# Electronic Supplementary Material (ESI) for Dalton Transactions.
# This journal is © The Royal Society of Chemistry 2023

data_BALU6GE7O24_publ

_pd_block_id
  2023-01-23T14:03|BALU6GE7O24|Lipina|Stadi_P

_audit_creation_method  "from EXP file using GSAS2CIF"
_audit_creation_date                   2023-01-23T14:03
_audit_author_name                     Lipina
_audit_update_record
; 2023-01-23T14:03  Initial CIF as created by GSAS2CIF
;

#=============================================================================
# this information describes the project, paper etc. for the CIF             #
# Acta Cryst. Section C papers and editorial correspondence is generated     #
# from the information in this section                                       #
#                                                                            #
#   (from)   CIF submission form for Rietveld refinements (Acta Cryst. C)    #
#                                                 Version 14 December 1998   #
#=============================================================================
# 1. SUBMISSION DETAILS

_publ_contact_author_name            'Lipina, Olga Andreevna'
_publ_contact_author_address         
'Inst. of Solid State Chemistry UB RAS 91, Pervomaiskaya, Ekaterinburg Russia'
_publ_contact_author_email           'LipinaOlgaA@yandex.ru'
_publ_contact_author_fax             ?
_publ_contact_author_phone           '+7 952 143 0282'

_publ_contact_letter
;
Please consider this CIF for publication. I certify that this contibution is the
original work of those listed as authors; that it has not been published
before (in any language or medium) and is not being considered for publication
elsewhere; that all authors concur with and are aware of the submission; that
all workers involved in the study are listed as authors or given proper credit
in the acknowledgements; that I have obtained permission for and acknowledged
the source of any excerpts from other copyright works; and that to the best of
my knowledge the paper contains no statements which are libellous, unlawful or
in any way actionable. All coauthors have made significant scientific
contributions to the work reported, including the ideas and their execution,
and share responsibility and accountability for the results.
;

_publ_requested_journal              'Dalton Transactions'
_publ_requested_coeditor_name        ?
_publ_requested_category             ?   # Acta C: one of CI/CM/CO/FI/FM/FO

#==============================================================================

# 2. PROCESSING SUMMARY (IUCr Office Use Only)

_journal_data_validation_number      ?

_journal_date_recd_electronic        ?
_journal_date_to_coeditor            ?
_journal_date_from_coeditor          ?
_journal_date_accepted               ?
_journal_date_printers_first         ?
_journal_date_printers_final         ?
_journal_date_proofs_out             ?
_journal_date_proofs_in              ?
_journal_coeditor_name               ?
_journal_coeditor_code               ?
_journal_coeditor_notes
; ?
;
_journal_techeditor_code             ?
_journal_techeditor_notes
; ?
;
_journal_coden_ASTM                  ?
_journal_name_full                   'Dalton Transactions'
_journal_year                        2023
_journal_volume                      ?
_journal_issue                       ?
_journal_page_first                  ?
_journal_page_last                   ?
_journal_paper_category              ?
_journal_suppl_publ_number           ?
_journal_suppl_publ_pages            ?

#==============================================================================

# 3. TITLE AND AUTHOR LIST

_publ_section_title
;
Structural, electronic and optical properties of BaRE6(Ge2O7)2(Ge3O10) (RE = Tm,
Yb, Lu) germanates, BaYb6(Ge2O7)2(Ge3O10):Tm3+ and
BaLu6(Ge2O7)2(Ge3O10):Yb3+,Tm3+ phosphors
;
_publ_section_title_footnote
; ?
;

# The loop structure below should contain the names and addresses of all
# authors, in the required order of publication. Repeat as necessary.

loop_
	_publ_author_name
        _publ_author_footnote
	_publ_author_address

'Lipina, Olga A.'
''
'Inst. of Solid State Chemistry, UB RAS, Pervomaiskaya 91, Ekaterinburg, Russia'

'Surat, Ludmila L.'
''
'Inst. of Solid State Chemistry, UB RAS, Pervomaiskaya 91, Ekaterinburg, Russia'

'Chufarov, Alexander Yu.'
''
'Inst. of Solid State Chemistry, UB RAS, Pervomaiskaya 91, Ekaterinburg, Russia'

'Baklanova, Inna V.'
''
'Inst. of Solid State Chemistry, UB RAS, Pervomaiskaya 91, Ekaterinburg, Russia'

'Enyashin, Andrey N.'
''
'Inst. of Solid State Chemistry, UB RAS, Pervomaiskaya 91, Ekaterinburg, Russia'

'Melkozerova, Marina A.'
''
'Inst. of Solid State Chemistry, UB RAS, Pervomaiskaya 91, Ekaterinburg, Russia'

'Tyutyunnik, Alexander P.'
''
'Inst. of Solid State Chemistry, UB RAS, Pervomaiskaya 91, Ekaterinburg, Russia'

'Zubkov, Vladimir G.'
''
'Inst. of Solid State Chemistry, UB RAS, Pervomaiskaya 91, Ekaterinburg, Russia'

#==============================================================================

# 4. TEXT

_publ_section_synopsis
;  ?
;
_publ_section_abstract
; ?
;
_publ_section_comment
; ?
;
_publ_section_exptl_prep      # Details of the preparation of the sample(s)
                              # should be given here.
; ?
;
_publ_section_exptl_refinement
; ?
;
_publ_section_references
; ?
;
_publ_section_figure_captions
; ?
;
_publ_section_acknowledgements
;
The work was carried out in accordance with the state assignment for the
Institute of Solid State Chemistry of the Ural Branch of the Russian Academy
of Sciences (No. AAAA-A19-119031890025-9).
;

#=============================================================================
# 5. OVERALL REFINEMENT & COMPUTING DETAILS

_refine_special_details
; ?
;
_pd_proc_ls_special_details
; ?
;

# The following items are used to identify the programs used.
_computing_molecular_graphics     'ATOMS V6.3.4 ((c) 2008 by Shape Software)'
_computing_publication_material   ?

_refine_ls_weighting_scheme       ?
_refine_ls_weighting_details      ?
_refine_ls_hydrogen_treatment     ?
_refine_ls_extinction_method      ?
_refine_ls_extinction_coef        ?
_refine_ls_number_constraints     ?

_refine_ls_restrained_S_all       ?
_refine_ls_restrained_S_obs       ?

#==============================================================================
# 6. SAMPLE PREPARATION DATA

# (In the unusual case where multiple samples are used in a single
#  Rietveld study, this information should be moved into the phase
#  blocks)

# The following three fields describe the preparation of the material.
# The cooling rate is in K/min.  The pressure at which the sample was
# prepared is in kPa.  The temperature of preparation is in K.

_pd_prep_cool_rate                ?
_pd_prep_pressure                 ?
_pd_prep_temperature              1623

_pd_char_colour                   white       # use ICDD colour descriptions

_refine_ls_shift/su_max                0.00
_refine_ls_shift/su_mean               0.00
_computing_structure_refinement        GSAS
_refine_ls_number_parameters           110
_refine_ls_goodness_of_fit_all         1.45
_refine_ls_number_restraints           0
_refine_ls_matrix_type                 full
#==============================================================================
# 7. CHEMICAL, STRUCTURAL AND CRYSTAL DATA

_pd_char_particle_morphology      ?

_chemical_name_systematic
"Barium hexalutetium heptagermanate"
_chemical_name_common             "Barium Lutetium Germanate"
_chemical_formula_moiety          "Ge7 Lu6 O24, Ba"
_chemical_formula_structural      "BaLu6(Ge2O7)2(Ge3O10)"
_chemical_formula_analytical      ?
_chemical_melting_point           ?
_chemical_compound_source         ?       # for minerals and
                                          # natural products
_symmetry_space_group_name_Hall   "-P 2yb"

_exptl_crystal_F_000               ?
_exptl_crystal_density_diffrn      6.604
_exptl_crystal_density_meas        ?
_exptl_crystal_density_method      "not measured"

_cell_measurement_temperature      298(2)

_cell_special_details
; ?
;

_geom_special_details             ?

# The following item identifies the program(s) used (if appropriate).
_computing_structure_solution
"GSAS (A.C. Larson and R.B. Von Dreele, 2004), EXPGUI (Toby, B.H., 2001)"

#==============================================================================

# 8. Phase information from GSAS




_pd_phase_name                         "BaLu6(Ge2O7)2(Ge3O10)"
_cell_length_a                         5.60323(4)
_cell_length_b                         27.89861(22)
_cell_length_c                         6.97976(5)
_cell_angle_alpha                      90.0
_cell_angle_beta                       106.5939(5)
_cell_angle_gamma                      90.0
_cell_volume                           1045.652(16)
_symmetry_cell_setting                 monoclinic
_symmetry_space_group_name_H-M         "P 1 21/m 1"
loop_ _symmetry_equiv_pos_site_id _symmetry_equiv_pos_as_xyz
       1 +x,+y,+z 
       2 -x,+y+1/2,-z 
      -1 -x,-y,-z 
      -2 +x,-y+1/2,+z 

# ATOMIC COORDINATES AND DISPLACEMENT PARAMETERS


loop_
      _atom_site_type_symbol
      _atom_site_label
      _atom_site_fract_x
      _atom_site_fract_y
      _atom_site_fract_z
      _atom_site_occupancy
      _atom_site_thermal_displace_type
      _atom_site_U_iso_or_equiv
      _atom_site_symmetry_multiplicity
Lu
Lu1     0.88195(24)  0.68530(5)   0.25827(19)  1.0        Uiso   0.0238(4)     4
Lu
Lu2     0.21864(26)  0.60010(4)   0.60525(19)  1.0        Uiso   0.0253(4)     4
Lu
Lu3     0.81145(23)  0.54158(5)   0.82399(19)  1.0        Uiso   0.0240(4)     4
Ba
Ba1     0.7086(4)    0.25         0.06900(32)  1.0        Uiso   0.0285(7)     2
Ge
Ge1     0.2704(6)    0.47531(11)  0.6908(4)    1.0        Uiso   0.0225(9)     4
Ge
Ge2     0.3133(5)    0.61316(11)  0.1238(4)    1.0        Uiso   0.0272(9)     4
Ge
Ge3     0.7647(5)    0.66510(11)  0.7403(4)    1.0        Uiso   0.0220(8)     4
Ge
Ge4     0.5436(7)    0.25         0.5415(5)    1.0        Uiso   0.0264(13)    2
O 
O1      0.0938(23)   0.4499(5)    0.4635(17)   1.0        Uiso   0.0161(10)    4
O 
O2      0.4118(24)   0.5278(5)    0.6773(18)   1.0        Uiso   0.0161(10)    4
O 
O3      0.5339(23)   0.4425(5)    0.7974(18)   1.0        Uiso   0.0161(10)    4
O 
O4      0.0894(22)   0.4798(5)    0.8505(19)   1.0        Uiso   0.0161(10)    4
O 
O5      0.4923(24)   0.6614(5)    0.1161(19)   1.0        Uiso   0.0161(10)    4
O 
O6      0.1168(24)   0.5973(5)   -0.1090(18)   1.0        Uiso   0.0161(10)    4
O 
O7      0.1581(21)   0.6265(5)    0.3101(18)   1.0        Uiso   0.0161(10)    4
O 
O8      0.9122(21)   0.6959(5)    0.9482(17)   1.0        Uiso   0.0161(10)    4
O 
O9      0.6242(24)   0.6129(5)    0.7603(18)   1.0        Uiso   0.0161(10)    4
O 
O10     0.9504(23)   0.6638(5)    0.5713(17)   1.0        Uiso   0.0161(10)    4
O 
O11     0.4896(23)   0.7008(5)    0.6271(16)   1.0        Uiso   0.0161(10)    4
O 
O12     0.3283(27)   0.25         0.6871(24)   1.0        Uiso   0.0161(10)    2
O 
O13     0.8520(32)   0.25         0.6988(25)   1.0        Uiso   0.0161(10)    2
 
# If you change Z, be sure to change all 3 of the following
_chemical_formula_sum                  "Ba Ge7 Lu6 O24"
_chemical_formula_weight               2079.24
_cell_formula_units_Z                  2

