7_11 F -0.09734(11) 0.56955(9) 0.58356(11) 0.0264(4) Uani 1 1 d D U . . .
C6_11 C 0.03422(18) 0.55667(14) 0.64609(17) 0.0188(6) Uani 1 1 d D U . . .
F8_11 F 0.06122(12) 0.52330(9) 0.58465(11) 0.0279(4) Uani 1 1 d D U . . .
F9_11 F 0.00483(12) 0.51419(8) 0.69599(11) 0.0270(4) Uani 1 1 d D U . . .
C7_11 C 0.10521(18) 0.59435(15) 0.68460(18) 0.0212(6) Uani 1 1 d D U . . .
F10_11 F 0.16515(12) 0.55356(10) 0.70901(13) 0.0346(5) Uani 1 1 d D U . . .
C8_11 C 0.07181(18) 0.63105(15) 0.75501(17) 0.0220(6) Uani 1 1 d D U . . .
F11_11 F 0.13286(12) 0.66311(11) 0.79161(12) 0.0371(5) Uani 1 1 d D U . . .
F12_11 F 0.04271(13) 0.59063(10) 0.80797(11) 0.0302(5) Uani 1 1 d D U . . .
C9_11 C 0.00329(18) 0.67749(14) 0.72733(16) 0.0172(6) Uani 1 1 d D U . . .
F13_11 F -0.02585(12) 0.70939(9) 0.78946(10) 0.0256(4) Uani 1 1 d D U . . .
C10_11 C -0.06755(17) 0.63902(14) 0.68908(16) 0.0161(6) Uani 1 1 d D U . . .
F14_11 F -0.12983(11) 0.67752(9) 0.66591(11) 0.0250(4) Uani 1 1 d D U . . .
F15_11 F -0.10022(11) 0.59879(9) 0.73997(11) 0.0228(4) Uani 1 1 d D U . . .


loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag1 C4_3 2.261(7) . ?
Ag1 C5_2 2.27(6) . ?
Ag1 C5_1 2.299(8) . ?
Ag1 C5_4 2.36(2) . ?
Ag1 C6_2 2.50(5) . ?
Ag1 C4_1 2.514(8) . ?
Ag1 C5_3 2.534(7) . ?
Ag1 C4_4 2.57(3) . ?
Ag1 C4_2 2.67(5) . ?
Ag1 C3_3 2.749(11) . ?
Ag1 C6_1 2.758(7) . ?
Ag1 C6_4 2.93(2) . ?
Ag2 C6_2 2.21(6) . ?
Ag2 C4_3 2.274(9) . ?
Ag2 C4_4 2.32(3) . ?
Ag2 C4_1 2.329(9) . ?
Ag2 C5_2 2.37(5) . ?
Ag2 C3_3 2.429(13) . ?
Ag2 C5_4 2.48(2) . ?
Ag2 C5_1 2.492(9) . ?
Ag2 C1_2 2.69(4) . ?
Ag2 C3_1 2.758(9) . ?
Ag2 C3_4 2.805(18) . ?
Ag2 C5_3 2.816(9) . ?
Ag3 C5_3 2.164(11) . ?
Ag3 C5_4 2.24(2) . ?
Ag3 C5_1 2.277(11) . ?
Ag3 C4_3 2.319(12) . ?
Ag3 C5_2 2.38(6) . ?
Ag3 C4_2 2.39(5) . ?
Ag3 C6_1 2.399(12) . ?
Ag3 C6_4 2.49(2) . ?
Ag3 C6_3 2.732(14) . ?
Ag3 C4_4 2.77(3) . ?
Ag3 C4_1 2.822(12) . ?
Ag3 C6_2 2.87(5) . ?
C1_1 F1_1 1.312(5) . ?
C1_1 C2_1 1.369(6) . ?
C1_1 C6_1 1.374(6) . ?
C2_1 F2_1 1.333(6) . ?
C2_1 C3_1 1.374(6) . ?
C3_1 C4_1 1.382(7) . ?
C3_1 H3_1 0.9500 . ?
C4_1 C5_1 1.385(8) . ?
C4_1 H4_1 0.9500 . ?
C5_1 C6_1 1.378(7) . ?
C5_1 H5_1 0.9500 . ?
C6_1 H6_1 0.9500 . ?
C1_2 F1_2 1.285(15) . ?
C1_2 C2_2 1.371(13) . ?
C1_2 C6_2 1.375(14) . ?
C2_2 F2_2 1.315(14) . ?
C2_2 C3_2 1.373(13) . ?
C3_2 C4_2 1.374(14) . ?
C3_2 H3_2 0.9500 . ?
C4_2 C5_2 1.380(14) . ?
C4_2 H4_2 0.9500 . ?
C5_2 C6_2 1.375(14) . ?
C5_2 H5_2 0.9500 . ?
C6_2 H6_2 0.9500 . ?
C1_3 F1_3 1.311(7) . ?
C1_3 C6_3 1.363(9) . ?
C1_3 C2_3 1.370(9) . ?
C2_3 F2_3 1.316(7) . ?
C2_3 C3_3 1.382(8) . ?
C3_3 C4_3 1.392(7) . ?
C3_3 H3_3 0.9500 . ?
C4_3 C5_3 1.382(8) . ?
C4_3 H4_3 0.9500 . ?
C5_3 C6_3 1.401(9) . ?
C5_3 H5_3 0.9500 . ?
C6_3 H6_3 0.9500 . ?
C1_4 F1_4 1.303(12) . ?
C1_4 C6_4 1.375(13) . ?
C1_4 C2_4 1.386(12) . ?
C2_4 F2_4 1.329(13) . ?
C2_4 C3_4 1.360(12) . ?
C3_4 C4_4 1.374(13) . ?
C3_4 H3_4 0.9500 . ?
C4_4 C5_4 1.385(13) . ?
C4_4 H4_4 0.9500 . ?
C5_4 C6_4 1.383(13) . ?
C5_4 H5_4 0.9500 . ?
C6_4 H6_4 0.9500 . ?
Al1 O1_7 1.686(3) . ?
Al1 O1_6 1.711(5) . ?
Al1 O1_11 1.713(2) . ?
Al1 O1_10 1.715(5) . ?
Al1 O1_9 1.717(7) . ?
Al1 O1_5 1.748(3) . ?
Al1 O1_8 1.767(5) . ?
O1_5 C1_5 1.347(5) . ?
C1_5 C3_5 1.547(6) . ?
C1_5 C2_5 1.553(6) . ?
C1_5 C4_5 1.564(7) . ?
C2_5 F1_5 1.345(6) . ?
C2_5 F2_5 1.358(6) . ?
C2_5 C9_5 1.542(6) . ?
C3_5 F4_5 1.342(6) . ?
C3_5 F3_5 1.355(6) . ?
C3_5 C7_5 1.558(7) . ?
C4_5 F5_5 1.340(6) . ?
C4_5 F6_5 1.348(6) . ?
C4_5 C5_5 1.555(7) . ?
C5_5 F7_5 1.362(7) . ?
C5_5 C10_5 1.541(8) . ?
C5_5 C6_5 1.547(8) . ?
C6_5 F8_5 1.340(6) . ?
C6_5 F9_5 1.347(6) . ?
C6_5 C7_5 1.544(7) . ?
C7_5 F10_5 1.351(6) . ?
C7_5 C8_5 1.544(8) . ?
C8_5 F11_5 1.345(7) . ?
C8_5 F12_5 1.349(7) . ?
C8_5 C9_5 1.536(8) . ?
C9_5 F13_5 1.371(6) . ?
C9_5 C10_5 1.546(7) . ?
C10_5 F15_5 1.344(6) . ?
C10_5 F14_5 1.356(6) . ?
O1_6 C1_6 1.358(8) . ?
C1_6 C4_6 1.547(9) . ?
C1_6 C3_6 1.550(9) . ?
C1_6 C2_6 1.559(10) . ?
C2_6 F1_6 1.338(10) . ?
C2_6 F2_6 1.345(9) . ?
C2_6 C9_6 1.557(11) . ?
C3_6 F4_6 1.344(8) . ?
C3_6 F3_6 1.350(8) . ?
C3_6 C7_6 1.547(9) . ?
C4_6 F5_6 1.336(9) . ?
C4_6 F6_6 1.350(9) . ?
C4_6 C5_6 1.551(10) . ?
C5_6 F7_6 1.353(10) . ?
C5_6 C6_6 1.543(11) . ?
C5_6 C10_6 1.545(11) . ?
C6_6 F8_6 1.343(10) . ?
C6_6 F9_6 1.348(10) . ?
C6_6 C7_6 1.544(11) . ?
C7_6 F10_6 1.363(9) . ?
C7_6 C8_6 1.535(10) . ?
C8_6 F11_6 1.353(10) . ?
C8_6 F12_6 1.354(9) . ?
C8_6 C9_6 1.547(11) . ?
C9_6 F13_6 1.360(11) . ?
C9_6 C10_6 1.540(11) . ?
C10_6 F14_6 1.343(10) . ?
C10_6 F15_6 1.346(9) . ?
O1_7 C1_7 1.358(5) . ?
C1_7 C2_7 1.555(6) . ?
C1_7 C4_7 1.559(6) . ?
C1_7 C3_7 1.560(6) . ?
C2_7 F2_7 1.345(5) . ?
C2_7 F1_7 1.350(5) . ?
C2_7 C9_7 1.544(6) . ?
C3_7 F4_7 1.341(6) . ?
C3_7 F3_7 1.342(5) . ?
C3_7 C7_7 1.552(7) . ?
C4_7 F5_7 1.343(6) . ?
C4_7 F6_7 1.347(6) . ?
C4_7 C5_7 1.548(7) . ?
C5_7 F7_7 1.363(7) . ?
C5_7 C10_7 1.543(8) . ?
C5_7 C6_7 1.549(7) . ?
C6_7 F8_7 1.345(6) . ?
C6_7 F9_7 1.345(6) . ?
C6_7 C7_7 1.542(8) . ?
C7_7 F10_7 1.362(7) . ?
C7_7 C8_7 1.548(7) . ?
C8_7 F11_7 1.343(6) . ?
C8_7 F12_7 1.349(6) . ?
C8_7 C9_7 1.536(7) . ?
C9_7 F13_7 1.366(5) . ?
C9_7 C10_7 1.545(7) . ?
C10_7 F15_7 1.348(6) . ?
C10_7 F14_7 1.351(7) . ?
O1_8 C1_8 1.364(8) . ?
C1_8 C2_8 1.548(9) . ?
C1_8 C4_8 1.551(9) . ?
C1_8 C3_8 1.555(9) . ?
C2_8 F1_8 1.343(8) . ?
C2_8 F2_8 1.351(8) . ?
C2_8 C9_8 1.543(9) . ?
C3_8 F4_8 1.346(8) . ?
C3_8 F3_8 1.348(9) . ?
C3_8 C7_8 1.556(11) . ?
C4_8 F5_8 1.336(8) . ?
C4_8 F6_8 1.358(9) . ?
C4_8 C5_8 1.548(10) . ?
C5_8 F7_8 1.361(10) . ?
C5_8 C10_8 1.542(11) . ?
C5_8 C6_8 1.545(11) . ?
C6_8 F9_8 1.341(9) . ?
C6_8 F8_8 1.349(9) . ?
C6_8 C7_8 1.547(11) . ?
C7_8 F10_8 1.359(10) . ?
C7_8 C8_8 1.548(11) . ?
C8_8 F11_8 1.343(9) . ?
C8_8 F12_8 1.347(8) . ?
C8_8 C9_8 1.538(10) . ?
C9_8 F13_8 1.369(8) . ?
C9_8 C10_8 1.544(10) . ?
C10_8 F15_8 1.344(9) . ?
C10_8 F14_8 1.346(10) . ?
O1_9 C1_9 1.344(10) . ?
C1_9 C3_9 1.558(10) . ?
C1_9 C4_9 1.560(10) . ?
C1_9 C2_9 1.565(10) . ?
C2_9 F1_9 1.344(9) . ?
C2_9 F2_9 1.351(9) . ?
C2_9 C9_9 1.545(9) . ?
C3_9 F4_9 1.346(9) . ?
C3_9 F3_9 1.352(8) . ?
C3_9 C7_9 1.552(10) . ?
C4_9 F5_9 1.342(9) . ?
C4_9 F6_9 1.352(9) . ?
C4_9 C5_9 1.550(9) . ?
C5_9 F7_9 1.364(8) . ?
C5_9 C10_9 1.536(9) . ?
C5_9 C6_9 1.540(10) . ?
C6_9 F9_9 1.344(8) . ?
C6_9 F8_9 1.355(9) . ?
C6_9 C7_9 1.544(10) . ?
C7_9 F10_9 1.362(10) . ?
C7_9 C8_9 1.539(10) . ?
C8_9 F11_9 1.349(9) . ?
C8_9 F12_9 1.355(9) . ?
C8_9 C9_9 1.555(10) . ?
C9_9 F13_9 1.352(9) . ?
C9_9 C10_9 1.549(9) . ?
C10_9 F15_9 1.349(9) . ?
C10_9 F14_9 1.358(9) . ?
O1_10 C1_10 1.348(7) . ?
C1_10 C3_10 1.554(8) . ?
C1_10 C2_10 1.559(8) . ?
C1_10 C4_10 1.566(8) . ?
C2_10 F2_10 1.352(7) . ?
C2_10 F1_10 1.357(7) . ?
C2_10 C9_10 1.541(7) . ?
C3_10 F4_10 1.346(7) . ?
C3_10 F3_10 1.358(7) . ?
C3_10 C7_10 1.549(7) . ?
C4_10 F5_10 1.342(7) . ?
C4_10 F6_10 1.353(7) . ?
C4_10 C5_10 1.553(8) . ?
C5_10 F7_10 1.366(7) . ?
C5_10 C10_10 1.547(8) . ?
C5_10 C6_10 1.549(8) . ?
C6_10 F8_10 1.339(6) . ?
C6_10 F9_10 1.344(7) . ?
C6_10 C7_10 1.541(8) . ?
C7_10 F10_10 1.366(6) . ?
C7_10 C8_10 1.542(7) . ?
C8_10 F12_10 1.343(6) . ?
C8_10 F11_10 1.349(6) . ?
C8_10 C9_10 1.546(7) . ?
C9_10 F13_10 1.357(6) . ?
C9_10 C10_10 1.542(7) . ?
C10_10 F15_10 1.338(6) . ?
C10_10 F14_10 1.344(6) . ?
O1_11 C1_11 1.344(3) . ?
C1_11 C4_11 1.557(4) . ?
C1_11 C3_11 1.559(4) . ?
C1_11 C2_11 1.561(4) . ?
C2_11 F2_11 1.342(4) . ?
C2_11 F1_11 1.350(4) . ?
C2_11 C9_11 1.546(4) . ?
C3_11 F3_11 1.344(4) . ?
C3_11 F4_11 1.345(4) . ?
C3_11 C7_11 1.549(4) . ?
C4_11 F5_11 1.350(3) . ?
C4_11 F6_11 1.354(3) . ?
C4_11 C5_11 1.549(4) . ?
C5_11 F7_11 1.372(3) . ?
C5_11 C6_11 1.541(4) . ?
C5_11 C10_11 1.542(4) . ?
C6_11 F9_11 1.338(3) . ?
C6_11 F8_11 1.352(3) . ?
C6_11 C7_11 1.539(4) . ?
C7_11 F10_11 1.360(3) . ?
C7_11 C8_11 1.547(4) . ?
C8_11 F12_11 1.343(4) . ?
C8_11 F11_11 1.345(4) . ?
C8_11 C9_11 1.551(4) . ?
C9_11 F13_11 1.358(3) . ?
C9_11 C10_11 1.544(4) . ?
C10_11 F15_11 1.339(3) . ?
C10_11 F14_11 1.351(3) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C4_3 Ag1 C5_1 157.8(2) . . ?
C5_2 Ag1 C5_4 154.2(10) . . ?
C5_2 Ag1 C6_2 33.1(8) . . ?
C5_4 Ag1 C6_2 141.1(8) . . ?
C4_3 Ag1 C4_1 145.4(2) . . ?
C5_1 Ag1 C4_1 33.05(19) . . ?
C4_3 Ag1 C5_3 32.88(19) . . ?
C5_1 Ag1 C5_3 129.4(3) . . ?
C4_1 Ag1 C5_3 145.2(2) . . ?
C5_2 Ag1 C4_4 143.0(9) . . ?
C5_4 Ag1 C4_4 32.2(4) . . ?
C6_2 Ag1 C4_4 113.5(9) . . ?
C5_2 Ag1 C4_2 31.1(7) . . ?
C5_4 Ag1 C4_2 124.4(10) . . ?
C6_2 Ag1 C4_2 54.8(9) . . ?
C4_4 Ag1 C4_2 131.0(9) . . ?
C4_3 Ag1 C3_3 30.3(2) . . ?
C5_1 Ag1 C3_3 138.0(2) . . ?
C4_1 Ag1 C3_3 115.1(2) . . ?
C5_3 Ag1 C3_3 53.6(2) . . ?
C4_3 Ag1 C6_1 128.4(2) . . ?
C5_1 Ag1 C6_1 29.90(16) . . ?
C4_1 Ag1 C6_1 53.46(19) . . ?
C5_3 Ag1 C6_1 100.2(2) . . ?
C3_3 Ag1 C6_1 119.2(2) . . ?
C5_2 Ag1 C6_4 127.3(10) . . ?
C5_4 Ag1 C6_4 27.7(4) . . ?
C6_2 Ag1 C6_4 129.5(7) . . ?
C4_4 Ag1 C6_4 51.0(5) . . ?
C4_2 Ag1 C6_4 96.7(9) . . ?
C6_2 Ag2 C4_4 139.0(10) . . ?
C4_3 Ag2 C4_1 164.2(3) . . ?
C6_2 Ag2 C5_2 34.7(8) . . ?
C4_4 Ag2 C5_2 156.7(10) . . ?
C4_3 Ag2 C3_3 34.2(2) . . ?
C4_1 Ag2 C3_3 138.1(4) . . ?
C6_2 Ag2 C5_4 154.8(9) . . ?
C4_4 Ag2 C5_4 33.3(4) . . ?
C5_2 Ag2 C5_4 136.7(11) . . ?
C4_3 Ag2 C5_1 139.7(4) . . ?
C4_1 Ag2 C5_1 33.2(2) . . ?
C3_3 Ag2 C5_1 146.8(3) . . ?
C6_2 Ag2 C1_2 30.6(6) . . ?
C4_4 Ag2 C1_2 110.3(8) . . ?
C5_2 Ag2 C1_2 55.1(9) . . ?
C5_4 Ag2 C1_2 126.5(8) . . ?
C4_3 Ag2 C3_1 137.8(3) . . ?
C4_1 Ag2 C3_1 30.05(19) . . ?
C3_3 Ag2 C3_1 108.1(3) . . ?
C5_1 Ag2 C3_1 54.4(2) . . ?
C6_2 Ag2 C3_4 110.8(9) . . ?
C4_4 Ag2 C3_4 29.2(4) . . ?
C5_2 Ag2 C3_4 131.2(9) . . ?
C5_4 Ag2 C3_4 53.7(5) . . ?
C1_2 Ag2 C3_4 81.2(8) . . ?
C4_3 Ag2 C5_3 29.1(2) . . ?
C4_1 Ag2 C5_3 138.7(3) . . ?
C3_3 Ag2 C5_3 53.6(3) . . ?
C5_1 Ag2 C5_3 110.7(3) . . ?
C3_1 Ag2 C5_3 126.7(3) . . ?
C5_3 Ag3 C5_1 159.6(7) . . ?
C5_3 Ag3 C4_3 35.7(2) . . ?
C5_1 Ag3 C4_3 153.7(7) . . ?
C5_4 Ag3 C5_2 155.7(11) . . ?
C5_4 Ag3 C4_2 148.5(11) . . ?
C5_2 Ag3 C4_2 33.6(7) . . ?
C5_3 Ag3 C6_1 125.7(6) . . ?
C5_1 Ag3 C6_1 34.1(2) . . ?
C4_3 Ag3 C6_1 147.1(4) . . ?
C5_4 Ag3 C6_4 33.5(4) . . ?
C5_2 Ag3 C6_4 147.2(10) . . ?
C4_2 Ag3 C6_4 118.5(11) . . ?
C5_3 Ag3 C6_3 30.5(3) . . ?
C5_1 Ag3 C6_3 129.3(5) . . ?
C4_3 Ag3 C6_3 56.6(3) . . ?
C6_1 Ag3 C6_3 96.7(5) . . ?
C5_4 Ag3 C4_4 29.8(5) . . ?
C5_2 Ag3 C4_4 126.0(11) . . ?
C4_2 Ag3 C4_4 135.1(9) . . ?
C6_4 Ag3 C4_4 53.8(6) . . ?
C5_3 Ag3 C4_1 149.8(5) . . ?
C5_1 Ag3 C4_1 29.1(2) . . ?
C4_3 Ag3 C4_1 124.7(6) . . ?
C6_1 Ag3 C4_1 53.5(2) . . ?
C6_3 Ag3 C4_1 127.3(4) . . ?
C5_4 Ag3 C6_2 127.2(11) . . ?
C5_2 Ag3 C6_2 28.5(7) . . ?
C4_2 Ag3 C6_2 52.9(9) . . ?
C6_4 Ag3 C6_2 133.0(8) . . ?
C4_4 Ag3 C6_2 97.6(10) . . ?
F1_1 C1_1 C2_1 122.5(5) . . ?
F1_1 C1_1 C6_1 116.3(5) . . ?
C2_1 C1_1 C6_1 121.2(4) . . ?
F2_1 C2_1 C1_1 117.9(5) . . ?
F2_1 C2_1 C3_1 122.0(5) . . ?
C1_1 C2_1 C3_1 120.1(5) . . ?
C2_1 C3_1 C4_1 118.9(5) . . ?
C2_1 C3_1 Ag2 98.1(4) . . ?
C4_1 C3_1 Ag2 57.6(4) . . ?
C2_1 C3_1 Ag1 93.1(3) . . ?
C4_1 C3_1 Ag1 51.9(3) . . ?
C2_1 C3_1 Ag3 82.0(4) . . ?
C4_1 C3_1 Ag3 55.1(4) . . ?
C2_1 C3_1 H3_1 120.5 . . ?
C4_1 C3_1 H3_1 120.5 . . ?
Ag2 C3_1 H3_1 112.9 . . ?
Ag1 C3_1 H3_1 123.7 . . ?
Ag3 C3_1 H3_1 134.5 . . ?
C3_1 C4_1 C5_1 121.1(5) . . ?
C3_1 C4_1 Ag2 92.4(4) . . ?
C5_1 C4_1 Ag2 79.9(5) . . ?
C3_1 C4_1 Ag1 102.5(4) . . ?
C5_1 C4_1 Ag1 64.9(4) . . ?
C3_1 C4_1 Ag3 101.2(4) . . ?
C5_1 C4_1 Ag3 53.0(4) . . ?
C3_1 C4_1 H4_1 119.4 . . ?
C5_1 C4_1 H4_1 119.4 . . ?
Ag2 C4_1 H4_1 97.8 . . ?
Ag1 C4_1 H4_1 102.2 . . ?
Ag3 C4_1 H4_1 114.5 . . ?
C6_1 C5_1 C4_1 119.1(5) . . ?
C6_1 C5_1 Ag3 77.8(5) . . ?
C4_1 C5_1 Ag3 97.9(6) . . ?
C6_1 C5_1 Ag1 93.8(4) . . ?
C4_1 C5_1 Ag1 82.0(4) . . ?
C6_1 C5_1 Ag2 98.4(4) . . ?
C4_1 C5_1 Ag2 66.9(4) . . ?
C6_1 C5_1 H5_1 120.4 . . ?
C4_1 C5_1 H5_1 120.4 . . ?
Ag3 C5_1 H5_1 94.2 . . ?
Ag1 C5_1 H5_1 94.1 . . ?
Ag2 C5_1 H5_1 104.0 . . ?
C1_1 C6_1 C5_1 119.5(5) . . ?
C1_1 C6_1 Ag3 103.0(4) . . ?
C5_1 C6_1 Ag3 68.1(5) . . ?
C1_1 C6_1 Ag1 101.2(4) . . ?
C5_1 C6_1 Ag1 56.3(3) . . ?
C1_1 C6_1 Ag2 91.6(4) . . ?
C5_1 C6_1 Ag2 54.7(4) . . ?
C1_1 C6_1 H6_1 120.2 . . ?
C5_1 C6_1 H6_1 120.2 . . ?
Ag3 C6_1 H6_1 98.5 . . ?
Ag1 C6_1 H6_1 111.0 . . ?
Ag2 C6_1 H6_1 123.0 . . ?
F1_2 C1_2 C2_2 121.3(18) . . ?
F1_2 C1_2 C6_2 115.9(18) . . ?
C2_2 C1_2 C6_2 122.8(14) . . ?
F1_2 C1_2 Ag2 113(2) . . ?
C2_2 C1_2 Ag2 98.9(16) . . ?
C6_2 C1_2 Ag2 55(2) . . ?
F2_2 C2_2 C1_2 116.8(18) . . ?
F2_2 C2_2 C3_2 124.7(19) . . ?
C1_2 C2_2 C3_2 118.5(15) . . ?
C2_2 C3_2 C4_2 119.6(15) . . ?
C2_2 C3_2 Ag3 95.9(14) . . ?
C4_2 C3_2 Ag3 55(2) . . ?
C2_2 C3_2 Ag1 85.8(13) . . ?
C4_2 C3_2 Ag1 55.1(18) . . ?
C2_2 C3_2 Ag2 74.2(12) . . ?
C4_2 C3_2 Ag2 62.4(17) . . ?
C2_2 C3_2 H3_2 120.2 . . ?
C4_2 C3_2 H3_2 120.2 . . ?
Ag3 C3_2 H3_2 117.7 . . ?
Ag1 C3_2 H3_2 129.8 . . ?
Ag2 C3_2 H3_2 137.0 . . ?
C3_2 C4_2 C5_2 121.3(16) . . ?
C3_2 C4_2 Ag3 97(2) . . ?
C5_2 C4_2 Ag3 73(3) . . ?
C3_2 C4_2 Ag1 100(2) . . ?
C5_2 C4_2 Ag1 58(3) . . ?
C3_2 C4_2 Ag2 93.0(19) . . ?
C5_2 C4_2 Ag2 53(2) . . ?
C3_2 C4_2 H4_2 119.4 . . ?
C5_2 C4_2 H4_2 119.4 . . ?
Ag3 C4_2 H4_2 100.5 . . ?
Ag1 C4_2 H4_2 111.3 . . ?
Ag2 C4_2 H4_2 123.9 . . ?
C6_2 C5_2 C4_2 119.6(17) . . ?
C6_2 C5_2 Ag1 83(3) . . ?
C4_2 C5_2 Ag1 91(3) . . ?
C6_2 C5_2 Ag2 66(3) . . ?
C4_2 C5_2 Ag2 99(3) . . ?
C6_2 C5_2 Ag3 96(3) . . ?
C4_2 C5_2 Ag3 74(3) . . ?
C6_2 C5_2 H5_2 120.2 . . ?
C4_2 C5_2 H5_2 120.2 . . ?
Ag1 C5_2 H5_2 96.6 . . ?
Ag2 C5_2 H5_2 104.1 . . ?
Ag3 C5_2 H5_2 100.3 . . ?
C1_2 C6_2 C5_2 118.2(15) . . ?
C1_2 C6_2 Ag2 94(2) . . ?
C5_2 C6_2 Ag2 79(3) . . ?
C1_2 C6_2 Ag1 101(2) . . ?
C5_2 C6_2 Ag1 64(3) . . ?
C1_2 C6_2 Ag3 96(2) . . ?
C5_2 C6_2 Ag3 56(2) . . ?
C1_2 C6_2 H6_2 120.9 . . ?
C5_2 C6_2 H6_2 120.9 . . ?
Ag2 C6_2 H6_2 96.3 . . ?
Ag1 C6_2 H6_2 103.9 . . ?
Ag3 C6_2 H6_2 117.1 . . ?
F1_3 C1_3 C6_3 122.8(8) . . ?
F1_3 C1_3 C2_3 117.1(8) . . ?
C6_3 C1_3 C2_3 120.1(6) . . ?
F2_3 C2_3 C1_3 119.6(7) . . ?
F2_3 C2_3 C3_3 118.7(7) . . ?
C1_3 C2_3 C3_3 121.7(6) . . ?
C2_3 C3_3 C4_3 119.0(7) . . ?
C2_3 C3_3 Ag2 103.4(5) . . ?
C4_3 C3_3 Ag2 66.8(5) . . ?
C2_3 C3_3 Ag1 103.4(5) . . ?
C4_3 C3_3 Ag1 55.1(5) . . ?
C2_3 C3_3 Ag3 94.6(5) . . ?
C4_3 C3_3 Ag3 49.8(4) . . ?
C2_3 C3_3 H3_3 120.5 . . ?
C4_3 C3_3 H3_3 120.5 . . ?
Ag2 C3_3 H3_3 99.2 . . ?
Ag1 C3_3 H3_3 109.6 . . ?
Ag3 C3_3 H3_3 123.8 . . ?
C5_3 C4_3 C3_3 119.0(6) . . ?
C5_3 C4_3 Ag1 84.5(4) . . ?
C3_3 C4_3 Ag1 94.6(6) . . ?
C5_3 C4_3 Ag2 97.7(5) . . ?
C3_3 C4_3 Ag2 79.0(6) . . ?
C5_3 C4_3 Ag3 66.0(5) . . ?
C3_3 C4_3 Ag3 102.9(6) . . ?
C5_3 C4_3 H4_3 120.5 . . ?
C3_3 C4_3 H4_3 120.5 . . ?
Ag1 C4_3 H4_3 90.9 . . ?
Ag2 C4_3 H4_3 93.2 . . ?
Ag3 C4_3 H4_3 100.4 . . ?
C4_3 C5_3 C6_3 121.0(7) . . ?
C4_3 C5_3 Ag3 78.3(6) . . ?
C6_3 C5_3 Ag3 97.8(7) . . ?
C4_3 C5_3 Ag1 62.7(4) . . ?
C6_3 C5_3 Ag1 105.6(6) . . ?
C4_3 C5_3 Ag2 53.2(4) . . ?
C6_3 C5_3 Ag2 102.2(6) . . ?
C4_3 C5_3 H5_3 119.5 . . ?
C6_3 C5_3 H5_3 119.5 . . ?
Ag3 C5_3 H5_3 94.0 . . ?
Ag1 C5_3 H5_3 101.1 . . ?
Ag2 C5_3 H5_3 113.2 . . ?
C1_3 C6_3 C5_3 119.2(7) . . ?
C1_3 C6_3 Ag3 101.1(6) . . ?
C5_3 C6_3 Ag3 51.7(5) . . ?
C1_3 C6_3 Ag1 93.3(5) . . ?
C5_3 C6_3 Ag1 49.5(4) . . ?
C1_3 C6_3 Ag2 82.6(5) . . ?
C5_3 C6_3 Ag2 54.0(4) . . ?
C1_3 C6_3 H6_3 120.4 . . ?
C5_3 C6_3 H6_3 120.4 . . ?
Ag3 C6_3 H6_3 115.0 . . ?
Ag1 C6_3 H6_3 125.8 . . ?
Ag2 C6_3 H6_3 135.0 . . ?
F1_4 C1_4 C6_4 122.8(15) . . ?
F1_4 C1_4 C2_4 114.9(14) . . ?
C6_4 C1_4 C2_4 122.3(11) . . ?
F2_4 C2_4 C3_4 121.6(14) . . ?
F2_4 C2_4 C1_4 119.1(13) . . ?
C3_4 C2_4 C1_4 119.2(11) . . ?
C2_4 C3_4 C4_4 119.2(13) . . ?
C2_4 C3_4 Ag2 105.9(9) . . ?
C4_4 C3_4 Ag2 55.2(13) . . ?
C2_4 C3_4 Ag1 98.7(9) . . ?
C4_4 C3_4 Ag1 51.8(13) . . ?
C2_4 C3_4 Ag3 86.8(9) . . ?
C4_4 C3_4 Ag3 54.7(12) . . ?
C2_4 C3_4 H3_4 120.4 . . ?
C4_4 C3_4 H3_4 120.4 . . ?
Ag2 C3_4 H3_4 107.0 . . ?
Ag1 C3_4 H3_4 117.5 . . ?
Ag3 C3_4 H3_4 128.7 . . ?
C3_4 C4_4 C5_4 121.4(13) . . ?
C3_4 C4_4 Ag2 95.6(15) . . ?
C5_4 C4_4 Ag2 80.1(14) . . ?
C3_4 C4_4 Ag1 103.4(15) . . ?
C5_4 C4_4 Ag1 65.5(13) . . ?
C3_4 C4_4 Ag3 101.4(14) . . ?
C5_4 C4_4 Ag3 53.4(12) . . ?
C3_4 C4_4 H4_4 119.3 . . ?
C5_4 C4_4 H4_4 119.3 . . ?
Ag2 C4_4 H4_4 94.4 . . ?
Ag1 C4_4 H4_4 100.7 . . ?
Ag3 C4_4 H4_4 114.1 . . ?
C6_4 C5_4 C4_4 119.5(13) . . ?
C6_4 C5_4 Ag3 83.2(14) . . ?
C4_4 C5_4 Ag3 96.9(16) . . ?
C6_4 C5_4 Ag1 99.8(14) . . ?
C4_4 C5_4 Ag1 82.2(15) . . ?
C6_4 C5_4 Ag2 106.3(13) . . ?
C4_4 C5_4 Ag2 66.6(14) . . ?
C6_4 C5_4 H5_4 120.2 . . ?
C4_4 C5_4 H5_4 120.2 . . ?
Ag3 C5_4 H5_4 89.9 . . ?
Ag1 C5_4 H5_4 88.0 . . ?
Ag2 C5_4 H5_4 96.6 . . ?
C1_4 C6_4 C5_4 117.9(12) . . ?
C1_4 C6_4 Ag3 105.5(12) . . ?
C5_4 C6_4 Ag3 63.2(12) . . ?
C1_4 C6_4 Ag1 104.0(11) . . ?
C5_4 C6_4 Ag1 52.5(11) . . ?
C1_4 C6_4 Ag2 95.9(10) . . ?
C5_4 C6_4 Ag2 48.9(10) . . ?
C1_4 C6_4 H6_4 121.0 . . ?
C5_4 C6_4 H6_4 121.0 . . ?
Ag3 C6_4 H6_4 100.2 . . ?
Ag1 C6_4 H6_4 110.8 . . ?
Ag2 C6_4 H6_4 122.6 . . ?
O1_7 Al1 O1_11 112.49(15) . . ?
O1_6 Al1 O1_11 116.9(2) . . ?
O1_6 Al1 O1_10 115.3(4) . . ?
O1_11 Al1 O1_10 112.6(3) . . ?
O1_7 Al1 O1_9 111.7(4) . . ?
O1_11 Al1 O1_9 109.4(4) . . ?
O1_7 Al1 O1_5 109.32(17) . . ?
O1_11 Al1 O1_5 102.32(16) . . ?
O1_9 Al1 O1_5 111.2(3) . . ?
O1_6 Al1 O1_8 108.0(3) . . ?
O1_11 Al1 O1_8 100.1(2) . . ?
O1_10 Al1 O1_8 101.2(4) . . ?
C1_5 O1_5 Al1 148.0(3) . . ?
O1_5 C1_5 C3_5 112.1(4) . . ?
O1_5 C1_5 C2_5 108.5(4) . . ?
C3_5 C1_5 C2_5 107.5(4) . . ?
O1_5 C1_5 C4_5 113.8(4) . . ?
C3_5 C1_5 C4_5 107.6(4) . . ?
C2_5 C1_5 C4_5 107.2(4) . . ?
F1_5 C2_5 F2_5 105.5(4) . . ?
F1_5 C2_5 C9_5 109.7(4) . . ?
F2_5 C2_5 C9_5 109.0(4) . . ?
F1_5 C2_5 C1_5 110.2(4) . . ?
F2_5 C2_5 C1_5 110.4(4) . . ?
C9_5 C2_5 C1_5 111.8(4) . . ?
F4_5 C3_5 F3_5 106.4(4) . . ?
F4_5 C3_5 C1_5 110.4(4) . . ?
F3_5 C3_5 C1_5 110.1(4) . . ?
F4_5 C3_5 C7_5 109.4(4) . . ?
F3_5 C3_5 C7_5 108.3(4) . . ?
C1_5 C3_5 C7_5 112.0(4) . . ?
F5_5 C4_5 F6_5 105.9(5) . . ?
F5_5 C4_5 C5_5 109.6(5) . . ?
F6_5 C4_5 C5_5 109.3(5) . . ?
F5_5 C4_5 C1_5 110.3(4) . . ?
F6_5 C4_5 C1_5 110.2(5) . . ?
C5_5 C4_5 C1_5 111.4(5) . . ?
F7_5 C5_5 C10_5 109.9(7) . . ?
F7_5 C5_5 C6_5 108.5(8) . . ?
C10_5 C5_5 C6_5 108.7(5) . . ?
F7_5 C5_5 C4_5 110.4(8) . . ?
C10_5 C5_5 C4_5 109.2(5) . . ?
C6_5 C5_5 C4_5 110.1(5) . . ?
F8_5 C6_5 F9_5 106.4(5) . . ?
F8_5 C6_5 C7_5 110.8(5) . . ?
F9_5 C6_5 C7_5 110.3(5) . . ?
F8_5 C6_5 C5_5 109.4(5) . . ?
F9_5 C6_5 C5_5 110.4(5) . . ?
C7_5 C6_5 C5_5 109.4(5) . . ?
F10_5 C7_5 C8_5 110.1(6) . . ?
F10_5 C7_5 C6_5 109.5(6) . . ?
C8_5 C7_5 C6_5 109.2(5) . . ?
F10_5 C7_5 C3_5 109.5(5) . . ?
C8_5 C7_5 C3_5 109.6(5) . . ?
C6_5 C7_5 C3_5 109.0(5) . . ?
F11_5 C8_5 F12_5 105.5(6) . . ?
F11_5 C8_5 C9_5 110.1(7) . . ?
F12_5 C8_5 C9_5 110.1(7) . . ?
F11_5 C8_5 C7_5 110.6(7) . . ?
F12_5 C8_5 C7_5 111.0(7) . . ?
C9_5 C8_5 C7_5 109.4(5) . . ?
F13_5 C9_5 C8_5 110.3(5) . . ?
F13_5 C9_5 C2_5 109.0(4) . . ?
C8_5 C9_5 C2_5 109.8(5) . . ?
F13_5 C9_5 C10_5 109.0(4) . . ?
C8_5 C9_5 C10_5 108.6(5) . . ?
C2_5 C9_5 C10_5 110.1(4) . . ?
F15_5 C10_5 F14_5 104.8(5) . . ?
F15_5 C10_5 C5_5 111.3(5) . . ?
F14_5 C10_5 C5_5 110.4(5) . . ?
F15_5 C10_5 C9_5 110.7(5) . . ?
F14_5 C10_5 C9_5 109.9(5) . . ?
C5_5 C10_5 C9_5 109.6(5) . . ?
C1_6 O1_6 Al1 148.0(5) . . ?
O1_6 C1_6 C4_6 109.5(6) . . ?
O1_6 C1_6 C3_6 111.7(6) . . ?
C4_6 C1_6 C3_6 107.9(6) . . ?
O1_6 C1_6 C2_6 112.2(7) . . ?
C4_6 C1_6 C2_6 107.5(7) . . ?
C3_6 C1_6 C2_6 107.9(6) . . ?
F1_6 C2_6 F2_6 106.2(9) . . ?
F1_6 C2_6 C9_6 108.2(9) . . ?
F2_6 C2_6 C9_6 109.1(8) . . ?
F1_6 C2_6 C1_6 111.0(9) . . ?
F2_6 C2_6 C1_6 110.9(8) . . ?
C9_6 C2_6 C1_6 111.3(8) . . ?
F4_6 C3_6 F3_6 105.9(6) . . ?
F4_6 C3_6 C7_6 109.0(7) . . ?
F3_6 C3_6 C7_6 109.0(7) . . ?
F4_6 C3_6 C1_6 110.5(7) . . ?
F3_6 C3_6 C1_6 110.8(6) . . ?
C7_6 C3_6 C1_6 111.5(6) . . ?
F5_6 C4_6 F6_6 106.3(7) . . ?
F5_6 C4_6 C1_6 110.1(7) . . ?
F6_6 C4_6 C1_6 109.6(7) . . ?
F5_6 C4_6 C5_6 110.3(7) . . ?
F6_6 C4_6 C5_6 109.3(7) . . ?
C1_6 C4_6 C5_6 111.2(7) . . ?
F7_6 C5_6 C6_6 108.3(11) . . ?
F7_6 C5_6 C10_6 110.7(10) . . ?
C6_6 C5_6 C10_6 110.3(9) . . ?
F7_6 C5_6 C4_6 108.9(8) . . ?
C6_6 C5_6 C4_6 109.1(8) . . ?
C10_6 C5_6 C4_6 109.5(8) . . ?
F8_6 C6_6 F9_6 105.2(11) . . ?
F8_6 C6_6 C5_6 110.5(12) . . ?
F9_6 C6_6 C5_6 109.7(12) . . ?
F8_6 C6_6 C7_6 111.0(11) . . ?
F9_6 C6_6 C7_6 111.4(11) . . ?
C5_6 C6_6 C7_6 109.0(9) . . ?
F10_6 C7_6 C8_6 108.5(7) . . ?
F10_6 C7_6 C6_6 108.9(8) . . ?
C8_6 C7_6 C6_6 109.2(8) . . ?
F10_6 C7_6 C3_6 111.2(7) . . ?
C8_6 C7_6 C3_6 109.8(7) . . ?
C6_6 C7_6 C3_6 109.2(7) . . ?
F11_6 C8_6 F12_6 105.5(8) . . ?
F11_6 C8_6 C7_6 110.7(8) . . ?
F12_6 C8_6 C7_6 111.1(8) . . ?
F11_6 C8_6 C9_6 110.0(9) . . ?
F12_6 C8_6 C9_6 109.4(8) . . ?
C7_6 C8_6 C9_6 110.1(8) . . ?
F13_6 C9_6 C10_6 111.2(13) . . ?
F13_6 C9_6 C8_6 108.7(11) . . ?
C10_6 C9_6 C8_6 109.1(9) . . ?
F13_6 C9_6 C2_6 109.5(13) . . ?
C10_6 C9_6 C2_6 108.8(9) . . ?
C8_6 C9_6 C2_6 109.5(9) . . ?
F14_6 C10_6 F15_6 105.3(8) . . ?
F14_6 C10_6 C9_6 111.8(9) . . ?
F15_6 C10_6 C9_6 111.2(9) . . ?
F14_6 C10_6 C5_6 110.2(9) . . ?
F15_6 C10_6 C5_6 109.0(9) . . ?
C9_6 C10_6 C5_6 109.3(9) . . ?
C1_7 O1_7 Al1 149.4(3) . . ?
O1_7 C1_7 C2_7 112.7(4) . . ?
O1_7 C1_7 C4_7 109.1(4) . . ?
C2_7 C1_7 C4_7 107.3(4) . . ?
O1_7 C1_7 C3_7 111.5(4) . . ?
C2_7 C1_7 C3_7 108.2(4) . . ?
C4_7 C1_7 C3_7 107.9(4) . . ?
F2_7 C2_7 F1_7 105.3(4) . . ?
F2_7 C2_7 C9_7 109.2(4) . . ?
F1_7 C2_7 C9_7 109.6(4) . . ?
F2_7 C2_7 C1_7 110.9(4) . . ?
F1_7 C2_7 C1_7 110.2(4) . . ?
C9_7 C2_7 C1_7 111.5(4) . . ?
F4_7 C3_7 F3_7 106.1(4) . . ?
F4_7 C3_7 C7_7 109.6(4) . . ?
F3_7 C3_7 C7_7 109.9(5) . . ?
F4_7 C3_7 C1_7 110.1(4) . . ?
F3_7 C3_7 C1_7 110.1(4) . . ?
C7_7 C3_7 C1_7 110.9(5) . . ?
F5_7 C4_7 F6_7 106.0(4) . . ?
F5_7 C4_7 C5_7 109.4(4) . . ?
F6_7 C4_7 C5_7 109.4(5) . . ?
F5_7 C4_7 C1_7 110.4(4) . . ?
F6_7 C4_7 C1_7 110.2(4) . . ?
C5_7 C4_7 C1_7 111.3(5) . . ?
F7_7 C5_7 C10_7 110.5(7) . . ?
F7_7 C5_7 C4_7 108.9(6) . . ?
C10_7 C5_7 C4_7 109.4(5) . . ?
F7_7 C5_7 C6_7 109.3(7) . . ?
C10_7 C5_7 C6_7 109.5(6) . . ?
C4_7 C5_7 C6_7 109.2(5) . . ?
F8_7 C6_7 F9_7 105.9(5) . . ?
F8_7 C6_7 C7_7 111.0(6) . . ?
F9_7 C6_7 C7_7 109.7(6) . . ?
F8_7 C6_7 C5_7 110.2(5) . . ?
F9_7 C6_7 C5_7 110.4(6) . . ?
C7_7 C6_7 C5_7 109.6(5) . . ?
F10_7 C7_7 C6_7 109.4(9) . . ?
F10_7 C7_7 C8_7 108.9(9) . . ?
C6_7 C7_7 C8_7 109.5(5) . . ?
F10_7 C7_7 C3_7 110.4(9) . . ?
C6_7 C7_7 C3_7 109.4(5) . . ?
C8_7 C7_7 C3_7 109.2(5) . . ?
F11_7 C8_7 F12_7 105.7(5) . . ?
F11_7 C8_7 C9_7 109.8(5) . . ?
F12_7 C8_7 C9_7 110.9(5) . . ?
F11_7 C8_7 C7_7 110.4(5) . . ?
F12_7 C8_7 C7_7 110.2(5) . . ?
C9_7 C8_7 C7_7 109.8(5) . . ?
F13_7 C9_7 C8_7 109.4(4) . . ?
F13_7 C9_7 C2_7 110.5(4) . . ?
C8_7 C9_7 C2_7 109.6(4) . . ?
F13_7 C9_7 C10_7 108.8(4) . . ?
C8_7 C9_7 C10_7 109.6(5) . . ?
C2_7 C9_7 C10_7 109.0(4) . . ?
F15_7 C10_7 F14_7 105.9(6) . . ?
F15_7 C10_7 C5_7 110.4(6) . . ?
F14_7 C10_7 C5_7 110.5(8) . . ?
F15_7 C10_7 C9_7 110.3(5) . . ?
F14_7 C10_7 C9_7 110.2(7) . . ?
C5_7 C10_7 C9_7 109.5(5) . . ?
C1_8 O1_8 Al1 151.0(5) . . ?
O1_8 C1_8 C2_8 109.3(6) . . ?
O1_8 C1_8 C4_8 111.1(6) . . ?
C2_8 C1_8 C4_8 108.9(6) . . ?
O1_8 C1_8 C3_8 112.8(6) . . ?
C2_8 C1_8 C3_8 107.4(6) . . ?
C4_8 C1_8 C3_8 107.3(6) . . ?
F1_8 C2_8 F2_8 105.2(6) . . ?
F1_8 C2_8 C9_8 109.8(6) . . ?
F2_8 C2_8 C9_8 109.0(6) . . ?
F1_8 C2_8 C1_8 111.1(6) . . ?
F2_8 C2_8 C1_8 110.2(6) . . ?
C9_8 C2_8 C1_8 111.4(6) . . ?
F4_8 C3_8 F3_8 105.6(7) . . ?
F4_8 C3_8 C1_8 111.2(7) . . ?
F3_8 C3_8 C1_8 110.8(7) . . ?
F4_8 C3_8 C7_8 109.2(7) . . ?
F3_8 C3_8 C7_8 108.8(8) . . ?
C1_8 C3_8 C7_8 111.2(7) . . ?
F5_8 C4_8 F6_8 106.0(7) . . ?
F5_8 C4_8 C5_8 110.0(7) . . ?
F6_8 C4_8 C5_8 108.2(8) . . ?
F5_8 C4_8 C1_8 111.5(7) . . ?
F6_8 C4_8 C1_8 109.5(7) . . ?
C5_8 C4_8 C1_8 111.4(7) . . ?
F7_8 C5_8 C10_8 108.1(11) . . ?
F7_8 C5_8 C6_8 110.0(11) . . ?
C10_8 C5_8 C6_8 108.9(9) . . ?
F7_8 C5_8 C4_8 110.5(9) . . ?
C10_8 C5_8 C4_8 110.2(8) . . ?
C6_8 C5_8 C4_8 109.1(8) . . ?
F9_8 C6_8 F8_8 105.8(8) . . ?
F9_8 C6_8 C5_8 110.9(9) . . ?
F8_8 C6_8 C5_8 110.1(9) . . ?
F9_8 C6_8 C7_8 110.4(9) . . ?
F8_8 C6_8 C7_8 110.3(9) . . ?
C5_8 C6_8 C7_8 109.3(9) . . ?
F10_8 C7_8 C6_8 109.7(14) . . ?
F10_8 C7_8 C8_8 109.6(15) . . ?
C6_8 C7_8 C8_8 108.9(8) . . ?
F10_8 C7_8 C3_8 109.7(14) . . ?
C6_8 C7_8 C3_8 109.6(8) . . ?
C8_8 C7_8 C3_8 109.3(8) . . ?
F11_8 C8_8 F12_8 105.0(7) . . ?
F11_8 C8_8 C9_8 110.4(8) . . ?
F12_8 C8_8 C9_8 110.6(8) . . ?
F11_8 C8_8 C7_8 110.7(8) . . ?
F12_8 C8_8 C7_8 110.4(8) . . ?
C9_8 C8_8 C7_8 109.6(8) . . ?
F13_8 C9_8 C8_8 109.6(7) . . ?
F13_8 C9_8 C2_8 109.3(6) . . ?
C8_8 C9_8 C2_8 109.5(7) . . ?
F13_8 C9_8 C10_8 109.5(7) . . ?
C8_8 C9_8 C10_8 108.6(8) . . ?
C2_8 C9_8 C10_8 110.2(7) . . ?
F15_8 C10_8 F14_8 104.9(10) . . ?
F15_8 C10_8 C5_8 112.1(10) . . ?
F14_8 C10_8 C5_8 109.8(12) . . ?
F15_8 C10_8 C9_8 109.6(9) . . ?
F14_8 C10_8 C9_8 110.8(12) . . ?
C5_8 C10_8 C9_8 109.5(8) . . ?
C1_9 O1_9 Al1 147.3(8) . . ?
O1_9 C1_9 C3_9 112.7(9) . . ?
O1_9 C1_9 C4_9 112.8(8) . . ?
C3_9 C1_9 C4_9 107.0(8) . . ?
O1_9 C1_9 C2_9 109.3(7) . . ?
C3_9 C1_9 C2_9 107.3(8) . . ?
C4_9 C1_9 C2_9 107.5(8) . . ?
F1_9 C2_9 F2_9 107.1(9) . . ?
F1_9 C2_9 C9_9 109.7(8) . . ?
F2_9 C2_9 C9_9 108.6(9) . . ?
F1_9 C2_9 C1_9 110.0(8) . . ?
F2_9 C2_9 C1_9 109.1(11) . . ?
C9_9 C2_9 C1_9 112.2(8) . . ?
F4_9 C3_9 F3_9 106.3(7) . . ?
F4_9 C3_9 C7_9 109.5(8) . . ?
F3_9 C3_9 C7_9 108.7(10) . . ?
F4_9 C3_9 C1_9 110.6(9) . . ?
F3_9 C3_9 C1_9 110.0(9) . . ?
C7_9 C3_9 C1_9 111.7(8) . . ?
F5_9 C4_9 F6_9 104.0(9) . . ?
F5_9 C4_9 C5_9 110.1(7) . . ?
F6_9 C4_9 C5_9 109.2(9) . . ?
F5_9 C4_9 C1_9 111.2(7) . . ?
F6_9 C4_9 C1_9 110.4(11) . . ?
C5_9 C4_9 C1_9 111.6(7) . . ?
F7_9 C5_9 C10_9 109.0(7) . . ?
F7_9 C5_9 C6_9 109.3(8) . . ?
C10_9 C5_9 C6_9 108.4(7) . . ?
F7_9 C5_9 C4_9 110.6(7) . . ?
C10_9 C5_9 C4_9 110.1(7) . . ?
C6_9 C5_9 C4_9 109.5(7) . . ?
F9_9 C6_9 F8_9 104.9(7) . . ?
F9_9 C6_9 C5_9 111.7(8) . . ?
F8_9 C6_9 C5_9 108.8(7) . . ?
F9_9 C6_9 C7_9 111.4(8) . . ?
F8_9 C6_9 C7_9 110.3(8) . . ?
C5_9 C6_9 C7_9 109.8(8) . . ?
F10_9 C7_9 C8_9 111.0(11) . . ?
F10_9 C7_9 C6_9 107.8(13) . . ?
C8_9 C7_9 C6_9 109.1(8) . . ?
F10_9 C7_9 C3_9 109.4(11) . . ?
C8_9 C7_9 C3_9 109.6(9) . . ?
C6_9 C7_9 C3_9 109.9(8) . . ?
F11_9 C8_9 F12_9 105.9(8) . . ?
F11_9 C8_9 C7_9 111.8(10) . . ?
F12_9 C8_9 C7_9 110.7(9) . . ?
F11_9 C8_9 C9_9 109.9(9) . . ?
F12_9 C8_9 C9_9 109.4(9) . . ?
C7_9 C8_9 C9_9 109.2(8) . . ?
F13_9 C9_9 C2_9 109.7(8) . . ?
F13_9 C9_9 C10_9 110.2(7) . . ?
C2_9 C9_9 C10_9 108.5(7) . . ?
F13_9 C9_9 C8_9 109.8(9) . . ?
C2_9 C9_9 C8_9 109.6(8) . . ?
C10_9 C9_9 C8_9 109.1(7) . . ?
F15_9 C10_9 F14_9 105.9(9) . . ?
F15_9 C10_9 C5_9 110.9(7) . . ?
F14_9 C10_9 C5_9 110.7(7) . . ?
F15_9 C10_9 C9_9 109.5(7) . . ?
F14_9 C10_9 C9_9 109.4(8) . . ?
C5_9 C10_9 C9_9 110.3(7) . . ?
C1_10 O1_10 Al1 155.1(7) . . ?
O1_10 C1_10 C3_10 111.6(6) . . ?
O1_10 C1_10 C2_10 109.7(6) . . ?
C3_10 C1_10 C2_10 107.3(6) . . ?
O1_10 C1_10 C4_10 113.8(7) . . ?
C3_10 C1_10 C4_10 106.8(6) . . ?
C2_10 C1_10 C4_10 107.3(6) . . ?
F2_10 C2_10 F1_10 106.8(6) . . ?
F2_10 C2_10 C9_10 110.0(5) . . ?
F1_10 C2_10 C9_10 109.0(6) . . ?
F2_10 C2_10 C1_10 109.8(5) . . ?
F1_10 C2_10 C1_10 108.8(8) . . ?
C9_10 C2_10 C1_10 112.4(5) . . ?
F4_10 C3_10 F3_10 104.8(6) . . ?
F4_10 C3_10 C7_10 109.1(6) . . ?
F3_10 C3_10 C7_10 108.5(6) . . ?
F4_10 C3_10 C1_10 110.6(6) . . ?
F3_10 C3_10 C1_10 111.5(8) . . ?
C7_10 C3_10 C1_10 112.0(6) . . ?
F5_10 C4_10 F6_10 105.4(5) . . ?
F5_10 C4_10 C5_10 109.8(7) . . ?
F6_10 C4_10 C5_10 109.6(6) . . ?
F5_10 C4_10 C1_10 110.5(6) . . ?
F6_10 C4_10 C1_10 109.9(6) . . ?
C5_10 C4_10 C1_10 111.4(6) . . ?
F7_10 C5_10 C10_10 109.6(9) . . ?
F7_10 C5_10 C6_10 108.2(8) . . ?
C10_10 C5_10 C6_10 109.8(5) . . ?
F7_10 C5_10 C4_10 110.2(7) . . ?
C10_10 C5_10 C4_10 109.4(6) . . ?
C6_10 C5_10 C4_10 109.7(6) . . ?
F8_10 C6_10 F9_10 106.5(6) . . ?
F8_10 C6_10 C7_10 110.7(6) . . ?
F9_10 C6_10 C7_10 111.4(7) . . ?
F8_10 C6_10 C5_10 109.6(7) . . ?
F9_10 C6_10 C5_10 109.9(6) . . ?
C7_10 C6_10 C5_10 108.7(6) . . ?
F10_10 C7_10 C6_10 109.7(6) . . ?
F10_10 C7_10 C8_10 108.2(5) . . ?
C6_10 C7_10 C8_10 109.7(5) . . ?
F10_10 C7_10 C3_10 110.2(5) . . ?
C6_10 C7_10 C3_10 109.5(6) . . ?
C8_10 C7_10 C3_10 109.6(5) . . ?
F12_10 C8_10 F11_10 104.9(6) . . ?
F12_10 C8_10 C7_10 111.1(5) . . ?
F11_10 C8_10 C7_10 110.5(5) . . ?
F12_10 C8_10 C9_10 109.9(4) . . ?
F11_10 C8_10 C9_10 110.8(5) . . ?
C7_10 C8_10 C9_10 109.6(5) . . ?
F13_10 C9_10 C2_10 110.2(5) . . ?
F13_10 C9_10 C10_10 108.6(5) . . ?
C2_10 C9_10 C10_10 109.6(5) . . ?
F13_10 C9_10 C8_10 110.2(4) . . ?
C2_10 C9_10 C8_10 109.1(5) . . ?
C10_10 C9_10 C8_10 109.1(4) . . ?
F15_10 C10_10 F14_10 105.5(5) . . ?
F15_10 C10_10 C9_10 110.8(5) . . ?
F14_10 C10_10 C9_10 111.0(5) . . ?
F15_10 C10_10 C5_10 110.2(5) . . ?
F14_10 C10_10 C5_10 110.0(5) . . ?
C9_10 C10_10 C5_10 109.4(5) . . ?
C1_11 O1_11 Al1 150.6(2) . . ?
O1_11 C1_11 C4_11 112.9(3) . . ?
O1_11 C1_11 C3_11 111.9(3) . . ?
C4_11 C1_11 C3_11 107.3(2) . . ?
O1_11 C1_11 C2_11 109.7(2) . . ?
C4_11 C1_11 C2_11 107.0(2) . . ?
C3_11 C1_11 C2_11 107.7(2) . . ?
F2_11 C2_11 F1_11 106.2(2) . . ?
F2_11 C2_11 C9_11 109.0(2) . . ?
F1_11 C2_11 C9_11 109.1(2) . . ?
F2_11 C2_11 C1_11 110.6(3) . . ?
F1_11 C2_11 C1_11 110.1(2) . . ?
C9_11 C2_11 C1_11 111.6(2) . . ?
F3_11 C3_11 F4_11 106.0(2) . . ?
F3_11 C3_11 C7_11 109.3(3) . . ?
F4_11 C3_11 C7_11 109.3(3) . . ?
F3_11 C3_11 C1_11 110.0(3) . . ?
F4_11 C3_11 C1_11 110.2(3) . . ?
C7_11 C3_11 C1_11 111.9(2) . . ?
F5_11 C4_11 F6_11 105.3(2) . . ?
F5_11 C4_11 C5_11 109.7(2) . . ?
F6_11 C4_11 C5_11 108.6(2) . . ?
F5_11 C4_11 C1_11 110.4(2) . . ?
F6_11 C4_11 C1_11 110.9(2) . . ?
C5_11 C4_11 C1_11 111.6(2) . . ?
F7_11 C5_11 C6_11 109.7(2) . . ?
F7_11 C5_11 C10_11 109.2(2) . . ?
C6_11 C5_11 C10_11 109.7(2) . . ?
F7_11 C5_11 C4_11 108.9(2) . . ?
C6_11 C5_11 C4_11 109.8(2) . . ?
C10_11 C5_11 C4_11 109.6(2) . . ?
F9_11 C6_11 F8_11 106.1(2) . . ?
F9_11 C6_11 C7_11 110.2(2) . . ?
F8_11 C6_11 C7_11 110.9(2) . . ?
F9_11 C6_11 C5_11 110.9(2) . . ?
F8_11 C6_11 C5_11 109.5(2) . . ?
C7_11 C6_11 C5_11 109.3(2) . . ?
F10_11 C7_11 C6_11 109.1(3) . . ?
F10_11 C7_11 C8_11 109.7(2) . . ?
C6_11 C7_11 C8_11 109.1(2) . . ?
F10_11 C7_11 C3_11 110.2(2) . . ?
C6_11 C7_11 C3_11 109.5(2) . . ?
C8_11 C7_11 C3_11 109.3(3) . . ?
F12_11 C8_11 F11_11 105.6(2) . . ?
F12_11 C8_11 C7_11 110.2(3) . . ?
F11_11 C8_11 C7_11 110.7(3) . . ?
F12_11 C8_11 C9_11 110.6(2) . . ?
F11_11 C8_11 C9_11 109.9(3) . . ?
C7_11 C8_11 C9_11 109.7(2) . . ?
F13_11 C9_11 C10_11 109.3(2) . . ?
F13_11 C9_11 C2_11 110.0(2) . . ?
C10_11 C9_11 C2_11 110.0(2) . . ?
F13_11 C9_11 C8_11 109.4(2) . . ?
C10_11 C9_11 C8_11 108.6(2) . . ?
C2_11 C9_11 C8_11 109.6(2) . . ?
F15_11 C10_11 F14_11 105.8(2) . . ?
F15_11 C10_11 C5_11 110.3(2) . . ?
F14_11 C10_11 C5_11 110.0(2) . . ?
F15_11 C10_11 C9_11 110.9(2) . . ?
F14_11 C10_11 C9_11 110.7(2) . . ?
C5_11 C10_11 C9_11 109.1(2) . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
F1_1 C1_1 C2_1 F2_1 -1.1(8) . . . . ?
C6_1 C1_1 C2_1 F2_1 -179.7(6) . . . . ?
F1_1 C1_1 C2_1 C3_1 178.2(6) . . . . ?
C6_1 C1_1 C2_1 C3_1 -0.4(7) . . . . ?
F2_1 C2_1 C3_1 C4_1 -179.5(6) . . . . ?
C1_1 C2_1 C3_1 C4_1 1.2(7) . . . . ?
F2_1 C2_1 C3_1 Ag2 123.2(6) . . . . ?
C1_1 C2_1 C3_1 Ag2 -56.1(5) . . . . ?
F2_1 C2_1 C3_1 Ag1 133.1(6) . . . . ?
C1_1 C2_1 C3_1 Ag1 -46.2(5) . . . . ?
F2_1 C2_1 C3_1 Ag3 138.1(6) . . . . ?
C1_1 C2_1 C3_1 Ag3 -41.2(5) . . . . ?
C2_1 C3_1 C4_1 C5_1 -1.1(9) . . . . ?
Ag2 C3_1 C4_1 C5_1 79.6(6) . . . . ?
Ag1 C3_1 C4_1 C5_1 68.1(6) . . . . ?
Ag3 C3_1 C4_1 C5_1 53.4(6) . . . . ?
C2_1 C3_1 C4_1 Ag2 -80.8(5) . . . . ?
C2_1 C3_1 C4_1 Ag1 -69.2(6) . . . . ?
C2_1 C3_1 C4_1 Ag3 -54.5(6) . . . . ?
C3_1 C4_1 C5_1 C6_1 0.2(9) . . . . ?
Ag2 C4_1 C5_1 C6_1 86.9(6) . . . . ?
Ag1 C4_1 C5_1 C6_1 90.0(6) . . . . ?
Ag3 C4_1 C5_1 C6_1 80.4(6) . . . . ?
C3_1 C4_1 C5_1 Ag3 -80.2(7) . . . . ?
C3_1 C4_1 C5_1 Ag1 -89.8(6) . . . . ?
C3_1 C4_1 C5_1 Ag2 -86.7(6) . . . . ?
F1_1 C1_1 C6_1 C5_1 -179.2(6) . . . . ?
C2_1 C1_1 C6_1 C5_1 -0.5(8) . . . . ?
F1_1 C1_1 C6_1 Ag3 -107.3(6) . . . . ?
C2_1 C1_1 C6_1 Ag3 71.4(6) . . . . ?
F1_1 C1_1 C6_1 Ag1 -121.8(5) . . . . ?
C2_1 C1_1 C6_1 Ag1 56.9(5) . . . . ?
F1_1 C1_1 C6_1 Ag2 -129.6(5) . . . . ?
C2_1 C1_1 C6_1 Ag2 49.1(5) . . . . ?
C4_1 C5_1 C6_1 C1_1 0.6(9) . . . . ?
Ag3 C5_1 C6_1 C1_1 92.9(6) . . . . ?
Ag1 C5_1 C6_1 C1_1 83.7(5) . . . . ?
Ag2 C5_1 C6_1 C1_1 68.9(6) . . . . ?
C4_1 C5_1 C6_1 Ag3 -92.3(6) . . . . ?
C4_1 C5_1 C6_1 Ag1 -83.0(6) . . . . ?
C4_1 C5_1 C6_1 Ag2 -68.2(6) . . . . ?
F1_2 C1_2 C2_2 F2_2 -1(4) . . . . ?
C6_2 C1_2 C2_2 F2_2 178(3) . . . . ?
Ag2 C1_2 C2_2 F2_2 124(2) . . . . ?
F1_2 C1_2 C2_2 C3_2 -180(3) . . . . ?
C6_2 C1_2 C2_2 C3_2 -2(3) . . . . ?
Ag2 C1_2 C2_2 C3_2 -55.4(14) . . . . ?
F2_2 C2_2 C3_2 C4_2 -180(4) . . . . ?
C1_2 C2_2 C3_2 C4_2 -1(3) . . . . ?
F2_2 C2_2 C3_2 Ag3 -127(3) . . . . ?
C1_2 C2_2 C3_2 Ag3 52.3(15) . . . . ?
F2_2 C2_2 C3_2 Ag1 -134(3) . . . . ?
C1_2 C2_2 C3_2 Ag1 44.8(14) . . . . ?
F2_2 C2_2 C3_2 Ag2 -135(3) . . . . ?
C1_2 C2_2 C3_2 Ag2 43.7(14) . . . . ?
C2_2 C3_2 C4_2 C5_2 2(5) . . . . ?
Ag3 C3_2 C4_2 C5_2 -74(4) . . . . ?
Ag1 C3_2 C4_2 C5_2 -59(4) . . . . ?
Ag2 C3_2 C4_2 C5_2 -48(4) . . . . ?
C2_2 C3_2 C4_2 Ag3 75(3) . . . . ?
C2_2 C3_2 C4_2 Ag1 60(3) . . . . ?
C2_2 C3_2 C4_2 Ag2 49(2) . . . . ?
C3_2 C4_2 C5_2 C6_2 0(7) . . . . ?
Ag3 C4_2 C5_2 C6_2 -88(4) . . . . ?
Ag1 C4_2 C5_2 C6_2 -82(4) . . . . ?
Ag2 C4_2 C5_2 C6_2 -68(4) . . . . ?
C3_2 C4_2 C5_2 Ag1 82(4) . . . . ?
C3_2 C4_2 C5_2 Ag2 68(4) . . . . ?
C3_2 C4_2 C5_2 Ag3 87(4) . . . . ?
F1_2 C1_2 C6_2 C5_2 -179(4) . . . . ?
C2_2 C1_2 C6_2 C5_2 3(5) . . . . ?
Ag2 C1_2 C6_2 C5_2 80(4) . . . . ?
F1_2 C1_2 C6_2 Ag2 101(3) . . . . ?
C2_2 C1_2 C6_2 Ag2 -77(3) . . . . ?
F1_2 C1_2 C6_2 Ag1 115(2) . . . . ?
C2_2 C1_2 C6_2 Ag1 -63(3) . . . . ?
F1_2 C1_2 C6_2 Ag3 128(2) . . . . ?
C2_2 C1_2 C6_2 Ag3 -51(3) . . . . ?
C4_2 C5_2 C6_2 C1_2 -2(6) . . . . ?
Ag1 C5_2 C6_2 C1_2 -89(4) . . . . ?
Ag2 C5_2 C6_2 C1_2 -89(4) . . . . ?
Ag3 C5_2 C6_2 C1_2 -77(4) . . . . ?
C4_2 C5_2 C6_2 Ag2 87(4) . . . . ?
C4_2 C5_2 C6_2 Ag1 87(4) . . . . ?
C4_2 C5_2 C6_2 Ag3 74(4) . . . . ?
F1_3 C1_3 C2_3 F2_3 -1.3(11) . . . . ?
C6_3 C1_3 C2_3 F2_3 178.9(8) . . . . ?
F1_3 C1_3 C2_3 C3_3 179.8(8) . . . . ?
C6_3 C1_3 C2_3 C3_3 -0.1(11) . . . . ?
F2_3 C2_3 C3_3 C4_3 -178.9(8) . . . . ?
C1_3 C2_3 C3_3 C4_3 0.0(12) . . . . ?
F2_3 C2_3 C3_3 Ag2 -108.2(6) . . . . ?
C1_3 C2_3 C3_3 Ag2 70.7(7) . . . . ?
F2_3 C2_3 C3_3 Ag1 -121.7(6) . . . . ?
C1_3 C2_3 C3_3 Ag1 57.3(7) . . . . ?
F2_3 C2_3 C3_3 Ag3 -133.0(6) . . . . ?
C1_3 C2_3 C3_3 Ag3 46.0(7) . . . . ?
C2_3 C3_3 C4_3 C5_3 0.2(13) . . . . ?
Ag2 C3_3 C4_3 C5_3 -92.8(7) . . . . ?
Ag1 C3_3 C4_3 C5_3 -86.2(7) . . . . ?
Ag3 C3_3 C4_3 C5_3 -69.5(7) . . . . ?
C2_3 C3_3 C4_3 Ag1 86.4(9) . . . . ?
C2_3 C3_3 C4_3 Ag2 92.9(8) . . . . ?
C2_3 C3_3 C4_3 Ag3 69.7(10) . . . . ?
C3_3 C4_3 C5_3 C6_3 -0.3(12) . . . . ?
Ag1 C4_3 C5_3 C6_3 -92.5(8) . . . . ?
Ag2 C4_3 C5_3 C6_3 -81.9(8) . . . . ?
Ag3 C4_3 C5_3 C6_3 -92.1(8) . . . . ?
C3_3 C4_3 C5_3 Ag3 91.8(8) . . . . ?
C3_3 C4_3 C5_3 Ag1 92.2(8) . . . . ?
C3_3 C4_3 C5_3 Ag2 81.6(8) . . . . ?
F1_3 C1_3 C6_3 C5_3 -179.9(8) . . . . ?
C2_3 C1_3 C6_3 C5_3 0.0(14) . . . . ?
F1_3 C1_3 C6_3 Ag3 128.0(7) . . . . ?
C2_3 C1_3 C6_3 Ag3 -52.1(9) . . . . ?
F1_3 C1_3 C6_3 Ag1 135.6(7) . . . . ?
C2_3 C1_3 C6_3 Ag1 -44.5(8) . . . . ?
F1_3 C1_3 C6_3 Ag2 138.8(8) . . . . ?
C2_3 C1_3 C6_3 Ag2 -41.3(7) . . . . ?
C4_3 C5_3 C6_3 C1_3 0.2(14) . . . . ?
Ag3 C5_3 C6_3 C1_3 -80.8(10) . . . . ?
Ag1 C5_3 C6_3 C1_3 -67.0(10) . . . . ?
Ag2 C5_3 C6_3 C1_3 -54.0(10) . . . . ?
C4_3 C5_3 C6_3 Ag3 81.0(8) . . . . ?
C4_3 C5_3 C6_3 Ag1 67.2(7) . . . . ?
C4_3 C5_3 C6_3 Ag2 54.2(6) . . . . ?
F1_4 C1_4 C2_4 F2_4 -2(2) . . . . ?
C6_4 C1_4 C2_4 F2_4 176.7(18) . . . . ?
F1_4 C1_4 C2_4 C3_4 179.9(16) . . . . ?
C6_4 C1_4 C2_4 C3_4 -1.1(18) . . . . ?
F2_4 C2_4 C3_4 C4_4 178(2) . . . . ?
C1_4 C2_4 C3_4 C4_4 -4.6(18) . . . . ?
F2_4 C2_4 C3_4 Ag2 -123.6(13) . . . . ?
C1_4 C2_4 C3_4 Ag2 54.1(11) . . . . ?
F2_4 C2_4 C3_4 Ag1 -131.5(12) . . . . ?
C1_4 C2_4 C3_4 Ag1 46.2(10) . . . . ?
F2_4 C2_4 C3_4 Ag3 -136.2(12) . . . . ?
C1_4 C2_4 C3_4 Ag3 41.5(9) . . . . ?
C2_4 C3_4 C4_4 C5_4 8(3) . . . . ?
Ag2 C3_4 C4_4 C5_4 -82(2) . . . . ?
Ag1 C3_4 C4_4 C5_4 -69(2) . . . . ?
Ag3 C3_4 C4_4 C5_4 -54(2) . . . . ?
C2_4 C3_4 C4_4 Ag2 89.7(14) . . . . ?
C2_4 C3_4 C4_4 Ag1 77.3(15) . . . . ?
C2_4 C3_4 C4_4 Ag3 61.8(16) . . . . ?
C3_4 C4_4 C5_4 C6_4 -6(4) . . . . ?
Ag2 C4_4 C5_4 C6_4 -96.2(19) . . . . ?
Ag1 C4_4 C5_4 C6_4 -96.9(19) . . . . ?
Ag3 C4_4 C5_4 C6_4 -86.1(19) . . . . ?
C3_4 C4_4 C5_4 Ag3 80(2) . . . . ?
C3_4 C4_4 C5_4 Ag1 91(2) . . . . ?
C3_4 C4_4 C5_4 Ag2 90(2) . . . . ?
F1_4 C1_4 C6_4 C5_4 -177.7(18) . . . . ?
C2_4 C1_4 C6_4 C5_4 3(3) . . . . ?
F1_4 C1_4 C6_4 Ag3 114.8(16) . . . . ?
C2_4 C1_4 C6_4 Ag3 -64.2(17) . . . . ?
F1_4 C1_4 C6_4 Ag1 127.5(15) . . . . ?
C2_4 C1_4 C6_4 Ag1 -51.4(17) . . . . ?
F1_4 C1_4 C6_4 Ag2 136.2(15) . . . . ?
C2_4 C1_4 C6_4 Ag2 -42.7(16) . . . . ?
C4_4 C5_4 C6_4 C1_4 0(3) . . . . ?
Ag3 C5_4 C6_4 C1_4 -94.1(18) . . . . ?
Ag1 C5_4 C6_4 C1_4 -86.6(19) . . . . ?
Ag2 C5_4 C6_4 C1_4 -72(2) . . . . ?
C4_4 C5_4 C6_4 Ag3 94(2) . . . . ?
C4_4 C5_4 C6_4 Ag1 87(2) . . . . ?
C4_4 C5_4 C6_4 Ag2 72.0(19) . . . . ?
O1_7 Al1 O1_5 C1_5 -35.5(6) . . . . ?
O1_11 Al1 O1_5 C1_5 83.9(6) . . . . ?
O1_9 Al1 O1_5 C1_5 -159.3(7) . . . . ?
Al1 O1_5 C1_5 C3_5 77.7(7) . . . . ?
Al1 O1_5 C1_5 C2_5 -163.7(5) . . . . ?
Al1 O1_5 C1_5 C4_5 -44.6(8) . . . . ?
O1_5 C1_5 C2_5 F1_5 -56.7(5) . . . . ?
C3_5 C1_5 C2_5 F1_5 64.7(5) . . . . ?
C4_5 C1_5 C2_5 F1_5 -180.0(4) . . . . ?
O1_5 C1_5 C2_5 F2_5 59.4(5) . . . . ?
C3_5 C1_5 C2_5 F2_5 -179.2(4) . . . . ?
C4_5 C1_5 C2_5 F2_5 -63.8(5) . . . . ?
O1_5 C1_5 C2_5 C9_5 -179.0(4) . . . . ?
C3_5 C1_5 C2_5 C9_5 -57.6(5) . . . . ?
C4_5 C1_5 C2_5 C9_5 57.8(5) . . . . ?
O1_5 C1_5 C3_5 F4_5 -61.7(5) . . . . ?
C2_5 C1_5 C3_5 F4_5 179.1(4) . . . . ?
C4_5 C1_5 C3_5 F4_5 64.0(5) . . . . ?
O1_5 C1_5 C3_5 F3_5 55.5(5) . . . . ?
C2_5 C1_5 C3_5 F3_5 -63.7(5) . . . . ?
C4_5 C1_5 C3_5 F3_5 -178.8(4) . . . . ?
O1_5 C1_5 C3_5 C7_5 176.1(4) . . . . ?
C2_5 C1_5 C3_5 C7_5 56.9(5) . . . . ?
C4_5 C1_5 C3_5 C7_5 -58.2(5) . . . . ?
O1_5 C1_5 C4_5 F5_5 59.8(6) . . . . ?
C3_5 C1_5 C4_5 F5_5 -65.0(5) . . . . ?
C2_5 C1_5 C4_5 F5_5 179.7(4) . . . . ?
O1_5 C1_5 C4_5 F6_5 -56.7(6) . . . . ?
C3_5 C1_5 C4_5 F6_5 178.5(4) . . . . ?
C2_5 C1_5 C4_5 F6_5 63.2(5) . . . . ?
O1_5 C1_5 C4_5 C5_5 -178.3(5) . . . . ?
C3_5 C1_5 C4_5 C5_5 57.0(5) . . . . ?
C2_5 C1_5 C4_5 C5_5 -58.3(5) . . . . ?
F5_5 C4_5 C5_5 F7_5 -56.3(8) . . . . ?
F6_5 C4_5 C5_5 F7_5 59.3(8) . . . . ?
C1_5 C4_5 C5_5 F7_5 -178.7(7) . . . . ?
F5_5 C4_5 C5_5 C10_5 -177.3(5) . . . . ?
F6_5 C4_5 C5_5 C10_5 -61.7(7) . . . . ?
C1_5 C4_5 C5_5 C10_5 60.4(6) . . . . ?
F5_5 C4_5 C5_5 C6_5 63.4(7) . . . . ?
F6_5 C4_5 C5_5 C6_5 179.0(5) . . . . ?
C1_5 C4_5 C5_5 C6_5 -58.9(6) . . . . ?
F7_5 C5_5 C6_5 F8_5 58.7(8) . . . . ?
C10_5 C5_5 C6_5 F8_5 178.2(5) . . . . ?
C4_5 C5_5 C6_5 F8_5 -62.2(7) . . . . ?
F7_5 C5_5 C6_5 F9_5 -58.1(9) . . . . ?
C10_5 C5_5 C6_5 F9_5 61.3(7) . . . . ?
C4_5 C5_5 C6_5 F9_5 -179.1(5) . . . . ?
F7_5 C5_5 C6_5 C7_5 -179.7(7) . . . . ?
C10_5 C5_5 C6_5 C7_5 -60.2(6) . . . . ?
C4_5 C5_5 C6_5 C7_5 59.4(6) . . . . ?
F8_5 C6_5 C7_5 F10_5 -58.5(7) . . . . ?
F9_5 C6_5 C7_5 F10_5 59.2(7) . . . . ?
C5_5 C6_5 C7_5 F10_5 -179.2(5) . . . . ?
F8_5 C6_5 C7_5 C8_5 -179.1(5) . . . . ?
F9_5 C6_5 C7_5 C8_5 -61.5(7) . . . . ?
C5_5 C6_5 C7_5 C8_5 60.2(6) . . . . ?
F8_5 C6_5 C7_5 C3_5 61.2(6) . . . . ?
F9_5 C6_5 C7_5 C3_5 178.9(5) . . . . ?
C5_5 C6_5 C7_5 C3_5 -59.5(6) . . . . ?
F4_5 C3_5 C7_5 F10_5 57.6(7) . . . . ?
F3_5 C3_5 C7_5 F10_5 -58.1(7) . . . . ?
C1_5 C3_5 C7_5 F10_5 -179.7(6) . . . . ?
F4_5 C3_5 C7_5 C8_5 178.4(5) . . . . ?
F3_5 C3_5 C7_5 C8_5 62.8(6) . . . . ?
C1_5 C3_5 C7_5 C8_5 -58.9(6) . . . . ?
F4_5 C3_5 C7_5 C6_5 -62.1(6) . . . . ?
F3_5 C3_5 C7_5 C6_5 -177.8(5) . . . . ?
C1_5 C3_5 C7_5 C6_5 60.6(6) . . . . ?
F10_5 C7_5 C8_5 F11_5 57.6(9) . . . . ?
C6_5 C7_5 C8_5 F11_5 177.8(7) . . . . ?
C3_5 C7_5 C8_5 F11_5 -62.8(8) . . . . ?
F10_5 C7_5 C8_5 F12_5 -59.2(8) . . . . ?
C6_5 C7_5 C8_5 F12_5 61.0(8) . . . . ?
C3_5 C7_5 C8_5 F12_5 -179.6(7) . . . . ?
F10_5 C7_5 C8_5 C9_5 179.1(6) . . . . ?
C6_5 C7_5 C8_5 C9_5 -60.7(7) . . . . ?
C3_5 C7_5 C8_5 C9_5 58.6(7) . . . . ?
F11_5 C8_5 C9_5 F13_5 -57.8(7) . . . . ?
F12_5 C8_5 C9_5 F13_5 58.1(8) . . . . ?
C7_5 C8_5 C9_5 F13_5 -179.6(5) . . . . ?
F11_5 C8_5 C9_5 C2_5 62.3(7) . . . . ?
F12_5 C8_5 C9_5 C2_5 178.2(6) . . . . ?
C7_5 C8_5 C9_5 C2_5 -59.5(7) . . . . ?
F11_5 C8_5 C9_5 C10_5 -177.3(6) . . . . ?
F12_5 C8_5 C9_5 C10_5 -61.4(7) . . . . ?
C7_5 C8_5 C9_5 C10_5 60.9(7) . . . . ?
F1_5 C2_5 C9_5 F13_5 58.6(6) . . . . ?
F2_5 C2_5 C9_5 F13_5 -56.5(6) . . . . ?
C1_5 C2_5 C9_5 F13_5 -178.9(4) . . . . ?
F1_5 C2_5 C9_5 C8_5 -62.3(6) . . . . ?
F2_5 C2_5 C9_5 C8_5 -177.4(5) . . . . ?
C1_5 C2_5 C9_5 C8_5 60.2(6) . . . . ?
F1_5 C2_5 C9_5 C10_5 178.1(4) . . . . ?
F2_5 C2_5 C9_5 C10_5 63.0(5) . . . . ?
C1_5 C2_5 C9_5 C10_5 -59.3(6) . . . . ?
F7_5 C5_5 C10_5 F15_5 56.8(9) . . . . ?
C6_5 C5_5 C10_5 F15_5 -61.8(7) . . . . ?
C4_5 C5_5 C10_5 F15_5 178.0(5) . . . . ?
F7_5 C5_5 C10_5 F14_5 -59.2(9) . . . . ?
C6_5 C5_5 C10_5 F14_5 -177.8(5) . . . . ?
C4_5 C5_5 C10_5 F14_5 62.0(6) . . . . ?
F7_5 C5_5 C10_5 C9_5 179.6(8) . . . . ?
C6_5 C5_5 C10_5 C9_5 61.0(6) . . . . ?
C4_5 C5_5 C10_5 C9_5 -59.2(6) . . . . ?
F13_5 C9_5 C10_5 F15_5 -58.5(6) . . . . ?
C8_5 C9_5 C10_5 F15_5 61.8(6) . . . . ?
C2_5 C9_5 C10_5 F15_5 -178.0(5) . . . . ?
F13_5 C9_5 C10_5 F14_5 56.8(6) . . . . ?
C8_5 C9_5 C10_5 F14_5 177.1(5) . . . . ?
C2_5 C9_5 C10_5 F14_5 -62.7(6) . . . . ?
F13_5 C9_5 C10_5 C5_5 178.4(5) . . . . ?
C8_5 C9_5 C10_5 C5_5 -61.4(6) . . . . ?
C2_5 C9_5 C10_5 C5_5 58.8(6) . . . . ?
O1_11 Al1 O1_6 C1_6 -41.2(11) . . . . ?
O1_10 Al1 O1_6 C1_6 94.7(11) . . . . ?
O1_8 Al1 O1_6 C1_6 -153.0(10) . . . . ?
Al1 O1_6 C1_6 C4_6 -171.0(8) . . . . ?
Al1 O1_6 C1_6 C3_6 -51.6(13) . . . . ?
Al1 O1_6 C1_6 C2_6 69.7(12) . . . . ?
O1_6 C1_6 C2_6 F1_6 -60.5(10) . . . . ?
C4_6 C1_6 C2_6 F1_6 179.1(8) . . . . ?
C3_6 C1_6 C2_6 F1_6 62.9(9) . . . . ?
O1_6 C1_6 C2_6 F2_6 57.2(10) . . . . ?
C4_6 C1_6 C2_6 F2_6 -63.2(9) . . . . ?
C3_6 C1_6 C2_6 F2_6 -179.4(7) . . . . ?
O1_6 C1_6 C2_6 C9_6 178.9(8) . . . . ?
C4_6 C1_6 C2_6 C9_6 58.5(9) . . . . ?
C3_6 C1_6 C2_6 C9_6 -57.7(9) . . . . ?
O1_6 C1_6 C3_6 F4_6 -56.8(8) . . . . ?
C4_6 C1_6 C3_6 F4_6 63.5(8) . . . . ?
C2_6 C1_6 C3_6 F4_6 179.4(7) . . . . ?
O1_6 C1_6 C3_6 F3_6 60.2(8) . . . . ?
C4_6 C1_6 C3_6 F3_6 -179.5(6) . . . . ?
C2_6 C1_6 C3_6 F3_6 -63.6(8) . . . . ?
O1_6 C1_6 C3_6 C7_6 -178.2(6) . . . . ?
C4_6 C1_6 C3_6 C7_6 -57.9(8) . . . . ?
C2_6 C1_6 C3_6 C7_6 58.0(8) . . . . ?
O1_6 C1_6 C4_6 F5_6 57.2(9) . . . . ?
C3_6 C1_6 C4_6 F5_6 -64.6(8) . . . . ?
C2_6 C1_6 C4_6 F5_6 179.3(7) . . . . ?
O1_6 C1_6 C4_6 F6_6 -59.4(8) . . . . ?
C3_6 C1_6 C4_6 F6_6 178.9(6) . . . . ?
C2_6 C1_6 C4_6 F6_6 62.7(8) . . . . ?
O1_6 C1_6 C4_6 C5_6 179.7(7) . . . . ?
C3_6 C1_6 C4_6 C5_6 58.0(9) . . . . ?
C2_6 C1_6 C4_6 C5_6 -58.2(9) . . . . ?
F5_6 C4_6 C5_6 F7_6 -56.1(12) . . . . ?
F6_6 C4_6 C5_6 F7_6 60.4(12) . . . . ?
C1_6 C4_6 C5_6 F7_6 -178.5(10) . . . . ?
F5_6 C4_6 C5_6 C6_6 61.9(10) . . . . ?
F6_6 C4_6 C5_6 C6_6 178.4(8) . . . . ?
C1_6 C4_6 C5_6 C6_6 -60.5(10) . . . . ?
F5_6 C4_6 C5_6 C10_6 -177.2(8) . . . . ?
F6_6 C4_6 C5_6 C10_6 -60.8(10) . . . . ?
C1_6 C4_6 C5_6 C10_6 60.3(10) . . . . ?
F7_6 C5_6 C6_6 F8_6 56.8(14) . . . . ?
C10_6 C5_6 C6_6 F8_6 178.1(11) . . . . ?
C4_6 C5_6 C6_6 F8_6 -61.6(13) . . . . ?
F7_6 C5_6 C6_6 F9_6 -58.8(14) . . . . ?
C10_6 C5_6 C6_6 F9_6 62.6(13) . . . . ?
C4_6 C5_6 C6_6 F9_6 -177.2(12) . . . . ?
F7_6 C5_6 C6_6 C7_6 179.0(10) . . . . ?
C10_6 C5_6 C6_6 C7_6 -59.7(11) . . . . ?
C4_6 C5_6 C6_6 C7_6 60.6(11) . . . . ?
F8_6 C6_6 C7_6 F10_6 -60.0(12) . . . . ?
F9_6 C6_6 C7_6 F10_6 56.8(13) . . . . ?
C5_6 C6_6 C7_6 F10_6 178.0(9) . . . . ?
F8_6 C6_6 C7_6 C8_6 -178.3(10) . . . . ?
F9_6 C6_6 C7_6 C8_6 -61.4(13) . . . . ?
C5_6 C6_6 C7_6 C8_6 59.7(11) . . . . ?
F8_6 C6_6 C7_6 C3_6 61.6(12) . . . . ?
F9_6 C6_6 C7_6 C3_6 178.4(11) . . . . ?
C5_6 C6_6 C7_6 C3_6 -60.4(11) . . . . ?
F4_6 C3_6 C7_6 F10_6 57.9(9) . . . . ?
F3_6 C3_6 C7_6 F10_6 -57.2(9) . . . . ?
C1_6 C3_6 C7_6 F10_6 -179.8(7) . . . . ?
F4_6 C3_6 C7_6 C8_6 178.0(7) . . . . ?
F3_6 C3_6 C7_6 C8_6 62.9(9) . . . . ?
C1_6 C3_6 C7_6 C8_6 -59.7(9) . . . . ?
F4_6 C3_6 C7_6 C6_6 -62.2(9) . . . . ?
F3_6 C3_6 C7_6 C6_6 -177.4(7) . . . . ?
C1_6 C3_6 C7_6 C6_6 60.0(9) . . . . ?
F10_6 C7_6 C8_6 F11_6 59.0(10) . . . . ?
C6_6 C7_6 C8_6 F11_6 177.5(8) . . . . ?
C3_6 C7_6 C8_6 F11_6 -62.8(10) . . . . ?
F10_6 C7_6 C8_6 F12_6 -57.9(10) . . . . ?
C6_6 C7_6 C8_6 F12_6 60.7(10) . . . . ?
C3_6 C7_6 C8_6 F12_6 -179.6(8) . . . . ?
F10_6 C7_6 C8_6 C9_6 -179.2(8) . . . . ?
C6_6 C7_6 C8_6 C9_6 -60.7(10) . . . . ?
C3_6 C7_6 C8_6 C9_6 59.0(9) . . . . ?
F11_6 C8_6 C9_6 F13_6 -55.9(15) . . . . ?
F12_6 C8_6 C9_6 F13_6 59.5(16) . . . . ?
C7_6 C8_6 C9_6 F13_6 -178.1(14) . . . . ?
F11_6 C8_6 C9_6 C10_6 -177.3(8) . . . . ?
F12_6 C8_6 C9_6 C10_6 -61.9(11) . . . . ?
C7_6 C8_6 C9_6 C10_6 60.5(10) . . . . ?
F11_6 C8_6 C9_6 C2_6 63.7(11) . . . . ?
F12_6 C8_6 C9_6 C2_6 179.1(9) . . . . ?
C7_6 C8_6 C9_6 C2_6 -58.6(11) . . . . ?
F1_6 C2_6 C9_6 F13_6 55.6(15) . . . . ?
F2_6 C2_6 C9_6 F13_6 -59.5(14) . . . . ?
C1_6 C2_6 C9_6 F13_6 177.8(13) . . . . ?
F1_6 C2_6 C9_6 C10_6 177.4(9) . . . . ?
F2_6 C2_6 C9_6 C10_6 62.3(11) . . . . ?
C1_6 C2_6 C9_6 C10_6 -60.4(11) . . . . ?
F1_6 C2_6 C9_6 C8_6 -63.5(11) . . . . ?
F2_6 C2_6 C9_6 C8_6 -178.5(9) . . . . ?
C1_6 C2_6 C9_6 C8_6 58.7(11) . . . . ?
F13_6 C9_6 C10_6 F14_6 58.6(15) . . . . ?
C8_6 C9_6 C10_6 F14_6 178.4(9) . . . . ?
C2_6 C9_6 C10_6 F14_6 -62.1(11) . . . . ?
F13_6 C9_6 C10_6 F15_6 -58.8(15) . . . . ?
C8_6 C9_6 C10_6 F15_6 61.1(11) . . . . ?
C2_6 C9_6 C10_6 F15_6 -179.5(9) . . . . ?
F13_6 C9_6 C10_6 C5_6 -179.1(13) . . . . ?
C8_6 C9_6 C10_6 C5_6 -59.3(11) . . . . ?
C2_6 C9_6 C10_6 C5_6 60.2(11) . . . . ?
F7_6 C5_6 C10_6 F14_6 -57.1(12) . . . . ?
C6_6 C5_6 C10_6 F14_6 -177.0(9) . . . . ?
C4_6 C5_6 C10_6 F14_6 62.9(11) . . . . ?
F7_6 C5_6 C10_6 F15_6 57.9(12) . . . . ?
C6_6 C5_6 C10_6 F15_6 -62.0(11) . . . . ?
C4_6 C5_6 C10_6 F15_6 177.9(9) . . . . ?
F7_6 C5_6 C10_6 C9_6 179.6(10) . . . . ?
C6_6 C5_6 C10_6 C9_6 59.7(10) . . . . ?
C4_6 C5_6 C10_6 C9_6 -60.4(10) . . . . ?
O1_11 Al1 O1_7 C1_7 45.6(6) . . . . ?
O1_9 Al1 O1_7 C1_7 -77.9(7) . . . . ?
O1_5 Al1 O1_7 C1_7 158.6(6) . . . . ?
Al1 O1_7 C1_7 C2_7 39.1(8) . . . . ?
Al1 O1_7 C1_7 C4_7 158.1(5) . . . . ?
Al1 O1_7 C1_7 C3_7 -82.8(7) . . . . ?
O1_7 C1_7 C2_7 F2_7 56.8(5) . . . . ?
C4_7 C1_7 C2_7 F2_7 -63.3(5) . . . . ?
C3_7 C1_7 C2_7 F2_7 -179.4(4) . . . . ?
O1_7 C1_7 C2_7 F1_7 -59.3(5) . . . . ?
C4_7 C1_7 C2_7 F1_7 -179.4(4) . . . . ?
C3_7 C1_7 C2_7 F1_7 64.5(5) . . . . ?
O1_7 C1_7 C2_7 C9_7 178.8(4) . . . . ?
C4_7 C1_7 C2_7 C9_7 58.7(5) . . . . ?
C3_7 C1_7 C2_7 C9_7 -57.5(5) . . . . ?
O1_7 C1_7 C3_7 F4_7 -56.4(5) . . . . ?
C2_7 C1_7 C3_7 F4_7 179.2(4) . . . . ?
C4_7 C1_7 C3_7 F4_7 63.4(5) . . . . ?
O1_7 C1_7 C3_7 F3_7 60.2(6) . . . . ?
C2_7 C1_7 C3_7 F3_7 -64.2(5) . . . . ?
C4_7 C1_7 C3_7 F3_7 -180.0(4) . . . . ?
O1_7 C1_7 C3_7 C7_7 -177.9(4) . . . . ?
C2_7 C1_7 C3_7 C7_7 57.7(5) . . . . ?
C4_7 C1_7 C3_7 C7_7 -58.0(5) . . . . ?
O1_7 C1_7 C4_7 F5_7 57.8(5) . . . . ?
C2_7 C1_7 C4_7 F5_7 -179.8(4) . . . . ?
C3_7 C1_7 C4_7 F5_7 -63.5(5) . . . . ?
O1_7 C1_7 C4_7 F6_7 -58.9(5) . . . . ?
C2_7 C1_7 C4_7 F6_7 63.4(5) . . . . ?
C3_7 C1_7 C4_7 F6_7 179.8(4) . . . . ?
O1_7 C1_7 C4_7 C5_7 179.6(4) . . . . ?
C2_7 C1_7 C4_7 C5_7 -58.1(5) . . . . ?
C3_7 C1_7 C4_7 C5_7 58.2(6) . . . . ?
F5_7 C4_7 C5_7 F7_7 -57.0(8) . . . . ?
F6_7 C4_7 C5_7 F7_7 58.8(8) . . . . ?
C1_7 C4_7 C5_7 F7_7 -179.2(7) . . . . ?
F5_7 C4_7 C5_7 C10_7 -177.8(5) . . . . ?
F6_7 C4_7 C5_7 C10_7 -62.1(6) . . . . ?
C1_7 C4_7 C5_7 C10_7 59.9(6) . . . . ?
F5_7 C4_7 C5_7 C6_7 62.4(6) . . . . ?
F6_7 C4_7 C5_7 C6_7 178.1(5) . . . . ?
C1_7 C4_7 C5_7 C6_7 -59.9(6) . . . . ?
F7_7 C5_7 C6_7 F8_7 56.6(8) . . . . ?
C10_7 C5_7 C6_7 F8_7 177.8(5) . . . . ?
C4_7 C5_7 C6_7 F8_7 -62.4(7) . . . . ?
F7_7 C5_7 C6_7 F9_7 -60.0(8) . . . . ?
C10_7 C5_7 C6_7 F9_7 61.2(7) . . . . ?
C4_7 C5_7 C6_7 F9_7 -179.0(5) . . . . ?
F7_7 C5_7 C6_7 C7_7 179.1(7) . . . . ?
C10_7 C5_7 C6_7 C7_7 -59.8(6) . . . . ?
C4_7 C5_7 C6_7 C7_7 60.0(7) . . . . ?
F8_7 C6_7 C7_7 F10_7 -59.3(10) . . . . ?
F9_7 C6_7 C7_7 F10_7 57.4(10) . . . . ?
C5_7 C6_7 C7_7 F10_7 178.7(9) . . . . ?
F8_7 C6_7 C7_7 C8_7 -178.6(5) . . . . ?
F9_7 C6_7 C7_7 C8_7 -61.9(7) . . . . ?
C5_7 C6_7 C7_7 C8_7 59.4(7) . . . . ?
F8_7 C6_7 C7_7 C3_7 61.8(7) . . . . ?
F9_7 C6_7 C7_7 C3_7 178.5(6) . . . . ?
C5_7 C6_7 C7_7 C3_7 -60.2(7) . . . . ?
F4_7 C3_7 C7_7 F10_7 58.8(10) . . . . ?
F3_7 C3_7 C7_7 F10_7 -57.5(10) . . . . ?
C1_7 C3_7 C7_7 F10_7 -179.5(9) . . . . ?
F4_7 C3_7 C7_7 C6_7 -61.7(6) . . . . ?
F3_7 C3_7 C7_7 C6_7 -177.9(5) . . . . ?
C1_7 C3_7 C7_7 C6_7 60.1(6) . . . . ?
F4_7 C3_7 C7_7 C8_7 178.5(5) . . . . ?
F3_7 C3_7 C7_7 C8_7 62.3(7) . . . . ?
C1_7 C3_7 C7_7 C8_7 -59.7(6) . . . . ?
F10_7 C7_7 C8_7 F11_7 59.6(10) . . . . ?
C6_7 C7_7 C8_7 F11_7 179.1(5) . . . . ?
C3_7 C7_7 C8_7 F11_7 -61.1(7) . . . . ?
F10_7 C7_7 C8_7 F12_7 -56.8(10) . . . . ?
C6_7 C7_7 C8_7 F12_7 62.7(7) . . . . ?
C3_7 C7_7 C8_7 F12_7 -177.5(5) . . . . ?
F10_7 C7_7 C8_7 C9_7 -179.2(9) . . . . ?
C6_7 C7_7 C8_7 C9_7 -59.7(6) . . . . ?
C3_7 C7_7 C8_7 C9_7 60.1(6) . . . . ?
F11_7 C8_7 C9_7 F13_7 -59.5(6) . . . . ?
F12_7 C8_7 C9_7 F13_7 56.9(6) . . . . ?
C7_7 C8_7 C9_7 F13_7 179.0(5) . . . . ?
F11_7 C8_7 C9_7 C2_7 61.8(6) . . . . ?
F12_7 C8_7 C9_7 C2_7 178.2(5) . . . . ?
C7_7 C8_7 C9_7 C2_7 -59.8(6) . . . . ?
F11_7 C8_7 C9_7 C10_7 -178.6(5) . . . . ?
F12_7 C8_7 C9_7 C10_7 -62.2(6) . . . . ?
C7_7 C8_7 C9_7 C10_7 59.8(6) . . . . ?
F2_7 C2_7 C9_7 F13_7 -57.2(5) . . . . ?
F1_7 C2_7 C9_7 F13_7 57.6(5) . . . . ?
C1_7 C2_7 C9_7 F13_7 179.9(4) . . . . ?
F2_7 C2_7 C9_7 C8_7 -177.8(4) . . . . ?
F1_7 C2_7 C9_7 C8_7 -63.0(5) . . . . ?
C1_7 C2_7 C9_7 C8_7 59.3(5) . . . . ?
F2_7 C2_7 C9_7 C10_7 62.2(5) . . . . ?
F1_7 C2_7 C9_7 C10_7 177.1(4) . . . . ?
C1_7 C2_7 C9_7 C10_7 -60.6(5) . . . . ?
F7_7 C5_7 C10_7 F15_7 58.7(8) . . . . ?
C4_7 C5_7 C10_7 F15_7 178.6(6) . . . . ?
C6_7 C5_7 C10_7 F15_7 -61.8(7) . . . . ?
F7_7 C5_7 C10_7 F14_7 -58.2(8) . . . . ?
C4_7 C5_7 C10_7 F14_7 61.7(8) . . . . ?
C6_7 C5_7 C10_7 F14_7 -178.6(6) . . . . ?
F7_7 C5_7 C10_7 C9_7 -179.7(6) . . . . ?
C4_7 C5_7 C10_7 C9_7 -59.8(7) . . . . ?
C6_7 C5_7 C10_7 C9_7 59.8(7) . . . . ?
F13_7 C9_7 C10_7 F15_7 -57.8(7) . . . . ?
C8_7 C9_7 C10_7 F15_7 61.7(7) . . . . ?
C2_7 C9_7 C10_7 F15_7 -178.3(5) . . . . ?
F13_7 C9_7 C10_7 F14_7 58.8(8) . . . . ?
C8_7 C9_7 C10_7 F14_7 178.3(7) . . . . ?
C2_7 C9_7 C10_7 F14_7 -61.8(7) . . . . ?
F13_7 C9_7 C10_7 C5_7 -179.5(5) . . . . ?
C8_7 C9_7 C10_7 C5_7 -60.0(6) . . . . ?
C2_7 C9_7 C10_7 C5_7 60.0(6) . . . . ?
O1_6 Al1 O1_8 C1_8 37.3(11) . . . . ?
O1_11 Al1 O1_8 C1_8 -85.5(11) . . . . ?
O1_10 Al1 O1_8 C1_8 158.8(11) . . . . ?
Al1 O1_8 C1_8 C2_8 161.7(8) . . . . ?
Al1 O1_8 C1_8 C4_8 -78.1(12) . . . . ?
Al1 O1_8 C1_8 C3_8 42.4(13) . . . . ?
O1_8 C1_8 C2_8 F1_8 -58.9(8) . . . . ?
C4_8 C1_8 C2_8 F1_8 179.6(6) . . . . ?
C3_8 C1_8 C2_8 F1_8 63.7(7) . . . . ?
O1_8 C1_8 C2_8 F2_8 57.3(7) . . . . ?
C4_8 C1_8 C2_8 F2_8 -64.2(7) . . . . ?
C3_8 C1_8 C2_8 F2_8 179.9(6) . . . . ?
O1_8 C1_8 C2_8 C9_8 178.3(6) . . . . ?
C4_8 C1_8 C2_8 C9_8 56.8(8) . . . . ?
C3_8 C1_8 C2_8 C9_8 -59.0(8) . . . . ?
O1_8 C1_8 C3_8 F4_8 -59.2(9) . . . . ?
C2_8 C1_8 C3_8 F4_8 -179.6(6) . . . . ?
C4_8 C1_8 C3_8 F4_8 63.5(8) . . . . ?
O1_8 C1_8 C3_8 F3_8 57.9(9) . . . . ?
C2_8 C1_8 C3_8 F3_8 -62.6(8) . . . . ?
C4_8 C1_8 C3_8 F3_8 -179.5(7) . . . . ?
O1_8 C1_8 C3_8 C7_8 179.0(7) . . . . ?
C2_8 C1_8 C3_8 C7_8 58.5(8) . . . . ?
C4_8 C1_8 C3_8 C7_8 -58.4(8) . . . . ?
O1_8 C1_8 C4_8 F5_8 59.6(9) . . . . ?
C2_8 C1_8 C4_8 F5_8 -180.0(6) . . . . ?
C3_8 C1_8 C4_8 F5_8 -64.1(8) . . . . ?
O1_8 C1_8 C4_8 F6_8 -57.4(9) . . . . ?
C2_8 C1_8 C4_8 F6_8 63.0(8) . . . . ?
C3_8 C1_8 C4_8 F6_8 179.0(7) . . . . ?
O1_8 C1_8 C4_8 C5_8 -177.0(7) . . . . ?
C2_8 C1_8 C4_8 C5_8 -56.6(8) . . . . ?
C3_8 C1_8 C4_8 C5_8 59.3(8) . . . . ?
F5_8 C4_8 C5_8 F7_8 -58.1(12) . . . . ?
F6_8 C4_8 C5_8 F7_8 57.4(12) . . . . ?
C1_8 C4_8 C5_8 F7_8 177.8(11) . . . . ?
F5_8 C4_8 C5_8 C10_8 -177.4(8) . . . . ?
F6_8 C4_8 C5_8 C10_8 -62.0(10) . . . . ?
C1_8 C4_8 C5_8 C10_8 58.4(10) . . . . ?
F5_8 C4_8 C5_8 C6_8 63.1(10) . . . . ?
F6_8 C4_8 C5_8 C6_8 178.5(8) . . . . ?
C1_8 C4_8 C5_8 C6_8 -61.1(10) . . . . ?
F7_8 C5_8 C6_8 F9_8 -56.9(12) . . . . ?
C10_8 C5_8 C6_8 F9_8 61.4(11) . . . . ?
C4_8 C5_8 C6_8 F9_8 -178.4(9) . . . . ?
F7_8 C5_8 C6_8 F8_8 59.8(12) . . . . ?
C10_8 C5_8 C6_8 F8_8 178.1(9) . . . . ?
C4_8 C5_8 C6_8 F8_8 -61.6(10) . . . . ?
F7_8 C5_8 C6_8 C7_8 -178.8(10) . . . . ?
C10_8 C5_8 C6_8 C7_8 -60.5(10) . . . . ?
C4_8 C5_8 C6_8 C7_8 59.7(10) . . . . ?
F9_8 C6_8 C7_8 F10_8 58.0(17) . . . . ?
F8_8 C6_8 C7_8 F10_8 -58.5(17) . . . . ?
C5_8 C6_8 C7_8 F10_8 -179.7(15) . . . . ?
F9_8 C6_8 C7_8 C8_8 -62.0(11) . . . . ?
F8_8 C6_8 C7_8 C8_8 -178.5(9) . . . . ?
C5_8 C6_8 C7_8 C8_8 60.2(10) . . . . ?
F9_8 C6_8 C7_8 C3_8 178.5(9) . . . . ?
F8_8 C6_8 C7_8 C3_8 62.0(11) . . . . ?
C5_8 C6_8 C7_8 C3_8 -59.3(10) . . . . ?
F4_8 C3_8 C7_8 F10_8 57.2(16) . . . . ?
F3_8 C3_8 C7_8 F10_8 -57.6(16) . . . . ?
C1_8 C3_8 C7_8 F10_8 -179.8(15) . . . . ?
F4_8 C3_8 C7_8 C6_8 -63.3(10) . . . . ?
F3_8 C3_8 C7_8 C6_8 -178.1(8) . . . . ?
C1_8 C3_8 C7_8 C6_8 59.7(10) . . . . ?
F4_8 C3_8 C7_8 C8_8 177.4(8) . . . . ?
F3_8 C3_8 C7_8 C8_8 62.6(10) . . . . ?
C1_8 C3_8 C7_8 C8_8 -59.6(10) . . . . ?
F10_8 C7_8 C8_8 F11_8 57.2(16) . . . . ?
C6_8 C7_8 C8_8 F11_8 177.3(8) . . . . ?
C3_8 C7_8 C8_8 F11_8 -63.0(11) . . . . ?
F10_8 C7_8 C8_8 F12_8 -58.7(16) . . . . ?
C6_8 C7_8 C8_8 F12_8 61.4(11) . . . . ?
C3_8 C7_8 C8_8 F12_8 -178.9(8) . . . . ?
F10_8 C7_8 C8_8 C9_8 179.2(15) . . . . ?
C6_8 C7_8 C8_8 C9_8 -60.7(10) . . . . ?
C3_8 C7_8 C8_8 C9_8 59.0(10) . . . . ?
F11_8 C8_8 C9_8 F13_8 -57.2(9) . . . . ?
F12_8 C8_8 C9_8 F13_8 58.6(9) . . . . ?
C7_8 C8_8 C9_8 F13_8 -179.4(7) . . . . ?
F11_8 C8_8 C9_8 C2_8 62.7(9) . . . . ?
F12_8 C8_8 C9_8 C2_8 178.6(7) . . . . ?
C7_8 C8_8 C9_8 C2_8 -59.5(9) . . . . ?
F11_8 C8_8 C9_8 C10_8 -176.8(8) . . . . ?
F12_8 C8_8 C9_8 C10_8 -61.0(9) . . . . ?
C7_8 C8_8 C9_8 C10_8 61.0(9) . . . . ?
F1_8 C2_8 C9_8 F13_8 57.3(8) . . . . ?
F2_8 C2_8 C9_8 F13_8 -57.5(8) . . . . ?
C1_8 C2_8 C9_8 F13_8 -179.2(6) . . . . ?
F1_8 C2_8 C9_8 C8_8 -62.8(8) . . . . ?
F2_8 C2_8 C9_8 C8_8 -177.5(6) . . . . ?
C1_8 C2_8 C9_8 C8_8 60.7(8) . . . . ?
F1_8 C2_8 C9_8 C10_8 177.7(7) . . . . ?
F2_8 C2_8 C9_8 C10_8 63.0(9) . . . . ?
C1_8 C2_8 C9_8 C10_8 -58.8(9) . . . . ?
F7_8 C5_8 C10_8 F15_8 58.8(13) . . . . ?
C6_8 C5_8 C10_8 F15_8 -60.7(12) . . . . ?
C4_8 C5_8 C10_8 F15_8 179.6(10) . . . . ?
F7_8 C5_8 C10_8 F14_8 -57.5(14) . . . . ?
C6_8 C5_8 C10_8 F14_8 -177.0(11) . . . . ?
C4_8 C5_8 C10_8 F14_8 63.4(13) . . . . ?
F7_8 C5_8 C10_8 C9_8 -179.4(10) . . . . ?
C6_8 C5_8 C10_8 C9_8 61.1(11) . . . . ?
C4_8 C5_8 C10_8 C9_8 -58.5(11) . . . . ?
F13_8 C9_8 C10_8 F15_8 -57.5(11) . . . . ?
C8_8 C9_8 C10_8 F15_8 62.1(11) . . . . ?
C2_8 C9_8 C10_8 F15_8 -177.9(9) . . . . ?
F13_8 C9_8 C10_8 F14_8 57.8(12) . . . . ?
C8_8 C9_8 C10_8 F14_8 177.4(10) . . . . ?
C2_8 C9_8 C10_8 F14_8 -62.5(12) . . . . ?
F13_8 C9_8 C10_8 C5_8 179.1(8) . . . . ?
C8_8 C9_8 C10_8 C5_8 -61.3(10) . . . . ?
C2_8 C9_8 C10_8 C5_8 58.8(10) . . . . ?
O1_7 Al1 O1_9 C1_9 -82.4(16) . . . . ?
O1_11 Al1 O1_9 C1_9 152.4(15) . . . . ?
O1_5 Al1 O1_9 C1_9 40.1(17) . . . . ?
Al1 O1_9 C1_9 C3_9 39.1(19) . . . . ?
Al1 O1_9 C1_9 C4_9 -82.2(18) . . . . ?
Al1 O1_9 C1_9 C2_9 158.3(14) . . . . ?
O1_9 C1_9 C2_9 F1_9 -56.9(12) . . . . ?
C3_9 C1_9 C2_9 F1_9 65.6(10) . . . . ?
C4_9 C1_9 C2_9 F1_9 -179.6(9) . . . . ?
O1_9 C1_9 C2_9 F2_9 60.3(12) . . . . ?
C3_9 C1_9 C2_9 F2_9 -177.3(9) . . . . ?
C4_9 C1_9 C2_9 F2_9 -62.4(11) . . . . ?
O1_9 C1_9 C2_9 C9_9 -179.4(9) . . . . ?
C3_9 C1_9 C2_9 C9_9 -56.9(10) . . . . ?
C4_9 C1_9 C2_9 C9_9 57.9(10) . . . . ?
O1_9 C1_9 C3_9 F4_9 -60.2(10) . . . . ?
C4_9 C1_9 C3_9 F4_9 64.3(9) . . . . ?
C2_9 C1_9 C3_9 F4_9 179.5(8) . . . . ?
O1_9 C1_9 C3_9 F3_9 56.9(11) . . . . ?
C4_9 C1_9 C3_9 F3_9 -178.6(9) . . . . ?
C2_9 C1_9 C3_9 F3_9 -63.5(10) . . . . ?
O1_9 C1_9 C3_9 C7_9 177.6(8) . . . . ?
C4_9 C1_9 C3_9 C7_9 -57.9(10) . . . . ?
C2_9 C1_9 C3_9 C7_9 57.3(10) . . . . ?
O1_9 C1_9 C4_9 F5_9 59.7(11) . . . . ?
C3_9 C1_9 C4_9 F5_9 -64.8(10) . . . . ?
C2_9 C1_9 C4_9 F5_9 -179.8(8) . . . . ?
O1_9 C1_9 C4_9 F6_9 -55.3(12) . . . . ?
C3_9 C1_9 C4_9 F6_9 -179.8(9) . . . . ?
C2_9 C1_9 C4_9 F6_9 65.3(11) . . . . ?
O1_9 C1_9 C4_9 C5_9 -176.9(9) . . . . ?
C3_9 C1_9 C4_9 C5_9 58.6(10) . . . . ?
C2_9 C1_9 C4_9 C5_9 -56.4(10) . . . . ?
F5_9 C4_9 C5_9 F7_9 -56.9(10) . . . . ?
F6_9 C4_9 C5_9 F7_9 56.7(13) . . . . ?
C1_9 C4_9 C5_9 F7_9 179.1(8) . . . . ?
F5_9 C4_9 C5_9 C10_9 -177.4(8) . . . . ?
F6_9 C4_9 C5_9 C10_9 -63.8(12) . . . . ?
C1_9 C4_9 C5_9 C10_9 58.6(9) . . . . ?
F5_9 C4_9 C5_9 C6_9 63.5(10) . . . . ?
F6_9 C4_9 C5_9 C6_9 177.2(11) . . . . ?
C1_9 C4_9 C5_9 C6_9 -60.4(10) . . . . ?
F7_9 C5_9 C6_9 F9_9 -55.7(10) . . . . ?
C10_9 C5_9 C6_9 F9_9 63.0(9) . . . . ?
C4_9 C5_9 C6_9 F9_9 -176.9(8) . . . . ?
F7_9 C5_9 C6_9 F8_9 59.6(9) . . . . ?
C10_9 C5_9 C6_9 F8_9 178.2(7) . . . . ?
C4_9 C5_9 C6_9 F8_9 -61.7(9) . . . . ?
F7_9 C5_9 C6_9 C7_9 -179.7(7) . . . . ?
C10_9 C5_9 C6_9 C7_9 -61.0(8) . . . . ?
C4_9 C5_9 C6_9 C7_9 59.1(9) . . . . ?
F9_9 C6_9 C7_9 F10_9 58.0(13) . . . . ?
F8_9 C6_9 C7_9 F10_9 -57.9(12) . . . . ?
C5_9 C6_9 C7_9 F10_9 -177.8(11) . . . . ?
F9_9 C6_9 C7_9 C8_9 -62.6(11) . . . . ?
F8_9 C6_9 C7_9 C8_9 -178.5(8) . . . . ?
C5_9 C6_9 C7_9 C8_9 61.6(10) . . . . ?
F9_9 C6_9 C7_9 C3_9 177.2(8) . . . . ?
F8_9 C6_9 C7_9 C3_9 61.2(10) . . . . ?
C5_9 C6_9 C7_9 C3_9 -58.6(10) . . . . ?
F4_9 C3_9 C7_9 F10_9 54.6(15) . . . . ?
F3_9 C3_9 C7_9 F10_9 -61.1(15) . . . . ?
C1_9 C3_9 C7_9 F10_9 177.4(13) . . . . ?
F4_9 C3_9 C7_9 C8_9 176.5(9) . . . . ?
F3_9 C3_9 C7_9 C8_9 60.8(11) . . . . ?
C1_9 C3_9 C7_9 C8_9 -60.7(10) . . . . ?
F4_9 C3_9 C7_9 C6_9 -63.5(11) . . . . ?
F3_9 C3_9 C7_9 C6_9 -179.3(9) . . . . ?
C1_9 C3_9 C7_9 C6_9 59.2(10) . . . . ?
F10_9 C7_9 C8_9 F11_9 59.2(16) . . . . ?
C6_9 C7_9 C8_9 F11_9 177.9(9) . . . . ?
C3_9 C7_9 C8_9 F11_9 -61.7(11) . . . . ?
F10_9 C7_9 C8_9 F12_9 -58.5(15) . . . . ?
C6_9 C7_9 C8_9 F12_9 60.1(11) . . . . ?
C3_9 C7_9 C8_9 F12_9 -179.5(9) . . . . ?
F10_9 C7_9 C8_9 C9_9 -179.0(13) . . . . ?
C6_9 C7_9 C8_9 C9_9 -60.3(10) . . . . ?
C3_9 C7_9 C8_9 C9_9 60.1(10) . . . . ?
F1_9 C2_9 C9_9 F13_9 57.0(11) . . . . ?
F2_9 C2_9 C9_9 F13_9 -59.7(12) . . . . ?
C1_9 C2_9 C9_9 F13_9 179.7(9) . . . . ?
F1_9 C2_9 C9_9 C10_9 177.4(8) . . . . ?
F2_9 C2_9 C9_9 C10_9 60.7(12) . . . . ?
C1_9 C2_9 C9_9 C10_9 -59.9(10) . . . . ?
F1_9 C2_9 C9_9 C8_9 -63.6(10) . . . . ?
F2_9 C2_9 C9_9 C8_9 179.7(11) . . . . ?
C1_9 C2_9 C9_9 C8_9 59.1(10) . . . . ?
F11_9 C8_9 C9_9 F13_9 -56.9(11) . . . . ?
F12_9 C8_9 C9_9 F13_9 58.9(10) . . . . ?
C7_9 C8_9 C9_9 F13_9 -179.9(8) . . . . ?
F11_9 C8_9 C9_9 C2_9 63.6(11) . . . . ?
F12_9 C8_9 C9_9 C2_9 179.4(8) . . . . ?
C7_9 C8_9 C9_9 C2_9 -59.3(10) . . . . ?
F11_9 C8_9 C9_9 C10_9 -177.7(9) . . . . ?
F12_9 C8_9 C9_9 C10_9 -61.9(10) . . . . ?
C7_9 C8_9 C9_9 C10_9 59.3(10) . . . . ?
F7_9 C5_9 C10_9 F15_9 57.7(10) . . . . ?
C6_9 C5_9 C10_9 F15_9 -61.1(9) . . . . ?
C4_9 C5_9 C10_9 F15_9 179.2(8) . . . . ?
F7_9 C5_9 C10_9 F14_9 -59.6(11) . . . . ?
C6_9 C5_9 C10_9 F14_9 -178.4(9) . . . . ?
C4_9 C5_9 C10_9 F14_9 61.9(10) . . . . ?
F7_9 C5_9 C10_9 C9_9 179.2(8) . . . . ?
C6_9 C5_9 C10_9 C9_9 60.4(9) . . . . ?
C4_9 C5_9 C10_9 C9_9 -59.3(9) . . . . ?
F13_9 C9_9 C10_9 F15_9 -58.1(11) . . . . ?
C2_9 C9_9 C10_9 F15_9 -178.2(8) . . . . ?
C8_9 C9_9 C10_9 F15_9 62.5(10) . . . . ?
F13_9 C9_9 C10_9 F14_9 57.5(11) . . . . ?
C2_9 C9_9 C10_9 F14_9 -62.5(10) . . . . ?
C8_9 C9_9 C10_9 F14_9 178.1(9) . . . . ?
F13_9 C9_9 C10_9 C5_9 179.6(8) . . . . ?
C2_9 C9_9 C10_9 C5_9 59.5(9) . . . . ?
C8_9 C9_9 C10_9 C5_9 -59.9(9) . . . . ?
O1_6 Al1 O1_10 C1_10 61.9(18) . . . . ?
O1_11 Al1 O1_10 C1_10 -160.4(16) . . . . ?
O1_8 Al1 O1_10 C1_10 -54.4(17) . . . . ?
Al1 O1_10 C1_10 C3_10 99.9(18) . . . . ?
Al1 O1_10 C1_10 C2_10 -141.3(16) . . . . ?
Al1 O1_10 C1_10 C4_10 -21(2) . . . . ?
O1_10 C1_10 C2_10 F2_10 58.5(8) . . . . ?
C3_10 C1_10 C2_10 F2_10 179.9(6) . . . . ?
C4_10 C1_10 C2_10 F2_10 -65.6(7) . . . . ?
O1_10 C1_10 C2_10 F1_10 -58.1(8) . . . . ?
C3_10 C1_10 C2_10 F1_10 63.3(7) . . . . ?
C4_10 C1_10 C2_10 F1_10 177.8(6) . . . . ?
O1_10 C1_10 C2_10 C9_10 -178.8(6) . . . . ?
C3_10 C1_10 C2_10 C9_10 -57.4(7) . . . . ?
C4_10 C1_10 C2_10 C9_10 57.1(7) . . . . ?
O1_10 C1_10 C3_10 F4_10 -61.2(8) . . . . ?
C2_10 C1_10 C3_10 F4_10 178.6(6) . . . . ?
C4_10 C1_10 C3_10 F4_10 63.8(7) . . . . ?
O1_10 C1_10 C3_10 F3_10 55.1(9) . . . . ?
C2_10 C1_10 C3_10 F3_10 -65.2(8) . . . . ?
C4_10 C1_10 C3_10 F3_10 -180.0(6) . . . . ?
O1_10 C1_10 C3_10 C7_10 176.9(6) . . . . ?
C2_10 C1_10 C3_10 C7_10 56.7(7) . . . . ?
C4_10 C1_10 C3_10 C7_10 -58.1(7) . . . . ?
O1_10 C1_10 C4_10 F5_10 58.8(9) . . . . ?
C3_10 C1_10 C4_10 F5_10 -64.8(8) . . . . ?
C2_10 C1_10 C4_10 F5_10 -179.6(6) . . . . ?
O1_10 C1_10 C4_10 F6_10 -57.1(8) . . . . ?
C3_10 C1_10 C4_10 F6_10 179.3(6) . . . . ?
C2_10 C1_10 C4_10 F6_10 64.5(7) . . . . ?
O1_10 C1_10 C4_10 C5_10 -178.8(6) . . . . ?
C3_10 C1_10 C4_10 C5_10 57.6(7) . . . . ?
C2_10 C1_10 C4_10 C5_10 -57.2(7) . . . . ?
F5_10 C4_10 C5_10 F7_10 -56.6(11) . . . . ?
F6_10 C4_10 C5_10 F7_10 58.8(10) . . . . ?
C1_10 C4_10 C5_10 F7_10 -179.3(9) . . . . ?
F5_10 C4_10 C5_10 C10_10 -177.1(6) . . . . ?
F6_10 C4_10 C5_10 C10_10 -61.7(7) . . . . ?
C1_10 C4_10 C5_10 C10_10 60.2(7) . . . . ?
F5_10 C4_10 C5_10 C6_10 62.5(8) . . . . ?
F6_10 C4_10 C5_10 C6_10 177.8(6) . . . . ?
C1_10 C4_10 C5_10 C6_10 -60.3(7) . . . . ?
F7_10 C5_10 C6_10 F8_10 59.3(10) . . . . ?
C10_10 C5_10 C6_10 F8_10 178.8(6) . . . . ?
C4_10 C5_10 C6_10 F8_10 -61.0(8) . . . . ?
F7_10 C5_10 C6_10 F9_10 -57.5(10) . . . . ?
C10_10 C5_10 C6_10 F9_10 62.0(8) . . . . ?
C4_10 C5_10 C6_10 F9_10 -177.8(7) . . . . ?
F7_10 C5_10 C6_10 C7_10 -179.7(9) . . . . ?
C10_10 C5_10 C6_10 C7_10 -60.2(7) . . . . ?
C4_10 C5_10 C6_10 C7_10 60.0(7) . . . . ?
F8_10 C6_10 C7_10 F10_10 -60.6(8) . . . . ?
F9_10 C6_10 C7_10 F10_10 57.7(7) . . . . ?
C5_10 C6_10 C7_10 F10_10 178.9(6) . . . . ?
F8_10 C6_10 C7_10 C8_10 -179.3(7) . . . . ?
F9_10 C6_10 C7_10 C8_10 -61.0(7) . . . . ?
C5_10 C6_10 C7_10 C8_10 60.3(7) . . . . ?
F8_10 C6_10 C7_10 C3_10 60.5(8) . . . . ?
F9_10 C6_10 C7_10 C3_10 178.7(6) . . . . ?
C5_10 C6_10 C7_10 C3_10 -60.0(7) . . . . ?
F4_10 C3_10 C7_10 F10_10 59.0(7) . . . . ?
F3_10 C3_10 C7_10 F10_10 -54.7(9) . . . . ?
C1_10 C3_10 C7_10 F10_10 -178.3(6) . . . . ?
F4_10 C3_10 C7_10 C6_10 -61.7(7) . . . . ?
F3_10 C3_10 C7_10 C6_10 -175.4(7) . . . . ?
C1_10 C3_10 C7_10 C6_10 61.0(7) . . . . ?
F4_10 C3_10 C7_10 C8_10 177.9(6) . . . . ?
F3_10 C3_10 C7_10 C8_10 64.2(8) . . . . ?
C1_10 C3_10 C7_10 C8_10 -59.4(7) . . . . ?
F10_10 C7_10 C8_10 F12_10 -58.6(7) . . . . ?
C6_10 C7_10 C8_10 F12_10 61.0(7) . . . . ?
C3_10 C7_10 C8_10 F12_10 -178.8(5) . . . . ?
F10_10 C7_10 C8_10 F11_10 57.4(7) . . . . ?
C6_10 C7_10 C8_10 F11_10 177.0(6) . . . . ?
C3_10 C7_10 C8_10 F11_10 -62.8(7) . . . . ?
F10_10 C7_10 C8_10 C9_10 179.7(5) . . . . ?
C6_10 C7_10 C8_10 C9_10 -60.7(6) . . . . ?
C3_10 C7_10 C8_10 C9_10 59.5(6) . . . . ?
F2_10 C2_10 C9_10 F13_10 -56.3(7) . . . . ?
F1_10 C2_10 C9_10 F13_10 60.4(8) . . . . ?
C1_10 C2_10 C9_10 F13_10 -178.9(6) . . . . ?
F2_10 C2_10 C9_10 C10_10 63.1(7) . . . . ?
F1_10 C2_10 C9_10 C10_10 179.9(7) . . . . ?
C1_10 C2_10 C9_10 C10_10 -59.5(7) . . . . ?
F2_10 C2_10 C9_10 C8_10 -177.5(5) . . . . ?
F1_10 C2_10 C9_10 C8_10 -60.7(8) . . . . ?
C1_10 C2_10 C9_10 C8_10 59.9(7) . . . . ?
F12_10 C8_10 C9_10 F13_10 56.9(7) . . . . ?
F11_10 C8_10 C9_10 F13_10 -58.6(7) . . . . ?
C7_10 C8_10 C9_10 F13_10 179.3(5) . . . . ?
F12_10 C8_10 C9_10 C2_10 178.0(5) . . . . ?
F11_10 C8_10 C9_10 C2_10 62.5(7) . . . . ?
C7_10 C8_10 C9_10 C2_10 -59.6(6) . . . . ?
F12_10 C8_10 C9_10 C10_10 -62.3(6) . . . . ?
F11_10 C8_10 C9_10 C10_10 -177.8(6) . . . . ?
C7_10 C8_10 C9_10 C10_10 60.1(6) . . . . ?
F13_10 C9_10 C10_10 F15_10 -58.3(6) . . . . ?
C2_10 C9_10 C10_10 F15_10 -178.7(5) . . . . ?
C8_10 C9_10 C10_10 F15_10 61.9(6) . . . . ?
F13_10 C9_10 C10_10 F14_10 58.5(6) . . . . ?
C2_10 C9_10 C10_10 F14_10 -61.9(6) . . . . ?
C8_10 C9_10 C10_10 F14_10 178.7(5) . . . . ?
F13_10 C9_10 C10_10 C5_10 180.0(5) . . . . ?
C2_10 C9_10 C10_10 C5_10 59.6(6) . . . . ?
C8_10 C9_10 C10_10 C5_10 -59.8(6) . . . . ?
F7_10 C5_10 C10_10 F15_10 57.0(8) . . . . ?
C6_10 C5_10 C10_10 F15_10 -61.7(7) . . . . ?
C4_10 C5_10 C10_10 F15_10 177.8(5) . . . . ?
F7_10 C5_10 C10_10 F14_10 -58.9(8) . . . . ?
C6_10 C5_10 C10_10 F14_10 -177.6(6) . . . . ?
C4_10 C5_10 C10_10 F14_10 62.0(7) . . . . ?
F7_10 C5_10 C10_10 C9_10 179.0(7) . . . . ?
C6_10 C5_10 C10_10 C9_10 60.3(7) . . . . ?
C4_10 C5_10 C10_10 C9_10 -60.1(7) . . . . ?
O1_7 Al1 O1_11 C1_11 -149.2(5) . . . . ?
O1_6 Al1 O1_11 C1_11 128.3(5) . . . . ?
O1_10 Al1 O1_11 C1_11 -8.7(7) . . . . ?
O1_9 Al1 O1_11 C1_11 -24.3(6) . . . . ?
O1_5 Al1 O1_11 C1_11 93.7(5) . . . . ?
O1_8 Al1 O1_11 C1_11 -115.4(5) . . . . ?
Al1 O1_11 C1_11 C4_11 -54.2(6) . . . . ?
Al1 O1_11 C1_11 C3_11 67.0(6) . . . . ?
Al1 O1_11 C1_11 C2_11 -173.4(4) . . . . ?
O1_11 C1_11 C2_11 F2_11 59.0(3) . . . . ?
C4_11 C1_11 C2_11 F2_11 -63.9(3) . . . . ?
C3_11 C1_11 C2_11 F2_11 -178.9(2) . . . . ?
O1_11 C1_11 C2_11 F1_11 -58.1(3) . . . . ?
C4_11 C1_11 C2_11 F1_11 179.0(2) . . . . ?
C3_11 C1_11 C2_11 F1_11 64.0(3) . . . . ?
O1_11 C1_11 C2_11 C9_11 -179.5(3) . . . . ?
C4_11 C1_11 C2_11 C9_11 57.7(3) . . . . ?
C3_11 C1_11 C2_11 C9_11 -57.4(3) . . . . ?
O1_11 C1_11 C3_11 F3_11 56.5(3) . . . . ?
C4_11 C1_11 C3_11 F3_11 -179.0(2) . . . . ?
C2_11 C1_11 C3_11 F3_11 -64.2(3) . . . . ?
O1_11 C1_11 C3_11 F4_11 -60.0(3) . . . . ?
C4_11 C1_11 C3_11 F4_11 64.4(3) . . . . ?
C2_11 C1_11 C3_11 F4_11 179.3(2) . . . . ?
O1_11 C1_11 C3_11 C7_11 178.2(3) . . . . ?
C4_11 C1_11 C3_11 C7_11 -57.4(3) . . . . ?
C2_11 C1_11 C3_11 C7_11 57.5(3) . . . . ?
O1_11 C1_11 C4_11 F5_11 58.7(3) . . . . ?
C3_11 C1_11 C4_11 F5_11 -65.1(3) . . . . ?
C2_11 C1_11 C4_11 F5_11 179.5(2) . . . . ?
O1_11 C1_11 C4_11 F6_11 -57.7(3) . . . . ?
C3_11 C1_11 C4_11 F6_11 178.5(2) . . . . ?
C2_11 C1_11 C4_11 F6_11 63.1(3) . . . . ?
O1_11 C1_11 C4_11 C5_11 -179.0(2) . . . . ?
C3_11 C1_11 C4_11 C5_11 57.2(3) . . . . ?
C2_11 C1_11 C4_11 C5_11 -58.1(3) . . . . ?
F5_11 C4_11 C5_11 F7_11 -57.3(3) . . . . ?
F6_11 C4_11 C5_11 F7_11 57.4(3) . . . . ?
C1_11 C4_11 C5_11 F7_11 -180.0(2) . . . . ?
F5_11 C4_11 C5_11 C6_11 62.8(3) . . . . ?
F6_11 C4_11 C5_11 C6_11 177.5(2) . . . . ?
C1_11 C4_11 C5_11 C6_11 -59.9(3) . . . . ?
F5_11 C4_11 C5_11 C10_11 -176.7(2) . . . . ?
F6_11 C4_11 C5_11 C10_11 -62.0(3) . . . . ?
C1_11 C4_11 C5_11 C10_11 60.6(3) . . . . ?
F7_11 C5_11 C6_11 F9_11 -58.9(3) . . . . ?
C10_11 C5_11 C6_11 F9_11 61.0(3) . . . . ?
C4_11 C5_11 C6_11 F9_11 -178.5(2) . . . . ?
F7_11 C5_11 C6_11 F8_11 57.8(3) . . . . ?
C10_11 C5_11 C6_11 F8_11 177.8(2) . . . . ?
C4_11 C5_11 C6_11 F8_11 -61.8(3) . . . . ?
F7_11 C5_11 C6_11 C7_11 179.4(2) . . . . ?
C10_11 C5_11 C6_11 C7_11 -60.6(3) . . . . ?
C4_11 C5_11 C6_11 C7_11 59.8(3) . . . . ?
F9_11 C6_11 C7_11 F10_11 57.6(3) . . . . ?
F8_11 C6_11 C7_11 F10_11 -59.5(3) . . . . ?
C5_11 C6_11 C7_11 F10_11 179.7(2) . . . . ?
F9_11 C6_11 C7_11 C8_11 -62.2(3) . . . . ?
F8_11 C6_11 C7_11 C8_11 -179.3(2) . . . . ?
C5_11 C6_11 C7_11 C8_11 59.9(3) . . . . ?
F9_11 C6_11 C7_11 C3_11 178.2(2) . . . . ?
F8_11 C6_11 C7_11 C3_11 61.1(3) . . . . ?
C5_11 C6_11 C7_11 C3_11 -59.6(3) . . . . ?
F3_11 C3_11 C7_11 F10_11 -58.0(3) . . . . ?
F4_11 C3_11 C7_11 F10_11 57.6(3) . . . . ?
C1_11 C3_11 C7_11 F10_11 179.9(2) . . . . ?
F3_11 C3_11 C7_11 C6_11 -178.0(2) . . . . ?
F4_11 C3_11 C7_11 C6_11 -62.4(3) . . . . ?
C1_11 C3_11 C7_11 C6_11 59.9(3) . . . . ?
F3_11 C3_11 C7_11 C8_11 62.6(3) . . . . ?
F4_11 C3_11 C7_11 C8_11 178.1(2) . . . . ?
C1_11 C3_11 C7_11 C8_11 -59.5(3) . . . . ?
F10_11 C7_11 C8_11 F12_11 -57.8(3) . . . . ?
C6_11 C7_11 C8_11 F12_11 61.7(3) . . . . ?
C3_11 C7_11 C8_11 F12_11 -178.6(2) . . . . ?
F10_11 C7_11 C8_11 F11_11 58.7(3) . . . . ?
C6_11 C7_11 C8_11 F11_11 178.1(2) . . . . ?
C3_11 C7_11 C8_11 F11_11 -62.2(3) . . . . ?
F10_11 C7_11 C8_11 C9_11 -179.9(2) . . . . ?
C6_11 C7_11 C8_11 C9_11 -60.4(3) . . . . ?
C3_11 C7_11 C8_11 C9_11 59.3(3) . . . . ?
F2_11 C2_11 C9_11 F13_11 -57.8(3) . . . . ?
F1_11 C2_11 C9_11 F13_11 57.9(3) . . . . ?
C1_11 C2_11 C9_11 F13_11 179.7(2) . . . . ?
F2_11 C2_11 C9_11 C10_11 62.6(3) . . . . ?
F1_11 C2_11 C9_11 C10_11 178.2(2) . . . . ?
C1_11 C2_11 C9_11 C10_11 -59.9(3) . . . . ?
F2_11 C2_11 C9_11 C8_11 -178.1(2) . . . . ?
F1_11 C2_11 C9_11 C8_11 -62.5(3) . . . . ?
C1_11 C2_11 C9_11 C8_11 59.4(3) . . . . ?
F12_11 C8_11 C9_11 F13_11 58.0(3) . . . . ?
F11_11 C8_11 C9_11 F13_11 -58.2(3) . . . . ?
C7_11 C8_11 C9_11 F13_11 179.8(2) . . . . ?
F12_11 C8_11 C9_11 C10_11 -61.2(3) . . . . ?
F11_11 C8_11 C9_11 C10_11 -177.4(2) . . . . ?
C7_11 C8_11 C9_11 C10_11 60.7(3) . . . . ?
F12_11 C8_11 C9_11 C2_11 178.7(2) . . . . ?
F11_11 C8_11 C9_11 C2_11 62.5(3) . . . . ?
C7_11 C8_11 C9_11 C2_11 -59.5(3) . . . . ?
F7_11 C5_11 C10_11 F15_11 59.2(3) . . . . ?
C6_11 C5_11 C10_11 F15_11 -61.1(3) . . . . ?
C4_11 C5_11 C10_11 F15_11 178.4(2) . . . . ?
F7_11 C5_11 C10_11 F14_11 -57.2(3) . . . . ?
C6_11 C5_11 C10_11 F14_11 -177.4(2) . . . . ?
C4_11 C5_11 C10_11 F14_11 62.0(3) . . . . ?
F7_11 C5_11 C10_11 C9_11 -178.7(2) . . . . ?
C6_11 C5_11 C10_11 C9_11 61.0(3) . . . . ?
C4_11 C5_11 C10_11 C9_11 -59.5(3) . . . . ?
F13_11 C9_11 C10_11 F15_11 -58.1(3) . . . . ?
C2_11 C9_11 C10_11 F15_11 -178.9(2) . . . . ?
C8_11 C9_11 C10_11 F15_11 61.1(3) . . . . ?
F13_11 C9_11 C10_11 F14_11 59.1(3) . . . . ?
C2_11 C9_11 C10_11 F14_11 -61.8(3) . . . . ?
C8_11 C9_11 C10_11 F14_11 178.3(2) . . . . ?
F13_11 C9_11 C10_11 C5_11 -179.8(2) . . . . ?
C2_11 C9_11 C10_11 C5_11 59.3(3) . . . . ?
C8_11 C9_11 C10_11 C5_11 -60.6(3) . . . . ?