# MOLECULAR GEOMETRY

loop_
      _geom_bond_atom_site_label_1
      _geom_bond_atom_site_label_2
      _geom_bond_distance
      _geom_bond_site_symmetry_1
      _geom_bond_site_symmetry_2
      _geom_bond_publ_flag
  Lu1       O5               2.227(13)  .      1_555  N
  Lu1       O7               2.213(12)  .      1_655  N
  Lu1       O8               2.238(11)  .      1_554  N
  Lu1       O10              2.191(12)  .      1_555  N
  Lu1       O12               2.247(9)  .      2_656  N
  Lu1       O13              2.306(10)  .      2_756  N
  Lu2       O1               2.181(13)  .     -1_566  N
  Lu2       O2               2.275(13)  .      1_555  N
  Lu2       O6               2.227(12)  .      1_556  N
  Lu2       O7               2.121(12)  .      1_555  N
  Lu2       O9               2.249(13)  .      1_555  N
  Lu2       O10              2.296(13)  .      1_455  N
  Lu3       O1               2.230(11)  .     -1_666  N
  Lu3       O2               2.214(13)  .      1_555  N
  Lu3       O4               2.295(12)  .      1_655  N
  Lu3       O4               2.259(13)  .     -1_667  N
  Lu3       O6               2.261(13)  .      1_656  N
  Lu3       O9               2.234(12)  .      1_555  N
  Ba1       O5               2.865(13)  .      2_645  N
  Ba1       O5               2.865(13)  .     -1_665  N
  Ba1       O8               2.636(12)  .      2_746  N
  Ba1       O8               2.636(12)  .     -1_766  N
  Ba1       O11              2.993(12)  .      2_646  N
  Ba1       O11              2.993(12)  .     -1_666  N
  Ba1       O12              2.898(15)  .      1_554  N
  Ba1       O13              2.916(16)  .      1_554  N
  Ge1       O1               1.762(12)  .      1_555  N
  Ge1       O1               2.903(13)  .     -1_566  N
  Ge1       O2               1.682(13)  .      1_555  N
  Ge1       O3               1.716(13)  .      1_555  N
  Ge1       O4               1.713(12)  .      1_555  N
  Ge2       O3               1.782(13)  .     -1_666  N
  Ge2       O5               1.689(13)  .      1_555  N
  Ge2       O6               1.739(13)  .      1_555  N
  Ge2       O7               1.798(12)  .      1_555  N
  Ge3       O6               2.718(13)  .      1_656  N
  Ge3       O8               1.686(12)  .      1_555  N
  Ge3       O9               1.681(12)  .      1_555  N
  Ge3       O10              1.782(12)  .      1_555  N
  Ge3       O11              1.816(12)  .      1_555  N
  Ge4       O11              1.782(11)  .      2_646  N
  Ge4       O11              1.782(11)  .     -1_666  N
  Ge4       O12              1.785(15)  .      1_555  N
  Ge4       O13              1.763(17)  .      1_555  N
  O1        Lu2              2.181(13)  .     -1_566  N
  O1        Lu3              2.230(11)  .     -1_666  N
  O1        Ge1              1.762(12)  .      1_555  N
  O1        Ge1              2.903(13)  .     -1_566  N
  O1        O1               3.081(27)  .     -1_566  N
  O1        O2               2.935(18)  .      1_555  N
  O1        O2               2.790(19)  .     -1_566  N
  O1        O3               2.876(17)  .      1_555  N
  O1        O4               2.834(16)  .      1_555  N
  O1        O4               2.902(19)  .     -1_566  N
  O1        O6               2.753(15)  .     -1_565  N
  O1        O9               3.068(17)  .     -1_666  N
  O2        Lu2              2.275(13)  .      1_555  N
  O2        Lu3              2.214(13)  .      1_555  N
  O2        Ge1              1.682(13)  .      1_555  N
  O2        O1               2.935(18)  .      1_555  N
  O2        O1               2.790(19)  .     -1_566  N
  O2        O3               2.553(17)  .      1_555  N
  O2        O4               2.788(18)  .      1_555  N
  O2        O9               2.643(16)  .      1_555  N
  O3        Ge1              1.716(13)  .      1_555  N
  O3        Ge2              1.782(13)  .     -1_666  N
  O3        O1               2.876(17)  .      1_555  N
  O3        O2               2.553(17)  .      1_555  N
  O3        O4               2.820(17)  .      1_555  N
  O3        O5               2.973(18)  .     -1_666  N
  O3        O6               2.713(17)  .     -1_666  N
  O3        O7               2.825(18)  .     -1_666  N
  O4        Lu3              2.295(12)  .      1_455  N
  O4        Lu3              2.259(13)  .     -1_667  N
  O4        Ge1              1.713(12)  .      1_555  N
  O4        O1               2.834(16)  .      1_555  N
  O4        O1               2.902(19)  .     -1_566  N
  O4        O2               2.788(18)  .      1_555  N
  O4        O3               2.820(17)  .      1_555  N
  O4        O4               2.797(25)  .     -1_567  N
  O5        Lu1              2.227(13)  .      1_555  N
  O5        Ba1              2.865(13)  .      2_655  N
  O5        Ge2              1.689(13)  .      1_555  N
  O5        O3               2.973(18)  .     -1_666  N
  O5        O6               2.864(18)  .      1_555  N
  O5        O7               2.782(17)  .      1_555  N
  O5        O8               3.068(16)  .      1_554  N
  O5        O9               3.098(17)  .      1_554  N
  O5        O12              2.866(15)  .      2_656  N
  O6        Lu2              2.227(12)  .      1_554  N
  O6        Lu3              2.261(13)  .      1_454  N
  O6        Ge2              1.739(13)  .      1_555  N
  O6        Ge3              2.718(13)  .      1_454  N
  O6        O1               2.753(15)  .     -1_565  N
  O6        O3               2.713(17)  .     -1_666  N
  O6        O5               2.864(18)  .      1_555  N
  O6        O7               2.981(17)  .      1_555  N
  O6        O8               3.050(18)  .      1_454  N
  O6        O9               2.684(18)  .      1_454  N
  O6        O10              2.846(17)  .      1_454  N
  O7        Lu1              2.213(12)  .      1_455  N
  O7        Lu2              2.121(12)  .      1_555  N
  O7        Ge2              1.798(12)  .      1_555  N
  O7        O3               2.825(18)  .     -1_666  N
  O7        O5               2.782(17)  .      1_555  N
  O7        O6               2.981(17)  .      1_555  N
  O7        O10              2.641(16)  .      1_455  N
  O8        Lu1              2.238(11)  .      1_556  N
  O8        Ba1              2.636(12)  .      2_756  N
  O8        Ge3              1.686(12)  .      1_555  N
  O8        O5               3.068(16)  .      1_556  N
  O8        O6               3.050(18)  .      1_656  N
  O8        O8               3.017(25)  .     -2_565  N
  O8        O9               2.913(18)  .      1_555  N
  O8        O10              2.844(16)  .      1_555  N
  O8        O11              2.760(18)  .      1_555  N
  O8        O13              2.869(19)  .      2_757  N
  O9        Lu2              2.249(13)  .      1_555  N
  O9        Lu3              2.234(12)  .      1_555  N
  O9        Ge3              1.681(12)  .      1_555  N
  O9        O1               3.068(17)  .     -1_666  N
  O9        O2               2.643(16)  .      1_555  N
  O9        O5               3.098(17)  .      1_556  N
  O9        O6               2.684(18)  .      1_656  N
  O9        O8               2.913(18)  .      1_555  N
  O9        O10              2.912(16)  .      1_555  N
  O9        O11              2.656(17)  .      1_555  N
  O10       Lu1              2.191(12)  .      1_555  N
  O10       Lu2              2.296(13)  .      1_655  N
  O10       Ge3              1.782(12)  .      1_555  N
  O10       O6               2.846(17)  .      1_656  N
  O10       O7               2.641(16)  .      1_655  N
  O10       O8               2.844(16)  .      1_555  N
  O10       O9               2.912(16)  .      1_555  N
  O10       O11              2.909(18)  .      1_555  N
  O11       Ba1              2.993(12)  .      2_656  N
  O11       Ge3              1.816(12)  .      1_555  N
  O11       Ge4              1.782(11)  .      2_656  N
  O11       O8               2.760(18)  .      1_555  N
  O11       O9               2.656(17)  .      1_555  N
  O11       O10              2.909(18)  .      1_555  N
  O11       O11              2.743(25)  .     -2_565  N
  O11       O12              3.002(17)  .      2_656  N
  O11       O13              2.869(19)  .      2_656  N
  O12       Lu1               2.247(9)  .      2_646  N
  O12       Lu1               2.247(9)  .     -1_666  N
  O12       Ba1              2.898(15)  .      1_556  N
  O12       Ge4              1.785(15)  .      1_555  N
  O12       O5               2.866(15)  .      2_646  N
  O12       O5               2.866(15)  .     -1_666  N
  O12       O11              3.002(17)  .      2_646  N
  O12       O11              3.002(17)  .     -1_666  N
  O12       O13              2.693(22)  .      1_455  N
  O12       O13              2.912(22)  .      1_555  N
  O13       Lu1              2.306(10)  .      2_746  N
  O13       Lu1              2.306(10)  .     -1_766  N
  O13       Ba1              2.916(16)  .      1_556  N
  O13       Ge4              1.763(17)  .      1_555  N
  O13       O8               2.869(19)  .      2_747  N
  O13       O8               2.869(19)  .     -1_767  N
  O13       O11              2.869(19)  .      2_646  N
  O13       O11              2.869(19)  .     -1_666  N
  O13       O12              2.912(22)  .      1_555  N
  O13       O12              2.693(22)  .      1_655  N

loop_
      _geom_angle_atom_site_label_1
      _geom_angle_atom_site_label_2
      _geom_angle_atom_site_label_3
      _geom_angle
      _geom_angle_site_symmetry_1
      _geom_angle_site_symmetry_2
      _geom_angle_site_symmetry_3
      _geom_angle_publ_flag
  O5        Lu1       O7                113.7(4)      1_555  .      1_655  N
  O5        Lu1       O8                 86.8(4)      1_555  .      1_554  N
  O5        Lu1       O10               103.5(5)      1_555  .      1_555  N
  O5        Lu1       O12                79.7(5)      1_555  .      2_656  N
  O5        Lu1       O13               143.8(5)      1_555  .      2_756  N
  O7        Lu1       O8                 90.8(4)      1_655  .      1_554  N
  O7        Lu1       O10                73.7(5)      1_655  .      1_555  N
  O7        Lu1       O12               160.7(5)      1_655  .      2_656  N
  O7        Lu1       O13                99.4(4)      1_655  .      2_756  N
  O8        Lu1       O10               163.8(5)      1_554  .      1_555  N
  O8        Lu1       O12               104.2(5)      1_554  .      2_656  N
  O8        Lu1       O13                78.3(5)      1_554  .      2_756  N
  O10       Lu1       O12                90.1(5)      1_555  .      2_656  N
  O10       Lu1       O13                99.3(5)      1_555  .      2_756  N
  O12       Lu1       O13                72.5(5)      2_656  .      2_756  N
  O1        Lu2       O2                 77.5(5)     -1_566  .      1_555  N
  O1        Lu2       O6                 77.3(4)     -1_566  .      1_556  N
  O1        Lu2       O7                 96.4(5)     -1_566  .      1_555  N
  O1        Lu2       O9                147.6(5)     -1_566  .      1_555  N
  O1        Lu2       O10                90.7(5)     -1_566  .      1_455  N
  O2        Lu2       O6                 89.9(4)      1_555  .      1_556  N
  O2        Lu2       O7                117.1(5)      1_555  .      1_555  N
  O2        Lu2       O9                 71.5(4)      1_555  .      1_555  N
  O2        Lu2       O10               164.7(5)      1_555  .      1_455  N
  O6        Lu2       O7                150.6(5)      1_556  .      1_555  N
  O6        Lu2       O9                 93.2(5)      1_556  .      1_555  N
  O6        Lu2       O10                78.0(4)      1_556  .      1_455  N
  O7        Lu2       O9                105.8(4)      1_555  .      1_555  N
  O7        Lu2       O10                73.3(4)      1_555  .      1_455  N
  O9        Lu2       O10               118.0(5)      1_555  .      1_455  N
  O1        Lu3       O2                 94.1(5)     -1_666  .      1_555  N
  O1        Lu3       O4                 79.8(5)     -1_666  .      1_655  N
  O1        Lu3       O4                151.6(4)     -1_666  .     -1_667  N
  O1        Lu3       O6                 75.6(4)     -1_666  .      1_656  N
  O1        Lu3       O9                 86.8(4)     -1_666  .      1_555  N
  O2        Lu3       O4                118.7(5)      1_555  .      1_655  N
  O2        Lu3       O4                110.2(4)      1_555  .     -1_667  N
  O2        Lu3       O6                145.2(5)      1_555  .      1_656  N
  O2        Lu3       O9                 72.9(5)      1_555  .      1_555  N
  O4        Lu3       O4                 75.8(5)      1_655  .     -1_667  N
  O4        Lu3       O6                 92.5(4)      1_655  .      1_656  N
  O4        Lu3       O9                162.6(5)      1_655  .      1_555  N
  O4        Lu3       O6                 91.1(5)     -1_667  .      1_656  N
  O4        Lu3       O9                113.7(4)     -1_667  .      1_555  N
  O6        Lu3       O9                 73.3(4)      1_656  .      1_555  N
  O5        Ba1       O5                119.2(5)      2_645  .     -1_665  N
  O5        Ba1       O8                 72.8(4)      2_645  .      2_746  N
  O5        Ba1       O8              133.70(33)      2_645  .     -1_766  N
  O5        Ba1       O11              75.33(34)      2_645  .      2_646  N
  O5        Ba1       O11             122.49(32)      2_645  .     -1_666  N
  O5        Ba1       O12              59.63(27)      2_645  .      1_554  N
  O5        Ba1       O13              76.87(28)      2_645  .      1_554  N
  O5        Ba1       O8              133.70(33)     -1_665  .      2_746  N
  O5        Ba1       O8                 72.8(4)     -1_665  .     -1_766  N
  O5        Ba1       O11             122.49(32)     -1_665  .      2_646  N
  O5        Ba1       O11              75.33(34)     -1_665  .     -1_666  N
  O5        Ba1       O12              59.63(27)     -1_665  .      1_554  N
  O5        Ba1       O13              76.87(28)     -1_665  .      1_554  N
  O8        Ba1       O8                 69.8(5)      2_746  .     -1_766  N
  O8        Ba1       O11               103.7(4)      2_746  .      2_646  N
  O8        Ba1       O11             139.59(34)      2_746  .     -1_666  N
  O8        Ba1       O12               110.4(4)      2_746  .      1_554  N
  O8        Ba1       O13                62.0(4)      2_746  .      1_554  N
  O8        Ba1       O11             139.59(34)     -1_766  .      2_646  N
  O8        Ba1       O11               103.7(4)     -1_766  .     -1_666  N
  O8        Ba1       O12               110.4(4)     -1_766  .      1_554  N
  O8        Ba1       O13                62.0(4)     -1_766  .      1_554  N
  O11       Ba1       O11                54.6(5)      2_646  .     -1_666  N
  O11       Ba1       O12               109.1(4)      2_646  .      1_554  N
  O11       Ba1       O13             151.59(25)      2_646  .      1_554  N
  O11       Ba1       O12               109.1(4)     -1_666  .      1_554  N
  O11       Ba1       O13             151.59(25)     -1_666  .      1_554  N
  O12       Ba1       O13                60.1(4)      1_554  .      1_554  N
  O1        Ge1       O1                 78.5(6)      1_555  .     -1_566  N
  O1        Ge1       O2                116.9(6)      1_555  .      1_555  N
  O1        Ge1       O3                111.6(6)      1_555  .      1_555  N
  O1        Ge1       O4                109.3(6)      1_555  .      1_555  N
  O1        Ge1       O2                 69.2(6)     -1_566  .      1_555  N
  O1        Ge1       O3                166.2(5)     -1_566  .      1_555  N
  O1        Ge1       O4                 72.8(5)     -1_566  .      1_555  N
  O2        Ge1       O3                 97.4(6)      1_555  .      1_555  N
  O2        Ge1       O4                110.4(6)      1_555  .      1_555  N
  O3        Ge1       O4                110.7(6)      1_555  .      1_555  N
  O3        Ge2       O5                117.8(6)     -1_666  .      1_555  N
  O3        Ge2       O6                100.8(6)     -1_666  .      1_555  N
  O3        Ge2       O7                104.2(6)     -1_666  .      1_555  N
  O5        Ge2       O6                113.3(6)      1_555  .      1_555  N
  O5        Ge2       O7                105.8(5)      1_555  .      1_555  N
  O6        Ge2       O7                114.9(6)      1_555  .      1_555  N
  O6        Ge3       O8                 84.2(5)      1_656  .      1_555  N
  O6        Ge3       O9                 70.8(5)      1_656  .      1_555  N
  O6        Ge3       O10                75.2(5)      1_656  .      1_555  N
  O6        Ge3       O11               169.2(5)      1_656  .      1_555  N
  O8        Ge3       O9                119.8(6)      1_555  .      1_555  N
  O8        Ge3       O10               110.1(6)      1_555  .      1_555  N
  O8        Ge3       O11               103.9(6)      1_555  .      1_555  N
  O9        Ge3       O10               114.4(6)      1_555  .      1_555  N
  O9        Ge3       O11                98.8(6)      1_555  .      1_555  N
  O10       Ge3       O11               107.9(6)      1_555  .      1_555  N
  O11       Ge4       O11               100.6(8)      2_646  .     -1_666  N
  O11       Ge4       O12               114.6(5)      2_646  .      1_555  N
  O11       Ge4       O13               108.1(6)      2_646  .      1_555  N
  O11       Ge4       O12               114.6(5)     -1_666  .      1_555  N
  O11       Ge4       O13               108.1(6)     -1_666  .      1_555  N
  O12       Ge4       O13               110.3(7)      1_555  .      1_555  N
  Lu2       O1        Lu3               104.6(5)     -1_566  .     -1_666  N
  Lu2       O1        Ge1               131.7(7)     -1_566  .      1_555  N
  Lu2       O1        Ge1                86.7(4)     -1_566  .     -1_566  N
  Lu2       O1        O1                109.1(6)     -1_566  .     -1_566  N
  Lu2       O1        O2                156.6(6)     -1_566  .      1_555  N
  Lu2       O1        O2                 52.8(4)     -1_566  .     -1_566  N
  Lu2       O1        O3                125.5(6)     -1_566  .      1_555  N
  Lu2       O1        O4                100.0(5)     -1_566  .      1_555  N
  Lu2       O1        O4                100.2(5)     -1_566  .     -1_566  N
  Lu2       O1        O6                 52.1(4)     -1_566  .     -1_565  N
  Lu2       O1        O9                 91.2(5)     -1_566  .     -1_666  N
  Lu3       O1        Ge1               123.4(7)     -1_666  .      1_555  N
  Lu3       O1        Ge1                85.0(4)     -1_666  .     -1_566  N
  Lu3       O1        O1                103.4(6)     -1_666  .     -1_566  N
  Lu3       O1        O2                 96.4(5)     -1_666  .      1_555  N
  Lu3       O1        O2                 97.9(5)     -1_666  .     -1_566  N
  Lu3       O1        O3                111.6(5)     -1_666  .      1_555  N
  Lu3       O1        O4                153.5(7)     -1_666  .      1_555  N
  Lu3       O1        O4                 51.1(4)     -1_666  .     -1_566  N
  Lu3       O1        O6                 52.7(4)     -1_666  .     -1_565  N
  Lu3       O1        O9               46.63(32)     -1_666  .     -1_666  N
  Ge1       O1        Ge1               101.5(6)      1_555  .     -1_566  N
  Ge1       O1        O1                 67.4(5)      1_555  .     -1_566  N
  Ge1       O1        O2                 30.7(4)      1_555  .      1_555  N
  Ge1       O1        O2                118.7(7)      1_555  .     -1_566  N
  Ge1       O1        O3                 33.7(4)      1_555  .      1_555  N
  Ge1       O1        O4                 34.8(4)      1_555  .      1_555  N
  Ge1       O1        O4                113.2(7)      1_555  .     -1_566  N
  Ge1       O1        O6                171.2(7)      1_555  .     -1_565  N
  Ge1       O1        O9                116.7(6)      1_555  .     -1_666  N
  Ge1       O1        O1               34.08(29)     -1_566  .     -1_566  N
  Ge1       O1        O2                 85.2(5)     -1_566  .      1_555  N
  Ge1       O1        O2               34.29(30)     -1_566  .     -1_566  N
  Ge1       O1        O3                134.5(6)     -1_566  .      1_555  N
  Ge1       O1        O4                 86.9(4)     -1_566  .      1_555  N
  Ge1       O1        O4               34.32(27)     -1_566  .     -1_566  N
  Ge1       O1        O6                 86.3(4)     -1_566  .     -1_565  N
  Ge1       O1        O9                129.1(5)     -1_566  .     -1_666  N
  O1        O1        O2                 55.2(5)     -1_566  .      1_555  N
  O1        O1        O2                 59.8(5)     -1_566  .     -1_566  N
  O1        O1        O3                100.7(6)     -1_566  .      1_555  N
  O1        O1        O4                 58.6(5)     -1_566  .      1_555  N
  O1        O1        O4                 56.5(4)     -1_566  .     -1_566  N
  O1        O1        O6                120.3(6)     -1_566  .     -1_565  N
  O1        O1        O9                148.4(7)     -1_566  .     -1_666  N
  O2        O1        O2                115.0(5)      1_555  .     -1_566  N
  O2        O1        O3                 52.1(4)      1_555  .      1_555  N
  O2        O1        O4                 57.8(4)      1_555  .      1_555  N
  O2        O1        O4                 85.1(5)      1_555  .     -1_566  N
  O2        O1        O6                148.6(6)      1_555  .     -1_565  N
  O2        O1        O9                110.8(5)      1_555  .     -1_666  N
  O2        O1        O3                148.3(5)     -1_566  .      1_555  N
  O2        O1        O4                 89.2(5)     -1_566  .      1_555  N
  O2        O1        O4                 58.6(4)     -1_566  .     -1_566  N
  O2        O1        O6                 70.0(4)     -1_566  .     -1_565  N
  O2        O1        O9                124.5(6)     -1_566  .     -1_666  N
  O3        O1        O4                 59.2(4)      1_555  .      1_555  N
  O3        O1        O4                134.2(6)      1_555  .     -1_566  N
  O3        O1        O6                137.9(6)      1_555  .     -1_565  N
  O3        O1        O9                 85.7(5)      1_555  .     -1_666  N
  O4        O1        O4                115.0(5)      1_555  .     -1_566  N
  O4        O1        O6                151.5(6)      1_555  .     -1_565  N
  O4        O1        O9                143.1(6)      1_555  .     -1_666  N
  O4        O1        O6                 71.1(4)     -1_566  .     -1_565  N
  O4        O1        O9                 97.1(5)     -1_566  .     -1_666  N
  O6        O1        O9                 54.6(4)     -1_565  .     -1_666  N
  Lu2       O2        Lu3               107.7(6)      1_555  .      1_555  N
  Lu2       O2        Ge1               125.6(7)      1_555  .      1_555  N
  Lu2       O2        O1                111.3(5)      1_555  .      1_555  N
  Lu2       O2        O1                 49.7(4)      1_555  .     -1_566  N
  Lu2       O2        O3                164.8(7)      1_555  .      1_555  N
  Lu2       O2        O4                101.3(5)      1_555  .      1_555  N
  Lu2       O2        O9                 53.8(4)      1_555  .      1_555  N
  Lu3       O2        Ge1               123.7(7)      1_555  .      1_555  N
  Lu3       O2        O1                138.6(6)      1_555  .      1_555  N
  Lu3       O2        O1                156.3(6)      1_555  .     -1_566  N
  Lu3       O2        O3                 82.5(5)      1_555  .      1_555  N
  Lu3       O2        O4                125.3(6)      1_555  .      1_555  N
  Lu3       O2        O9                 53.9(4)      1_555  .      1_555  N
  Ge1       O2        O1                 32.3(4)      1_555  .      1_555  N
  Ge1       O2        O1                 76.5(6)      1_555  .     -1_566  N
  Ge1       O2        O3                 41.8(4)      1_555  .      1_555  N
  Ge1       O2        O4                 35.2(4)      1_555  .      1_555  N
  Ge1       O2        O9                163.7(7)      1_555  .      1_555  N
  O1        O2        O1                 65.0(5)      1_555  .     -1_566  N
  O1        O2        O3                 62.8(5)      1_555  .      1_555  N
  O1        O2        O4                 59.3(4)      1_555  .      1_555  N
  O1        O2        O9                161.2(6)      1_555  .      1_555  N
  O1        O2        O3                118.2(7)     -1_566  .      1_555  N
  O1        O2        O4                 62.7(5)     -1_566  .      1_555  N
  O1        O2        O9                103.0(5)     -1_566  .      1_555  N
  O3        O2        O4                 63.6(5)      1_555  .      1_555  N
  O3        O2        O9                134.7(6)      1_555  .      1_555  N
  O4        O2        O9                130.1(6)      1_555  .      1_555  N
  Ge1       O3        Ge2               151.3(7)      1_555  .     -1_666  N
  Ge1       O3        O1                 34.7(4)      1_555  .      1_555  N