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
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# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
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# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
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data_IKmjs_RF17_a
_database_code_depnum_ccdc_archive 'CCDC 2224629'
loop_
_audit_author_name
_audit_author_address
'Burkhard Butschke'
;Albert Ludwigs Universitaet Freiburg
Germany
;
_audit_update_record             
;
2022-12-06 deposited with the CCDC.	2023-03-10 downloaded from the CCDC.
;
_audit_creation_method           
;FinalCif V113 by Daniel Kratzert, Freiburg 2022,
https://dkratzert.de/finalcif.html
;
_shelx_SHELXL_version_number     2018/3
_chemical_name_systematic        ?
_chemical_name_common            ?
_chemical_formula_sum            'C48 H21 Al F60 O6'
_chemical_formula_moiety         'C40 Al F60 O4 1-, C4 H11 O 1+, C4 H10 O'
_chemical_formula_weight         1860.63
_chemical_melting_point          ?
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_H-M_alt        'P 21/n'
_space_group_name_Hall           '-P 2yn'
_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;

loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'

_cell_length_a                   18.440(4)
_cell_length_b                   14.863(4)
_cell_length_c                   22.062(5)
_cell_angle_alpha                90
_cell_angle_beta                 104.402(9)
_cell_angle_gamma                90
_cell_volume                     5857(3)
_cell_formula_units_Z            4
_cell_measurement_temperature    100(2)
_cell_measurement_reflns_used    9912
_cell_measurement_theta_min      2.2805
_cell_measurement_theta_max      27.093
_exptl_crystal_description       plate
_exptl_crystal_colour            colourless
_exptl_crystal_recrystallization_method 
'Crystals were obtained from a solution in 1,2-difluorobenzene at -40 °C.'
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_density_diffrn    2.110
_exptl_crystal_F_000             3640
_exptl_crystal_size_max          0.277
_exptl_crystal_size_mid          0.204
_exptl_crystal_size_min          0.088
_exptl_absorpt_coefficient_mu    0.279
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_correction_T_min  0.6626
_exptl_absorpt_correction_T_max  0.7455
_exptl_absorpt_process_details   
;
SADABS-2016/2 - Bruker AXS area detector scaling and absorption correction:
Krause, L., Herbst-Irmer, R., Sheldrick G.M. & Stalke D., J. Appl. Cryst. 48
(2015) 3-10
;
_exptl_absorpt_special_details   ?
_shelx_estimated_absorpt_T_min   0.927
_shelx_estimated_absorpt_T_max   0.976
_exptl_transmission_factor_min   ?
_exptl_transmission_factor_max   ?
_exptl_special_details           ?
_diffrn_ambient_temperature      100(2)
_diffrn_ambient_environment      N~2~
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_monochromator  'mirror optics'
_olex2_diffrn_ambient_temperature_device 'Oxford Cryostream 800'
_diffrn_measurement_ambient_temperature_device_make ?
_diffrn_radiation_probe          x-ray
_diffrn_source                   'microfocus sealed X-ray tube'
_diffrn_source_type              'Incoatec I\ms'
_diffrn_source_voltage           50.0
_diffrn_source_current           1.4
_diffrn_detector                 CPAD
_diffrn_detector_type            'Bruker PHOTON III'
_diffrn_detector_area_resol_mean 7.41
_diffrn_measurement_device       'three-circle diffractometer'
_diffrn_measurement_device_type  'Bruker D8 VENTURE dual wavelength Mo/Cu'
_diffrn_measurement_method       'ω and φ scans'
_diffrn_measurement_specimen_support 'MiTeGen micromount'
_diffrn_reflns_number            119781
_diffrn_reflns_av_unetI/netI     0.0301
_diffrn_reflns_av_R_equivalents  0.0561
_diffrn_reflns_theta_min         1.658
_diffrn_reflns_theta_max         27.126
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_limit_h_min       -23
_diffrn_reflns_limit_h_max       23
_diffrn_reflns_limit_k_min       -19
_diffrn_reflns_limit_k_max       19
_diffrn_reflns_limit_l_min       -28
_diffrn_reflns_limit_l_max       27
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measured_fraction_theta_full 1.000
_diffrn_reflns_Laue_measured_fraction_max 0.999
_diffrn_reflns_Laue_measured_fraction_full 1.000
_diffrn_reflns_point_group_measured_fraction_max 0.999
_diffrn_reflns_point_group_measured_fraction_full 1.000
_reflns_number_total             12932
_reflns_number_gt                9687
_reflns_threshold_expression     'I > 2σ(I)'
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_max     .
_reflns_Friedel_fraction_full    .
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_computing_data_collection       'Bruker BIS V6.2.12/2019-08-12'
_computing_cell_refinement       'SAINT V8.40B'
_computing_data_reduction        'SAINT V8.40B'
_computing_structure_solution    'SHELXT 2018/2 (Sheldrick, 2018)'
_computing_structure_refinement  'SHELXL-2018/3 (Sheldrick, 2018)'
_computing_molecular_graphics    ?
_computing_publication_material  ?
_refine_special_details          
;
The bridging hydrogen atom H1 has been refined without the application of any
bond-distance restraints. This decision has been made because all three
diethylether molecules are in different chemical environments. Thus, the
realization of different O-H-bond distances makes chemical sense. The data
quality allows for the description of this subtlety.
;
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0285P)²+20.7009P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   ?
_atom_sites_solution_hydrogens   mixed
_refine_ls_hydrogen_treatment    mixed
_refine_ls_number_reflns         12932
_refine_ls_number_parameters     1091
_refine_ls_number_restraints     198
_refine_ls_R_factor_all          0.0866
_refine_ls_R_factor_gt           0.0614
_refine_ls_wR_factor_ref         0.1387
_refine_ls_wR_factor_gt          0.1269
_refine_ls_goodness_of_fit_ref   1.101
_refine_ls_restrained_S_all      1.094
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_diff_density_max         0.439
_refine_diff_density_min         -0.443
_refine_diff_density_rms         0.082
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       .