  Ge1       O3        O2                 40.8(4)      1_555  .      1_555  N
  Ge1       O3        O4                 34.6(4)      1_555  .      1_555  N
  Ge1       O3        O5                121.5(6)      1_555  .     -1_666  N
  Ge1       O3        O6                154.2(6)      1_555  .     -1_666  N
  Ge1       O3        O7                139.8(7)      1_555  .     -1_666  N
  Ge2       O3        O1                122.5(6)     -1_666  .      1_555  N
  Ge2       O3        O2                166.9(7)     -1_666  .      1_555  N
  Ge2       O3        O4                130.2(6)     -1_666  .      1_555  N
  Ge2       O3        O5               30.16(33)     -1_666  .     -1_666  N
  Ge2       O3        O6                 39.0(4)     -1_666  .     -1_666  N
  Ge2       O3        O7                 38.1(4)     -1_666  .     -1_666  N
  O1        O3        O2                 65.1(5)      1_555  .      1_555  N
  O1        O3        O4                 59.7(4)      1_555  .      1_555  N
  O1        O3        O5                 98.9(5)      1_555  .     -1_666  N
  O1        O3        O6                159.1(7)      1_555  .     -1_666  N
  O1        O3        O7                106.3(5)      1_555  .     -1_666  N
  O2        O3        O4                 62.3(5)      1_555  .      1_555  N
  O2        O3        O5                162.2(6)      1_555  .     -1_666  N
  O2        O3        O6                135.2(6)      1_555  .     -1_666  N
  O2        O3        O7                132.4(5)      1_555  .     -1_666  N
  O4        O3        O5                103.7(5)      1_555  .     -1_666  N
  O4        O3        O6                120.5(5)      1_555  .     -1_666  N
  O4        O3        O7                156.3(6)      1_555  .     -1_666  N
  O5        O3        O6                 60.3(5)     -1_666  .     -1_666  N
  O5        O3        O7                 57.3(4)     -1_666  .     -1_666  N
  O6        O3        O7                 65.1(5)     -1_666  .     -1_666  N
  Lu3       O4        Lu3               104.2(5)      1_455  .     -1_667  N
  Lu3       O4        Ge1               121.1(7)      1_455  .      1_555  N
  Lu3       O4        O1                109.6(5)      1_455  .      1_555  N
  Lu3       O4        O1               49.14(33)      1_455  .     -1_566  N
  Lu3       O4        O2                 96.5(5)      1_455  .      1_555  N
  Lu3       O4        O3                150.6(6)      1_455  .      1_555  N
  Lu3       O4        O4                 51.5(4)      1_455  .     -1_567  N
  Lu3       O4        Ge1               127.9(7)     -1_667  .      1_555  N
  Lu3       O4        O1                144.5(6)     -1_667  .      1_555  N
  Lu3       O4        O1                150.5(6)     -1_667  .     -1_566  N
  Lu3       O4        O2                124.0(6)     -1_667  .      1_555  N
  Lu3       O4        O3                 93.5(5)     -1_667  .      1_555  N
  Lu3       O4        O4                 52.7(4)     -1_667  .     -1_567  N
  Ge1       O4        O1                 35.9(4)      1_555  .      1_555  N
  Ge1       O4        O1                 72.9(5)      1_555  .     -1_566  N
  Ge1       O4        O2                 34.4(4)      1_555  .      1_555  N
  Ge1       O4        O3                 34.7(4)      1_555  .      1_555  N
  Ge1       O4        O4                156.9(9)      1_555  .     -1_567  N
  O1        O4        O1                 65.0(5)      1_555  .     -1_566  N
  O1        O4        O2                 62.9(5)      1_555  .      1_555  N
  O1        O4        O3                 61.2(4)      1_555  .      1_555  N
  O1        O4        O4                158.8(8)      1_555  .     -1_567  N
  O1        O4        O2                 58.7(5)     -1_566  .      1_555  N
  O1        O4        O3                106.6(5)     -1_566  .      1_555  N
  O1        O4        O4                 99.6(6)     -1_566  .     -1_567  N
  O2        O4        O3                 54.2(4)      1_555  .      1_555  N
  O2        O4        O4                123.0(8)      1_555  .     -1_567  N
  O3        O4        O4                139.9(7)      1_555  .     -1_567  N
  Lu1       O5        Ba1                98.7(5)      1_555  .      2_655  N
  Lu1       O5        Ge2               137.7(7)      1_555  .      1_555  N
  Lu1       O5        O3                107.5(5)      1_555  .     -1_666  N
  Lu1       O5        O6                154.7(6)      1_555  .      1_555  N
  Lu1       O5        O7                126.8(6)      1_555  .      1_555  N
  Lu1       O5        O8               46.76(32)      1_555  .      1_554  N
  Lu1       O5        O9                 93.4(4)      1_555  .      1_554  N
  Lu1       O5        O12                50.5(4)      1_555  .      2_656  N
  Ba1       O5        Ge2               122.8(6)      2_655  .      1_555  N
  Ba1       O5        O3                153.7(6)      2_655  .     -1_666  N
  Ba1       O5        O6                 99.1(5)      2_655  .      1_555  N
  Ba1       O5        O7                106.8(5)      2_655  .      1_555  N
  Ba1       O5        O8                 78.6(4)      2_655  .      1_554  N
  Ba1       O5        O9                 99.7(4)      2_655  .      1_554  N
  Ba1       O5        O12                60.8(4)      2_655  .      2_656  N
  Ge2       O5        O3                 32.0(4)      1_555  .     -1_666  N
  Ge2       O5        O6                 33.9(4)      1_555  .      1_555  N
  Ge2       O5        O7                 38.4(4)      1_555  .      1_555  N
  Ge2       O5        O8                142.1(6)      1_555  .      1_554  N
  Ge2       O5        O9                 87.5(5)      1_555  .      1_554  N
  Ge2       O5        O12               143.4(7)      1_555  .      2_656  N
  O3        O5        O6                 55.4(4)     -1_666  .      1_555  N
  O3        O5        O7                 58.7(4)     -1_666  .      1_555  N
  O3        O5        O8                118.1(5)     -1_666  .      1_554  N
  O3        O5        O9                 76.9(4)     -1_666  .      1_554  N
  O3        O5        O12               140.7(6)     -1_666  .      2_656  N
  O6        O5        O7                 63.7(5)      1_555  .      1_555  N
  O6        O5        O8                120.6(5)      1_555  .      1_554  N
  O6        O5        O9                 66.0(4)      1_555  .      1_554  N
  O6        O5        O12               154.6(6)      1_555  .      2_656  N
  O7        O5        O8                172.9(6)      1_555  .      1_554  N
  O7        O5        O9                125.8(6)      1_555  .      1_554  N
  O7        O5        O12               105.2(6)      1_555  .      2_656  N
  O8        O5        O9                 56.4(4)      1_554  .      1_554  N
  O8        O5        O12                73.2(5)      1_554  .      2_656  N
  O9        O5        O12               129.0(6)      1_554  .      2_656  N
  Lu2       O6        Lu3               102.2(5)      1_554  .      1_454  N
  Lu2       O6        Ge2               124.9(7)      1_554  .      1_555  N
  Lu2       O6        Ge3                88.4(4)      1_554  .      1_454  N
  Lu2       O6        O1                 50.6(4)      1_554  .     -1_565  N
  Lu2       O6        O3                114.9(5)      1_554  .     -1_666  N
  Lu2       O6        O5                 97.7(5)      1_554  .      1_555  N
  Lu2       O6        O7                154.4(6)      1_554  .      1_555  N
  Lu2       O6        O8                106.7(5)      1_554  .      1_454  N
  Lu2       O6        O9                101.1(5)      1_554  .      1_454  N
  Lu2       O6        O10              52.09(35)      1_554  .      1_454  N
  Lu3       O6        Ge2               127.4(7)      1_454  .      1_555  N
  Lu3       O6        Ge3                88.6(4)      1_454  .      1_454  N
  Lu3       O6        O1               51.69(34)      1_454  .     -1_565  N
  Lu3       O6        O3                102.4(5)      1_454  .     -1_666  N
  Lu3       O6        O5                159.6(6)      1_454  .      1_555  N
  Lu3       O6        O7                103.4(5)      1_454  .      1_555  N
  Lu3       O6        O8                110.9(5)      1_454  .      1_454  N
  Lu3       O6        O9                 52.9(4)      1_454  .      1_454  N
  Lu3       O6        O10               103.1(5)      1_454  .      1_454  N
  Ge2       O6        Ge3               112.4(6)      1_555  .      1_454  N
  Ge2       O6        O1                162.8(6)      1_555  .     -1_565  N
  Ge2       O6        O3                 40.2(4)      1_555  .     -1_666  N
  Ge2       O6        O5                 32.8(4)      1_555  .      1_555  N
  Ge2       O6        O7                 33.2(4)      1_555  .      1_555  N
  Ge2       O6        O8                 79.1(5)      1_555  .      1_454  N
  Ge2       O6        O9                126.3(7)      1_555  .      1_454  N
  Ge2       O6        O10               123.1(7)      1_555  .      1_454  N
  Ge3       O6        O1                 84.7(4)      1_454  .     -1_565  N
  Ge3       O6        O3                150.8(6)      1_454  .     -1_666  N
  Ge3       O6        O5                 96.7(5)      1_454  .      1_555  N
  Ge3       O6        O7                 92.0(4)      1_454  .      1_555  N
  Ge3       O6        O8               33.37(25)      1_454  .      1_454  N
  Ge3       O6        O9               36.25(32)      1_454  .      1_454  N
  Ge3       O6        O10              37.28(29)      1_454  .      1_454  N
  O1        O6        O3                123.4(5)     -1_565  .     -1_666  N
  O1        O6        O5                148.3(6)     -1_565  .      1_555  N
  O1        O6        O7                154.9(6)     -1_565  .      1_555  N
  O1        O6        O8                117.9(5)     -1_565  .      1_454  N
  O1        O6        O9                 68.7(4)     -1_565  .      1_454  N
  O1        O6        O10                69.3(4)     -1_565  .      1_454  N
  O3        O6        O5                 64.4(5)     -1_666  .      1_555  N
  O3        O6        O7                 59.3(4)     -1_666  .      1_555  N
  O3        O6        O8                118.4(5)     -1_666  .      1_454  N
  O3        O6        O9                140.8(6)     -1_666  .      1_454  N
  O3        O6        O10               153.5(6)     -1_666  .      1_454  N
  O5        O6        O7                 56.8(4)      1_555  .      1_555  N
  O5        O6        O8                 67.0(5)      1_555  .      1_454  N
  O5        O6        O9                127.5(6)      1_555  .      1_454  N
  O5        O6        O10                92.8(5)      1_555  .      1_454  N
  O7        O6        O8                 63.4(4)      1_555  .      1_454  N
  O7        O6        O9                 94.2(5)      1_555  .      1_454  N
  O7        O6        O10               120.5(5)      1_555  .      1_454  N
  O8        O6        O9                 60.7(4)      1_454  .      1_454  N
  O8        O6        O10                57.6(4)      1_454  .      1_454  N
  O9        O6        O10                63.5(4)      1_454  .      1_454  N
  Lu1       O7        Lu2               109.0(5)      1_455  .      1_555  N
  Lu1       O7        Ge2               119.7(6)      1_455  .      1_555  N
  Lu1       O7        O3                155.9(6)      1_455  .     -1_666  N
  Lu1       O7        O5                101.3(5)      1_455  .      1_555  N
  Lu1       O7        O6                100.8(5)      1_455  .      1_555  N
  Lu1       O7        O10                52.8(4)      1_455  .      1_455  N
  Lu2       O7        Ge2               130.9(7)      1_555  .      1_555  N
  Lu2       O7        O3                 94.7(5)      1_555  .     -1_666  N
  Lu2       O7        O5                130.6(6)      1_555  .      1_555  N
  Lu2       O7        O6                143.6(6)      1_555  .      1_555  N
  Lu2       O7        O10                56.4(4)      1_555  .      1_455  N
  Ge2       O7        O3               37.69(35)      1_555  .     -1_666  N
  Ge2       O7        O5               35.74(35)      1_555  .      1_555  N
  Ge2       O7        O6                 32.0(4)      1_555  .      1_555  N
  Ge2       O7        O10               168.7(7)      1_555  .      1_455  N
  O3        O7        O5                 64.0(4)     -1_666  .      1_555  N
  O3        O7        O6                 55.6(4)     -1_666  .      1_555  N
  O3        O7        O10               151.0(6)     -1_666  .      1_455  N
  O5        O7        O6                 59.5(5)      1_555  .      1_555  N
  O5        O7        O10               133.5(7)      1_555  .      1_455  N
  O6        O7        O10               149.2(6)      1_555  .      1_455  N
  Lu1       O8        Ba1               113.9(5)      1_556  .      2_756  N
  Lu1       O8        Ge3               127.6(7)      1_556  .      1_555  N
  Lu1       O8        O5               46.45(32)      1_556  .      1_556  N
  Lu1       O8        O6                 98.2(5)      1_556  .      1_656  N
  Lu1       O8        O8               97.62(32)      1_556  .     -2_575  N
  Lu1       O8        O9                 98.3(5)      1_556  .      1_555  N
  Lu1       O8        O10               154.0(6)      1_556  .      1_555  N
  Lu1       O8        O11               120.5(5)      1_556  .      1_555  N
  Lu1       O8        O13                51.9(4)      1_556  .      2_757  N
  Ba1       O8        Ge3               117.1(5)      2_756  .      1_555  N
  Ba1       O8        O5                155.9(5)      2_756  .      1_556  N
  Ba1       O8        O6                 99.9(4)      2_756  .      1_656  N
  Ba1       O8        O8               55.10(26)      2_756  .     -2_575  N
  Ba1       O8        O9                141.7(5)      2_756  .      1_555  N
  Ba1       O8        O10                82.2(4)      2_756  .      1_555  N
  Ba1       O8        O11               116.8(5)      2_756  .      1_555  N
  Ba1       O8        O13                63.8(4)      2_756  .      2_757  N
  Ge3       O8        O5                 85.9(5)      1_555  .      1_556  N
  Ge3       O8        O6                 62.4(5)      1_555  .      1_656  N
  Ge3       O8        O8                120.7(4)      1_555  .     -2_575  N
  Ge3       O8        O9               30.05(35)      1_555  .      1_555  N
  Ge3       O8        O10              36.03(35)      1_555  .      1_555  N
  Ge3       O8        O11                39.7(4)      1_555  .      1_555  N
  Ge3       O8        O13               178.1(7)      1_555  .      2_757  N
  O5        O8        O6                 97.2(5)      1_556  .      1_656  N
  O5        O8        O8              108.29(32)      1_556  .     -2_575  N
  O5        O8        O9                 62.3(4)      1_556  .      1_555  N
  O5        O8        O10               121.5(5)      1_556  .      1_555  N
  O5        O8        O11                75.6(4)      1_556  .      1_555  N
  O5        O8        O13                93.0(5)      1_556  .      2_757  N
  O6        O8        O8              154.40(32)      1_656  .     -2_575  N
  O6        O8        O9                 53.4(4)      1_656  .      1_555  N
  O6        O8        O10                57.6(4)      1_656  .      1_555  N
  O6        O8        O11               101.9(5)      1_656  .      1_555  N
  O6        O8        O13               119.2(5)      1_656  .      2_757  N
  O8        O8        O9                142.7(4)     -2_575  .      1_555  N
  O8        O8        O10             108.37(33)     -2_575  .      1_555  N
  O8        O8        O11              87.16(35)     -2_575  .      1_555  N
  O8        O8        O13              58.28(30)     -2_575  .      2_757  N
  O9        O8        O10                60.7(4)      1_555  .      1_555  N
  O9        O8        O11                55.8(4)      1_555  .      1_555  N
  O9        O8        O13               149.9(5)      1_555  .      2_757  N
  O10       O8        O11                62.5(4)      1_555  .      1_555  N
  O10       O8        O13               145.3(6)      1_555  .      2_757  N
  O11       O8        O13               138.5(6)      1_555  .      2_757  N
  Lu2       O9        Lu3               107.9(5)      1_555  .      1_555  N
  Lu2       O9        Ge3               122.0(7)      1_555  .      1_555  N
  Lu2       O9        O1                105.1(5)      1_555  .     -1_666  N
  Lu2       O9        O2                 54.7(4)      1_555  .      1_555  N
  Lu2       O9        O5                 90.9(4)      1_555  .      1_556  N
  Lu2       O9        O6                159.7(6)      1_555  .      1_656  N
  Lu2       O9        O8                134.1(6)      1_555  .      1_555  N
  Lu2       O9        O10               122.6(6)      1_555  .      1_555  N
  Lu2       O9        O11                80.3(5)      1_555  .      1_555  N
  Lu3       O9        Ge3               125.7(7)      1_555  .      1_555  N
  Lu3       O9        O1               46.54(32)      1_555  .     -1_666  N
  Lu3       O9        O2                 53.2(4)      1_555  .      1_555  N
  Lu3       O9        O5                115.9(5)      1_555  .      1_556  N
  Lu3       O9        O6                 53.8(4)      1_555  .      1_656  N
  Lu3       O9        O8                116.8(6)      1_555  .      1_555  N
  Lu3       O9        O10               101.8(5)      1_555  .      1_555  N
  Lu3       O9        O11               164.3(6)      1_555  .      1_555  N
  Ge3       O9        O1                 97.5(6)      1_555  .     -1_666  N
  Ge3       O9        O2                162.2(7)      1_555  .      1_555  N
  Ge3       O9        O5                 85.0(5)      1_555  .      1_556  N
  Ge3       O9        O6                 73.0(6)      1_555  .      1_656  N
  Ge3       O9        O8                 30.2(4)      1_555  .      1_555  N
  Ge3       O9        O10              33.87(35)      1_555  .      1_555  N
  Ge3       O9        O11                42.5(4)      1_555  .      1_555  N
  O1        O9        O2                 69.0(5)     -1_666  .      1_555  N
  O1        O9        O5                158.9(6)     -1_666  .      1_556  N
  O1        O9        O6                 56.7(4)     -1_666  .      1_656  N
  O1        O9        O8                112.6(5)     -1_666  .      1_555  N
  O1        O9        O10                64.3(4)     -1_666  .      1_555  N
  O1        O9        O11               119.0(5)     -1_666  .      1_555  N
  O2        O9        O5                111.9(5)      1_555  .      1_556  N
  O2        O9        O6                106.5(5)      1_555  .      1_656  N
  O2        O9        O8                165.8(6)      1_555  .      1_555  N
  O2        O9        O10               129.8(5)      1_555  .      1_555  N
  O2        O9        O11               133.4(6)      1_555  .      1_555  N
  O5        O9        O6                104.8(5)      1_556  .      1_656  N
  O5        O9        O8                 61.3(4)      1_556  .      1_555  N
  O5        O9        O10               118.3(6)      1_556  .      1_555  N
  O5        O9        O11                76.6(5)      1_556  .      1_555  N
  O6        O9        O8                 65.9(5)      1_656  .      1_555  N
  O6        O9        O10                61.0(4)      1_656  .      1_555  N
  O6        O9        O11               115.5(6)      1_656  .      1_555  N
  O8        O9        O10                58.5(4)      1_555  .      1_555  N
  O8        O9        O11                59.2(5)      1_555  .      1_555  N
  O10       O9        O11                62.8(5)      1_555  .      1_555  N
  Lu1       O10       Lu2               103.8(5)      1_555  .      1_655  N
  Lu1       O10       Ge3               133.2(7)      1_555  .      1_555  N
  Lu1       O10       O6                152.2(6)      1_555  .      1_656  N
  Lu1       O10       O7                 53.5(4)      1_555  .      1_655  N
  Lu1       O10       O8                142.9(6)      1_555  .      1_555  N
  Lu1       O10       O9                129.2(6)      1_555  .      1_555  N
  Lu1       O10       O11                97.3(5)      1_555  .      1_555  N
  Lu2       O10       Ge3               115.9(6)      1_655  .      1_555  N
  Lu2       O10       O6               49.94(33)      1_655  .      1_656  N
  Lu2       O10       O7               50.31(35)      1_655  .      1_655  N
  Lu2       O10       O8                111.6(5)      1_655  .      1_555  N
  Lu2       O10       O9                 93.0(5)      1_655  .      1_555  N
  Lu2       O10       O11               147.3(6)      1_655  .      1_555  N
  Ge3       O10       O6                 67.5(5)      1_555  .      1_656  N
  Ge3       O10       O7                157.0(7)      1_555  .      1_655  N
  Ge3       O10       O8               33.82(34)      1_555  .      1_555  N
  Ge3       O10       O9               31.71(34)      1_555  .      1_555  N
  Ge3       O10       O11              36.45(35)      1_555  .      1_555  N
  O6        O10       O7                100.0(5)      1_656  .      1_655  N
  O6        O10       O8                 64.8(4)      1_656  .      1_555  N
  O6        O10       O9                 55.6(4)      1_656  .      1_555  N
  O6        O10       O11               103.4(5)      1_656  .      1_555  N
  O7        O10       O8                158.0(6)      1_655  .      1_555  N
  O7        O10       O9                125.3(6)      1_655  .      1_555  N
  O7        O10       O11               144.6(6)      1_655  .      1_555  N
  O8        O10       O9                 60.8(4)      1_555  .      1_555  N
  O8        O10       O11                57.3(4)      1_555  .      1_555  N
  O9        O10       O11                54.3(4)      1_555  .      1_555  N
  Ba1       O11       Ge3               112.6(5)      2_656  .      1_555  N
  Ba1       O11       Ge4                97.2(5)      2_656  .      2_656  N
  Ba1       O11       O8                 81.6(4)      2_656  .      1_555  N
  Ba1       O11       O9                107.5(4)      2_656  .      1_555  N
  Ba1       O11       O10               141.3(5)      2_656  .      1_555  N
  Ba1       O11       O11              62.72(23)      2_656  .     -2_575  N
  Ba1       O11       O12               125.5(5)      2_656  .      2_656  N
  Ba1       O11       O13                92.5(4)      2_656  .      2_656  N
  Ge3       O11       Ge4               128.7(7)      1_555  .      2_656  N
  Ge3       O11       O8                 36.4(4)      1_555  .      1_555  N
  Ge3       O11       O9                 38.7(4)      1_555  .      1_555  N
  Ge3       O11       O10              35.67(34)      1_555  .      1_555  N
  Ge3       O11       O11               123.3(4)      1_555  .     -2_575  N
  Ge3       O11       O12                98.3(5)      1_555  .      2_656  N
  Ge3       O11       O13               153.9(6)      1_555  .      2_656  N
  Ge4       O11       O8                118.5(6)      2_656  .      1_555  N
  Ge4       O11       O9                155.2(7)      2_656  .      1_555  N
  Ge4       O11       O10                96.5(5)      2_656  .      1_555  N
  Ge4       O11       O11                39.7(4)      2_656  .     -2_575  N
  Ge4       O11       O12              32.74(32)      2_656  .      2_656  N
  Ge4       O11       O13                35.7(4)      2_656  .      2_656  N
  O8        O11       O9                 65.0(5)      1_555  .      1_555  N
  O8        O11       O10                60.2(4)      1_555  .      1_555  N
  O8        O11       O11              92.84(35)      1_555  .     -2_575  N
  O8        O11       O12               102.9(5)      1_555  .      2_656  N
  O8        O11       O13               153.0(5)      1_555  .      2_656  N
  O9        O11       O10                62.9(5)      1_555  .      1_555  N
  O9        O11       O11               157.5(4)      1_555  .     -2_575  N
  O9        O11       O12               123.8(5)      1_555  .      2_656  N
  O9        O11       O13               141.0(6)      1_555  .      2_656  N
  O10       O11       O11               110.8(4)      1_555  .     -2_575  N
  O10       O11       O12                64.2(4)      1_555  .      2_656  N
  O10       O11       O13               118.7(5)      1_555  .      2_656  N
  O11       O11       O12              62.81(28)     -2_575  .      2_656  N
  O11       O11       O13              61.44(29)     -2_575  .      2_656  N
  O12       O11       O13                59.4(5)      2_656  .      2_656  N
  Lu1       O12       Lu1               106.9(6)      2_646  .     -1_666  N
  Lu1       O12       Ba1                97.3(5)      2_646  .      1_556  N
  Lu1       O12       Ge4               124.7(4)      2_646  .      1_555  N
  Lu1       O12       O5               49.85(28)      2_646  .      2_646  N
  Lu1       O12       O5                137.8(7)      2_646  .     -1_666  N
  Lu1       O12       O11                93.5(4)      2_646  .      2_646  N
  Lu1       O12       O11               142.7(6)      2_646  .     -1_666  N
  Lu1       O12       O13              54.74(32)      2_646  .      1_455  N
  Lu1       O12       O13             124.63(34)      2_646  .      1_555  N
  Lu1       O12       Ba1                97.3(5)     -1_666  .      1_556  N
  Lu1       O12       Ge4               124.7(4)     -1_666  .      1_555  N
  Lu1       O12       O5                137.8(7)     -1_666  .      2_646  N
  Lu1       O12       O5               49.85(28)     -1_666  .     -1_666  N
  Lu1       O12       O11               142.7(6)     -1_666  .      2_646  N
  Lu1       O12       O11                93.5(4)     -1_666  .     -1_666  N
  Lu1       O12       O13              54.74(32)     -1_666  .      1_455  N
  Lu1       O12       O13             124.63(34)     -1_666  .      1_555  N
  Ba1       O12       Ge4                94.9(6)      1_556  .      1_555  N
  Ba1       O12       O5                 59.6(4)      1_556  .      2_646  N
  Ba1       O12       O5                 59.6(4)      1_556  .     -1_666  N
  Ba1       O12       O11               111.0(5)      1_556  .      2_646  N
  Ba1       O12       O11               111.0(5)      1_556  .     -1_666  N
  Ba1       O12       O13               116.5(7)      1_556  .      1_455  N
  Ba1       O12       O13                60.3(4)      1_556  .      1_555  N
  Ge4       O12       O5                 94.1(5)      1_555  .      2_646  N
  Ge4       O12       O5                 94.1(5)      1_555  .     -1_666  N
  Ge4       O12       O11              32.67(32)      1_555  .      2_646  N
  Ge4       O12       O11              32.67(32)      1_555  .     -1_666  N
  Ge4       O12       O13               148.6(9)      1_555  .      1_455  N
  Ge4       O12       O13                34.6(4)      1_555  .      1_555  N
  O5        O12       O5                119.1(7)      2_646  .     -1_666  N
  O5        O12       O11                79.1(4)      2_646  .      2_646  N
  O5        O12       O11               126.7(6)      2_646  .     -1_666  N
  O5        O12       O13               101.6(5)      2_646  .      1_455  N
  O5        O12       O13                76.9(4)      2_646  .      1_555  N
  O5        O12       O11               126.7(6)     -1_666  .      2_646  N
  O5        O12       O11                79.1(4)     -1_666  .     -1_666  N
  O5        O12       O13               101.6(5)     -1_666  .      1_455  N
  O5        O12       O13                76.9(4)     -1_666  .      1_555  N
  O11       O12       O11                54.4(6)      2_646  .     -1_666  N
  O11       O12       O13               124.7(6)      2_646  .      1_455  N
  O11       O12       O13                58.0(5)      2_646  .      1_555  N
  O11       O12       O13               124.7(6)     -1_666  .      1_455  N
  O11       O12       O13                58.0(5)     -1_666  .      1_555  N
  O13       O12       O13              176.8(10)      1_455  .      1_555  N
  Lu1       O13       Lu1               103.1(7)      2_746  .     -1_766  N
  Lu1       O13       Ba1               102.5(5)      2_746  .      1_556  N
  Lu1       O13       Ge4               124.3(4)      2_746  .      1_555  N
  Lu1       O13       O8               49.81(35)      2_746  .      2_747  N
  Lu1       O13       O8                100.2(6)      2_746  .     -1_767  N
  Lu1       O13       O11                89.4(4)      2_746  .      2_646  N
  Lu1       O13       O11               137.5(7)      2_746  .     -1_666  N
  Lu1       O13       O12             127.78(34)      2_746  .      1_555  N
  Lu1       O13       O12              52.72(34)      2_746  .      1_655  N
  Lu1       O13       Ba1               102.5(5)     -1_766  .      1_556  N
  Lu1       O13       Ge4               124.3(4)     -1_766  .      1_555  N
  Lu1       O13       O8                100.2(6)     -1_766  .      2_747  N
  Lu1       O13       O8               49.81(35)     -1_766  .     -1_767  N
  Lu1       O13       O11               137.5(7)     -1_766  .      2_646  N
  Lu1       O13       O11                89.4(4)     -1_766  .     -1_666  N
  Lu1       O13       O12             127.78(34)     -1_766  .      1_555  N
  Lu1       O13       O12              52.72(34)     -1_766  .      1_655  N
  Ba1       O13       Ge4                94.7(6)      1_556  .      1_555  N
  Ba1       O13       O8               54.21(35)      1_556  .      2_747  N
  Ba1       O13       O8               54.21(35)      1_556  .     -1_767  N
  Ba1       O13       O11               114.4(5)      1_556  .      2_646  N
  Ba1       O13       O11               114.4(5)      1_556  .     -1_666  N
  Ba1       O13       O12                59.6(4)      1_556  .      1_555  N
  Ba1       O13       O12               123.6(7)      1_556  .      1_655  N
  Ge4       O13       O8                131.6(6)      1_555  .      2_747  N
  Ge4       O13       O8                131.6(6)      1_555  .     -1_767  N
  Ge4       O13       O11                36.2(4)      1_555  .      2_646  N
  Ge4       O13       O11                36.2(4)      1_555  .     -1_666  N
  Ge4       O13       O12                35.1(5)      1_555  .      1_555  N
  Ge4       O13       O12               141.7(9)      1_555  .      1_655  N
  O8        O13       O8                 63.4(6)      2_747  .     -1_767  N
  O8        O13       O11               118.0(4)      2_747  .      2_646  N
  O8        O13       O11               166.3(7)      2_747  .     -1_666  N
  O8        O13       O12               103.7(6)      2_747  .      1_555  N
  O8        O13       O12                79.0(6)      2_747  .      1_655  N
  O8        O13       O11               166.3(7)     -1_767  .      2_646  N
  O8        O13       O11               118.0(4)     -1_767  .     -1_666  N
  O8        O13       O12               103.7(6)     -1_767  .      1_555  N
  O8        O13       O12                79.0(6)     -1_767  .      1_655  N
  O11       O13       O11                57.1(6)      2_646  .     -1_666  N
  O11       O13       O12                62.6(5)      2_646  .      1_555  N
  O11       O13       O12               114.7(6)      2_646  .      1_655  N
  O11       O13       O12                62.6(5)     -1_666  .      1_555  N
  O11       O13       O12               114.7(6)     -1_666  .      1_655  N
  O12       O13       O12              176.8(10)      1_555  .      1_655  N