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Al Al 0.0645 0.0514 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Al1 Al 0.50217(5) 0.36883(6) 0.25435(4) 0.01191(19) Uani 1 1 d . . . . .
H1 H 0.849(2) 0.397(2) 0.0698(17) 0.018 Uiso 1 1 d . U . . .
O1_1 O 0.58060(12) 0.35139(16) 0.31489(10) 0.0170(5) Uani 1 1 d . . . . .
C1_1 C 0.61294(18) 0.3581(2) 0.37691(14) 0.0159(6) Uani 1 1 d . . . . .
C2_1 C 0.69951(18) 0.3507(2) 0.38847(15) 0.0177(7) Uani 1 1 d . . . . .
F1_1 F 0.71767(11) 0.27241(14) 0.36546(9) 0.0259(5) Uani 1 1 d . . . . .
F2_1 F 0.72538(11) 0.41613(15) 0.35698(9) 0.0246(5) Uani 1 1 d . . . . .
C3_1 C 0.58735(19) 0.2815(2) 0.41506(16) 0.0209(7) Uani 1 1 d . . . . .
F3_1 F 0.60178(12) 0.20033(14) 0.39307(10) 0.0279(5) Uani 1 1 d . . . . .
F4_1 F 0.51237(11) 0.28369(15) 0.40760(9) 0.0263(5) Uani 1 1 d . . . . .
C4_1 C 0.59533(19) 0.4495(2) 0.40543(15) 0.0183(7) Uani 1 1 d . . . . .
F5_1 F 0.52089(11) 0.45943(15) 0.39695(9) 0.0258(5) Uani 1 1 d . . . . .
F6_1 F 0.61727(12) 0.51907(14) 0.37501(9) 0.0248(5) Uani 1 1 d . . . . .
C5_1 C 0.6347(2) 0.4562(3) 0.47597(16) 0.0227(8) Uani 1 1 d . . . . .
F7_1 F 0.61819(13) 0.53692(15) 0.49908(10) 0.0318(5) Uani 1 1 d . . . . .
C6_1 C 0.6074(2) 0.3789(3) 0.51157(16) 0.0252(8) Uani 1 1 d . . . . .
F8_1 F 0.53309(12) 0.38604(17) 0.50550(10) 0.0322(5) Uani 1 1 d . . . . .
F9_1 F 0.63920(13) 0.38388(17) 0.57335(9) 0.0335(5) Uani 1 1 d . . . . .
C7_1 C 0.6264(2) 0.2878(3) 0.48545(16) 0.0235(8) Uani 1 1 d . . . . .
F10_1 F 0.60224(13) 0.21969(16) 0.51703(10) 0.0346(5) Uani 1 1 d . . . . .
C8_1 C 0.7125(2) 0.2803(3) 0.49477(16) 0.0250(8) Uani 1 1 d . . . . .
F11_1 F 0.73030(13) 0.19974(15) 0.47407(10) 0.0335(5) Uani 1 1 d . . . . .
F12_1 F 0.74712(12) 0.28375(17) 0.55587(10) 0.0338(5) Uani 1 1 d . . . . .
C9_1 C 0.73942(18) 0.3573(3) 0.45889(15) 0.0204(7) Uani 1 1 d . . . . .
F13_1 F 0.81495(11) 0.35134(16) 0.46697(10) 0.0307(5) Uani 1 1 d . . . . .
C10_1 C 0.7205(2) 0.4480(3) 0.48517(16) 0.0236(8) Uani 1 1 d . . . . .
F14_1 F 0.74504(12) 0.51715(15) 0.45606(10) 0.0308(5) Uani 1 1 d . . . . .
F15_1 F 0.75550(12) 0.45603(17) 0.54589(10) 0.0328(5) Uani 1 1 d . . . . .
O1_2 O 0.42449(12) 0.34492(15) 0.28198(10) 0.0157(5) Uani 1 1 d . . . . .
C1_2 C 0.34964(17) 0.3530(2) 0.27442(14) 0.0131(6) Uani 1 1 d . . . . .
C2_2 C 0.32998(18) 0.4411(2) 0.30611(15) 0.0166(7) Uani 1 1 d . . . . .
F1_2 F 0.36567(11) 0.44156(14) 0.36703(9) 0.0234(4) Uani 1 1 d . . . . .
F2_2 F 0.35424(11) 0.51364(13) 0.28043(9) 0.0219(4) Uani 1 1 d . . . . .
C3_2 C 0.32021(18) 0.2719(2) 0.30616(15) 0.0158(6) Uani 1 1 d . . . . .
F3_2 F 0.35544(11) 0.26719(14) 0.36755(9) 0.0217(4) Uani 1 1 d . . . . .
F4_2 F 0.33528(11) 0.19400(13) 0.28089(10) 0.0223(4) Uani 1 1 d . . . . .
C4_2 C 0.30547(18) 0.3542(2) 0.20449(15) 0.0155(6) Uani 1 1 d . . . . .
F5_2 F 0.31953(11) 0.27957(13) 0.17514(9) 0.0214(4) Uani 1 1 d . . . . .
F6_2 F 0.32868(11) 0.42382(13) 0.17434(9) 0.0198(4) Uani 1 1 d . . . . .
C5_2 C 0.22001(18) 0.3625(2) 0.19775(15) 0.0156(6) Uani 1 1 d . . . . .
F7_2 F 0.18253(11) 0.36428(14) 0.13569(9) 0.0233(4) Uani 1 1 d . . . . .
C6_2 C 0.19328(18) 0.2806(2) 0.22943(16) 0.0180(7) Uani 1 1 d . . . . .
F8_2 F 0.20472(11) 0.20359(13) 0.20131(10) 0.0259(5) Uani 1 1 d . . . . .
F9_2 F 0.11803(11) 0.28584(14) 0.22200(10) 0.0248(5) Uani 1 1 d . . . . .
C7_2 C 0.23429(18) 0.2787(2) 0.29926(16) 0.0165(7) Uani 1 1 d . . . . .
F10_2 F 0.21130(11) 0.20723(14) 0.32801(10) 0.0258(5) Uani 1 1 d . . . . .
C8_2 C 0.21748(18) 0.3668(2) 0.33102(15) 0.0191(7) Uani 1 1 d . . . . .
F11_2 F 0.25065(12) 0.36525(15) 0.39256(9) 0.0261(5) Uani 1 1 d . . . . .
F12_2 F 0.14307(11) 0.37337(14) 0.32649(10) 0.0255(5) Uani 1 1 d . . . . .
C9_2 C 0.24435(19) 0.4489(2) 0.29922(15) 0.0170(7) Uani 1 1 d . . . . .
F13_2 F 0.22855(12) 0.52646(14) 0.32626(10) 0.0260(5) Uani 1 1 d . . . . .
C10_2 C 0.20366(18) 0.4499(2) 0.22932(16) 0.0181(7) Uani 1 1 d . . . . .
F14_2 F 0.22456(11) 0.52190(13) 0.20064(10) 0.0236(4) Uani 1 1 d . . . . .
F15_2 F 0.12844(11) 0.45940(14) 0.22186(10) 0.0243(4) Uani 1 1 d . . . . .
O1_3 O 0.50705(13) 0.30011(15) 0.19231(10) 0.0164(5) Uani 1 1 d . . . . .
C1_3 C 0.52503(18) 0.2187(2) 0.17330(14) 0.0140(6) Uani 1 1 d . . . . .
C2_3 C 0.61091(19) 0.2100(2) 0.17987(16) 0.0197(7) Uani 1 1 d . . . . .
F1_3 F 0.63421(12) 0.27667(14) 0.14769(11) 0.0286(5) Uani 1 1 d . . . . .
F2_3 F 0.64905(12) 0.22182(15) 0.24024(10) 0.0289(5) Uani 1 1 d . . . . .
C3_3 C 0.48531(18) 0.2048(2) 0.10263(15) 0.0162(7) Uani 1 1 d . . . . .
F3_3 F 0.50482(12) 0.27084(13) 0.06818(9) 0.0246(5) Uani 1 1 d . . . . .
F4_3 F 0.41065(11) 0.21065(14) 0.09399(9) 0.0246(5) Uani 1 1 d . . . . .
C4_3 C 0.50112(19) 0.1394(2) 0.21013(15) 0.0183(7) Uani 1 1 d . . . . .
F5_3 F 0.42719(11) 0.14159(14) 0.20535(10) 0.0244(4) Uani 1 1 d . . . . .
F6_3 F 0.53403(13) 0.14779(14) 0.27196(9) 0.0266(5) Uani 1 1 d . . . . .
C5_3 C 0.5221(2) 0.0474(2) 0.18668(16) 0.0190(7) Uani 1 1 d . . . . .
F7_3 F 0.50092(14) -0.02047(14) 0.22050(10) 0.0312(5) Uani 1 1 d . . . . .
C6_3 C 0.48127(19) 0.0363(2) 0.11663(16) 0.0181(7) Uani 1 1 d . . . . .
F8_3 F 0.40675(11) 0.03768(14) 0.10931(10) 0.0252(5) Uani 1 1 d . . . . .
F9_3 F 0.49724(12) -0.04478(13) 0.09610(10) 0.0252(5) Uani 1 1 d . . . . .
C7_3 C 0.50552(19) 0.1124(2) 0.07858(15) 0.0175(7) Uani 1 1 d . . . . .
F10_3 F 0.46973(12) 0.10258(14) 0.01708(9) 0.0251(5) Uani 1 1 d . . . . .
C8_3 C 0.5914(2) 0.1072(2) 0.08627(17) 0.0212(7) Uani 1 1 d . . . . .
F11_3 F 0.61363(13) 0.17122(15) 0.05171(11) 0.0319(5) Uani 1 1 d . . . . .
F12_3 F 0.60961(12) 0.02786(15) 0.06462(11) 0.0306(5) Uani 1 1 d . . . . .
C9_3 C 0.63169(19) 0.1182(2) 0.15603(18) 0.0230(8) Uani 1 1 d . . . . .
F13_3 F 0.70746(12) 0.11388(17) 0.16299(12) 0.0387(6) Uani 1 1 d . . . . .
C10_3 C 0.6075(2) 0.0425(2) 0.19439(17) 0.0259(8) Uani 1 1 d . . . . .
F14_3 F 0.64341(14) 0.05002(15) 0.25538(10) 0.0363(6) Uani 1 1 d . . . . .
F15_3 F 0.62718(13) -0.03880(15) 0.17633(11) 0.0346(6) Uani 1 1 d . . . . .
O1_4 O 0.49777(13) 0.47886(15) 0.22806(10) 0.0163(5) Uani 1 1 d . . . . .
C1_4 C 0.52086(18) 0.5421(2) 0.19349(15) 0.0136(6) Uani 1 1 d . . . . .
C2_4 C 0.50430(18) 0.6368(2) 0.21765(15) 0.0165(7) Uani 1 1 d . . . . .
F1_4 F 0.43058(11) 0.64428(13) 0.21408(10) 0.0228(4) Uani 1 1 d . . . . .
F2_4 F 0.53969(12) 0.64692(14) 0.27839(9) 0.0251(5) Uani 1 1 d . . . . .
C3_4 C 0.47886(19) 0.5362(2) 0.12264(16) 0.0172(7) Uani 1 1 d . . . . .
F3_4 F 0.40386(11) 0.54100(14) 0.11591(10) 0.0245(5) Uani 1 1 d . . . . .
F4_4 F 0.49155(12) 0.45625(13) 0.09908(9) 0.0239(4) Uani 1 1 d . . . . .
C4_4 C 0.60654(19) 0.5382(2) 0.19752(16) 0.0175(7) Uani 1 1 d . . . . .
F5_4 F 0.62408(11) 0.45740(13) 0.17676(10) 0.0237(4) Uani 1 1 d . . . . .
F6_4 F 0.64639(11) 0.54402(14) 0.25710(10) 0.0254(5) Uani 1 1 d . . . . .
C5_4 C 0.63046(18) 0.6142(2) 0.15835(17) 0.0196(7) Uani 1 1 d . . . . .
F7_4 F 0.70582(11) 0.60802(15) 0.16313(11) 0.0317(5) Uani 1 1 d . . . . .
C6_4 C 0.5877(2) 0.6060(2) 0.08922(17) 0.0218(7) Uani 1 1 d . . . . .
F8_4 F 0.60406(13) 0.52694(15) 0.06553(10) 0.0303(5) Uani 1 1 d . . . . .
F9_4 F 0.60959(13) 0.67033(15) 0.05466(10) 0.0315(5) Uani 1 1 d . . . . .
C7_4 C 0.5027(2) 0.6129(2) 0.08404(15) 0.0190(7) Uani 1 1 d . . . . .
F10_4 F 0.46388(13) 0.60541(15) 0.02290(10) 0.0303(5) Uani 1 1 d . . . . .
C8_4 C 0.4854(2) 0.7049(2) 0.10970(17) 0.0207(7) Uani 1 1 d . . . . .
F11_4 F 0.41085(12) 0.71333(14) 0.10335(10) 0.0283(5) Uani 1 1 d . . . . .
F12_4 F 0.50415(13) 0.77178(14) 0.07549(10) 0.0287(5) Uani 1 1 d . . . . .
C9_4 C 0.5282(2) 0.7128(2) 0.17883(16) 0.0190(7) Uani 1 1 d . . . . .
F13_4 F 0.51331(13) 0.79468(13) 0.20179(10) 0.0282(5) Uani 1 1 d . . . . .
C10_4 C 0.6132(2) 0.7060(2) 0.18398(17) 0.0224(7) Uani 1 1 d . . . . .
F14_4 F 0.65216(12) 0.71596(15) 0.24384(11) 0.0312(5) Uani 1 1 d . . . . .
F15_4 F 0.63530(12) 0.77375(14) 0.15217(11) 0.0313(5) Uani 1 1 d . . . . .
O1_5 O 0.92332(15) 0.40452(18) 0.08235(13) 0.0303(6) Uani 1 1 d D U . . .
C1_5 C 0.9519(2) 0.4873(3) 0.1166(2) 0.0350(9) Uani 1 1 d D U . . .
H1A_5 H 0.972694 0.472829 0.161332 0.042 Uiso 1 1 calc R U . . .
H1B_5 H 0.909985 0.530128 0.113650 0.042 Uiso 1 1 calc R U . . .
C2_5 C 1.0110(2) 0.5306(3) 0.0912(2) 0.0400(10) Uani 1 1 d D U . . .
H2A_5 H 0.990321 0.545824 0.047091 0.060 Uiso 1 1 calc R U . . .
H2B_5 H 1.053033 0.488943 0.094995 0.060 Uiso 1 1 calc R U . . .
H2C_5 H 1.028423 0.585549 0.114962 0.060 Uiso 1 1 calc R U . . .
C3_5 C 0.9658(3) 0.3236(3) 0.1057(2) 0.0440(11) Uani 1 1 d D U . . .
H3A_5 H 0.967922 0.315226 0.150609 0.053 Uiso 1 1 calc R U . . .
H3B_5 H 1.017640 0.329258 0.101078 0.053 Uiso 1 1 calc R U . . .
C4_5 C 0.9284(3) 0.2449(3) 0.0692(3) 0.0634(16) Uani 1 1 d D U . . .
H4A_5 H 0.923705 0.255346 0.024549 0.095 Uiso 1 1 calc R U . . .
H4B_5 H 0.878583 0.236910 0.076593 0.095 Uiso 1 1 calc R U . . .
H4C_5 H 0.958442 0.190726 0.082521 0.095 Uiso 1 1 calc R U . . .
O1_6 O 0.7862(6) 0.3996(9) 0.0546(3) 0.0233(18) Uani 0.644(10) 1 d D U P A 1
C1_6 C 0.7529(4) 0.3823(6) -0.0121(3) 0.041(2) Uani 0.644(10) 1 d D U P A 1
H1A_6 H 0.698321 0.393984 -0.022500 0.049 Uiso 0.644(10) 1 calc R U P A 1
H1B_6 H 0.761158 0.318995 -0.022546 0.049 Uiso 0.644(10) 1 calc R U P A 1
C2_6 C 0.7905(12) 0.4446(14) -0.0479(6) 0.077(7) Uani 0.644(10) 1 d D U P A 1
H2A_6 H 0.766686 0.439365 -0.092710 0.116 Uiso 0.644(10) 1 calc R U P A 1
H2B_6 H 0.843565 0.428708 -0.040170 0.116 Uiso 0.644(10) 1 calc R U P A 1
H2C_6 H 0.785838 0.506645 -0.034260 0.116 Uiso 0.644(10) 1 calc R U P A 1
C3_6 C 0.7497(3) 0.3542(5) 0.0974(3) 0.0282(16) Uani 0.644(10) 1 d D U P A 1
H3A_6 H 0.753609 0.288218 0.093135 0.034 Uiso 0.644(10) 1 calc R U P A 1
H3B_6 H 0.695927 0.370489 0.087370 0.034 Uiso 0.644(10) 1 calc R U P A 1
C4_6 C 0.7865(6) 0.3819(8) 0.1626(4) 0.026(2) Uani 0.644(10) 1 d D U P A 1
H4A_6 H 0.837052 0.356452 0.174824 0.039 Uiso 0.644(10) 1 calc R U P A 1
H4B_6 H 0.757170 0.359824 0.190994 0.039 Uiso 0.644(10) 1 calc R U P A 1
H4C_6 H 0.789484 0.447698 0.164958 0.039 Uiso 0.644(10) 1 calc R U P A 1
O1_7 O 0.7917(14) 0.402(2) 0.0589(7) 0.038(4) Uani 0.356(10) 1 d D U P A 2
C1_7 C 0.7594(7) 0.4157(11) 0.1130(5) 0.036(3) Uani 0.356(10) 1 d D U P A 2
H1A_7 H 0.706130 0.397379 0.101848 0.043 Uiso 0.356(10) 1 calc R U P A 2
H1B_7 H 0.762096 0.480201 0.124392 0.043 Uiso 0.356(10) 1 calc R U P A 2
C2_7 C 0.8013(14) 0.3617(19) 0.1668(8) 0.040(6) Uani 0.356(10) 1 d D U P A 2
H2A_7 H 0.796255 0.297640 0.156045 0.059 Uiso 0.356(10) 1 calc R U P A 2
H2B_7 H 0.781051 0.373139 0.203116 0.059 Uiso 0.356(10) 1 calc R U P A 2
H2C_7 H 0.854319 0.378636 0.176758 0.059 Uiso 0.356(10) 1 calc R U P A 2
C3_7 C 0.7522(8) 0.4501(13) 0.0027(5) 0.049(4) Uani 0.356(10) 1 d D U P A 2
H3A_7 H 0.758164 0.515630 0.010619 0.058 Uiso 0.356(10) 1 calc R U P A 2
H3B_7 H 0.698174 0.435973 -0.005949 0.058 Uiso 0.356(10) 1 calc R U P A 2
C4_7 C 0.7795(17) 0.427(2) -0.0531(10) 0.043(5) Uani 0.356(10) 1 d D U P A 2
H4A_7 H 0.774756 0.362489 -0.060756 0.065 Uiso 0.356(10) 1 calc R U P A 2
H4B_7 H 0.832217 0.444995 -0.045927 0.065 Uiso 0.356(10) 1 calc R U P A 2
H4C_7 H 0.749705 0.459759 -0.089551 0.065 Uiso 0.356(10) 1 calc R U P A 2


loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Al1 O1_1 1.727(2) . ?
Al1 O1_2 1.728(2) . ?
Al1 O1_3 1.728(2) . ?
Al1 O1_4 1.730(2) . ?
O1_1 C1_1 1.353(4) . ?
C1_1 C2_1 1.557(4) . ?
C1_1 C3_1 1.557(5) . ?
C1_1 C4_1 1.565(5) . ?
C2_1 F1_1 1.344(4) . ?
C2_1 F2_1 1.350(4) . ?
C2_1 C9_1 1.548(4) . ?
C3_1 F3_1 1.351(4) . ?
C3_1 F4_1 1.352(4) . ?
C3_1 C7_1 1.544(5) . ?
C4_1 F5_1 1.347(4) . ?
C4_1 F6_1 1.349(4) . ?
C4_1 C5_1 1.548(5) . ?
C5_1 F7_1 1.367(4) . ?
C5_1 C6_1 1.546(5) . ?
C5_1 C10_1 1.549(5) . ?
C6_1 F9_1 1.346(4) . ?
C6_1 F8_1 1.347(4) . ?
C6_1 C7_1 1.546(5) . ?
C7_1 F10_1 1.365(4) . ?
C7_1 C8_1 1.554(5) . ?
C8_1 F12_1 1.341(4) . ?
C8_1 F11_1 1.351(4) . ?
C8_1 C9_1 1.542(5) . ?
C9_1 F13_1 1.362(4) . ?
C9_1 C10_1 1.542(5) . ?
C10_1 F15_1 1.340(4) . ?
C10_1 F14_1 1.348(4) . ?
O1_2 C1_2 1.354(4) . ?
C1_2 C4_2 1.555(4) . ?
C1_2 C3_2 1.557(4) . ?
C1_2 C2_2 1.569(4) . ?
C2_2 F1_2 1.341(4) . ?
C2_2 F2_2 1.346(4) . ?
C2_2 C9_2 1.553(5) . ?
C3_2 F4_2 1.344(4) . ?
C3_2 F3_2 1.351(4) . ?
C3_2 C7_2 1.557(4) . ?
C4_2 F5_2 1.342(4) . ?
C4_2 F6_2 1.356(4) . ?
C4_2 C5_2 1.550(4) . ?
C5_2 F7_2 1.372(4) . ?
C5_2 C10_2 1.539(5) . ?
C5_2 C6_2 1.544(5) . ?
C6_2 F8_2 1.343(4) . ?
C6_2 F9_2 1.358(4) . ?
C6_2 C7_2 1.538(5) . ?
C7_2 F10_2 1.358(4) . ?
C7_2 C8_2 1.552(5) . ?
C8_2 F11_2 1.343(4) . ?
C8_2 F12_2 1.354(4) . ?
C8_2 C9_2 1.549(5) . ?
C9_2 F13_2 1.363(4) . ?
C9_2 C10_2 1.538(5) . ?
C10_2 F14_2 1.347(4) . ?
C10_2 F15_2 1.363(4) . ?
O1_3 C1_3 1.349(4) . ?
C1_3 C4_3 1.556(5) . ?
C1_3 C2_3 1.559(5) . ?
C1_3 C3_3 1.563(4) . ?
C2_3 F1_3 1.350(4) . ?
C2_3 F2_3 1.354(4) . ?
C2_3 C9_3 1.545(5) . ?
C3_3 F3_3 1.344(4) . ?
C3_3 F4_3 1.345(4) . ?
C3_3 C7_3 1.550(4) . ?
C4_3 F5_3 1.341(4) . ?
C4_3 F6_3 1.354(4) . ?
C4_3 C5_3 1.545(5) . ?
C5_3 F7_3 1.368(4) . ?
C5_3 C10_3 1.544(5) . ?
C5_3 C6_3 1.550(5) . ?
C6_3 F8_3 1.343(4) . ?
C6_3 F9_3 1.345(4) . ?
C6_3 C7_3 1.540(5) . ?
C7_3 F10_3 1.361(4) . ?
C7_3 C8_3 1.551(5) . ?
C8_3 F11_3 1.346(4) . ?
C8_3 F12_3 1.347(4) . ?
C8_3 C9_3 1.542(5) . ?
C9_3 F13_3 1.369(4) . ?
C9_3 C10_3 1.538(5) . ?
C10_3 F14_3 1.348(4) . ?
C10_3 F15_3 1.350(4) . ?
O1_4 C1_4 1.345(4) . ?
C1_4 C2_4 1.561(4) . ?
C1_4 C4_4 1.561(4) . ?
C1_4 C3_4 1.565(5) . ?
C2_4 F2_4 1.345(4) . ?
C2_4 F1_4 1.347(4) . ?
C2_4 C9_4 1.548(5) . ?
C3_4 F4_4 1.341(4) . ?
C3_4 F3_4 1.356(4) . ?
C3_4 C7_4 1.549(4) . ?
C4_4 F6_4 1.340(4) . ?
C4_4 F5_4 1.352(4) . ?
C4_4 C5_4 1.552(5) . ?
C5_4 F7_4 1.370(4) . ?
C5_4 C6_4 1.538(5) . ?
C5_4 C10_4 1.541(5) . ?
C6_4 F9_4 1.347(4) . ?
C6_4 F8_4 1.350(4) . ?
C6_4 C7_4 1.546(5) . ?
C7_4 F10_4 1.365(4) . ?
C7_4 C8_4 1.544(5) . ?
C8_4 F12_4 1.344(4) . ?
C8_4 F11_4 1.353(4) . ?
C8_4 C9_4 1.538(5) . ?
C9_4 F13_4 1.372(4) . ?
C9_4 C10_4 1.546(5) . ?
C10_4 F14_4 1.345(4) . ?
C10_4 F15_4 1.347(4) . ?
O1_5 C3_5 1.458(5) . ?
O1_5 C1_5 1.472(5) . ?
O1_5 O1_7 2.35(2) . ?
O1_5 O1_6 2.451(12) . ?
O1_5 H1 1.33(4) . ?
C1_5 C2_5 1.489(6) . ?
C1_5 H1A_5 0.9900 . ?
C1_5 H1B_5 0.9900 . ?
C2_5 H2A_5 0.9800 . ?
C2_5 H2B_5 0.9800 . ?
C2_5 H2C_5 0.9800 . ?
C3_5 C4_5 1.487(7) . ?
C3_5 H3A_5 0.9900 . ?
C3_5 H3B_5 0.9900 . ?
C4_5 H4A_5 0.9800 . ?
C4_5 H4B_5 0.9800 . ?
C4_5 H4C_5 0.9800 . ?
O1_6 C3_6 1.456(10) . ?
O1_6 C1_6 1.469(10) . ?
O1_6 H1 1.13(4) . ?
C1_6 C2_6 1.494(13) . ?
C1_6 H1A_6 0.9900 . ?
C1_6 H1B_6 0.9900 . ?
C2_6 H2A_6 0.9800 . ?
C2_6 H2B_6 0.9800 . ?
C2_6 H2C_6 0.9800 . ?
C3_6 C4_6 1.487(10) . ?
C3_6 H3A_6 0.9900 . ?
C3_6 H3B_6 0.9900 . ?
C4_6 H4A_6 0.9800 . ?
C4_6 H4B_6 0.9800 . ?
C4_6 H4C_6 0.9800 . ?
O1_7 C3_7 1.461(14) . ?
O1_7 C1_7 1.472(14) . ?
O1_7 H1 1.03(4) . ?
C1_7 C2_7 1.481(13) . ?
C1_7 H1A_7 0.9900 . ?
C1_7 H1B_7 0.9900 . ?
C2_7 H2A_7 0.9800 . ?
C2_7 H2B_7 0.9800 . ?
C2_7 H2C_7 0.9800 . ?
C3_7 C4_7 1.481(14) . ?
C3_7 H3A_7 0.9900 . ?
C3_7 H3B_7 0.9900 . ?
C4_7 H4A_7 0.9800 . ?
C4_7 H4B_7 0.9800 . ?
C4_7 H4C_7 0.9800 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O1_1 Al1 O1_2 107.74(12) . . ?
O1_1 Al1 O1_3 108.99(12) . . ?
O1_2 Al1 O1_3 111.65(12) . . ?
O1_1 Al1 O1_4 111.20(12) . . ?
O1_2 Al1 O1_4 109.80(12) . . ?
O1_3 Al1 O1_4 107.48(12) . . ?
C1_1 O1_1 Al1 147.6(2) . . ?
O1_1 C1_1 C2_1 109.7(3) . . ?
O1_1 C1_1 C3_1 112.1(3) . . ?
C2_1 C1_1 C3_1 107.2(3) . . ?
O1_1 C1_1 C4_1 112.8(3) . . ?
C2_1 C1_1 C4_1 107.6(3) . . ?
C3_1 C1_1 C4_1 107.2(3) . . ?
F1_1 C2_1 F2_1 106.0(3) . . ?
F1_1 C2_1 C9_1 109.5(3) . . ?
F2_1 C2_1 C9_1 109.3(3) . . ?
F1_1 C2_1 C1_1 109.9(3) . . ?
F2_1 C2_1 C1_1 110.1(3) . . ?
C9_1 C2_1 C1_1 111.9(3) . . ?
F3_1 C3_1 F4_1 105.4(3) . . ?
F3_1 C3_1 C7_1 109.4(3) . . ?
F4_1 C3_1 C7_1 109.2(3) . . ?
F3_1 C3_1 C1_1 110.2(3) . . ?
F4_1 C3_1 C1_1 110.8(3) . . ?
C7_1 C3_1 C1_1 111.8(3) . . ?
F5_1 C4_1 F6_1 105.6(3) . . ?
F5_1 C4_1 C5_1 109.9(3) . . ?
F6_1 C4_1 C5_1 109.1(3) . . ?
F5_1 C4_1 C1_1 110.2(3) . . ?
F6_1 C4_1 C1_1 110.4(3) . . ?
C5_1 C4_1 C1_1 111.6(3) . . ?
F7_1 C5_1 C6_1 109.4(3) . . ?
F7_1 C5_1 C4_1 109.8(3) . . ?
C6_1 C5_1 C4_1 109.4(3) . . ?
F7_1 C5_1 C10_1 109.6(3) . . ?
C6_1 C5_1 C10_1 109.1(3) . . ?
C4_1 C5_1 C10_1 109.6(3) . . ?
F9_1 C6_1 F8_1 105.8(3) . . ?
F9_1 C6_1 C5_1 111.0(3) . . ?
F8_1 C6_1 C5_1 110.1(3) . . ?
F9_1 C6_1 C7_1 110.1(3) . . ?
F8_1 C6_1 C7_1 110.6(3) . . ?
C5_1 C6_1 C7_1 109.2(3) . . ?
F10_1 C7_1 C3_1 109.8(3) . . ?
F10_1 C7_1 C6_1 109.0(3) . . ?
C3_1 C7_1 C6_1 109.6(3) . . ?
F10_1 C7_1 C8_1 109.4(3) . . ?
C3_1 C7_1 C8_1 109.5(3) . . ?
C6_1 C7_1 C8_1 109.4(3) . . ?
F12_1 C8_1 F11_1 106.2(3) . . ?
F12_1 C8_1 C9_1 110.8(3) . . ?
F11_1 C8_1 C9_1 110.4(3) . . ?
F12_1 C8_1 C7_1 110.2(3) . . ?
F11_1 C8_1 C7_1 110.2(3) . . ?
C9_1 C8_1 C7_1 109.1(3) . . ?
F13_1 C9_1 C8_1 109.5(3) . . ?
F13_1 C9_1 C10_1 109.1(3) . . ?
C8_1 C9_1 C10_1 108.9(3) . . ?
F13_1 C9_1 C2_1 110.0(3) . . ?
C8_1 C9_1 C2_1 109.6(3) . . ?
C10_1 C9_1 C2_1 109.7(3) . . ?
F15_1 C10_1 F14_1 105.9(3) . . ?
F15_1 C10_1 C9_1 110.9(3) . . ?
F14_1 C10_1 C9_1 110.7(3) . . ?
F15_1 C10_1 C5_1 110.2(3) . . ?
F14_1 C10_1 C5_1 109.3(3) . . ?
C9_1 C10_1 C5_1 109.8(3) . . ?
C1_2 O1_2 Al1 148.0(2) . . ?
O1_2 C1_2 C4_2 112.9(3) . . ?
O1_2 C1_2 C3_2 109.6(2) . . ?
C4_2 C1_2 C3_2 107.5(2) . . ?
O1_2 C1_2 C2_2 111.1(3) . . ?
C4_2 C1_2 C2_2 108.1(2) . . ?
C3_2 C1_2 C2_2 107.5(2) . . ?
F1_2 C2_2 F2_2 106.6(3) . . ?
F1_2 C2_2 C9_2 109.3(3) . . ?
F2_2 C2_2 C9_2 109.6(3) . . ?
F1_2 C2_2 C1_2 109.9(3) . . ?
F2_2 C2_2 C1_2 110.1(3) . . ?
C9_2 C2_2 C1_2 111.1(3) . . ?
F4_2 C3_2 F3_2 105.9(3) . . ?
F4_2 C3_2 C7_2 109.0(3) . . ?
F3_2 C3_2 C7_2 109.0(3) . . ?
F4_2 C3_2 C1_2 110.4(3) . . ?
F3_2 C3_2 C1_2 110.9(3) . . ?
C7_2 C3_2 C1_2 111.5(3) . . ?
F5_2 C4_2 F6_2 105.8(2) . . ?
F5_2 C4_2 C5_2 109.5(3) . . ?
F6_2 C4_2 C5_2 109.3(3) . . ?
F5_2 C4_2 C1_2 110.6(3) . . ?
F6_2 C4_2 C1_2 110.1(3) . . ?
C5_2 C4_2 C1_2 111.4(3) . . ?
F7_2 C5_2 C10_2 109.2(3) . . ?
F7_2 C5_2 C6_2 109.2(3) . . ?
C10_2 C5_2 C6_2 109.9(3) . . ?
F7_2 C5_2 C4_2 110.2(3) . . ?
C10_2 C5_2 C4_2 109.4(3) . . ?
C6_2 C5_2 C4_2 109.0(3) . . ?
F8_2 C6_2 F9_2 105.4(3) . . ?
F8_2 C6_2 C7_2 110.6(3) . . ?
F9_2 C6_2 C7_2 110.8(3) . . ?
F8_2 C6_2 C5_2 111.0(3) . . ?
F9_2 C6_2 C5_2 109.4(3) . . ?
C7_2 C6_2 C5_2 109.6(3) . . ?
F10_2 C7_2 C6_2 110.4(3) . . ?
F10_2 C7_2 C8_2 109.2(3) . . ?
C6_2 C7_2 C8_2 109.4(3) . . ?
F10_2 C7_2 C3_2 109.4(3) . . ?
C6_2 C7_2 C3_2 109.5(3) . . ?
C8_2 C7_2 C3_2 108.8(3) . . ?
F11_2 C8_2 F12_2 105.9(3) . . ?
F11_2 C8_2 C9_2 110.8(3) . . ?
F12_2 C8_2 C9_2 110.0(3) . . ?
F11_2 C8_2 C7_2 110.5(3) . . ?
F12_2 C8_2 C7_2 109.9(3) . . ?
C9_2 C8_2 C7_2 109.7(3) . . ?
F13_2 C9_2 C10_2 109.0(3) . . ?
F13_2 C9_2 C8_2 109.9(3) . . ?
C10_2 C9_2 C8_2 109.3(3) . . ?
F13_2 C9_2 C2_2 110.1(3) . . ?
C10_2 C9_2 C2_2 109.2(3) . . ?
C8_2 C9_2 C2_2 109.2(3) . . ?
F14_2 C10_2 F15_2 105.2(3) . . ?
F14_2 C10_2 C9_2 110.7(3) . . ?
F15_2 C10_2 C9_2 110.5(3) . . ?
F14_2 C10_2 C5_2 110.3(3) . . ?
F15_2 C10_2 C5_2 109.9(3) . . ?
C9_2 C10_2 C5_2 110.1(3) . . ?
C1_3 O1_3 Al1 147.3(2) . . ?
O1_3 C1_3 C4_3 113.2(3) . . ?
O1_3 C1_3 C2_3 111.6(3) . . ?
C4_3 C1_3 C2_3 107.6(3) . . ?
O1_3 C1_3 C3_3 109.8(3) . . ?
C4_3 C1_3 C3_3 107.3(3) . . ?
C2_3 C1_3 C3_3 107.2(3) . . ?
F1_3 C2_3 F2_3 105.5(3) . . ?
F1_3 C2_3 C9_3 109.3(3) . . ?
F2_3 C2_3 C9_3 109.7(3) . . ?
F1_3 C2_3 C1_3 109.8(3) . . ?
F2_3 C2_3 C1_3 110.4(3) . . ?
C9_3 C2_3 C1_3 111.9(3) . . ?
F3_3 C3_3 F4_3 106.3(3) . . ?
F3_3 C3_3 C7_3 109.4(3) . . ?
F4_3 C3_3 C7_3 109.5(3) . . ?
F3_3 C3_3 C1_3 110.0(3) . . ?
F4_3 C3_3 C1_3 110.0(3) . . ?
C7_3 C3_3 C1_3 111.5(3) . . ?
F5_3 C4_3 F6_3 105.6(3) . . ?
F5_3 C4_3 C5_3 109.2(3) . . ?
F6_3 C4_3 C5_3 109.4(3) . . ?
F5_3 C4_3 C1_3 110.8(3) . . ?
F6_3 C4_3 C1_3 110.0(3) . . ?
C5_3 C4_3 C1_3 111.6(3) . . ?
F7_3 C5_3 C10_3 109.1(3) . . ?
F7_3 C5_3 C4_3 109.9(3) . . ?
C10_3 C5_3 C4_3 109.8(3) . . ?
F7_3 C5_3 C6_3 109.4(3) . . ?
C10_3 C5_3 C6_3 109.5(3) . . ?
C4_3 C5_3 C6_3 109.2(3) . . ?
F8_3 C6_3 F9_3 106.1(3) . . ?
F8_3 C6_3 C7_3 110.5(3) . . ?
F9_3 C6_3 C7_3 110.9(3) . . ?
F8_3 C6_3 C5_3 110.3(3) . . ?
F9_3 C6_3 C5_3 109.8(3) . . ?
C7_3 C6_3 C5_3 109.3(3) . . ?
F10_3 C7_3 C6_3 109.3(3) . . ?
F10_3 C7_3 C3_3 109.8(3) . . ?
C6_3 C7_3 C3_3 109.7(3) . . ?
F10_3 C7_3 C8_3 109.4(3) . . ?
C6_3 C7_3 C8_3 109.3(3) . . ?
C3_3 C7_3 C8_3 109.4(3) . . ?
F11_3 C8_3 F12_3 106.2(3) . . ?
F11_3 C8_3 C9_3 110.6(3) . . ?
F12_3 C8_3 C9_3 110.2(3) . . ?
F11_3 C8_3 C7_3 110.5(3) . . ?
F12_3 C8_3 C7_3 110.1(3) . . ?
C9_3 C8_3 C7_3 109.2(3) . . ?
F13_3 C9_3 C10_3 109.4(3) . . ?
F13_3 C9_3 C8_3 109.4(3) . . ?
C10_3 C9_3 C8_3 109.8(3) . . ?
F13_3 C9_3 C2_3 109.6(3) . . ?
C10_3 C9_3 C2_3 109.2(3) . . ?
C8_3 C9_3 C2_3 109.5(3) . . ?
F14_3 C10_3 F15_3 105.5(3) . . ?
F14_3 C10_3 C9_3 110.5(3) . . ?
F15_3 C10_3 C9_3 110.9(3) . . ?
F14_3 C10_3 C5_3 109.9(3) . . ?
F15_3 C10_3 C5_3 110.6(3) . . ?
C9_3 C10_3 C5_3 109.4(3) . . ?
C1_4 O1_4 Al1 148.9(2) . . ?
O1_4 C1_4 C2_4 108.7(3) . . ?
O1_4 C1_4 C4_4 113.6(3) . . ?
C2_4 C1_4 C4_4 107.2(2) . . ?
O1_4 C1_4 C3_4 112.3(3) . . ?
C2_4 C1_4 C3_4 107.5(3) . . ?
C4_4 C1_4 C3_4 107.3(3) . . ?
F2_4 C2_4 F1_4 106.3(3) . . ?
F2_4 C2_4 C9_4 109.6(3) . . ?
F1_4 C2_4 C9_4 109.3(3) . . ?
F2_4 C2_4 C1_4 110.7(3) . . ?
F1_4 C2_4 C1_4 109.6(3) . . ?
C9_4 C2_4 C1_4 111.2(3) . . ?
F4_4 C3_4 F3_4 106.0(3) . . ?
F4_4 C3_4 C7_4 109.7(3) . . ?
F3_4 C3_4 C7_4 108.8(3) . . ?
F4_4 C3_4 C1_4 110.2(3) . . ?
F3_4 C3_4 C1_4 110.1(3) . . ?
C7_4 C3_4 C1_4 111.7(3) . . ?
F6_4 C4_4 F5_4 105.7(3) . . ?
F6_4 C4_4 C5_4 109.7(3) . . ?
F5_4 C4_4 C5_4 109.4(3) . . ?
F6_4 C4_4 C1_4 110.7(3) . . ?
F5_4 C4_4 C1_4 109.8(3) . . ?
C5_4 C4_4 C1_4 111.4(3) . . ?
F7_4 C5_4 C6_4 109.4(3) . . ?
F7_4 C5_4 C10_4 109.2(3) . . ?
C6_4 C5_4 C10_4 109.4(3) . . ?
F7_4 C5_4 C4_4 109.4(3) . . ?
C6_4 C5_4 C4_4 110.3(3) . . ?
C10_4 C5_4 C4_4 109.1(3) . . ?
F9_4 C6_4 F8_4 105.7(3) . . ?
F9_4 C6_4 C5_4 110.7(3) . . ?
F8_4 C6_4 C5_4 110.1(3) . . ?
F9_4 C6_4 C7_4 110.7(3) . . ?
F8_4 C6_4 C7_4 110.5(3) . . ?
C5_4 C6_4 C7_4 109.2(3) . . ?
F10_4 C7_4 C8_4 109.2(3) . . ?
F10_4 C7_4 C6_4 109.9(3) . . ?
C8_4 C7_4 C6_4 109.2(3) . . ?
F10_4 C7_4 C3_4 109.4(3) . . ?
C8_4 C7_4 C3_4 109.7(3) . . ?
C6_4 C7_4 C3_4 109.4(3) . . ?
F12_4 C8_4 F11_4 105.7(3) . . ?
F12_4 C8_4 C9_4 111.1(3) . . ?
F11_4 C8_4 C9_4 110.7(3) . . ?
F12_4 C8_4 C7_4 110.1(3) . . ?
F11_4 C8_4 C7_4 109.9(3) . . ?
C9_4 C8_4 C7_4 109.2(3) . . ?
F13_4 C9_4 C8_4 109.5(3) . . ?
F13_4 C9_4 C10_4 108.9(3) . . ?
C8_4 C9_4 C10_4 109.2(3) . . ?
F13_4 C9_4 C2_4 109.4(3) . . ?
C8_4 C9_4 C2_4 110.2(3) . . ?
C10_4 C9_4 C2_4 109.6(3) . . ?
F14_4 C10_4 F15_4 105.8(3) . . ?
F14_4 C10_4 C5_4 110.4(3) . . ?
F15_4 C10_4 C5_4 110.8(3) . . ?
F14_4 C10_4 C9_4 110.4(3) . . ?
F15_4 C10_4 C9_4 110.2(3) . . ?
C5_4 C10_4 C9_4 109.2(3) . . ?
C3_5 O1_5 C1_5 114.6(3) . . ?
C3_5 O1_5 O1_7 119.8(8) . . ?
C1_5 O1_5 O1_7 110.2(8) . . ?
C3_5 O1_5 O1_6 119.6(4) . . ?
C1_5 O1_5 O1_6 111.6(4) . . ?
C3_5 O1_5 H1 116.1(16) . . ?
C1_5 O1_5 H1 113.2(16) . . ?
O1_7 O1_5 H1 3.8(18) . . ?
O1_6 O1_5 H1 3.8(16) . . ?
O1_5 C1_5 C2_5 111.7(3) . . ?
O1_5 C1_5 H1A_5 109.3 . . ?
C2_5 C1_5 H1A_5 109.3 . . ?
O1_5 C1_5 H1B_5 109.3 . . ?
C2_5 C1_5 H1B_5 109.3 . . ?
H1A_5 C1_5 H1B_5 107.9 . . ?
C1_5 C2_5 H2A_5 109.5 . . ?
C1_5 C2_5 H2B_5 109.5 . . ?
H2A_5 C2_5 H2B_5 109.5 . . ?
C1_5 C2_5 H2C_5 109.5 . . ?
H2A_5 C2_5 H2C_5 109.5 . . ?
H2B_5 C2_5 H2C_5 109.5 . . ?
O1_5 C3_5 C4_5 108.8(4) . . ?
O1_5 C3_5 H3A_5 109.9 . . ?
C4_5 C3_5 H3A_5 109.9 . . ?
O1_5 C3_5 H3B_5 109.9 . . ?
C4_5 C3_5 H3B_5 109.9 . . ?
H3A_5 C3_5 H3B_5 108.3 . . ?
C3_5 C4_5 H4A_5 109.5 . . ?
C3_5 C4_5 H4B_5 109.5 . . ?
H4A_5 C4_5 H4B_5 109.5 . . ?
C3_5 C4_5 H4C_5 109.5 . . ?
H4A_5 C4_5 H4C_5 109.5 . . ?
H4B_5 C4_5 H4C_5 109.5 . . ?
C3_6 O1_6 C1_6 115.1(9) . . ?
C3_6 O1_6 O1_5 117.8(5) . . ?
C1_6 O1_6 O1_5 113.8(6) . . ?
C3_6 O1_6 H1 113.6(19) . . ?
C1_6 O1_6 H1 116(2) . . ?
O1_5 O1_6 H1 4.5(19) . . ?
O1_6 C1_6 C2_6 106.7(9) . . ?
O1_6 C1_6 H1A_6 110.4 . . ?
C2_6 C1_6 H1A_6 110.4 . . ?
O1_6 C1_6 H1B_6 110.4 . . ?
C2_6 C1_6 H1B_6 110.4 . . ?
H1A_6 C1_6 H1B_6 108.6 . . ?
C1_6 C2_6 H2A_6 109.5 . . ?
C1_6 C2_6 H2B_6 109.5 . . ?
H2A_6 C2_6 H2B_6 109.5 . . ?
C1_6 C2_6 H2C_6 109.5 . . ?
H2A_6 C2_6 H2C_6 109.5 . . ?
H2B_6 C2_6 H2C_6 109.5 . . ?
O1_6 C3_6 C4_6 109.0(7) . . ?
O1_6 C3_6 H3A_6 109.9 . . ?
C4_6 C3_6 H3A_6 109.9 . . ?
O1_6 C3_6 H3B_6 109.9 . . ?
C4_6 C3_6 H3B_6 109.9 . . ?
H3A_6 C3_6 H3B_6 108.3 . . ?
C3_6 C4_6 H4A_6 109.5 . . ?
C3_6 C4_6 H4B_6 109.5 . . ?
H4A_6 C4_6 H4B_6 109.5 . . ?
C3_6 C4_6 H4C_6 109.5 . . ?
H4A_6 C4_6 H4C_6 109.5 . . ?
H4B_6 C4_6 H4C_6 109.5 . . ?
C3_7 O1_7 C1_7 113.7(16) . . ?
C3_7 O1_7 O1_5 116.5(13) . . ?
C1_7 O1_7 O1_5 115.0(13) . . ?
C3_7 O1_7 H1 120(3) . . ?
C1_7 O1_7 H1 115(3) . . ?
O1_5 O1_7 H1 5(2) . . ?
O1_7 C1_7 C2_7 109.8(13) . . ?
O1_7 C1_7 H1A_7 109.7 . . ?
C2_7 C1_7 H1A_7 109.7 . . ?
O1_7 C1_7 H1B_7 109.7 . . ?
C2_7 C1_7 H1B_7 109.7 . . ?
H1A_7 C1_7 H1B_7 108.2 . . ?
C1_7 C2_7 H2A_7 109.5 . . ?
C1_7 C2_7 H2B_7 109.5 . . ?
H2A_7 C2_7 H2B_7 109.5 . . ?
C1_7 C2_7 H2C_7 109.5 . . ?
H2A_7 C2_7 H2C_7 109.5 . . ?
H2B_7 C2_7 H2C_7 109.5 . . ?
O1_7 C3_7 C4_7 113.2(15) . . ?
O1_7 C3_7 H3A_7 108.9 . . ?
C4_7 C3_7 H3A_7 108.9 . . ?
O1_7 C3_7 H3B_7 108.9 . . ?
C4_7 C3_7 H3B_7 108.9 . . ?
H3A_7 C3_7 H3B_7 107.8 . . ?
C3_7 C4_7 H4A_7 109.5 . . ?
C3_7 C4_7 H4B_7 109.5 . . ?
H4A_7 C4_7 H4B_7 109.5 . . ?
C3_7 C4_7 H4C_7 109.5 . . ?
H4A_7 C4_7 H4C_7 109.5 . . ?
H4B_7 C4_7 H4C_7 109.5 . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
O1_2 Al1 O1_1 C1_1 -37.7(4) . . . . ?
O1_3 Al1 O1_1 C1_1 -159.0(4) . . . . ?
O1_4 Al1 O1_1 C1_1 82.7(4) . . . . ?
Al1 O1_1 C1_1 C2_1 -162.4(3) . . . . ?
Al1 O1_1 C1_1 C3_1 78.6(5) . . . . ?
Al1 O1_1 C1_1 C4_1 -42.6(5) . . . . ?
O1_1 C1_1 C2_1 F1_1 -57.8(3) . . . . ?
C3_1 C1_1 C2_1 F1_1 64.1(3) . . . . ?
C4_1 C1_1 C2_1 F1_1 179.2(3) . . . . ?
O1_1 C1_1 C2_1 F2_1 58.7(3) . . . . ?
C3_1 C1_1 C2_1 F2_1 -179.4(3) . . . . ?
C4_1 C1_1 C2_1 F2_1 -64.3(3) . . . . ?
O1_1 C1_1 C2_1 C9_1 -179.6(3) . . . . ?
C3_1 C1_1 C2_1 C9_1 -57.7(4) . . . . ?
C4_1 C1_1 C2_1 C9_1 57.4(4) . . . . ?
O1_1 C1_1 C3_1 F3_1 56.3(4) . . . . ?
C2_1 C1_1 C3_1 F3_1 -64.1(3) . . . . ?
C4_1 C1_1 C3_1 F3_1 -179.4(3) . . . . ?
O1_1 C1_1 C3_1 F4_1 -59.9(4) . . . . ?
C2_1 C1_1 C3_1 F4_1 179.7(3) . . . . ?
C4_1 C1_1 C3_1 F4_1 64.4(3) . . . . ?
O1_1 C1_1 C3_1 C7_1 178.2(3) . . . . ?
C2_1 C1_1 C3_1 C7_1 57.8(4) . . . . ?
C4_1 C1_1 C3_1 C7_1 -57.5(4) . . . . ?
O1_1 C1_1 C4_1 F5_1 59.2(4) . . . . ?
C2_1 C1_1 C4_1 F5_1 -179.8(3) . . . . ?
C3_1 C1_1 C4_1 F5_1 -64.7(3) . . . . ?
O1_1 C1_1 C4_1 F6_1 -57.1(4) . . . . ?
C2_1 C1_1 C4_1 F6_1 64.0(3) . . . . ?
C3_1 C1_1 C4_1 F6_1 179.1(3) . . . . ?
O1_1 C1_1 C4_1 C5_1 -178.5(3) . . . . ?
C2_1 C1_1 C4_1 C5_1 -57.4(3) . . . . ?
C3_1 C1_1 C4_1 C5_1 57.6(3) . . . . ?
F5_1 C4_1 C5_1 F7_1 -57.6(4) . . . . ?
F6_1 C4_1 C5_1 F7_1 57.7(4) . . . . ?
C1_1 C4_1 C5_1 F7_1 179.8(3) . . . . ?
F5_1 C4_1 C5_1 C6_1 62.4(4) . . . . ?
F6_1 C4_1 C5_1 C6_1 177.7(3) . . . . ?
C1_1 C4_1 C5_1 C6_1 -60.2(4) . . . . ?
F5_1 C4_1 C5_1 C10_1 -178.1(3) . . . . ?
F6_1 C4_1 C5_1 C10_1 -62.8(4) . . . . ?
C1_1 C4_1 C5_1 C10_1 59.4(4) . . . . ?
F7_1 C5_1 C6_1 F9_1 -58.3(4) . . . . ?
C4_1 C5_1 C6_1 F9_1 -178.6(3) . . . . ?
C10_1 C5_1 C6_1 F9_1 61.6(4) . . . . ?
F7_1 C5_1 C6_1 F8_1 58.6(4) . . . . ?
C4_1 C5_1 C6_1 F8_1 -61.7(4) . . . . ?
C10_1 C5_1 C6_1 F8_1 178.5(3) . . . . ?
F7_1 C5_1 C6_1 C7_1 -179.8(3) . . . . ?
C4_1 C5_1 C6_1 C7_1 59.9(4) . . . . ?
C10_1 C5_1 C6_1 C7_1 -60.0(3) . . . . ?
F3_1 C3_1 C7_1 F10_1 -57.9(4) . . . . ?
F4_1 C3_1 C7_1 F10_1 57.0(4) . . . . ?
C1_1 C3_1 C7_1 F10_1 179.8(3) . . . . ?
F3_1 C3_1 C7_1 C6_1 -177.6(3) . . . . ?
F4_1 C3_1 C7_1 C6_1 -62.8(4) . . . . ?
C1_1 C3_1 C7_1 C6_1 60.1(4) . . . . ?
F3_1 C3_1 C7_1 C8_1 62.3(4) . . . . ?
F4_1 C3_1 C7_1 C8_1 177.1(3) . . . . ?
C1_1 C3_1 C7_1 C8_1 -60.0(4) . . . . ?
F9_1 C6_1 C7_1 F10_1 57.8(4) . . . . ?
F8_1 C6_1 C7_1 F10_1 -58.8(4) . . . . ?
C5_1 C6_1 C7_1 F10_1 179.9(3) . . . . ?
F9_1 C6_1 C7_1 C3_1 178.0(3) . . . . ?
F8_1 C6_1 C7_1 C3_1 61.4(4) . . . . ?
C5_1 C6_1 C7_1 C3_1 -59.9(4) . . . . ?
F9_1 C6_1 C7_1 C8_1 -61.8(4) . . . . ?
F8_1 C6_1 C7_1 C8_1 -178.4(3) . . . . ?
C5_1 C6_1 C7_1 C8_1 60.3(3) . . . . ?
F10_1 C7_1 C8_1 F12_1 -58.3(4) . . . . ?
C3_1 C7_1 C8_1 F12_1 -178.7(3) . . . . ?
C6_1 C7_1 C8_1 F12_1 61.1(4) . . . . ?
F10_1 C7_1 C8_1 F11_1 58.5(4) . . . . ?
C3_1 C7_1 C8_1 F11_1 -61.8(4) . . . . ?
C6_1 C7_1 C8_1 F11_1 178.0(3) . . . . ?
F10_1 C7_1 C8_1 C9_1 179.9(3) . . . . ?
C3_1 C7_1 C8_1 C9_1 59.5(4) . . . . ?
C6_1 C7_1 C8_1 C9_1 -60.7(4) . . . . ?
F12_1 C8_1 C9_1 F13_1 58.3(4) . . . . ?
F11_1 C8_1 C9_1 F13_1 -59.0(4) . . . . ?
C7_1 C8_1 C9_1 F13_1 179.8(3) . . . . ?
F12_1 C8_1 C9_1 C10_1 -60.9(4) . . . . ?
F11_1 C8_1 C9_1 C10_1 -178.2(3) . . . . ?
C7_1 C8_1 C9_1 C10_1 60.6(3) . . . . ?
F12_1 C8_1 C9_1 C2_1 179.1(3) . . . . ?
F11_1 C8_1 C9_1 C2_1 61.8(3) . . . . ?
C7_1 C8_1 C9_1 C2_1 -59.4(4) . . . . ?
F1_1 C2_1 C9_1 F13_1 58.5(4) . . . . ?
F2_1 C2_1 C9_1 F13_1 -57.2(4) . . . . ?
C1_1 C2_1 C9_1 F13_1 -179.4(3) . . . . ?
F1_1 C2_1 C9_1 C8_1 -62.0(3) . . . . ?
F2_1 C2_1 C9_1 C8_1 -177.7(3) . . . . ?
C1_1 C2_1 C9_1 C8_1 60.1(4) . . . . ?
F1_1 C2_1 C9_1 C10_1 178.5(3) . . . . ?
F2_1 C2_1 C9_1 C10_1 62.8(3) . . . . ?
C1_1 C2_1 C9_1 C10_1 -59.4(4) . . . . ?
F13_1 C9_1 C10_1 F15_1 -58.3(4) . . . . ?
C8_1 C9_1 C10_1 F15_1 61.1(4) . . . . ?
C2_1 C9_1 C10_1 F15_1 -178.9(3) . . . . ?
F13_1 C9_1 C10_1 F14_1 58.9(4) . . . . ?
C8_1 C9_1 C10_1 F14_1 178.3(3) . . . . ?
C2_1 C9_1 C10_1 F14_1 -61.7(4) . . . . ?
F13_1 C9_1 C10_1 C5_1 179.6(3) . . . . ?
C8_1 C9_1 C10_1 C5_1 -60.9(3) . . . . ?
C2_1 C9_1 C10_1 C5_1 59.0(4) . . . . ?
F7_1 C5_1 C10_1 F15_1 57.8(4) . . . . ?
C6_1 C5_1 C10_1 F15_1 -61.9(4) . . . . ?
C4_1 C5_1 C10_1 F15_1 178.4(3) . . . . ?
F7_1 C5_1 C10_1 F14_1 -58.1(4) . . . . ?
C6_1 C5_1 C10_1 F14_1 -177.8(3) . . . . ?
C4_1 C5_1 C10_1 F14_1 62.5(4) . . . . ?
F7_1 C5_1 C10_1 C9_1 -179.7(3) . . . . ?
C6_1 C5_1 C10_1 C9_1 60.6(4) . . . . ?
C4_1 C5_1 C10_1 C9_1 -59.2(4) . . . . ?
O1_1 Al1 O1_2 C1_2 162.8(4) . . . . ?
O1_3 Al1 O1_2 C1_2 -77.6(4) . . . . ?
O1_4 Al1 O1_2 C1_2 41.5(4) . . . . ?
Al1 O1_2 C1_2 C4_2 33.5(5) . . . . ?
Al1 O1_2 C1_2 C3_2 153.3(3) . . . . ?
Al1 O1_2 C1_2 C2_2 -88.1(4) . . . . ?
O1_2 C1_2 C2_2 F1_2 -57.1(3) . . . . ?
C4_2 C1_2 C2_2 F1_2 178.5(2) . . . . ?
C3_2 C1_2 C2_2 F1_2 62.8(3) . . . . ?
O1_2 C1_2 C2_2 F2_2 60.1(3) . . . . ?
C4_2 C1_2 C2_2 F2_2 -64.3(3) . . . . ?
C3_2 C1_2 C2_2 F2_2 180.0(2) . . . . ?
O1_2 C1_2 C2_2 C9_2 -178.3(3) . . . . ?
C4_2 C1_2 C2_2 C9_2 57.3(3) . . . . ?
C3_2 C1_2 C2_2 C9_2 -58.4(3) . . . . ?
O1_2 C1_2 C3_2 F4_2 -59.2(3) . . . . ?
C4_2 C1_2 C3_2 F4_2 63.8(3) . . . . ?
C2_2 C1_2 C3_2 F4_2 179.9(2) . . . . ?
O1_2 C1_2 C3_2 F3_2 57.8(3) . . . . ?
C4_2 C1_2 C3_2 F3_2 -179.2(2) . . . . ?
C2_2 C1_2 C3_2 F3_2 -63.1(3) . . . . ?
O1_2 C1_2 C3_2 C7_2 179.5(3) . . . . ?
C4_2 C1_2 C3_2 C7_2 -57.5(3) . . . . ?
C2_2 C1_2 C3_2 C7_2 58.6(3) . . . . ?
O1_2 C1_2 C4_2 F5_2 57.4(3) . . . . ?
C3_2 C1_2 C4_2 F5_2 -63.6(3) . . . . ?
C2_2 C1_2 C4_2 F5_2 -179.3(2) . . . . ?
O1_2 C1_2 C4_2 F6_2 -59.2(3) . . . . ?
C3_2 C1_2 C4_2 F6_2 179.9(2) . . . . ?
C2_2 C1_2 C4_2 F6_2 64.1(3) . . . . ?
O1_2 C1_2 C4_2 C5_2 179.4(3) . . . . ?
C3_2 C1_2 C4_2 C5_2 58.5(3) . . . . ?
C2_2 C1_2 C4_2 C5_2 -57.3(3) . . . . ?
F5_2 C4_2 C5_2 F7_2 -57.9(3) . . . . ?
F6_2 C4_2 C5_2 F7_2 57.5(3) . . . . ?
C1_2 C4_2 C5_2 F7_2 179.4(2) . . . . ?
F5_2 C4_2 C5_2 C10_2 -177.9(2) . . . . ?
F6_2 C4_2 C5_2 C10_2 -62.5(3) . . . . ?
C1_2 C4_2 C5_2 C10_2 59.4(3) . . . . ?
F5_2 C4_2 C5_2 C6_2 61.9(3) . . . . ?
F6_2 C4_2 C5_2 C6_2 177.3(2) . . . . ?
C1_2 C4_2 C5_2 C6_2 -60.8(3) . . . . ?
F7_2 C5_2 C6_2 F8_2 58.2(3) . . . . ?
C10_2 C5_2 C6_2 F8_2 178.0(3) . . . . ?
C4_2 C5_2 C6_2 F8_2 -62.1(3) . . . . ?
F7_2 C5_2 C6_2 F9_2 -57.7(3) . . . . ?
C10_2 C5_2 C6_2 F9_2 62.1(3) . . . . ?
C4_2 C5_2 C6_2 F9_2 -178.1(3) . . . . ?
F7_2 C5_2 C6_2 C7_2 -179.3(2) . . . . ?
C10_2 C5_2 C6_2 C7_2 -59.6(3) . . . . ?
C4_2 C5_2 C6_2 C7_2 60.3(3) . . . . ?
F8_2 C6_2 C7_2 F10_2 -57.5(3) . . . . ?
F9_2 C6_2 C7_2 F10_2 59.0(3) . . . . ?
C5_2 C6_2 C7_2 F10_2 179.8(3) . . . . ?
F8_2 C6_2 C7_2 C8_2 -177.8(2) . . . . ?
F9_2 C6_2 C7_2 C8_2 -61.2(3) . . . . ?
C5_2 C6_2 C7_2 C8_2 59.6(3) . . . . ?
F8_2 C6_2 C7_2 C3_2 63.0(3) . . . . ?
F9_2 C6_2 C7_2 C3_2 179.6(3) . . . . ?
C5_2 C6_2 C7_2 C3_2 -59.7(3) . . . . ?
F4_2 C3_2 C7_2 F10_2 58.4(3) . . . . ?
F3_2 C3_2 C7_2 F10_2 -56.7(3) . . . . ?
C1_2 C3_2 C7_2 F10_2 -179.5(3) . . . . ?
F4_2 C3_2 C7_2 C6_2 -62.8(3) . . . . ?
F3_2 C3_2 C7_2 C6_2 -177.9(3) . . . . ?
C1_2 C3_2 C7_2 C6_2 59.3(3) . . . . ?
F4_2 C3_2 C7_2 C8_2 177.6(2) . . . . ?
F3_2 C3_2 C7_2 C8_2 62.5(3) . . . . ?
C1_2 C3_2 C7_2 C8_2 -60.3(3) . . . . ?
F10_2 C7_2 C8_2 F11_2 56.9(3) . . . . ?
C6_2 C7_2 C8_2 F11_2 177.9(3) . . . . ?
C3_2 C7_2 C8_2 F11_2 -62.5(3) . . . . ?
F10_2 C7_2 C8_2 F12_2 -59.6(3) . . . . ?
C6_2 C7_2 C8_2 F12_2 61.4(3) . . . . ?
C3_2 C7_2 C8_2 F12_2 -179.0(2) . . . . ?
F10_2 C7_2 C8_2 C9_2 179.3(3) . . . . ?
C6_2 C7_2 C8_2 C9_2 -59.7(3) . . . . ?
C3_2 C7_2 C8_2 C9_2 59.9(3) . . . . ?
F11_2 C8_2 C9_2 F13_2 -58.8(4) . . . . ?
F12_2 C8_2 C9_2 F13_2 58.0(4) . . . . ?
C7_2 C8_2 C9_2 F13_2 179.0(3) . . . . ?
F11_2 C8_2 C9_2 C10_2 -178.4(3) . . . . ?
F12_2 C8_2 C9_2 C10_2 -61.7(3) . . . . ?
C7_2 C8_2 C9_2 C10_2 59.3(3) . . . . ?
F11_2 C8_2 C9_2 C2_2 62.1(3) . . . . ?
F12_2 C8_2 C9_2 C2_2 178.8(3) . . . . ?
C7_2 C8_2 C9_2 C2_2 -60.2(3) . . . . ?
F1_2 C2_2 C9_2 F13_2 59.3(3) . . . . ?
F2_2 C2_2 C9_2 F13_2 -57.2(3) . . . . ?
C1_2 C2_2 C9_2 F13_2 -179.1(2) . . . . ?
F1_2 C2_2 C9_2 C10_2 179.0(3) . . . . ?
F2_2 C2_2 C9_2 C10_2 62.5(3) . . . . ?
C1_2 C2_2 C9_2 C10_2 -59.4(3) . . . . ?
F1_2 C2_2 C9_2 C8_2 -61.4(3) . . . . ?
F2_2 C2_2 C9_2 C8_2 -178.0(3) . . . . ?
C1_2 C2_2 C9_2 C8_2 60.1(3) . . . . ?
F13_2 C9_2 C10_2 F14_2 58.3(3) . . . . ?
C8_2 C9_2 C10_2 F14_2 178.5(3) . . . . ?
C2_2 C9_2 C10_2 F14_2 -62.0(3) . . . . ?
F13_2 C9_2 C10_2 F15_2 -57.9(3) . . . . ?
C8_2 C9_2 C10_2 F15_2 62.4(3) . . . . ?
C2_2 C9_2 C10_2 F15_2 -178.2(3) . . . . ?
F13_2 C9_2 C10_2 C5_2 -179.5(3) . . . . ?
C8_2 C9_2 C10_2 C5_2 -59.3(3) . . . . ?
C2_2 C9_2 C10_2 C5_2 60.2(3) . . . . ?
F7_2 C5_2 C10_2 F14_2 -58.3(3) . . . . ?
C6_2 C5_2 C10_2 F14_2 -178.0(3) . . . . ?
C4_2 C5_2 C10_2 F14_2 62.4(3) . . . . ?
F7_2 C5_2 C10_2 F15_2 57.3(3) . . . . ?
C6_2 C5_2 C10_2 F15_2 -62.4(3) . . . . ?
C4_2 C5_2 C10_2 F15_2 178.0(2) . . . . ?
F7_2 C5_2 C10_2 C9_2 179.3(3) . . . . ?
C6_2 C5_2 C10_2 C9_2 59.6(3) . . . . ?
C4_2 C5_2 C10_2 C9_2 -60.1(3) . . . . ?
O1_1 Al1 O1_3 C1_3 39.9(4) . . . . ?
O1_2 Al1 O1_3 C1_3 -79.0(4) . . . . ?
O1_4 Al1 O1_3 C1_3 160.5(4) . . . . ?
Al1 O1_3 C1_3 C4_3 41.0(5) . . . . ?
Al1 O1_3 C1_3 C2_3 -80.5(4) . . . . ?
Al1 O1_3 C1_3 C3_3 160.8(3) . . . . ?
O1_3 C1_3 C2_3 F1_3 -56.4(3) . . . . ?
C4_3 C1_3 C2_3 F1_3 179.0(2) . . . . ?
C3_3 C1_3 C2_3 F1_3 63.9(3) . . . . ?
O1_3 C1_3 C2_3 F2_3 59.5(4) . . . . ?
C4_3 C1_3 C2_3 F2_3 -65.2(3) . . . . ?
C3_3 C1_3 C2_3 F2_3 179.7(3) . . . . ?
O1_3 C1_3 C2_3 C9_3 -178.0(3) . . . . ?
C4_3 C1_3 C2_3 C9_3 57.3(3) . . . . ?
C3_3 C1_3 C2_3 C9_3 -57.8(4) . . . . ?
O1_3 C1_3 C3_3 F3_3 57.6(3) . . . . ?
C4_3 C1_3 C3_3 F3_3 -179.1(3) . . . . ?
C2_3 C1_3 C3_3 F3_3 -63.8(3) . . . . ?
O1_3 C1_3 C3_3 F4_3 -59.3(3) . . . . ?
C4_3 C1_3 C3_3 F4_3 64.1(3) . . . . ?
C2_3 C1_3 C3_3 F4_3 179.4(3) . . . . ?
O1_3 C1_3 C3_3 C7_3 179.1(3) . . . . ?
C4_3 C1_3 C3_3 C7_3 -57.5(3) . . . . ?
C2_3 C1_3 C3_3 C7_3 57.7(3) . . . . ?
O1_3 C1_3 C4_3 F5_3 57.6(3) . . . . ?
C2_3 C1_3 C4_3 F5_3 -178.7(2) . . . . ?
C3_3 C1_3 C4_3 F5_3 -63.7(3) . . . . ?
O1_3 C1_3 C4_3 F6_3 -58.8(4) . . . . ?
C2_3 C1_3 C4_3 F6_3 64.9(3) . . . . ?
C3_3 C1_3 C4_3 F6_3 179.9(3) . . . . ?
O1_3 C1_3 C4_3 C5_3 179.5(3) . . . . ?
C2_3 C1_3 C4_3 C5_3 -56.7(3) . . . . ?
C3_3 C1_3 C4_3 C5_3 58.3(3) . . . . ?
F5_3 C4_3 C5_3 F7_3 -57.7(4) . . . . ?
F6_3 C4_3 C5_3 F7_3 57.4(4) . . . . ?
C1_3 C4_3 C5_3 F7_3 179.4(3) . . . . ?
F5_3 C4_3 C5_3 C10_3 -177.7(3) . . . . ?
F6_3 C4_3 C5_3 C10_3 -62.6(4) . . . . ?
C1_3 C4_3 C5_3 C10_3 59.4(4) . . . . ?
F5_3 C4_3 C5_3 C6_3 62.2(3) . . . . ?
F6_3 C4_3 C5_3 C6_3 177.4(3) . . . . ?
C1_3 C4_3 C5_3 C6_3 -60.6(3) . . . . ?
F7_3 C5_3 C6_3 F8_3 58.7(3) . . . . ?
C10_3 C5_3 C6_3 F8_3 178.2(3) . . . . ?
C4_3 C5_3 C6_3 F8_3 -61.6(3) . . . . ?
F7_3 C5_3 C6_3 F9_3 -57.8(3) . . . . ?
C10_3 C5_3 C6_3 F9_3 61.7(3) . . . . ?
C4_3 C5_3 C6_3 F9_3 -178.1(3) . . . . ?
F7_3 C5_3 C6_3 C7_3 -179.7(3) . . . . ?
C10_3 C5_3 C6_3 C7_3 -60.2(3) . . . . ?
C4_3 C5_3 C6_3 C7_3 60.0(3) . . . . ?
F8_3 C6_3 C7_3 F10_3 -58.6(3) . . . . ?
F9_3 C6_3 C7_3 F10_3 58.8(4) . . . . ?
C5_3 C6_3 C7_3 F10_3 179.9(3) . . . . ?
F8_3 C6_3 C7_3 C3_3 61.8(3) . . . . ?
F9_3 C6_3 C7_3 C3_3 179.1(3) . . . . ?
C5_3 C6_3 C7_3 C3_3 -59.7(3) . . . . ?
F8_3 C6_3 C7_3 C8_3 -178.2(3) . . . . ?
F9_3 C6_3 C7_3 C8_3 -60.9(3) . . . . ?
C5_3 C6_3 C7_3 C8_3 60.3(3) . . . . ?
F3_3 C3_3 C7_3 F10_3 -58.3(3) . . . . ?
F4_3 C3_3 C7_3 F10_3 57.8(3) . . . . ?
C1_3 C3_3 C7_3 F10_3 179.7(3) . . . . ?
F3_3 C3_3 C7_3 C6_3 -178.4(3) . . . . ?
F4_3 C3_3 C7_3 C6_3 -62.3(3) . . . . ?
C1_3 C3_3 C7_3 C6_3 59.7(3) . . . . ?
F3_3 C3_3 C7_3 C8_3 61.7(3) . . . . ?
F4_3 C3_3 C7_3 C8_3 177.9(3) . . . . ?
C1_3 C3_3 C7_3 C8_3 -60.2(3) . . . . ?
F10_3 C7_3 C8_3 F11_3 58.3(3) . . . . ?
C6_3 C7_3 C8_3 F11_3 177.9(3) . . . . ?
C3_3 C7_3 C8_3 F11_3 -62.0(3) . . . . ?
F10_3 C7_3 C8_3 F12_3 -58.7(4) . . . . ?
C6_3 C7_3 C8_3 F12_3 60.9(4) . . . . ?
C3_3 C7_3 C8_3 F12_3 -179.0(3) . . . . ?
F10_3 C7_3 C8_3 C9_3 -179.8(3) . . . . ?
C6_3 C7_3 C8_3 C9_3 -60.3(3) . . . . ?
C3_3 C7_3 C8_3 C9_3 59.9(3) . . . . ?
F11_3 C8_3 C9_3 F13_3 -58.0(4) . . . . ?
F12_3 C8_3 C9_3 F13_3 59.1(4) . . . . ?
C7_3 C8_3 C9_3 F13_3 -179.8(3) . . . . ?
F11_3 C8_3 C9_3 C10_3 -178.0(3) . . . . ?
F12_3 C8_3 C9_3 C10_3 -60.9(3) . . . . ?
C7_3 C8_3 C9_3 C10_3 60.2(4) . . . . ?
F11_3 C8_3 C9_3 C2_3 62.1(4) . . . . ?
F12_3 C8_3 C9_3 C2_3 179.3(3) . . . . ?
C7_3 C8_3 C9_3 C2_3 -59.7(4) . . . . ?
F1_3 C2_3 C9_3 F13_3 58.3(4) . . . . ?
F2_3 C2_3 C9_3 F13_3 -57.0(4) . . . . ?
C1_3 C2_3 C9_3 F13_3 -179.8(3) . . . . ?
F1_3 C2_3 C9_3 C10_3 178.0(3) . . . . ?
F2_3 C2_3 C9_3 C10_3 62.8(4) . . . . ?
C1_3 C2_3 C9_3 C10_3 -60.1(4) . . . . ?
F1_3 C2_3 C9_3 C8_3 -61.8(3) . . . . ?
F2_3 C2_3 C9_3 C8_3 -177.0(3) . . . . ?
C1_3 C2_3 C9_3 C8_3 60.1(4) . . . . ?
F13_3 C9_3 C10_3 F14_3 58.8(4) . . . . ?
C8_3 C9_3 C10_3 F14_3 178.8(3) . . . . ?
C2_3 C9_3 C10_3 F14_3 -61.2(4) . . . . ?
F13_3 C9_3 C10_3 F15_3 -57.9(4) . . . . ?
C8_3 C9_3 C10_3 F15_3 62.1(4) . . . . ?
C2_3 C9_3 C10_3 F15_3 -177.8(3) . . . . ?
F13_3 C9_3 C10_3 C5_3 179.9(3) . . . . ?
C8_3 C9_3 C10_3 C5_3 -60.1(3) . . . . ?
C2_3 C9_3 C10_3 C5_3 60.0(4) . . . . ?
F7_3 C5_3 C10_3 F14_3 -58.9(4) . . . . ?
C4_3 C5_3 C10_3 F14_3 61.6(4) . . . . ?
C6_3 C5_3 C10_3 F14_3 -178.6(3) . . . . ?
F7_3 C5_3 C10_3 F15_3 57.2(4) . . . . ?
C4_3 C5_3 C10_3 F15_3 177.7(3) . . . . ?
C6_3 C5_3 C10_3 F15_3 -62.5(4) . . . . ?
F7_3 C5_3 C10_3 C9_3 179.5(3) . . . . ?
C4_3 C5_3 C10_3 C9_3 -59.9(4) . . . . ?
C6_3 C5_3 C10_3 C9_3 59.9(3) . . . . ?
O1_1 Al1 O1_4 C1_4 79.4(4) . . . . ?
O1_2 Al1 O1_4 C1_4 -161.4(4) . . . . ?
O1_3 Al1 O1_4 C1_4 -39.8(4) . . . . ?
Al1 O1_4 C1_4 C2_4 -159.9(3) . . . . ?
Al1 O1_4 C1_4 C4_4 -40.7(5) . . . . ?
Al1 O1_4 C1_4 C3_4 81.3(5) . . . . ?
O1_4 C1_4 C2_4 F2_4 59.0(3) . . . . ?
C4_4 C1_4 C2_4 F2_4 -64.1(3) . . . . ?
C3_4 C1_4 C2_4 F2_4 -179.2(2) . . . . ?
O1_4 C1_4 C2_4 F1_4 -58.0(3) . . . . ?
C4_4 C1_4 C2_4 F1_4 178.9(2) . . . . ?
C3_4 C1_4 C2_4 F1_4 63.8(3) . . . . ?
O1_4 C1_4 C2_4 C9_4 -178.9(3) . . . . ?
C4_4 C1_4 C2_4 C9_4 58.0(3) . . . . ?
C3_4 C1_4 C2_4 C9_4 -57.1(3) . . . . ?
O1_4 C1_4 C3_4 F4_4 -61.0(3) . . . . ?
C2_4 C1_4 C3_4 F4_4 179.5(2) . . . . ?
C4_4 C1_4 C3_4 F4_4 64.5(3) . . . . ?
O1_4 C1_4 C3_4 F3_4 55.6(3) . . . . ?
C2_4 C1_4 C3_4 F3_4 -63.9(3) . . . . ?
C4_4 C1_4 C3_4 F3_4 -178.9(2) . . . . ?
O1_4 C1_4 C3_4 C7_4 176.7(3) . . . . ?
C2_4 C1_4 C3_4 C7_4 57.2(3) . . . . ?
C4_4 C1_4 C3_4 C7_4 -57.9(3) . . . . ?
O1_4 C1_4 C4_4 F6_4 -56.1(3) . . . . ?
C2_4 C1_4 C4_4 F6_4 63.9(3) . . . . ?
C3_4 C1_4 C4_4 F6_4 179.2(2) . . . . ?
O1_4 C1_4 C4_4 F5_4 60.3(3) . . . . ?
C2_4 C1_4 C4_4 F5_4 -179.7(2) . . . . ?
C3_4 C1_4 C4_4 F5_4 -64.4(3) . . . . ?
O1_4 C1_4 C4_4 C5_4 -178.4(3) . . . . ?
C2_4 C1_4 C4_4 C5_4 -58.4(3) . . . . ?
C3_4 C1_4 C4_4 C5_4 56.9(3) . . . . ?
F6_4 C4_4 C5_4 F7_4 57.2(4) . . . . ?
F5_4 C4_4 C5_4 F7_4 -58.3(4) . . . . ?
C1_4 C4_4 C5_4 F7_4 -179.9(3) . . . . ?
F6_4 C4_4 C5_4 C6_4 177.6(3) . . . . ?
F5_4 C4_4 C5_4 C6_4 62.0(3) . . . . ?
C1_4 C4_4 C5_4 C6_4 -59.5(3) . . . . ?
F6_4 C4_4 C5_4 C10_4 -62.2(3) . . . . ?
F5_4 C4_4 C5_4 C10_4 -177.7(3) . . . . ?
C1_4 C4_4 C5_4 C10_4 60.7(3) . . . . ?
F7_4 C5_4 C6_4 F9_4 -58.0(4) . . . . ?
C10_4 C5_4 C6_4 F9_4 61.5(4) . . . . ?
C4_4 C5_4 C6_4 F9_4 -178.4(3) . . . . ?
F7_4 C5_4 C6_4 F8_4 58.5(3) . . . . ?
C10_4 C5_4 C6_4 F8_4 178.1(3) . . . . ?
C4_4 C5_4 C6_4 F8_4 -61.9(3) . . . . ?
F7_4 C5_4 C6_4 C7_4 180.0(3) . . . . ?
C10_4 C5_4 C6_4 C7_4 -60.5(3) . . . . ?
C4_4 C5_4 C6_4 C7_4 59.6(3) . . . . ?
F9_4 C6_4 C7_4 F10_4 58.1(4) . . . . ?
F8_4 C6_4 C7_4 F10_4 -58.6(4) . . . . ?
C5_4 C6_4 C7_4 F10_4 -179.8(3) . . . . ?
F9_4 C6_4 C7_4 C8_4 -61.6(4) . . . . ?
F8_4 C6_4 C7_4 C8_4 -178.4(3) . . . . ?
C5_4 C6_4 C7_4 C8_4 60.4(3) . . . . ?
F9_4 C6_4 C7_4 C3_4 178.3(3) . . . . ?
F8_4 C6_4 C7_4 C3_4 61.6(3) . . . . ?
C5_4 C6_4 C7_4 C3_4 -59.7(3) . . . . ?
F4_4 C3_4 C7_4 F10_4 58.2(4) . . . . ?
F3_4 C3_4 C7_4 F10_4 -57.4(3) . . . . ?
C1_4 C3_4 C7_4 F10_4 -179.2(3) . . . . ?
F4_4 C3_4 C7_4 C8_4 178.0(3) . . . . ?
F3_4 C3_4 C7_4 C8_4 62.4(3) . . . . ?
C1_4 C3_4 C7_4 C8_4 -59.4(4) . . . . ?
F4_4 C3_4 C7_4 C6_4 -62.3(3) . . . . ?
F3_4 C3_4 C7_4 C6_4 -177.8(3) . . . . ?
C1_4 C3_4 C7_4 C6_4 60.3(3) . . . . ?
F10_4 C7_4 C8_4 F12_4 -58.5(4) . . . . ?
C6_4 C7_4 C8_4 F12_4 61.7(4) . . . . ?
C3_4 C7_4 C8_4 F12_4 -178.5(3) . . . . ?
F10_4 C7_4 C8_4 F11_4 57.5(3) . . . . ?
C6_4 C7_4 C8_4 F11_4 177.7(3) . . . . ?
C3_4 C7_4 C8_4 F11_4 -62.4(4) . . . . ?
F10_4 C7_4 C8_4 C9_4 179.2(3) . . . . ?
C6_4 C7_4 C8_4 C9_4 -60.6(3) . . . . ?
C3_4 C7_4 C8_4 C9_4 59.3(4) . . . . ?
F12_4 C8_4 C9_4 F13_4 58.1(4) . . . . ?
F11_4 C8_4 C9_4 F13_4 -59.0(3) . . . . ?
C7_4 C8_4 C9_4 F13_4 179.8(3) . . . . ?
F12_4 C8_4 C9_4 C10_4 -61.1(3) . . . . ?
F11_4 C8_4 C9_4 C10_4 -178.2(3) . . . . ?
C7_4 C8_4 C9_4 C10_4 60.6(3) . . . . ?
F12_4 C8_4 C9_4 C2_4 178.5(3) . . . . ?
F11_4 C8_4 C9_4 C2_4 61.4(3) . . . . ?
C7_4 C8_4 C9_4 C2_4 -59.8(3) . . . . ?
F2_4 C2_4 C9_4 F13_4 -56.8(4) . . . . ?
F1_4 C2_4 C9_4 F13_4 59.3(3) . . . . ?
C1_4 C2_4 C9_4 F13_4 -179.5(3) . . . . ?
F2_4 C2_4 C9_4 C8_4 -177.3(3) . . . . ?
F1_4 C2_4 C9_4 C8_4 -61.1(3) . . . . ?
C1_4 C2_4 C9_4 C8_4 60.0(3) . . . . ?
F2_4 C2_4 C9_4 C10_4 62.5(3) . . . . ?
F1_4 C2_4 C9_4 C10_4 178.7(3) . . . . ?
C1_4 C2_4 C9_4 C10_4 -60.2(3) . . . . ?
F7_4 C5_4 C10_4 F14_4 -58.2(4) . . . . ?
C6_4 C5_4 C10_4 F14_4 -177.9(3) . . . . ?
C4_4 C5_4 C10_4 F14_4 61.3(3) . . . . ?
F7_4 C5_4 C10_4 F15_4 58.7(4) . . . . ?
C6_4 C5_4 C10_4 F15_4 -60.9(4) . . . . ?
C4_4 C5_4 C10_4 F15_4 178.2(3) . . . . ?
F7_4 C5_4 C10_4 C9_4 -179.8(3) . . . . ?
C6_4 C5_4 C10_4 C9_4 60.5(4) . . . . ?
C4_4 C5_4 C10_4 C9_4 -60.3(4) . . . . ?
F13_4 C9_4 C10_4 F14_4 58.3(3) . . . . ?
C8_4 C9_4 C10_4 F14_4 177.8(3) . . . . ?
C2_4 C9_4 C10_4 F14_4 -61.3(3) . . . . ?
F13_4 C9_4 C10_4 F15_4 -58.2(4) . . . . ?
C8_4 C9_4 C10_4 F15_4 61.3(3) . . . . ?
C2_4 C9_4 C10_4 F15_4 -177.9(3) . . . . ?
F13_4 C9_4 C10_4 C5_4 179.9(3) . . . . ?
C8_4 C9_4 C10_4 C5_4 -60.6(3) . . . . ?
C2_4 C9_4 C10_4 C5_4 60.3(4) . . . . ?
C3_5 O1_5 C1_5 C2_5 87.0(4) . . . . ?
O1_7 O1_5 C1_5 C2_5 -134.3(5) . . . . ?
O1_6 O1_5 C1_5 C2_5 -133.0(4) . . . . ?
C1_5 O1_5 C3_5 C4_5 176.9(4) . . . . ?
O1_7 O1_5 C3_5 C4_5 42.5(7) . . . . ?
O1_6 O1_5 C3_5 C4_5 40.3(5) . . . . ?
C3_6 O1_6 C1_6 C2_6 171.8(12) . . . . ?
O1_5 O1_6 C1_6 C2_6 -47.8(13) . . . . ?
C1_6 O1_6 C3_6 C4_6 -176.8(9) . . . . ?
O1_5 O1_6 C3_6 C4_6 44.5(11) . . . . ?
C3_7 O1_7 C1_7 C2_7 178(2) . . . . ?
O1_5 O1_7 C1_7 C2_7 -44(3) . . . . ?
C1_7 O1_7 C3_7 C4_7 -173(2) . . . . ?
O1_5 O1_7 C3_7 C4_7 49(3) . . . . ?