# Powder diffraction data for histogram  1
#==============================================================================
# 9. INSTRUMENT CHARACTERIZATION

_exptl_special_details
; ?
;

# if regions of the data are excluded, the reason(s) are supplied here:
_pd_proc_info_excluded_regions
; ?
;

# The following item is used to identify the equipment used to record
# the powder pattern when the diffractogram was measured at a laboratory
# other than the authors' home institution, e.g. when neutron or synchrotron
# radiation is used.

_pd_instr_location
; ?
;
_pd_calibration_special_details           # description of the method used
                                          # to calibrate the instrument
"external Si standard"

_diffrn_ambient_temperature       298
_diffrn_source                    "sealed X-ray tube"
_diffrn_source_target             Cu
_diffrn_source_type               "PHILIPS PW 2283/20"
_diffrn_measurement_device_type   "transmission diffractometer Stadi-P (STOE)"
_diffrn_detector                  "position sensitive detector"
_diffrn_detector_type             "linear mini-PSD (STOE)"
       # make or model of detector

_pd_meas_scan_method              step       # options are 'step', 'cont',
                                          # 'tof', 'fixed' or
                                          # 'disp' (= dispersive)
_pd_meas_special_details
;  ?
;

# The following two items identify the program(s) used (if appropriate).
_computing_data_collection
"STOE Powder Software Package (STOE, Germany)"
_computing_data_reduction
"STOE Powder Software Package (STOE, Germany)"

# Describe any processing performed on the data, prior to refinement.
# For example: a manual Lp correction or a precomputed absorption correction
_pd_proc_info_data_reduction      ?

# The following item is used for angular dispersive measurements only.

_diffrn_radiation_monochromator   "Primary, curved Ge 111"

# The following items are used to define the size of the instrument.
# Not all distances are appropriate for all instrument types.

_pd_instr_dist_src/mono           260
_pd_instr_dist_mono/spec          130
_pd_instr_dist_src/spec           ?
_pd_instr_dist_spec/anal          ?
_pd_instr_dist_anal/detc          ?
_pd_instr_dist_spec/detc          220

# 10. Specimen size and mounting information

# The next three fields give the specimen dimensions in mm.  The equatorial
# plane contains the incident and diffracted beam.

_pd_spec_size_axial               7       # perpendicular to
                                          # equatorial plane

_pd_spec_size_equat               0.1       # parallel to
                                          # scattering vector
                                          # in transmission

_pd_spec_size_thick               ?       # parallel to
                                          # scattering vector
                                          # in reflection

_pd_spec_mounting                         # This field should be
                                          # used to give details of the
                                          # container.
"powder on Mylar film"

_pd_spec_mount_mode               transmission       # options are 'reflection'
                                          # or 'transmission'

_pd_spec_shape                    flat_sheet       # options are 'cylinder'
                                          # 'flat_sheet' or 'irregular'







loop_ _atom_type_symbol
      _atom_type_number_in_cell
      _atom_type_scat_dispersion_real
      _atom_type_scat_dispersion_imag
      _atom_type_scat_Cromer_Mann_a1
      _atom_type_scat_Cromer_Mann_a2
      _atom_type_scat_Cromer_Mann_a3
      _atom_type_scat_Cromer_Mann_a4
      _atom_type_scat_Cromer_Mann_b1
      _atom_type_scat_Cromer_Mann_b2
      _atom_type_scat_Cromer_Mann_b3
      _atom_type_scat_Cromer_Mann_b4
      _atom_type_scat_Cromer_Mann_c
      _atom_type_scat_source
  Lu        12.0    0.000    0.000
 28.9476 1.90182 15.2208 9.98519 15.1000 0.26103 3.71601 84.3298 7.97628 
  International_Tables_Vol_C
  Ba         2.0    0.000    0.000
 20.3361 3.21600 19.2970 0.27560 10.8880 20.2073 2.69590 167.202 2.77310 
  International_Tables_Vol_C
  Ge        14.0    0.000    0.000
 16.0816 2.85090 6.37470 0.25160 3.70680 11.4468 3.68300 54.7625 2.13130 
  International_Tables_Vol_C
  O         48.0    0.000    0.000
 3.04850 13.2771 2.28680 5.70110 1.54630 0.32390 0.86700 32.9089 0.25080 
  International_Tables_Vol_C
_diffrn_radiation_probe                x-ray
_diffrn_radiation_polarisn_ratio       0.8
_diffrn_radiation_wavelength           1.54056
_diffrn_radiation_type                 'Cu K\a~1~'
_pd_proc_ls_prof_R_factor              0.0275
_pd_proc_ls_prof_wR_factor             0.0399
_pd_proc_ls_prof_wR_expected           0.0197
_refine_ls_R_Fsqd_factor               0.01962

_pd_proc_ls_background_function
;   GSAS Background function number 1 with 36 terms.
 Shifted Chebyshev function of 1st kind
      1:    1454.33     2:   -1671.99     3:    949.638     4:   -513.868    
      5:    175.992     6:   -31.5241     7:   -25.2923     8:    39.3038    
      9:   -22.4416    10:    1.06988    11:   -22.6221    12:    20.7618    
     13:    13.9871    14:   -10.0807    15:   -8.97806    16:    23.0774    
     17:   -22.3635    18:    8.47021    19:    1.88614    20:   -6.49599    
     21:    4.66845    22:   -3.90024    23:   -4.08751    24:    10.1656    
     25:   -2.05495    26:  -0.744074    27:    2.85984    28:   3.354650E-02
     29:   -4.55771    30:    10.1967    31:   -3.33416    32:   -5.89015    
     33:    8.05196    34:   -6.93768    35:    2.02599    36:    1.41774    
;

_exptl_absorpt_process_details
;   GSAS Absorption/surface roughness correction: function number 4
 Flat plate transmission absorption correction
Terms =     0.12128         0.0000    
Correction is not refined.
;
_exptl_absorpt_correction_T_min        0.0
_exptl_absorpt_correction_T_max        1.0
# Extinction correction
_gsas_exptl_extinct_corr_T_min         1.00000
_gsas_exptl_extinct_corr_T_max         1.00000

_pd_proc_ls_profile_function
;
 CW Profile function number 4 with  21 terms
 Pseudovoigt profile coefficients as parameterized in
 P. Thompson, D.E. Cox & J.B. Hastings (1987). J. Appl. Cryst.,20,79-83.
 Asymmetry correction of L.W. Finger, D.E. Cox & A. P. Jephcoat (1994).
 J. Appl. Cryst.,27,892-900.
 Microstrain broadening by P.W. Stephens,  (1999). J. Appl. Cryst.,32,281-289.
 #1(GU)   =   39.756 #2(GV)   =    0.000 #3(GW)   =   16.426
 #4(GP)   =    0.000 #5(LX)   =    3.562 #6(ptec) =    -0.59
 #7(trns) =     0.00 #8(shft) =   0.0000 #9(sfec) =     0.00
 #10(S/L) =   0.0215 #11(H/L) =   0.0219 #12(eta) =   1.0000
 #13(S400 ) =  3.9E-04 #14(S040 ) =  1.4E-04 #15(S004 ) =  0.0E+00
 #16(S220 ) = -9.1E-04 #17(S202 ) =  1.3E-02 #18(S022 ) =  8.9E-04
 #19(S301 ) =  2.9E-03 #20(S103 ) =  1.8E-02 #21(S121 ) = -1.4E-03
 Peak tails are ignored  where the intensity is below 0.0010 times the peak
   Aniso. broadening axis   0.0   1.0   0.0
;
_pd_proc_ls_peak_cutoff 0.00100
_pd_proc_info_datetime                 2023-01-23T14:03:02
_pd_calc_method                        "Rietveld Refinement"

#---- raw/calc data loop -----
_pd_meas_2theta_range_min              5.0
_pd_meas_2theta_range_max              119.98
_pd_meas_2theta_range_inc              0.02
_pd_proc_2theta_range_min              4.97143
_pd_proc_2theta_range_max              119.95143
_pd_proc_2theta_range_inc              0.02

loop_
      _pd_meas_counts_total
      _pd_proc_ls_weight
      _pd_proc_intensity_bkg_calc
      _pd_calc_intensity_total
  4547.0      0.0001100   4634.64160   4636.57861
  4615.0      0.0001083   4634.59766   4636.59766
  4672.0      0.0001070   4634.75977   4636.82666
  4627.0      0.0001081   4635.09912   4637.23584
  4638.0      0.0001078   4635.58838   4637.79932
  4599.0      0.0001087   4636.20166   4638.49072
  4642.0      0.0001077   4636.91504   4639.28613
  4675.0      0.0001070   4637.70703   4640.16455
  4795.0      0.0001043   4638.55566   4641.10547
  4583.0      0.0001091   4639.44336   4642.09033
  4686.0      0.0001067   4640.35059   4643.10059
  4625.0      0.0001081   4641.26172   4644.12061
  4673.0      0.0001070   4642.16162   4645.13672
  4613.0      0.0001084   4643.03564   4646.13379
  4696.0      0.0001065   4643.87158   4647.10059
  4707.0      0.0001062   4644.65674   4648.02637
  4561.0      0.0001096   4645.38135   4648.89990
  4627.0      0.0001081   4646.03467   4649.71338
  4717.0      0.0001060   4646.60889   4650.45898
  4629.0      0.0001080   4647.09521   4651.12842
  4485.0      0.0001115   4647.48682   4651.71826
  4576.0      0.0001093   4647.77783   4652.22119
  4740.0      0.0001055   4647.96143   4652.63525
  4709.0      0.0001062   4648.03418   4652.95654
  4740.0      0.0001055   4647.99072   4653.18311
  4684.0      0.0001067   4647.82764   4653.31348
  4639.0      0.0001078   4647.54297   4653.34912
  4600.0      0.0001087   4647.13281   4653.29053
  4739.0      0.0001055   4646.59619   4653.13916
  4631.0      0.0001080   4645.93115   4652.89893
  4702.0      0.0001063   4645.13672   4652.57520
  4709.0      0.0001062   4644.21289   4652.17529
  4790.0      0.0001044   4643.15869   4651.70654
  4564.0      0.0001096   4641.97510   4651.18262
  4721.0      0.0001059   4640.66211   4650.61768
  4681.0      0.0001068   4639.22070   4650.03564
  4681.0      0.0001068   4637.65186   4649.47168
  4502.0      0.0001111   4635.95703   4648.99414
  4687.0      0.0001067   4634.13818   4648.73535
  4671.0      0.0001070   4632.19727   4648.93750
  4663.0      0.0001072   4630.13574   4650.00830
  4607.0      0.0001085   4627.95654   4652.52881
  4662.0      0.0001073   4625.66162   4657.19043
  4629.0      0.0001080   4623.25391   4664.61914
  4574.0      0.0001093   4620.73584   4675.16016
  4689.0      0.0001066   4618.11084   4688.80811
  4746.0      0.0001054   4615.38135   4705.29395
  4632.0      0.0001079   4612.55078   4724.31104
  4768.0      0.0001049   4609.62158   4745.65723
  4887.0      0.0001023   4606.59766   4769.29492
  4834.0      0.0001034   4603.48242   4795.35986
  4750.0      0.0001053   4600.27881   4824.11816
  4719.0      0.0001060   4596.99023   4855.95947
  4840.0      0.0001033   4593.61963   4891.39990
  4929.0      0.0001014   4590.17090   4931.09766
  5051.0      0.0000990   4586.64746   4975.91113
  5046.0      0.0000991   4583.05225   5026.98779
  4999.0      0.0001000   4579.38965   5085.90527
  5076.0      0.0000985   4575.66162   5154.95801
  5331.0      0.0000938   4571.87256   5237.65332
  5321.0      0.0000940   4568.02490   5339.46924
  5419.0      0.0000923   4564.12305   5468.49756
  5525.0      0.0000905   4560.16943   5634.50000
  5874.0      0.0000851   4556.16699   5843.70361
  5866.0      0.0000852   4552.11963   6087.54150
  6309.0      0.0000793   4548.02979   6329.06006
  6335.0      0.0000789   4543.90088   6497.94678
  6379.0      0.0000784   4539.73584   6506.59766
  6299.0      0.0000794   4535.53711   6299.07764
  6104.0      0.0000819   4531.30811   5919.97607
  5597.0      0.0000893   4527.05127   5496.67285
  5239.0      0.0000954   4522.76953   5135.91064
  4864.0      0.0001028   4518.46533   4880.83789
  4670.0      0.0001071   4514.14063   4725.12793
  4807.0      0.0001040   4509.79883   4639.52441
  4638.0      0.0001078   4505.44189   4594.01025
  4556.0      0.0001097   4501.07227   4568.07471
  4464.0      0.0001120   4496.69141   4550.91162
  4599.0      0.0001087   4492.30225   4537.79004
  4541.0      0.0001101   4487.90723   4526.82715
  4556.0      0.0001097   4483.50684   4517.24023
  4529.0      0.0001104   4479.10449   4508.63818
  4428.0      0.0001129   4474.70068   4500.77979
  4564.0      0.0001096   4470.29834   4493.50049
  4465.0      0.0001120   4465.89844   4486.67822
  4461.0      0.0001121   4461.50195   4480.22363
  4503.0      0.0001110   4457.11182   4474.06885
  4449.0      0.0001124   4452.72803   4468.16113
  4498.0      0.0001112   4448.35254   4462.45996
  4517.0      0.0001107   4443.98682   4456.93359
  4409.0      0.0001134   4439.63135   4451.55566
  4409.0      0.0001134   4435.28760   4446.30811
  4407.0      0.0001135   4430.95654   4441.17285
  4370.0      0.0001144   4426.63965   4436.13623
  4472.0      0.0001118   4422.33643   4431.18848
  4519.0      0.0001106   4418.04932   4426.32031
  4354.0      0.0001148   4413.77734   4421.52295
  4445.0      0.0001125   4409.52197   4416.79150
  4365.0      0.0001145   4405.28467   4412.12012
  4454.0      0.0001123   4401.06396   4407.50439
  4444.0      0.0001125   4396.86230   4402.94043
  4488.0      0.0001114   4392.67871   4398.42480
  4462.0      0.0001121   4388.51416   4393.95508
  4275.0      0.0001170   4384.36865   4389.52783
  4452.0      0.0001123   4380.24219   4385.14111
  4378.0      0.0001142   4376.13574   4380.79395
  4336.0      0.0001153   4372.04883   4376.48389
  4264.0      0.0001173   4367.98145   4372.20850
  4321.0      0.0001157   4363.93359   4367.96729
  4513.0      0.0001108   4359.90576   4363.75879
  4517.0      0.0001107   4355.89697   4359.58203
  4500.0      0.0001111   4351.90771   4355.43555
  4339.0      0.0001152   4347.93799   4351.31787
  4280.0      0.0001168   4343.98682   4347.22803
  4364.0      0.0001146   4340.05469   4343.16553
  4367.0      0.0001145   4336.14111   4339.12988
  4240.0      0.0001179   4332.24512   4335.11865
  4319.0      0.0001158   4328.36768   4331.13232
  4236.0      0.0001180   4324.50732   4327.16895
  4259.0      0.0001174   4320.66357   4323.22852
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  6649.0      0.0000752   2112.11450   6387.95654
  5140.0      0.0000973   2109.64697   5273.91260
  4307.0      0.0001161   2107.17871   4479.03564
  3793.0      0.0001318   2104.71045   3998.91626
  3543.0      0.0001411   2102.24194   3717.53833
  3342.0      0.0001496   2099.77368   3493.17456
  3199.0      0.0001563   2097.30469   3240.00830
  2931.0      0.0001706   2094.83569   2962.89966
  2669.0      0.0001873   2092.36646   2708.49512
  2523.0      0.0001982   2089.89746   2510.19385
  2391.0      0.0002091   2087.42822   2375.17749
  2320.0      0.0002155   2084.95874   2291.86914
  2319.0      0.0002156   2082.48901   2242.40430
  2170.0      0.0002304   2080.01929   2211.76050
  2226.0      0.0002246   2077.54980   2190.66284
  2236.0      0.0002236   2075.08008   2174.45850
  2173.0      0.0002301   2072.61011   2161.07837
  2109.0      0.0002371   2070.14014   2149.60034
  2049.0      0.0002440   2067.67065   2139.54688
  2125.0      0.0002353   2065.20068   2130.61743
  2089.0      0.0002393   2062.73096   2122.59937
  2064.0      0.0002422   2060.26123   2115.32959
  2148.0      0.0002328   2057.79175   2108.68262
  2080.0      0.0002404   2055.32227   2102.55859
  2092.0      0.0002390   2052.85278   2096.87866
  2008.0      0.0002490   2050.38379   2091.57886
  2029.0      0.0002464   2047.91504   2086.60718
  2108.0      0.0002372   2045.44653   2081.92090
  2075.0      0.0002410   2042.97803   2077.48584
  2094.0      0.0002388   2040.51001   2073.27197
  2118.0      0.0002361   2038.04260   2069.25757
  1993.0      0.0002509   2035.57532   2065.42163
  2027.0      0.0002467   2033.10864   2061.74927
  2118.0      0.0002361   2030.64233   2058.22681
  1927.0      0.0002595   2028.17676   2054.84473
  1956.0      0.0002556   2025.71155   2051.59473
  1977.0      0.0002529   2023.24695   2048.47192
  2042.0      0.0002449   2020.78320   2045.47339
  2037.0      0.0002455   2018.32007   2042.59741
  2042.0      0.0002449   2015.85791   2039.84595
  2117.0      0.0002362   2013.39636   2037.22217
  2061.0      0.0002426   2010.93567   2034.73364
  1973.0      0.0002534   2008.47607   2032.38989
  1972.0      0.0002535   2006.01733   2030.20544
  2002.0      0.0002498   2003.55981   2028.19922
  1990.0      0.0002513   2001.10315   2026.39722
  1988.0      0.0002515   1998.64771   2024.83337
  1967.0      0.0002542   1996.19373   2023.55383
  1983.0      0.0002521   1993.74072   2022.61963
  2037.0      0.0002455   1991.28918   2021.84937
  2027.0      0.0002467   1988.83899   2021.91760
  2022.0      0.0002473   1986.39050   2022.76782
  1989.0      0.0002514   1983.94324   2024.80920
  2015.0      0.0002481   1981.49756   2029.48083
  1995.0      0.0002506   1979.05371   2037.13330
  2055.0      0.0002433   1976.61145   2051.29590
  2091.0      0.0002391   1974.17114   2077.20264
  2132.0      0.0002345   1971.73254   2121.95898
  2231.0      0.0002241   1969.29578   2196.06152
  2316.0      0.0002159   1966.86145   2310.44824
  2521.0      0.0001983   1964.42883   2472.15747
  2777.0      0.0001801   1961.99854   2677.35132
  2922.0      0.0001711   1959.57019   2902.88257
  3136.0      0.0001594   1957.14429   3103.24414
  3312.0      0.0001510   1954.72095   3216.49707
  3292.0      0.0001519   1952.29980   3187.70190
  3147.0      0.0001589   1949.88135   3008.10791
  2757.0      0.0001814   1947.46533   2755.71362
  2492.0      0.0002006   1945.05225   2504.02026
  2300.0      0.0002174   1942.64172   2300.71509
  2173.0      0.0002301   1940.23389   2159.53955
  2047.0      0.0002443   1937.82922   2072.47949
  2060.0      0.0002427   1935.42749   2022.92334
  1989.0      0.0002514   1933.02893   1995.24744
  1964.0      0.0002546   1930.63342   1978.81738
  1981.0      0.0002524   1928.24097   1967.80835
  1967.0      0.0002542   1925.85229   1959.48596
  1961.0      0.0002550   1923.46655   1952.66528
  1924.0      0.0002599   1921.08472   1946.81860
  1903.0      0.0002627   1918.70618   1941.67432
  1922.0      0.0002601   1916.33154   1937.06738
  1929.0      0.0002592   1913.96033   1932.88342
  1898.0      0.0002634   1911.59302   1929.04138
  1851.0      0.0002701   1909.22986   1925.48047
  1993.0      0.0002509   1906.87073   1922.15637
  1936.0      0.0002583   1904.51538   1919.03491
  1926.0      0.0002596   1902.16431   1916.09229
  1918.0      0.0002607   1899.81750   1913.31177
  1801.0      0.0002776   1897.47510   1910.68201
  1854.0      0.0002697   1895.13721   1908.19800
  1870.0      0.0002674   1892.80383   1905.85901
  1932.0      0.0002588   1890.47498   1903.66956
  1847.0      0.0002707   1888.15076   1901.64136
  1950.0      0.0002564   1885.83167   1899.89392
  1945.0      0.0002571   1883.51721   1898.25464
  1950.0      0.0002564   1881.20776   1898.51465
  1947.0      0.0002568   1878.90332   1897.48926
  1870.0      0.0002674   1876.60437   1896.90430
  1938.0      0.0002580   1874.31030   1897.00488
  1954.0      0.0002559   1872.02148   1898.30518
  1947.0      0.0002568   1869.73840   1901.85559
  1986.0      0.0002518   1867.46094   1909.64392
  2040.0      0.0002451   1865.18872   1925.08313
  2004.0      0.0002495   1862.92212   1954.40979