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_IKmjs_AM11_a
_database_code_depnum_ccdc_archive 'CCDC 2224627'
loop_
_audit_author_name
_audit_author_address
'Burkhard Butschke'
;Albert Ludwigs Universitaet Freiburg
Germany
;
_audit_update_record             
;
2022-12-06 deposited with the CCDC.	2023-03-10 downloaded from the CCDC.
;
_audit_creation_method           
;FinalCif V113 by Daniel Kratzert, Freiburg 2022,
https://dkratzert.de/finalcif.html
;
_shelx_SHELXL_version_number     2018/3
_chemical_name_systematic        ?
_chemical_name_common            ?
_chemical_formula_sum            'C90 H20 Ag3 Al F100 O6'
_chemical_formula_moiety         'C40 Al F60 O4, C20 Ag3 F30 O2, 5(C6 H4 F2)'
_chemical_formula_weight         3447.66
_chemical_melting_point          ?
_chemical_absolute_configuration ad
_space_group_crystal_system      orthorhombic
_space_group_IT_number           19
_space_group_name_H-M_alt        'P 21 21 21'
_space_group_name_Hall           'P 2ac 2ab'
_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;

loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, -y, z+1/2'
'-x, y+1/2, -z+1/2'
'x+1/2, -y+1/2, -z'

_cell_length_a                   14.9498(7)
_cell_length_b                   18.4428(12)
_cell_length_c                   36.6960(19)
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_volume                     10117.7(10)
_cell_formula_units_Z            4
_cell_measurement_temperature    100(2)
_cell_measurement_reflns_used    9971
_cell_measurement_theta_min      2.28
_cell_measurement_theta_max      28.235
_exptl_crystal_description       needle
_exptl_crystal_colour            colourless
_exptl_crystal_recrystallization_method 
'Crystals were obtained at room temperature by slow diffusion of pentane into asolution of the compound dissolved in 1,2-difluorobenzene by the aid oflayering.'
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_density_diffrn    2.263
_exptl_crystal_F_000             6648
_exptl_crystal_size_max          0.300
_exptl_crystal_size_mid          0.150
_exptl_crystal_size_min          0.070
_vrf_PLAT090_IKmjs_AM11_a        
;PROBLEM: Poor Data / Parameter Ratio (Zmax > 18) ........       3.83 Note  
RESPONSE: Due to the extensive disorder model as well as the non-centrosymmetric
spacegroup, a high number of parameters was needed. However, restraints have
been applied to generate a meaningful model.
;
_exptl_absorpt_coefficient_mu    0.826
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_correction_T_min  0.6959
_exptl_absorpt_correction_T_max  0.7458
_exptl_absorpt_process_details   
;SADABS-2016/2 - Bruker AXS area detector scaling and absorption correction:
Krause, L., Herbst-Irmer, R., Sheldrick G.M. & Stalke D., J. Appl. Cryst. 48
(2015) 3-10
;
_exptl_absorpt_special_details   ?
_shelx_estimated_absorpt_T_min   ?
_shelx_estimated_absorpt_T_max   ?
_exptl_transmission_factor_min   ?
_exptl_transmission_factor_max   ?
_exptl_special_details           ?
_diffrn_ambient_temperature      100(2)
_diffrn_ambient_environment      N~2~
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_monochromator  'mirror optics'
_olex2_diffrn_ambient_temperature_device 'Oxford Cryostream 800'
_diffrn_measurement_ambient_temperature_device_make ?
_diffrn_radiation_probe          x-ray
_diffrn_source                   'microfocus sealed X-ray tube'
_diffrn_source_type              'Incoatec I\ms'
_diffrn_source_voltage           50.0
_diffrn_source_current           0.6
_diffrn_detector                 CCD
_diffrn_detector_type            'Bruker APEXII'
_diffrn_detector_area_resol_mean 8.3
_diffrn_measurement_device       'three-circle diffractometer'
_diffrn_measurement_device_type  'Bruker APEX2 QUAZAR'
_diffrn_measurement_method       'ω and φ scans'
_diffrn_measurement_specimen_support 'MiTeGen micromount'
_diffrn_reflns_number            91049
_diffrn_reflns_av_unetI/netI     0.0375
_diffrn_reflns_av_R_equivalents  0.0293
_diffrn_reflns_theta_min         1.110
_diffrn_reflns_theta_max         28.711
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_limit_h_min       -20
_diffrn_reflns_limit_h_max       18
_diffrn_reflns_limit_k_min       -23
_diffrn_reflns_limit_k_max       24
_diffrn_reflns_limit_l_min       -49
_diffrn_reflns_limit_l_max       46
_diffrn_measured_fraction_theta_max 0.979
_diffrn_measured_fraction_theta_full 1.000
_diffrn_reflns_Laue_measured_fraction_max 0.979
_diffrn_reflns_Laue_measured_fraction_full 1.000
_diffrn_reflns_point_group_measured_fraction_max 0.962
_diffrn_reflns_point_group_measured_fraction_full 1.000
_reflns_number_total             25175
_reflns_number_gt                22252
_reflns_threshold_expression     'I > 2σ(I)'
_reflns_Friedel_coverage         0.820
_reflns_Friedel_fraction_max     0.943
_reflns_Friedel_fraction_full    1.000
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences. Completness statistics refer to single and
 composite reflections containing twin component 1 only.
;
_computing_data_collection       
'Bruker BIS 2018.9.0.3/05-Dec-2018 && APEX2_2014.11-0'
_computing_cell_refinement       'SAINT V8.40B'
_computing_data_reduction        'SAINT V8.40B'
_computing_structure_solution    'SHELXT 2018/2 (Sheldrick, 2018)'
_computing_structure_refinement  'SHELXL-2018/3 (Sheldrick, 2018)'
_computing_molecular_graphics    ?
_computing_publication_material  ?
_refine_special_details          
;
 Refined as a 2-component inversion twin.
;
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0244P)²+16.4196P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   ?
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    constr
_refine_ls_number_reflns         25175
_refine_ls_number_parameters     3609
_refine_ls_number_restraints     68351
_refine_ls_R_factor_all          0.0499
_refine_ls_R_factor_gt           0.0402
_refine_ls_wR_factor_ref         0.0822
_refine_ls_wR_factor_gt          0.0782
_refine_ls_goodness_of_fit_ref   1.078
_refine_ls_restrained_S_all      1.202
_refine_ls_shift/su_max          0.004
_refine_ls_shift/su_mean         0.000
_refine_diff_density_max         0.706
_refine_diff_density_min         -0.619
_refine_diff_density_rms         0.081
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       .
_refine_ls_abs_structure_Flack   0.447(19)
_refine_ls_abs_structure_details 
;
 Refined as an inversion twin.
;

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Al Al 0.0645 0.0514 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1A Ag 0.07652(3) 0.49548(4) 0.41471(2) 0.01883(17) Uani 0.961(3) 1 d . U P A
6
Ag1B Ag 0.0832(9) 0.5151(9) 0.4013(6) 0.0213(16) Uani 0.039(3) 1 d . U P A 7
Ag2A Ag -0.02791(4) 0.60498(2) 0.35609(2) 0.02135(13) Uani 0.9646(15) 1 d . U P
A 8
Ag2B Ag -0.0823(12) 0.6050(6) 0.3487(3) 0.0237(16) Uani 0.0354(15) 1 d . U P A
9
Ag3A Ag -0.1483(2) 0.50072(16) 0.41368(16) 0.0216(4) Uani 0.90(3) 1 d . U P A
10
Ag3B Ag -0.1555(16) 0.5049(13) 0.4064(9) 0.0221(15) Uani 0.10(3) 1 d . U P A 11
Al1 Al 0.46911(12) 0.14582(7) 0.37995(4) 0.0157(3) Uani 1 1 d D . . . .
O1_1 O -0.0348(3) 0.48133(16) 0.36865(8) 0.0188(7) Uani 1 1 d D U . . .
C1_1 C -0.0358(4) 0.4272(2) 0.34358(12) 0.0172(9) Uani 1 1 d D U . . .
C2_1 C 0.0482(4) 0.4288(3) 0.31874(13) 0.0215(11) Uani 1 1 d D U . . .
F1_1 F 0.0530(2) 0.49379(19) 0.30121(8) 0.0307(8) Uani 1 1 d D U . . .
F2_1 F 0.1232(2) 0.4256(2) 0.33945(10) 0.0298(8) Uani 1 1 d D U . . .
C3_1 C -0.1191(4) 0.4308(3) 0.31817(14) 0.0213(11) Uani 1 1 d D U . . .
F3_1 F -0.1215(2) 0.49443(19) 0.30069(8) 0.0305(8) Uani 1 1 d D U . . .
F4_1 F -0.1945(2) 0.4278(2) 0.33813(9) 0.0299(8) Uani 1 1 d D U . . .
C4_1 C -0.0370(4) 0.3514(2) 0.36235(11) 0.0185(9) Uani 1 1 d D U . . .
F5_1 F -0.1091(2) 0.34547(18) 0.38424(8) 0.0247(7) Uani 1 1 d D U . . .
F6_1 F 0.0344(3) 0.34466(16) 0.38481(7) 0.0251(7) Uani 1 1 d D U . . .
C5_1 C -0.0361(5) 0.2884(2) 0.33447(13) 0.0240(11) Uani 1 1 d D U . . .
F7_1 F -0.0380(3) 0.22344(15) 0.35243(9) 0.0400(9) Uani 1 1 d D U . . .
C6_1 C -0.1206(4) 0.2944(3) 0.31036(15) 0.0280(13) Uani 1 1 d D U . . .
F8_1 F -0.1947(3) 0.2882(2) 0.33038(10) 0.0399(10) Uani 1 1 d D U . . .
F9_1 F -0.1227(3) 0.2396(2) 0.28599(10) 0.0439(11) Uani 1 1 d D U . . .
C7_1 C -0.1190(4) 0.3680(3) 0.28971(14) 0.0255(12) Uani 1 1 d D U . . .
F10_1 F -0.1926(3) 0.3733(2) 0.26818(10) 0.0378(10) Uani 1 1 d D U . . .
C8_1 C -0.0335(5) 0.3727(3) 0.26615(13) 0.0266(11) Uani 1 1 d D U . . .
F11_1 F -0.0335(3) 0.43544(16) 0.24746(8) 0.0341(8) Uani 1 1 d D U . . .
F12_1 F -0.0350(3) 0.31968(17) 0.24078(8) 0.0366(8) Uani 1 1 d D U . . .
C9_1 C 0.0492(4) 0.3668(3) 0.29047(13) 0.0239(12) Uani 1 1 d D U . . .
F13_1 F 0.1238(3) 0.3711(2) 0.26925(10) 0.0402(10) Uani 1 1 d D U . . .
C10_1 C 0.0482(4) 0.2935(3) 0.31104(14) 0.0286(14) Uani 1 1 d D U . . .
F14_1 F 0.1223(3) 0.2867(2) 0.33153(10) 0.0389(10) Uani 1 1 d D U . . .
F15_1 F 0.0513(3) 0.23822(19) 0.28697(9) 0.0431(11) Uani 1 1 d D U . . .
O1_2 O -0.0340(3) 0.58443(16) 0.41997(8) 0.0185(7) Uani 1 1 d D U . . .
C1_2 C -0.0331(4) 0.6365(2) 0.44598(12) 0.0165(9) Uani 1 1 d D U . . .
C2_2 C 0.0505(4) 0.6870(3) 0.44220(13) 0.0188(11) Uani 1 1 d D U . . .
F1_2 F 0.1258(2) 0.64742(19) 0.44396(9) 0.0257(8) Uani 1 1 d D U . . .
F2_2 F 0.0513(2) 0.71758(16) 0.40867(8) 0.0250(8) Uani 1 1 d D U . . .
C3_2 C -0.0299(4) 0.6038(2) 0.48547(11) 0.0200(9) Uani 1 1 d D U . . .
F3_2 F 0.0425(3) 0.56016(16) 0.48901(8) 0.0252(7) Uani 1 1 d D U . . .
F4_2 F -0.1012(2) 0.55956(17) 0.49037(9) 0.0265(7) Uani 1 1 d D U . . .
C4_2 C -0.1173(4) 0.6858(3) 0.44394(14) 0.0215(11) Uani 1 1 d D U . . .
F5_2 F -0.1922(2) 0.64532(19) 0.44753(10) 0.0290(8) Uani 1 1 d D U . . .
F6_2 F -0.1234(2) 0.71668(17) 0.41061(9) 0.0269(7) Uani 1 1 d D U . . .
C5_2 C -0.1164(4) 0.7461(3) 0.47345(16) 0.0278(13) Uani 1 1 d D U . . .
F7_2 F -0.1913(3) 0.7874(2) 0.47041(11) 0.0406(10) Uani 1 1 d D U . . .
C6_2 C -0.1135(5) 0.7098(3) 0.51160(15) 0.0313(13) Uani 1 1 d D U . . .
F8_2 F -0.1871(3) 0.6691(2) 0.51687(10) 0.0383(9) Uani 1 1 d D U . . .
F9_2 F -0.1143(3) 0.7607(2) 0.53780(10) 0.0466(11) Uani 1 1 d D U . . .
C7_2 C -0.0288(5) 0.6630(3) 0.51481(12) 0.0247(11) Uani 1 1 d D U . . .
F10_2 F -0.0257(3) 0.63203(17) 0.54872(8) 0.0372(8) Uani 1 1 d D U . . .
C8_2 C 0.0553(4) 0.7108(3) 0.50969(14) 0.0282(13) Uani 1 1 d D U . . .
F11_2 F 0.1294(3) 0.6709(2) 0.51327(10) 0.0358(9) Uani 1 1 d D U . . .
F12_2 F 0.0589(3) 0.7621(2) 0.53586(10) 0.0434(12) Uani 1 1 d D U . . .
C9_2 C 0.0525(4) 0.7473(3) 0.47157(15) 0.0258(13) Uani 1 1 d D U . . .
F13_2 F 0.1263(3) 0.7893(2) 0.46720(11) 0.0360(9) Uani 1 1 d D U . . .
C10_2 C -0.0326(5) 0.7941(3) 0.46826(13) 0.0278(11) Uani 1 1 d D U . . .
F14_2 F -0.0351(3) 0.82704(15) 0.43555(8) 0.0349(8) Uani 1 1 d D U . . .
F15_2 F -0.0320(4) 0.84765(17) 0.49309(9) 0.0433(9) Uani 1 1 d D U . . .
C1_10 C 0.2177(8) 0.6178(5) 0.3364(3) 0.043(2) Uani 0.837(10) 1 d D U P A 1
C2_10 C 0.2221(10) 0.6913(5) 0.3304(3) 0.037(2) Uani 0.837(10) 1 d D U P A 1
C3_10 C 0.2503(11) 0.7164(6) 0.2968(3) 0.040(2) Uani 0.837(10) 1 d D U P A 1
H3_10 H 0.252679 0.766919 0.291937 0.047 Uiso 0.837(10) 1 calc R U P A 1
C4_10 C 0.2750(10) 0.6669(5) 0.2704(3) 0.042(3) Uani 0.837(10) 1 d D U P A 1
H4_10 H 0.294276 0.683441 0.247143 0.050 Uiso 0.837(10) 1 calc R U P A 1
C5_10 C 0.2716(12) 0.5935(6) 0.2777(3) 0.045(2) Uani 0.837(10) 1 d D U P A 1
H5_10 H 0.288880 0.559667 0.259491 0.054 Uiso 0.837(10) 1 calc R U P A 1
C6_10 C 0.2436(9) 0.5693(5) 0.3110(3) 0.045(2) Uani 0.837(10) 1 d D U P A 1
H6_10 H 0.242373 0.518888 0.316204 0.054 Uiso 0.837(10) 1 calc R U P A 1
F1_10 F 0.1841(8) 0.5967(6) 0.3698(3) 0.069(3) Uani 0.837(10) 1 d D U P A 1
F2_10 F 0.1984(4) 0.7384(3) 0.35590(15) 0.0596(18) Uani 0.837(10) 1 d D U P A 1
C1_20 C 0.231(4) 0.6275(19) 0.3387(11) 0.044(6) Uani 0.163(10) 1 d D U P A 2
C2_20 C 0.254(4) 0.5705(17) 0.3164(11) 0.045(6) Uani 0.163(10) 1 d D U P A 2
C3_20 C 0.272(6) 0.582(3) 0.2799(11) 0.043(6) Uani 0.163(10) 1 d D U P A 2
H3_20 H 0.289085 0.542223 0.264688 0.051 Uiso 0.163(10) 1 calc R U P A 2
C4_20 C 0.266(6) 0.651(3) 0.2661(12) 0.041(6) Uani 0.163(10) 1 d D U P A 2
H4_20 H 0.274708 0.658986 0.240842 0.049 Uiso 0.163(10) 1 calc R U P A 2
C5_20 C 0.246(6) 0.708(2) 0.2887(13) 0.038(6) Uani 0.163(10) 1 d D U P A 2
H5_20 H 0.242592 0.755616 0.278921 0.046 Uiso 0.163(10) 1 calc R U P A 2
C6_20 C 0.230(6) 0.697(2) 0.3255(13) 0.039(6) Uani 0.163(10) 1 d D U P A 2
H6_20 H 0.219415 0.737197 0.341311 0.046 Uiso 0.163(10) 1 calc R U P A 2
F1_20 F 0.212(4) 0.612(2) 0.3738(10) 0.049(10) Uani 0.163(10) 1 d D U P A 2
F2_20 F 0.258(2) 0.5015(14) 0.3273(7) 0.061(8) Uani 0.163(10) 1 d D U P A 2
C1_11 C -0.3562(11) 0.5969(11) 0.3293(5) 0.066(4) Uani 0.707(12) 1 d D U P A 1
C2_11 C -0.3105(11) 0.6279(9) 0.3581(4) 0.054(3) Uani 0.707(12) 1 d D U P A 1
C3_11 C -0.3493(11) 0.6809(9) 0.3791(4) 0.059(3) Uani 0.707(12) 1 d D U P A 1
H3_11 H -0.316279 0.702595 0.398367 0.070 Uiso 0.707(12) 1 calc R U P A 1
C4_11 C -0.4369(10) 0.7029(10) 0.3724(4) 0.066(4) Uani 0.707(12) 1 d D U P A 1
H4_11 H -0.464495 0.739367 0.386859 0.079 Uiso 0.707(12) 1 calc R U P A 1
C5_11 C -0.4828(11) 0.6697(9) 0.3440(4) 0.064(4) Uani 0.707(12) 1 d D U P A 1
H5_11 H -0.542844 0.683588 0.339103 0.077 Uiso 0.707(12) 1 calc R U P A 1
C6_11 C -0.4431(11) 0.6168(10) 0.3226(4) 0.068(4) Uani 0.707(12) 1 d D U P A 1
H6_11 H -0.475792 0.594520 0.303477 0.081 Uiso 0.707(12) 1 calc R U P A 1
F1_11 F -0.3091(6) 0.5497(4) 0.3079(3) 0.090(3) Uani 0.707(12) 1 d D U P A 1
F2_11 F -0.2265(11) 0.6041(15) 0.3661(6) 0.069(5) Uani 0.707(12) 1 d D U P A 1
C1_19 C -0.358(2) 0.669(2) 0.3712(9) 0.065(6) Uani 0.293(12) 1 d D U P A 2
C2_19 C -0.306(2) 0.624(2) 0.3505(10) 0.061(5) Uani 0.293(12) 1 d D U P A 2
C3_19 C -0.344(2) 0.593(3) 0.3208(10) 0.058(5) Uani 0.293(12) 1 d D U P A 2
H3_19 H -0.309474 0.560174 0.306597 0.069 Uiso 0.293(12) 1 calc R U P A 2
C4_19 C -0.430(2) 0.606(2) 0.3106(9) 0.051(5) Uani 0.293(12) 1 d D U P A 2
H4_19 H -0.452565 0.586167 0.288536 0.061 Uiso 0.293(12) 1 calc R U P A 2
C5_19 C -0.485(2) 0.649(2) 0.3325(9) 0.060(6) Uani 0.293(12) 1 d D U P A 2
H5_19 H -0.546787 0.655029 0.327040 0.073 Uiso 0.293(12) 1 calc R U P A 2
C6_19 C -0.447(2) 0.682(2) 0.3624(10) 0.062(6) Uani 0.293(12) 1 d D U P A 2
H6_19 H -0.481831 0.714283 0.376983 0.074 Uiso 0.293(12) 1 calc R U P A 2
F1_19 F -0.3187(14) 0.7028(12) 0.3989(6) 0.087(7) Uani 0.293(12) 1 d D U P A 2
F2_19 F -0.219(3) 0.611(4) 0.3589(16) 0.059(7) Uani 0.293(12) 1 d D U P A 2
C1_8 C -0.1505(8) 0.6711(6) 0.2780(3) 0.043(2) Uani 0.840(9) 1 d D U P A 5
C2_8 C -0.0659(9) 0.6423(8) 0.2751(3) 0.0331(17) Uani 0.840(9) 1 d D U P A 5
C3_8 C 0.0022(8) 0.6646(9) 0.2979(4) 0.0312(18) Uani 0.840(9) 1 d D U P A 5
H3_8 H 0.059994 0.643473 0.295859 0.037 Uiso 0.840(9) 1 calc R U P A 5
C4_8 C -0.0139(8) 0.7182(6) 0.3239(4) 0.0346(19) Uani 0.840(9) 1 d D U P A 5
H4_8 H 0.032706 0.734584 0.339437 0.042 Uiso 0.840(9) 1 calc R U P A 5
C5_8 C -0.0993(8) 0.7470(8) 0.3266(4) 0.044(2) Uani 0.840(9) 1 d D U P A 5
H5_8 H -0.111276 0.783047 0.344463 0.052 Uiso 0.840(9) 1 calc R U P A 5
C6_8 C -0.1668(8) 0.7243(7) 0.3039(3) 0.053(2) Uani 0.840(9) 1 d D U P A 5
H6_8 H -0.224682 0.745137 0.305938 0.063 Uiso 0.840(9) 1 calc R U P A 5
F1_8 F -0.2134(10) 0.6493(7) 0.2550(4) 0.071(3) Uani 0.840(9) 1 d D U P A 5
F2_8 F -0.0498(4) 0.5946(2) 0.24830(11) 0.0453(15) Uani 0.840(9) 1 d D U P A 5
C1_21 C -0.153(3) 0.733(3) 0.3047(14) 0.046(4) Uani 0.160(9) 1 d D U P A 4
C2_21 C -0.145(4) 0.681(3) 0.2774(15) 0.043(3) Uani 0.160(9) 1 d D U P A 4
C3_21 C -0.066(4) 0.644(4) 0.2721(19) 0.036(3) Uani 0.160(9) 1 d D U P A 4
H3_21 H -0.062153 0.607878 0.253789 0.044 Uiso 0.160(9) 1 calc R U P A 4
C4_21 C 0.007(4) 0.660(5) 0.294(2) 0.034(4) Uani 0.160(9) 1 d D U P A 4
H4_21 H 0.063161 0.638398 0.288483 0.041 Uiso 0.160(9) 1 calc R U P A 4
C5_21 C -0.002(3) 0.708(4) 0.323(2) 0.036(4) Uani 0.160(9) 1 d D U P A 4
H5_21 H 0.045934 0.713275 0.339435 0.043 Uiso 0.160(9) 1 calc R U P A 4
C6_21 C -0.080(3) 0.747(4) 0.327(2) 0.042(4) Uani 0.160(9) 1 d D U P A 4
H6_21 H -0.084214 0.782856 0.345272 0.050 Uiso 0.160(9) 1 calc R U P A 4
F1_21 F -0.234(2) 0.7630(19) 0.3094(9) 0.072(7) Uani 0.160(9) 1 d D U P A 4
F2_21 F -0.214(5) 0.668(3) 0.2551(18) 0.044(6) Uani 0.160(9) 1 d D U P A 4
C1_9 C -0.3358(8) 0.5272(5) 0.4666(3) 0.031(2) Uani 0.685(9) 1 d D U P A 4
C2_9 C -0.3920(6) 0.5377(5) 0.4377(3) 0.0267(18) Uani 0.685(9) 1 d D U P A 4
C3_9 C -0.3848(7) 0.4960(6) 0.4063(3) 0.034(2) Uani 0.685(9) 1 d D U P A 4
H3_9 H -0.423563 0.503496 0.386155 0.041 Uiso 0.685(9) 1 calc R U P A 4
C4_9 C -0.3189(9) 0.4428(8) 0.4054(4) 0.040(3) Uani 0.685(9) 1 d D U P A 4
H4_9 H -0.310969 0.414649 0.384009 0.049 Uiso 0.685(9) 1 calc R U P A 4
C5_9 C -0.2646(11) 0.4303(9) 0.4354(4) 0.037(3) Uani 0.685(9) 1 d D U P A 4
H5_9 H -0.222606 0.391646 0.435001 0.045 Uiso 0.685(9) 1 calc R U P A 4
C6_9 C -0.2714(8) 0.4737(6) 0.4658(3) 0.034(2) Uani 0.685(9) 1 d D U P A 4
H6_9 H -0.232271 0.466953 0.485956 0.040 Uiso 0.685(9) 1 calc R U P A 4
F1_9 F -0.3449(6) 0.5694(4) 0.49586(16) 0.066(2) Uani 0.685(9) 1 d D U P A 4
F2_9 F -0.4552(5) 0.5894(3) 0.4403(2) 0.0488(18) Uani 0.685(9) 1 d D U P A 4
C1_18 C -0.3742(13) 0.5299(10) 0.4541(6) 0.032(4) Uani 0.315(9) 1 d D U P A 5
C2_18 C -0.3935(12) 0.4979(13) 0.4214(5) 0.042(4) Uani 0.315(9) 1 d D U P A 5
C3_18 C -0.3404(17) 0.4438(17) 0.4067(7) 0.036(5) Uani 0.315(9) 1 d D U P A 5
H3_18 H -0.355064 0.421899 0.384039 0.043 Uiso 0.315(9) 1 calc R U P A 5
C4_18 C -0.266(2) 0.4229(17) 0.4259(7) 0.023(4) Uani 0.315(9) 1 d D U P A 5
H4_18 H -0.226525 0.387563 0.415839 0.027 Uiso 0.315(9) 1 calc R U P A 5
C5_18 C -0.2471(13) 0.4527(12) 0.4595(5) 0.019(4) Uani 0.315(9) 1 d D U P A 5
H5_18 H -0.197234 0.435488 0.473007 0.023 Uiso 0.315(9) 1 calc R U P A 5
C6_18 C -0.3003(13) 0.5076(11) 0.4738(5) 0.026(4) Uani 0.315(9) 1 d D U P A 5
H6_18 H -0.286184 0.529225 0.496537 0.031 Uiso 0.315(9) 1 calc R U P A 5
F1_18 F -0.4277(12) 0.5827(9) 0.4654(5) 0.074(5) Uani 0.315(9) 1 d D U P A 5
F2_18 F -0.4641(10) 0.5135(11) 0.4014(4) 0.092(6) Uani 0.315(9) 1 d D U P A 5
C1_7 C 0.3184(7) 0.5033(7) 0.4130(3) 0.040(2) Uani 0.702(18) 1 d D U P A 4
C2_7 C 0.3027(6) 0.5389(5) 0.4459(3) 0.032(2) Uani 0.702(18) 1 d D U P A 4
C3_7 C 0.2380(7) 0.5161(6) 0.4693(3) 0.025(2) Uani 0.702(18) 1 d D U P A 4
H3_7 H 0.228099 0.540648 0.491674 0.030 Uiso 0.702(18) 1 calc R U P A 4
C4_7 C 0.1864(7) 0.4560(6) 0.4598(3) 0.026(2) Uani 0.702(18) 1 d D U P A 4
H4_7 H 0.140386 0.440020 0.475774 0.031 Uiso 0.702(18) 1 calc R U P A 4
C5_7 C 0.2015(9) 0.4192(6) 0.4273(3) 0.028(2) Uani 0.702(18) 1 d D U P A 4
H5_7 H 0.166564 0.377932 0.421276 0.033 Uiso 0.702(18) 1 calc R U P A 4
C6_7 C 0.2684(10) 0.4432(8) 0.4035(4) 0.037(3) Uani 0.702(18) 1 d D U P A 4
H6_7 H 0.279280 0.418632 0.381221 0.045 Uiso 0.702(18) 1 calc R U P A 4
F1_7 F 0.3837(7) 0.5276(7) 0.3916(3) 0.081(3) Uani 0.702(18) 1 d D U P A 4
F2_7 F 0.3531(5) 0.5970(4) 0.4535(3) 0.057(3) Uani 0.702(18) 1 d D U P A 4
C1_22 C 0.3161(15) 0.5505(11) 0.4314(7) 0.034(4) Uani 0.298(18) 1 d D U P A 5
C2_22 C 0.3082(16) 0.5067(13) 0.4012(6) 0.036(5) Uani 0.298(18) 1 d D U P A 5
C3_22 C 0.251(2) 0.4486(17) 0.4020(8) 0.036(5) Uani 0.298(18) 1 d D U P A 5
H3_22 H 0.244228 0.418588 0.381150 0.043 Uiso 0.298(18) 1 calc R U P A 5
C4_22 C 0.203(3) 0.4338(17) 0.4340(8) 0.033(5) Uani 0.298(18) 1 d D U P A 5
H4_22 H 0.165281 0.392509 0.435152 0.040 Uiso 0.298(18) 1 calc R U P A 5
C5_22 C 0.2106(17) 0.4789(14) 0.4637(6) 0.028(4) Uani 0.298(18) 1 d D U P A 5
H5_22 H 0.174114 0.470995 0.484572 0.034 Uiso 0.298(18) 1 calc R U P A 5
C6_22 C 0.2713(19) 0.5358(13) 0.4634(6) 0.031(4) Uani 0.298(18) 1 d D U P A 5
H6_22 H 0.281712 0.563912 0.484653 0.037 Uiso 0.298(18) 1 calc R U P A 5
F1_22 F 0.3726(12) 0.6070(9) 0.4292(8) 0.061(6) Uani 0.298(18) 1 d D U P A 5
F2_22 F 0.3631(14) 0.5258(13) 0.3736(6) 0.060(6) Uani 0.298(18) 1 d D U P A 5
O1_5 O 0.5004(7) 0.1930(5) 0.4184(2) 0.031(2) Uani 0.500(8) 1 d D U P B 1
C1_5 C 0.4841(7) 0.2232(6) 0.4515(3) 0.0196(16) Uani 0.500(8) 1 d D U P B 1
C2_5 C 0.4006(8) 0.2719(6) 0.4527(3) 0.0224(17) Uani 0.500(8) 1 d D U P B 1
F1_5 F 0.4070(7) 0.3248(5) 0.4271(2) 0.037(2) Uani 0.500(8) 1 d D U P B 1
F2_5 F 0.3256(6) 0.2341(5) 0.4438(2) 0.034(2) Uani 0.500(8) 1 d D U P B 1
C3_5 C 0.5665(8) 0.2709(6) 0.4626(3) 0.0216(17) Uani 0.500(8) 1 d D U P B 1
F3_5 F 0.5785(6) 0.3227(4) 0.4373(2) 0.0287(19) Uani 0.500(8) 1 d D U P B 1
F4_5 F 0.6406(5) 0.2298(4) 0.4623(3) 0.0316(18) Uani 0.500(8) 1 d D U P B 1
C4_5 C 0.4716(10) 0.1638(7) 0.4812(4) 0.0191(19) Uani 0.500(8) 1 d D U P B 1
F5_5 F 0.5433(8) 0.1197(6) 0.4830(3) 0.025(2) Uani 0.500(8) 1 d D U P B 1
F6_5 F 0.4026(10) 0.1202(10) 0.4737(6) 0.027(3) Uani 0.500(8) 1 d D U P B 1
C5_5 C 0.4589(8) 0.1987(8) 0.5193(4) 0.0158(16) Uani 0.500(8) 1 d D U P B 1
F7_5 F 0.4499(9) 0.1448(8) 0.5446(5) 0.024(3) Uani 0.500(8) 1 d D U P B 1
C6_5 C 0.5421(8) 0.2451(6) 0.5293(3) 0.0178(18) Uani 0.500(8) 1 d D U P B 1
F8_5 F 0.6160(6) 0.2048(5) 0.5305(3) 0.032(2) Uani 0.500(8) 1 d D U P B 1
F9_5 F 0.5328(7) 0.2746(5) 0.5625(2) 0.0274(19) Uani 0.500(8) 1 d D U P B 1
C7_5 C 0.5529(8) 0.3059(6) 0.5009(3) 0.0203(17) Uani 0.500(8) 1 d D U P B 1
F10_5 F 0.6265(7) 0.3464(6) 0.5089(2) 0.030(2) Uani 0.500(8) 1 d D U P B 1
C8_5 C 0.4688(10) 0.3538(9) 0.4996(5) 0.0285(19) Uani 0.500(8) 1 d D U P B 1
F11_5 F 0.4814(13) 0.4073(11) 0.4748(7) 0.043(3) Uani 0.500(8) 1 d D U P B 1
F12_5 F 0.4570(12) 0.3877(12) 0.5315(4) 0.038(3) Uani 0.500(8) 1 d D U P B 1
C9_5 C 0.3859(9) 0.3073(7) 0.4904(3) 0.0231(18) Uani 0.500(8) 1 d D U P B 1
F13_5 F 0.3119(7) 0.3498(6) 0.4911(3) 0.040(2) Uani 0.500(8) 1 d D U P B 1
C10_5 C 0.3751(8) 0.2475(7) 0.5193(3) 0.0200(19) Uani 0.500(8) 1 d D U P B 1
F14_5 F 0.3026(7) 0.2056(6) 0.5119(3) 0.033(2) Uani 0.500(8) 1 d D U P B 1
F15_5 F 0.3624(7) 0.2749(6) 0.5529(3) 0.034(2) Uani 0.500(8) 1 d D U P B 1
O1_12 O 0.4401(7) 0.1986(6) 0.4163(2) 0.039(2) Uani 0.500(8) 1 d D U P B 2
C1_12 C 0.4515(8) 0.2269(6) 0.4502(3) 0.0223(16) Uani 0.500(8) 1 d D U P B 2
C2_12 C 0.4579(10) 0.1655(8) 0.4791(4) 0.0196(19) Uani 0.500(8) 1 d D U P B 2
F1_12 F 0.3830(10) 0.1252(11) 0.4792(6) 0.033(3) Uani 0.500(8) 1 d D U P B 2
F2_12 F 0.5258(9) 0.1193(7) 0.4720(3) 0.025(2) Uani 0.500(8) 1 d D U P B 2
C3_12 C 0.3718(8) 0.2767(6) 0.4606(3) 0.0262(19) Uani 0.500(8) 1 d D U P B 2
F3_12 F 0.2943(6) 0.2395(5) 0.4594(2) 0.042(2) Uani 0.500(8) 1 d D U P B 2
F4_12 F 0.3639(8) 0.3305(5) 0.4361(2) 0.048(3) Uani 0.500(8) 1 d D U P B 2
C4_12 C 0.5384(8) 0.2712(6) 0.4525(3) 0.0259(18) Uani 0.500(8) 1 d D U P B 2
F5_12 F 0.5335(9) 0.3254(5) 0.4277(3) 0.058(3) Uani 0.500(8) 1 d D U P B 2
F6_12 F 0.6096(6) 0.2309(5) 0.4438(3) 0.035(2) Uani 0.500(8) 1 d D U P B 2
C5_12 C 0.5489(8) 0.3049(6) 0.4909(3) 0.0234(18) Uani 0.500(8) 1 d D U P B 2
F7_12 F 0.6250(7) 0.3452(6) 0.4918(4) 0.050(3) Uani 0.500(8) 1 d D U P B 2
C6_12 C 0.4688(10) 0.3543(8) 0.5010(5) 0.0276(19) Uani 0.500(8) 1 d D U P B 2
F8_12 F 0.4625(13) 0.4105(12) 0.4774(7) 0.048(4) Uani 0.500(8) 1 d D U P B 2
F9_12 F 0.4796(11) 0.3823(11) 0.5346(5) 0.038(3) Uani 0.500(8) 1 d D U P B 2
C7_12 C 0.3825(8) 0.3083(7) 0.4995(3) 0.0195(17) Uani 0.500(8) 1 d D U P B 2
F10_12 F 0.3107(7) 0.3517(6) 0.5074(2) 0.033(2) Uani 0.500(8) 1 d D U P B 2
C8_12 C 0.3903(8) 0.2460(7) 0.5277(3) 0.0171(18) Uani 0.500(8) 1 d D U P B 2
F11_12 F 0.3130(7) 0.2082(6) 0.5274(3) 0.031(2) Uani 0.500(8) 1 d D U P B 2
F12_12 F 0.3976(7) 0.2739(6) 0.5614(2) 0.027(2) Uani 0.500(8) 1 d D U P B 2
C9_12 C 0.4698(9) 0.1974(7) 0.5178(4) 0.0153(16) Uani 0.500(8) 1 d D U P B 2
F13_12 F 0.4761(10) 0.1422(8) 0.5429(5) 0.027(3) Uani 0.500(8) 1 d D U P B 2
C10_12 C 0.5561(8) 0.2433(6) 0.5192(3) 0.0190(18) Uani 0.500(8) 1 d D U P B 2
F14_12 F 0.6274(5) 0.2010(5) 0.5122(3) 0.0271(18) Uani 0.500(8) 1 d D U P B 2
F15_12 F 0.5697(7) 0.2701(5) 0.5528(3) 0.035(2) Uani 0.500(8) 1 d D U P B 2
O1_4 O 0.5513(9) 0.0841(7) 0.3900(5) 0.023(3) Uani 0.276(4) 1 d D U P B 1
C1_4 C 0.6301(11) 0.0504(8) 0.3830(4) 0.022(2) Uani 0.276(4) 1 d D U P B 1
C2_4 C 0.6951(11) 0.0926(9) 0.3576(5) 0.034(3) Uani 0.276(4) 1 d D U P B 1
F1_4 F 0.6559(16) 0.1062(12) 0.3248(5) 0.041(4) Uani 0.276(4) 1 d D U P B 1
F2_4 F 0.7076(16) 0.1612(9) 0.3699(6) 0.046(5) Uani 0.276(4) 1 d D U P B 1
C3_4 C 0.6094(10) -0.0232(8) 0.3647(4) 0.028(3) Uani 0.276(4) 1 d D U P B 1
F3_4 F 0.5683(14) -0.0216(10) 0.3320(5) 0.038(4) Uani 0.276(4) 1 d D U P B 1
F4_4 F 0.5604(12) -0.0649(8) 0.3876(5) 0.044(4) Uani 0.276(4) 1 d D U P B 1
C4_4 C 0.6802(11) 0.0325(9) 0.4193(4) 0.031(3) Uani 0.276(4) 1 d D U P B 1
F5_4 F 0.6267(15) -0.0066(11) 0.4412(5) 0.038(4) Uani 0.276(4) 1 d D U P B 1
F6_4 F 0.7040(13) 0.0918(10) 0.4379(5) 0.051(4) Uani 0.276(4) 1 d D U P B 1
C5_4 C 0.7674(11) -0.0103(9) 0.4113(4) 0.036(3) Uani 0.276(4) 1 d D U P B 1
F7_4 F 0.8082(13) -0.0230(11) 0.4431(4) 0.056(5) Uani 0.276(4) 1 d D U P B 1
C6_4 C 0.7421(12) -0.0827(9) 0.3935(4) 0.036(3) Uani 0.276(4) 1 d D U P B 1
F8_4 F 0.6889(15) -0.1234(11) 0.4149(5) 0.048(5) Uani 0.276(4) 1 d D U P B 1
F9_4 F 0.8155(12) -0.1233(11) 0.3877(6) 0.051(5) Uani 0.276(4) 1 d D U P B 1
C7_4 C 0.6953(11) -0.0666(9) 0.3570(4) 0.030(3) Uani 0.276(4) 1 d D U P B 1
F10_4 F 0.6750(14) -0.1296(10) 0.3409(5) 0.047(4) Uani 0.276(4) 1 d D U P B 1
C8_4 C 0.7566(11) -0.0246(9) 0.3320(4) 0.025(3) Uani 0.276(4) 1 d D U P B 1
F11_4 F 0.7208(16) -0.0121(11) 0.2990(4) 0.038(4) Uani 0.276(4) 1 d D U P B 1
F12_4 F 0.8310(10) -0.0645(9) 0.3244(4) 0.036(3) Uani 0.276(4) 1 d D U P B 1
C9_4 C 0.7810(11) 0.0488(9) 0.3495(5) 0.034(3) Uani 0.276(4) 1 d D U P B 1
F13_4 F 0.8393(14) 0.0830(11) 0.3269(6) 0.062(6) Uani 0.276(4) 1 d D U P B 1
C10_4 C 0.8288(11) 0.0337(9) 0.3860(5) 0.040(3) Uani 0.276(4) 1 d D U P B 1
F14_4 F 0.8547(12) 0.0986(10) 0.3998(6) 0.067(5) Uani 0.276(4) 1 d D U P B 1
F15_4 F 0.9053(9) -0.0044(11) 0.3808(5) 0.064(4) Uani 0.276(4) 1 d D U P B 1
O1_6 O 0.4672(15) 0.1893(9) 0.3388(4) 0.020(3) Uani 0.269(3) 1 d D U P B 1
C1_6 C 0.4716(11) 0.2529(9) 0.3198(5) 0.020(2) Uani 0.269(3) 1 d D U P B 1
C2_6 C 0.5545(10) 0.3013(8) 0.3117(4) 0.023(2) Uani 0.269(3) 1 d D U P B 1
F1_6 F 0.5872(10) 0.3366(6) 0.3416(3) 0.028(3) Uani 0.269(3) 1 d D U P B 1
F2_6 F 0.6271(9) 0.2635(8) 0.2996(4) 0.025(3) Uani 0.269(3) 1 d D U P B 1
C3_6 C 0.3837(11) 0.2972(10) 0.3274(4) 0.024(3) Uani 0.269(3) 1 d D U P B 1
F3_6 F 0.3786(12) 0.3153(9) 0.3632(4) 0.030(3) Uani 0.269(3) 1 d D U P B 1
F4_6 F 0.3079(10) 0.2590(8) 0.3207(5) 0.036(3) Uani 0.269(3) 1 d D U P B 1
C4_6 C 0.4473(12) 0.2156(9) 0.2821(4) 0.023(3) Uani 0.269(3) 1 d D U P B 1
F5_6 F 0.3800(9) 0.1704(7) 0.2899(4) 0.030(3) Uani 0.269(3) 1 d D U P B 1
F6_6 F 0.5154(12) 0.1729(9) 0.2717(6) 0.022(4) Uani 0.269(3) 1 d D U P B 1
C5_6 C 0.4266(11) 0.2734(8) 0.2538(4) 0.030(2) Uani 0.269(3) 1 d D U P B 1
F7_6 F 0.4027(11) 0.2386(8) 0.2228(3) 0.043(4) Uani 0.269(3) 1 d D U P B 1
C6_6 C 0.3683(12) 0.3402(8) 0.2628(4) 0.036(3) Uani 0.269(3) 1 d D U P B 1
F8_6 F 0.2924(10) 0.3098(8) 0.2565(4) 0.046(3) Uani 0.269(3) 1 d D U P B 1
F9_6 F 0.3648(11) 0.3968(8) 0.2404(4) 0.052(3) Uani 0.269(3) 1 d D U P B 1
C7_6 C 0.3770(12) 0.3649(9) 0.3029(4) 0.029(3) Uani 0.269(3) 1 d D U P B 1
F10_6 F 0.3074(13) 0.4081(13) 0.3123(7) 0.041(5) Uani 0.269(3) 1 d D U P B 1
C8_6 C 0.4620(12) 0.4105(9) 0.2984(5) 0.034(3) Uani 0.269(3) 1 d D U P B 1
F11_6 F 0.4819(13) 0.4446(9) 0.3285(5) 0.044(4) Uani 0.269(3) 1 d D U P B 1
F12_6 F 0.4535(14) 0.4716(9) 0.2771(5) 0.054(4) Uani 0.269(3) 1 d D U P B 1
C9_6 C 0.5356(11) 0.3609(7) 0.2827(4) 0.026(2) Uani 0.269(3) 1 d D U P B 1
F13_6 F 0.6062(9) 0.4041(7) 0.2751(4) 0.043(3) Uani 0.269(3) 1 d D U P B 1
C10_6 C 0.5081(11) 0.3218(8) 0.2468(4) 0.030(3) Uani 0.269(3) 1 d D U P B 1
F14_6 F 0.5757(10) 0.2824(9) 0.2332(4) 0.040(3) Uani 0.269(3) 1 d D U P B 1
F15_6 F 0.4852(12) 0.3705(11) 0.2207(5) 0.043(5) Uani 0.269(3) 1 d D U P B 1
O1_3 O 0.3886(5) 0.0834(4) 0.38787(17) 0.0380(16) Uani 0.726(3) 1 d D U P B 1
C1_3 C 0.3107(6) 0.0515(4) 0.3786(2) 0.0264(15) Uani 0.726(3) 1 d D U P B 1
C2_3 C 0.3018(5) 0.0407(5) 0.3365(2) 0.0309(15) Uani 0.726(3) 1 d D U P B 1
F1_3 F 0.3032(4) 0.1040(3) 0.31897(14) 0.0475(15) Uani 0.726(3) 1 d D U P B 1
F2_3 F 0.3717(4) 0.0032(5) 0.32333(16) 0.0526(16) Uani 0.726(3) 1 d D U P B 1
C3_3 C 0.2287(6) 0.0965(5) 0.3915(2) 0.0328(16) Uani 0.726(3) 1 d D U P B 1
F3_3 F 0.2296(5) 0.1621(3) 0.37669(18) 0.0523(18) Uani 0.726(3) 1 d D U P B 1
F4_3 F 0.2320(4) 0.1051(4) 0.42790(13) 0.0476(15) Uani 0.726(3) 1 d D U P B 1
C4_3 C 0.3067(6) -0.0241(4) 0.3971(2) 0.0313(17) Uani 0.726(3) 1 d D U P B 1
F5_3 F 0.3130(4) -0.0174(3) 0.43341(14) 0.0437(15) Uani 0.726(3) 1 d D U P B 1
F6_3 F 0.3759(5) -0.0649(4) 0.3865(2) 0.052(2) Uani 0.726(3) 1 d D U P B 1
C5_3 C 0.2184(6) -0.0648(5) 0.3873(2) 0.0359(16) Uani 0.726(3) 1 d D U P B 1
F7_3 F 0.2169(5) -0.1307(3) 0.40351(19) 0.065(2) Uani 0.726(3) 1 d D U P B 1
C6_3 C 0.1386(6) -0.0188(5) 0.4004(2) 0.0421(19) Uani 0.726(3) 1 d D U P B 1
F8_3 F 0.1406(4) -0.0125(5) 0.43663(15) 0.0573(18) Uani 0.726(3) 1 d D U P B 1
F9_3 F 0.0624(5) -0.0539(5) 0.39238(19) 0.069(2) Uani 0.726(3) 1 d D U P B 1
C7_3 C 0.1400(6) 0.0567(5) 0.3821(2) 0.0360(17) Uani 0.726(3) 1 d D U P B 1
F10_3 F 0.0691(6) 0.0957(5) 0.39370(18) 0.066(2) Uani 0.726(3) 1 d D U P B 1
C8_3 C 0.1327(5) 0.0463(4) 0.3404(2) 0.0296(15) Uani 0.726(3) 1 d D U P B 1
F11_3 F 0.1327(4) 0.1118(3) 0.32350(14) 0.0454(15) Uani 0.726(3) 1 d D U P B 1
F12_3 F 0.0561(3) 0.0138(3) 0.33125(14) 0.0434(14) Uani 0.726(3) 1 d D U P B 1
C9_3 C 0.2136(5) 0.0016(4) 0.32680(18) 0.0253(13) Uani 0.726(3) 1 d D U P B 1
F13_3 F 0.2073(3) -0.0077(3) 0.29012(12) 0.0370(12) Uani 0.726(3) 1 d D U P B 1
C10_3 C 0.2128(6) -0.0737(4) 0.3456(2) 0.0362(17) Uani 0.726(3) 1 d D U P B 1
F14_3 F 0.2801(5) -0.1147(3) 0.33283(19) 0.0576(17) Uani 0.726(3) 1 d D U P B 1
F15_3 F 0.1381(4) -0.1100(3) 0.33580(17) 0.0522(16) Uani 0.726(3) 1 d D U P B 1
O1_15 O 0.3826(9) 0.0915(8) 0.3606(4) 0.029(3) Uani 0.274(3) 1 d D U P B 2
C1_15 C 0.3074(11) 0.0507(9) 0.3648(4) 0.026(3) Uani 0.274(3) 1 d D U P B 2
C2_15 C 0.2199(10) 0.0958(8) 0.3688(4) 0.033(3) Uani 0.274(3) 1 d D U P B 2
F1_15 F 0.2278(11) 0.1418(8) 0.3972(4) 0.042(3) Uani 0.274(3) 1 d D U P B 2
F2_15 F 0.2106(11) 0.1386(8) 0.3391(4) 0.047(4) Uani 0.274(3) 1 d D U P B 2
C3_15 C 0.3125(11) 0.0027(9) 0.3993(4) 0.027(3) Uani 0.274(3) 1 d D U P B 2
F3_15 F 0.3236(10) 0.0421(8) 0.4299(3) 0.039(3) Uani 0.274(3) 1 d D U P B 2
F4_15 F 0.3862(11) -0.0387(10) 0.3979(6) 0.049(4) Uani 0.274(3) 1 d D U P B 2
C4_15 C 0.2933(11) -0.0006(9) 0.3321(4) 0.035(3) Uani 0.274(3) 1 d D U P B 2
F5_15 F 0.3662(10) -0.0441(9) 0.3291(5) 0.048(4) Uani 0.274(3) 1 d D U P B 2
F6_15 F 0.2866(12) 0.0386(9) 0.3014(3) 0.052(4) Uani 0.274(3) 1 d D U P B 2
C5_15 C 0.2092(11) -0.0486(8) 0.3366(4) 0.034(3) Uani 0.274(3) 1 d D U P B 2
F7_15 F 0.1998(11) -0.0931(8) 0.3075(3) 0.056(4) Uani 0.274(3) 1 d D U P B 2
C6_15 C 0.2188(10) -0.0952(8) 0.3710(4) 0.034(3) Uani 0.274(3) 1 d D U P B 2
F8_15 F 0.2888(9) -0.1410(6) 0.3689(4) 0.048(4) Uani 0.274(3) 1 d D U P B 2
F9_15 F 0.1468(9) -0.1395(7) 0.3756(4) 0.045(4) Uani 0.274(3) 1 d D U P B 2
C7_15 C 0.2299(10) -0.0460(8) 0.4049(4) 0.030(3) Uani 0.274(3) 1 d D U P B 2
F10_15 F 0.2375(10) -0.0877(8) 0.4355(4) 0.052(4) Uani 0.274(3) 1 d D U P B 2
C8_15 C 0.1453(11) 0.0024(8) 0.4081(4) 0.032(3) Uani 0.274(3) 1 d D U P B 2
F11_15 F 0.1514(10) 0.0439(9) 0.4381(4) 0.045(4) Uani 0.274(3) 1 d D U P B 2
F12_15 F 0.0723(9) -0.0398(8) 0.4132(5) 0.050(4) Uani 0.274(3) 1 d D U P B 2
C9_15 C 0.1357(11) 0.0491(9) 0.3737(4) 0.031(3) Uani 0.274(3) 1 d D U P B 2
F13_15 F 0.0619(12) 0.0909(9) 0.3763(5) 0.057(5) Uani 0.274(3) 1 d D U P B 2
C10_15 C 0.1253(10) -0.0015(9) 0.3402(4) 0.039(3) Uani 0.274(3) 1 d D U P B 2
F14_15 F 0.1118(11) 0.0371(9) 0.3100(4) 0.058(4) Uani 0.274(3) 1 d D U P B 2
F15_15 F 0.0505(9) -0.0421(8) 0.3437(4) 0.053(4) Uani 0.274(3) 1 d D U P B 2
O1_16 O 0.4343(7) 0.2062(5) 0.3467(2) 0.0188(18) Uani 0.460(3) 1 d D U P B 3
C1_16 C 0.4552(8) 0.2552(6) 0.3210(3) 0.0164(18) Uani 0.460(3) 1 d D U P B 3
C2_16 C 0.4927(7) 0.2193(6) 0.2859(3) 0.0206(18) Uani 0.460(3) 1 d D U P B 3
F1_16 F 0.5668(5) 0.1808(4) 0.2928(2) 0.0284(17) Uani 0.460(3) 1 d D U P B 3
F2_16 F 0.4332(7) 0.1706(4) 0.2725(2) 0.0284(18) Uani 0.460(3) 1 d D U P B 3
C3_16 C 0.5263(8) 0.3109(6) 0.3339(3) 0.0220(18) Uani 0.460(3) 1 d D U P B 3
F3_16 F 0.6029(5) 0.2773(4) 0.3436(2) 0.0312(17) Uani 0.460(3) 1 d D U P B 3
F4_16 F 0.4980(6) 0.3464(4) 0.36403(18) 0.0319(18) Uani 0.460(3) 1 d D U P B 3
C4_16 C 0.3704(7) 0.2991(6) 0.3100(3) 0.0221(18) Uani 0.460(3) 1 d D U P B 3
F5_16 F 0.3355(6) 0.3326(4) 0.3394(2) 0.0341(18) Uani 0.460(3) 1 d D U P B 3
F6_16 F 0.3060(5) 0.2537(4) 0.2982(2) 0.0293(17) Uani 0.460(3) 1 d D U P B 3
C5_16 C 0.3909(8) 0.3567(6) 0.2796(3) 0.0296(18) Uani 0.460(3) 1 d D U P B 3
F7_16 F 0.3155(6) 0.3933(5) 0.2711(2) 0.043(2) Uani 0.460(3) 1 d D U P B 3
C6_16 C 0.4604(9) 0.4082(6) 0.2935(3) 0.032(2) Uani 0.460(3) 1 d D U P B 3
F8_16 F 0.4341(8) 0.4461(5) 0.3228(2) 0.042(2) Uani 0.460(3) 1 d D U P B 3
F9_16 F 0.4756(10) 0.4575(4) 0.2672(2) 0.063(4) Uani 0.460(3) 1 d D U P B 3
C7_16 C 0.5483(9) 0.3684(7) 0.3038(3) 0.0275(19) Uani 0.460(3) 1 d D U P B 3
F10_16 F 0.6117(9) 0.4146(9) 0.3168(4) 0.043(3) Uani 0.460(3) 1 d D U P B 3
C8_16 C 0.5852(8) 0.3301(6) 0.2699(3) 0.0298(19) Uani 0.460(3) 1 d D U P B 3
F11_16 F 0.6611(5) 0.2930(5) 0.2779(2) 0.0351(18) Uani 0.460(3) 1 d D U P B 3
F12_16 F 0.6063(6) 0.3790(5) 0.2441(2) 0.042(2) Uani 0.460(3) 1 d D U P B 3
C9_16 C 0.5137(7) 0.2763(5) 0.2557(3) 0.0241(17) Uani 0.460(3) 1 d D U P B 3
F13_16 F 0.5466(6) 0.2430(5) 0.22560(19) 0.037(2) Uani 0.460(3) 1 d D U P B 3
C10_16 C 0.4279(8) 0.3174(6) 0.2458(3) 0.0263(19) Uani 0.460(3) 1 d D U P B 3
F14_16 F 0.3660(6) 0.2718(5) 0.2322(2) 0.0357(19) Uani 0.460(3) 1 d D U P B 3
F15_16 F 0.4461(7) 0.3660(6) 0.2189(3) 0.037(3) Uani 0.460(3) 1 d D U P B 3
O1_14 O 0.5014(12) 0.2027(8) 0.3457(4) 0.022(3) Uani 0.271(3) 1 d D U P B 2
C1_14 C 0.4717(12) 0.2486(10) 0.3196(4) 0.019(2) Uani 0.271(3) 1 d D U P B 2
C2_14 C 0.4650(12) 0.2316(9) 0.2784(4) 0.024(3) Uani 0.271(3) 1 d D U P B 2
F1_14 F 0.5340(12) 0.1915(9) 0.2668(6) 0.023(4) Uani 0.271(3) 1 d D U P B 2
F2_14 F 0.3905(11) 0.1914(8) 0.2701(4) 0.027(3) Uani 0.271(3) 1 d D U P B 2
C3_14 C 0.5544(11) 0.3000(9) 0.3255(4) 0.024(3) Uani 0.271(3) 1 d D U P B 2
F3_14 F 0.6259(9) 0.2592(9) 0.3172(5) 0.030(3) Uani 0.271(3) 1 d D U P B 2
F4_14 F 0.5543(11) 0.3143(7) 0.3615(3) 0.030(3) Uani 0.271(3) 1 d D U P B 2
C4_14 C 0.3959(11) 0.2988(9) 0.3339(4) 0.023(3) Uani 0.271(3) 1 d D U P B 2
F5_14 F 0.4193(11) 0.3362(8) 0.3641(3) 0.026(3) Uani 0.271(3) 1 d D U P B 2
F6_14 F 0.3258(8) 0.2591(7) 0.3411(4) 0.025(2) Uani 0.271(3) 1 d D U P B 2
C5_14 C 0.3759(12) 0.3607(9) 0.3059(4) 0.028(2) Uani 0.271(3) 1 d D U P B 2
F7_14 F 0.3015(12) 0.3971(12) 0.3167(6) 0.032(4) Uani 0.271(3) 1 d D U P B 2
C6_14 C 0.4590(11) 0.4093(8) 0.3129(4) 0.030(3) Uani 0.271(3) 1 d D U P B 2
F8_14 F 0.4623(12) 0.4319(7) 0.3478(3) 0.044(3) Uani 0.271(3) 1 d D U P B 2
F9_14 F 0.4570(12) 0.4721(7) 0.2945(4) 0.050(4) Uani 0.271(3) 1 d D U P B 2
C7_14 C 0.5465(12) 0.3692(10) 0.3024(4) 0.025(2) Uani 0.271(3) 1 d D U P B 2
F10_14 F 0.6208(14) 0.4094(15) 0.3091(7) 0.043(5) Uani 0.271(3) 1 d D U P B 2
C8_14 C 0.5397(11) 0.3481(7) 0.2619(4) 0.026(2) Uani 0.271(3) 1 d D U P B 2
F11_14 F 0.6165(9) 0.3113(7) 0.2521(4) 0.031(3) Uani 0.271(3) 1 d D U P B 2
F12_14 F 0.5432(10) 0.4108(6) 0.2419(3) 0.036(3) Uani 0.271(3) 1 d D U P B 2
C9_14 C 0.4547(10) 0.3024(9) 0.2548(4) 0.026(2) Uani 0.271(3) 1 d D U P B 2
F13_14 F 0.4535(9) 0.2860(7) 0.2187(3) 0.034(3) Uani 0.271(3) 1 d D U P B 2
C10_14 C 0.3578(10) 0.3221(10) 0.2690(4) 0.039(3) Uani 0.271(3) 1 d D U P B 2
F14_14 F 0.2829(9) 0.2784(8) 0.2733(4) 0.041(3) Uani 0.271(3) 1 d D U P B 2
F15_14 F 0.3169(10) 0.3635(10) 0.2436(4) 0.050(4) Uani 0.271(3) 1 d D U P B 2
O1_17 O 0.5749(8) 0.1137(8) 0.3884(4) 0.026(3) Uani 0.325(3) 1 d D U P B 3
C1_17 C 0.6386(10) 0.0647(8) 0.3803(4) 0.024(2) Uani 0.325(3) 1 d D U P B 3
C2_17 C 0.7293(10) 0.1025(8) 0.3878(4) 0.032(2) Uani 0.325(3) 1 d D U P B 3
F1_17 F 0.7431(19) 0.1604(10) 0.3665(6) 0.050(5) Uani 0.325(3) 1 d D U P B 3
F2_17 F 0.7325(12) 0.1247(8) 0.4229(4) 0.061(4) Uani 0.325(3) 1 d D U P B 3
C3_17 C 0.6402(10) 0.0384(8) 0.3403(4) 0.029(2) Uani 0.325(3) 1 d D U P B 3
F3_17 F 0.6399(16) 0.0948(11) 0.3170(5) 0.056(5) Uani 0.325(3) 1 d D U P B 3
F4_17 F 0.5639(10) 0.0078(9) 0.3315(4) 0.037(3) Uani 0.325(3) 1 d D U P B 3
C4_17 C 0.6320(9) -0.0044(8) 0.4047(4) 0.027(2) Uani 0.325(3) 1 d D U P B 3
F5_17 F 0.5536(8) -0.0377(8) 0.3987(4) 0.041(3) Uani 0.325(3) 1 d D U P B 3
F6_17 F 0.6341(14) 0.0163(11) 0.4403(4) 0.045(4) Uani 0.325(3) 1 d D U P B 3
C5_17 C 0.7137(10) -0.0538(8) 0.3982(4) 0.031(2) Uani 0.325(3) 1 d D U P B 3
F7_17 F 0.7124(14) -0.1114(10) 0.4212(5) 0.069(5) Uani 0.325(3) 1 d D U P B 3
C6_17 C 0.7104(11) -0.0787(8) 0.3581(4) 0.039(3) Uani 0.325(3) 1 d D U P B 3
F8_17 F 0.6344(11) -0.1154(8) 0.3509(5) 0.072(4) Uani 0.325(3) 1 d D U P B 3
F9_17 F 0.7770(11) -0.1257(7) 0.3506(4) 0.073(4) Uani 0.325(3) 1 d D U P B 3
C7_17 C 0.7192(9) -0.0133(8) 0.3327(4) 0.032(2) Uani 0.325(3) 1 d D U P B 3
F10_17 F 0.7158(16) -0.0338(11) 0.2974(4) 0.055(5) Uani 0.325(3) 1 d D U P B 3
C8_17 C 0.8074(10) 0.0256(9) 0.3403(4) 0.040(3) Uani 0.325(3) 1 d D U P B 3
F11_17 F 0.8137(12) 0.0825(11) 0.3172(4) 0.058(4) Uani 0.325(3) 1 d D U P B 3
F12_17 F 0.8777(9) -0.0197(9) 0.3342(5) 0.074(4) Uani 0.325(3) 1 d D U P B 3
C9_17 C 0.8089(9) 0.0520(8) 0.3799(4) 0.032(2) Uani 0.325(3) 1 d D U P B 3
F13_17 F 0.8874(9) 0.0868(9) 0.3856(4) 0.058(4) Uani 0.325(3) 1 d D U P B 3
C10_17 C 0.8017(10) -0.0132(9) 0.4061(4) 0.040(3) Uani 0.325(3) 1 d D U P B 3
F14_17 F 0.8066(13) 0.0121(11) 0.4404(4) 0.067(5) Uani 0.325(3) 1 d D U P B 3
F15_17 F 0.8710(10) -0.0586(9) 0.4004(5) 0.063(4) Uani 0.325(3) 1 d D U P B 3
O1_13 O 0.5628(6) 0.1014(5) 0.3631(2) 0.0193(18) Uani 0.399(3) 1 d D U P B 2
C1_13 C 0.6345(8) 0.0567(7) 0.3678(3) 0.022(2) Uani 0.399(3) 1 d D U P B 2
C2_13 C 0.6469(9) 0.0298(7) 0.4073(3) 0.034(2) Uani 0.399(3) 1 d D U P B 2
F1_13 F 0.6610(10) 0.0869(7) 0.4302(3) 0.058(3) Uani 0.399(3) 1 d D U P B 2
F2_13 F 0.5722(7) -0.0027(7) 0.4195(4) 0.060(3) Uani 0.399(3) 1 d D U P B 2
C3_13 C 0.7244(8) 0.0952(7) 0.3582(4) 0.035(2) Uani 0.399(3) 1 d D U P B 2
F3_13 F 0.7374(17) 0.1512(8) 0.3812(5) 0.063(5) Uani 0.399(3) 1 d D U P B 2
F4_13 F 0.7190(9) 0.1200(6) 0.3235(3) 0.059(3) Uani 0.399(3) 1 d D U P B 2
C4_13 C 0.6244(9) -0.0106(7) 0.3427(3) 0.034(2) Uani 0.399(3) 1 d D U P B 2
F5_13 F 0.6153(9) 0.0107(7) 0.3083(3) 0.062(3) Uani 0.399(3) 1 d D U P B 2
F6_13 F 0.5476(7) -0.0449(6) 0.3527(4) 0.062(3) Uani 0.399(3) 1 d D U P B 2
C5_13 C 0.7041(9) -0.0625(7) 0.3466(3) 0.031(2) Uani 0.399(3) 1 d D U P B 2
F7_13 F 0.6914(11) -0.1215(7) 0.3257(4) 0.071(5) Uani 0.399(3) 1 d D U P B 2
C6_13 C 0.7886(9) -0.0231(8) 0.3356(3) 0.038(2) Uani 0.399(3) 1 d D U P B 2
F8_13 F 0.7834(9) -0.0049(8) 0.3001(3) 0.066(3) Uani 0.399(3) 1 d D U P B 2
F9_13 F 0.8591(10) -0.0693(8) 0.3385(4) 0.059(4) Uani 0.399(3) 1 d D U P B 2
C7_13 C 0.8044(9) 0.0426(7) 0.3604(4) 0.034(2) Uani 0.399(3) 1 d D U P B 2
F10_13 F 0.8804(7) 0.0760(6) 0.3487(4) 0.063(3) Uani 0.399(3) 1 d D U P B 2
C8_13 C 0.8136(9) 0.0164(7) 0.4000(4) 0.035(2) Uani 0.399(3) 1 d D U P B 2
F11_13 F 0.8323(10) 0.0721(6) 0.4220(4) 0.068(4) Uani 0.399(3) 1 d D U P B 2
F12_13 F 0.8852(8) -0.0270(6) 0.4034(4) 0.046(3) Uani 0.399(3) 1 d D U P B 2
C9_13 C 0.7275(9) -0.0235(7) 0.4115(3) 0.031(2) Uani 0.399(3) 1 d D U P B 2
F13_13 F 0.7371(9) -0.0469(7) 0.4464(2) 0.062(3) Uani 0.399(3) 1 d D U P B 2
C10_13 C 0.7113(9) -0.0890(7) 0.3863(4) 0.033(2) Uani 0.399(3) 1 d D U P B 2
F14_13 F 0.6387(7) -0.1250(5) 0.3980(4) 0.054(3) Uani 0.399(3) 1 d D U P B 2
F15_13 F 0.7800(8) -0.1371(6) 0.3890(4) 0.039(3) Uani 0.399(3) 1 d D U P B 2


loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag1A C4_22 2.32(4) . ?
Ag1A O1_2 2.337(4) . ?
Ag1A C5_7 2.384(15) . ?
Ag1A O1_1 2.387(4) . ?
Ag1A C4_7 2.443(10) . ?
Ag1A C5_22 2.71(3) . ?
Ag1A C3_22 2.79(4) . ?
Ag1A C6_7 3.054(16) . ?
Ag1B O1_1 2.223(14) . ?
Ag1B O1_2 2.274(13) . ?
Ag1B F1_10 2.42(2) . ?
Ag1B C4_22 2.63(5) . ?
Ag1B C5_7 2.68(2) . ?
Ag1B C3_22 2.80(4) . ?
Ag1B C4_7 2.86(2) . ?
Ag1B C5_22 3.05(3) . ?
Ag1B C6_7 3.07(2) . ?
Ag2A C5_21 2.29(9) . ?
Ag2A O1_1 2.329(3) . ?
Ag2A O1_2 2.376(3) . ?
Ag2A C4_8 2.408(14) . ?
Ag2A C3_8 2.444(17) . ?
Ag2A C4_21 2.56(10) . ?
Ag2A C6_21 2.93(8) . ?
Ag2A C5_8 3.028(14) . ?
Ag2A C2_8 3.104(14) . ?
Ag2A C3_21 3.22(8) . ?
Ag2B F2_19 2.09(4) . ?
Ag2B F2_11 2.25(3) . ?
Ag2B C5_21 2.44(9) . ?
Ag2B O1_1 2.497(13) . ?
Ag2B C4_8 2.497(19) . ?
Ag2B C3_8 2.51(2) . ?
Ag2B C6_21 2.73(9) . ?
Ag2B C4_21 2.63(10) . ?
Ag2B C5_8 2.75(2) . ?
Ag2B C2_8 2.800(19) . ?
Ag2B C3_21 2.91(8) . ?
Ag3A C4_18 2.31(4) . ?
Ag3A C5_9 2.312(19) . ?
Ag3A O1_2 2.315(5) . ?
Ag3A O1_1 2.395(5) . ?
Ag3A C5_18 2.41(2) . ?
Ag3A C6_9 2.701(12) . ?
Ag3A C4_9 2.781(16) . ?
Ag3A C3_18 3.07(3) . ?
Ag3A C6_18 3.168(18) . ?
Ag3B O1_1 2.32(2) . ?
Ag3B C4_18 2.35(5) . ?
Ag3B O1_2 2.39(2) . ?
Ag3B C5_9 2.38(3) . ?
Ag3B C5_18 2.57(4) . ?
Ag3B C4_9 2.70(3) . ?
Ag3B C6_9 2.84(3) . ?
Ag3B C3_18 2.98(4) . ?
Ag3B C6_18 3.29(3) . ?
Al1 O1_3 1.691(6) . ?
Al1 O1_14 1.706(13) . ?
Al1 O1_12 1.707(7) . ?
Al1 O1_6 1.710(12) . ?
Al1 O1_4 1.715(12) . ?
Al1 O1_17 1.718(11) . ?
Al1 O1_5 1.723(8) . ?
Al1 O1_16 1.733(8) . ?
Al1 O1_13 1.737(8) . ?
Al1 O1_15 1.783(13) . ?
O1_1 C1_1 1.357(5) . ?
C1_1 C2_1 1.552(7) . ?
C1_1 C3_1 1.557(7) . ?
C1_1 C4_1 1.558(6) . ?
C2_1 F2_1 1.356(6) . ?
C2_1 F1_1 1.363(6) . ?
C2_1 C9_1 1.543(7) . ?
C3_1 F3_1 1.338(6) . ?
C3_1 F4_1 1.346(6) . ?
C3_1 C7_1 1.559(7) . ?
C4_1 F5_1 1.349(6) . ?
C4_1 F6_1 1.355(6) . ?
C4_1 C5_1 1.549(6) . ?
C5_1 F7_1 1.368(5) . ?
C5_1 C10_1 1.529(8) . ?
C5_1 C6_1 1.546(8) . ?
C6_1 F8_1 1.334(7) . ?
C6_1 F9_1 1.349(6) . ?
C6_1 C7_1 1.555(7) . ?
C7_1 F10_1 1.358(6) . ?
C7_1 C8_1 1.545(8) . ?
C8_1 F11_1 1.345(6) . ?
C8_1 F12_1 1.351(5) . ?
C8_1 C9_1 1.528(8) . ?
C9_1 F13_1 1.363(6) . ?
C9_1 C10_1 1.549(7) . ?
C10_1 F14_1 1.345(7) . ?
C10_1 F15_1 1.349(6) . ?
O1_2 C1_2 1.354(5) . ?
C1_2 C4_2 1.556(7) . ?
C1_2 C2_2 1.564(7) . ?
C1_2 C3_2 1.570(6) . ?
C2_2 F1_2 1.344(6) . ?
C2_2 F2_2 1.354(5) . ?
C2_2 C9_2 1.548(7) . ?
C3_2 F4_2 1.354(6) . ?
C3_2 F3_2 1.356(6) . ?
C3_2 C7_2 1.534(6) . ?
C4_2 F6_2 1.352(6) . ?
C4_2 F5_2 1.353(6) . ?
C4_2 C5_2 1.552(7) . ?
C5_2 F7_2 1.359(7) . ?
C5_2 C10_2 1.545(8) . ?
C5_2 C6_2 1.552(8) . ?
C6_2 F9_2 1.343(6) . ?
C6_2 F8_2 1.346(7) . ?
C6_2 C7_2 1.537(9) . ?
C7_2 F10_2 1.370(5) . ?
C7_2 C8_2 1.546(8) . ?
C8_2 F11_2 1.336(7) . ?
C8_2 F12_2 1.349(6) . ?
C8_2 C9_2 1.553(7) . ?
C9_2 F13_2 1.358(6) . ?
C9_2 C10_2 1.543(8) . ?
C10_2 F15_2 1.344(5) . ?
C10_2 F14_2 1.346(6) . ?
C1_10 C6_10 1.348(11) . ?
C1_10 C2_10 1.376(10) . ?
C1_10 F1_10 1.379(9) . ?
C2_10 F2_10 1.325(10) . ?
C2_10 C3_10 1.381(10) . ?
C3_10 C4_10 1.381(11) . ?
C3_10 H3_10 0.9500 . ?
C4_10 C5_10 1.381(11) . ?
C4_10 H4_10 0.9500 . ?
C5_10 C6_10 1.367(11) . ?
C5_10 H5_10 0.9500 . ?
C6_10 H6_10 0.9500 . ?
C1_20 F1_20 1.35(2) . ?
C1_20 C2_20 1.374(19) . ?
C1_20 C6_20 1.376(19) . ?
C2_20 F2_20 1.34(2) . ?
C2_20 C3_20 1.38(2) . ?
C3_20 C4_20 1.38(2) . ?
C3_20 H3_20 0.9500 . ?
C4_20 C5_20 1.37(2) . ?
C4_20 H4_20 0.9500 . ?
C5_20 C6_20 1.39(2) . ?
C5_20 H5_20 0.9500 . ?
C6_20 H6_20 0.9500 . ?
C1_11 F1_11 1.368(14) . ?
C1_11 C6_11 1.373(14) . ?
C1_11 C2_11 1.380(13) . ?
C2_11 F2_11 1.362(12) . ?
C2_11 C3_11 1.375(14) . ?
C3_11 C4_11 1.393(14) . ?
C3_11 H3_11 0.9500 . ?
C4_11 C5_11 1.391(14) . ?
C4_11 H4_11 0.9500 . ?
C5_11 C6_11 1.384(15) . ?
C5_11 H5_11 0.9500 . ?
C6_11 H6_11 0.9500 . ?
C1_19 F1_19 1.332(19) . ?
C1_19 C2_19 1.376(18) . ?
C1_19 C6_19 1.385(19) . ?
C2_19 F2_19 1.349(19) . ?
C2_19 C3_19 1.359(19) . ?
C3_19 C4_19 1.360(19) . ?
C3_19 H3_19 0.9500 . ?
C4_19 C5_19 1.398(19) . ?
C4_19 H4_19 0.9500 . ?
C5_19 C6_19 1.379(19) . ?
C5_19 H5_19 0.9500 . ?
C6_19 H6_19 0.9500 . ?
C1_8 F1_8 1.328(10) . ?
C1_8 C2_8 1.376(11) . ?
C1_8 C6_8 1.387(11) . ?
C2_8 F2_8 1.340(10) . ?
C2_8 C3_8 1.381(10) . ?
C3_8 C4_8 1.395(9) . ?
C3_8 H3_8 0.9500 . ?
C4_8 C5_8 1.386(11) . ?
C4_8 H4_8 0.9500 . ?
C5_8 C6_8 1.374(12) . ?
C5_8 H5_8 0.9500 . ?
C6_8 H6_8 0.9500 . ?
C1_21 F1_21 1.35(2) . ?
C1_21 C6_21 1.378(19) . ?
C1_21 C2_21 1.387(19) . ?
C2_21 F2_21 1.34(2) . ?
C2_21 C3_21 1.377(19) . ?
C3_21 C4_21 1.38(2) . ?
C3_21 H3_21 0.9500 . ?
C4_21 C5_21 1.38(2) . ?
C4_21 H4_21 0.9500 . ?
C5_21 C6_21 1.39(2) . ?
C5_21 H5_21 0.9500 . ?
C6_21 H6_21 0.9500 . ?
C1_9 F1_9 1.333(10) . ?
C1_9 C2_9 1.368(12) . ?
C1_9 C6_9 1.379(12) . ?
C2_9 F2_9 1.346(10) . ?
C2_9 C3_9 1.388(11) . ?
C3_9 C4_9 1.390(13) . ?
C3_9 H3_9 0.9500 . ?
C4_9 C5_9 1.387(14) . ?
C4_9 H4_9 0.9500 . ?
C5_9 C6_9 1.377(13) . ?
C5_9 H5_9 0.9500 . ?
C6_9 H6_9 0.9500 . ?
C1_18 F1_18 1.327(16) . ?
C1_18 C2_18 1.367(17) . ?
C1_18 C6_18 1.383(17) . ?
C2_18 F2_18 1.318(16) . ?
C2_18 C3_18 1.385(18) . ?
C3_18 C4_18 1.375(18) . ?
C3_18 H3_18 0.9500 . ?
C4_18 C5_18 1.378(16) . ?
C4_18 H4_18 0.9500 . ?
C5_18 C6_18 1.391(16) . ?
C5_18 H5_18 0.9500 . ?
C6_18 H6_18 0.9500 . ?
C1_7 F1_7 1.331(11) . ?
C1_7 C6_7 1.380(12) . ?
C1_7 C2_7 1.393(12) . ?
C2_7 F2_7 1.340(9) . ?
C2_7 C3_7 1.361(12) . ?
C3_7 C4_7 1.393(11) . ?
C3_7 H3_7 0.9500 . ?
C4_7 C5_7 1.391(11) . ?
C4_7 H4_7 0.9500 . ?
C5_7 C6_7 1.400(13) . ?
C5_7 H5_7 0.9500 . ?
C6_7 H6_7 0.9500 . ?
C1_22 F1_22 1.343(17) . ?
C1_22 C2_22 1.377(17) . ?
C1_22 C6_22 1.380(17) . ?
C2_22 F2_22 1.350(17) . ?
C2_22 C3_22 1.370(18) . ?
C3_22 C4_22 1.403(19) . ?
C3_22 H3_22 0.9500 . ?
C4_22 C5_22 1.376(18) . ?
C4_22 H4_22 0.9500 . ?
C5_22 C6_22 1.387(18) . ?
C5_22 H5_22 0.9500 . ?
C6_22 H6_22 0.9500 . ?
O1_5 C1_5 1.357(11) . ?
C1_5 C2_5 1.538(13) . ?
C1_5 C4_5 1.559(13) . ?
C1_5 C3_5 1.568(12) . ?
C2_5 F1_5 1.357(11) . ?
C2_5 F2_5 1.360(11) . ?
C2_5 C9_5 1.547(13) . ?
C3_5 F4_5 1.343(12) . ?
C3_5 F3_5 1.345(11) . ?
C3_5 C7_5 1.558(12) . ?
C4_5 F6_5 1.336(13) . ?
C4_5 F5_5 1.347(13) . ?
C4_5 C5_5 1.549(14) . ?
C5_5 F7_5 1.369(12) . ?
C5_5 C10_5 1.542(13) . ?
C5_5 C6_5 1.554(14) . ?
C6_5 F8_5 1.332(12) . ?
C6_5 F9_5 1.342(10) . ?
C6_5 C7_5 1.539(12) . ?
C7_5 F10_5 1.362(11) . ?
C7_5 C8_5 1.537(14) . ?
C8_5 F12_5 1.338(13) . ?
C8_5 F11_5 1.356(14) . ?
C8_5 C9_5 1.544(15) . ?
C9_5 F13_5 1.355(12) . ?
C9_5 C10_5 1.539(13) . ?
C10_5 F15_5 1.343(11) . ?
C10_5 F14_5 1.359(12) . ?
O1_12 C1_12 1.360(12) . ?
C1_12 C4_12 1.537(14) . ?
C1_12 C3_12 1.552(12) . ?
C1_12 C2_12 1.555(13) . ?
C2_12 F1_12 1.344(13) . ?
C2_12 F2_12 1.351(12) . ?
C2_12 C9_12 1.547(14) . ?
C3_12 F4_12 1.345(12) . ?
C3_12 F3_12 1.348(13) . ?
C3_12 C7_12 1.548(12) . ?
C4_12 F6_12 1.335(11) . ?
C4_12 F5_12 1.354(10) . ?
C4_12 C5_12 1.548(13) . ?
C5_12 F7_12 1.359(12) . ?
C5_12 C10_12 1.543(13) . ?
C5_12 C6_12 1.550(14) . ?
C6_12 F9_12 1.347(13) . ?
C6_12 F8_12 1.353(13) . ?
C6_12 C7_12 1.545(15) . ?
C7_12 F10_12 1.371(11) . ?
C7_12 C8_12 1.551(12) . ?
C8_12 F12_12 1.345(11) . ?
C8_12 F11_12 1.350(12) . ?
C8_12 C9_12 1.532(13) . ?
C9_12 F13_12 1.374(12) . ?
C9_12 C10_12 1.545(14) . ?
C10_12 F14_12 1.345(11) . ?
C10_12 F15_12 1.346(11) . ?
O1_4 C1_4 1.357(16) . ?
C1_4 C3_4 1.546(16) . ?
C1_4 C2_4 1.556(16) . ?
C1_4 C4_4 1.564(16) . ?
C2_4 F2_4 1.358(16) . ?
C2_4 F1_4 1.361(16) . ?
C2_4 C9_4 1.545(16) . ?
C3_4 F3_4 1.348(16) . ?
C3_4 F4_4 1.355(15) . ?
C3_4 C7_4 1.539(16) . ?
C4_4 F6_4 1.337(15) . ?
C4_4 F5_4 1.343(16) . ?
C4_4 C5_4 1.552(16) . ?
C5_4 F7_4 1.337(15) . ?
C5_4 C6_4 1.534(16) . ?
C5_4 C10_4 1.538(17) . ?
C6_4 F8_4 1.345(16) . ?
C6_4 F9_4 1.345(15) . ?
C6_4 C7_4 1.541(16) . ?
C7_4 F10_4 1.338(15) . ?
C7_4 C8_4 1.511(16) . ?
C8_4 F11_4 1.344(15) . ?
C8_4 F12_4 1.362(15) . ?
C8_4 C9_4 1.542(16) . ?
C9_4 F13_4 1.358(16) . ?
C9_4 C10_4 1.543(17) . ?
C10_4 F15_4 1.355(15) . ?
C10_4 F14_4 1.357(15) . ?
O1_6 C1_6 1.365(17) . ?
C1_6 C2_6 1.557(16) . ?
C1_6 C3_6 1.572(17) . ?
C1_6 C4_6 1.588(17) . ?
C2_6 F2_6 1.364(15) . ?
C2_6 F1_6 1.367(14) . ?
C2_6 C9_6 1.557(16) . ?
C3_6 F4_6 1.357(16) . ?
C3_6 F3_6 1.358(15) . ?
C3_6 C7_6 1.542(16) . ?
C4_6 F5_6 1.339(15) . ?
C4_6 F6_6 1.342(15) . ?
C4_6 C5_6 1.520(16) . ?
C5_6 F7_6 1.354(14) . ?
C5_6 C10_6 1.532(17) . ?
C5_6 C6_6 1.545(16) . ?
C6_6 F8_6 1.287(16) . ?
C6_6 F9_6 1.330(15) . ?
C6_6 C7_6 1.543(16) . ?
F9_6 F12_6 2.34(2) . ?
C7_6 F10_6 1.356(15) . ?
C7_6 C8_6 1.533(17) . ?
C8_6 F11_6 1.306(15) . ?
C8_6 F12_6 1.378(15) . ?
C8_6 C9_6 1.541(17) . ?
C9_6 F13_6 1.351(14) . ?
C9_6 C10_6 1.558(16) . ?
C10_6 F14_6 1.339(15) . ?
C10_6 F15_6 1.356(15) . ?
O1_3 C1_3 1.349(9) . ?
C1_3 C4_3 1.553(10) . ?
C1_3 C3_3 1.554(11) . ?
C1_3 C2_3 1.563(10) . ?
C2_3 F1_3 1.333(9) . ?
C2_3 F2_3 1.344(10) . ?
C2_3 C9_3 1.545(10) . ?
C3_3 F3_3 1.325(9) . ?
C3_3 F4_3 1.347(9) . ?
C3_3 C7_3 1.554(11) . ?
C4_3 F6_3 1.338(10) . ?
C4_3 F5_3 1.342(9) . ?
C4_3 C5_3 1.561(11) . ?
C5_3 F7_3 1.354(9) . ?
C5_3 C6_3 1.542(12) . ?
C5_3 C10_3 1.542(11) . ?
C6_3 F8_3 1.333(9) . ?
C6_3 F9_3 1.344(10) . ?
C6_3 C7_3 1.546(12) . ?
C7_3 F10_3 1.349(10) . ?
C7_3 C8_3 1.547(10) . ?
C8_3 F12_3 1.335(8) . ?
C8_3 F11_3 1.359(9) . ?
C8_3 C9_3 1.547(10) . ?
C9_3 F13_3 1.360(8) . ?
C9_3 C10_3 1.549(10) . ?
C10_3 F14_3 1.343(10) . ?
C10_3 F15_3 1.351(9) . ?
O1_15 C1_15 1.361(16) . ?
C1_15 C4_15 1.543(16) . ?
C1_15 C3_15 1.545(16) . ?
C1_15 C2_15 1.557(16) . ?
C2_15 F1_15 1.348(15) . ?
C2_15 F2_15 1.353(15) . ?
C2_15 C9_15 1.536(17) . ?
C3_15 F4_15 1.342(16) . ?
C3_15 F3_15 1.347(15) . ?
C3_15 C7_15 1.541(16) . ?
C4_15 F6_15 1.345(15) . ?
C4_15 F5_15 1.359(15) . ?
C4_15 C5_15 1.546(17) . ?
C5_15 F7_15 1.354(15) . ?
C5_15 C10_15 1.532(16) . ?
C5_15 C6_15 1.536(16) . ?
C6_15 F8_15 1.347(15) . ?
C6_15 F9_15 1.360(14) . ?
C6_15 C7_15 1.549(16) . ?
C7_15 F10_15 1.366(14) . ?
C7_15 C8_15 1.553(16) . ?
C8_15 F11_15 1.343(15) . ?
C8_15 F12_15 1.353(15) . ?
C8_15 C9_15 1.535(17) . ?
C9_15 F13_15 1.351(15) . ?
C9_15 C10_15 1.548(16) . ?
C10_15 F14_15 1.333(15) . ?
C10_15 F15_15 1.353(15) . ?
O1_16 C1_16 1.343(12) . ?
C1_16 C3_16 1.553(13) . ?
C1_16 C2_16 1.554(13) . ?
C1_16 C4_16 1.559(13) . ?
C2_16 F1_16 1.339(11) . ?
C2_16 F2_16 1.355(11) . ?
C2_16 C9_16 1.560(12) . ?
C3_16 F3_16 1.350(12) . ?
C3_16 F4_16 1.352(11) . ?
C3_16 C7_16 1.567(13) . ?
C4_16 F5_16 1.348(11) . ?
C4_16 F6_16 1.346(11) . ?
C4_16 C5_16 1.570(13) . ?
C5_16 F7_16 1.351(12) . ?
C5_16 C6_16 1.498(14) . ?
C5_16 C10_16 1.539(13) . ?
C6_16 F8_16 1.343(12) . ?
C6_16 F9_16 1.347(12) . ?
C6_16 C7_16 1.552(15) . ?
C7_16 F10_16 1.360(12) . ?
C7_16 C8_16 1.535(14) . ?
C8_16 F12_16 1.346(11) . ?
C8_16 F11_16 1.357(12) . ?
C8_16 C9_16 1.548(13) . ?
C9_16 F13_16 1.356(11) . ?
C9_16 C10_16 1.533(13) . ?
C10_16 F14_16 1.345(12) . ?
C10_16 F15_16 1.360(11) . ?
O1_14 C1_14 1.354(16) . ?
C1_14 C2_14 1.546(16) . ?
C1_14 C4_14 1.555(16) . ?
C1_14 C3_14 1.573(17) . ?
C2_14 F1_14 1.339(15) . ?
C2_14 F2_14 1.374(15) . ?
C2_14 C9_14 1.573(16) . ?
C3_14 F3_14 1.342(15) . ?
C3_14 F4_14 1.349(14) . ?
C3_14 C7_14 1.537(16) . ?
C4_14 F6_14 1.305(15) . ?
C4_14 F5_14 1.351(15) . ?
C4_14 C5_14 1.566(16) . ?
C5_14 F7_14 1.359(15) . ?
C5_14 C6_14 1.554(16) . ?
C5_14 C10_14 1.552(16) . ?
C6_14 F8_14 1.348(14) . ?
C6_14 F9_14 1.340(14) . ?
C6_14 C7_14 1.552(17) . ?
C7_14 F10_14 1.357(16) . ?
C7_14 C8_14 1.541(16) . ?
C8_14 F12_14 1.371(14) . ?
C8_14 F11_14 1.382(15) . ?
C8_14 C9_14 1.548(16) . ?
C9_14 F13_14 1.360(13) . ?
C9_14 C10_14 1.581(16) . ?
C10_14 F15_14 1.351(15) . ?
C10_14 F14_14 1.389(15) . ?
O1_17 C1_17 1.346(15) . ?
C1_17 C3_17 1.548(15) . ?
C1_17 C2_17 1.549(16) . ?
C1_17 C4_17 1.559(15) . ?
C2_17 F1_17 1.340(15) . ?
C2_17 F2_17 1.353(14) . ?
C2_17 C9_17 1.538(16) . ?
C3_17 F4_17 1.313(15) . ?
C3_17 F3_17 1.346(15) . ?
C3_17 C7_17 1.543(15) . ?
C4_17 F5_17 1.342(14) . ?
C4_17 F6_17 1.361(15) . ?
C4_17 C5_17 1.543(15) . ?
C5_17 F7_17 1.354(15) . ?
C5_17 C10_17 1.540(16) . ?
C5_17 C6_17 1.545(16) . ?
C6_17 F9_17 1.349(15) . ?
C6_17 F8_17 1.348(15) . ?
C6_17 C7_17 1.530(16) . ?
C7_17 F10_17 1.351(14) . ?
C7_17 C8_17 1.527(16) . ?
C8_17 F11_17 1.354(15) . ?
C8_17 F12_17 1.361(15) . ?
C8_17 C9_17 1.532(16) . ?
C9_17 F13_17 1.354(14) . ?
C9_17 C10_17 1.544(16) . ?
C10_17 F14_17 1.343(15) . ?
C10_17 F15_17 1.349(15) . ?
O1_13 C1_13 1.363(13) . ?
C1_13 C2_13 1.542(14) . ?
C1_13 C4_13 1.553(14) . ?
C1_13 C3_13 1.559(14) . ?
C2_13 F2_13 1.344(14) . ?
C2_13 F1_13 1.364(14) . ?
C2_13 C9_13 1.563(14) . ?
C3_13 F3_13 1.349(15) . ?
C3_13 F4_13 1.357(14) . ?
C3_13 C7_13 1.542(14) . ?
C4_13 F5_13 1.331(13) . ?
C4_13 F6_13 1.361(14) . ?
C4_13 C5_13 1.534(14) . ?
C5_13 F7_13 1.344(13) . ?
C5_13 C6_13 1.512(15) . ?
C5_13 C10_13 1.543(14) . ?
C6_13 F8_13 1.347(13) . ?
C6_13 F9_13 1.360(13) . ?
C6_13 C7_13 1.535(15) . ?
C7_13 F10_13 1.362(13) . ?
C7_13 C8_13 1.535(15) . ?
C8_13 F11_13 1.338(13) . ?
C8_13 F12_13 1.341(13) . ?
C8_13 C9_13 1.543(15) . ?
C9_13 F13_13 1.357(12) . ?
C9_13 C10_13 1.540(14) . ?
C10_13 F14_13 1.342(13) . ?
C10_13 F15_13 1.362(13) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C4_22 Ag1A O1_2 153.7(7) . . ?
O1_2 Ag1A C5_7 162.3(3) . . ?
C4_22 Ag1A O1_1 137.1(7) . . ?
O1_2 Ag1A O1_1 69.02(11) . . ?
C5_7 Ag1A O1_1 128.3(3) . . ?
O1_2 Ag1A C4_7 128.9(3) . . ?
C5_7 Ag1A C4_7 33.5(3) . . ?
O1_1 Ag1A C4_7 156.4(3) . . ?
C4_22 Ag1A C5_22 30.5(5) . . ?
O1_2 Ag1A C5_22 123.2(5) . . ?
O1_1 Ag1A C5_22 166.8(6) . . ?
C4_22 Ag1A C3_22 30.1(6) . . ?
O1_2 Ag1A C3_22 153.3(6) . . ?
O1_1 Ag1A C3_22 120.0(6) . . ?
C5_22 Ag1A C3_22 52.0(6) . . ?
O1_2 Ag1A C6_7 153.8(3) . . ?
C5_7 Ag1A C6_7 26.3(3) . . ?
O1_1 Ag1A C6_7 121.7(3) . . ?
C4_7 Ag1A C6_7 50.6(4) . . ?
O1_1 Ag1B O1_2 73.0(4) . . ?
O1_1 Ag1B F1_10 114.2(10) . . ?
O1_2 Ag1B F1_10 105.9(8) . . ?
O1_1 Ag1B C4_22 128.9(9) . . ?
O1_2 Ag1B C4_22 135.2(12) . . ?
O1_1 Ag1B C5_7 122.1(7) . . ?
O1_2 Ag1B C5_7 140.6(11) . . ?
O1_1 Ag1B C3_22 126.5(7) . . ?
O1_2 Ag1B C3_22 159.4(9) . . ?
C4_22 Ag1B C3_22 29.8(6) . . ?
O1_1 Ag1B C4_7 136.6(10) . . ?
O1_2 Ag1B C4_7 113.8(8) . . ?
C5_7 Ag1B C4_7 28.9(3) . . ?
O1_1 Ag1B C5_22 147.0(11) . . ?
O1_2 Ag1B C5_22 112.2(8) . . ?
C4_22 Ag1B C5_22 26.7(5) . . ?
C3_22 Ag1B C5_22 48.4(7) . . ?
O1_1 Ag1B C6_7 127.5(5) . . ?
O1_2 Ag1B C6_7 158.3(7) . . ?
C5_7 Ag1B C6_7 27.1(3) . . ?
C4_7 Ag1B C6_7 47.9(4) . . ?
C5_21 Ag2A O1_1 157.3(17) . . ?
C5_21 Ag2A O1_2 131.9(17) . . ?
O1_1 Ag2A O1_2 69.32(10) . . ?
O1_1 Ag2A C4_8 161.8(3) . . ?
O1_2 Ag2A C4_8 128.7(3) . . ?
O1_1 Ag2A C3_8 128.4(3) . . ?
O1_2 Ag2A C3_8 160.2(3) . . ?
C4_8 Ag2A C3_8 33.4(3) . . ?
C5_21 Ag2A C4_21 32.5(13) . . ?
O1_1 Ag2A C4_21 125.1(17) . . ?
O1_2 Ag2A C4_21 162.6(19) . . ?
C5_21 Ag2A C6_21 27.5(13) . . ?
O1_1 Ag2A C6_21 159.0(10) . . ?
O1_2 Ag2A C6_21 119.5(12) . . ?
C4_21 Ag2A C6_21 51.2(15) . . ?
O1_1 Ag2A C5_8 154.4(3) . . ?
O1_2 Ag2A C5_8 118.5(3) . . ?
C4_8 Ag2A C5_8 26.5(3) . . ?
C3_8 Ag2A C5_8 50.5(3) . . ?
O1_1 Ag2A C2_8 113.5(3) . . ?
O1_2 Ag2A C2_8 166.7(2) . . ?
C4_8 Ag2A C2_8 49.7(3) . . ?
C3_8 Ag2A C2_8 25.5(3) . . ?
C5_8 Ag2A C2_8 53.3(3) . . ?
C5_21 Ag2A C3_21 47.9(15) . . ?
O1_1 Ag2A C3_21 113.7(13) . . ?
O1_2 Ag2A C3_21 166.9(10) . . ?
C4_21 Ag2A C3_21 24.4(10) . . ?
C6_21 Ag2A C3_21 53.3(12) . . ?
F2_19 Ag2B O1_1 106.2(19) . . ?
F2_11 Ag2B O1_1 100.5(8) . . ?
C5_21 Ag2B O1_1 133.1(13) . . ?
O1_1 Ag2B C4_8 138.9(8) . . ?
O1_1 Ag2B C3_8 118.4(6) . . ?
C4_8 Ag2B C3_8 32.4(3) . . ?
C5_21 Ag2B C6_21 30.5(10) . . ?
O1_1 Ag2B C6_21 162.9(13) . . ?
C5_21 Ag2B C4_21 31.4(12) . . ?
O1_1 Ag2B C4_21 115.7(15) . . ?
C6_21 Ag2B C4_21 53.1(17) . . ?
O1_1 Ag2B C5_8 168.8(8) . . ?
C4_8 Ag2B C5_8 30.1(3) . . ?
C3_8 Ag2B C5_8 53.9(4) . . ?
O1_1 Ag2B C2_8 118.8(5) . . ?
C4_8 Ag2B C2_8 53.6(4) . . ?
C3_8 Ag2B C2_8 29.5(3) . . ?
C5_8 Ag2B C2_8 59.3(4) . . ?
C5_21 Ag2B C3_21 52.2(15) . . ?
O1_1 Ag2B C3_21 119.0(11) . . ?
C6_21 Ag2B C3_21 58.6(15) . . ?
C4_21 Ag2B C3_21 28.2(9) . . ?
C4_18 Ag3A O1_2 162.9(6) . . ?
C5_9 Ag3A O1_2 153.5(4) . . ?
C4_18 Ag3A O1_1 125.4(5) . . ?
C5_9 Ag3A O1_1 133.4(4) . . ?
O1_2 Ag3A O1_1 69.23(13) . . ?
C4_18 Ag3A C5_18 33.9(5) . . ?
O1_2 Ag3A C5_18 129.0(5) . . ?
O1_1 Ag3A C5_18 149.5(5) . . ?
C5_9 Ag3A C6_9 30.7(3) . . ?
O1_2 Ag3A C6_9 123.7(3) . . ?
O1_1 Ag3A C6_9 160.7(3) . . ?
C5_9 Ag3A C4_9 29.8(4) . . ?
O1_2 Ag3A C4_9 160.7(3) . . ?
O1_1 Ag3A C4_9 121.2(3) . . ?
C6_9 Ag3A C4_9 51.8(4) . . ?
C4_18 Ag3A C3_18 24.9(6) . . ?
O1_2 Ag3A C3_18 158.1(5) . . ?
O1_1 Ag3A C3_18 123.7(5) . . ?
C5_18 Ag3A C3_18 50.1(6) . . ?
C4_18 Ag3A C6_18 49.1(6) . . ?
O1_2 Ag3A C6_18 115.7(4) . . ?
O1_1 Ag3A C6_18 173.7(4) . . ?
C5_18 Ag3A C6_18 24.3(5) . . ?
C3_18 Ag3A C6_18 53.2(5) . . ?
O1_1 Ag3B C4_18 127.4(11) . . ?
O1_1 Ag3B O1_2 69.3(6) . . ?
C4_18 Ag3B O1_2 150.1(17) . . ?
O1_1 Ag3B C5_9 133.8(11) . . ?
O1_2 Ag3B C5_9 141.4(16) . . ?
O1_1 Ag3B C5_18 143.0(13) . . ?
C4_18 Ag3B C5_18 32.2(6) . . ?
O1_2 Ag3B C5_18 118.6(14) . . ?
O1_1 Ag3B C4_9 128.2(11) . . ?
O1_2 Ag3B C4_9 162.2(11) . . ?
C5_9 Ag3B C4_9 30.9(5) . . ?
O1_1 Ag3B C6_9 153.6(13) . . ?
O1_2 Ag3B C6_9 115.3(12) . . ?
C5_9 Ag3B C6_9 28.9(5) . . ?
C4_9 Ag3B C6_9 51.2(5) . . ?
O1_1 Ag3B C3_18 130.8(12) . . ?
C4_18 Ag3B C3_18 26.6(7) . . ?
O1_2 Ag3B C3_18 159.4(11) . . ?
C5_18 Ag3B C3_18 50.4(7) . . ?
O1_1 Ag3B C6_18 165.0(14) . . ?
C4_18 Ag3B C6_18 47.1(7) . . ?
O1_2 Ag3B C6_18 109.6(10) . . ?
C5_18 Ag3B C6_18 23.7(5) . . ?
C3_18 Ag3B C6_18 52.6(6) . . ?
O1_14 Al1 O1_12 107.2(7) . . ?
O1_3 Al1 O1_6 117.3(8) . . ?
O1_3 Al1 O1_4 91.2(5) . . ?
O1_6 Al1 O1_4 120.8(9) . . ?
O1_3 Al1 O1_5 113.4(4) . . ?
O1_6 Al1 O1_5 119.4(7) . . ?
O1_4 Al1 O1_5 88.0(7) . . ?
O1_17 Al1 O1_16 128.8(6) . . ?
O1_14 Al1 O1_13 78.5(7) . . ?
O1_12 Al1 O1_13 138.7(5) . . ?
O1_14 Al1 O1_15 104.9(7) . . ?
O1_12 Al1 O1_15 116.6(6) . . ?
O1_13 Al1 O1_15 100.2(6) . . ?
C1_1 O1_1 Ag1B 125.5(5) . . ?
C1_1 O1_1 Ag3B 122.3(7) . . ?
C1_1 O1_1 Ag2A 125.9(3) . . ?
C1_1 O1_1 Ag1A 124.6(3) . . ?
C1_1 O1_1 Ag3A 124.7(3) . . ?
C1_1 O1_1 Ag2B 118.0(4) . . ?
O1_1 C1_1 C2_1 112.1(4) . . ?
O1_1 C1_1 C3_1 112.6(4) . . ?
C2_1 C1_1 C3_1 107.1(4) . . ?
O1_1 C1_1 C4_1 111.1(3) . . ?
C2_1 C1_1 C4_1 106.6(4) . . ?
C3_1 C1_1 C4_1 107.0(4) . . ?
F2_1 C2_1 F1_1 105.0(4) . . ?
F2_1 C2_1 C9_1 109.7(4) . . ?
F1_1 C2_1 C9_1 109.5(4) . . ?
F2_1 C2_1 C1_1 109.8(4) . . ?
F1_1 C2_1 C1_1 109.6(4) . . ?
C9_1 C2_1 C1_1 112.9(4) . . ?
F3_1 C3_1 F4_1 105.9(4) . . ?
F3_1 C3_1 C1_1 110.2(4) . . ?
F4_1 C3_1 C1_1 110.0(4) . . ?
F3_1 C3_1 C7_1 109.3(4) . . ?
F4_1 C3_1 C7_1 109.6(4) . . ?
C1_1 C3_1 C7_1 111.6(4) . . ?
F5_1 C4_1 F6_1 105.1(3) . . ?
F5_1 C4_1 C5_1 109.9(4) . . ?
F6_1 C4_1 C5_1 109.0(4) . . ?
F5_1 C4_1 C1_1 110.2(4) . . ?
F6_1 C4_1 C1_1 110.0(4) . . ?
C5_1 C4_1 C1_1 112.4(3) . . ?
F7_1 C5_1 C10_1 110.0(5) . . ?
F7_1 C5_1 C6_1 108.7(5) . . ?
C10_1 C5_1 C6_1 110.3(4) . . ?
F7_1 C5_1 C4_1 109.8(4) . . ?
C10_1 C5_1 C4_1 109.5(5) . . ?
C6_1 C5_1 C4_1 108.5(5) . . ?
F8_1 C6_1 F9_1 106.4(5) . . ?
F8_1 C6_1 C5_1 110.9(5) . . ?
F9_1 C6_1 C5_1 110.2(5) . . ?
F8_1 C6_1 C7_1 110.8(5) . . ?
F9_1 C6_1 C7_1 109.3(4) . . ?
C5_1 C6_1 C7_1 109.2(4) . . ?
F10_1 C7_1 C8_1 109.9(4) . . ?
F10_1 C7_1 C6_1 109.5(5) . . ?
C8_1 C7_1 C6_1 109.6(5) . . ?
F10_1 C7_1 C3_1 109.5(5) . . ?
C8_1 C7_1 C3_1 109.5(4) . . ?
C6_1 C7_1 C3_1 108.8(4) . . ?
F11_1 C8_1 F12_1 105.7(4) . . ?
F11_1 C8_1 C9_1 111.0(5) . . ?
F12_1 C8_1 C9_1 111.3(5) . . ?
F11_1 C8_1 C7_1 109.5(5) . . ?
F12_1 C8_1 C7_1 109.3(5) . . ?
C9_1 C8_1 C7_1 109.8(4) . . ?
F13_1 C9_1 C8_1 108.9(4) . . ?
F13_1 C9_1 C2_1 110.4(4) . . ?
C8_1 C9_1 C2_1 109.4(4) . . ?
F13_1 C9_1 C10_1 109.7(5) . . ?
C8_1 C9_1 C10_1 109.8(5) . . ?
C2_1 C9_1 C10_1 108.6(4) . . ?
F14_1 C10_1 F15_1 105.6(4) . . ?
F14_1 C10_1 C5_1 111.1(4) . . ?
F15_1 C10_1 C5_1 110.5(5) . . ?
F14_1 C10_1 C9_1 110.2(5) . . ?
F15_1 C10_1 C9_1 109.9(4) . . ?
C5_1 C10_1 C9_1 109.6(4) . . ?
C1_2 O1_2 Ag1B 127.0(5) . . ?
C1_2 O1_2 Ag3A 123.5(3) . . ?
C1_2 O1_2 Ag1A 123.3(3) . . ?
C1_2 O1_2 Ag2A 125.6(3) . . ?
C1_2 O1_2 Ag3B 126.2(7) . . ?
O1_2 C1_2 C4_2 111.9(4) . . ?
O1_2 C1_2 C2_2 111.6(4) . . ?
C4_2 C1_2 C2_2 107.0(4) . . ?
O1_2 C1_2 C3_2 112.3(3) . . ?
C4_2 C1_2 C3_2 107.0(4) . . ?
C2_2 C1_2 C3_2 106.7(4) . . ?
F1_2 C2_2 F2_2 105.2(4) . . ?
F1_2 C2_2 C9_2 109.9(4) . . ?
F2_2 C2_2 C9_2 109.5(4) . . ?
F1_2 C2_2 C1_2 110.0(4) . . ?
F2_2 C2_2 C1_2 109.6(4) . . ?
C9_2 C2_2 C1_2 112.4(4) . . ?
F4_2 C3_2 F3_2 104.9(4) . . ?
F4_2 C3_2 C7_2 110.2(4) . . ?
F3_2 C3_2 C7_2 110.3(4) . . ?
F4_2 C3_2 C1_2 109.3(4) . . ?
F3_2 C3_2 C1_2 109.9(4) . . ?
C7_2 C3_2 C1_2 112.0(4) . . ?
F6_2 C4_2 F5_2 105.4(4) . . ?
F6_2 C4_2 C5_2 109.3(4) . . ?
F5_2 C4_2 C5_2 109.5(4) . . ?
F6_2 C4_2 C1_2 110.1(4) . . ?
F5_2 C4_2 C1_2 110.0(4) . . ?
C5_2 C4_2 C1_2 112.3(4) . . ?
F7_2 C5_2 C10_2 109.7(5) . . ?
F7_2 C5_2 C6_2 109.8(5) . . ?
C10_2 C5_2 C6_2 109.6(5) . . ?
F7_2 C5_2 C4_2 109.7(5) . . ?
C10_2 C5_2 C4_2 109.3(5) . . ?
C6_2 C5_2 C4_2 108.7(4) . . ?
F9_2 C6_2 F8_2 106.3(5) . . ?
F9_2 C6_2 C7_2 110.1(5) . . ?
F8_2 C6_2 C7_2 110.4(5) . . ?
F9_2 C6_2 C5_2 110.1(5) . . ?
F8_2 C6_2 C5_2 110.3(5) . . ?
C7_2 C6_2 C5_2 109.5(4) . . ?
F10_2 C7_2 C3_2 109.9(4) . . ?
F10_2 C7_2 C6_2 109.4(5) . . ?
C3_2 C7_2 C6_2 109.7(5) . . ?
F10_2 C7_2 C8_2 108.7(5) . . ?
C3_2 C7_2 C8_2 109.2(5) . . ?
C6_2 C7_2 C8_2 109.9(4) . . ?
F11_2 C8_2 F12_2 106.4(5) . . ?
F11_2 C8_2 C7_2 110.4(5) . . ?
F12_2 C8_2 C7_2 110.2(5) . . ?
F11_2 C8_2 C9_2 110.4(5) . . ?
F12_2 C8_2 C9_2 109.8(4) . . ?
C7_2 C8_2 C9_2 109.5(4) . . ?
F13_2 C9_2 C10_2 109.9(4) . . ?
F13_2 C9_2 C2_2 110.1(4) . . ?
C10_2 C9_2 C2_2 109.3(4) . . ?
F13_2 C9_2 C8_2 109.4(5) . . ?
C10_2 C9_2 C8_2 109.6(5) . . ?
C2_2 C9_2 C8_2 108.5(4) . . ?
F15_2 C10_2 F14_2 105.8(4) . . ?
F15_2 C10_2 C9_2 110.6(5) . . ?
F14_2 C10_2 C9_2 110.2(5) . . ?
F15_2 C10_2 C5_2 110.1(5) . . ?
F14_2 C10_2 C5_2 110.3(5) . . ?
C9_2 C10_2 C5_2 109.8(4) . . ?
C6_10 C1_10 C2_10 121.8(8) . . ?
C6_10 C1_10 F1_10 122.1(8) . . ?
C2_10 C1_10 F1_10 116.1(8) . . ?
F2_10 C2_10 C1_10 121.2(8) . . ?
F2_10 C2_10 C3_10 119.6(8) . . ?
C1_10 C2_10 C3_10 119.2(8) . . ?
C4_10 C3_10 C2_10 119.1(8) . . ?
C4_10 C3_10 H3_10 120.4 . . ?
C2_10 C3_10 H3_10 120.4 . . ?
C3_10 C4_10 C5_10 120.1(9) . . ?
C3_10 C4_10 H4_10 120.0 . . ?
C5_10 C4_10 H4_10 120.0 . . ?
C6_10 C5_10 C4_10 120.3(9) . . ?
C6_10 C5_10 H5_10 119.8 . . ?
C4_10 C5_10 H5_10 119.8 . . ?
C1_10 C6_10 C5_10 119.4(9) . . ?
C1_10 C6_10 H6_10 120.3 . . ?
C5_10 C6_10 H6_10 120.3 . . ?
C1_10 F1_10 Ag1B 145.6(8) . . ?
F1_20 C1_20 C2_20 118(2) . . ?
F1_20 C1_20 C6_20 122(3) . . ?
C2_20 C1_20 C6_20 121(2) . . ?
F2_20 C2_20 C1_20 124(3) . . ?
F2_20 C2_20 C3_20 115(2) . . ?
C1_20 C2_20 C3_20 121(2) . . ?
C4_20 C3_20 C2_20 119(3) . . ?
C4_20 C3_20 H3_20 120.7 . . ?
C2_20 C3_20 H3_20 120.7 . . ?
C5_20 C4_20 C3_20 120(3) . . ?
C5_20 C4_20 H4_20 119.8 . . ?
C3_20 C4_20 H4_20 119.8 . . ?
C4_20 C5_20 C6_20 121(3) . . ?
C4_20 C5_20 H5_20 119.5 . . ?
C6_20 C5_20 H5_20 119.5 . . ?
C1_20 C6_20 C5_20 118(3) . . ?
C1_20 C6_20 H6_20 120.8 . . ?
C5_20 C6_20 H6_20 120.8 . . ?
F1_11 C1_11 C6_11 123.7(12) . . ?
F1_11 C1_11 C2_11 116.6(12) . . ?
C6_11 C1_11 C2_11 119.6(12) . . ?
F2_11 C2_11 C3_11 119.7(13) . . ?
F2_11 C2_11 C1_11 119.3(13) . . ?
C3_11 C2_11 C1_11 121.0(11) . . ?
C2_11 C3_11 C4_11 120.3(13) . . ?
C2_11 C3_11 H3_11 119.8 . . ?
C4_11 C3_11 H3_11 119.8 . . ?
C5_11 C4_11 C3_11 117.9(13) . . ?
C5_11 C4_11 H4_11 121.0 . . ?
C3_11 C4_11 H4_11 121.0 . . ?
C6_11 C5_11 C4_11 121.5(13) . . ?
C6_11 C5_11 H5_11 119.2 . . ?
C4_11 C5_11 H5_11 119.2 . . ?
C1_11 C6_11 C5_11 119.6(12) . . ?
C1_11 C6_11 H6_11 120.2 . . ?
C5_11 C6_11 H6_11 120.2 . . ?
C2_11 F2_11 Ag2B 145.0(15) . . ?
F1_19 C1_19 C2_19 117(2) . . ?
F1_19 C1_19 C6_19 122(2) . . ?
C2_19 C1_19 C6_19 122(2) . . ?
F2_19 C2_19 C3_19 121(3) . . ?
F2_19 C2_19 C1_19 122(3) . . ?
C3_19 C2_19 C1_19 117(2) . . ?
C2_19 C3_19 C4_19 123(2) . . ?
C2_19 C3_19 H3_19 118.5 . . ?
C4_19 C3_19 H3_19 118.5 . . ?
C3_19 C4_19 C5_19 120(2) . . ?
C3_19 C4_19 H4_19 120.0 . . ?
C5_19 C4_19 H4_19 120.0 . . ?
C6_19 C5_19 C4_19 118(2) . . ?
C6_19 C5_19 H5_19 121.1 . . ?
C4_19 C5_19 H5_19 121.1 . . ?
C5_19 C6_19 C1_19 120(2) . . ?
C5_19 C6_19 H6_19 120.0 . . ?
C1_19 C6_19 H6_19 120.0 . . ?
C2_19 F2_19 Ag2B 155(4) . . ?
F1_8 C1_8 C2_8 118.9(9) . . ?
F1_8 C1_8 C6_8 121.8(9) . . ?
C2_8 C1_8 C6_8 119.3(8) . . ?
F2_8 C2_8 C1_8 118.5(9) . . ?
F2_8 C2_8 C3_8 120.5(9) . . ?
C1_8 C2_8 C3_8 121.0(7) . . ?
F2_8 C2_8 Ag2B 124.2(9) . . ?
C1_8 C2_8 Ag2B 86.5(6) . . ?
C3_8 C2_8 Ag2B 63.4(7) . . ?
F2_8 C2_8 Ag2A 121.6(8) . . ?
C1_8 C2_8 Ag2A 100.3(6) . . ?
C3_8 C2_8 Ag2A 49.5(6) . . ?
C2_8 C3_8 C4_8 119.9(8) . . ?
C2_8 C3_8 Ag2A 105.0(7) . . ?
C4_8 C3_8 Ag2A 71.9(7) . . ?
C2_8 C3_8 Ag2B 87.1(8) . . ?
C4_8 C3_8 Ag2B 73.4(7) . . ?
C2_8 C3_8 H3_8 120.1 . . ?
C4_8 C3_8 H3_8 120.1 . . ?
Ag2A C3_8 H3_8 93.0 . . ?
Ag2B C3_8 H3_8 109.7 . . ?
C5_8 C4_8 C3_8 118.7(8) . . ?
C5_8 C4_8 Ag2A 102.6(9) . . ?
C3_8 C4_8 Ag2A 74.7(7) . . ?
C5_8 C4_8 Ag2B 85.3(9) . . ?
C3_8 C4_8 Ag2B 74.2(8) . . ?
C5_8 C4_8 H4_8 120.6 . . ?
C3_8 C4_8 H4_8 120.6 . . ?
Ag2A C4_8 H4_8 92.6 . . ?
Ag2B C4_8 H4_8 110.3 . . ?
C6_8 C5_8 C4_8 121.0(8) . . ?
C6_8 C5_8 Ag2B 87.5(8) . . ?
C4_8 C5_8 Ag2B 64.6(8) . . ?
C6_8 C5_8 Ag2A 102.2(8) . . ?
C4_8 C5_8 Ag2A 50.9(7) . . ?
C6_8 C5_8 H5_8 119.5 . . ?
C4_8 C5_8 H5_8 119.5 . . ?
Ag2B C5_8 H5_8 118.6 . . ?
Ag2A C5_8 H5_8 115.2 . . ?
C5_8 C6_8 C1_8 120.1(9) . . ?
C5_8 C6_8 H6_8 119.9 . . ?
C1_8 C6_8 H6_8 119.9 . . ?
F1_21 C1_21 C6_21 124(3) . . ?
F1_21 C1_21 C2_21 117(3) . . ?
C6_21 C1_21 C2_21 119(2) . . ?
F2_21 C2_21 C3_21 118(3) . . ?
F2_21 C2_21 C1_21 120(3) . . ?
C3_21 C2_21 C1_21 121(2) . . ?
C4_21 C3_21 C2_21 119(2) . . ?
C4_21 C3_21 Ag2B 64(3) . . ?
C2_21 C3_21 Ag2B 85(2) . . ?
C4_21 C3_21 Ag2A 50(3) . . ?
C2_21 C3_21 Ag2A 97(2) . . ?
C4_21 C3_21 H3_21 120.3 . . ?
C2_21 C3_21 H3_21 120.3 . . ?
Ag2B C3_21 H3_21 120.8 . . ?
Ag2A C3_21 H3_21 120.5 . . ?
C3_21 C4_21 C5_21 120(2) . . ?
C3_21 C4_21 Ag2A 106(4) . . ?
C5_21 C4_21 Ag2A 63(4) . . ?
C3_21 C4_21 Ag2B 88(4) . . ?
C5_21 C4_21 Ag2B 67(4) . . ?
C3_21 C4_21 H4_21 120.0 . . ?
C5_21 C4_21 H4_21 120.0 . . ?
Ag2A C4_21 H4_21 100.9 . . ?
Ag2B C4_21 H4_21 116.0 . . ?
C6_21 C5_21 C4_21 120(2) . . ?
C6_21 C5_21 Ag2A 103(5) . . ?
C4_21 C5_21 Ag2A 85(4) . . ?
C6_21 C5_21 Ag2B 87(4) . . ?
C4_21 C5_21 Ag2B 82(4) . . ?
C6_21 C5_21 H5_21 120.1 . . ?
C4_21 C5_21 H5_21 120.1 . . ?
Ag2A C5_21 H5_21 82.6 . . ?
Ag2B C5_21 H5_21 101.6 . . ?
C1_21 C6_21 C5_21 120(2) . . ?
C1_21 C6_21 Ag2B 90(3) . . ?
C5_21 C6_21 Ag2B 63(4) . . ?
C1_21 C6_21 Ag2A 105(3) . . ?
C5_21 C6_21 Ag2A 50(4) . . ?
C1_21 C6_21 H6_21 119.9 . . ?
C5_21 C6_21 H6_21 119.9 . . ?
Ag2B C6_21 H6_21 117.6 . . ?
Ag2A C6_21 H6_21 112.6 . . ?
F1_9 C1_9 C2_9 118.7(10) . . ?
F1_9 C1_9 C6_9 120.3(11) . . ?
C2_9 C1_9 C6_9 121.0(8) . . ?
F2_9 C2_9 C1_9 118.4(9) . . ?
F2_9 C2_9 C3_9 120.5(9) . . ?
C1_9 C2_9 C3_9 121.1(8) . . ?
C2_9 C3_9 C4_9 117.7(10) . . ?
C2_9 C3_9 H3_9 121.1 . . ?
C4_9 C3_9 H3_9 121.1 . . ?
C5_9 C4_9 C3_9 120.9(11) . . ?
C5_9 C4_9 Ag3B 62.0(12) . . ?
C3_9 C4_9 Ag3B 110.0(10) . . ?
C5_9 C4_9 Ag3A 56.0(9) . . ?
C3_9 C4_9 Ag3A 112.1(9) . . ?
C5_9 C4_9 H4_9 119.5 . . ?
C3_9 C4_9 H4_9 119.5 . . ?
Ag3B C4_9 H4_9 97.5 . . ?
Ag3A C4_9 H4_9 100.7 . . ?
C6_9 C5_9 C4_9 120.2(11) . . ?
C6_9 C5_9 Ag3A 90.5(10) . . ?
C4_9 C5_9 Ag3A 94.2(11) . . ?
C6_9 C5_9 Ag3B 94.4(12) . . ?
C4_9 C5_9 Ag3B 87.1(13) . . ?
C6_9 C5_9 H5_9 119.9 . . ?
C4_9 C5_9 H5_9 119.9 . . ?
Ag3A C5_9 H5_9 85.4 . . ?
Ag3B C5_9 H5_9 88.5 . . ?
C5_9 C6_9 C1_9 118.9(9) . . ?
C5_9 C6_9 Ag3A 58.9(9) . . ?
C1_9 C6_9 Ag3A 111.0(7) . . ?
C5_9 C6_9 Ag3B 56.7(10) . . ?
C1_9 C6_9 Ag3B 107.2(9) . . ?
C5_9 C6_9 H6_9 120.5 . . ?
C1_9 C6_9 H6_9 120.5 . . ?
Ag3A C6_9 H6_9 99.0 . . ?
Ag3B C6_9 H6_9 104.4 . . ?
F1_18 C1_18 C2_18 117.7(18) . . ?
F1_18 C1_18 C6_18 122.5(18) . . ?
C2_18 C1_18 C6_18 119.8(14) . . ?
F2_18 C2_18 C1_18 124.3(18) . . ?
F2_18 C2_18 C3_18 113.5(18) . . ?
C1_18 C2_18 C3_18 122.2(15) . . ?
C4_18 C3_18 C2_18 117.9(18) . . ?
C4_18 C3_18 Ag3B 49.9(19) . . ?
C2_18 C3_18 Ag3B 105.1(14) . . ?
C4_18 C3_18 Ag3A 45.0(18) . . ?
C2_18 C3_18 Ag3A 105.0(13) . . ?
C4_18 C3_18 H3_18 121.0 . . ?
C2_18 C3_18 H3_18 121.0 . . ?
Ag3B C3_18 H3_18 111.8 . . ?
Ag3A C3_18 H3_18 115.8 . . ?
C3_18 C4_18 C5_18 120.7(19) . . ?
C3_18 C4_18 Ag3A 110(2) . . ?
C5_18 C4_18 Ag3A 76.8(16) . . ?
C3_18 C4_18 Ag3B 104(2) . . ?
C5_18 C4_18 Ag3B 82.7(19) . . ?
C3_18 C4_18 H4_18 119.7 . . ?
C5_18 C4_18 H4_18 119.7 . . ?
Ag3A C4_18 H4_18 83.3 . . ?
Ag3B C4_18 H4_18 83.8 . . ?
C4_18 C5_18 C6_18 120.8(17) . . ?
C4_18 C5_18 Ag3A 69.3(17) . . ?
C6_18 C5_18 Ag3A 110.3(15) . . ?
C4_18 C5_18 Ag3B 65.1(18) . . ?
C6_18 C5_18 Ag3B 108.6(16) . . ?
C4_18 C5_18 H5_18 119.6 . . ?
C6_18 C5_18 H5_18 119.6 . . ?
Ag3A C5_18 H5_18 90.4 . . ?
Ag3B C5_18 H5_18 96.0 . . ?
C1_18 C6_18 C5_18 118.5(15) . . ?
C1_18 C6_18 Ag3A 102.8(11) . . ?
C5_18 C6_18 Ag3A 45.4(12) . . ?
C1_18 C6_18 Ag3B 97.9(13) . . ?
C5_18 C6_18 Ag3B 47.8(12) . . ?
C1_18 C6_18 H6_18 120.7 . . ?
C5_18 C6_18 H6_18 120.7 . . ?
Ag3A C6_18 H6_18 118.0 . . ?
Ag3B C6_18 H6_18 121.5 . . ?
F1_7 C1_7 C6_7 121.2(10) . . ?
F1_7 C1_7 C2_7 118.5(9) . . ?
C6_7 C1_7 C2_7 120.3(9) . . ?
F2_7 C2_7 C3_7 121.1(9) . . ?
F2_7 C2_7 C1_7 117.6(9) . . ?
C3_7 C2_7 C1_7 121.4(8) . . ?
C2_7 C3_7 C4_7 118.8(8) . . ?
C2_7 C3_7 H3_7 120.6 . . ?
C4_7 C3_7 H3_7 120.6 . . ?
C5_7 C4_7 C3_7 120.7(9) . . ?
C5_7 C4_7 Ag1A 70.9(7) . . ?
C3_7 C4_7 Ag1A 107.7(6) . . ?
C5_7 C4_7 Ag1B 68.3(7) . . ?
C3_7 C4_7 Ag1B 100.5(7) . . ?
C5_7 C4_7 H4_7 119.6 . . ?
C3_7 C4_7 H4_7 119.6 . . ?
Ag1A C4_7 H4_7 91.3 . . ?
Ag1B C4_7 H4_7 101.0 . . ?
C4_7 C5_7 C6_7 119.8(9) . . ?
C4_7 C5_7 Ag1A 75.6(7) . . ?
C6_7 C5_7 Ag1A 104.6(10) . . ?
C4_7 C5_7 Ag1B 82.9(8) . . ?
C6_7 C5_7 Ag1B 92.3(10) . . ?
C4_7 C5_7 H5_7 120.1 . . ?
C6_7 C5_7 H5_7 120.1 . . ?
Ag1A C5_7 H5_7 89.8 . . ?
Ag1B C5_7 H5_7 94.8 . . ?
C1_7 C6_7 C5_7 118.9(10) . . ?
C1_7 C6_7 Ag1A 102.8(8) . . ?
C5_7 C6_7 Ag1A 49.0(7) . . ?
C1_7 C6_7 Ag1B 98.6(9) . . ?
C5_7 C6_7 Ag1B 60.6(9) . . ?
C1_7 C6_7 H6_7 120.5 . . ?
C5_7 C6_7 H6_7 120.5 . . ?
Ag1A C6_7 H6_7 115.3 . . ?
Ag1B C6_7 H6_7 109.7 . . ?
F1_22 C1_22 C2_22 117.5(16) . . ?
F1_22 C1_22 C6_22 120.6(17) . . ?
C2_22 C1_22 C6_22 121.9(15) . . ?
F2_22 C2_22 C3_22 126.8(18) . . ?
F2_22 C2_22 C1_22 113.5(17) . . ?
C3_22 C2_22 C1_22 119.6(16) . . ?
C2_22 C3_22 C4_22 119.3(19) . . ?
C2_22 C3_22 Ag1A 110.1(15) . . ?
C4_22 C3_22 Ag1A 56.0(19) . . ?
C2_22 C3_22 Ag1B 102.5(15) . . ?
C4_22 C3_22 Ag1B 68(2) . . ?
C2_22 C3_22 H3_22 120.3 . . ?
C4_22 C3_22 H3_22 120.3 . . ?
Ag1A C3_22 H3_22 102.3 . . ?
Ag1B C3_22 H3_22 98.6 . . ?
C5_22 C4_22 C3_22 120.3(19) . . ?
C5_22 C4_22 Ag1A 91(2) . . ?
C3_22 C4_22 Ag1A 94(2) . . ?
C5_22 C4_22 Ag1B 94(2) . . ?
C3_22 C4_22 Ag1B 82(2) . . ?
C5_22 C4_22 H4_22 119.8 . . ?
C3_22 C4_22 H4_22 119.8 . . ?
Ag1A C4_22 H4_22 85.4 . . ?
Ag1B C4_22 H4_22 94.1 . . ?
C4_22 C5_22 C6_22 120.1(17) . . ?
C4_22 C5_22 Ag1A 59(2) . . ?
C6_22 C5_22 Ag1A 113.1(16) . . ?
C4_22 C5_22 Ag1B 59.1(19) . . ?
C6_22 C5_22 Ag1B 103.6(15) . . ?
C4_22 C5_22 H5_22 119.9 . . ?
C6_22 C5_22 H5_22 119.9 . . ?
Ag1A C5_22 H5_22 97.3 . . ?
Ag1B C5_22 H5_22 106.2 . . ?
C1_22 C6_22 C5_22 118.4(16) . . ?
C1_22 C6_22 H6_22 120.8 . . ?
C5_22 C6_22 H6_22 120.8 . . ?
C1_5 O1_5 Al1 153.0(8) . . ?
O1_5 C1_5 C2_5 114.3(9) . . ?
O1_5 C1_5 C4_5 111.0(9) . . ?
C2_5 C1_5 C4_5 107.0(9) . . ?
O1_5 C1_5 C3_5 108.8(9) . . ?
C2_5 C1_5 C3_5 107.6(8) . . ?
C4_5 C1_5 C3_5 107.8(9) . . ?
F1_5 C2_5 F2_5 105.1(8) . . ?
F1_5 C2_5 C1_5 110.0(9) . . ?
F2_5 C2_5 C1_5 111.3(9) . . ?
F1_5 C2_5 C9_5 109.0(9) . . ?
F2_5 C2_5 C9_5 108.2(9) . . ?
C1_5 C2_5 C9_5 112.8(8) . . ?
F4_5 C3_5 F3_5 106.6(9) . . ?
F4_5 C3_5 C7_5 110.5(9) . . ?
F3_5 C3_5 C7_5 110.3(8) . . ?
F4_5 C3_5 C1_5 109.2(8) . . ?
F3_5 C3_5 C1_5 108.8(8) . . ?
C7_5 C3_5 C1_5 111.4(8) . . ?
F6_5 C4_5 F5_5 105.1(11) . . ?
F6_5 C4_5 C5_5 109.9(13) . . ?
F5_5 C4_5 C5_5 107.7(10) . . ?
F6_5 C4_5 C1_5 111.8(12) . . ?
F5_5 C4_5 C1_5 111.3(11) . . ?
C5_5 C4_5 C1_5 110.7(10) . . ?
F7_5 C5_5 C10_5 110.0(10) . . ?
F7_5 C5_5 C4_5 108.8(12) . . ?
C10_5 C5_5 C4_5 110.1(10) . . ?
F7_5 C5_5 C6_5 108.5(11) . . ?
C10_5 C5_5 C6_5 109.2(10) . . ?
C4_5 C5_5 C6_5 110.1(10) . . ?
F8_5 C6_5 F9_5 106.4(9) . . ?
F8_5 C6_5 C7_5 110.0(9) . . ?
F9_5 C6_5 C7_5 109.4(8) . . ?
F8_5 C6_5 C5_5 111.3(9) . . ?
F9_5 C6_5 C5_5 110.7(9) . . ?
C7_5 C6_5 C5_5 108.9(9) . . ?
F10_5 C7_5 C8_5 110.7(10) . . ?
F10_5 C7_5 C6_5 109.7(9) . . ?
C8_5 C7_5 C6_5 110.7(10) . . ?
F10_5 C7_5 C3_5 108.5(9) . . ?
C8_5 C7_5 C3_5 108.5(9) . . ?
C6_5 C7_5 C3_5 108.8(8) . . ?
F12_5 C8_5 F11_5 105.3(16) . . ?
F12_5 C8_5 C7_5 110.5(12) . . ?
F11_5 C8_5 C7_5 109.0(13) . . ?
F12_5 C8_5 C9_5 110.1(13) . . ?
F11_5 C8_5 C9_5 111.6(14) . . ?
C7_5 C8_5 C9_5 110.2(11) . . ?
F13_5 C9_5 C10_5 108.5(10) . . ?
F13_5 C9_5 C8_5 109.3(10) . . ?
C10_5 C9_5 C8_5 109.3(10) . . ?
F13_5 C9_5 C2_5 112.1(9) . . ?
C10_5 C9_5 C2_5 109.3(9) . . ?
C8_5 C9_5 C2_5 108.4(10) . . ?
F15_5 C10_5 F14_5 106.6(10) . . ?
F15_5 C10_5 C9_5 112.1(10) . . ?
F14_5 C10_5 C9_5 110.6(9) . . ?
F15_5 C10_5 C5_5 109.6(10) . . ?
F14_5 C10_5 C5_5 108.4(10) . . ?
C9_5 C10_5 C5_5 109.4(10) . . ?
C1_12 O1_12 Al1 154.4(8) . . ?
O1_12 C1_12 C4_12 111.1(10) . . ?
O1_12 C1_12 C3_12 110.8(9) . . ?
C4_12 C1_12 C3_12 108.7(9) . . ?
O1_12 C1_12 C2_12 110.7(10) . . ?
C4_12 C1_12 C2_12 107.4(9) . . ?
C3_12 C1_12 C2_12 108.0(9) . . ?
F1_12 C2_12 F2_12 106.1(12) . . ?
F1_12 C2_12 C9_12 107.7(13) . . ?
F2_12 C2_12 C9_12 109.4(10) . . ?
F1_12 C2_12 C1_12 110.7(13) . . ?
F2_12 C2_12 C1_12 111.8(11) . . ?
C9_12 C2_12 C1_12 110.9(10) . . ?
F4_12 C3_12 F3_12 106.1(10) . . ?
F4_12 C3_12 C7_12 110.3(9) . . ?
F3_12 C3_12 C7_12 108.1(9) . . ?
F4_12 C3_12 C1_12 109.9(9) . . ?
F3_12 C3_12 C1_12 110.6(9) . . ?
C7_12 C3_12 C1_12 111.7(9) . . ?
F6_12 C4_12 F5_12 107.1(9) . . ?
F6_12 C4_12 C1_12 111.4(9) . . ?
F5_12 C4_12 C1_12 108.1(10) . . ?
F6_12 C4_12 C5_12 111.1(10) . . ?
F5_12 C4_12 C5_12 108.7(9) . . ?
C1_12 C4_12 C5_12 110.4(8) . . ?
F7_12 C5_12 C10_12 109.0(10) . . ?
F7_12 C5_12 C4_12 109.1(9) . . ?
C10_12 C5_12 C4_12 108.9(8) . . ?
F7_12 C5_12 C6_12 108.6(10) . . ?
C10_12 C5_12 C6_12 109.0(10) . . ?
C4_12 C5_12 C6_12 112.1(10) . . ?
F9_12 C6_12 F8_12 107.5(16) . . ?
F9_12 C6_12 C7_12 110.2(13) . . ?
F8_12 C6_12 C7_12 109.8(14) . . ?
F9_12 C6_12 C5_12 110.6(12) . . ?
F8_12 C6_12 C5_12 110.5(13) . . ?
C7_12 C6_12 C5_12 108.2(10) . . ?
F10_12 C7_12 C6_12 109.0(10) . . ?
F10_12 C7_12 C3_12 109.5(9) . . ?
C6_12 C7_12 C3_12 109.1(10) . . ?
F10_12 C7_12 C8_12 110.4(9) . . ?
C6_12 C7_12 C8_12 108.6(10) . . ?
C3_12 C7_12 C8_12 110.1(9) . . ?
F12_12 C8_12 F11_12 105.9(9) . . ?
F12_12 C8_12 C9_12 112.2(9) . . ?
F11_12 C8_12 C9_12 111.1(10) . . ?
F12_12 C8_12 C7_12 109.8(9) . . ?
F11_12 C8_12 C7_12 108.2(9) . . ?
C9_12 C8_12 C7_12 109.5(9) . . ?
F13_12 C9_12 C8_12 109.2(10) . . ?
F13_12 C9_12 C10_12 109.1(11) . . ?
C8_12 C9_12 C10_12 108.6(10) . . ?
F13_12 C9_12 C2_12 109.9(13) . . ?
C8_12 C9_12 C2_12 110.5(10) . . ?
C10_12 C9_12 C2_12 109.5(10) . . ?
F14_12 C10_12 F15_12 105.6(9) . . ?
F14_12 C10_12 C5_12 110.8(9) . . ?
F15_12 C10_12 C5_12 111.0(9) . . ?
F14_12 C10_12 C9_12 109.8(9) . . ?
F15_12 C10_12 C9_12 110.9(9) . . ?
C5_12 C10_12 C9_12 108.9(9) . . ?
C1_4 O1_4 Al1 152.4(13) . . ?
O1_4 C1_4 C3_4 108.0(13) . . ?
O1_4 C1_4 C2_4 115.3(13) . . ?
C3_4 C1_4 C2_4 107.6(12) . . ?
O1_4 C1_4 C4_4 110.6(13) . . ?
C3_4 C1_4 C4_4 106.4(12) . . ?
C2_4 C1_4 C4_4 108.6(13) . . ?
F2_4 C2_4 F1_4 100.5(17) . . ?
F2_4 C2_4 C9_4 115.9(15) . . ?
F1_4 C2_4 C9_4 106.6(15) . . ?
F2_4 C2_4 C1_4 110.6(15) . . ?
F1_4 C2_4 C1_4 110.7(15) . . ?
C9_4 C2_4 C1_4 111.9(12) . . ?
F3_4 C3_4 F4_4 108.6(16) . . ?
F3_4 C3_4 C7_4 103.2(14) . . ?
F4_4 C3_4 C7_4 105.6(13) . . ?
F3_4 C3_4 C1_4 117.4(14) . . ?
F4_4 C3_4 C1_4 109.6(12) . . ?
C7_4 C3_4 C1_4 111.6(12) . . ?
F6_4 C4_4 F5_4 107.0(17) . . ?
F6_4 C4_4 C5_4 106.8(14) . . ?
F5_4 C4_4 C5_4 109.9(15) . . ?
F6_4 C4_4 C1_4 113.0(14) . . ?
F5_4 C4_4 C1_4 109.7(14) . . ?
C5_4 C4_4 C1_4 110.3(12) . . ?
F7_4 C5_4 C6_4 109.4(14) . . ?
F7_4 C5_4 C10_4 110.3(15) . . ?
C6_4 C5_4 C10_4 110.4(13) . . ?
F7_4 C5_4 C4_4 107.9(13) . . ?
C6_4 C5_4 C4_4 108.5(12) . . ?
C10_4 C5_4 C4_4 110.3(13) . . ?
F8_4 C6_4 F9_4 105.3(16) . . ?
F8_4 C6_4 C5_4 112.6(15) . . ?
F9_4 C6_4 C5_4 110.6(15) . . ?
F8_4 C6_4 C7_4 110.2(15) . . ?
F9_4 C6_4 C7_4 109.9(14) . . ?
C5_4 C6_4 C7_4 108.3(12) . . ?
F10_4 C7_4 C8_4 108.4(13) . . ?
F10_4 C7_4 C3_4 110.1(15) . . ?
C8_4 C7_4 C3_4 110.6(12) . . ?
F10_4 C7_4 C6_4 108.6(14) . . ?
C8_4 C7_4 C6_4 110.5(13) . . ?
C3_4 C7_4 C6_4 108.7(12) . . ?
F11_4 C8_4 F12_4 103.5(15) . . ?
F11_4 C8_4 C7_4 113.1(15) . . ?
F12_4 C8_4 C7_4 110.1(13) . . ?
F11_4 C8_4 C9_4 108.5(14) . . ?
F12_4 C8_4 C9_4 111.5(13) . . ?
C7_4 C8_4 C9_4 109.9(12) . . ?
F13_4 C9_4 C10_4 108.5(14) . . ?
F13_4 C9_4 C8_4 107.7(14) . . ?
C10_4 C9_4 C8_4 108.1(12) . . ?
F13_4 C9_4 C2_4 114.1(15) . . ?
C10_4 C9_4 C2_4 108.3(13) . . ?
C8_4 C9_4 C2_4 110.0(13) . . ?
F15_4 C10_4 F14_4 105.6(15) . . ?
F15_4 C10_4 C5_4 108.3(14) . . ?
F14_4 C10_4 C5_4 114.2(15) . . ?
F15_4 C10_4 C9_4 111.4(14) . . ?
F14_4 C10_4 C9_4 107.3(14) . . ?
C5_4 C10_4 C9_4 110.1(13) . . ?
C1_6 O1_6 Al1 148.4(15) . . ?
O1_6 C1_6 C2_6 128.9(16) . . ?
O1_6 C1_6 C3_6 108.5(14) . . ?
C2_6 C1_6 C3_6 113.6(13) . . ?
O1_6 C1_6 C4_6 93.5(12) . . ?
C2_6 C1_6 C4_6 105.2(12) . . ?
C3_6 C1_6 C4_6 100.9(12) . . ?
F2_6 C2_6 F1_6 102.7(13) . . ?
F2_6 C2_6 C9_6 106.4(12) . . ?
F1_6 C2_6 C9_6 106.1(12) . . ?
F2_6 C2_6 C1_6 113.8(13) . . ?
F1_6 C2_6 C1_6 113.8(13) . . ?
C9_6 C2_6 C1_6 113.1(12) . . ?
F4_6 C3_6 F3_6 104.8(15) . . ?
F4_6 C3_6 C7_6 105.0(13) . . ?
F3_6 C3_6 C7_6 111.3(14) . . ?
F4_6 C3_6 C1_6 113.3(14) . . ?
F3_6 C3_6 C1_6 110.2(14) . . ?
C7_6 C3_6 C1_6 111.9(13) . . ?
F5_6 C4_6 F6_6 105.4(14) . . ?
F5_6 C4_6 C5_6 115.5(14) . . ?
F6_6 C4_6 C5_6 111.8(14) . . ?
F5_6 C4_6 C1_6 104.7(12) . . ?
F6_6 C4_6 C1_6 109.2(15) . . ?
C5_6 C4_6 C1_6 109.9(12) . . ?
F7_6 C5_6 C4_6 107.2(12) . . ?
F7_6 C5_6 C10_6 110.2(13) . . ?
C4_6 C5_6 C10_6 111.2(12) . . ?
F7_6 C5_6 C6_6 114.2(13) . . ?
C4_6 C5_6 C6_6 121.8(12) . . ?
C10_6 C5_6 C6_6 91.1(11) . . ?
F8_6 C6_6 F9_6 101.2(14) . . ?
F8_6 C6_6 C7_6 111.9(14) . . ?
F9_6 C6_6 C7_6 111.1(13) . . ?
F8_6 C6_6 C5_6 96.4(13) . . ?
F9_6 C6_6 C5_6 121.0(14) . . ?
C7_6 C6_6 C5_6 113.1(12) . . ?
C6_6 F9_6 F12_6 94.8(10) . . ?
F10_6 C7_6 C3_6 112.1(15) . . ?
F10_6 C7_6 C8_6 110.0(15) . . ?
C3_6 C7_6 C8_6 116.9(14) . . ?
F10_6 C7_6 C6_6 110.7(15) . . ?
C3_6 C7_6 C6_6 108.8(12) . . ?
C8_6 C7_6 C6_6 97.4(12) . . ?
F11_6 C8_6 F12_6 96.1(15) . . ?
F11_6 C8_6 C7_6 111.3(15) . . ?
F12_6 C8_6 C7_6 115.7(15) . . ?
F11_6 C8_6 C9_6 116.0(15) . . ?
F12_6 C8_6 C9_6 109.8(14) . . ?
C7_6 C8_6 C9_6 107.9(13) . . ?
C8_6 F12_6 F9_6 84.1(11) . . ?
F13_6 C9_6 C8_6 106.6(12) . . ?
F13_6 C9_6 C2_6 114.5(13) . . ?
C8_6 C9_6 C2_6 107.1(12) . . ?
F13_6 C9_6 C10_6 107.7(12) . . ?
C8_6 C9_6 C10_6 113.7(13) . . ?
C2_6 C9_6 C10_6 107.4(11) . . ?
F14_6 C10_6 F15_6 106.8(14) . . ?
F14_6 C10_6 C5_6 110.3(13) . . ?
F15_6 C10_6 C5_6 107.7(13) . . ?
F14_6 C10_6 C9_6 111.4(13) . . ?
F15_6 C10_6 C9_6 110.8(14) . . ?
C5_6 C10_6 C9_6 109.7(11) . . ?
C1_3 O1_3 Al1 150.2(5) . . ?
O1_3 C1_3 C4_3 108.2(6) . . ?
O1_3 C1_3 C3_3 111.8(7) . . ?
C4_3 C1_3 C3_3 108.4(7) . . ?
O1_3 C1_3 C2_3 112.3(7) . . ?
C4_3 C1_3 C2_3 108.4(7) . . ?
C3_3 C1_3 C2_3 107.6(6) . . ?
F1_3 C2_3 F2_3 105.5(7) . . ?
F1_3 C2_3 C9_3 108.2(6) . . ?
F2_3 C2_3 C9_3 110.0(7) . . ?
F1_3 C2_3 C1_3 111.3(7) . . ?
F2_3 C2_3 C1_3 110.7(7) . . ?
C9_3 C2_3 C1_3 111.0(6) . . ?
F3_3 C3_3 F4_3 107.4(7) . . ?
F3_3 C3_3 C7_3 110.5(7) . . ?
F4_3 C3_3 C7_3 107.9(7) . . ?
F3_3 C3_3 C1_3 110.7(7) . . ?
F4_3 C3_3 C1_3 109.7(7) . . ?
C7_3 C3_3 C1_3 110.7(7) . . ?
F6_3 C4_3 F5_3 106.6(7) . . ?
F6_3 C4_3 C1_3 110.4(7) . . ?
F5_3 C4_3 C1_3 110.5(7) . . ?
F6_3 C4_3 C5_3 108.4(7) . . ?
F5_3 C4_3 C5_3 109.5(7) . . ?
C1_3 C4_3 C5_3 111.3(6) . . ?
F7_3 C5_3 C6_3 110.1(7) . . ?
F7_3 C5_3 C10_3 109.9(7) . . ?
C6_3 C5_3 C10_3 109.1(7) . . ?
F7_3 C5_3 C4_3 110.2(7) . . ?
C6_3 C5_3 C4_3 108.4(7) . . ?
C10_3 C5_3 C4_3 109.0(7) . . ?
F8_3 C6_3 F9_3 106.2(7) . . ?
F8_3 C6_3 C5_3 110.1(8) . . ?
F9_3 C6_3 C5_3 108.8(8) . . ?
F8_3 C6_3 C7_3 110.8(8) . . ?
F9_3 C6_3 C7_3 110.5(8) . . ?
C5_3 C6_3 C7_3 110.5(7) . . ?
F10_3 C7_3 C8_3 108.8(7) . . ?
F10_3 C7_3 C6_3 109.4(8) . . ?
C8_3 C7_3 C6_3 108.5(7) . . ?
F10_3 C7_3 C3_3 110.4(8) . . ?
C8_3 C7_3 C3_3 109.8(7) . . ?
C6_3 C7_3 C3_3 109.9(7) . . ?
F12_3 C8_3 F11_3 106.5(6) . . ?
F12_3 C8_3 C7_3 111.5(7) . . ?
F11_3 C8_3 C7_3 110.0(7) . . ?
F12_3 C8_3 C9_3 110.5(6) . . ?
F11_3 C8_3 C9_3 109.1(6) . . ?
C7_3 C8_3 C9_3 109.3(6) . . ?
F13_3 C9_3 C2_3 110.2(6) . . ?
F13_3 C9_3 C8_3 109.4(6) . . ?
C2_3 C9_3 C8_3 110.1(6) . . ?
F13_3 C9_3 C10_3 109.1(6) . . ?
C2_3 C9_3 C10_3 108.8(6) . . ?
C8_3 C9_3 C10_3 109.2(6) . . ?
F14_3 C10_3 F15_3 104.3(7) . . ?
F14_3 C10_3 C5_3 111.4(8) . . ?
F15_3 C10_3 C5_3 111.1(7) . . ?
F14_3 C10_3 C9_3 110.2(7) . . ?
F15_3 C10_3 C9_3 109.4(7) . . ?
C5_3 C10_3 C9_3 110.3(6) . . ?
C1_15 O1_15 Al1 149.7(13) . . ?
O1_15 C1_15 C4_15 111.3(13) . . ?
O1_15 C1_15 C3_15 111.7(13) . . ?
C4_15 C1_15 C3_15 107.0(12) . . ?
O1_15 C1_15 C2_15 114.2(13) . . ?
C4_15 C1_15 C2_15 106.5(12) . . ?
C3_15 C1_15 C2_15 105.7(12) . . ?
F1_15 C2_15 F2_15 105.3(14) . . ?
F1_15 C2_15 C9_15 109.6(13) . . ?
F2_15 C2_15 C9_15 109.7(13) . . ?
F1_15 C2_15 C1_15 109.5(13) . . ?
F2_15 C2_15 C1_15 108.8(13) . . ?
C9_15 C2_15 C1_15 113.6(12) . . ?
F4_15 C3_15 F3_15 103.8(15) . . ?
F4_15 C3_15 C7_15 109.3(14) . . ?
F3_15 C3_15 C7_15 107.5(13) . . ?
F4_15 C3_15 C1_15 109.6(15) . . ?
F3_15 C3_15 C1_15 112.3(13) . . ?
C7_15 C3_15 C1_15 113.9(12) . . ?
F6_15 C4_15 F5_15 108.0(15) . . ?
F6_15 C4_15 C1_15 109.5(13) . . ?
F5_15 C4_15 C1_15 108.4(13) . . ?
F6_15 C4_15 C5_15 109.7(13) . . ?
F5_15 C4_15 C5_15 108.8(14) . . ?
C1_15 C4_15 C5_15 112.4(12) . . ?
F7_15 C5_15 C10_15 109.1(13) . . ?
F7_15 C5_15 C6_15 108.6(13) . . ?
C10_15 C5_15 C6_15 108.8(12) . . ?
F7_15 C5_15 C4_15 110.4(13) . . ?
C10_15 C5_15 C4_15 110.5(12) . . ?
C6_15 C5_15 C4_15 109.4(12) . . ?
F8_15 C6_15 F9_15 104.2(13) . . ?
F8_15 C6_15 C5_15 112.0(13) . . ?
F9_15 C6_15 C5_15 111.3(13) . . ?
F8_15 C6_15 C7_15 109.3(13) . . ?
F9_15 C6_15 C7_15 109.8(12) . . ?
C5_15 C6_15 C7_15 110.1(11) . . ?
F10_15 C7_15 C3_15 111.8(13) . . ?
F10_15 C7_15 C6_15 109.9(13) . . ?
C3_15 C7_15 C6_15 108.7(12) . . ?
F10_15 C7_15 C8_15 109.3(13) . . ?
C3_15 C7_15 C8_15 109.1(12) . . ?
C6_15 C7_15 C8_15 108.0(11) . . ?
F11_15 C8_15 F12_15 105.6(14) . . ?
F11_15 C8_15 C9_15 111.1(13) . . ?
F12_15 C8_15 C9_15 111.2(14) . . ?
F11_15 C8_15 C7_15 109.4(13) . . ?
F12_15 C8_15 C7_15 109.7(12) . . ?
C9_15 C8_15 C7_15 109.7(12) . . ?
F13_15 C9_15 C8_15 109.7(14) . . ?
F13_15 C9_15 C2_15 110.9(15) . . ?
C8_15 C9_15 C2_15 109.5(12) . . ?
F13_15 C9_15 C10_15 108.7(14) . . ?
C8_15 C9_15 C10_15 108.9(12) . . ?
C2_15 C9_15 C10_15 109.2(13) . . ?
F14_15 C10_15 F15_15 104.4(14) . . ?
F14_15 C10_15 C5_15 110.7(14) . . ?
F15_15 C10_15 C5_15 111.8(14) . . ?
F14_15 C10_15 C9_15 110.7(14) . . ?
F15_15 C10_15 C9_15 110.0(13) . . ?
C5_15 C10_15 C9_15 109.2(12) . . ?
C1_16 O1_16 Al1 149.0(9) . . ?
O1_16 C1_16 C3_16 112.9(9) . . ?
O1_16 C1_16 C2_16 112.3(9) . . ?
C3_16 C1_16 C2_16 106.8(9) . . ?
O1_16 C1_16 C4_16 110.0(9) . . ?
C3_16 C1_16 C4_16 107.0(9) . . ?
C2_16 C1_16 C4_16 107.4(9) . . ?
F1_16 C2_16 F2_16 105.1(9) . . ?
F1_16 C2_16 C1_16 111.5(9) . . ?
F2_16 C2_16 C1_16 110.2(9) . . ?
F1_16 C2_16 C9_16 109.0(9) . . ?
F2_16 C2_16 C9_16 108.8(8) . . ?
C1_16 C2_16 C9_16 112.0(8) . . ?
F3_16 C3_16 F4_16 105.9(9) . . ?
F3_16 C3_16 C1_16 110.9(9) . . ?
F4_16 C3_16 C1_16 110.9(9) . . ?
F3_16 C3_16 C7_16 108.5(9) . . ?
F4_16 C3_16 C7_16 108.3(8) . . ?
C1_16 C3_16 C7_16 112.0(9) . . ?
F5_16 C4_16 F6_16 105.3(9) . . ?
F5_16 C4_16 C1_16 110.2(9) . . ?
F6_16 C4_16 C1_16 109.9(9) . . ?
F5_16 C4_16 C5_16 109.6(8) . . ?
F6_16 C4_16 C5_16 109.5(9) . . ?
C1_16 C4_16 C5_16 112.1(8) . . ?
F7_16 C5_16 C6_16 109.9(9) . . ?
F7_16 C5_16 C10_16 110.5(9) . . ?
C6_16 C5_16 C10_16 109.0(9) . . ?
F7_16 C5_16 C4_16 109.8(9) . . ?
C6_16 C5_16 C4_16 108.8(9) . . ?
C10_16 C5_16 C4_16 108.9(8) . . ?
F8_16 C6_16 F9_16 105.8(9) . . ?
F8_16 C6_16 C5_16 113.6(11) . . ?
F9_16 C6_16 C5_16 107.5(10) . . ?
F8_16 C6_16 C7_16 107.4(10) . . ?
F9_16 C6_16 C7_16 110.6(11) . . ?
C5_16 C6_16 C7_16 111.8(9) . . ?
F10_16 C7_16 C8_16 108.8(11) . . ?
F10_16 C7_16 C6_16 112.3(11) . . ?
C8_16 C7_16 C6_16 108.9(9) . . ?
F10_16 C7_16 C3_16 108.9(11) . . ?
C8_16 C7_16 C3_16 109.7(9) . . ?
C6_16 C7_16 C3_16 108.3(10) . . ?
F12_16 C8_16 F11_16 107.2(9) . . ?
F12_16 C8_16 C7_16 110.2(9) . . ?
F11_16 C8_16 C7_16 110.8(9) . . ?
F12_16 C8_16 C9_16 110.7(9) . . ?
F11_16 C8_16 C9_16 109.2(9) . . ?
C7_16 C8_16 C9_16 108.6(9) . . ?
F13_16 C9_16 C10_16 109.6(8) . . ?
F13_16 C9_16 C8_16 108.3(9) . . ?
C10_16 C9_16 C8_16 110.0(8) . . ?
F13_16 C9_16 C2_16 110.2(8) . . ?
C10_16 C9_16 C2_16 109.5(8) . . ?
C8_16 C9_16 C2_16 109.4(8) . . ?
F14_16 C10_16 F15_16 106.4(9) . . ?
F14_16 C10_16 C9_16 110.8(9) . . ?
F15_16 C10_16 C9_16 109.2(9) . . ?
F14_16 C10_16 C5_16 110.2(10) . . ?
F15_16 C10_16 C5_16 110.2(10) . . ?
C9_16 C10_16 C5_16 110.0(8) . . ?
C1_14 O1_14 Al1 144.4(15) . . ?
O1_14 C1_14 C2_14 125.9(15) . . ?
O1_14 C1_14 C4_14 111.9(14) . . ?
C2_14 C1_14 C4_14 113.8(13) . . ?
O1_14 C1_14 C3_14 91.2(13) . . ?
C2_14 C1_14 C3_14 107.9(13) . . ?
C4_14 C1_14 C3_14 99.7(12) . . ?
F1_14 C2_14 F2_14 104.8(14) . . ?
F1_14 C2_14 C1_14 111.9(15) . . ?
F2_14 C2_14 C1_14 112.4(14) . . ?
F1_14 C2_14 C9_14 111.0(13) . . ?
F2_14 C2_14 C9_14 104.2(13) . . ?
C1_14 C2_14 C9_14 112.1(12) . . ?
F3_14 C3_14 F4_14 109.5(14) . . ?
F3_14 C3_14 C7_14 113.7(14) . . ?
F4_14 C3_14 C7_14 112.2(13) . . ?
F3_14 C3_14 C1_14 104.9(13) . . ?
F4_14 C3_14 C1_14 104.6(13) . . ?
C7_14 C3_14 C1_14 111.3(13) . . ?
F6_14 C4_14 F5_14 109.2(14) . . ?
F6_14 C4_14 C1_14 108.6(13) . . ?
F5_14 C4_14 C1_14 113.1(13) . . ?
F6_14 C4_14 C5_14 112.8(13) . . ?
F5_14 C4_14 C5_14 102.5(12) . . ?
C1_14 C4_14 C5_14 110.6(12) . . ?
F7_14 C5_14 C6_14 108.7(14) . . ?
F7_14 C5_14 C10_14 109.9(13) . . ?
C6_14 C5_14 C10_14 123.3(13) . . ?
F7_14 C5_14 C4_14 108.9(15) . . ?
C6_14 C5_14 C4_14 99.1(11) . . ?
C10_14 C5_14 C4_14 105.8(12) . . ?
F8_14 C6_14 F9_14 102.3(13) . . ?
F8_14 C6_14 C7_14 110.6(13) . . ?
F9_14 C6_14 C7_14 107.8(13) . . ?
F8_14 C6_14 C5_14 111.4(13) . . ?
F9_14 C6_14 C5_14 113.4(14) . . ?
C7_14 C6_14 C5_14 111.0(13) . . ?
F10_14 C7_14 C8_14 111.5(15) . . ?
F10_14 C7_14 C3_14 106.9(17) . . ?
C8_14 C7_14 C3_14 109.1(12) . . ?
F10_14 C7_14 C6_14 112.6(15) . . ?
C8_14 C7_14 C6_14 107.7(12) . . ?
C3_14 C7_14 C6_14 108.9(13) . . ?
F12_14 C8_14 F11_14 104.2(12) . . ?
F12_14 C8_14 C7_14 107.5(11) . . ?
F11_14 C8_14 C7_14 108.6(13) . . ?
F12_14 C8_14 C9_14 113.7(13) . . ?
F11_14 C8_14 C9_14 111.8(12) . . ?
C7_14 C8_14 C9_14 110.7(12) . . ?
F13_14 C9_14 C8_14 107.2(12) . . ?
F13_14 C9_14 C2_14 110.7(12) . . ?
C8_14 C9_14 C2_14 106.2(11) . . ?
F13_14 C9_14 C10_14 111.1(12) . . ?
C8_14 C9_14 C10_14 124.9(13) . . ?
C2_14 C9_14 C10_14 95.7(11) . . ?
F15_14 C10_14 F14_14 92.4(13) . . ?
F15_14 C10_14 C5_14 114.9(15) . . ?
F14_14 C10_14 C5_14 107.9(12) . . ?
F15_14 C10_14 C9_14 108.5(13) . . ?
F14_14 C10_14 C9_14 129.9(15) . . ?
C5_14 C10_14 C9_14 103.5(12) . . ?
C1_17 O1_17 Al1 147.4(12) . . ?
O1_17 C1_17 C3_17 115.6(13) . . ?
O1_17 C1_17 C2_17 106.1(12) . . ?
C3_17 C1_17 C2_17 107.2(11) . . ?
O1_17 C1_17 C4_17 112.2(13) . . ?
C3_17 C1_17 C4_17 106.7(11) . . ?
C2_17 C1_17 C4_17 108.8(11) . . ?
F1_17 C2_17 F2_17 108.0(15) . . ?
F1_17 C2_17 C9_17 104.7(15) . . ?
F2_17 C2_17 C9_17 109.5(13) . . ?
F1_17 C2_17 C1_17 113.0(16) . . ?
F2_17 C2_17 C1_17 109.7(13) . . ?
C9_17 C2_17 C1_17 111.8(11) . . ?
F4_17 C3_17 F3_17 99.9(14) . . ?
F4_17 C3_17 C7_17 110.8(13) . . ?
F3_17 C3_17 C7_17 111.5(15) . . ?
F4_17 C3_17 C1_17 110.8(12) . . ?
F3_17 C3_17 C1_17 111.1(13) . . ?
C7_17 C3_17 C1_17 112.2(11) . . ?
F5_17 C4_17 F6_17 107.8(14) . . ?
F5_17 C4_17 C5_17 113.4(13) . . ?
F6_17 C4_17 C5_17 107.1(14) . . ?
F5_17 C4_17 C1_17 109.6(12) . . ?
F6_17 C4_17 C1_17 108.6(13) . . ?
C5_17 C4_17 C1_17 110.2(11) . . ?
F7_17 C5_17 C10_17 106.1(13) . . ?
F7_17 C5_17 C4_17 110.9(15) . . ?
C10_17 C5_17 C4_17 111.1(12) . . ?
F7_17 C5_17 C6_17 111.0(14) . . ?
C10_17 C5_17 C6_17 110.6(12) . . ?
C4_17 C5_17 C6_17 107.2(11) . . ?
F9_17 C6_17 F8_17 105.1(14) . . ?
F9_17 C6_17 C7_17 108.6(12) . . ?
F8_17 C6_17 C7_17 110.4(13) . . ?
F9_17 C6_17 C5_17 111.2(13) . . ?
F8_17 C6_17 C5_17 111.3(13) . . ?
C7_17 C6_17 C5_17 110.1(11) . . ?
F10_17 C7_17 C6_17 111.1(13) . . ?
F10_17 C7_17 C8_17 109.9(14) . . ?
C6_17 C7_17 C8_17 109.4(11) . . ?
F10_17 C7_17 C3_17 108.5(14) . . ?
C6_17 C7_17 C3_17 108.1(11) . . ?
C8_17 C7_17 C3_17 109.7(11) . . ?
F11_17 C8_17 F12_17 108.5(15) . . ?
F11_17 C8_17 C9_17 110.3(13) . . ?
F12_17 C8_17 C9_17 109.9(13) . . ?
F11_17 C8_17 C7_17 108.0(13) . . ?
F12_17 C8_17 C7_17 110.4(13) . . ?
C9_17 C8_17 C7_17 109.7(11) . . ?
F13_17 C9_17 C8_17 108.1(12) . . ?
F13_17 C9_17 C2_17 110.8(13) . . ?
C8_17 C9_17 C2_17 111.1(11) . . ?
F13_17 C9_17 C10_17 109.5(12) . . ?
C8_17 C9_17 C10_17 110.0(12) . . ?
C2_17 C9_17 C10_17 107.5(12) . . ?
F14_17 C10_17 F15_17 108.7(16) . . ?
F14_17 C10_17 C5_17 113.0(14) . . ?
F15_17 C10_17 C5_17 108.9(13) . . ?
F14_17 C10_17 C9_17 108.0(14) . . ?
F15_17 C10_17 C9_17 109.4(13) . . ?
C5_17 C10_17 C9_17 108.8(11) . . ?
C1_13 O1_13 Al1 151.0(8) . . ?
O1_13 C1_13 C2_13 114.1(10) . . ?
O1_13 C1_13 C4_13 109.3(10) . . ?
C2_13 C1_13 C4_13 108.1(10) . . ?
O1_13 C1_13 C3_13 112.0(10) . . ?
C2_13 C1_13 C3_13 104.8(10) . . ?
C4_13 C1_13 C3_13 108.3(10) . . ?
F2_13 C2_13 F1_13 105.5(13) . . ?
F2_13 C2_13 C1_13 110.9(11) . . ?
F1_13 C2_13 C1_13 110.4(11) . . ?
F2_13 C2_13 C9_13 109.1(11) . . ?
F1_13 C2_13 C9_13 107.8(11) . . ?
C1_13 C2_13 C9_13 112.9(10) . . ?
F3_13 C3_13 F4_13 109.7(13) . . ?
F3_13 C3_13 C7_13 109.7(13) . . ?
F4_13 C3_13 C7_13 107.9(11) . . ?
F3_13 C3_13 C1_13 109.3(15) . . ?
F4_13 C3_13 C1_13 108.4(11) . . ?
C7_13 C3_13 C1_13 111.7(10) . . ?
F5_13 C4_13 F6_13 107.8(13) . . ?
F5_13 C4_13 C5_13 110.5(11) . . ?
F6_13 C4_13 C5_13 109.9(11) . . ?
F5_13 C4_13 C1_13 109.7(10) . . ?
F6_13 C4_13 C1_13 107.2(11) . . ?
C5_13 C4_13 C1_13 111.7(10) . . ?
F7_13 C5_13 C6_13 110.8(12) . . ?
F7_13 C5_13 C4_13 110.1(11) . . ?
C6_13 C5_13 C4_13 108.9(10) . . ?
F7_13 C5_13 C10_13 107.0(11) . . ?
C6_13 C5_13 C10_13 110.2(10) . . ?
C4_13 C5_13 C10_13 109.7(10) . . ?
F8_13 C6_13 F9_13 106.0(12) . . ?
F8_13 C6_13 C5_13 109.2(12) . . ?
F9_13 C6_13 C5_13 109.0(12) . . ?
F8_13 C6_13 C7_13 112.9(12) . . ?
F9_13 C6_13 C7_13 109.1(11) . . ?
C5_13 C6_13 C7_13 110.5(10) . . ?
F10_13 C7_13 C6_13 107.3(11) . . ?
F10_13 C7_13 C8_13 111.5(11) . . ?
C6_13 C7_13 C8_13 109.1(10) . . ?
F10_13 C7_13 C3_13 110.2(11) . . ?
C6_13 C7_13 C3_13 110.2(11) . . ?
C8_13 C7_13 C3_13 108.5(10) . . ?
F11_13 C8_13 F12_13 103.6(11) . . ?
F11_13 C8_13 C7_13 110.3(12) . . ?
F12_13 C8_13 C7_13 110.4(11) . . ?
F11_13 C8_13 C9_13 112.0(12) . . ?
F12_13 C8_13 C9_13 110.8(11) . . ?
C7_13 C8_13 C9_13 109.6(10) . . ?
F13_13 C9_13 C10_13 109.4(11) . . ?
F13_13 C9_13 C8_13 108.8(11) . . ?
C10_13 C9_13 C8_13 109.9(10) . . ?
F13_13 C9_13 C2_13 112.1(10) . . ?
C10_13 C9_13 C2_13 108.2(10) . . ?
C8_13 C9_13 C2_13 108.4(10) . . ?
F14_13 C10_13 F15_13 105.3(11) . . ?
F14_13 C10_13 C9_13 108.9(11) . . ?
F15_13 C10_13 C9_13 110.4(11) . . ?
F14_13 C10_13 C5_13 113.7(12) . . ?
F15_13 C10_13 C5_13 109.1(11) . . ?
C9_13 C10_13 C5_13 109.3(10) . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Ag1B O1_1 C1_1 C2_1 -43.3(9) . . . . ?
Ag3B O1_1 C1_1 C2_1 173.1(10) . . . . ?
Ag2A O1_1 C1_1 C2_1 58.6(6) . . . . ?
Ag1A O1_1 C1_1 C2_1 -61.5(5) . . . . ?
Ag3A O1_1 C1_1 C2_1 -179.1(3) . . . . ?
Ag2B O1_1 C1_1 C2_1 80.5(6) . . . . ?
Ag1B O1_1 C1_1 C3_1 -164.2(9) . . . . ?
Ag3B O1_1 C1_1 C3_1 52.2(11) . . . . ?
Ag2A O1_1 C1_1 C3_1 -62.2(6) . . . . ?
Ag1A O1_1 C1_1 C3_1 177.6(3) . . . . ?
Ag3A O1_1 C1_1 C3_1 60.1(5) . . . . ?
Ag2B O1_1 C1_1 C3_1 -40.4(7) . . . . ?
Ag1B O1_1 C1_1 C4_1 75.8(10) . . . . ?
Ag3B O1_1 C1_1 C4_1 -67.8(11) . . . . ?
Ag2A O1_1 C1_1 C4_1 177.8(3) . . . . ?
Ag1A O1_1 C1_1 C4_1 57.6(6) . . . . ?
Ag3A O1_1 C1_1 C4_1 -59.9(6) . . . . ?
Ag2B O1_1 C1_1 C4_1 -160.4(5) . . . . ?
O1_1 C1_1 C2_1 F2_1 56.2(5) . . . . ?
C3_1 C1_1 C2_1 F2_1 -179.8(4) . . . . ?
C4_1 C1_1 C2_1 F2_1 -65.5(5) . . . . ?
O1_1 C1_1 C2_1 F1_1 -58.7(5) . . . . ?
C3_1 C1_1 C2_1 F1_1 65.3(5) . . . . ?
C4_1 C1_1 C2_1 F1_1 179.6(4) . . . . ?
O1_1 C1_1 C2_1 C9_1 179.0(4) . . . . ?
C3_1 C1_1 C2_1 C9_1 -57.1(5) . . . . ?
C4_1 C1_1 C2_1 C9_1 57.2(5) . . . . ?
O1_1 C1_1 C3_1 F3_1 58.5(5) . . . . ?
C2_1 C1_1 C3_1 F3_1 -65.1(5) . . . . ?
C4_1 C1_1 C3_1 F3_1 -179.1(4) . . . . ?
O1_1 C1_1 C3_1 F4_1 -57.9(5) . . . . ?
C2_1 C1_1 C3_1 F4_1 178.5(4) . . . . ?
C4_1 C1_1 C3_1 F4_1 64.5(5) . . . . ?
O1_1 C1_1 C3_1 C7_1 -179.8(4) . . . . ?
C2_1 C1_1 C3_1 C7_1 56.6(5) . . . . ?
C4_1 C1_1 C3_1 C7_1 -57.5(5) . . . . ?
O1_1 C1_1 C4_1 F5_1 58.3(6) . . . . ?
C2_1 C1_1 C4_1 F5_1 -179.3(4) . . . . ?
C3_1 C1_1 C4_1 F5_1 -64.9(5) . . . . ?
O1_1 C1_1 C4_1 F6_1 -57.1(6) . . . . ?
C2_1 C1_1 C4_1 F6_1 65.3(5) . . . . ?
C3_1 C1_1 C4_1 F6_1 179.7(4) . . . . ?
O1_1 C1_1 C4_1 C5_1 -178.7(5) . . . . ?
C2_1 C1_1 C4_1 C5_1 -56.4(6) . . . . ?
C3_1 C1_1 C4_1 C5_1 58.0(6) . . . . ?
F5_1 C4_1 C5_1 F7_1 -56.3(6) . . . . ?
F6_1 C4_1 C5_1 F7_1 58.3(6) . . . . ?
C1_1 C4_1 C5_1 F7_1 -179.5(5) . . . . ?
F5_1 C4_1 C5_1 C10_1 -177.2(4) . . . . ?
F6_1 C4_1 C5_1 C10_1 -62.6(5) . . . . ?
C1_1 C4_1 C5_1 C10_1 59.7(6) . . . . ?
F5_1 C4_1 C5_1 C6_1 62.4(5) . . . . ?
F6_1 C4_1 C5_1 C6_1 177.0(4) . . . . ?
C1_1 C4_1 C5_1 C6_1 -60.8(6) . . . . ?
F7_1 C5_1 C6_1 F8_1 57.8(6) . . . . ?
C10_1 C5_1 C6_1 F8_1 178.5(5) . . . . ?
C4_1 C5_1 C6_1 F8_1 -61.6(6) . . . . ?
F7_1 C5_1 C6_1 F9_1 -59.8(6) . . . . ?
C10_1 C5_1 C6_1 F9_1 60.9(5) . . . . ?
C4_1 C5_1 C6_1 F9_1 -179.2(4) . . . . ?
F7_1 C5_1 C6_1 C7_1 -179.8(4) . . . . ?
C10_1 C5_1 C6_1 C7_1 -59.1(5) . . . . ?
C4_1 C5_1 C6_1 C7_1 60.8(6) . . . . ?
F8_1 C6_1 C7_1 F10_1 -58.1(6) . . . . ?
F9_1 C6_1 C7_1 F10_1 58.8(6) . . . . ?
C5_1 C6_1 C7_1 F10_1 179.4(4) . . . . ?
F8_1 C6_1 C7_1 C8_1 -178.8(4) . . . . ?
F9_1 C6_1 C7_1 C8_1 -61.8(6) . . . . ?
C5_1 C6_1 C7_1 C8_1 58.8(6) . . . . ?
F8_1 C6_1 C7_1 C3_1 61.5(6) . . . . ?
F9_1 C6_1 C7_1 C3_1 178.5(5) . . . . ?
C5_1 C6_1 C7_1 C3_1 -60.9(6) . . . . ?
F3_1 C3_1 C7_1 F10_1 -57.8(6) . . . . ?
F4_1 C3_1 C7_1 F10_1 57.9(6) . . . . ?
C1_1 C3_1 C7_1 F10_1 -179.9(4) . . . . ?
F3_1 C3_1 C7_1 C8_1 62.8(6) . . . . ?
F4_1 C3_1 C7_1 C8_1 178.5(4) . . . . ?
C1_1 C3_1 C7_1 C8_1 -59.3(5) . . . . ?
F3_1 C3_1 C7_1 C6_1 -177.5(5) . . . . ?
F4_1 C3_1 C7_1 C6_1 -61.8(6) . . . . ?
C1_1 C3_1 C7_1 C6_1 60.4(6) . . . . ?
F10_1 C7_1 C8_1 F11_1 57.8(6) . . . . ?
C6_1 C7_1 C8_1 F11_1 178.2(4) . . . . ?
C3_1 C7_1 C8_1 F11_1 -62.6(5) . . . . ?
F10_1 C7_1 C8_1 F12_1 -57.7(6) . . . . ?
C6_1 C7_1 C8_1 F12_1 62.7(5) . . . . ?
C3_1 C7_1 C8_1 F12_1 -178.1(4) . . . . ?
F10_1 C7_1 C8_1 C9_1 179.9(4) . . . . ?
C6_1 C7_1 C8_1 C9_1 -59.7(5) . . . . ?
C3_1 C7_1 C8_1 C9_1 59.5(5) . . . . ?
F11_1 C8_1 C9_1 F13_1 -58.8(5) . . . . ?
F12_1 C8_1 C9_1 F13_1 58.8(6) . . . . ?
C7_1 C8_1 C9_1 F13_1 -180.0(5) . . . . ?
F11_1 C8_1 C9_1 C2_1 62.0(5) . . . . ?
F12_1 C8_1 C9_1 C2_1 179.6(4) . . . . ?
C7_1 C8_1 C9_1 C2_1 -59.2(5) . . . . ?
F11_1 C8_1 C9_1 C10_1 -178.9(4) . . . . ?
F12_1 C8_1 C9_1 C10_1 -61.3(6) . . . . ?
C7_1 C8_1 C9_1 C10_1 59.9(5) . . . . ?
F2_1 C2_1 C9_1 F13_1 -57.7(5) . . . . ?
F1_1 C2_1 C9_1 F13_1 57.0(6) . . . . ?
C1_1 C2_1 C9_1 F13_1 179.5(4) . . . . ?
F2_1 C2_1 C9_1 C8_1 -177.5(4) . . . . ?
F1_1 C2_1 C9_1 C8_1 -62.8(6) . . . . ?
C1_1 C2_1 C9_1 C8_1 59.7(5) . . . . ?
F2_1 C2_1 C9_1 C10_1 62.6(6) . . . . ?
F1_1 C2_1 C9_1 C10_1 177.4(4) . . . . ?
C1_1 C2_1 C9_1 C10_1 -60.2(6) . . . . ?
F7_1 C5_1 C10_1 F14_1 -58.7(5) . . . . ?
C6_1 C5_1 C10_1 F14_1 -178.6(5) . . . . ?
C4_1 C5_1 C10_1 F14_1 62.1(5) . . . . ?
F7_1 C5_1 C10_1 F15_1 58.1(6) . . . . ?
C6_1 C5_1 C10_1 F15_1 -61.8(5) . . . . ?
C4_1 C5_1 C10_1 F15_1 178.9(4) . . . . ?
F7_1 C5_1 C10_1 C9_1 179.3(4) . . . . ?
C6_1 C5_1 C10_1 C9_1 59.4(5) . . . . ?
C4_1 C5_1 C10_1 C9_1 -59.9(5) . . . . ?
F13_1 C9_1 C10_1 F14_1 58.2(5) . . . . ?
C8_1 C9_1 C10_1 F14_1 177.8(4) . . . . ?
C2_1 C9_1 C10_1 F14_1 -62.6(6) . . . . ?
F13_1 C9_1 C10_1 F15_1 -57.8(6) . . . . ?
C8_1 C9_1 C10_1 F15_1 61.9(6) . . . . ?
C2_1 C9_1 C10_1 F15_1 -178.5(5) . . . . ?
F13_1 C9_1 C10_1 C5_1 -179.3(4) . . . . ?
C8_1 C9_1 C10_1 C5_1 -59.6(5) . . . . ?
C2_1 C9_1 C10_1 C5_1 59.9(6) . . . . ?
Ag1B O1_2 C1_2 C4_2 164.4(9) . . . . ?
Ag3A O1_2 C1_2 C4_2 -57.4(5) . . . . ?
Ag1A O1_2 C1_2 C4_2 -177.3(3) . . . . ?
Ag2A O1_2 C1_2 C4_2 64.4(5) . . . . ?
Ag3B O1_2 C1_2 C4_2 -49.5(11) . . . . ?
Ag1B O1_2 C1_2 C2_2 44.5(9) . . . . ?
Ag3A O1_2 C1_2 C2_2 -177.3(3) . . . . ?
Ag1A O1_2 C1_2 C2_2 62.8(4) . . . . ?
Ag2A O1_2 C1_2 C2_2 -55.5(6) . . . . ?
Ag3B O1_2 C1_2 C2_2 -169.4(10) . . . . ?
Ag1B O1_2 C1_2 C3_2 -75.2(10) . . . . ?
Ag3A O1_2 C1_2 C3_2 63.0(6) . . . . ?
Ag1A O1_2 C1_2 C3_2 -56.9(6) . . . . ?
Ag2A O1_2 C1_2 C3_2 -175.3(3) . . . . ?
Ag3B O1_2 C1_2 C3_2 70.9(11) . . . . ?
O1_2 C1_2 C2_2 F1_2 -57.6(5) . . . . ?
C4_2 C1_2 C2_2 F1_2 179.7(4) . . . . ?
C3_2 C1_2 C2_2 F1_2 65.4(5) . . . . ?
O1_2 C1_2 C2_2 F2_2 57.6(5) . . . . ?
C4_2 C1_2 C2_2 F2_2 -65.1(4) . . . . ?
C3_2 C1_2 C2_2 F2_2 -179.4(4) . . . . ?
O1_2 C1_2 C2_2 C9_2 179.6(4) . . . . ?
C4_2 C1_2 C2_2 C9_2 56.9(5) . . . . ?
C3_2 C1_2 C2_2 C9_2 -57.4(5) . . . . ?
O1_2 C1_2 C3_2 F4_2 -57.6(6) . . . . ?
C4_2 C1_2 C3_2 F4_2 65.5(5) . . . . ?
C2_2 C1_2 C3_2 F4_2 179.8(4) . . . . ?
O1_2 C1_2 C3_2 F3_2 57.0(6) . . . . ?
C4_2 C1_2 C3_2 F3_2 -179.8(4) . . . . ?
C2_2 C1_2 C3_2 F3_2 -65.5(5) . . . . ?
O1_2 C1_2 C3_2 C7_2 180.0(5) . . . . ?
C4_2 C1_2 C3_2 C7_2 -56.9(6) . . . . ?
C2_2 C1_2 C3_2 C7_2 57.4(6) . . . . ?
O1_2 C1_2 C4_2 F6_2 -57.5(5) . . . . ?
C2_2 C1_2 C4_2 F6_2 65.1(5) . . . . ?
C3_2 C1_2 C4_2 F6_2 179.1(4) . . . . ?
O1_2 C1_2 C4_2 F5_2 58.2(5) . . . . ?
C2_2 C1_2 C4_2 F5_2 -179.2(4) . . . . ?
C3_2 C1_2 C4_2 F5_2 -65.1(5) . . . . ?
O1_2 C1_2 C4_2 C5_2 -179.5(4) . . . . ?
C2_2 C1_2 C4_2 C5_2 -56.9(5) . . . . ?
C3_2 C1_2 C4_2 C5_2 57.1(5) . . . . ?
F6_2 C4_2 C5_2 F7_2 57.5(6) . . . . ?
F5_2 C4_2 C5_2 F7_2 -57.5(6) . . . . ?
C1_2 C4_2 C5_2 F7_2 -180.0(4) . . . . ?
F6_2 C4_2 C5_2 C10_2 -62.8(6) . . . . ?
F5_2 C4_2 C5_2 C10_2 -177.8(4) . . . . ?
C1_2 C4_2 C5_2 C10_2 59.7(6) . . . . ?
F6_2 C4_2 C5_2 C6_2 177.6(5) . . . . ?
F5_2 C4_2 C5_2 C6_2 62.6(6) . . . . ?
C1_2 C4_2 C5_2 C6_2 -59.9(6) . . . . ?
F7_2 C5_2 C6_2 F9_2 -58.9(7) . . . . ?
C10_2 C5_2 C6_2 F9_2 61.6(6) . . . . ?
C4_2 C5_2 C6_2 F9_2 -178.9(5) . . . . ?
F7_2 C5_2 C6_2 F8_2 58.1(6) . . . . ?
C10_2 C5_2 C6_2 F8_2 178.6(4) . . . . ?
C4_2 C5_2 C6_2 F8_2 -61.9(6) . . . . ?
F7_2 C5_2 C6_2 C7_2 179.8(5) . . . . ?
C10_2 C5_2 C6_2 C7_2 -59.7(6) . . . . ?
C4_2 C5_2 C6_2 C7_2 59.8(6) . . . . ?
F4_2 C3_2 C7_2 F10_2 58.3(6) . . . . ?
F3_2 C3_2 C7_2 F10_2 -57.0(6) . . . . ?
C1_2 C3_2 C7_2 F10_2 -179.8(5) . . . . ?
F4_2 C3_2 C7_2 C6_2 -62.0(5) . . . . ?
F3_2 C3_2 C7_2 C6_2 -177.3(4) . . . . ?
C1_2 C3_2 C7_2 C6_2 59.9(6) . . . . ?
F4_2 C3_2 C7_2 C8_2 177.5(4) . . . . ?
F3_2 C3_2 C7_2 C8_2 62.1(5) . . . . ?
C1_2 C3_2 C7_2 C8_2 -60.6(6) . . . . ?
F9_2 C6_2 C7_2 F10_2 57.7(6) . . . . ?
F8_2 C6_2 C7_2 F10_2 -59.3(6) . . . . ?
C5_2 C6_2 C7_2 F10_2 179.0(5) . . . . ?
F9_2 C6_2 C7_2 C3_2 178.4(4) . . . . ?
F8_2 C6_2 C7_2 C3_2 61.3(5) . . . . ?
C5_2 C6_2 C7_2 C3_2 -60.3(6) . . . . ?
F9_2 C6_2 C7_2 C8_2 -61.5(5) . . . . ?
F8_2 C6_2 C7_2 C8_2 -178.6(4) . . . . ?
C5_2 C6_2 C7_2 C8_2 59.8(5) . . . . ?
F10_2 C7_2 C8_2 F11_2 58.9(5) . . . . ?
C3_2 C7_2 C8_2 F11_2 -61.0(5) . . . . ?
C6_2 C7_2 C8_2 F11_2 178.6(4) . . . . ?
F10_2 C7_2 C8_2 F12_2 -58.4(6) . . . . ?
C3_2 C7_2 C8_2 F12_2 -178.3(4) . . . . ?
C6_2 C7_2 C8_2 F12_2 61.3(5) . . . . ?
F10_2 C7_2 C8_2 C9_2 -179.3(4) . . . . ?
C3_2 C7_2 C8_2 C9_2 60.8(6) . . . . ?
C6_2 C7_2 C8_2 C9_2 -59.6(5) . . . . ?
F1_2 C2_2 C9_2 F13_2 56.9(6) . . . . ?
F2_2 C2_2 C9_2 F13_2 -58.1(6) . . . . ?
C1_2 C2_2 C9_2 F13_2 179.8(4) . . . . ?
F1_2 C2_2 C9_2 C10_2 177.8(4) . . . . ?
F2_2 C2_2 C9_2 C10_2 62.7(5) . . . . ?
C1_2 C2_2 C9_2 C10_2 -59.4(5) . . . . ?
F1_2 C2_2 C9_2 C8_2 -62.7(5) . . . . ?
F2_2 C2_2 C9_2 C8_2 -177.8(4) . . . . ?
C1_2 C2_2 C9_2 C8_2 60.1(6) . . . . ?
F11_2 C8_2 C9_2 F13_2 -58.4(6) . . . . ?
F12_2 C8_2 C9_2 F13_2 58.6(6) . . . . ?
C7_2 C8_2 C9_2 F13_2 179.8(4) . . . . ?
F11_2 C8_2 C9_2 C10_2 -179.0(4) . . . . ?
F12_2 C8_2 C9_2 C10_2 -62.0(6) . . . . ?
C7_2 C8_2 C9_2 C10_2 59.2(5) . . . . ?
F11_2 C8_2 C9_2 C2_2 61.8(6) . . . . ?
F12_2 C8_2 C9_2 C2_2 178.8(5) . . . . ?
C7_2 C8_2 C9_2 C2_2 -60.1(6) . . . . ?
F13_2 C9_2 C10_2 F15_2 -58.0(6) . . . . ?
C2_2 C9_2 C10_2 F15_2 -179.0(4) . . . . ?
C8_2 C9_2 C10_2 F15_2 62.3(6) . . . . ?
F13_2 C9_2 C10_2 F14_2 58.7(5) . . . . ?
C2_2 C9_2 C10_2 F14_2 -62.3(5) . . . . ?
C8_2 C9_2 C10_2 F14_2 179.0(4) . . . . ?
F13_2 C9_2 C10_2 C5_2 -179.7(5) . . . . ?
C2_2 C9_2 C10_2 C5_2 59.3(5) . . . . ?
C8_2 C9_2 C10_2 C5_2 -59.4(5) . . . . ?
F7_2 C5_2 C10_2 F15_2 58.2(6) . . . . ?
C6_2 C5_2 C10_2 F15_2 -62.4(6) . . . . ?
C4_2 C5_2 C10_2 F15_2 178.5(4) . . . . ?
F7_2 C5_2 C10_2 F14_2 -58.2(6) . . . . ?
C6_2 C5_2 C10_2 F14_2 -178.8(4) . . . . ?
C4_2 C5_2 C10_2 F14_2 62.1(6) . . . . ?
F7_2 C5_2 C10_2 C9_2 -179.8(5) . . . . ?
C6_2 C5_2 C10_2 C9_2 59.6(5) . . . . ?
C4_2 C5_2 C10_2 C9_2 -59.5(5) . . . . ?
C6_10 C1_10 C2_10 F2_10 -178.4(13) . . . . ?
F1_10 C1_10 C2_10 F2_10 2.4(16) . . . . ?
C6_10 C1_10 C2_10 C3_10 2.8(15) . . . . ?
F1_10 C1_10 C2_10 C3_10 -176.4(11) . . . . ?
F2_10 C2_10 C3_10 C4_10 179.9(13) . . . . ?
C1_10 C2_10 C3_10 C4_10 -1.3(15) . . . . ?
C2_10 C3_10 C4_10 C5_10 -0.2(18) . . . . ?
C3_10 C4_10 C5_10 C6_10 0.3(19) . . . . ?
C2_10 C1_10 C6_10 C5_10 -2.8(16) . . . . ?
F1_10 C1_10 C6_10 C5_10 176.3(11) . . . . ?
C4_10 C5_10 C6_10 C1_10 1.2(17) . . . . ?
C6_10 C1_10 F1_10 Ag1B -45(2) . . . . ?
C2_10 C1_10 F1_10 Ag1B 134.6(14) . . . . ?
F1_20 C1_20 C2_20 F2_20 0(6) . . . . ?
C6_20 C1_20 C2_20 F2_20 179(5) . . . . ?
F1_20 C1_20 C2_20 C3_20 179(4) . . . . ?
C6_20 C1_20 C2_20 C3_20 -2(4) . . . . ?
F2_20 C2_20 C3_20 C4_20 177(6) . . . . ?
C1_20 C2_20 C3_20 C4_20 -2(4) . . . . ?
C2_20 C3_20 C4_20 C5_20 4(8) . . . . ?
C3_20 C4_20 C5_20 C6_20 -1(10) . . . . ?
F1_20 C1_20 C6_20 C5_20 -176(6) . . . . ?
C2_20 C1_20 C6_20 C5_20 5(7) . . . . ?
C4_20 C5_20 C6_20 C1_20 -3(9) . . . . ?
F1_11 C1_11 C2_11 F2_11 -8(2) . . . . ?
C6_11 C1_11 C2_11 F2_11 175.3(18) . . . . ?
F1_11 C1_11 C2_11 C3_11 174.1(17) . . . . ?
C6_11 C1_11 C2_11 C3_11 -2.9(18) . . . . ?
F2_11 C2_11 C3_11 C4_11 -176.4(17) . . . . ?
C1_11 C2_11 C3_11 C4_11 1.8(17) . . . . ?
C2_11 C3_11 C4_11 C5_11 0(2) . . . . ?
C3_11 C4_11 C5_11 C6_11 -1(2) . . . . ?
F1_11 C1_11 C6_11 C5_11 -174.5(17) . . . . ?
C2_11 C1_11 C6_11 C5_11 2(2) . . . . ?
C4_11 C5_11 C6_11 C1_11 -1(2) . . . . ?
C3_11 C2_11 F2_11 Ag2B -108(3) . . . . ?
C1_11 C2_11 F2_11 Ag2B 74(3) . . . . ?
F1_19 C1_19 C2_19 F2_19 3(4) . . . . ?
C6_19 C1_19 C2_19 F2_19 180(4) . . . . ?
F1_19 C1_19 C2_19 C3_19 -176(3) . . . . ?
C6_19 C1_19 C2_19 C3_19 0(3) . . . . ?
F2_19 C2_19 C3_19 C4_19 -178(4) . . . . ?
C1_19 C2_19 C3_19 C4_19 2(3) . . . . ?
C2_19 C3_19 C4_19 C5_19 -5(5) . . . . ?
C3_19 C4_19 C5_19 C6_19 6(5) . . . . ?
C4_19 C5_19 C6_19 C1_19 -4(5) . . . . ?
F1_19 C1_19 C6_19 C5_19 177(4) . . . . ?
C2_19 C1_19 C6_19 C5_19 1(5) . . . . ?
C3_19 C2_19 F2_19 Ag2B 52(10) . . . . ?
C1_19 C2_19 F2_19 Ag2B -128(9) . . . . ?
F1_8 C1_8 C2_8 F2_8 1.9(15) . . . . ?
C6_8 C1_8 C2_8 F2_8 -175.4(13) . . . . ?
F1_8 C1_8 C2_8 C3_8 178.4(11) . . . . ?
C6_8 C1_8 C2_8 C3_8 1.1(12) . . . . ?
F1_8 C1_8 C2_8 Ag2B -125.6(10) . . . . ?
C6_8 C1_8 C2_8 Ag2B 57.1(9) . . . . ?
F1_8 C1_8 C2_8 Ag2A -132.9(10) . . . . ?
C6_8 C1_8 C2_8 Ag2A 49.8(9) . . . . ?
F2_8 C2_8 C3_8 C4_8 175.2(14) . . . . ?
C1_8 C2_8 C3_8 C4_8 -1.3(14) . . . . ?
Ag2B C2_8 C3_8 C4_8 -68.9(10) . . . . ?
Ag2A C2_8 C3_8 C4_8 -77.5(10) . . . . ?
F2_8 C2_8 C3_8 Ag2A -107.3(11) . . . . ?
C1_8 C2_8 C3_8 Ag2A 76.2(9) . . . . ?
F2_8 C2_8 C3_8 Ag2B -115.8(11) . . . . ?
C1_8 C2_8 C3_8 Ag2B 67.7(9) . . . . ?
C2_8 C3_8 C4_8 C5_8 1.1(17) . . . . ?
Ag2A C3_8 C4_8 C5_8 -96.2(11) . . . . ?
Ag2B C3_8 C4_8 C5_8 -75.4(12) . . . . ?
C2_8 C3_8 C4_8 Ag2A 97.3(10) . . . . ?
C2_8 C3_8 C4_8 Ag2B 76.5(11) . . . . ?
C3_8 C4_8 C5_8 C6_8 -0.9(19) . . . . ?
Ag2A C4_8 C5_8 C6_8 -80.2(13) . . . . ?
Ag2B C4_8 C5_8 C6_8 -70.0(13) . . . . ?
C3_8 C4_8 C5_8 Ag2B 69.1(11) . . . . ?
C3_8 C4_8 C5_8 Ag2A 79.3(11) . . . . ?
C4_8 C5_8 C6_8 C1_8 0.8(19) . . . . ?
Ag2B C5_8 C6_8 C1_8 -57.4(11) . . . . ?
Ag2A C5_8 C6_8 C1_8 -50.7(12) . . . . ?
F1_8 C1_8 C6_8 C5_8 -178.1(12) . . . . ?
C2_8 C1_8 C6_8 C5_8 -0.9(15) . . . . ?
F1_21 C1_21 C2_21 F2_21 6(5) . . . . ?
C6_21 C1_21 C2_21 F2_21 -179(5) . . . . ?
F1_21 C1_21 C2_21 C3_21 -176(4) . . . . ?
C6_21 C1_21 C2_21 C3_21 0(4) . . . . ?
F2_21 C2_21 C3_21 C4_21 177(5) . . . . ?
C1_21 C2_21 C3_21 C4_21 -2(4) . . . . ?
F2_21 C2_21 C3_21 Ag2B -126(4) . . . . ?
C1_21 C2_21 C3_21 Ag2B 55(2) . . . . ?
F2_21 C2_21 C3_21 Ag2A -135(4) . . . . ?
C1_21 C2_21 C3_21 Ag2A 46(2) . . . . ?
C2_21 C3_21 C4_21 C5_21 7(8) . . . . ?
Ag2B C3_21 C4_21 C5_21 -61(6) . . . . ?
Ag2A C3_21 C4_21 C5_21 -67(5) . . . . ?
C2_21 C3_21 C4_21 Ag2A 74(4) . . . . ?
C2_21 C3_21 C4_21 Ag2B 68(3) . . . . ?
C3_21 C4_21 C5_21 C6_21 -9(10) . . . . ?
Ag2A C4_21 C5_21 C6_21 -102(6) . . . . ?
Ag2B C4_21 C5_21 C6_21 -81(6) . . . . ?
C3_21 C4_21 C5_21 Ag2A 93(6) . . . . ?
C3_21 C4_21 C5_21 Ag2B 72(6) . . . . ?
F1_21 C1_21 C6_21 C5_21 173(6) . . . . ?
C2_21 C1_21 C6_21 C5_21 -2(8) . . . . ?
F1_21 C1_21 C6_21 Ag2B 115(4) . . . . ?
C2_21 C1_21 C6_21 Ag2B -60(4) . . . . ?
F1_21 C1_21 C6_21 Ag2A 121(4) . . . . ?
C2_21 C1_21 C6_21 Ag2A -54(4) . . . . ?
C4_21 C5_21 C6_21 C1_21 6(10) . . . . ?
Ag2A C5_21 C6_21 C1_21 -85(6) . . . . ?
Ag2B C5_21 C6_21 C1_21 -72(6) . . . . ?
C4_21 C5_21 C6_21 Ag2B 79(6) . . . . ?
C4_21 C5_21 C6_21 Ag2A 91(6) . . . . ?
F1_9 C1_9 C2_9 F2_9 -1.1(13) . . . . ?
C6_9 C1_9 C2_9 F2_9 178.3(9) . . . . ?
F1_9 C1_9 C2_9 C3_9 179.2(9) . . . . ?
C6_9 C1_9 C2_9 C3_9 -1.5(13) . . . . ?
F2_9 C2_9 C3_9 C4_9 -179.2(11) . . . . ?
C1_9 C2_9 C3_9 C4_9 0.5(13) . . . . ?
C2_9 C3_9 C4_9 C5_9 2.3(19) . . . . ?
C2_9 C3_9 C4_9 Ag3B -66.3(13) . . . . ?
C2_9 C3_9 C4_9 Ag3A -60.3(11) . . . . ?
C3_9 C4_9 C5_9 C6_9 -4(2) . . . . ?
Ag3B C4_9 C5_9 C6_9 93.4(16) . . . . ?
Ag3A C4_9 C5_9 C6_9 93.0(15) . . . . ?
C3_9 C4_9 C5_9 Ag3A -97.2(14) . . . . ?
C3_9 C4_9 C5_9 Ag3B -97.6(15) . . . . ?
C4_9 C5_9 C6_9 C1_9 3(2) . . . . ?
Ag3A C5_9 C6_9 C1_9 98.3(10) . . . . ?
Ag3B C5_9 C6_9 C1_9 92.4(13) . . . . ?
C4_9 C5_9 C6_9 Ag3A -95.1(16) . . . . ?
C4_9 C5_9 C6_9 Ag3B -89.2(17) . . . . ?
F1_9 C1_9 C6_9 C5_9 178.9(12) . . . . ?
C2_9 C1_9 C6_9 C5_9 -0.4(16) . . . . ?
F1_9 C1_9 C6_9 Ag3A -115.9(9) . . . . ?
C2_9 C1_9 C6_9 Ag3A 64.7(11) . . . . ?
F1_9 C1_9 C6_9 Ag3B -120.0(10) . . . . ?
C2_9 C1_9 C6_9 Ag3B 60.6(12) . . . . ?
F1_18 C1_18 C2_18 F2_18 -3(3) . . . . ?
C6_18 C1_18 C2_18 F2_18 177(2) . . . . ?
F1_18 C1_18 C2_18 C3_18 178(2) . . . . ?
C6_18 C1_18 C2_18 C3_18 -1(2) . . . . ?
F2_18 C2_18 C3_18 C4_18 -179(3) . . . . ?
C1_18 C2_18 C3_18 C4_18 0(3) . . . . ?
F2_18 C2_18 C3_18 Ag3B 128.7(18) . . . . ?
C1_18 C2_18 C3_18 Ag3B -52.7(17) . . . . ?
F2_18 C2_18 C3_18 Ag3A 134.3(17) . . . . ?
C1_18 C2_18 C3_18 Ag3A -47.1(15) . . . . ?
C2_18 C3_18 C4_18 C5_18 3(4) . . . . ?
Ag3B C3_18 C4_18 C5_18 89(3) . . . . ?
Ag3A C3_18 C4_18 C5_18 86(3) . . . . ?
C2_18 C3_18 C4_18 Ag3A -83(2) . . . . ?
C2_18 C3_18 C4_18 Ag3B -87(2) . . . . ?
C3_18 C4_18 C5_18 C6_18 -4(4) . . . . ?
Ag3A C4_18 C5_18 C6_18 102(2) . . . . ?
Ag3B C4_18 C5_18 C6_18 98(2) . . . . ?
C3_18 C4_18 C5_18 Ag3A -106(3) . . . . ?
C3_18 C4_18 C5_18 Ag3B -101(3) . . . . ?
F1_18 C1_18 C6_18 C5_18 -179(2) . . . . ?
C2_18 C1_18 C6_18 C5_18 0(3) . . . . ?
F1_18 C1_18 C6_18 Ag3A -133.0(18) . . . . ?
C2_18 C1_18 C6_18 Ag3A 46(2) . . . . ?
F1_18 C1_18 C6_18 Ag3B -133.1(19) . . . . ?
C2_18 C1_18 C6_18 Ag3B 46.2(19) . . . . ?
C4_18 C5_18 C6_18 C1_18 2(4) . . . . ?
Ag3A C5_18 C6_18 C1_18 80(2) . . . . ?
Ag3B C5_18 C6_18 C1_18 74(2) . . . . ?
C4_18 C5_18 C6_18 Ag3A -77(2) . . . . ?
C4_18 C5_18 C6_18 Ag3B -72(2) . . . . ?
F1_7 C1_7 C2_7 F2_7 1.7(15) . . . . ?
C6_7 C1_7 C2_7 F2_7 -179.7(12) . . . . ?
F1_7 C1_7 C2_7 C3_7 -179.0(11) . . . . ?
C6_7 C1_7 C2_7 C3_7 -0.4(15) . . . . ?
F2_7 C2_7 C3_7 C4_7 178.9(9) . . . . ?
C1_7 C2_7 C3_7 C4_7 -0.3(13) . . . . ?
C2_7 C3_7 C4_7 C5_7 1.0(14) . . . . ?
C2_7 C3_7 C4_7 Ag1A -77.0(9) . . . . ?
C2_7 C3_7 C4_7 Ag1B -69.9(9) . . . . ?
C3_7 C4_7 C5_7 C6_7 -0.9(17) . . . . ?
Ag1A C4_7 C5_7 C6_7 98.8(13) . . . . ?
Ag1B C4_7 C5_7 C6_7 88.6(13) . . . . ?
C3_7 C4_7 C5_7 Ag1A -99.7(9) . . . . ?
C3_7 C4_7 C5_7 Ag1B -89.5(10) . . . . ?
F1_7 C1_7 C6_7 C5_7 179.0(14) . . . . ?
C2_7 C1_7 C6_7 C5_7 0.5(19) . . . . ?
F1_7 C1_7 C6_7 Ag1A -130.9(10) . . . . ?
C2_7 C1_7 C6_7 Ag1A 50.5(12) . . . . ?
F1_7 C1_7 C6_7 Ag1B -120.0(12) . . . . ?
C2_7 C1_7 C6_7 Ag1B 61.5(12) . . . . ?
C4_7 C5_7 C6_7 C1_7 0(2) . . . . ?
Ag1A C5_7 C6_7 C1_7 81.7(14) . . . . ?
Ag1B C5_7 C6_7 C1_7 83.3(13) . . . . ?
C4_7 C5_7 C6_7 Ag1A -81.6(11) . . . . ?
C4_7 C5_7 C6_7 Ag1B -83.1(11) . . . . ?
F1_22 C1_22 C2_22 F2_22 3(3) . . . . ?
C6_22 C1_22 C2_22 F2_22 -174(2) . . . . ?
F1_22 C1_22 C2_22 C3_22 -180(2) . . . . ?
C6_22 C1_22 C2_22 C3_22 3(2) . . . . ?
F2_22 C2_22 C3_22 C4_22 176(3) . . . . ?
C1_22 C2_22 C3_22 C4_22 -1(3) . . . . ?
F2_22 C2_22 C3_22 Ag1A -123(2) . . . . ?
C1_22 C2_22 C3_22 Ag1A 60.1(16) . . . . ?
F2_22 C2_22 C3_22 Ag1B -112(2) . . . . ?
C1_22 C2_22 C3_22 Ag1B 70.7(16) . . . . ?
C2_22 C3_22 C4_22 C5_22 3(5) . . . . ?
Ag1A C3_22 C4_22 C5_22 -93(3) . . . . ?
Ag1B C3_22 C4_22 C5_22 -90(3) . . . . ?
C2_22 C3_22 C4_22 Ag1A 96(2) . . . . ?
C2_22 C3_22 C4_22 Ag1B 93(2) . . . . ?
C3_22 C4_22 C5_22 C6_22 -5(5) . . . . ?
Ag1A C4_22 C5_22 C6_22 -100(2) . . . . ?
Ag1B C4_22 C5_22 C6_22 -88(3) . . . . ?
C3_22 C4_22 C5_22 Ag1A 95(3) . . . . ?
C3_22 C4_22 C5_22 Ag1B 83(3) . . . . ?
F1_22 C1_22 C6_22 C5_22 177(2) . . . . ?
C2_22 C1_22 C6_22 C5_22 -6(3) . . . . ?
C4_22 C5_22 C6_22 C1_22 7(4) . . . . ?
Ag1A C5_22 C6_22 C1_22 -59(3) . . . . ?
Ag1B C5_22 C6_22 C1_22 -55(2) . . . . ?
O1_3 Al1 O1_5 C1_5 -32(2) . . . . ?
O1_6 Al1 O1_5 C1_5 113(2) . . . . ?
O1_4 Al1 O1_5 C1_5 -122.0(19) . . . . ?
Al1 O1_5 C1_5 C2_5 -50(2) . . . . ?
Al1 O1_5 C1_5 C4_5 72(2) . . . . ?
Al1 O1_5 C1_5 C3_5 -169.9(15) . . . . ?
O1_5 C1_5 C2_5 F1_5 -56.2(12) . . . . ?
C4_5 C1_5 C2_5 F1_5 -179.6(9) . . . . ?
C3_5 C1_5 C2_5 F1_5 64.8(11) . . . . ?
O1_5 C1_5 C2_5 F2_5 60.0(12) . . . . ?
C4_5 C1_5 C2_5 F2_5 -63.4(11) . . . . ?
C3_5 C1_5 C2_5 F2_5 -179.0(8) . . . . ?
O1_5 C1_5 C2_5 C9_5 -178.2(9) . . . . ?
C4_5 C1_5 C2_5 C9_5 58.4(12) . . . . ?
C3_5 C1_5 C2_5 C9_5 -57.2(11) . . . . ?
O1_5 C1_5 C3_5 F4_5 -56.4(11) . . . . ?
C2_5 C1_5 C3_5 F4_5 179.2(8) . . . . ?
C4_5 C1_5 C3_5 F4_5 64.1(11) . . . . ?
O1_5 C1_5 C3_5 F3_5 59.5(12) . . . . ?
C2_5 C1_5 C3_5 F3_5 -64.9(11) . . . . ?
C4_5 C1_5 C3_5 F3_5 -180.0(9) . . . . ?
O1_5 C1_5 C3_5 C7_5 -178.7(9) . . . . ?
C2_5 C1_5 C3_5 C7_5 56.9(11) . . . . ?
C4_5 C1_5 C3_5 C7_5 -58.2(11) . . . . ?
O1_5 C1_5 C4_5 F6_5 -60.6(15) . . . . ?
C2_5 C1_5 C4_5 F6_5 64.8(13) . . . . ?
C3_5 C1_5 C4_5 F6_5 -179.7(11) . . . . ?
O1_5 C1_5 C4_5 F5_5 56.6(13) . . . . ?
C2_5 C1_5 C4_5 F5_5 -177.9(10) . . . . ?
C3_5 C1_5 C4_5 F5_5 -62.5(12) . . . . ?
O1_5 C1_5 C4_5 C5_5 176.5(10) . . . . ?
C2_5 C1_5 C4_5 C5_5 -58.1(12) . . . . ?
C3_5 C1_5 C4_5 C5_5 57.3(12) . . . . ?
F6_5 C4_5 C5_5 F7_5 57.1(15) . . . . ?
F5_5 C4_5 C5_5 F7_5 -56.9(14) . . . . ?
C1_5 C4_5 C5_5 F7_5 -178.9(11) . . . . ?
F6_5 C4_5 C5_5 C10_5 -63.5(15) . . . . ?
F5_5 C4_5 C5_5 C10_5 -177.6(11) . . . . ?
C1_5 C4_5 C5_5 C10_5 60.5(13) . . . . ?
F6_5 C4_5 C5_5 C6_5 176.0(12) . . . . ?
F5_5 C4_5 C5_5 C6_5 61.9(13) . . . . ?
C1_5 C4_5 C5_5 C6_5 -60.0(13) . . . . ?
F7_5 C5_5 C6_5 F8_5 58.5(13) . . . . ?
C10_5 C5_5 C6_5 F8_5 178.4(9) . . . . ?
C4_5 C5_5 C6_5 F8_5 -60.6(12) . . . . ?
F7_5 C5_5 C6_5 F9_5 -59.7(13) . . . . ?
C10_5 C5_5 C6_5 F9_5 60.2(12) . . . . ?
C4_5 C5_5 C6_5 F9_5 -178.8(10) . . . . ?
F7_5 C5_5 C6_5 C7_5 180.0(11) . . . . ?
C10_5 C5_5 C6_5 C7_5 -60.1(12) . . . . ?
C4_5 C5_5 C6_5 C7_5 60.9(12) . . . . ?
F8_5 C6_5 C7_5 F10_5 -56.7(12) . . . . ?
F9_5 C6_5 C7_5 F10_5 59.9(12) . . . . ?
C5_5 C6_5 C7_5 F10_5 -179.0(9) . . . . ?
F8_5 C6_5 C7_5 C8_5 -179.1(10) . . . . ?
F9_5 C6_5 C7_5 C8_5 -62.5(12) . . . . ?
C5_5 C6_5 C7_5 C8_5 58.6(12) . . . . ?
F8_5 C6_5 C7_5 C3_5 61.8(11) . . . . ?
F9_5 C6_5 C7_5 C3_5 178.4(9) . . . . ?
C5_5 C6_5 C7_5 C3_5 -60.5(11) . . . . ?
F4_5 C3_5 C7_5 F10_5 58.4(11) . . . . ?
F3_5 C3_5 C7_5 F10_5 -59.1(12) . . . . ?
C1_5 C3_5 C7_5 F10_5 180.0(9) . . . . ?
F4_5 C3_5 C7_5 C8_5 178.7(10) . . . . ?
F3_5 C3_5 C7_5 C8_5 61.1(12) . . . . ?
C1_5 C3_5 C7_5 C8_5 -59.8(12) . . . . ?
F4_5 C3_5 C7_5 C6_5 -60.9(11) . . . . ?
F3_5 C3_5 C7_5 C6_5 -178.4(9) . . . . ?
C1_5 C3_5 C7_5 C6_5 60.7(11) . . . . ?
F10_5 C7_5 C8_5 F12_5 -58.2(16) . . . . ?
C6_5 C7_5 C8_5 F12_5 63.6(16) . . . . ?
C3_5 C7_5 C8_5 F12_5 -177.1(14) . . . . ?
F10_5 C7_5 C8_5 F11_5 57.1(16) . . . . ?
C6_5 C7_5 C8_5 F11_5 178.9(14) . . . . ?
C3_5 C7_5 C8_5 F11_5 -61.8(16) . . . . ?
F10_5 C7_5 C8_5 C9_5 179.9(10) . . . . ?
C6_5 C7_5 C8_5 C9_5 -58.3(13) . . . . ?
C3_5 C7_5 C8_5 C9_5 61.0(13) . . . . ?
F12_5 C8_5 C9_5 F13_5 55.1(15) . . . . ?
F11_5 C8_5 C9_5 F13_5 -61.5(16) . . . . ?
C7_5 C8_5 C9_5 F13_5 177.2(10) . . . . ?
F12_5 C8_5 C9_5 C10_5 -63.5(15) . . . . ?
F11_5 C8_5 C9_5 C10_5 179.9(14) . . . . ?
C7_5 C8_5 C9_5 C10_5 58.6(13) . . . . ?
F12_5 C8_5 C9_5 C2_5 177.5(13) . . . . ?
F11_5 C8_5 C9_5 C2_5 60.9(16) . . . . ?
C7_5 C8_5 C9_5 C2_5 -60.4(13) . . . . ?
F1_5 C2_5 C9_5 F13_5 57.6(13) . . . . ?
F2_5 C2_5 C9_5 F13_5 -56.2(12) . . . . ?
C1_5 C2_5 C9_5 F13_5 -179.8(10) . . . . ?
F1_5 C2_5 C9_5 C10_5 177.9(9) . . . . ?
F2_5 C2_5 C9_5 C10_5 64.1(11) . . . . ?
C1_5 C2_5 C9_5 C10_5 -59.5(12) . . . . ?
F1_5 C2_5 C9_5 C8_5 -63.1(12) . . . . ?
F2_5 C2_5 C9_5 C8_5 -176.9(10) . . . . ?
C1_5 C2_5 C9_5 C8_5 59.5(12) . . . . ?
F13_5 C9_5 C10_5 F15_5 -57.8(13) . . . . ?
C8_5 C9_5 C10_5 F15_5 61.3(13) . . . . ?
C2_5 C9_5 C10_5 F15_5 179.7(10) . . . . ?
F13_5 C9_5 C10_5 F14_5 61.0(13) . . . . ?
C8_5 C9_5 C10_5 F14_5 -179.8(10) . . . . ?
C2_5 C9_5 C10_5 F14_5 -61.4(12) . . . . ?
F13_5 C9_5 C10_5 C5_5 -179.6(10) . . . . ?
C8_5 C9_5 C10_5 C5_5 -60.5(12) . . . . ?
C2_5 C9_5 C10_5 C5_5 57.9(12) . . . . ?
F7_5 C5_5 C10_5 F15_5 57.3(15) . . . . ?
C4_5 C5_5 C10_5 F15_5 177.2(11) . . . . ?
C6_5 C5_5 C10_5 F15_5 -61.7(13) . . . . ?
F7_5 C5_5 C10_5 F14_5 -58.8(14) . . . . ?
C4_5 C5_5 C10_5 F14_5 61.2(12) . . . . ?
C6_5 C5_5 C10_5 F14_5 -177.8(9) . . . . ?
F7_5 C5_5 C10_5 C9_5 -179.4(12) . . . . ?
C4_5 C5_5 C10_5 C9_5 -59.5(13) . . . . ?
C6_5 C5_5 C10_5 C9_5 61.6(12) . . . . ?
O1_14 Al1 O1_12 C1_12 -109(2) . . . . ?
O1_13 Al1 O1_12 C1_12 -17(3) . . . . ?
O1_15 Al1 O1_12 C1_12 134(2) . . . . ?
Al1 O1_12 C1_12 C4_12 61(3) . . . . ?
Al1 O1_12 C1_12 C3_12 -177.7(19) . . . . ?
Al1 O1_12 C1_12 C2_12 -58(3) . . . . ?
O1_12 C1_12 C2_12 F1_12 -59.8(15) . . . . ?
C4_12 C1_12 C2_12 F1_12 178.8(12) . . . . ?
C3_12 C1_12 C2_12 F1_12 61.7(14) . . . . ?
O1_12 C1_12 C2_12 F2_12 58.2(14) . . . . ?
C4_12 C1_12 C2_12 F2_12 -63.1(13) . . . . ?
C3_12 C1_12 C2_12 F2_12 179.8(10) . . . . ?
O1_12 C1_12 C2_12 C9_12 -179.3(10) . . . . ?
C4_12 C1_12 C2_12 C9_12 59.3(12) . . . . ?
C3_12 C1_12 C2_12 C9_12 -57.8(13) . . . . ?
O1_12 C1_12 C3_12 F4_12 -58.4(13) . . . . ?
C4_12 C1_12 C3_12 F4_12 64.0(12) . . . . ?
C2_12 C1_12 C3_12 F4_12 -179.8(10) . . . . ?
O1_12 C1_12 C3_12 F3_12 58.4(12) . . . . ?
C4_12 C1_12 C3_12 F3_12 -179.2(9) . . . . ?
C2_12 C1_12 C3_12 F3_12 -63.0(12) . . . . ?
O1_12 C1_12 C3_12 C7_12 178.8(10) . . . . ?
C4_12 C1_12 C3_12 C7_12 -58.8(11) . . . . ?
C2_12 C1_12 C3_12 C7_12 57.4(12) . . . . ?
O1_12 C1_12 C4_12 F6_12 -57.9(11) . . . . ?
C3_12 C1_12 C4_12 F6_12 179.9(8) . . . . ?
C2_12 C1_12 C4_12 F6_12 63.2(11) . . . . ?
O1_12 C1_12 C4_12 F5_12 59.5(11) . . . . ?
C3_12 C1_12 C4_12 F5_12 -62.7(11) . . . . ?
C2_12 C1_12 C4_12 F5_12 -179.3(9) . . . . ?
O1_12 C1_12 C4_12 C5_12 178.3(9) . . . . ?
C3_12 C1_12 C4_12 C5_12 56.0(11) . . . . ?
C2_12 C1_12 C4_12 C5_12 -60.6(11) . . . . ?
F6_12 C4_12 C5_12 F7_12 57.5(12) . . . . ?
F5_12 C4_12 C5_12 F7_12 -60.2(13) . . . . ?
C1_12 C4_12 C5_12 F7_12 -178.5(9) . . . . ?
F6_12 C4_12 C5_12 C10_12 -61.4(11) . . . . ?
F5_12 C4_12 C5_12 C10_12 -179.1(10) . . . . ?
C1_12 C4_12 C5_12 C10_12 62.6(11) . . . . ?
F6_12 C4_12 C5_12 C6_12 177.9(10) . . . . ?
F5_12 C4_12 C5_12 C6_12 60.2(13) . . . . ?
C1_12 C4_12 C5_12 C6_12 -58.1(12) . . . . ?
F7_12 C5_12 C6_12 F9_12 -59.8(16) . . . . ?
C10_12 C5_12 C6_12 F9_12 58.9(16) . . . . ?
C4_12 C5_12 C6_12 F9_12 179.6(13) . . . . ?
F7_12 C5_12 C6_12 F8_12 59.1(18) . . . . ?
C10_12 C5_12 C6_12 F8_12 177.8(15) . . . . ?
C4_12 C5_12 C6_12 F8_12 -61.5(18) . . . . ?
F7_12 C5_12 C6_12 C7_12 179.4(10) . . . . ?
C10_12 C5_12 C6_12 C7_12 -61.9(13) . . . . ?
C4_12 C5_12 C6_12 C7_12 58.7(13) . . . . ?
F9_12 C6_12 C7_12 F10_12 60.5(14) . . . . ?
F8_12 C6_12 C7_12 F10_12 -57.7(16) . . . . ?
C5_12 C6_12 C7_12 F10_12 -178.4(10) . . . . ?
F9_12 C6_12 C7_12 C3_12 -179.9(12) . . . . ?
F8_12 C6_12 C7_12 C3_12 61.9(17) . . . . ?
C5_12 C6_12 C7_12 C3_12 -58.8(13) . . . . ?
F9_12 C6_12 C7_12 C8_12 -59.8(14) . . . . ?
F8_12 C6_12 C7_12 C8_12 -178.0(15) . . . . ?
C5_12 C6_12 C7_12 C8_12 61.3(13) . . . . ?
F4_12 C3_12 C7_12 F10_12 57.5(13) . . . . ?
F3_12 C3_12 C7_12 F10_12 -58.0(12) . . . . ?
C1_12 C3_12 C7_12 F10_12 -179.9(10) . . . . ?
F4_12 C3_12 C7_12 C6_12 -61.7(12) . . . . ?
F3_12 C3_12 C7_12 C6_12 -177.3(10) . . . . ?
C1_12 C3_12 C7_12 C6_12 60.8(12) . . . . ?
F4_12 C3_12 C7_12 C8_12 179.2(10) . . . . ?
F3_12 C3_12 C7_12 C8_12 63.6(11) . . . . ?
C1_12 C3_12 C7_12 C8_12 -58.3(12) . . . . ?
F10_12 C7_12 C8_12 F12_12 -57.5(13) . . . . ?
C6_12 C7_12 C8_12 F12_12 61.9(12) . . . . ?
C3_12 C7_12 C8_12 F12_12 -178.7(10) . . . . ?
F10_12 C7_12 C8_12 F11_12 57.6(12) . . . . ?
C6_12 C7_12 C8_12 F11_12 177.0(10) . . . . ?
C3_12 C7_12 C8_12 F11_12 -63.5(12) . . . . ?
F10_12 C7_12 C8_12 C9_12 178.8(10) . . . . ?
C6_12 C7_12 C8_12 C9_12 -61.7(12) . . . . ?
C3_12 C7_12 C8_12 C9_12 57.7(12) . . . . ?
F12_12 C8_12 C9_12 F13_12 58.0(15) . . . . ?
F11_12 C8_12 C9_12 F13_12 -60.3(14) . . . . ?
C7_12 C8_12 C9_12 F13_12 -179.8(12) . . . . ?
F12_12 C8_12 C9_12 C10_12 -60.8(13) . . . . ?
F11_12 C8_12 C9_12 C10_12 -179.2(9) . . . . ?
C7_12 C8_12 C9_12 C10_12 61.3(12) . . . . ?
F12_12 C8_12 C9_12 C2_12 179.1(10) . . . . ?
F11_12 C8_12 C9_12 C2_12 60.7(13) . . . . ?
C7_12 C8_12 C9_12 C2_12 -58.8(13) . . . . ?
F1_12 C2_12 C9_12 F13_12 59.3(15) . . . . ?
F2_12 C2_12 C9_12 F13_12 -55.6(14) . . . . ?
C1_12 C2_12 C9_12 F13_12 -179.4(11) . . . . ?
F1_12 C2_12 C9_12 C8_12 -61.3(15) . . . . ?
F2_12 C2_12 C9_12 C8_12 -176.2(11) . . . . ?
C1_12 C2_12 C9_12 C8_12 60.0(13) . . . . ?
F1_12 C2_12 C9_12 C10_12 179.1(13) . . . . ?
F2_12 C2_12 C9_12 C10_12 64.2(14) . . . . ?
C1_12 C2_12 C9_12 C10_12 -59.6(13) . . . . ?
F7_12 C5_12 C10_12 F14_12 -58.8(12) . . . . ?
C4_12 C5_12 C10_12 F14_12 60.1(12) . . . . ?
C6_12 C5_12 C10_12 F14_12 -177.3(10) . . . . ?
F7_12 C5_12 C10_12 F15_12 58.1(12) . . . . ?
C4_12 C5_12 C10_12 F15_12 177.0(9) . . . . ?
C6_12 C5_12 C10_12 F15_12 -60.4(12) . . . . ?
F7_12 C5_12 C10_12 C9_12 -179.6(10) . . . . ?
C4_12 C5_12 C10_12 C9_12 -60.7(11) . . . . ?
C6_12 C5_12 C10_12 C9_12 61.9(12) . . . . ?
F13_12 C9_12 C10_12 F14_12 58.4(13) . . . . ?
C8_12 C9_12 C10_12 F14_12 177.3(9) . . . . ?
C2_12 C9_12 C10_12 F14_12 -62.0(12) . . . . ?
F13_12 C9_12 C10_12 F15_12 -57.9(14) . . . . ?
C8_12 C9_12 C10_12 F15_12 61.0(12) . . . . ?
C2_12 C9_12 C10_12 F15_12 -178.2(10) . . . . ?
F13_12 C9_12 C10_12 C5_12 179.8(11) . . . . ?
C8_12 C9_12 C10_12 C5_12 -61.3(11) . . . . ?
C2_12 C9_12 C10_12 C5_12 59.4(12) . . . . ?
O1_3 Al1 O1_4 C1_4 134(3) . . . . ?
O1_6 Al1 O1_4 C1_4 11(3) . . . . ?
O1_5 Al1 O1_4 C1_4 -113(3) . . . . ?
Al1 O1_4 C1_4 C3_4 -99(3) . . . . ?
Al1 O1_4 C1_4 C2_4 21(4) . . . . ?
Al1 O1_4 C1_4 C4_4 145(3) . . . . ?
O1_4 C1_4 C2_4 F2_4 52(2) . . . . ?
C3_4 C1_4 C2_4 F2_4 172.7(16) . . . . ?
C4_4 C1_4 C2_4 F2_4 -72.5(18) . . . . ?
O1_4 C1_4 C2_4 F1_4 -58(2) . . . . ?
C3_4 C1_4 C2_4 F1_4 62.2(18) . . . . ?
C4_4 C1_4 C2_4 F1_4 176.9(15) . . . . ?
O1_4 C1_4 C2_4 C9_4 -177.1(15) . . . . ?
C3_4 C1_4 C2_4 C9_4 -56.5(17) . . . . ?
C4_4 C1_4 C2_4 C9_4 58.2(16) . . . . ?
O1_4 C1_4 C3_4 F3_4 63(2) . . . . ?
C2_4 C1_4 C3_4 F3_4 -62(2) . . . . ?
C4_4 C1_4 C3_4 F3_4 -178.0(16) . . . . ?
O1_4 C1_4 C3_4 F4_4 -61.3(18) . . . . ?
C2_4 C1_4 C3_4 F4_4 173.7(14) . . . . ?
C4_4 C1_4 C3_4 F4_4 57.5(17) . . . . ?
O1_4 C1_4 C3_4 C7_4 -177.9(13) . . . . ?
C2_4 C1_4 C3_4 C7_4 57.0(16) . . . . ?
C4_4 C1_4 C3_4 C7_4 -59.2(15) . . . . ?
O1_4 C1_4 C4_4 F6_4 -64.1(19) . . . . ?
C3_4 C1_4 C4_4 F6_4 178.9(15) . . . . ?
C2_4 C1_4 C4_4 F6_4 63.3(18) . . . . ?
O1_4 C1_4 C4_4 F5_4 55.2(18) . . . . ?
C3_4 C1_4 C4_4 F5_4 -61.8(17) . . . . ?
C2_4 C1_4 C4_4 F5_4 -177.4(14) . . . . ?
O1_4 C1_4 C4_4 C5_4 176.4(13) . . . . ?
C3_4 C1_4 C4_4 C5_4 59.3(15) . . . . ?
C2_4 C1_4 C4_4 C5_4 -56.2(16) . . . . ?
F6_4 C4_4 C5_4 F7_4 55.7(19) . . . . ?
F5_4 C4_4 C5_4 F7_4 -60.0(19) . . . . ?
C1_4 C4_4 C5_4 F7_4 178.9(15) . . . . ?
F6_4 C4_4 C5_4 C6_4 174.1(15) . . . . ?
F5_4 C4_4 C5_4 C6_4 58.4(18) . . . . ?
C1_4 C4_4 C5_4 C6_4 -62.7(16) . . . . ?
F6_4 C4_4 C5_4 C10_4 -64.8(18) . . . . ?
F5_4 C4_4 C5_4 C10_4 179.4(15) . . . . ?
C1_4 C4_4 C5_4 C10_4 58.3(16) . . . . ?
F7_4 C5_4 C6_4 F8_4 58(2) . . . . ?
C10_4 C5_4 C6_4 F8_4 179.5(16) . . . . ?
C4_4 C5_4 C6_4 F8_4 -59.5(19) . . . . ?
F7_4 C5_4 C6_4 F9_4 -59.6(19) . . . . ?
C10_4 C5_4 C6_4 F9_4 62.0(18) . . . . ?
C4_4 C5_4 C6_4 F9_4 -177.0(15) . . . . ?
F7_4 C5_4 C6_4 C7_4 180.0(14) . . . . ?
C10_4 C5_4 C6_4 C7_4 -58.4(16) . . . . ?
C4_4 C5_4 C6_4 C7_4 62.6(16) . . . . ?
F3_4 C3_4 C7_4 F10_4 -52.6(17) . . . . ?
F4_4 C3_4 C7_4 F10_4 61.4(17) . . . . ?
C1_4 C3_4 C7_4 F10_4 -179.5(13) . . . . ?
F3_4 C3_4 C7_4 C8_4 67.1(17) . . . . ?
F4_4 C3_4 C7_4 C8_4 -179.0(14) . . . . ?
C1_4 C3_4 C7_4 C8_4 -59.9(16) . . . . ?
F3_4 C3_4 C7_4 C6_4 -171.4(14) . . . . ?
F4_4 C3_4 C7_4 C6_4 -57.5(16) . . . . ?
C1_4 C3_4 C7_4 C6_4 61.6(16) . . . . ?
F8_4 C6_4 C7_4 F10_4 -58.0(19) . . . . ?
F9_4 C6_4 C7_4 F10_4 57.6(19) . . . . ?
C5_4 C6_4 C7_4 F10_4 178.5(14) . . . . ?
F8_4 C6_4 C7_4 C8_4 -176.7(15) . . . . ?
F9_4 C6_4 C7_4 C8_4 -61.1(18) . . . . ?
C5_4 C6_4 C7_4 C8_4 59.8(16) . . . . ?
F8_4 C6_4 C7_4 C3_4 61.8(18) . . . . ?
F9_4 C6_4 C7_4 C3_4 177.4(15) . . . . ?
C5_4 C6_4 C7_4 C3_4 -61.7(16) . . . . ?
F10_4 C7_4 C8_4 F11_4 58(2) . . . . ?
C3_4 C7_4 C8_4 F11_4 -62.7(18) . . . . ?
C6_4 C7_4 C8_4 F11_4 176.9(15) . . . . ?
F10_4 C7_4 C8_4 F12_4 -57.2(19) . . . . ?
C3_4 C7_4 C8_4 F12_4 -177.9(13) . . . . ?
C6_4 C7_4 C8_4 F12_4 61.7(17) . . . . ?
F10_4 C7_4 C8_4 C9_4 179.5(15) . . . . ?
C3_4 C7_4 C8_4 C9_4 58.8(16) . . . . ?
C6_4 C7_4 C8_4 C9_4 -61.6(16) . . . . ?
F11_4 C8_4 C9_4 F13_4 -59(2) . . . . ?
F12_4 C8_4 C9_4 F13_4 54.8(19) . . . . ?
C7_4 C8_4 C9_4 F13_4 177.2(15) . . . . ?
F11_4 C8_4 C9_4 C10_4 -175.6(16) . . . . ?
F12_4 C8_4 C9_4 C10_4 -62.2(16) . . . . ?
C7_4 C8_4 C9_4 C10_4 60.2(16) . . . . ?
F11_4 C8_4 C9_4 C2_4 66.4(18) . . . . ?
F12_4 C8_4 C9_4 C2_4 179.7(14) . . . . ?
C7_4 C8_4 C9_4 C2_4 -57.8(16) . . . . ?
F2_4 C2_4 C9_4 F13_4 -53(2) . . . . ?
F1_4 C2_4 C9_4 F13_4 58(2) . . . . ?
C1_4 C2_4 C9_4 F13_4 179.0(15) . . . . ?
F2_4 C2_4 C9_4 C10_4 67.9(19) . . . . ?
F1_4 C2_4 C9_4 C10_4 178.7(16) . . . . ?
C1_4 C2_4 C9_4 C10_4 -60.1(17) . . . . ?
F2_4 C2_4 C9_4 C8_4 -174.2(16) . . . . ?
F1_4 C2_4 C9_4 C8_4 -63.3(18) . . . . ?
C1_4 C2_4 C9_4 C8_4 57.8(17) . . . . ?
F7_4 C5_4 C10_4 F15_4 58.6(18) . . . . ?
C6_4 C5_4 C10_4 F15_4 -62.4(17) . . . . ?
C4_4 C5_4 C10_4 F15_4 177.7(13) . . . . ?
F7_4 C5_4 C10_4 F14_4 -58.7(19) . . . . ?
C6_4 C5_4 C10_4 F14_4 -179.7(15) . . . . ?
C4_4 C5_4 C10_4 F14_4 60.4(19) . . . . ?
F7_4 C5_4 C10_4 C9_4 -179.4(13) . . . . ?
C6_4 C5_4 C10_4 C9_4 59.6(16) . . . . ?
C4_4 C5_4 C10_4 C9_4 -60.3(16) . . . . ?
F13_4 C9_4 C10_4 F15_4 -55(2) . . . . ?
C8_4 C9_4 C10_4 F15_4 61.1(18) . . . . ?
C2_4 C9_4 C10_4 F15_4 -179.7(15) . . . . ?
F13_4 C9_4 C10_4 F14_4 59.6(19) . . . . ?
C8_4 C9_4 C10_4 F14_4 176.2(14) . . . . ?
C2_4 C9_4 C10_4 F14_4 -64.7(17) . . . . ?
F13_4 C9_4 C10_4 C5_4 -175.6(15) . . . . ?
C8_4 C9_4 C10_4 C5_4 -59.0(16) . . . . ?
C2_4 C9_4 C10_4 C5_4 60.1(16) . . . . ?
O1_3 Al1 O1_6 C1_6 133(3) . . . . ?
O1_4 Al1 O1_6 C1_6 -118(3) . . . . ?
O1_5 Al1 O1_6 C1_6 -11(4) . . . . ?
Al1 O1_6 C1_6 C2_6 74(4) . . . . ?
Al1 O1_6 C1_6 C3_6 -70(4) . . . . ?
Al1 O1_6 C1_6 C4_6 -173(3) . . . . ?
O1_6 C1_6 C2_6 F2_6 47(2) . . . . ?
C3_6 C1_6 C2_6 F2_6 -170.3(14) . . . . ?
C4_6 C1_6 C2_6 F2_6 -60.9(16) . . . . ?
O1_6 C1_6 C2_6 F1_6 -71(2) . . . . ?
C3_6 C1_6 C2_6 F1_6 72.5(17) . . . . ?
C4_6 C1_6 C2_6 F1_6 -178.2(13) . . . . ?
O1_6 C1_6 C2_6 C9_6 168.2(17) . . . . ?
C3_6 C1_6 C2_6 C9_6 -48.7(17) . . . . ?
C4_6 C1_6 C2_6 C9_6 60.7(15) . . . . ?
O1_6 C1_6 C3_6 F4_6 -53(2) . . . . ?
C2_6 C1_6 C3_6 F4_6 156.1(15) . . . . ?
C4_6 C1_6 C3_6 F4_6 44.1(17) . . . . ?
O1_6 C1_6 C3_6 F3_6 63.6(19) . . . . ?
C2_6 C1_6 C3_6 F3_6 -86.8(17) . . . . ?
C4_6 C1_6 C3_6 F3_6 161.2(14) . . . . ?
O1_6 C1_6 C3_6 C7_6 -171.9(15) . . . . ?
C2_6 C1_6 C3_6 C7_6 37.6(18) . . . . ?
C4_6 C1_6 C3_6 C7_6 -74.4(15) . . . . ?
O1_6 C1_6 C4_6 F5_6 43.9(16) . . . . ?
C2_6 C1_6 C4_6 F5_6 175.9(13) . . . . ?
C3_6 C1_6 C4_6 F5_6 -65.8(15) . . . . ?
O1_6 C1_6 C4_6 F6_6 -68.5(17) . . . . ?
C2_6 C1_6 C4_6 F6_6 63.5(16) . . . . ?
C3_6 C1_6 C4_6 F6_6 -178.2(13) . . . . ?
O1_6 C1_6 C4_6 C5_6 168.4(15) . . . . ?
C2_6 C1_6 C4_6 C5_6 -59.6(16) . . . . ?
C3_6 C1_6 C4_6 C5_6 58.8(15) . . . . ?
F5_6 C4_6 C5_6 F7_6 -59.2(18) . . . . ?
F6_6 C4_6 C5_6 F7_6 61.2(19) . . . . ?
C1_6 C4_6 C5_6 F7_6 -177.3(14) . . . . ?
F5_6 C4_6 C5_6 C10_6 -179.8(13) . . . . ?
F6_6 C4_6 C5_6 C10_6 -59.3(18) . . . . ?
C1_6 C4_6 C5_6 C10_6 62.2(16) . . . . ?
F5_6 C4_6 C5_6 C6_6 74.9(19) . . . . ?
F6_6 C4_6 C5_6 C6_6 -164.7(16) . . . . ?
C1_6 C4_6 C5_6 C6_6 -43.2(19) . . . . ?
F7_6 C5_6 C6_6 F8_6 45.4(17) . . . . ?
C4_6 C5_6 C6_6 F8_6 -85.8(17) . . . . ?
C10_6 C5_6 C6_6 F8_6 158.3(12) . . . . ?
F7_6 C5_6 C6_6 F9_6 -62(2) . . . . ?
C4_6 C5_6 C6_6 F9_6 166.9(15) . . . . ?
C10_6 C5_6 C6_6 F9_6 51.0(17) . . . . ?
F7_6 C5_6 C6_6 C7_6 162.6(14) . . . . ?
C4_6 C5_6 C6_6 C7_6 31(2) . . . . ?
C10_6 C5_6 C6_6 C7_6 -84.6(14) . . . . ?
F8_6 C6_6 F9_6 F12_6 149.7(12) . . . . ?
C7_6 C6_6 F9_6 F12_6 30.7(14) . . . . ?
C5_6 C6_6 F9_6 F12_6 -105.7(15) . . . . ?
F4_6 C3_6 C7_6 F10_6 64.4(19) . . . . ?
F3_6 C3_6 C7_6 F10_6 -49(2) . . . . ?
C1_6 C3_6 C7_6 F10_6 -172.3(16) . . . . ?
F4_6 C3_6 C7_6 C8_6 -167.4(15) . . . . ?
F3_6 C3_6 C7_6 C8_6 79.8(18) . . . . ?
C1_6 C3_6 C7_6 C8_6 -44.1(18) . . . . ?
F4_6 C3_6 C7_6 C6_6 -58.4(17) . . . . ?
F3_6 C3_6 C7_6 C6_6 -171.2(15) . . . . ?
C1_6 C3_6 C7_6 C6_6 64.9(17) . . . . ?
F8_6 C6_6 C7_6 F10_6 -54.3(19) . . . . ?
F9_6 C6_6 C7_6 F10_6 58(2) . . . . ?
C5_6 C6_6 C7_6 F10_6 -161.9(16) . . . . ?
F8_6 C6_6 C7_6 C3_6 69.3(17) . . . . ?
F9_6 C6_6 C7_6 C3_6 -178.3(14) . . . . ?
C5_6 C6_6 C7_6 C3_6 -38.3(18) . . . . ?
F8_6 C6_6 C7_6 C8_6 -168.9(14) . . . . ?
F9_6 C6_6 C7_6 C8_6 -56.6(16) . . . . ?
C5_6 C6_6 C7_6 C8_6 83.4(15) . . . . ?
F10_6 C7_6 C8_6 F11_6 59(2) . . . . ?
C3_6 C7_6 C8_6 F11_6 -70.1(19) . . . . ?
C6_6 C7_6 C8_6 F11_6 174.4(15) . . . . ?
F10_6 C7_6 C8_6 F12_6 -49(2) . . . . ?
C3_6 C7_6 C8_6 F12_6 -178.4(15) . . . . ?
C6_6 C7_6 C8_6 F12_6 66.1(17) . . . . ?
F10_6 C7_6 C8_6 C9_6 -172.5(15) . . . . ?
C3_6 C7_6 C8_6 C9_6 58.2(18) . . . . ?
C6_6 C7_6 C8_6 C9_6 -57.3(15) . . . . ?
F11_6 C8_6 F12_6 F9_6 -157.1(13) . . . . ?
C7_6 C8_6 F12_6 F9_6 -40.0(14) . . . . ?
C9_6 C8_6 F12_6 F9_6 82.4(13) . . . . ?
F11_6 C8_6 C9_6 F13_6 -61.3(19) . . . . ?
F12_6 C8_6 C9_6 F13_6 46.2(18) . . . . ?
C7_6 C8_6 C9_6 F13_6 173.1(13) . . . . ?
F11_6 C8_6 C9_6 C2_6 61.7(18) . . . . ?
F12_6 C8_6 C9_6 C2_6 169.2(14) . . . . ?
C7_6 C8_6 C9_6 C2_6 -63.9(15) . . . . ?
F11_6 C8_6 C9_6 C10_6 -179.9(15) . . . . ?
F12_6 C8_6 C9_6 C10_6 -72.3(17) . . . . ?
C7_6 C8_6 C9_6 C10_6 54.5(16) . . . . ?
F2_6 C2_6 C9_6 F13_6 -54.6(16) . . . . ?
F1_6 C2_6 C9_6 F13_6 54.4(17) . . . . ?
C1_6 C2_6 C9_6 F13_6 179.7(13) . . . . ?
F2_6 C2_6 C9_6 C8_6 -172.5(13) . . . . ?
F1_6 C2_6 C9_6 C8_6 -63.6(15) . . . . ?
C1_6 C2_6 C9_6 C8_6 61.8(15) . . . . ?
F2_6 C2_6 C9_6 C10_6 65.0(15) . . . . ?
F1_6 C2_6 C9_6 C10_6 173.9(13) . . . . ?
C1_6 C2_6 C9_6 C10_6 -60.7(16) . . . . ?
F7_6 C5_6 C10_6 F14_6 -56.3(17) . . . . ?
C4_6 C5_6 C10_6 F14_6 62.4(16) . . . . ?
C6_6 C5_6 C10_6 F14_6 -172.7(13) . . . . ?
F7_6 C5_6 C10_6 F15_6 59.8(18) . . . . ?
C4_6 C5_6 C10_6 F15_6 178.6(15) . . . . ?
C6_6 C5_6 C10_6 F15_6 -56.5(15) . . . . ?
F7_6 C5_6 C10_6 C9_6 -179.5(13) . . . . ?
C4_6 C5_6 C10_6 C9_6 -60.7(15) . . . . ?
C6_6 C5_6 C10_6 C9_6 64.2(13) . . . . ?
F13_6 C9_6 C10_6 F14_6 58.9(16) . . . . ?
C8_6 C9_6 C10_6 F14_6 176.8(13) . . . . ?
C2_6 C9_6 C10_6 F14_6 -64.9(16) . . . . ?
F13_6 C9_6 C10_6 F15_6 -59.9(17) . . . . ?
C8_6 C9_6 C10_6 F15_6 58.0(17) . . . . ?
C2_6 C9_6 C10_6 F15_6 176.3(14) . . . . ?
F13_6 C9_6 C10_6 C5_6 -178.7(12) . . . . ?
C8_6 C9_6 C10_6 C5_6 -60.8(15) . . . . ?
C2_6 C9_6 C10_6 C5_6 57.5(15) . . . . ?
O1_6 Al1 O1_3 C1_3 -11.5(17) . . . . ?
O1_4 Al1 O1_3 C1_3 -137.5(15) . . . . ?
O1_5 Al1 O1_3 C1_3 134.2(14) . . . . ?
Al1 O1_3 C1_3 C4_3 159.7(11) . . . . ?
Al1 O1_3 C1_3 C3_3 -81.0(15) . . . . ?
Al1 O1_3 C1_3 C2_3 40.2(17) . . . . ?
O1_3 C1_3 C2_3 F1_3 -61.6(9) . . . . ?
C4_3 C1_3 C2_3 F1_3 178.9(7) . . . . ?
C3_3 C1_3 C2_3 F1_3 61.9(8) . . . . ?
O1_3 C1_3 C2_3 F2_3 55.4(10) . . . . ?
C4_3 C1_3 C2_3 F2_3 -64.1(9) . . . . ?
C3_3 C1_3 C2_3 F2_3 178.9(7) . . . . ?
O1_3 C1_3 C2_3 C9_3 177.8(7) . . . . ?
C4_3 C1_3 C2_3 C9_3 58.3(9) . . . . ?
C3_3 C1_3 C2_3 C9_3 -58.7(9) . . . . ?
O1_3 C1_3 C3_3 F3_3 60.0(8) . . . . ?
C4_3 C1_3 C3_3 F3_3 179.3(7) . . . . ?
C2_3 C1_3 C3_3 F3_3 -63.7(8) . . . . ?
O1_3 C1_3 C3_3 F4_3 -58.3(9) . . . . ?
C4_3 C1_3 C3_3 F4_3 61.0(9) . . . . ?
C2_3 C1_3 C3_3 F4_3 178.0(7) . . . . ?
O1_3 C1_3 C3_3 C7_3 -177.1(7) . . . . ?
C4_3 C1_3 C3_3 C7_3 -57.9(8) . . . . ?
C2_3 C1_3 C3_3 C7_3 59.1(8) . . . . ?
O1_3 C1_3 C4_3 F6_3 -59.0(9) . . . . ?
C3_3 C1_3 C4_3 F6_3 179.6(7) . . . . ?
C2_3 C1_3 C4_3 F6_3 63.0(9) . . . . ?
O1_3 C1_3 C4_3 F5_3 58.7(9) . . . . ?
C3_3 C1_3 C4_3 F5_3 -62.8(9) . . . . ?
C2_3 C1_3 C4_3 F5_3 -179.3(7) . . . . ?
O1_3 C1_3 C4_3 C5_3 -179.4(7) . . . . ?
C3_3 C1_3 C4_3 C5_3 59.1(9) . . . . ?
C2_3 C1_3 C4_3 C5_3 -57.4(9) . . . . ?
F6_3 C4_3 C5_3 F7_3 57.9(10) . . . . ?
F5_3 C4_3 C5_3 F7_3 -58.1(10) . . . . ?
C1_3 C4_3 C5_3 F7_3 179.5(7) . . . . ?
F6_3 C4_3 C5_3 C6_3 178.4(7) . . . . ?
F5_3 C4_3 C5_3 C6_3 62.5(9) . . . . ?
C1_3 C4_3 C5_3 C6_3 -59.9(9) . . . . ?
F6_3 C4_3 C5_3 C10_3 -62.9(9) . . . . ?
F5_3 C4_3 C5_3 C10_3 -178.8(7) . . . . ?
C1_3 C4_3 C5_3 C10_3 58.8(9) . . . . ?
F7_3 C5_3 C6_3 F8_3 57.1(10) . . . . ?
C10_3 C5_3 C6_3 F8_3 177.9(7) . . . . ?
C4_3 C5_3 C6_3 F8_3 -63.5(9) . . . . ?
F7_3 C5_3 C6_3 F9_3 -58.8(9) . . . . ?
C10_3 C5_3 C6_3 F9_3 62.0(9) . . . . ?
C4_3 C5_3 C6_3 F9_3 -179.4(7) . . . . ?
F7_3 C5_3 C6_3 C7_3 179.8(7) . . . . ?
C10_3 C5_3 C6_3 C7_3 -59.4(9) . . . . ?
C4_3 C5_3 C6_3 C7_3 59.2(9) . . . . ?
F8_3 C6_3 C7_3 F10_3 -58.5(10) . . . . ?
F9_3 C6_3 C7_3 F10_3 58.9(10) . . . . ?
C5_3 C6_3 C7_3 F10_3 179.3(7) . . . . ?
F8_3 C6_3 C7_3 C8_3 -177.0(7) . . . . ?
F9_3 C6_3 C7_3 C8_3 -59.7(10) . . . . ?
C5_3 C6_3 C7_3 C8_3 60.7(9) . . . . ?
F8_3 C6_3 C7_3 C3_3 62.9(9) . . . . ?
F9_3 C6_3 C7_3 C3_3 -179.7(8) . . . . ?
C5_3 C6_3 C7_3 C3_3 -59.3(9) . . . . ?
F3_3 C3_3 C7_3 F10_3 -57.6(10) . . . . ?
F4_3 C3_3 C7_3 F10_3 59.5(10) . . . . ?
C1_3 C3_3 C7_3 F10_3 179.4(7) . . . . ?
F3_3 C3_3 C7_3 C8_3 62.3(9) . . . . ?
F4_3 C3_3 C7_3 C8_3 179.4(7) . . . . ?
C1_3 C3_3 C7_3 C8_3 -60.6(9) . . . . ?
F3_3 C3_3 C7_3 C6_3 -178.4(7) . . . . ?
F4_3 C3_3 C7_3 C6_3 -61.3(9) . . . . ?
C1_3 C3_3 C7_3 C6_3 58.6(9) . . . . ?
F10_3 C7_3 C8_3 F12_3 -57.5(10) . . . . ?
C6_3 C7_3 C8_3 F12_3 61.4(9) . . . . ?
C3_3 C7_3 C8_3 F12_3 -178.4(7) . . . . ?
F10_3 C7_3 C8_3 F11_3 60.3(10) . . . . ?
C6_3 C7_3 C8_3 F11_3 179.3(7) . . . . ?
C3_3 C7_3 C8_3 F11_3 -60.5(9) . . . . ?
F10_3 C7_3 C8_3 C9_3 -179.9(8) . . . . ?
C6_3 C7_3 C8_3 C9_3 -61.0(9) . . . . ?
C3_3 C7_3 C8_3 C9_3 59.2(9) . . . . ?
F1_3 C2_3 C9_3 F13_3 58.0(9) . . . . ?
F2_3 C2_3 C9_3 F13_3 -56.7(9) . . . . ?
C1_3 C2_3 C9_3 F13_3 -179.7(7) . . . . ?
F1_3 C2_3 C9_3 C8_3 -62.9(8) . . . . ?
F2_3 C2_3 C9_3 C8_3 -177.6(6) . . . . ?
C1_3 C2_3 C9_3 C8_3 59.5(8) . . . . ?
F1_3 C2_3 C9_3 C10_3 177.5(7) . . . . ?
F2_3 C2_3 C9_3 C10_3 62.8(8) . . . . ?
C1_3 C2_3 C9_3 C10_3 -60.1(9) . . . . ?
F12_3 C8_3 C9_3 F13_3 57.0(8) . . . . ?
F11_3 C8_3 C9_3 F13_3 -59.7(8) . . . . ?
C7_3 C8_3 C9_3 F13_3 180.0(7) . . . . ?
F12_3 C8_3 C9_3 C2_3 178.3(6) . . . . ?
F11_3 C8_3 C9_3 C2_3 61.5(7) . . . . ?
C7_3 C8_3 C9_3 C2_3 -58.8(8) . . . . ?
F12_3 C8_3 C9_3 C10_3 -62.3(8) . . . . ?
F11_3 C8_3 C9_3 C10_3 -179.0(6) . . . . ?
C7_3 C8_3 C9_3 C10_3 60.7(8) . . . . ?
F7_3 C5_3 C10_3 F14_3 -57.9(10) . . . . ?
C6_3 C5_3 C10_3 F14_3 -178.8(7) . . . . ?
C4_3 C5_3 C10_3 F14_3 63.0(9) . . . . ?
F7_3 C5_3 C10_3 F15_3 57.9(10) . . . . ?
C6_3 C5_3 C10_3 F15_3 -62.9(9) . . . . ?
C4_3 C5_3 C10_3 F15_3 178.8(7) . . . . ?
F7_3 C5_3 C10_3 C9_3 179.5(7) . . . . ?
C6_3 C5_3 C10_3 C9_3 58.6(9) . . . . ?
C4_3 C5_3 C10_3 C9_3 -59.7(9) . . . . ?
F13_3 C9_3 C10_3 F14_3 57.5(8) . . . . ?
C2_3 C9_3 C10_3 F14_3 -62.7(8) . . . . ?
C8_3 C9_3 C10_3 F14_3 177.1(6) . . . . ?
F13_3 C9_3 C10_3 F15_3 -56.6(9) . . . . ?
C2_3 C9_3 C10_3 F15_3 -176.8(7) . . . . ?
C8_3 C9_3 C10_3 F15_3 62.9(8) . . . . ?
F13_3 C9_3 C10_3 C5_3 -179.1(6) . . . . ?
C2_3 C9_3 C10_3 C5_3 60.6(9) . . . . ?
C8_3 C9_3 C10_3 C5_3 -59.6(8) . . . . ?
O1_14 Al1 O1_15 C1_15 -153(2) . . . . ?
O1_12 Al1 O1_15 C1_15 -35(3) . . . . ?
O1_13 Al1 O1_15 C1_15 126(2) . . . . ?
Al1 O1_15 C1_15 C4_15 -160(2) . . . . ?
Al1 O1_15 C1_15 C3_15 -40(3) . . . . ?
Al1 O1_15 C1_15 C2_15 80(3) . . . . ?
O1_15 C1_15 C2_15 F1_15 -56.9(18) . . . . ?
C4_15 C1_15 C2_15 F1_15 179.8(13) . . . . ?
C3_15 C1_15 C2_15 F1_15 66.2(16) . . . . ?
O1_15 C1_15 C2_15 F2_15 57.7(18) . . . . ?
C4_15 C1_15 C2_15 F2_15 -65.6(16) . . . . ?
C3_15 C1_15 C2_15 F2_15 -179.1(13) . . . . ?
O1_15 C1_15 C2_15 C9_15 -179.9(13) . . . . ?
C4_15 C1_15 C2_15 C9_15 56.9(16) . . . . ?
C3_15 C1_15 C2_15 C9_15 -56.7(16) . . . . ?
O1_15 C1_15 C3_15 F4_15 -55.8(18) . . . . ?
C4_15 C1_15 C3_15 F4_15 66.1(16) . . . . ?
C2_15 C1_15 C3_15 F4_15 179.4(14) . . . . ?
O1_15 C1_15 C3_15 F3_15 59.0(18) . . . . ?
C4_15 C1_15 C3_15 F3_15 -179.1(14) . . . . ?
C2_15 C1_15 C3_15 F3_15 -65.8(16) . . . . ?
O1_15 C1_15 C3_15 C7_15 -178.6(14) . . . . ?
C4_15 C1_15 C3_15 C7_15 -56.6(16) . . . . ?
C2_15 C1_15 C3_15 C7_15 56.7(16) . . . . ?
O1_15 C1_15 C4_15 F6_15 -59.0(18) . . . . ?
C3_15 C1_15 C4_15 F6_15 178.8(14) . . . . ?
C2_15 C1_15 C4_15 F6_15 66.1(16) . . . . ?
O1_15 C1_15 C4_15 F5_15 58.6(18) . . . . ?
C3_15 C1_15 C4_15 F5_15 -63.6(16) . . . . ?
C2_15 C1_15 C4_15 F5_15 -176.3(13) . . . . ?
O1_15 C1_15 C4_15 C5_15 178.9(14) . . . . ?
C3_15 C1_15 C4_15 C5_15 56.7(16) . . . . ?
C2_15 C1_15 C4_15 C5_15 -56.0(16) . . . . ?
F6_15 C4_15 C5_15 F7_15 58.5(18) . . . . ?
F5_15 C4_15 C5_15 F7_15 -59.4(17) . . . . ?
C1_15 C4_15 C5_15 F7_15 -179.5(14) . . . . ?
F6_15 C4_15 C5_15 C10_15 -62.3(17) . . . . ?
F5_15 C4_15 C5_15 C10_15 179.8(13) . . . . ?
C1_15 C4_15 C5_15 C10_15 59.7(16) . . . . ?
F6_15 C4_15 C5_15 C6_15 178.0(14) . . . . ?
F5_15 C4_15 C5_15 C6_15 60.1(16) . . . . ?
C1_15 C4_15 C5_15 C6_15 -60.0(16) . . . . ?
F7_15 C5_15 C6_15 F8_15 58.1(17) . . . . ?
C10_15 C5_15 C6_15 F8_15 176.7(12) . . . . ?
C4_15 C5_15 C6_15 F8_15 -62.5(16) . . . . ?
F7_15 C5_15 C6_15 F9_15 -58.2(17) . . . . ?
C10_15 C5_15 C6_15 F9_15 60.5(16) . . . . ?
C4_15 C5_15 C6_15 F9_15 -178.8(12) . . . . ?
F7_15 C5_15 C6_15 C7_15 179.9(13) . . . . ?
C10_15 C5_15 C6_15 C7_15 -61.5(15) . . . . ?
C4_15 C5_15 C6_15 C7_15 59.3(15) . . . . ?
F4_15 C3_15 C7_15 F10_15 56.8(19) . . . . ?
F3_15 C3_15 C7_15 F10_15 -55.3(17) . . . . ?
C1_15 C3_15 C7_15 F10_15 179.7(14) . . . . ?
F4_15 C3_15 C7_15 C6_15 -64.7(17) . . . . ?
F3_15 C3_15 C7_15 C6_15 -176.7(13) . . . . ?
C1_15 C3_15 C7_15 C6_15 58.2(16) . . . . ?
F4_15 C3_15 C7_15 C8_15 177.8(15) . . . . ?
F3_15 C3_15 C7_15 C8_15 65.7(16) . . . . ?
C1_15 C3_15 C7_15 C8_15 -59.3(16) . . . . ?
F8_15 C6_15 C7_15 F10_15 -57.2(16) . . . . ?
F9_15 C6_15 C7_15 F10_15 56.6(17) . . . . ?
C5_15 C6_15 C7_15 F10_15 179.5(13) . . . . ?
F8_15 C6_15 C7_15 C3_15 65.5(15) . . . . ?
F9_15 C6_15 C7_15 C3_15 179.2(13) . . . . ?
C5_15 C6_15 C7_15 C3_15 -57.9(15) . . . . ?
F8_15 C6_15 C7_15 C8_15 -176.3(12) . . . . ?
F9_15 C6_15 C7_15 C8_15 -62.5(15) . . . . ?
C5_15 C6_15 C7_15 C8_15 60.4(15) . . . . ?
F10_15 C7_15 C8_15 F11_15 58.2(17) . . . . ?
C3_15 C7_15 C8_15 F11_15 -64.3(16) . . . . ?
C6_15 C7_15 C8_15 F11_15 177.7(13) . . . . ?
F10_15 C7_15 C8_15 F12_15 -57.2(17) . . . . ?
C3_15 C7_15 C8_15 F12_15 -179.7(13) . . . . ?
C6_15 C7_15 C8_15 F12_15 62.3(16) . . . . ?
F10_15 C7_15 C8_15 C9_15 -179.6(13) . . . . ?
C3_15 C7_15 C8_15 C9_15 57.9(15) . . . . ?
C6_15 C7_15 C8_15 C9_15 -60.1(15) . . . . ?
F11_15 C8_15 C9_15 F13_15 -59.1(18) . . . . ?
F12_15 C8_15 C9_15 F13_15 58.3(18) . . . . ?
C7_15 C8_15 C9_15 F13_15 179.8(14) . . . . ?
F11_15 C8_15 C9_15 C2_15 62.9(17) . . . . ?
F12_15 C8_15 C9_15 C2_15 -179.8(13) . . . . ?
C7_15 C8_15 C9_15 C2_15 -58.3(16) . . . . ?
F11_15 C8_15 C9_15 C10_15 -177.9(13) . . . . ?
F12_15 C8_15 C9_15 C10_15 -60.5(16) . . . . ?
C7_15 C8_15 C9_15 C10_15 61.0(15) . . . . ?
F1_15 C2_15 C9_15 F13_15 58.1(19) . . . . ?
F2_15 C2_15 C9_15 F13_15 -57.1(18) . . . . ?
C1_15 C2_15 C9_15 F13_15 -179.0(14) . . . . ?
F1_15 C2_15 C9_15 C8_15 -63.1(17) . . . . ?
F2_15 C2_15 C9_15 C8_15 -178.3(14) . . . . ?
C1_15 C2_15 C9_15 C8_15 59.8(16) . . . . ?
F1_15 C2_15 C9_15 C10_15 177.8(14) . . . . ?
F2_15 C2_15 C9_15 C10_15 62.6(17) . . . . ?
C1_15 C2_15 C9_15 C10_15 -59.3(16) . . . . ?
F7_15 C5_15 C10_15 F14_15 -58.3(17) . . . . ?
C6_15 C5_15 C10_15 F14_15 -176.7(13) . . . . ?
C4_15 C5_15 C10_15 F14_15 63.2(16) . . . . ?
F7_15 C5_15 C10_15 F15_15 57.6(17) . . . . ?
C6_15 C5_15 C10_15 F15_15 -60.7(16) . . . . ?
C4_15 C5_15 C10_15 F15_15 179.2(13) . . . . ?
F7_15 C5_15 C10_15 C9_15 179.6(13) . . . . ?
C6_15 C5_15 C10_15 C9_15 61.2(15) . . . . ?
C4_15 C5_15 C10_15 C9_15 -58.9(16) . . . . ?
F13_15 C9_15 C10_15 F14_15 57.1(18) . . . . ?
C8_15 C9_15 C10_15 F14_15 176.6(14) . . . . ?
C2_15 C9_15 C10_15 F14_15 -63.9(17) . . . . ?
F13_15 C9_15 C10_15 F15_15 -57.8(18) . . . . ?
C8_15 C9_15 C10_15 F15_15 61.7(17) . . . . ?
C2_15 C9_15 C10_15 F15_15 -178.8(13) . . . . ?
F13_15 C9_15 C10_15 C5_15 179.2(14) . . . . ?
C8_15 C9_15 C10_15 C5_15 -61.3(16) . . . . ?
C2_15 C9_15 C10_15 C5_15 58.2(16) . . . . ?
O1_17 Al1 O1_16 C1_16 -12(2) . . . . ?
Al1 O1_16 C1_16 C3_16 -46(2) . . . . ?
Al1 O1_16 C1_16 C2_16 75.0(19) . . . . ?
Al1 O1_16 C1_16 C4_16 -165.3(14) . . . . ?
O1_16 C1_16 C2_16 F1_16 -59.5(12) . . . . ?
C3_16 C1_16 C2_16 F1_16 64.8(11) . . . . ?
C4_16 C1_16 C2_16 F1_16 179.3(8) . . . . ?
O1_16 C1_16 C2_16 F2_16 56.8(12) . . . . ?
C3_16 C1_16 C2_16 F2_16 -178.9(8) . . . . ?
C4_16 C1_16 C2_16 F2_16 -64.4(11) . . . . ?
O1_16 C1_16 C2_16 C9_16 178.0(9) . . . . ?
C3_16 C1_16 C2_16 C9_16 -57.7(11) . . . . ?
C4_16 C1_16 C2_16 C9_16 56.8(11) . . . . ?
O1_16 C1_16 C3_16 F3_16 59.6(12) . . . . ?
C2_16 C1_16 C3_16 F3_16 -64.3(11) . . . . ?
C4_16 C1_16 C3_16 F3_16 -179.2(8) . . . . ?
O1_16 C1_16 C3_16 F4_16 -57.8(12) . . . . ?
C2_16 C1_16 C3_16 F4_16 178.3(8) . . . . ?
C4_16 C1_16 C3_16 F4_16 63.5(11) . . . . ?
O1_16 C1_16 C3_16 C7_16 -178.9(10) . . . . ?
C2_16 C1_16 C3_16 C7_16 57.1(11) . . . . ?
C4_16 C1_16 C3_16 C7_16 -57.7(11) . . . . ?
O1_16 C1_16 C4_16 F5_16 58.4(12) . . . . ?
C3_16 C1_16 C4_16 F5_16 -64.7(11) . . . . ?
C2_16 C1_16 C4_16 F5_16 -179.1(9) . . . . ?
O1_16 C1_16 C4_16 F6_16 -57.2(12) . . . . ?
C3_16 C1_16 C4_16 F6_16 179.7(8) . . . . ?
C2_16 C1_16 C4_16 F6_16 65.3(11) . . . . ?
O1_16 C1_16 C4_16 C5_16 -179.3(9) . . . . ?
C3_16 C1_16 C4_16 C5_16 57.7(11) . . . . ?
C2_16 C1_16 C4_16 C5_16 -56.7(11) . . . . ?
F5_16 C4_16 C5_16 F7_16 -57.1(12) . . . . ?
F6_16 C4_16 C5_16 F7_16 57.9(11) . . . . ?
C1_16 C4_16 C5_16 F7_16 -179.8(9) . . . . ?
F5_16 C4_16 C5_16 C6_16 63.2(11) . . . . ?
F6_16 C4_16 C5_16 C6_16 178.2(9) . . . . ?
C1_16 C4_16 C5_16 C6_16 -59.5(11) . . . . ?
F5_16 C4_16 C5_16 C10_16 -178.2(9) . . . . ?
F6_16 C4_16 C5_16 C10_16 -63.2(11) . . . . ?
C1_16 C4_16 C5_16 C10_16 59.1(11) . . . . ?
F7_16 C5_16 C6_16 F8_16 57.9(13) . . . . ?
C10_16 C5_16 C6_16 F8_16 179.1(9) . . . . ?
C4_16 C5_16 C6_16 F8_16 -62.3(12) . . . . ?
F7_16 C5_16 C6_16 F9_16 -58.8(13) . . . . ?
C10_16 C5_16 C6_16 F9_16 62.4(12) . . . . ?
C4_16 C5_16 C6_16 F9_16 -179.0(9) . . . . ?
F7_16 C5_16 C6_16 C7_16 179.7(9) . . . . ?
C10_16 C5_16 C6_16 C7_16 -59.1(12) . . . . ?
C4_16 C5_16 C6_16 C7_16 59.5(12) . . . . ?
F8_16 C6_16 C7_16 F10_16 -54.2(14) . . . . ?
F9_16 C6_16 C7_16 F10_16 60.8(13) . . . . ?
C5_16 C6_16 C7_16 F10_16 -179.5(11) . . . . ?
F8_16 C6_16 C7_16 C8_16 -174.8(10) . . . . ?
F9_16 C6_16 C7_16 C8_16 -59.8(12) . . . . ?
C5_16 C6_16 C7_16 C8_16 59.9(12) . . . . ?
F8_16 C6_16 C7_16 C3_16 66.0(12) . . . . ?
F9_16 C6_16 C7_16 C3_16 -179.0(9) . . . . ?
C5_16 C6_16 C7_16 C3_16 -59.3(12) . . . . ?
F3_16 C3_16 C7_16 F10_16 -56.3(13) . . . . ?
F4_16 C3_16 C7_16 F10_16 58.2(13) . . . . ?
C1_16 C3_16 C7_16 F10_16 -179.1(11) . . . . ?
F3_16 C3_16 C7_16 C8_16 62.7(11) . . . . ?
F4_16 C3_16 C7_16 C8_16 177.2(9) . . . . ?
C1_16 C3_16 C7_16 C8_16 -60.2(12) . . . . ?
F3_16 C3_16 C7_16 C6_16 -178.6(9) . . . . ?
F4_16 C3_16 C7_16 C6_16 -64.1(11) . . . . ?
C1_16 C3_16 C7_16 C6_16 58.5(12) . . . . ?
F10_16 C7_16 C8_16 F12_16 -59.7(14) . . . . ?
C6_16 C7_16 C8_16 F12_16 63.0(12) . . . . ?
C3_16 C7_16 C8_16 F12_16 -178.7(9) . . . . ?
F10_16 C7_16 C8_16 F11_16 58.9(13) . . . . ?
C6_16 C7_16 C8_16 F11_16 -178.5(9) . . . . ?
C3_16 C7_16 C8_16 F11_16 -60.1(12) . . . . ?
F10_16 C7_16 C8_16 C9_16 178.8(11) . . . . ?
C6_16 C7_16 C8_16 C9_16 -58.5(11) . . . . ?
C3_16 C7_16 C8_16 C9_16 59.8(11) . . . . ?
F12_16 C8_16 C9_16 F13_16 58.5(12) . . . . ?
F11_16 C8_16 C9_16 F13_16 -59.3(11) . . . . ?
C7_16 C8_16 C9_16 F13_16 179.7(9) . . . . ?
F12_16 C8_16 C9_16 C10_16 -61.2(12) . . . . ?
F11_16 C8_16 C9_16 C10_16 -179.0(8) . . . . ?
C7_16 C8_16 C9_16 C10_16 60.0(11) . . . . ?
F12_16 C8_16 C9_16 C2_16 178.6(9) . . . . ?
F11_16 C8_16 C9_16 C2_16 60.7(11) . . . . ?
C7_16 C8_16 C9_16 C2_16 -60.2(11) . . . . ?
F1_16 C2_16 C9_16 F13_16 55.8(11) . . . . ?
F2_16 C2_16 C9_16 F13_16 -58.3(11) . . . . ?
C1_16 C2_16 C9_16 F13_16 179.7(9) . . . . ?
F1_16 C2_16 C9_16 C10_16 176.4(8) . . . . ?
F2_16 C2_16 C9_16 C10_16 62.3(11) . . . . ?
C1_16 C2_16 C9_16 C10_16 -59.7(11) . . . . ?
F1_16 C2_16 C9_16 C8_16 -63.1(11) . . . . ?
F2_16 C2_16 C9_16 C8_16 -177.1(9) . . . . ?
C1_16 C2_16 C9_16 C8_16 60.8(11) . . . . ?
F13_16 C9_16 C10_16 F14_16 59.0(11) . . . . ?
C8_16 C9_16 C10_16 F14_16 177.9(9) . . . . ?
C2_16 C9_16 C10_16 F14_16 -61.9(11) . . . . ?
F13_16 C9_16 C10_16 F15_16 -57.8(12) . . . . ?
C8_16 C9_16 C10_16 F15_16 61.1(11) . . . . ?
C2_16 C9_16 C10_16 F15_16 -178.7(9) . . . . ?
F13_16 C9_16 C10_16 C5_16 -178.9(9) . . . . ?
C8_16 C9_16 C10_16 C5_16 -60.0(11) . . . . ?
C2_16 C9_16 C10_16 C5_16 60.2(11) . . . . ?
F7_16 C5_16 C10_16 F14_16 -57.9(12) . . . . ?
C6_16 C5_16 C10_16 F14_16 -178.8(9) . . . . ?
C4_16 C5_16 C10_16 F14_16 62.7(11) . . . . ?
F7_16 C5_16 C10_16 F15_16 59.2(12) . . . . ?
C6_16 C5_16 C10_16 F15_16 -61.7(12) . . . . ?
C4_16 C5_16 C10_16 F15_16 179.8(9) . . . . ?
F7_16 C5_16 C10_16 C9_16 179.7(9) . . . . ?
C6_16 C5_16 C10_16 C9_16 58.8(11) . . . . ?
C4_16 C5_16 C10_16 C9_16 -59.7(11) . . . . ?
O1_12 Al1 O1_14 C1_14 -77(2) . . . . ?
O1_13 Al1 O1_14 C1_14 146(2) . . . . ?
O1_15 Al1 O1_14 C1_14 48(3) . . . . ?
Al1 O1_14 C1_14 C2_14 -102(3) . . . . ?
Al1 O1_14 C1_14 C4_14 44(3) . . . . ?
Al1 O1_14 C1_14 C3_14 144(2) . . . . ?
O1_14 C1_14 C2_14 F1_14 -38(2) . . . . ?
C4_14 C1_14 C2_14 F1_14 176.7(14) . . . . ?
C3_14 C1_14 C2_14 F1_14 67.1(17) . . . . ?
O1_14 C1_14 C2_14 F2_14 79(2) . . . . ?
C4_14 C1_14 C2_14 F2_14 -65.8(18) . . . . ?
C3_14 C1_14 C2_14 F2_14 -175.4(14) . . . . ?
O1_14 C1_14 C2_14 C9_14 -163.6(17) . . . . ?
C4_14 C1_14 C2_14 C9_14 51.2(18) . . . . ?
C3_14 C1_14 C2_14 C9_14 -58.4(16) . . . . ?
O1_14 C1_14 C3_14 F3_14 61.8(15) . . . . ?
C2_14 C1_14 C3_14 F3_14 -66.8(16) . . . . ?
C4_14 C1_14 C3_14 F3_14 174.2(13) . . . . ?
O1_14 C1_14 C3_14 F4_14 -53.5(15) . . . . ?
C2_14 C1_14 C3_14 F4_14 178.0(13) . . . . ?
C4_14 C1_14 C3_14 F4_14 59.0(14) . . . . ?
O1_14 C1_14 C3_14 C7_14 -174.8(14) . . . . ?
C2_14 C1_14 C3_14 C7_14 56.7(16) . . . . ?
C4_14 C1_14 C3_14 C7_14 -62.4(15) . . . . ?
O1_14 C1_14 C4_14 F6_14 -66.6(18) . . . . ?
C2_14 C1_14 C4_14 F6_14 83.5(17) . . . . ?
C3_14 C1_14 C4_14 F6_14 -161.9(13) . . . . ?
O1_14 C1_14 C4_14 F5_14 54.8(19) . . . . ?
C2_14 C1_14 C4_14 F5_14 -155.1(14) . . . . ?
C3_14 C1_14 C4_14 F5_14 -40.5(16) . . . . ?
O1_14 C1_14 C4_14 C5_14 169.1(14) . . . . ?
C2_14 C1_14 C4_14 C5_14 -40.8(18) . . . . ?
C3_14 C1_14 C4_14 C5_14 73.8(14) . . . . ?
F6_14 C4_14 C5_14 F7_14 49.7(18) . . . . ?
F5_14 C4_14 C5_14 F7_14 -67.6(16) . . . . ?
C1_14 C4_14 C5_14 F7_14 171.5(14) . . . . ?
F6_14 C4_14 C5_14 C6_14 163.1(14) . . . . ?
F5_14 C4_14 C5_14 C6_14 45.8(14) . . . . ?
C1_14 C4_14 C5_14 C6_14 -75.0(14) . . . . ?
F6_14 C4_14 C5_14 C10_14 -68.4(16) . . . . ?
F5_14 C4_14 C5_14 C10_14 174.3(13) . . . . ?
C1_14 C4_14 C5_14 C10_14 53.5(16) . . . . ?
F7_14 C5_14 C6_14 F8_14 54.0(18) . . . . ?
C10_14 C5_14 C6_14 F8_14 -175.4(15) . . . . ?
C4_14 C5_14 C6_14 F8_14 -59.6(15) . . . . ?
F7_14 C5_14 C6_14 F9_14 -60.8(19) . . . . ?
C10_14 C5_14 C6_14 F9_14 69.8(19) . . . . ?
C4_14 C5_14 C6_14 F9_14 -174.4(13) . . . . ?
F7_14 C5_14 C6_14 C7_14 177.7(15) . . . . ?
C10_14 C5_14 C6_14 C7_14 -51.6(19) . . . . ?
C4_14 C5_14 C6_14 C7_14 64.1(14) . . . . ?
F3_14 C3_14 C7_14 F10_14 -61.3(19) . . . . ?
F4_14 C3_14 C7_14 F10_14 63.7(19) . . . . ?
C1_14 C3_14 C7_14 F10_14 -179.5(15) . . . . ?
F3_14 C3_14 C7_14 C8_14 59.5(18) . . . . ?
F4_14 C3_14 C7_14 C8_14 -175.6(14) . . . . ?
C1_14 C3_14 C7_14 C8_14 -58.8(16) . . . . ?
F3_14 C3_14 C7_14 C6_14 176.8(14) . . . . ?
F4_14 C3_14 C7_14 C6_14 -58.2(18) . . . . ?
C1_14 C3_14 C7_14 C6_14 58.5(16) . . . . ?
F8_14 C6_14 C7_14 F10_14 -54(2) . . . . ?
F9_14 C6_14 C7_14 F10_14 57(2) . . . . ?
C5_14 C6_14 C7_14 F10_14 -178.4(16) . . . . ?
F8_14 C6_14 C7_14 C8_14 -177.5(13) . . . . ?
F9_14 C6_14 C7_14 C8_14 -66.5(16) . . . . ?
C5_14 C6_14 C7_14 C8_14 58.2(16) . . . . ?
F8_14 C6_14 C7_14 C3_14 64.3(17) . . . . ?
F9_14 C6_14 C7_14 C3_14 175.3(14) . . . . ?
C5_14 C6_14 C7_14 C3_14 -60.0(16) . . . . ?
F10_14 C7_14 C8_14 F12_14 -55(2) . . . . ?
C3_14 C7_14 C8_14 F12_14 -173.1(13) . . . . ?
C6_14 C7_14 C8_14 F12_14 68.8(16) . . . . ?
F10_14 C7_14 C8_14 F11_14 56.9(19) . . . . ?
C3_14 C7_14 C8_14 F11_14 -61.0(16) . . . . ?
C6_14 C7_14 C8_14 F11_14 -179.1(12) . . . . ?
F10_14 C7_14 C8_14 C9_14 180.0(16) . . . . ?
C3_14 C7_14 C8_14 C9_14 62.2(16) . . . . ?
C6_14 C7_14 C8_14 C9_14 -55.9(16) . . . . ?
F12_14 C8_14 C9_14 F13_14 58.9(16) . . . . ?
F11_14 C8_14 C9_14 F13_14 -58.7(16) . . . . ?
C7_14 C8_14 C9_14 F13_14 -180.0(12) . . . . ?
F12_14 C8_14 C9_14 C2_14 177.3(11) . . . . ?
F11_14 C8_14 C9_14 C2_14 59.7(14) . . . . ?
C7_14 C8_14 C9_14 C2_14 -61.6(14) . . . . ?
F12_14 C8_14 C9_14 C10_14 -73.5(17) . . . . ?
F11_14 C8_14 C9_14 C10_14 168.9(14) . . . . ?
C7_14 C8_14 C9_14 C10_14 47.6(18) . . . . ?
F1_14 C2_14 C9_14 F13_14 50.9(19) . . . . ?
F2_14 C2_14 C9_14 F13_14 -61.3(16) . . . . ?
C1_14 C2_14 C9_14 F13_14 176.9(14) . . . . ?
F1_14 C2_14 C9_14 C8_14 -65.1(17) . . . . ?
F2_14 C2_14 C9_14 C8_14 -177.3(13) . . . . ?
C1_14 C2_14 C9_14 C8_14 60.9(16) . . . . ?
F1_14 C2_14 C9_14 C10_14 166.1(15) . . . . ?
F2_14 C2_14 C9_14 C10_14 53.8(14) . . . . ?
C1_14 C2_14 C9_14 C10_14 -68.0(15) . . . . ?
F7_14 C5_14 C10_14 F15_14 46(2) . . . . ?
C6_14 C5_14 C10_14 F15_14 -83.9(19) . . . . ?
C4_14 C5_14 C10_14 F15_14 163.6(14) . . . . ?
F7_14 C5_14 C10_14 F14_14 -55.2(19) . . . . ?
C6_14 C5_14 C10_14 F14_14 174.7(14) . . . . ?
C4_14 C5_14 C10_14 F14_14 62.2(16) . . . . ?
F7_14 C5_14 C10_14 C9_14 164.4(15) . . . . ?
C6_14 C5_14 C10_14 C9_14 34.2(19) . . . . ?
C4_14 C5_14 C10_14 C9_14 -78.2(14) . . . . ?
F13_14 C9_14 C10_14 F15_14 -41.1(19) . . . . ?
C8_14 C9_14 C10_14 F15_14 89.8(18) . . . . ?
C2_14 C9_14 C10_14 F15_14 -155.9(15) . . . . ?
F13_14 C9_14 C10_14 F14_14 69(2) . . . . ?
C8_14 C9_14 C10_14 F14_14 -160.4(15) . . . . ?
C2_14 C9_14 C10_14 F14_14 -46.1(18) . . . . ?
F13_14 C9_14 C10_14 C5_14 -163.5(13) . . . . ?
C8_14 C9_14 C10_14 C5_14 -32.7(18) . . . . ?
C2_14 C9_14 C10_14 C5_14 81.6(13) . . . . ?
O1_16 Al1 O1_17 C1_17 -85(2) . . . . ?
Al1 O1_17 C1_17 C3_17 32(3) . . . . ?
Al1 O1_17 C1_17 C2_17 150(2) . . . . ?
Al1 O1_17 C1_17 C4_17 -91(2) . . . . ?
O1_17 C1_17 C2_17 F1_17 -62.7(18) . . . . ?
C3_17 C1_17 C2_17 F1_17 61.3(17) . . . . ?
C4_17 C1_17 C2_17 F1_17 176.4(14) . . . . ?
O1_17 C1_17 C2_17 F2_17 57.8(17) . . . . ?
C3_17 C1_17 C2_17 F2_17 -178.1(13) . . . . ?
C4_17 C1_17 C2_17 F2_17 -63.0(16) . . . . ?
O1_17 C1_17 C2_17 C9_17 179.5(13) . . . . ?
C3_17 C1_17 C2_17 C9_17 -56.4(15) . . . . ?
C4_17 C1_17 C2_17 C9_17 58.6(15) . . . . ?
O1_17 C1_17 C3_17 F4_17 -59.7(18) . . . . ?
C2_17 C1_17 C3_17 F4_17 -177.8(13) . . . . ?
C4_17 C1_17 C3_17 F4_17 65.8(15) . . . . ?
O1_17 C1_17 C3_17 F3_17 50(2) . . . . ?
C2_17 C1_17 C3_17 F3_17 -67.7(17) . . . . ?
C4_17 C1_17 C3_17 F3_17 175.9(15) . . . . ?
O1_17 C1_17 C3_17 C7_17 175.9(13) . . . . ?
C2_17 C1_17 C3_17 C7_17 57.8(15) . . . . ?
C4_17 C1_17 C3_17 C7_17 -58.6(15) . . . . ?
O1_17 C1_17 C4_17 F5_17 62.6(16) . . . . ?
C3_17 C1_17 C4_17 F5_17 -64.9(15) . . . . ?
C2_17 C1_17 C4_17 F5_17 179.7(13) . . . . ?
O1_17 C1_17 C4_17 F6_17 -54.9(18) . . . . ?
C3_17 C1_17 C4_17 F6_17 177.5(14) . . . . ?
C2_17 C1_17 C4_17 F6_17 62.2(16) . . . . ?
O1_17 C1_17 C4_17 C5_17 -171.9(12) . . . . ?
C3_17 C1_17 C4_17 C5_17 60.5(14) . . . . ?
C2_17 C1_17 C4_17 C5_17 -54.9(14) . . . . ?
F5_17 C4_17 C5_17 F7_17 -61.3(17) . . . . ?
F6_17 C4_17 C5_17 F7_17 57.4(17) . . . . ?
C1_17 C4_17 C5_17 F7_17 175.4(13) . . . . ?
F5_17 C4_17 C5_17 C10_17 -179.1(12) . . . . ?
F6_17 C4_17 C5_17 C10_17 -60.3(15) . . . . ?
C1_17 C4_17 C5_17 C10_17 57.7(14) . . . . ?
F5_17 C4_17 C5_17 C6_17 60.0(15) . . . . ?
F6_17 C4_17 C5_17 C6_17 178.7(13) . . . . ?
C1_17 C4_17 C5_17 C6_17 -63.3(14) . . . . ?
F7_17 C5_17 C6_17 F9_17 -55.3(18) . . . . ?
C10_17 C5_17 C6_17 F9_17 62.2(16) . . . . ?
C4_17 C5_17 C6_17 F9_17 -176.5(13) . . . . ?
F7_17 C5_17 C6_17 F8_17 61.5(18) . . . . ?
C10_17 C5_17 C6_17 F8_17 179.0(13) . . . . ?
C4_17 C5_17 C6_17 F8_17 -59.7(16) . . . . ?
F7_17 C5_17 C6_17 C7_17 -175.7(14) . . . . ?
C10_17 C5_17 C6_17 C7_17 -58.2(15) . . . . ?
C4_17 C5_17 C6_17 C7_17 63.1(14) . . . . ?
F9_17 C6_17 C7_17 F10_17 58.4(18) . . . . ?
F8_17 C6_17 C7_17 F10_17 -56.3(19) . . . . ?
C5_17 C6_17 C7_17 F10_17 -179.6(15) . . . . ?
F9_17 C6_17 C7_17 C8_17 -63.1(16) . . . . ?
F8_17 C6_17 C7_17 C8_17 -177.8(13) . . . . ?
C5_17 C6_17 C7_17 C8_17 58.9(15) . . . . ?
F9_17 C6_17 C7_17 C3_17 177.5(13) . . . . ?
F8_17 C6_17 C7_17 C3_17 62.8(16) . . . . ?
C5_17 C6_17 C7_17 C3_17 -60.6(14) . . . . ?
F4_17 C3_17 C7_17 F10_17 55.6(17) . . . . ?
F3_17 C3_17 C7_17 F10_17 -54.8(18) . . . . ?
C1_17 C3_17 C7_17 F10_17 179.9(14) . . . . ?
F4_17 C3_17 C7_17 C6_17 -65.1(15) . . . . ?
F3_17 C3_17 C7_17 C6_17 -175.4(13) . . . . ?
C1_17 C3_17 C7_17 C6_17 59.3(15) . . . . ?
F4_17 C3_17 C7_17 C8_17 175.6(13) . . . . ?
F3_17 C3_17 C7_17 C8_17 65.3(16) . . . . ?
C1_17 C3_17 C7_17 C8_17 -60.0(15) . . . . ?
F10_17 C7_17 C8_17 F11_17 56.9(19) . . . . ?
C6_17 C7_17 C8_17 F11_17 179.2(14) . . . . ?
C3_17 C7_17 C8_17 F11_17 -62.3(17) . . . . ?
F10_17 C7_17 C8_17 F12_17 -61.5(18) . . . . ?
C6_17 C7_17 C8_17 F12_17 60.7(16) . . . . ?
C3_17 C7_17 C8_17 F12_17 179.2(13) . . . . ?
F10_17 C7_17 C8_17 C9_17 177.2(14) . . . . ?
C6_17 C7_17 C8_17 C9_17 -60.5(15) . . . . ?
C3_17 C7_17 C8_17 C9_17 58.0(15) . . . . ?
F11_17 C8_17 C9_17 F13_17 -60.6(18) . . . . ?
F12_17 C8_17 C9_17 F13_17 59.1(17) . . . . ?
C7_17 C8_17 C9_17 F13_17 -179.4(13) . . . . ?
F11_17 C8_17 C9_17 C2_17 61.2(17) . . . . ?
F12_17 C8_17 C9_17 C2_17 -179.2(13) . . . . ?
C7_17 C8_17 C9_17 C2_17 -57.7(15) . . . . ?
F11_17 C8_17 C9_17 C10_17 -180.0(13) . . . . ?
F12_17 C8_17 C9_17 C10_17 -60.3(16) . . . . ?
C7_17 C8_17 C9_17 C10_17 61.2(15) . . . . ?
F1_17 C2_17 C9_17 F13_17 55.6(18) . . . . ?
F2_17 C2_17 C9_17 F13_17 -60.0(16) . . . . ?
C1_17 C2_17 C9_17 F13_17 178.2(12) . . . . ?
F1_17 C2_17 C9_17 C8_17 -64.5(17) . . . . ?
F2_17 C2_17 C9_17 C8_17 179.9(13) . . . . ?
C1_17 C2_17 C9_17 C8_17 58.1(15) . . . . ?
F1_17 C2_17 C9_17 C10_17 175.2(15) . . . . ?
F2_17 C2_17 C9_17 C10_17 59.5(15) . . . . ?
C1_17 C2_17 C9_17 C10_17 -62.2(15) . . . . ?
F7_17 C5_17 C10_17 F14_17 -62(2) . . . . ?
C4_17 C5_17 C10_17 F14_17 58.7(18) . . . . ?
C6_17 C5_17 C10_17 F14_17 177.7(15) . . . . ?
F7_17 C5_17 C10_17 F15_17 59.0(18) . . . . ?
C4_17 C5_17 C10_17 F15_17 179.6(13) . . . . ?
C6_17 C5_17 C10_17 F15_17 -61.5(16) . . . . ?
F7_17 C5_17 C10_17 C9_17 178.2(15) . . . . ?
C4_17 C5_17 C10_17 C9_17 -61.2(15) . . . . ?
C6_17 C5_17 C10_17 C9_17 57.7(15) . . . . ?
F13_17 C9_17 C10_17 F14_17 59.2(18) . . . . ?
C8_17 C9_17 C10_17 F14_17 177.8(14) . . . . ?
C2_17 C9_17 C10_17 F14_17 -61.2(16) . . . . ?
F13_17 C9_17 C10_17 F15_17 -59.0(17) . . . . ?
C8_17 C9_17 C10_17 F15_17 59.6(16) . . . . ?
C2_17 C9_17 C10_17 F15_17 -179.4(13) . . . . ?
F13_17 C9_17 C10_17 C5_17 -177.8(13) . . . . ?
C8_17 C9_17 C10_17 C5_17 -59.2(15) . . . . ?
C2_17 C9_17 C10_17 C5_17 61.8(15) . . . . ?
O1_14 Al1 O1_13 C1_13 151.5(19) . . . . ?
O1_12 Al1 O1_13 C1_13 48(2) . . . . ?
O1_15 Al1 O1_13 C1_13 -105.2(19) . . . . ?
Al1 O1_13 C1_13 C2_13 -2(2) . . . . ?
Al1 O1_13 C1_13 C4_13 118.7(17) . . . . ?
Al1 O1_13 C1_13 C3_13 -121.3(17) . . . . ?
O1_13 C1_13 C2_13 F2_13 55.1(15) . . . . ?
C4_13 C1_13 C2_13 F2_13 -66.7(13) . . . . ?
C3_13 C1_13 C2_13 F2_13 177.9(11) . . . . ?
O1_13 C1_13 C2_13 F1_13 -61.4(15) . . . . ?
C4_13 C1_13 C2_13 F1_13 176.7(11) . . . . ?
C3_13 C1_13 C2_13 F1_13 61.4(13) . . . . ?
O1_13 C1_13 C2_13 C9_13 177.9(10) . . . . ?
C4_13 C1_13 C2_13 C9_13 56.0(14) . . . . ?
C3_13 C1_13 C2_13 C9_13 -59.3(13) . . . . ?
O1_13 C1_13 C3_13 F3_13 63.2(15) . . . . ?
C2_13 C1_13 C3_13 F3_13 -61.0(14) . . . . ?
C4_13 C1_13 C3_13 F3_13 -176.2(12) . . . . ?
O1_13 C1_13 C3_13 F4_13 -56.3(14) . . . . ?
C2_13 C1_13 C3_13 F4_13 179.5(11) . . . . ?
C4_13 C1_13 C3_13 F4_13 64.3(13) . . . . ?
O1_13 C1_13 C3_13 C7_13 -175.1(10) . . . . ?
C2_13 C1_13 C3_13 C7_13 60.7(13) . . . . ?
C4_13 C1_13 C3_13 C7_13 -54.5(13) . . . . ?
O1_13 C1_13 C4_13 F5_13 56.4(14) . . . . ?
C2_13 C1_13 C4_13 F5_13 -178.8(11) . . . . ?
C3_13 C1_13 C4_13 F5_13 -65.8(13) . . . . ?
O1_13 C1_13 C4_13 F6_13 -60.3(13) . . . . ?
C2_13 C1_13 C4_13 F6_13 64.5(13) . . . . ?
C3_13 C1_13 C4_13 F6_13 177.5(11) . . . . ?
O1_13 C1_13 C4_13 C5_13 179.3(10) . . . . ?
C2_13 C1_13 C4_13 C5_13 -56.0(13) . . . . ?
C3_13 C1_13 C4_13 C5_13 57.0(13) . . . . ?
F5_13 C4_13 C5_13 F7_13 -60.2(16) . . . . ?
F6_13 C4_13 C5_13 F7_13 58.7(15) . . . . ?
C1_13 C4_13 C5_13 F7_13 177.4(12) . . . . ?
F5_13 C4_13 C5_13 C6_13 61.5(14) . . . . ?
F6_13 C4_13 C5_13 C6_13 -179.7(12) . . . . ?
C1_13 C4_13 C5_13 C6_13 -60.9(13) . . . . ?
F5_13 C4_13 C5_13 C10_13 -177.8(12) . . . . ?
F6_13 C4_13 C5_13 C10_13 -58.9(14) . . . . ?
C1_13 C4_13 C5_13 C10_13 59.9(14) . . . . ?
F7_13 C5_13 C6_13 F8_13 57.4(15) . . . . ?
C4_13 C5_13 C6_13 F8_13 -63.8(14) . . . . ?
C10_13 C5_13 C6_13 F8_13 175.7(11) . . . . ?
F7_13 C5_13 C6_13 F9_13 -58.0(15) . . . . ?
C4_13 C5_13 C6_13 F9_13 -179.2(11) . . . . ?
C10_13 C5_13 C6_13 F9_13 60.3(14) . . . . ?
F7_13 C5_13 C6_13 C7_13 -177.9(11) . . . . ?
C4_13 C5_13 C6_13 C7_13 60.9(13) . . . . ?
C10_13 C5_13 C6_13 C7_13 -59.6(13) . . . . ?
F8_13 C6_13 C7_13 F10_13 -56.5(15) . . . . ?
F9_13 C6_13 C7_13 F10_13 61.1(14) . . . . ?
C5_13 C6_13 C7_13 F10_13 -179.1(11) . . . . ?
F8_13 C6_13 C7_13 C8_13 -177.4(12) . . . . ?
F9_13 C6_13 C7_13 C8_13 -59.9(14) . . . . ?
C5_13 C6_13 C7_13 C8_13 60.0(13) . . . . ?
F8_13 C6_13 C7_13 C3_13 63.5(15) . . . . ?
F9_13 C6_13 C7_13 C3_13 -178.9(11) . . . . ?
C5_13 C6_13 C7_13 C3_13 -59.1(13) . . . . ?
F3_13 C3_13 C7_13 F10_13 -64.2(17) . . . . ?
F4_13 C3_13 C7_13 F10_13 55.4(15) . . . . ?
C1_13 C3_13 C7_13 F10_13 174.4(12) . . . . ?
F3_13 C3_13 C7_13 C6_13 177.6(14) . . . . ?
F4_13 C3_13 C7_13 C6_13 -62.9(14) . . . . ?
C1_13 C3_13 C7_13 C6_13 56.2(14) . . . . ?
F3_13 C3_13 C7_13 C8_13 58.2(16) . . . . ?
F4_13 C3_13 C7_13 C8_13 177.7(11) . . . . ?
C1_13 C3_13 C7_13 C8_13 -63.2(14) . . . . ?
F10_13 C7_13 C8_13 F11_13 58.4(15) . . . . ?
C6_13 C7_13 C8_13 F11_13 176.7(12) . . . . ?
C3_13 C7_13 C8_13 F11_13 -63.2(14) . . . . ?
F10_13 C7_13 C8_13 F12_13 -55.6(14) . . . . ?
C6_13 C7_13 C8_13 F12_13 62.8(13) . . . . ?
C3_13 C7_13 C8_13 F12_13 -177.2(10) . . . . ?
F10_13 C7_13 C8_13 C9_13 -177.9(11) . . . . ?
C6_13 C7_13 C8_13 C9_13 -59.5(13) . . . . ?
C3_13 C7_13 C8_13 C9_13 60.5(13) . . . . ?
F11_13 C8_13 C9_13 F13_13 -57.8(14) . . . . ?
F12_13 C8_13 C9_13 F13_13 57.3(14) . . . . ?
C7_13 C8_13 C9_13 F13_13 179.4(10) . . . . ?
F11_13 C8_13 C9_13 C10_13 -177.6(11) . . . . ?
F12_13 C8_13 C9_13 C10_13 -62.5(13) . . . . ?
C7_13 C8_13 C9_13 C10_13 59.6(13) . . . . ?
F11_13 C8_13 C9_13 C2_13 64.3(14) . . . . ?
F12_13 C8_13 C9_13 C2_13 179.5(10) . . . . ?
C7_13 C8_13 C9_13 C2_13 -58.5(13) . . . . ?
F2_13 C2_13 C9_13 F13_13 -55.9(15) . . . . ?
F1_13 C2_13 C9_13 F13_13 58.1(15) . . . . ?
C1_13 C2_13 C9_13 F13_13 -179.7(12) . . . . ?
F2_13 C2_13 C9_13 C10_13 64.8(14) . . . . ?
F1_13 C2_13 C9_13 C10_13 178.9(11) . . . . ?
C1_13 C2_13 C9_13 C10_13 -58.9(14) . . . . ?
F2_13 C2_13 C9_13 C8_13 -176.1(12) . . . . ?
F1_13 C2_13 C9_13 C8_13 -62.0(14) . . . . ?
C1_13 C2_13 C9_13 C8_13 60.2(13) . . . . ?
F13_13 C9_13 C10_13 F14_13 57.4(14) . . . . ?
C8_13 C9_13 C10_13 F14_13 176.8(10) . . . . ?
C2_13 C9_13 C10_13 F14_13 -65.0(13) . . . . ?
F13_13 C9_13 C10_13 F15_13 -57.8(15) . . . . ?
C8_13 C9_13 C10_13 F15_13 61.6(13) . . . . ?
C2_13 C9_13 C10_13 F15_13 179.8(11) . . . . ?
F13_13 C9_13 C10_13 C5_13 -177.8(11) . . . . ?
C8_13 C9_13 C10_13 C5_13 -58.4(13) . . . . ?
C2_13 C9_13 C10_13 C5_13 59.8(13) . . . . ?
F7_13 C5_13 C10_13 F14_13 -59.0(15) . . . . ?
C6_13 C5_13 C10_13 F14_13 -179.6(11) . . . . ?
C4_13 C5_13 C10_13 F14_13 60.4(14) . . . . ?
F7_13 C5_13 C10_13 F15_13 58.2(15) . . . . ?
C6_13 C5_13 C10_13 F15_13 -62.4(13) . . . . ?
C4_13 C5_13 C10_13 F15_13 177.7(11) . . . . ?
F7_13 C5_13 C10_13 C9_13 179.0(12) . . . . ?
C6_13 C5_13 C10_13 C9_13 58.5(13) . . . . ?
C4_13 C5_13 C10_13 C9_13 -61.5(13) . . . . ?

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_IKmjs_AM31_a
_database_code_depnum_ccdc_archive 'CCDC 2224628'
loop_
_audit_author_name
_audit_author_address
'Burkhard Butschke'
;Albert Ludwigs Universitaet Freiburg
Germany
;
_audit_update_record             
;
2022-12-06 deposited with the CCDC.	2023-03-10 downloaded from the CCDC.
;
_audit_creation_method           
;FinalCif V113 by Daniel Kratzert, Freiburg 2022,
https://dkratzert.de/finalcif.html
;
_shelx_SHELXL_version_number     2018/3
_chemical_name_systematic        ?
_chemical_name_common            ?
_chemical_formula_sum            'C60 H17 Al Cl2 F60 O4'
_chemical_formula_moiety         'C40 Al F60 O4 1-, C19 H15 1+, C H2 Cl2'
_chemical_formula_weight         2039.62
_chemical_melting_point          ?
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_H-M_alt        'P 21/n'
_space_group_name_Hall           '-P 2yn'
_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;

loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'

_cell_length_a                   12.724(9)
_cell_length_b                   22.259(17)
_cell_length_c                   23.784(18)
_cell_angle_alpha                90
_cell_angle_beta                 101.54(2)
_cell_angle_gamma                90
_cell_volume                     6600(8)
_cell_formula_units_Z            4
_cell_measurement_temperature    100(2)
_cell_measurement_reflns_used    9044
_cell_measurement_theta_min      2.2
_cell_measurement_theta_max      31.4815
_exptl_crystal_description       block
_exptl_crystal_colour            yellow
_exptl_crystal_recrystallization_method 
'Crystals were obtained at roomtemperature by slow diffusionof pentane into a solution ofthe compound dissolved in1,2-difluorobenzene by the aidof layering.'
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_density_diffrn    2.053
_exptl_crystal_F_000             3984
_exptl_crystal_size_max          0.350
_exptl_crystal_size_mid          0.200
_exptl_crystal_size_min          0.200
_exptl_absorpt_coefficient_mu    0.334
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_correction_T_min  0.7076
_exptl_absorpt_correction_T_max  0.7462
_exptl_absorpt_process_details   
;SADABS-2016/2 - Bruker AXS area detector scaling and absorption correction:
Krause, L., Herbst-Irmer, R., Sheldrick G.M. & Stalke D., J. Appl. Cryst. 48
(2015) 3-10
;
_exptl_absorpt_special_details   ?
_shelx_estimated_absorpt_T_min   0.892
_shelx_estimated_absorpt_T_max   0.936
_exptl_transmission_factor_min   ?
_exptl_transmission_factor_max   ?
_exptl_special_details           ?
_diffrn_ambient_temperature      100(2)
_diffrn_ambient_environment      N~2~
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_monochromator  'mirror optics'
_olex2_diffrn_ambient_temperature_device 'Oxford Cryostream 800'
_diffrn_measurement_ambient_temperature_device_make ?
_diffrn_radiation_probe          x-ray
_diffrn_source                   'microfocus sealed X-ray tube'
_diffrn_source_type              'Incoatec I\ms'
_diffrn_source_voltage           50.0
_diffrn_source_current           0.6
_diffrn_detector                 CCD
_diffrn_detector_type            'Bruker APEXII'
_diffrn_detector_area_resol_mean 8.3
_diffrn_measurement_device       'three-circle diffractometer'
_diffrn_measurement_device_type  'Bruker APEX2 QUAZAR'
_diffrn_measurement_method       'ω and φ scans'
_diffrn_measurement_specimen_support 'MiTeGen micromount'
_diffrn_reflns_number            240992
_diffrn_reflns_av_unetI/netI     0.0217
_diffrn_reflns_av_R_equivalents  0.0410
_diffrn_reflns_theta_min         1.265
_diffrn_reflns_theta_max         31.540
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_limit_h_min       -18
_diffrn_reflns_limit_h_max       18
_diffrn_reflns_limit_k_min       -32
_diffrn_reflns_limit_k_max       32
_diffrn_reflns_limit_l_min       -34
_diffrn_reflns_limit_l_max       34
_diffrn_measured_fraction_theta_max 0.995
_diffrn_measured_fraction_theta_full 1.000
_diffrn_reflns_Laue_measured_fraction_max 0.995
_diffrn_reflns_Laue_measured_fraction_full 1.000
_diffrn_reflns_point_group_measured_fraction_max 0.995
_diffrn_reflns_point_group_measured_fraction_full 1.000
_reflns_number_total             21931
_reflns_number_gt                16820
_reflns_threshold_expression     'I > 2σ(I)'
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_max     .
_reflns_Friedel_fraction_full    .
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_computing_data_collection       
'Bruker BIS 2018.9.0.3/05-Dec-2018 && APEX3_2018.7-2'
_computing_cell_refinement       'SAINT V8.40B'
_computing_data_reduction        'SAINT V8.40B'
_computing_structure_solution    'SHELXT 2018/2 (Sheldrick, 2018)'
_computing_structure_refinement  'SHELXL-2018/3 (Sheldrick, 2018)'
_computing_molecular_graphics    ?
_computing_publication_material  ?
_refine_special_details          ?
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0532P)²+6.6430P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   ?
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    constr
_refine_ls_number_reflns         21931
_refine_ls_number_parameters     1172
_refine_ls_number_restraints     83
_refine_ls_R_factor_all          0.0655
_refine_ls_R_factor_gt           0.0458
_refine_ls_wR_factor_ref         0.1270
_refine_ls_wR_factor_gt          0.1143
_refine_ls_goodness_of_fit_ref   1.049
_refine_ls_restrained_S_all      1.048
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_diff_density_max         0.811
_refine_diff_density_min         -0.625
_refine_diff_density_rms         0.073
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       .

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Al Al 0.0645 0.0514 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Al1 Al 0.55020(3) 0.73692(2) 0.48876(2) 0.00989(8) Uani 1 1 d . . . . .
C1 C 0.87668(12) 0.55257(7) 0.28866(6) 0.0142(3) Uani 1 1 d . . . . .
C2 C 0.94674(13) 0.53025(7) 0.25271(7) 0.0152(3) Uani 1 1 d . . . . .
C3 C 1.01165(13) 0.57012(7) 0.22866(7) 0.0162(3) Uani 1 1 d . . . . .
H3 H 1.011554 0.611756 0.237440 0.019 Uiso 1 1 calc R U . . .
C4 C 1.07556(14) 0.54881(9) 0.19227(7) 0.0220(3) Uani 1 1 d . . . . .
H4 H 1.117535 0.575870 0.175089 0.026 Uiso 1 1 calc R U . . .
C5 C 1.07797(15) 0.48748(9) 0.18100(8) 0.0246(4) Uani 1 1 d . . . . .
H5 H 1.122339 0.472852 0.156296 0.029 Uiso 1 1 calc R U . . .
C6 C 1.01632(16) 0.44745(8) 0.20542(7) 0.0238(4) Uani 1 1 d . . . . .
H6 H 1.019933 0.405635 0.198041 0.029 Uiso 1 1 calc R U . . .
C7 C 0.94967(15) 0.46836(7) 0.24046(7) 0.0197(3) Uani 1 1 d . . . . .
H7 H 0.905950 0.441081 0.256234 0.024 Uiso 1 1 calc R U . . .
C8 C 0.77735(14) 0.52153(7) 0.28966(7) 0.0183(3) Uani 1 1 d . . . . .
C9 C 0.71673(16) 0.49597(9) 0.23925(8) 0.0266(4) Uani 1 1 d . . . . .
H9 H 0.740191 0.499581 0.203910 0.032 Uiso 1 1 calc R U . . .
C10 C 0.62290(17) 0.46563(11) 0.24156(10) 0.0353(5) Uani 1 1 d . . . . .
H10 H 0.580596 0.449624 0.207379 0.042 Uiso 1 1 calc R U . . .
C11 C 0.59001(17) 0.45833(9) 0.29320(10) 0.0322(4) Uani 1 1 d . . . . .
H11 H 0.526526 0.436307 0.294384 0.039 Uiso 1 1 calc R U . . .
C12 C 0.64918(16) 0.48297(8) 0.34329(9) 0.0263(4) Uani 1 1 d . . . . .
H12 H 0.626311 0.477608 0.378617 0.032 Uiso 1 1 calc R U . . .
C13 C 0.74127(15) 0.51528(8) 0.34180(8) 0.0207(3) Uani 1 1 d . . . . .
H13 H 0.780350 0.533305 0.375838 0.025 Uiso 1 1 calc R U . . .
C14 C 0.90430(12) 0.60546(7) 0.32350(6) 0.0134(3) Uani 1 1 d . . . . .
C15 C 0.82234(12) 0.64476(7) 0.33237(7) 0.0157(3) Uani 1 1 d . . . . .
H15 H 0.749633 0.636002 0.315872 0.019 Uiso 1 1 calc R U . . .
C16 C 0.84762(13) 0.69606(7) 0.36506(7) 0.0178(3) Uani 1 1 d . . . . .
H16 H 0.792740 0.723489 0.369625 0.021 Uiso 1 1 calc R U . . .
C17 C 0.95361(13) 0.70739(8) 0.39122(8) 0.0193(3) Uani 1 1 d . . . . .
H17 H 0.970389 0.741969 0.414712 0.023 Uiso 1 1 calc R U . . .
C18 C 1.03545(13) 0.66867(8) 0.38343(8) 0.0200(3) Uani 1 1 d . . . . .
H18 H 1.107452 0.676634 0.401897 0.024 Uiso 1 1 calc R U . . .
C19 C 1.01179(12) 0.61863(7) 0.34877(7) 0.0166(3) Uani 1 1 d . . . . .
H19 H 1.067858 0.593148 0.341995 0.020 Uiso 1 1 calc R U . . .
O1_1 O 0.60298(9) 0.66555(5) 0.49974(5) 0.0173(2) Uani 1 1 d . . . . .
C1_1 C 0.67626(12) 0.62788(7) 0.52951(6) 0.0132(3) Uani 1 1 d . . . . .
C2_1 C 0.78131(14) 0.62691(7) 0.50502(7) 0.0180(3) Uani 1 1 d . . . . .
F1_1 F 0.75871(10) 0.61230(5) 0.44885(4) 0.0267(2) Uani 1 1 d . . . . .
F2_1 F 0.82476(9) 0.68216(5) 0.50787(5) 0.0270(2) Uani 1 1 d . . . . .
C3_1 C 0.63058(13) 0.56251(7) 0.52455(7) 0.0176(3) Uani 1 1 d . . . . .
F3_1 F 0.60315(10) 0.54603(5) 0.46900(5) 0.0283(2) Uani 1 1 d . . . . .
F4_1 F 0.53982(8) 0.56005(5) 0.54557(5) 0.0280(2) Uani 1 1 d . . . . .
C4_1 C 0.70782(13) 0.64348(7) 0.59458(7) 0.0161(3) Uani 1 1 d . . . . .
F5_1 F 0.62066(9) 0.64350(5) 0.61849(5) 0.0251(2) Uani 1 1 d . . . . .
F6_1 F 0.74763(9) 0.69963(5) 0.60119(5) 0.0245(2) Uani 1 1 d . . . . .
C5_1 C 0.79137(13) 0.59822(8) 0.62713(7) 0.0177(3) Uani 1 1 d . . . . .
F7_1 F 0.81715(10) 0.61279(6) 0.68380(5) 0.0302(3) Uani 1 1 d . . . . .
C6_1 C 0.74198(14) 0.53469(8) 0.62124(7) 0.0190(3) Uani 1 1 d . . . . .
F8_1 F 0.65462(10) 0.53210(5) 0.64499(5) 0.0299(3) Uani 1 1 d . . . . .
F9_1 F 0.81248(10) 0.49504(5) 0.65112(5) 0.0269(2) Uani 1 1 d . . . . .
C7_1 C 0.71313(13) 0.51681(7) 0.55727(7) 0.0178(3) Uani 1 1 d . . . . .
F10_1 F 0.67110(10) 0.46064(5) 0.55197(6) 0.0317(3) Uani 1 1 d . . . . .
C8_1 C 0.81571(15) 0.51801(8) 0.53184(7) 0.0202(3) Uani 1 1 d . . . . .
F11_1 F 0.79393(11) 0.50043(5) 0.47659(5) 0.0303(3) Uani 1 1 d . . . . .
F12_1 F 0.88754(10) 0.47767(5) 0.55900(5) 0.0283(2) Uani 1 1 d . . . . .
C9_1 C 0.86460(13) 0.58169(8) 0.53728(8) 0.0199(3) Uani 1 1 d . . . . .
F13_1 F 0.95498(10) 0.58245(6) 0.51484(6) 0.0347(3) Uani 1 1 d . . . . .
C10_1 C 0.89335(13) 0.59935(8) 0.60133(8) 0.0216(3) Uani 1 1 d . . . . .
F14_1 F 0.93833(9) 0.65430(6) 0.60772(6) 0.0342(3) Uani 1 1 d . . . . .
F15_1 F 0.96790(9) 0.56127(6) 0.63023(5) 0.0321(3) Uani 1 1 d . . . . .
O1_2 O 0.65298(9) 0.78732(5) 0.48551(5) 0.0163(2) Uani 1 1 d . . . . .
C1_2 C 0.69522(12) 0.84284(7) 0.49283(6) 0.0124(3) Uani 1 1 d . . . . .
C2_2 C 0.62182(12) 0.89194(7) 0.45826(7) 0.0157(3) Uani 1 1 d . . . . .
F1_2 F 0.59967(9) 0.87807(5) 0.40201(4) 0.0234(2) Uani 1 1 d . . . . .
F2_2 F 0.52665(8) 0.89315(5) 0.47524(5) 0.0248(2) Uani 1 1 d . . . . .
C3_2 C 0.80414(12) 0.84400(7) 0.47172(7) 0.0152(3) Uani 1 1 d . . . . .
F3_2 F 0.78832(9) 0.82805(5) 0.41594(5) 0.0220(2) Uani 1 1 d . . . . .
F4_2 F 0.87299(8) 0.80319(5) 0.50041(5) 0.0223(2) Uani 1 1 d . . . . .
C4_2 C 0.72031(13) 0.86266(7) 0.55709(7) 0.0155(3) Uani 1 1 d . . . . .
F5_2 F 0.78545(9) 0.82261(5) 0.58908(5) 0.0238(2) Uani 1 1 d . . . . .
F6_2 F 0.62965(9) 0.86354(5) 0.57828(5) 0.0242(2) Uani 1 1 d . . . . .
C5_2 C 0.77286(12) 0.92584(7) 0.56484(7) 0.0148(3) Uani 1 1 d . . . . .
F7_2 F 0.79159(9) 0.94181(5) 0.62141(4) 0.0240(2) Uani 1 1 d . . . . .
C6_2 C 0.87993(12) 0.92451(7) 0.54378(7) 0.0176(3) Uani 1 1 d . . . . .
F8_2 F 0.94853(8) 0.88566(5) 0.57501(5) 0.0265(2) Uani 1 1 d . . . . .
F9_2 F 0.92822(8) 0.97881(5) 0.55144(5) 0.0257(2) Uani 1 1 d . . . . .
C7_2 C 0.85762(12) 0.90692(7) 0.47956(7) 0.0167(3) Uani 1 1 d . . . . .
F10_2 F 0.95199(9) 0.90606(5) 0.46059(5) 0.0284(2) Uani 1 1 d . . . . .
C8_2 C 0.78174(14) 0.95374(7) 0.44463(7) 0.0192(3) Uani 1 1 d . . . . .
F11_2 F 0.76420(10) 0.94017(5) 0.38823(5) 0.0290(2) Uani 1 1 d . . . . .
F12_2 F 0.82727(10) 1.00864(5) 0.44961(5) 0.0278(2) Uani 1 1 d . . . . .
C9_2 C 0.67439(13) 0.95509(7) 0.46590(7) 0.0166(3) Uani 1 1 d . . . . .
F13_2 F 0.60805(9) 0.99639(5) 0.43502(5) 0.0281(2) Uani 1 1 d . . . . .
C10_2 C 0.69675(13) 0.97263(7) 0.52995(7) 0.0174(3) Uani 1 1 d . . . . .
F14_2 F 0.60441(9) 0.97554(5) 0.54927(5) 0.0260(2) Uani 1 1 d . . . . .
F15_2 F 0.74023(9) 1.02806(5) 0.53749(5) 0.0250(2) Uani 1 1 d . . . . .
O1_3 O 0.48698(9) 0.75711(6) 0.54384(5) 0.0176(2) Uani 1 1 d . . . . .
C1_3 C 0.39659(12) 0.75954(7) 0.56511(7) 0.0141(3) Uani 1 1 d . . . . .
C2_3 C 0.32170(14) 0.81165(8) 0.53756(7) 0.0195(3) Uani 1 1 d . . . . .
F1_3 F 0.37423(10) 0.86435(5) 0.54464(5) 0.0287(2) Uani 1 1 d . . . . .
F2_3 F 0.29297(9) 0.80335(6) 0.48031(5) 0.0294(3) Uani 1 1 d . . . . .
C3_3 C 0.42577(13) 0.77197(8) 0.63109(7) 0.0182(3) Uani 1 1 d . . . . .
F3_3 F 0.48256(9) 0.82313(6) 0.64160(5) 0.0279(2) Uani 1 1 d . . . . .
F4_3 F 0.48981(9) 0.72836(6) 0.65822(5) 0.0280(2) Uani 1 1 d . . . . .
C4_3 C 0.33055(13) 0.70003(8) 0.55668(8) 0.0189(3) Uani 1 1 d . . . . .
F5_3 F 0.39109(9) 0.65364(5) 0.58073(5) 0.0276(2) Uani 1 1 d . . . . .
F6_3 F 0.30207(9) 0.68698(5) 0.50028(5) 0.0273(2) Uani 1 1 d . . . . .
C5_3 C 0.22843(14) 0.70445(8) 0.58308(8) 0.0219(3) Uani 1 1 d . . . . .
F7_3 F 0.17280(10) 0.65176(6) 0.57454(7) 0.0382(3) Uani 1 1 d . . . . .
C6_3 C 0.26090(15) 0.71687(8) 0.64814(8) 0.0234(3) Uani 1 1 d . . . . .
F8_3 F 0.32140(11) 0.67180(6) 0.67491(6) 0.0351(3) Uani 1 1 d . . . . .
F9_3 F 0.17321(10) 0.71954(6) 0.67187(6) 0.0319(3) Uani 1 1 d . . . . .
C7_3 C 0.32390(14) 0.77665(8) 0.65748(7) 0.0193(3) Uani 1 1 d . . . . .
F10_3 F 0.35280(10) 0.78803(6) 0.71496(5) 0.0313(3) Uani 1 1 d . . . . .
C8_3 C 0.25206(14) 0.82849(8) 0.62846(8) 0.0205(3) Uani 1 1 d . . . . .
F11_3 F 0.30469(10) 0.88133(5) 0.63836(6) 0.0300(3) Uani 1 1 d . . . . .
F12_3 F 0.16440(9) 0.83417(5) 0.65187(5) 0.0274(2) Uani 1 1 d . . . . .
C9_3 C 0.21953(13) 0.81604(8) 0.56360(8) 0.0205(3) Uani 1 1 d . . . . .
F13_3 F 0.15615(10) 0.86157(6) 0.53782(6) 0.0337(3) Uani 1 1 d . . . . .
C10_3 C 0.15678(13) 0.75629(9) 0.55405(8) 0.0240(4) Uani 1 1 d . . . . .
F14_3 F 0.12516(9) 0.74573(7) 0.49751(5) 0.0371(3) Uani 1 1 d . . . . .
F15_3 F 0.06635(8) 0.75981(6) 0.57538(6) 0.0330(3) Uani 1 1 d . . . . .
O1_4 O 0.45633(9) 0.73514(6) 0.42503(5) 0.0159(2) Uani 1 1 d . . . . .
C1_4 C 0.43329(11) 0.71947(7) 0.36914(6) 0.0115(2) Uani 1 1 d . . . . .
C2_4 C 0.53355(12) 0.71968(7) 0.34075(6) 0.0136(3) Uani 1 1 d . . . . .
F1_4 F 0.58201(8) 0.77365(5) 0.34678(4) 0.01908(19) Uani 1 1 d . . . . .
F2_4 F 0.60685(7) 0.68022(5) 0.36855(4) 0.0195(2) Uani 1 1 d . . . . .
C3_4 C 0.35076(12) 0.76482(7) 0.33510(7) 0.0137(3) Uani 1 1 d . . . . .
F3_4 F 0.39067(8) 0.82115(4) 0.34164(4) 0.0198(2) Uani 1 1 d . . . . .
F4_4 F 0.26075(7) 0.76537(5) 0.35719(4) 0.0198(2) Uani 1 1 d . . . . .
C4_4 C 0.38230(12) 0.65549(7) 0.35952(7) 0.0153(3) Uani 1 1 d . . . . .
F5_4 F 0.29315(8) 0.65225(5) 0.38221(4) 0.0205(2) Uani 1 1 d . . . . .
F6_4 F 0.45058(8) 0.61407(5) 0.38730(5) 0.0222(2) Uani 1 1 d . . . . .
C5_4 C 0.35242(13) 0.63915(7) 0.29470(7) 0.0177(3) Uani 1 1 d . . . . .
F7_4 F 0.30771(10) 0.58347(5) 0.28810(5) 0.0285(2) Uani 1 1 d . . . . .
C6_4 C 0.27121(13) 0.68561(8) 0.26310(7) 0.0182(3) Uani 1 1 d . . . . .
F8_4 F 0.17973(8) 0.68406(5) 0.28336(5) 0.0241(2) Uani 1 1 d . . . . .
F9_4 F 0.24260(9) 0.67167(5) 0.20688(5) 0.0266(2) Uani 1 1 d . . . . .
C7_4 C 0.32128(12) 0.74914(7) 0.27022(7) 0.0150(3) Uani 1 1 d . . . . .
F10_4 F 0.24920(8) 0.78960(5) 0.24251(5) 0.0234(2) Uani 1 1 d . . . . .
C8_4 C 0.42377(13) 0.74991(7) 0.24456(7) 0.0160(3) Uani 1 1 d . . . . .
F11_4 F 0.46809(8) 0.80505(5) 0.24918(4) 0.0207(2) Uani 1 1 d . . . . .
F12_4 F 0.39992(9) 0.73763(5) 0.18805(4) 0.0237(2) Uani 1 1 d . . . . .
C9_4 C 0.50479(12) 0.70339(7) 0.27612(7) 0.0144(3) Uani 1 1 d . . . . .
F13_4 F 0.59546(8) 0.70432(5) 0.25389(4) 0.0222(2) Uani 1 1 d . . . . .
C10_4 C 0.45467(14) 0.64012(8) 0.26902(7) 0.0187(3) Uani 1 1 d . . . . .
F14_4 F 0.52569(9) 0.59905(5) 0.29464(5) 0.0273(2) Uani 1 1 d . . . . .
F15_4 F 0.43109(10) 0.62482(5) 0.21287(5) 0.0283(2) Uani 1 1 d . . . . .
Cl1_5 Cl 0.02263(16) 0.83540(7) 0.3368(2) 0.0558(7) Uani 0.720(14) 1 d D U P A
1
Cl2_5 Cl 0.1657(2) 0.92388(12) 0.30449(18) 0.0594(7) Uani 0.720(14) 1 d D U P A
1
C1_5 C 0.1232(5) 0.8892(3) 0.3617(2) 0.0493(12) Uani 0.720(14) 1 d D U P A 1
H1A_5 H 0.094649 0.919890 0.384835 0.059 Uiso 0.720(14) 1 calc R U P A 1
H1B_5 H 0.184936 0.869323 0.386723 0.059 Uiso 0.720(14) 1 calc R U P A 1
Cl1_6 Cl 0.1699(6) 0.9202(3) 0.3147(6) 0.069(2) Uani 0.280(14) 1 d D U P A 2
Cl2_6 Cl 0.0141(4) 0.8253(4) 0.3063(8) 0.074(3) Uani 0.280(14) 1 d D U P A 2
C1_6 C 0.0976(13) 0.8732(7) 0.3540(6) 0.055(4) Uani 0.280(14) 1 d D U P A 2
H1A_6 H 0.148308 0.849245 0.382249 0.066 Uiso 0.280(14) 1 calc R U P A 2
H1B_6 H 0.053913 0.898159 0.375041 0.066 Uiso 0.280(14) 1 calc R U P A 2


loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Al1 O1_1 1.7241(16) . ?
Al1 O1_3 1.7283(15) . ?
Al1 O1_4 1.7324(16) . ?
Al1 O1_2 1.7365(15) . ?
C1 C2 1.441(2) . ?
C1 C14 1.442(2) . ?
C1 C8 1.445(2) . ?
C1 F1_1 4.563(3) . ?
C2 C3 1.409(2) . ?
C2 C7 1.410(2) . ?
C3 C4 1.384(2) . ?
C3 H3 0.9500 . ?
C4 C5 1.393(3) . ?
C4 H4 0.9500 . ?
C5 C6 1.389(3) . ?
C5 H5 0.9500 . ?
C6 C7 1.383(3) . ?
C6 H6 0.9500 . ?
C7 H7 0.9500 . ?
C8 C9 1.409(3) . ?
C8 C13 1.413(2) . ?
C9 C10 1.382(3) . ?
C9 H9 0.9500 . ?
C10 C11 1.384(3) . ?
C10 H10 0.9500 . ?
C11 C12 1.389(3) . ?
C11 H11 0.9500 . ?
C12 C13 1.381(3) . ?
C12 H12 0.9500 . ?
C13 H13 0.9500 . ?
C14 C15 1.409(2) . ?
C14 C19 1.410(2) . ?
C15 C16 1.383(2) . ?
C15 H15 0.9500 . ?
C16 C17 1.391(2) . ?
C16 H16 0.9500 . ?
C17 C18 1.392(2) . ?
C17 H17 0.9500 . ?
C18 C19 1.383(2) . ?
C18 H18 0.9500 . ?
C19 H19 0.9500 . ?
O1_1 C1_1 1.3452(19) . ?
C1_1 C4_1 1.558(2) . ?
C1_1 C2_1 1.561(2) . ?
C1_1 C3_1 1.563(2) . ?
C2_1 F2_1 1.344(2) . ?
C2_1 F1_1 1.349(2) . ?
C2_1 C9_1 1.549(2) . ?
C3_1 F4_1 1.348(2) . ?
C3_1 F3_1 1.348(2) . ?
C3_1 C7_1 1.555(2) . ?
C4_1 F5_1 1.344(2) . ?
C4_1 F6_1 1.346(2) . ?
C4_1 C5_1 1.554(2) . ?
C5_1 F7_1 1.361(2) . ?
C5_1 C10_1 1.543(3) . ?
C5_1 C6_1 1.542(3) . ?
C6_1 F8_1 1.345(2) . ?
C6_1 F9_1 1.354(2) . ?
C6_1 C7_1 1.544(3) . ?
C7_1 F10_1 1.356(2) . ?
C7_1 C8_1 1.545(3) . ?
C8_1 F11_1 1.346(2) . ?
C8_1 F12_1 1.350(2) . ?
C8_1 C9_1 1.543(3) . ?
F11_1 H13 2.4784 . ?
C9_1 F13_1 1.361(2) . ?
C9_1 C10_1 1.545(3) . ?
C10_1 F14_1 1.346(2) . ?
C10_1 F15_1 1.353(2) . ?
O1_2 C1_2 1.345(2) . ?
C1_2 C2_2 1.561(2) . ?
C1_2 C4_2 1.561(2) . ?
C1_2 C3_2 1.566(2) . ?
C2_2 F1_2 1.347(2) . ?
C2_2 F2_2 1.351(2) . ?
C2_2 C9_2 1.552(2) . ?
C3_2 F4_2 1.349(2) . ?
C3_2 F3_2 1.349(2) . ?
C3_2 C7_2 1.552(2) . ?
C4_2 F5_2 1.345(2) . ?
C4_2 F6_2 1.3481(19) . ?
C4_2 C5_2 1.552(2) . ?
C5_2 F7_2 1.366(2) . ?
C5_2 C6_2 1.543(2) . ?
C5_2 C10_2 1.546(2) . ?
C6_2 F8_2 1.342(2) . ?
C6_2 F9_2 1.352(2) . ?
C6_2 C7_2 1.547(3) . ?
C7_2 F10_2 1.3647(19) . ?
C7_2 C8_2 1.545(3) . ?
C8_2 F12_2 1.347(2) . ?
C8_2 F11_2 1.349(2) . ?
C8_2 C9_2 1.549(3) . ?
C9_2 F13_2 1.3599(19) . ?
C9_2 C10_2 1.543(3) . ?
C10_2 F14_2 1.346(2) . ?
C10_2 F15_2 1.349(2) . ?
O1_3 C1_3 1.3470(19) . ?
C1_3 C2_3 1.560(2) . ?
C1_3 C4_3 1.560(2) . ?
C1_3 C3_3 1.563(2) . ?
C2_3 F1_3 1.344(2) . ?
C2_3 F2_3 1.350(2) . ?
C2_3 C9_3 1.551(2) . ?
C3_3 F3_3 1.345(2) . ?
C3_3 F4_3 1.346(2) . ?
C3_3 C7_3 1.553(2) . ?
C4_3 F5_3 1.345(2) . ?
C4_3 F6_3 1.349(2) . ?
C4_3 C5_3 1.555(2) . ?
C5_3 F7_3 1.364(2) . ?
C5_3 C6_3 1.545(3) . ?
C5_3 C10_3 1.545(3) . ?
C6_3 F8_3 1.345(2) . ?
C6_3 F9_3 1.349(2) . ?
C6_3 C7_3 1.546(3) . ?
C7_3 F10_3 1.366(2) . ?
C7_3 C8_3 1.546(3) . ?
C8_3 F12_3 1.349(2) . ?
C8_3 F11_3 1.351(2) . ?
C8_3 C9_3 1.540(3) . ?
C9_3 F13_3 1.362(2) . ?
C9_3 C10_3 1.545(3) . ?
C10_3 F14_3 1.345(2) . ?
C10_3 F15_3 1.349(2) . ?
O1_4 C1_4 1.349(2) . ?
C1_4 C2_4 1.558(2) . ?
C1_4 C3_4 1.561(2) . ?
C1_4 C4_4 1.563(2) . ?
C2_4 F1_4 1.345(2) . ?
C2_4 F2_4 1.3534(19) . ?
C2_4 C9_4 1.550(2) . ?
C3_4 F3_4 1.350(2) . ?
C3_4 F4_4 1.3522(19) . ?
C3_4 C7_4 1.553(2) . ?
C4_4 F6_4 1.3460(19) . ?
C4_4 F5_4 1.3520(19) . ?
C4_4 C5_4 1.555(3) . ?
C5_4 F7_4 1.360(2) . ?
C5_4 C10_4 1.544(3) . ?
C5_4 C6_4 1.546(2) . ?
C6_4 F8_4 1.346(2) . ?
C6_4 F9_4 1.350(2) . ?
C6_4 C7_4 1.546(2) . ?
C7_4 F10_4 1.3582(19) . ?
C7_4 C8_4 1.546(2) . ?
C8_4 F12_4 1.345(2) . ?
C8_4 F11_4 1.346(2) . ?
C8_4 C9_4 1.546(2) . ?
C9_4 F13_4 1.3619(19) . ?
C9_4 C10_4 1.541(2) . ?
C10_4 F14_4 1.343(2) . ?
C10_4 F15_4 1.352(2) . ?
Cl1_5 C1_5 1.766(5) . ?
Cl2_5 C1_5 1.743(6) . ?
C1_5 H1A_5 0.9900 . ?
C1_5 H1B_5 0.9900 . ?
Cl1_6 C1_6 1.776(8) . ?
Cl2_6 C1_6 1.752(8) . ?
C1_6 H1A_6 0.9900 . ?
C1_6 H1B_6 0.9900 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O1_1 Al1 O1_3 110.55(7) . . ?
O1_1 Al1 O1_4 106.92(6) . . ?
O1_3 Al1 O1_4 108.97(8) . . ?
O1_1 Al1 O1_2 109.16(8) . . ?
O1_3 Al1 O1_2 109.54(7) . . ?
O1_4 Al1 O1_2 111.68(7) . . ?
C2 C1 C14 120.92(14) . . ?
C2 C1 C8 119.46(14) . . ?
C14 C1 C8 119.63(14) . . ?
C2 C1 F1_1 160.29(10) . . ?
C14 C1 F1_1 50.61(8) . . ?
C8 C1 F1_1 71.98(9) . . ?
C3 C2 C7 119.31(15) . . ?
C3 C2 C1 120.38(15) . . ?
C7 C2 C1 120.30(15) . . ?
C4 C3 C2 120.20(16) . . ?
C4 C3 H3 119.9 . . ?
C2 C3 H3 119.9 . . ?
C3 C4 C5 119.65(17) . . ?
C3 C4 H4 120.2 . . ?
C5 C4 H4 120.2 . . ?
C6 C5 C4 120.81(16) . . ?
C6 C5 H5 119.6 . . ?
C4 C5 H5 119.6 . . ?
C7 C6 C5 120.12(17) . . ?
C7 C6 H6 119.9 . . ?
C5 C6 H6 119.9 . . ?
C6 C7 C2 119.87(17) . . ?
C6 C7 H7 120.1 . . ?
C2 C7 H7 120.1 . . ?
C9 C8 C13 119.23(16) . . ?
C9 C8 C1 120.71(16) . . ?
C13 C8 C1 120.04(15) . . ?
C10 C9 C8 119.57(18) . . ?
C10 C9 H9 120.2 . . ?
C8 C9 H9 120.2 . . ?
C9 C10 C11 120.63(19) . . ?
C9 C10 H10 119.7 . . ?
C11 C10 H10 119.7 . . ?
C10 C11 C12 120.44(19) . . ?
C10 C11 H11 119.8 . . ?
C12 C11 H11 119.8 . . ?
C13 C12 C11 120.04(18) . . ?
C13 C12 H12 120.0 . . ?
C11 C12 H12 120.0 . . ?
C12 C13 C8 120.01(17) . . ?
C12 C13 H13 120.0 . . ?
C8 C13 H13 120.0 . . ?
C15 C14 C19 119.40(15) . . ?
C15 C14 C1 119.36(14) . . ?
C19 C14 C1 121.24(14) . . ?
C16 C15 C14 120.07(15) . . ?
C16 C15 H15 120.0 . . ?
C14 C15 H15 120.0 . . ?
C15 C16 C17 119.81(15) . . ?
C15 C16 H16 120.1 . . ?
C17 C16 H16 120.1 . . ?
C16 C17 C18 120.82(16) . . ?
C16 C17 H17 119.6 . . ?
C18 C17 H17 119.6 . . ?
C19 C18 C17 119.91(16) . . ?
C19 C18 H18 120.0 . . ?
C17 C18 H18 120.0 . . ?
C18 C19 C14 119.90(14) . . ?
C18 C19 H19 120.1 . . ?
C14 C19 H19 120.1 . . ?
C1_1 O1_1 Al1 149.54(11) . . ?
O1_1 C1_1 C4_1 113.43(13) . . ?
O1_1 C1_1 C2_1 111.55(13) . . ?
C4_1 C1_1 C2_1 107.69(13) . . ?
O1_1 C1_1 C3_1 109.42(13) . . ?
C4_1 C1_1 C3_1 107.49(12) . . ?
C2_1 C1_1 C3_1 106.99(13) . . ?
F2_1 C2_1 F1_1 105.93(13) . . ?
F2_1 C2_1 C9_1 109.61(15) . . ?
F1_1 C2_1 C9_1 108.85(14) . . ?
F2_1 C2_1 C1_1 110.04(13) . . ?
F1_1 C2_1 C1_1 110.12(14) . . ?
C9_1 C2_1 C1_1 112.10(13) . . ?
C2_1 F1_1 C1 148.94(10) . . ?
F4_1 C3_1 F3_1 106.22(14) . . ?
F4_1 C3_1 C7_1 109.33(14) . . ?
F3_1 C3_1 C7_1 109.21(14) . . ?
F4_1 C3_1 C1_1 110.07(13) . . ?
F3_1 C3_1 C1_1 110.29(13) . . ?
C7_1 C3_1 C1_1 111.58(13) . . ?
F5_1 C4_1 F6_1 105.87(13) . . ?
F5_1 C4_1 C5_1 109.24(14) . . ?
F6_1 C4_1 C5_1 109.87(14) . . ?
F5_1 C4_1 C1_1 110.48(13) . . ?
F6_1 C4_1 C1_1 109.83(13) . . ?
C5_1 C4_1 C1_1 111.41(13) . . ?
F7_1 C5_1 C10_1 109.56(14) . . ?
F7_1 C5_1 C6_1 108.75(14) . . ?
C10_1 C5_1 C6_1 109.79(14) . . ?
F7_1 C5_1 C4_1 110.14(13) . . ?
C10_1 C5_1 C4_1 109.70(14) . . ?
C6_1 C5_1 C4_1 108.87(14) . . ?
F8_1 C6_1 F9_1 105.54(13) . . ?
F8_1 C6_1 C5_1 110.92(14) . . ?
F9_1 C6_1 C5_1 109.57(15) . . ?
F8_1 C6_1 C7_1 110.44(15) . . ?
F9_1 C6_1 C7_1 110.55(14) . . ?
C5_1 C6_1 C7_1 109.76(13) . . ?
F10_1 C7_1 C6_1 109.93(14) . . ?
F10_1 C7_1 C8_1 109.16(14) . . ?
C6_1 C7_1 C8_1 109.17(14) . . ?
F10_1 C7_1 C3_1 110.03(14) . . ?
C6_1 C7_1 C3_1 109.15(14) . . ?
C8_1 C7_1 C3_1 109.38(14) . . ?
F11_1 C8_1 F12_1 105.13(14) . . ?
F11_1 C8_1 C9_1 110.48(14) . . ?
F12_1 C8_1 C9_1 110.36(16) . . ?
F11_1 C8_1 C7_1 110.62(15) . . ?
F12_1 C8_1 C7_1 110.20(14) . . ?
C9_1 C8_1 C7_1 109.95(13) . . ?
C8_1 F11_1 H13 145.0 . . ?
F13_1 C9_1 C8_1 109.66(14) . . ?
F13_1 C9_1 C10_1 109.37(15) . . ?
C8_1 C9_1 C10_1 109.17(14) . . ?
F13_1 C9_1 C2_1 110.22(14) . . ?
C8_1 C9_1 C2_1 109.33(15) . . ?
C10_1 C9_1 C2_1 109.07(14) . . ?
F14_1 C10_1 F15_1 105.84(15) . . ?
F14_1 C10_1 C5_1 110.03(15) . . ?
F15_1 C10_1 C5_1 110.35(15) . . ?
F14_1 C10_1 C9_1 110.73(15) . . ?
F15_1 C10_1 C9_1 110.20(15) . . ?
C5_1 C10_1 C9_1 109.64(14) . . ?
C1_2 O1_2 Al1 150.80(11) . . ?
O1_2 C1_2 C2_2 113.19(13) . . ?
O1_2 C1_2 C4_2 112.61(12) . . ?
C2_2 C1_2 C4_2 107.54(13) . . ?
O1_2 C1_2 C3_2 109.27(12) . . ?
C2_2 C1_2 C3_2 107.12(12) . . ?
C4_2 C1_2 C3_2 106.77(13) . . ?
F1_2 C2_2 F2_2 106.23(13) . . ?
F1_2 C2_2 C9_2 108.89(13) . . ?
F2_2 C2_2 C9_2 109.76(13) . . ?
F1_2 C2_2 C1_2 110.31(13) . . ?
F2_2 C2_2 C1_2 109.51(13) . . ?
C9_2 C2_2 C1_2 111.98(13) . . ?
F4_2 C3_2 F3_2 105.93(13) . . ?
F4_2 C3_2 C7_2 108.80(14) . . ?
F3_2 C3_2 C7_2 109.34(13) . . ?
F4_2 C3_2 C1_2 110.71(13) . . ?
F3_2 C3_2 C1_2 110.09(13) . . ?
C7_2 C3_2 C1_2 111.79(12) . . ?
F5_2 C4_2 F6_2 105.95(13) . . ?
F5_2 C4_2 C5_2 109.35(14) . . ?
F6_2 C4_2 C5_2 108.84(13) . . ?
F5_2 C4_2 C1_2 110.41(13) . . ?
F6_2 C4_2 C1_2 110.33(13) . . ?
C5_2 C4_2 C1_2 111.79(12) . . ?
F7_2 C5_2 C6_2 109.48(13) . . ?
F7_2 C5_2 C10_2 108.70(13) . . ?
C6_2 C5_2 C10_2 109.73(13) . . ?
F7_2 C5_2 C4_2 109.81(13) . . ?
C6_2 C5_2 C4_2 109.35(13) . . ?
C10_2 C5_2 C4_2 109.75(14) . . ?
F8_2 C6_2 F9_2 105.89(14) . . ?
F8_2 C6_2 C5_2 110.56(14) . . ?
F9_2 C6_2 C5_2 110.25(13) . . ?
F8_2 C6_2 C7_2 110.73(14) . . ?
F9_2 C6_2 C7_2 110.37(14) . . ?
C5_2 C6_2 C7_2 109.02(13) . . ?
F10_2 C7_2 C8_2 109.15(14) . . ?
F10_2 C7_2 C6_2 109.28(14) . . ?
C8_2 C7_2 C6_2 109.37(13) . . ?
F10_2 C7_2 C3_2 109.95(13) . . ?
C8_2 C7_2 C3_2 109.41(14) . . ?
C6_2 C7_2 C3_2 109.66(13) . . ?
F12_2 C8_2 F11_2 105.85(13) . . ?
F12_2 C8_2 C7_2 110.67(15) . . ?
F11_2 C8_2 C7_2 110.18(14) . . ?
F12_2 C8_2 C9_2 110.20(14) . . ?
F11_2 C8_2 C9_2 110.36(15) . . ?
C7_2 C8_2 C9_2 109.53(13) . . ?
F13_2 C9_2 C10_2 109.52(14) . . ?
F13_2 C9_2 C8_2 109.23(14) . . ?
C10_2 C9_2 C8_2 109.09(14) . . ?
F13_2 C9_2 C2_2 110.04(14) . . ?
C10_2 C9_2 C2_2 109.57(13) . . ?
C8_2 C9_2 C2_2 109.38(13) . . ?
F14_2 C10_2 F15_2 105.86(13) . . ?
F14_2 C10_2 C9_2 110.38(14) . . ?
F15_2 C10_2 C9_2 110.63(14) . . ?
F14_2 C10_2 C5_2 110.18(14) . . ?
F15_2 C10_2 C5_2 110.40(14) . . ?
C9_2 C10_2 C5_2 109.35(13) . . ?
C1_3 O1_3 Al1 148.98(11) . . ?
O1_3 C1_3 C2_3 111.58(13) . . ?
O1_3 C1_3 C4_3 113.34(13) . . ?
C2_3 C1_3 C4_3 108.02(14) . . ?
O1_3 C1_3 C3_3 109.57(13) . . ?
C2_3 C1_3 C3_3 107.00(13) . . ?
C4_3 C1_3 C3_3 107.03(13) . . ?
F1_3 C2_3 F2_3 105.86(14) . . ?
F1_3 C2_3 C9_3 109.30(14) . . ?
F2_3 C2_3 C9_3 109.39(15) . . ?
F1_3 C2_3 C1_3 110.47(15) . . ?
F2_3 C2_3 C1_3 109.95(14) . . ?
C9_3 C2_3 C1_3 111.70(14) . . ?
F3_3 C3_3 F4_3 105.67(14) . . ?
F3_3 C3_3 C7_3 109.20(14) . . ?
F4_3 C3_3 C7_3 109.20(14) . . ?
F3_3 C3_3 C1_3 110.32(13) . . ?
F4_3 C3_3 C1_3 110.67(14) . . ?
C7_3 C3_3 C1_3 111.59(13) . . ?
F5_3 C4_3 F6_3 105.94(14) . . ?
F5_3 C4_3 C5_3 109.29(15) . . ?
F6_3 C4_3 C5_3 109.58(14) . . ?
F5_3 C4_3 C1_3 110.43(14) . . ?
F6_3 C4_3 C1_3 109.94(14) . . ?
C5_3 C4_3 C1_3 111.50(13) . . ?
F7_3 C5_3 C6_3 109.27(15) . . ?
F7_3 C5_3 C10_3 109.47(16) . . ?
C6_3 C5_3 C10_3 109.24(14) . . ?
F7_3 C5_3 C4_3 109.64(14) . . ?
C6_3 C5_3 C4_3 109.77(15) . . ?
C10_3 C5_3 C4_3 109.44(15) . . ?
F8_3 C6_3 F9_3 106.13(14) . . ?
F8_3 C6_3 C5_3 110.71(15) . . ?
F9_3 C6_3 C5_3 110.44(16) . . ?
F8_3 C6_3 C7_3 110.04(17) . . ?
F9_3 C6_3 C7_3 110.52(15) . . ?
C5_3 C6_3 C7_3 108.97(14) . . ?
F10_3 C7_3 C6_3 109.34(14) . . ?
F10_3 C7_3 C8_3 108.97(14) . . ?
C6_3 C7_3 C8_3 109.56(15) . . ?
F10_3 C7_3 C3_3 109.73(14) . . ?
C6_3 C7_3 C3_3 109.56(14) . . ?
C8_3 C7_3 C3_3 109.65(14) . . ?
F12_3 C8_3 F11_3 105.57(14) . . ?
F12_3 C8_3 C9_3 110.59(15) . . ?
F11_3 C8_3 C9_3 110.85(15) . . ?
F12_3 C8_3 C7_3 110.45(14) . . ?
F11_3 C8_3 C7_3 110.11(16) . . ?
C9_3 C8_3 C7_3 109.23(14) . . ?
F13_3 C9_3 C8_3 109.47(15) . . ?
F13_3 C9_3 C10_3 109.42(15) . . ?
C8_3 C9_3 C10_3 109.24(14) . . ?
F13_3 C9_3 C2_3 109.59(14) . . ?
C8_3 C9_3 C2_3 109.42(14) . . ?
C10_3 C9_3 C2_3 109.69(14) . . ?
F14_3 C10_3 F15_3 106.20(14) . . ?
F14_3 C10_3 C9_3 109.87(16) . . ?
F15_3 C10_3 C9_3 110.44(15) . . ?
F14_3 C10_3 C5_3 110.37(16) . . ?
F15_3 C10_3 C5_3 110.28(16) . . ?
C9_3 C10_3 C5_3 109.63(15) . . ?
C1_4 O1_4 Al1 147.58(10) . . ?
O1_4 C1_4 C2_4 113.02(12) . . ?
O1_4 C1_4 C3_4 109.57(13) . . ?
C2_4 C1_4 C3_4 107.30(12) . . ?
O1_4 C1_4 C4_4 112.46(12) . . ?
C2_4 C1_4 C4_4 106.93(12) . . ?
C3_4 C1_4 C4_4 107.27(12) . . ?
F1_4 C2_4 F2_4 105.73(13) . . ?
F1_4 C2_4 C9_4 109.08(12) . . ?
F2_4 C2_4 C9_4 109.61(13) . . ?
F1_4 C2_4 C1_4 110.74(13) . . ?
F2_4 C2_4 C1_4 109.29(13) . . ?
C9_4 C2_4 C1_4 112.19(12) . . ?
F3_4 C3_4 F4_4 105.97(12) . . ?
F3_4 C3_4 C7_4 109.50(12) . . ?
F4_4 C3_4 C7_4 109.45(13) . . ?
F3_4 C3_4 C1_4 110.02(13) . . ?
F4_4 C3_4 C1_4 109.78(13) . . ?
C7_4 C3_4 C1_4 111.94(13) . . ?
F6_4 C4_4 F5_4 106.15(13) . . ?
F6_4 C4_4 C5_4 109.39(14) . . ?
F5_4 C4_4 C5_4 108.97(13) . . ?
F6_4 C4_4 C1_4 110.13(13) . . ?
F5_4 C4_4 C1_4 110.32(13) . . ?
C5_4 C4_4 C1_4 111.73(12) . . ?
F7_4 C5_4 C10_4 109.47(14) . . ?
F7_4 C5_4 C6_4 109.27(14) . . ?
C10_4 C5_4 C6_4 109.40(14) . . ?
F7_4 C5_4 C4_4 109.96(13) . . ?
C10_4 C5_4 C4_4 109.31(13) . . ?
C6_4 C5_4 C4_4 109.42(14) . . ?
F8_4 C6_4 F9_4 105.52(13) . . ?
F8_4 C6_4 C5_4 110.51(14) . . ?
F9_4 C6_4 C5_4 110.45(15) . . ?
F8_4 C6_4 C7_4 110.53(14) . . ?
F9_4 C6_4 C7_4 110.02(13) . . ?
C5_4 C6_4 C7_4 109.74(13) . . ?
F10_4 C7_4 C6_4 109.26(13) . . ?
F10_4 C7_4 C8_4 110.00(13) . . ?
C6_4 C7_4 C8_4 109.16(13) . . ?
F10_4 C7_4 C3_4 109.78(13) . . ?
C6_4 C7_4 C3_4 109.07(12) . . ?
C8_4 C7_4 C3_4 109.54(13) . . ?
F12_4 C8_4 F11_4 105.90(12) . . ?
F12_4 C8_4 C9_4 110.13(14) . . ?
F11_4 C8_4 C9_4 110.09(14) . . ?
F12_4 C8_4 C7_4 110.65(13) . . ?
F11_4 C8_4 C7_4 110.51(13) . . ?
C9_4 C8_4 C7_4 109.52(13) . . ?
F13_4 C9_4 C10_4 109.60(13) . . ?
F13_4 C9_4 C8_4 109.62(13) . . ?
C10_4 C9_4 C8_4 109.75(14) . . ?
F13_4 C9_4 C2_4 109.34(13) . . ?
C10_4 C9_4 C2_4 109.44(13) . . ?
C8_4 C9_4 C2_4 109.09(13) . . ?
F14_4 C10_4 F15_4 105.84(14) . . ?
F14_4 C10_4 C9_4 110.26(15) . . ?
F15_4 C10_4 C9_4 110.08(14) . . ?
F14_4 C10_4 C5_4 110.77(14) . . ?
F15_4 C10_4 C5_4 110.43(14) . . ?
C9_4 C10_4 C5_4 109.41(13) . . ?
Cl2_5 C1_5 Cl1_5 110.8(3) . . ?
Cl2_5 C1_5 H1A_5 109.5 . . ?
Cl1_5 C1_5 H1A_5 109.5 . . ?
Cl2_5 C1_5 H1B_5 109.5 . . ?
Cl1_5 C1_5 H1B_5 109.5 . . ?
H1A_5 C1_5 H1B_5 108.1 . . ?
Cl2_6 C1_6 Cl1_6 109.2(6) . . ?
Cl2_6 C1_6 H1A_6 109.8 . . ?
Cl1_6 C1_6 H1A_6 109.8 . . ?
Cl2_6 C1_6 H1B_6 109.8 . . ?
Cl1_6 C1_6 H1B_6 109.8 . . ?
H1A_6 C1_6 H1B_6 108.3 . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
C14 C1 C2 C3 -30.8(2) . . . . ?
C8 C1 C2 C3 149.14(16) . . . . ?
F1_1 C1 C2 C3 -89.3(3) . . . . ?
C14 C1 C2 C7 150.33(16) . . . . ?
C8 C1 C2 C7 -29.8(2) . . . . ?
F1_1 C1 C2 C7 91.8(3) . . . . ?
C7 C2 C3 C4 1.6(2) . . . . ?
C1 C2 C3 C4 -177.35(15) . . . . ?
C2 C3 C4 C5 -2.0(3) . . . . ?
C3 C4 C5 C6 0.6(3) . . . . ?
C4 C5 C6 C7 1.4(3) . . . . ?
C5 C6 C7 C2 -1.9(3) . . . . ?
C3 C2 C7 C6 0.4(2) . . . . ?
C1 C2 C7 C6 179.31(16) . . . . ?
C2 C1 C8 C9 -37.1(2) . . . . ?
C14 C1 C8 C9 142.76(17) . . . . ?
F1_1 C1 C8 C9 160.45(18) . . . . ?
C2 C1 C8 C13 141.35(16) . . . . ?
C14 C1 C8 C13 -38.7(2) . . . . ?
F1_1 C1 C8 C13 -21.06(14) . . . . ?
C13 C8 C9 C10 0.4(3) . . . . ?
C1 C8 C9 C10 178.90(19) . . . . ?
C8 C9 C10 C11 -2.3(3) . . . . ?
C9 C10 C11 C12 1.9(4) . . . . ?
C10 C11 C12 C13 0.3(3) . . . . ?
C11 C12 C13 C8 -2.2(3) . . . . ?
C9 C8 C13 C12 1.8(3) . . . . ?
C1 C8 C13 C12 -176.70(17) . . . . ?
C2 C1 C14 C15 145.34(16) . . . . ?
C8 C1 C14 C15 -34.6(2) . . . . ?
F1_1 C1 C14 C15 -56.52(12) . . . . ?
C2 C1 C14 C19 -34.5(2) . . . . ?
C8 C1 C14 C19 145.56(16) . . . . ?
F1_1 C1 C14 C19 123.60(18) . . . . ?
C19 C14 C15 C16 0.7(2) . . . . ?
C1 C14 C15 C16 -179.17(15) . . . . ?
C14 C15 C16 C17 -2.8(3) . . . . ?
C15 C16 C17 C18 2.1(3) . . . . ?
C16 C17 C18 C19 0.7(3) . . . . ?
C17 C18 C19 C14 -2.9(3) . . . . ?
C15 C14 C19 C18 2.1(2) . . . . ?
C1 C14 C19 C18 -177.98(15) . . . . ?
O1_3 Al1 O1_1 C1_1 -70.2(2) . . . . ?
O1_4 Al1 O1_1 C1_1 171.3(2) . . . . ?
O1_2 Al1 O1_1 C1_1 50.3(2) . . . . ?
Al1 O1_1 C1_1 C4_1 34.7(3) . . . . ?
Al1 O1_1 C1_1 C2_1 -87.1(2) . . . . ?
Al1 O1_1 C1_1 C3_1 154.70(18) . . . . ?
O1_1 C1_1 C2_1 F2_1 60.17(18) . . . . ?
C4_1 C1_1 C2_1 F2_1 -64.90(16) . . . . ?
C3_1 C1_1 C2_1 F2_1 179.80(13) . . . . ?
O1_1 C1_1 C2_1 F1_1 -56.24(17) . . . . ?
C4_1 C1_1 C2_1 F1_1 178.69(12) . . . . ?
C3_1 C1_1 C2_1 F1_1 63.39(16) . . . . ?
O1_1 C1_1 C2_1 C9_1 -177.58(13) . . . . ?
C4_1 C1_1 C2_1 C9_1 57.35(17) . . . . ?
C3_1 C1_1 C2_1 C9_1 -57.94(17) . . . . ?
F2_1 C2_1 F1_1 C1 75.1(2) . . . . ?
C9_1 C2_1 F1_1 C1 -42.6(2) . . . . ?
C1_1 C2_1 F1_1 C1 -165.90(12) . . . . ?
O1_1 C1_1 C3_1 F4_1 -59.57(17) . . . . ?
C4_1 C1_1 C3_1 F4_1 64.01(16) . . . . ?
C2_1 C1_1 C3_1 F4_1 179.44(13) . . . . ?
O1_1 C1_1 C3_1 F3_1 57.30(17) . . . . ?
C4_1 C1_1 C3_1 F3_1 -179.12(12) . . . . ?
C2_1 C1_1 C3_1 F3_1 -63.69(16) . . . . ?
O1_1 C1_1 C3_1 C7_1 178.87(13) . . . . ?
C4_1 C1_1 C3_1 C7_1 -57.55(17) . . . . ?
C2_1 C1_1 C3_1 C7_1 57.88(17) . . . . ?
O1_1 C1_1 C4_1 F5_1 57.62(17) . . . . ?
C2_1 C1_1 C4_1 F5_1 -178.45(12) . . . . ?
C3_1 C1_1 C4_1 F5_1 -63.48(16) . . . . ?
O1_1 C1_1 C4_1 F6_1 -58.80(18) . . . . ?
C2_1 C1_1 C4_1 F6_1 65.14(15) . . . . ?
C3_1 C1_1 C4_1 F6_1 -179.90(12) . . . . ?
O1_1 C1_1 C4_1 C5_1 179.23(13) . . . . ?
C2_1 C1_1 C4_1 C5_1 -56.83(17) . . . . ?
C3_1 C1_1 C4_1 C5_1 58.14(17) . . . . ?
F5_1 C4_1 C5_1 F7_1 -57.46(18) . . . . ?
F6_1 C4_1 C5_1 F7_1 58.26(18) . . . . ?
C1_1 C4_1 C5_1 F7_1 -179.79(13) . . . . ?
F5_1 C4_1 C5_1 C10_1 -178.13(13) . . . . ?
F6_1 C4_1 C5_1 C10_1 -62.41(17) . . . . ?
C1_1 C4_1 C5_1 C10_1 59.53(18) . . . . ?
F5_1 C4_1 C5_1 C6_1 61.70(17) . . . . ?
F6_1 C4_1 C5_1 C6_1 177.42(13) . . . . ?
C1_1 C4_1 C5_1 C6_1 -60.64(17) . . . . ?
F7_1 C5_1 C6_1 F8_1 58.31(18) . . . . ?
C10_1 C5_1 C6_1 F8_1 178.17(13) . . . . ?
C4_1 C5_1 C6_1 F8_1 -61.71(18) . . . . ?
F7_1 C5_1 C6_1 F9_1 -57.82(17) . . . . ?
C10_1 C5_1 C6_1 F9_1 62.04(17) . . . . ?
C4_1 C5_1 C6_1 F9_1 -177.84(12) . . . . ?
F7_1 C5_1 C6_1 C7_1 -179.38(13) . . . . ?
C10_1 C5_1 C6_1 C7_1 -59.52(17) . . . . ?
C4_1 C5_1 C6_1 C7_1 60.60(17) . . . . ?
F8_1 C6_1 C7_1 F10_1 -58.26(18) . . . . ?
F9_1 C6_1 C7_1 F10_1 58.16(19) . . . . ?
C5_1 C6_1 C7_1 F10_1 179.14(13) . . . . ?
F8_1 C6_1 C7_1 C8_1 -177.98(13) . . . . ?
F9_1 C6_1 C7_1 C8_1 -61.55(17) . . . . ?
C5_1 C6_1 C7_1 C8_1 59.43(17) . . . . ?
F8_1 C6_1 C7_1 C3_1 62.51(17) . . . . ?
F9_1 C6_1 C7_1 C3_1 178.93(13) . . . . ?
C5_1 C6_1 C7_1 C3_1 -60.09(17) . . . . ?
F4_1 C3_1 C7_1 F10_1 58.17(18) . . . . ?
F3_1 C3_1 C7_1 F10_1 -57.66(18) . . . . ?
C1_1 C3_1 C7_1 F10_1 -179.84(13) . . . . ?
F4_1 C3_1 C7_1 C6_1 -62.54(17) . . . . ?
F3_1 C3_1 C7_1 C6_1 -178.37(13) . . . . ?
C1_1 C3_1 C7_1 C6_1 59.45(17) . . . . ?
F4_1 C3_1 C7_1 C8_1 178.07(13) . . . . ?
F3_1 C3_1 C7_1 C8_1 62.24(17) . . . . ?
C1_1 C3_1 C7_1 C8_1 -59.94(18) . . . . ?
F10_1 C7_1 C8_1 F11_1 57.51(17) . . . . ?
C6_1 C7_1 C8_1 F11_1 177.70(13) . . . . ?
C3_1 C7_1 C8_1 F11_1 -62.92(18) . . . . ?
F10_1 C7_1 C8_1 F12_1 -58.32(19) . . . . ?
C6_1 C7_1 C8_1 F12_1 61.87(18) . . . . ?
C3_1 C7_1 C8_1 F12_1 -178.76(13) . . . . ?
F10_1 C7_1 C8_1 C9_1 179.80(14) . . . . ?
C6_1 C7_1 C8_1 C9_1 -60.01(17) . . . . ?
C3_1 C7_1 C8_1 C9_1 59.37(18) . . . . ?
F12_1 C8_1 F11_1 H13 -129.8 . . . . ?
C9_1 C8_1 F11_1 H13 -10.8 . . . . ?
C7_1 C8_1 F11_1 H13 111.2 . . . . ?
F11_1 C8_1 C9_1 F13_1 -57.65(19) . . . . ?
F12_1 C8_1 C9_1 F13_1 58.19(19) . . . . ?
C7_1 C8_1 C9_1 F13_1 179.97(14) . . . . ?
F11_1 C8_1 C9_1 C10_1 -177.47(13) . . . . ?
F12_1 C8_1 C9_1 C10_1 -61.62(17) . . . . ?
C7_1 C8_1 C9_1 C10_1 60.15(17) . . . . ?
F11_1 C8_1 C9_1 C2_1 63.29(17) . . . . ?
F12_1 C8_1 C9_1 C2_1 179.13(13) . . . . ?
C7_1 C8_1 C9_1 C2_1 -59.09(18) . . . . ?
F2_1 C2_1 C9_1 F13_1 -57.21(19) . . . . ?
F1_1 C2_1 C9_1 F13_1 58.22(19) . . . . ?
C1_1 C2_1 C9_1 F13_1 -179.71(14) . . . . ?
F2_1 C2_1 C9_1 C8_1 -177.82(13) . . . . ?
F1_1 C2_1 C9_1 C8_1 -62.39(17) . . . . ?
C1_1 C2_1 C9_1 C8_1 59.68(18) . . . . ?
F2_1 C2_1 C9_1 C10_1 62.88(17) . . . . ?
F1_1 C2_1 C9_1 C10_1 178.31(13) . . . . ?
C1_1 C2_1 C9_1 C10_1 -59.62(18) . . . . ?
F7_1 C5_1 C10_1 F14_1 -59.02(18) . . . . ?
C6_1 C5_1 C10_1 F14_1 -178.39(13) . . . . ?
C4_1 C5_1 C10_1 F14_1 62.00(18) . . . . ?
F7_1 C5_1 C10_1 F15_1 57.40(19) . . . . ?
C6_1 C5_1 C10_1 F15_1 -61.96(18) . . . . ?
C4_1 C5_1 C10_1 F15_1 178.43(14) . . . . ?
F7_1 C5_1 C10_1 C9_1 178.96(14) . . . . ?
C6_1 C5_1 C10_1 C9_1 59.60(17) . . . . ?
C4_1 C5_1 C10_1 C9_1 -60.01(18) . . . . ?
F13_1 C9_1 C10_1 F14_1 58.74(18) . . . . ?
C8_1 C9_1 C10_1 F14_1 178.73(13) . . . . ?
C2_1 C9_1 C10_1 F14_1 -61.87(18) . . . . ?
F13_1 C9_1 C10_1 F15_1 -58.02(19) . . . . ?
C8_1 C9_1 C10_1 F15_1 61.97(18) . . . . ?
C2_1 C9_1 C10_1 F15_1 -178.62(14) . . . . ?
F13_1 C9_1 C10_1 C5_1 -179.67(14) . . . . ?
C8_1 C9_1 C10_1 C5_1 -59.68(17) . . . . ?
C2_1 C9_1 C10_1 C5_1 59.72(18) . . . . ?
O1_1 Al1 O1_2 C1_2 -152.1(2) . . . . ?
O1_3 Al1 O1_2 C1_2 -30.9(2) . . . . ?
O1_4 Al1 O1_2 C1_2 89.9(2) . . . . ?
Al1 O1_2 C1_2 C2_2 -57.0(3) . . . . ?
Al1 O1_2 C1_2 C4_2 65.3(3) . . . . ?
Al1 O1_2 C1_2 C3_2 -176.23(18) . . . . ?
O1_2 C1_2 C2_2 F1_2 -56.60(17) . . . . ?
C4_2 C1_2 C2_2 F1_2 178.36(12) . . . . ?
C3_2 C1_2 C2_2 F1_2 63.91(16) . . . . ?
O1_2 C1_2 C2_2 F2_2 59.98(17) . . . . ?
C4_2 C1_2 C2_2 F2_2 -65.06(15) . . . . ?
C3_2 C1_2 C2_2 F2_2 -179.51(12) . . . . ?
O1_2 C1_2 C2_2 C9_2 -178.03(13) . . . . ?
C4_2 C1_2 C2_2 C9_2 56.93(16) . . . . ?
C3_2 C1_2 C2_2 C9_2 -57.52(16) . . . . ?
O1_2 C1_2 C3_2 F4_2 -58.01(17) . . . . ?
C2_2 C1_2 C3_2 F4_2 179.02(12) . . . . ?
C4_2 C1_2 C3_2 F4_2 64.05(16) . . . . ?
O1_2 C1_2 C3_2 F3_2 58.78(16) . . . . ?
C2_2 C1_2 C3_2 F3_2 -64.19(16) . . . . ?
C4_2 C1_2 C3_2 F3_2 -179.16(12) . . . . ?
O1_2 C1_2 C3_2 C7_2 -179.48(13) . . . . ?
C2_2 C1_2 C3_2 C7_2 57.55(17) . . . . ?
C4_2 C1_2 C3_2 C7_2 -57.43(16) . . . . ?
O1_2 C1_2 C4_2 F5_2 55.91(17) . . . . ?
C2_2 C1_2 C4_2 F5_2 -178.70(12) . . . . ?
C3_2 C1_2 C4_2 F5_2 -64.02(15) . . . . ?
O1_2 C1_2 C4_2 F6_2 -60.86(17) . . . . ?
C2_2 C1_2 C4_2 F6_2 64.52(16) . . . . ?
C3_2 C1_2 C4_2 F6_2 179.21(12) . . . . ?
O1_2 C1_2 C4_2 C5_2 177.88(12) . . . . ?
C2_2 C1_2 C4_2 C5_2 -56.74(16) . . . . ?
C3_2 C1_2 C4_2 C5_2 57.95(16) . . . . ?
F5_2 C4_2 C5_2 F7_2 -58.52(16) . . . . ?
F6_2 C4_2 C5_2 F7_2 56.79(17) . . . . ?
C1_2 C4_2 C5_2 F7_2 178.91(12) . . . . ?
F5_2 C4_2 C5_2 C6_2 61.63(17) . . . . ?
F6_2 C4_2 C5_2 C6_2 176.93(13) . . . . ?
C1_2 C4_2 C5_2 C6_2 -60.95(17) . . . . ?
F5_2 C4_2 C5_2 C10_2 -177.96(12) . . . . ?
F6_2 C4_2 C5_2 C10_2 -62.65(17) . . . . ?
C1_2 C4_2 C5_2 C10_2 59.47(16) . . . . ?
F7_2 C5_2 C6_2 F8_2 58.54(17) . . . . ?
C10_2 C5_2 C6_2 F8_2 177.76(13) . . . . ?
C4_2 C5_2 C6_2 F8_2 -61.81(17) . . . . ?
F7_2 C5_2 C6_2 F9_2 -58.21(17) . . . . ?
C10_2 C5_2 C6_2 F9_2 61.01(18) . . . . ?
C4_2 C5_2 C6_2 F9_2 -178.56(13) . . . . ?
F7_2 C5_2 C6_2 C7_2 -179.51(12) . . . . ?
C10_2 C5_2 C6_2 C7_2 -60.29(17) . . . . ?
C4_2 C5_2 C6_2 C7_2 60.14(16) . . . . ?
F8_2 C6_2 C7_2 F10_2 -58.55(17) . . . . ?
F9_2 C6_2 C7_2 F10_2 58.36(17) . . . . ?
C5_2 C6_2 C7_2 F10_2 179.60(13) . . . . ?
F8_2 C6_2 C7_2 C8_2 -177.99(13) . . . . ?
F9_2 C6_2 C7_2 C8_2 -61.07(17) . . . . ?
C5_2 C6_2 C7_2 C8_2 60.16(16) . . . . ?
F8_2 C6_2 C7_2 C3_2 62.03(17) . . . . ?
F9_2 C6_2 C7_2 C3_2 178.95(12) . . . . ?
C5_2 C6_2 C7_2 C3_2 -59.81(16) . . . . ?
F4_2 C3_2 C7_2 F10_2 57.55(18) . . . . ?
F3_2 C3_2 C7_2 F10_2 -57.71(17) . . . . ?
C1_2 C3_2 C7_2 F10_2 -179.88(13) . . . . ?
F4_2 C3_2 C7_2 C8_2 177.41(12) . . . . ?
F3_2 C3_2 C7_2 C8_2 62.15(16) . . . . ?
C1_2 C3_2 C7_2 C8_2 -60.01(18) . . . . ?
F4_2 C3_2 C7_2 C6_2 -62.63(16) . . . . ?
F3_2 C3_2 C7_2 C6_2 -177.89(12) . . . . ?
C1_2 C3_2 C7_2 C6_2 59.94(17) . . . . ?
F10_2 C7_2 C8_2 F12_2 -58.24(18) . . . . ?
C6_2 C7_2 C8_2 F12_2 61.27(17) . . . . ?
C3_2 C7_2 C8_2 F12_2 -178.59(13) . . . . ?
F10_2 C7_2 C8_2 F11_2 58.48(17) . . . . ?
C6_2 C7_2 C8_2 F11_2 178.00(13) . . . . ?
C3_2 C7_2 C8_2 F11_2 -61.87(17) . . . . ?
F10_2 C7_2 C8_2 C9_2 -179.94(13) . . . . ?
C6_2 C7_2 C8_2 C9_2 -60.43(17) . . . . ?
C3_2 C7_2 C8_2 C9_2 59.70(17) . . . . ?
F12_2 C8_2 C9_2 F13_2 57.98(18) . . . . ?
F11_2 C8_2 C9_2 F13_2 -58.57(18) . . . . ?
C7_2 C8_2 C9_2 F13_2 179.96(13) . . . . ?
F12_2 C8_2 C9_2 C10_2 -61.70(17) . . . . ?
F11_2 C8_2 C9_2 C10_2 -178.25(13) . . . . ?
C7_2 C8_2 C9_2 C10_2 60.28(17) . . . . ?
F12_2 C8_2 C9_2 C2_2 178.47(13) . . . . ?
F11_2 C8_2 C9_2 C2_2 61.92(17) . . . . ?
C7_2 C8_2 C9_2 C2_2 -59.55(17) . . . . ?
F1_2 C2_2 C9_2 F13_2 57.59(17) . . . . ?
F2_2 C2_2 C9_2 F13_2 -58.32(18) . . . . ?
C1_2 C2_2 C9_2 F13_2 179.83(13) . . . . ?
F1_2 C2_2 C9_2 C10_2 178.06(12) . . . . ?
F2_2 C2_2 C9_2 C10_2 62.16(16) . . . . ?
C1_2 C2_2 C9_2 C10_2 -59.69(17) . . . . ?
F1_2 C2_2 C9_2 C8_2 -62.41(16) . . . . ?
F2_2 C2_2 C9_2 C8_2 -178.31(13) . . . . ?
C1_2 C2_2 C9_2 C8_2 59.84(17) . . . . ?
F13_2 C9_2 C10_2 F14_2 59.06(17) . . . . ?
C8_2 C9_2 C10_2 F14_2 178.55(13) . . . . ?
C2_2 C9_2 C10_2 F14_2 -61.73(16) . . . . ?
F13_2 C9_2 C10_2 F15_2 -57.77(18) . . . . ?
C8_2 C9_2 C10_2 F15_2 61.72(16) . . . . ?
C2_2 C9_2 C10_2 F15_2 -178.57(12) . . . . ?
F13_2 C9_2 C10_2 C5_2 -179.57(13) . . . . ?
C8_2 C9_2 C10_2 C5_2 -60.08(16) . . . . ?
C2_2 C9_2 C10_2 C5_2 59.63(17) . . . . ?
F7_2 C5_2 C10_2 F14_2 -58.29(17) . . . . ?
C6_2 C5_2 C10_2 F14_2 -177.99(13) . . . . ?
C4_2 C5_2 C10_2 F14_2 61.82(17) . . . . ?
F7_2 C5_2 C10_2 F15_2 58.29(17) . . . . ?
C6_2 C5_2 C10_2 F15_2 -61.41(17) . . . . ?
C4_2 C5_2 C10_2 F15_2 178.40(12) . . . . ?
F7_2 C5_2 C10_2 C9_2 -179.78(12) . . . . ?
C6_2 C5_2 C10_2 C9_2 60.53(17) . . . . ?
C4_2 C5_2 C10_2 C9_2 -59.66(16) . . . . ?
O1_1 Al1 O1_3 C1_3 -91.8(2) . . . . ?
O1_4 Al1 O1_3 C1_3 25.4(2) . . . . ?
O1_2 Al1 O1_3 C1_3 147.9(2) . . . . ?
Al1 O1_3 C1_3 C2_3 -77.7(3) . . . . ?
Al1 O1_3 C1_3 C4_3 44.5(3) . . . . ?
Al1 O1_3 C1_3 C3_3 164.00(18) . . . . ?
O1_3 C1_3 C2_3 F1_3 -55.99(18) . . . . ?
C4_3 C1_3 C2_3 F1_3 178.78(13) . . . . ?
C3_3 C1_3 C2_3 F1_3 63.85(16) . . . . ?
O1_3 C1_3 C2_3 F2_3 60.48(18) . . . . ?
C4_3 C1_3 C2_3 F2_3 -64.74(16) . . . . ?
C3_3 C1_3 C2_3 F2_3 -179.67(13) . . . . ?
O1_3 C1_3 C2_3 C9_3 -177.88(14) . . . . ?
C4_3 C1_3 C2_3 C9_3 56.90(18) . . . . ?
C3_3 C1_3 C2_3 C9_3 -58.03(18) . . . . ?
O1_3 C1_3 C3_3 F3_3 57.10(18) . . . . ?
C2_3 C1_3 C3_3 F3_3 -64.03(17) . . . . ?
C4_3 C1_3 C3_3 F3_3 -179.62(13) . . . . ?
O1_3 C1_3 C3_3 F4_3 -59.49(18) . . . . ?
C2_3 C1_3 C3_3 F4_3 179.38(13) . . . . ?
C4_3 C1_3 C3_3 F4_3 63.78(17) . . . . ?
O1_3 C1_3 C3_3 C7_3 178.69(14) . . . . ?
C2_3 C1_3 C3_3 C7_3 57.56(17) . . . . ?
C4_3 C1_3 C3_3 C7_3 -58.04(17) . . . . ?
O1_3 C1_3 C4_3 F5_3 57.00(18) . . . . ?
C2_3 C1_3 C4_3 F5_3 -178.83(13) . . . . ?
C3_3 C1_3 C4_3 F5_3 -63.91(16) . . . . ?
O1_3 C1_3 C4_3 F6_3 -59.54(18) . . . . ?
C2_3 C1_3 C4_3 F6_3 64.63(16) . . . . ?
C3_3 C1_3 C4_3 F6_3 179.54(12) . . . . ?
O1_3 C1_3 C4_3 C5_3 178.72(14) . . . . ?
C2_3 C1_3 C4_3 C5_3 -57.11(18) . . . . ?
C3_3 C1_3 C4_3 C5_3 57.80(18) . . . . ?
F5_3 C4_3 C5_3 F7_3 -58.0(2) . . . . ?
F6_3 C4_3 C5_3 F7_3 57.7(2) . . . . ?
C1_3 C4_3 C5_3 F7_3 179.67(15) . . . . ?
F5_3 C4_3 C5_3 C6_3 62.08(18) . . . . ?
F6_3 C4_3 C5_3 C6_3 177.76(14) . . . . ?
C1_3 C4_3 C5_3 C6_3 -60.29(19) . . . . ?
F5_3 C4_3 C5_3 C10_3 -178.04(14) . . . . ?
F6_3 C4_3 C5_3 C10_3 -62.37(18) . . . . ?
C1_3 C4_3 C5_3 C10_3 59.58(19) . . . . ?
F7_3 C5_3 C6_3 F8_3 58.84(19) . . . . ?
C10_3 C5_3 C6_3 F8_3 178.58(14) . . . . ?
C4_3 C5_3 C6_3 F8_3 -61.42(19) . . . . ?
F7_3 C5_3 C6_3 F9_3 -58.41(19) . . . . ?
C10_3 C5_3 C6_3 F9_3 61.32(18) . . . . ?
C4_3 C5_3 C6_3 F9_3 -178.68(14) . . . . ?
F7_3 C5_3 C6_3 C7_3 -179.99(14) . . . . ?
C10_3 C5_3 C6_3 C7_3 -60.26(18) . . . . ?
C4_3 C5_3 C6_3 C7_3 59.74(18) . . . . ?
F8_3 C6_3 C7_3 F10_3 -58.52(18) . . . . ?
F9_3 C6_3 C7_3 F10_3 58.4(2) . . . . ?
C5_3 C6_3 C7_3 F10_3 179.91(13) . . . . ?
F8_3 C6_3 C7_3 C8_3 -177.88(13) . . . . ?
F9_3 C6_3 C7_3 C8_3 -60.99(19) . . . . ?
C5_3 C6_3 C7_3 C8_3 60.55(17) . . . . ?
F8_3 C6_3 C7_3 C3_3 61.78(18) . . . . ?
F9_3 C6_3 C7_3 C3_3 178.68(14) . . . . ?
C5_3 C6_3 C7_3 C3_3 -59.79(18) . . . . ?
F3_3 C3_3 C7_3 F10_3 -57.24(19) . . . . ?
F4_3 C3_3 C7_3 F10_3 57.86(19) . . . . ?
C1_3 C3_3 C7_3 F10_3 -179.47(14) . . . . ?
F3_3 C3_3 C7_3 C6_3 -177.30(14) . . . . ?
F4_3 C3_3 C7_3 C6_3 -62.20(18) . . . . ?
C1_3 C3_3 C7_3 C6_3 60.47(18) . . . . ?
F3_3 C3_3 C7_3 C8_3 62.41(18) . . . . ?
F4_3 C3_3 C7_3 C8_3 177.51(14) . . . . ?
C1_3 C3_3 C7_3 C8_3 -59.82(18) . . . . ?
F10_3 C7_3 C8_3 F12_3 -58.36(19) . . . . ?
C6_3 C7_3 C8_3 F12_3 61.23(18) . . . . ?
C3_3 C7_3 C8_3 F12_3 -178.48(14) . . . . ?
F10_3 C7_3 C8_3 F11_3 57.85(17) . . . . ?
C6_3 C7_3 C8_3 F11_3 177.45(13) . . . . ?
C3_3 C7_3 C8_3 F11_3 -62.27(18) . . . . ?
F10_3 C7_3 C8_3 C9_3 179.80(13) . . . . ?
C6_3 C7_3 C8_3 C9_3 -60.61(17) . . . . ?
C3_3 C7_3 C8_3 C9_3 59.68(18) . . . . ?
F12_3 C8_3 C9_3 F13_3 58.20(19) . . . . ?
F11_3 C8_3 C9_3 F13_3 -58.54(19) . . . . ?
C7_3 C8_3 C9_3 F13_3 179.95(14) . . . . ?
F12_3 C8_3 C9_3 C10_3 -61.60(18) . . . . ?
F11_3 C8_3 C9_3 C10_3 -178.34(13) . . . . ?
C7_3 C8_3 C9_3 C10_3 60.16(18) . . . . ?
F12_3 C8_3 C9_3 C2_3 178.31(14) . . . . ?
F11_3 C8_3 C9_3 C2_3 61.57(18) . . . . ?
C7_3 C8_3 C9_3 C2_3 -59.93(18) . . . . ?
F1_3 C2_3 C9_3 F13_3 58.16(19) . . . . ?
F2_3 C2_3 C9_3 F13_3 -57.3(2) . . . . ?
C1_3 C2_3 C9_3 F13_3 -179.28(14) . . . . ?
F1_3 C2_3 C9_3 C8_3 -61.87(18) . . . . ?
F2_3 C2_3 C9_3 C8_3 -177.35(14) . . . . ?
C1_3 C2_3 C9_3 C8_3 60.69(19) . . . . ?
F1_3 C2_3 C9_3 C10_3 178.31(14) . . . . ?
F2_3 C2_3 C9_3 C10_3 62.83(18) . . . . ?
C1_3 C2_3 C9_3 C10_3 -59.13(19) . . . . ?
F13_3 C9_3 C10_3 F14_3 58.40(18) . . . . ?
C8_3 C9_3 C10_3 F14_3 178.22(13) . . . . ?
C2_3 C9_3 C10_3 F14_3 -61.85(18) . . . . ?
F13_3 C9_3 C10_3 F15_3 -58.4(2) . . . . ?
C8_3 C9_3 C10_3 F15_3 61.39(19) . . . . ?
C2_3 C9_3 C10_3 F15_3 -178.68(15) . . . . ?
F13_3 C9_3 C10_3 C5_3 179.85(14) . . . . ?
C8_3 C9_3 C10_3 C5_3 -60.32(18) . . . . ?
C2_3 C9_3 C10_3 C5_3 59.61(19) . . . . ?
F7_3 C5_3 C10_3 F14_3 -58.81(19) . . . . ?
C6_3 C5_3 C10_3 F14_3 -178.43(14) . . . . ?
C4_3 C5_3 C10_3 F14_3 61.37(19) . . . . ?
F7_3 C5_3 C10_3 F15_3 58.22(19) . . . . ?
C6_3 C5_3 C10_3 F15_3 -61.40(18) . . . . ?
C4_3 C5_3 C10_3 F15_3 178.40(14) . . . . ?
F7_3 C5_3 C10_3 C9_3 -179.97(14) . . . . ?
C6_3 C5_3 C10_3 C9_3 60.42(18) . . . . ?
C4_3 C5_3 C10_3 C9_3 -59.78(18) . . . . ?
O1_1 Al1 O1_4 C1_4 -49.5(2) . . . . ?
O1_3 Al1 O1_4 C1_4 -168.98(19) . . . . ?
O1_2 Al1 O1_4 C1_4 69.9(2) . . . . ?
Al1 O1_4 C1_4 C2_4 -28.9(3) . . . . ?
Al1 O1_4 C1_4 C3_4 -148.50(16) . . . . ?
Al1 O1_4 C1_4 C4_4 92.3(2) . . . . ?
O1_4 C1_4 C2_4 F1_4 -56.17(17) . . . . ?
C3_4 C1_4 C2_4 F1_4 64.73(16) . . . . ?
C4_4 C1_4 C2_4 F1_4 179.56(12) . . . . ?
O1_4 C1_4 C2_4 F2_4 59.91(17) . . . . ?
C3_4 C1_4 C2_4 F2_4 -179.20(12) . . . . ?
C4_4 C1_4 C2_4 F2_4 -64.37(15) . . . . ?
O1_4 C1_4 C2_4 C9_4 -178.31(13) . . . . ?
C3_4 C1_4 C2_4 C9_4 -57.41(16) . . . . ?
C4_4 C1_4 C2_4 C9_4 57.42(16) . . . . ?
O1_4 C1_4 C3_4 F3_4 57.86(16) . . . . ?
C2_4 C1_4 C3_4 F3_4 -65.19(15) . . . . ?
C4_4 C1_4 C3_4 F3_4 -179.79(12) . . . . ?
O1_4 C1_4 C3_4 F4_4 -58.39(16) . . . . ?
C2_4 C1_4 C3_4 F4_4 178.56(12) . . . . ?
C4_4 C1_4 C3_4 F4_4 63.96(15) . . . . ?
O1_4 C1_4 C3_4 C7_4 179.84(12) . . . . ?
C2_4 C1_4 C3_4 C7_4 56.79(16) . . . . ?
C4_4 C1_4 C3_4 C7_4 -57.81(15) . . . . ?
O1_4 C1_4 C4_4 F6_4 -60.32(16) . . . . ?
C2_4 C1_4 C4_4 F6_4 64.30(16) . . . . ?
C3_4 C1_4 C4_4 F6_4 179.15(12) . . . . ?
O1_4 C1_4 C4_4 F5_4 56.53(16) . . . . ?
C2_4 C1_4 C4_4 F5_4 -178.85(12) . . . . ?
C3_4 C1_4 C4_4 F5_4 -64.01(16) . . . . ?
O1_4 C1_4 C4_4 C5_4 177.90(12) . . . . ?
C2_4 C1_4 C4_4 C5_4 -57.48(16) . . . . ?
C3_4 C1_4 C4_4 C5_4 57.37(16) . . . . ?
F6_4 C4_4 C5_4 F7_4 58.22(17) . . . . ?
F5_4 C4_4 C5_4 F7_4 -57.42(17) . . . . ?
C1_4 C4_4 C5_4 F7_4 -179.58(13) . . . . ?
F6_4 C4_4 C5_4 C10_4 -61.98(16) . . . . ?
F5_4 C4_4 C5_4 C10_4 -177.62(12) . . . . ?
C1_4 C4_4 C5_4 C10_4 60.23(16) . . . . ?
F6_4 C4_4 C5_4 C6_4 178.24(12) . . . . ?
F5_4 C4_4 C5_4 C6_4 62.59(16) . . . . ?
C1_4 C4_4 C5_4 C6_4 -59.56(17) . . . . ?
F7_4 C5_4 C6_4 F8_4 57.95(18) . . . . ?
C10_4 C5_4 C6_4 F8_4 177.78(13) . . . . ?
C4_4 C5_4 C6_4 F8_4 -62.49(17) . . . . ?
F7_4 C5_4 C6_4 F9_4 -58.44(17) . . . . ?
C10_4 C5_4 C6_4 F9_4 61.39(17) . . . . ?
C4_4 C5_4 C6_4 F9_4 -178.88(12) . . . . ?
F7_4 C5_4 C6_4 C7_4 -179.90(13) . . . . ?
C10_4 C5_4 C6_4 C7_4 -60.07(17) . . . . ?
C4_4 C5_4 C6_4 C7_4 59.66(17) . . . . ?
F8_4 C6_4 C7_4 F10_4 -57.63(17) . . . . ?
F9_4 C6_4 C7_4 F10_4 58.51(17) . . . . ?
C5_4 C6_4 C7_4 F10_4 -179.76(13) . . . . ?
F8_4 C6_4 C7_4 C8_4 -177.96(12) . . . . ?
F9_4 C6_4 C7_4 C8_4 -61.82(17) . . . . ?
C5_4 C6_4 C7_4 C8_4 59.91(17) . . . . ?
F8_4 C6_4 C7_4 C3_4 62.38(16) . . . . ?
F9_4 C6_4 C7_4 C3_4 178.52(13) . . . . ?
C5_4 C6_4 C7_4 C3_4 -59.75(17) . . . . ?
F3_4 C3_4 C7_4 F10_4 -57.93(16) . . . . ?
F4_4 C3_4 C7_4 F10_4 57.83(16) . . . . ?
C1_4 C3_4 C7_4 F10_4 179.78(12) . . . . ?
F3_4 C3_4 C7_4 C6_4 -177.62(12) . . . . ?
F4_4 C3_4 C7_4 C6_4 -61.86(16) . . . . ?
C1_4 C3_4 C7_4 C6_4 60.10(16) . . . . ?
F3_4 C3_4 C7_4 C8_4 62.96(16) . . . . ?
F4_4 C3_4 C7_4 C8_4 178.72(12) . . . . ?
C1_4 C3_4 C7_4 C8_4 -59.33(16) . . . . ?
F10_4 C7_4 C8_4 F12_4 -58.00(18) . . . . ?
C6_4 C7_4 C8_4 F12_4 61.88(16) . . . . ?
C3_4 C7_4 C8_4 F12_4 -178.76(12) . . . . ?
F10_4 C7_4 C8_4 F11_4 58.97(17) . . . . ?
C6_4 C7_4 C8_4 F11_4 178.85(12) . . . . ?
C3_4 C7_4 C8_4 F11_4 -61.79(16) . . . . ?
F10_4 C7_4 C8_4 C9_4 -179.58(13) . . . . ?
C6_4 C7_4 C8_4 C9_4 -59.71(17) . . . . ?
C3_4 C7_4 C8_4 C9_4 59.66(17) . . . . ?
F12_4 C8_4 C9_4 F13_4 58.58(17) . . . . ?
F11_4 C8_4 C9_4 F13_4 -57.82(17) . . . . ?
C7_4 C8_4 C9_4 F13_4 -179.52(12) . . . . ?
F12_4 C8_4 C9_4 C10_4 -61.84(16) . . . . ?
F11_4 C8_4 C9_4 C10_4 -178.24(12) . . . . ?
C7_4 C8_4 C9_4 C10_4 60.06(17) . . . . ?
F12_4 C8_4 C9_4 C2_4 178.27(12) . . . . ?
F11_4 C8_4 C9_4 C2_4 61.87(16) . . . . ?
C7_4 C8_4 C9_4 C2_4 -59.83(16) . . . . ?
F1_4 C2_4 C9_4 F13_4 56.95(16) . . . . ?
F2_4 C2_4 C9_4 F13_4 -58.38(16) . . . . ?
C1_4 C2_4 C9_4 F13_4 -179.98(12) . . . . ?
F1_4 C2_4 C9_4 C10_4 177.00(12) . . . . ?
F2_4 C2_4 C9_4 C10_4 61.67(16) . . . . ?
C1_4 C2_4 C9_4 C10_4 -59.93(16) . . . . ?
F1_4 C2_4 C9_4 C8_4 -62.92(16) . . . . ?
F2_4 C2_4 C9_4 C8_4 -178.24(12) . . . . ?
C1_4 C2_4 C9_4 C8_4 60.16(16) . . . . ?
F13_4 C9_4 C10_4 F14_4 57.49(17) . . . . ?
C8_4 C9_4 C10_4 F14_4 177.92(13) . . . . ?
C2_4 C9_4 C10_4 F14_4 -62.40(16) . . . . ?
F13_4 C9_4 C10_4 F15_4 -58.91(17) . . . . ?
C8_4 C9_4 C10_4 F15_4 61.52(17) . . . . ?
C2_4 C9_4 C10_4 F15_4 -178.80(12) . . . . ?
F13_4 C9_4 C10_4 C5_4 179.56(13) . . . . ?
C8_4 C9_4 C10_4 C5_4 -60.01(17) . . . . ?
C2_4 C9_4 C10_4 C5_4 59.67(17) . . . . ?
F7_4 C5_4 C10_4 F14_4 -58.67(18) . . . . ?
C6_4 C5_4 C10_4 F14_4 -178.38(13) . . . . ?
C4_4 C5_4 C10_4 F14_4 61.82(17) . . . . ?
F7_4 C5_4 C10_4 F15_4 58.25(18) . . . . ?
C6_4 C5_4 C10_4 F15_4 -61.46(18) . . . . ?
C4_4 C5_4 C10_4 F15_4 178.75(13) . . . . ?
F7_4 C5_4 C10_4 C9_4 179.57(13) . . . . ?
C6_4 C5_4 C10_4 C9_4 59.86(17) . . . . ?
C4_4 C5_4 C10_4 C9_4 -59.93(17) . . . . ?