  2099.0      0.0002382   1860.66150   2002.35339
  2074.0      0.0002411   1858.40686   2076.41797
  2151.0      0.0002325   1856.15820   2179.12988
  2276.0      0.0002197   1853.91541   2303.71533
  2472.0      0.0002023   1851.67871   2429.44873
  2299.0      0.0002175   1849.44849   2522.62378
  2439.0      0.0002050   1847.22424   2545.78223
  2410.0      0.0002075   1845.00647   2480.51294
  2219.0      0.0002253   1842.79541   2350.21338
  2128.0      0.0002350   1840.59082   2203.27588
  2025.0      0.0002469   1838.39307   2077.22974
  1954.0      0.0002559   1836.20178   1987.92297
  1892.0      0.0002643   1834.01733   1934.76160
  1900.0      0.0002632   1831.84009   1909.52295
  1939.0      0.0002579   1829.66980   1903.92773
  1913.0      0.0002614   1827.50647   1913.30847
  1935.0      0.0002584   1825.35022   1936.46301
  1935.0      0.0002584   1823.20129   1973.28979
  2035.0      0.0002457   1821.05994   2021.95728
  2113.0      0.0002366   1818.92603   2076.39551
  2087.0      0.0002396   1816.79944   2124.78906
  2142.0      0.0002334   1814.68030   2151.58203
  2145.0      0.0002331   1812.56934   2143.02197
  2098.0      0.0002383   1810.46570   2098.30420
  2063.0      0.0002424   1808.37024   2033.62109
  1954.0      0.0002559   1806.28235   1968.64453
  1928.0      0.0002593   1804.20288   1915.30103
  1884.0      0.0002654   1802.13123   1877.27075
  1829.0      0.0002734   1800.06775   1852.90063
  1840.0      0.0002717   1798.01245   1838.28845
  1911.0      0.0002616   1795.96582   1828.65088
  1873.0      0.0002670   1793.92749   1824.66016
  1808.0      0.0002765   1791.89734   1820.87378
  1787.0      0.0002798   1789.87585   1817.98108
  1827.0      0.0002737   1787.86304   1815.65198
  1842.0      0.0002714   1785.85901   1813.74646
  1738.0      0.0002877   1783.86377   1812.20349
  1775.0      0.0002817   1781.87720   1810.99744
  1754.0      0.0002851   1779.89954   1810.12415
  1818.0      0.0002750   1777.93115   1809.59473
  1785.0      0.0002801   1775.97156   1809.43445
  1774.0      0.0002818   1774.02124   1809.68518
  1826.0      0.0002738   1772.07996   1810.40540
  1736.0      0.0002880   1770.14832   1811.67786
  1891.0      0.0002644   1768.22559   1813.61426
  1893.0      0.0002641   1766.31226   1816.37219
  1815.0      0.0002755   1764.40869   1820.18677
  1852.0      0.0002700   1762.51440   1825.43701
  1890.0      0.0002646   1760.62976   1832.79736
  1852.0      0.0002700   1758.75476   1843.54236
  1856.0      0.0002694   1756.88928   1860.11230
  1959.0      0.0002552   1755.03394   1887.01184
  1963.0      0.0002547   1753.18811   1931.99219
  2038.0      0.0002453   1751.35229   2007.14258
  2215.0      0.0002257   1749.52637   2133.00781
  2470.0      0.0002024   1747.71057   2320.36060
  2611.0      0.0001915   1745.90466   2586.67065
  2957.0      0.0001691   1744.10876   2928.85571
  3296.0      0.0001517   1742.32312   3316.35889
  3569.0      0.0001401   1740.54761   3683.91797
  3808.0      0.0001313   1738.78259   3941.59009
  4065.0      0.0001230   1737.02759   4003.69629
  3737.0      0.0001338   1735.28296   3845.45776
  3397.0      0.0001472   1733.54883   3556.44434
  3154.0      0.0001585   1731.82507   3283.24829
  3101.0      0.0001612   1730.11182   3124.47363
  3131.0      0.0001597   1728.40906   3104.02710
  3187.0      0.0001569   1726.71667   3177.67285
  3357.0      0.0001489   1725.03528   3256.29468
  3298.0      0.0001516   1723.36414   3242.85278
  3101.0      0.0001612   1721.70398   3084.00708
  2911.0      0.0001718   1720.05432   2814.09229
  2613.0      0.0001914   1718.41553   2517.72363
  2288.0      0.0002185   1716.78735   2261.12842
  2055.0      0.0002433   1715.17004   2072.33350
  1979.0      0.0002527   1713.56372   1950.13184
  1879.0      0.0002661   1711.96814   1878.31531
  1851.0      0.0002701   1710.38354   1838.16626
  1886.0      0.0002651   1708.80969   1815.37256
  1764.0      0.0002834   1707.24683   1801.39465
  1784.0      0.0002803   1705.69507   1791.97009
  1867.0      0.0002678   1704.15405   1785.20630
  1887.0      0.0002650   1702.62439   1795.17200
  1876.0      0.0002665   1701.10547   1792.19983
  1807.0      0.0002767   1699.59766   1790.58777
  1809.0      0.0002764   1698.10120   1790.29529
  1874.0      0.0002668   1696.61548   1791.38196
  1800.0      0.0002778   1695.14111   1794.04480
  1743.0      0.0002869   1693.67773   1799.93945
  1833.0      0.0002728   1692.22559   1807.65649
  1829.0      0.0002734   1690.78442   1820.44556
  1842.0      0.0002714   1689.35437   1842.22778
  1802.0      0.0002775   1687.93567   1881.28210
  1939.0      0.0002579   1686.52795   1950.21277
  2032.0      0.0002461   1685.13159   2067.58423
  2267.0      0.0002206   1683.74622   2254.88770
  2549.0      0.0001962   1682.37195   2527.56738
  2827.0      0.0001769   1681.00916   2880.68823
  3194.0      0.0001565   1679.65723   3274.74463
  3433.0      0.0001456   1678.31665   3627.37964
  3763.0      0.0001329   1676.98718   3828.47046
  3830.0      0.0001305   1675.66895   3784.64136
  3472.0      0.0001440   1674.36169   3497.04834
  3173.0      0.0001576   1673.06555   3081.50146
  2672.0      0.0001871   1671.78076   2671.49487
  2399.0      0.0002084   1670.50720   2345.35596
  2204.0      0.0002269   1669.24438   2125.09180
  2084.0      0.0002399   1667.99280   1996.34570
  2010.0      0.0002488   1666.75220   1930.99622
  1904.0      0.0002626   1665.52295   1903.34998
  2072.0      0.0002413   1664.30469   1896.67859
  2010.0      0.0002488   1663.09729   1902.94397
  2046.0      0.0002444   1661.90088   1920.56445
  2071.0      0.0002414   1660.71545   1953.46228
  2095.0      0.0002387   1659.54126   2012.53870
  2182.0      0.0002291   1658.37769   2119.37549
  2389.0      0.0002093   1657.22522   2310.80005
  2713.0      0.0001843   1656.08362   2640.79150
  3331.0      0.0001501   1654.95288   3172.69824
  4034.0      0.0001239   1653.83289   3952.84253
  5126.0      0.0000975   1652.72363   4967.19727
  6107.0      0.0000819   1651.62524   6098.77930
  6996.0      0.0000715   1650.53772   7104.98438
  7449.0      0.0000671   1649.46069   7664.35449
  7429.0      0.0000673   1648.39417   7512.71387
  6642.0      0.0000753   1647.33838   6669.10645
  5616.0      0.0000890   1646.29333   5477.55225
  4436.0      0.0001127   1645.25879   4320.04248
  3430.0      0.0001458   1644.23462   3417.76245
  2828.0      0.0001768   1643.22083   2828.08105
  2585.0      0.0001934   1642.21765   2502.04297
  2456.0      0.0002036   1641.22461   2355.69360
  2354.0      0.0002124   1640.24207   2317.19116
  2292.0      0.0002182   1639.26965   2304.12769
  2314.0      0.0002161   1638.30737   2292.57544
  2226.0      0.0002246   1637.35547   2270.28760
  2242.0      0.0002230   1636.41345   2244.03687
  2133.0      0.0002344   1635.48145   2227.53247
  2214.0      0.0002258   1634.55969   2230.52979
  2173.0      0.0002301   1633.64783   2262.60181
  2305.0      0.0002169   1632.74561   2331.27808
  2381.0      0.0002100   1631.85327   2454.04028
  2667.0      0.0001875   1630.97070   2670.03516
  3173.0      0.0001576   1630.09790   3056.16650
  3822.0      0.0001308   1629.23486   3748.54614
  5026.0      0.0000995   1628.38123   4950.66162
  7007.0      0.0000714   1627.53699   6907.55762
  9673.0      0.0000517   1626.70239   9809.06348
  13532.0     0.0000369   1625.87695   13622.33594
  17614.0     0.0000284   1625.06091   17925.19922
  21318.0     0.0000235   1624.25415   21818.42969
  23796.0     0.0000210   1623.45642   24088.71680
  23658.0     0.0000211   1622.66785   23720.29883
  21268.0     0.0000235   1621.88818   20744.45313
  17229.0     0.0000290   1621.11743   16433.79688
  12746.0     0.0000392   1620.35571   12208.92090
  9097.0      0.0000550   1619.60278   8883.32324
  6680.0      0.0000749   1618.85852   6621.31592
  5032.0      0.0000994   1618.12268   5191.24463
  4036.0      0.0001239   1617.39551   4259.74414
  3412.0      0.0001465   1616.67688   3599.50024
  2967.0      0.0001685   1615.96667   3107.76782
  2551.0      0.0001960   1615.26465   2743.08862
  2278.0      0.0002195   1614.57080   2509.31104
  2080.0      0.0002404   1613.88513   2333.89331
  2054.0      0.0002434   1613.20752   2220.18823
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  1912.0      0.0002615   1611.87598   2104.98462
  2022.0      0.0002473   1611.22205   2081.51563
  1942.0      0.0002575   1610.57568   2074.09912
  1970.0      0.0002538   1609.93689   2078.55200
  1993.0      0.0002509   1609.30579   2094.30884
  2013.0      0.0002484   1608.68176   2114.58179
  1984.0      0.0002520   1608.06543   2132.03345
  2102.0      0.0002379   1607.45605   2139.81299
  2059.0      0.0002428   1606.85388   2136.77271
  2035.0      0.0002457   1606.25879   2130.38452
  2014.0      0.0002483   1605.67065   2132.54346
  2141.0      0.0002335   1605.08936   2155.42407
  2193.0      0.0002280   1604.51477   2214.53540
  2252.0      0.0002220   1603.94678   2337.31982
  2575.0      0.0001942   1603.38538   2663.00537
  3043.0      0.0001643   1602.83032   3110.24707
  3974.0      0.0001258   1602.28186   3897.27246
  5286.0      0.0000946   1601.73950   5177.68359
  7068.0      0.0000707   1601.20337   7051.94141
  9485.0      0.0000527   1600.67310   9452.08301
  12083.0     0.0000414   1600.14880   12039.35840
  14187.0     0.0000352   1599.63049   14180.26172
  15146.0     0.0000330   1599.11768   15110.75293
  14746.0     0.0000339   1598.61072   14333.74805
  12567.0     0.0000398   1598.10913   12119.31641
  9802.0      0.0000510   1597.61292   9386.76172
  6987.0      0.0000716   1597.12207   6875.63184
  5126.0      0.0000975   1596.63635   5024.29688
  3897.0      0.0001283   1596.15588   3876.23804
  3263.0      0.0001532   1595.68030   3275.68286
  2985.0      0.0001675   1595.20959   3012.32886
  2893.0      0.0001728   1594.74365   2911.47144
  2800.0      0.0001786   1594.28223   2861.53809
  2698.0      0.0001853   1593.82556   2811.84546
  2626.0      0.0001904   1593.37305   2763.68481
  2531.0      0.0001976   1592.92517   2748.33179
  2519.0      0.0001985   1592.48132   2807.08081
  2630.0      0.0001901   1592.04150   2990.04956
  3019.0      0.0001656   1591.60571   3363.00122
  3769.0      0.0001327   1591.17383   3975.43970
  4789.0      0.0001044   1590.74585   4861.42969
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  7258.0      0.0000689   1589.90027   7104.76465
  8364.0      0.0000598   1589.48279   8040.86719
  8970.0      0.0000557   1589.06848   8494.15723
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  9051.0      0.0000552   1588.24951   8339.25293
  9533.0      0.0000524   1587.84448   8857.54102
  11163.0     0.0000448   1587.44226   10650.70801
  14235.0     0.0000351   1587.04272   14104.78125
  19093.0     0.0000262   1586.64600   19129.14453
  24595.0     0.0000203   1586.25159   24961.03711
  29315.0     0.0000171   1585.85974   30120.02930
  32031.0     0.0000156   1585.46997   32746.14648
  31660.0     0.0000158   1585.08240   31492.92188
  27278.0     0.0000183   1584.69702   26738.89844
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  15010.0     0.0000333   1583.93176   14722.19531
  10592.0     0.0000472   1583.55164   10457.78809
  8017.0      0.0000624   1583.17310   7810.72412
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  5590.0      0.0000894   1204.01514   5626.58740
  5564.0      0.0000899   1202.44055   5520.59814
  5749.0      0.0000870   1200.87036   5795.32568
  6152.0      0.0000813   1199.30481   6383.86377
  6684.0      0.0000748   1197.74341   7038.04346
  6965.0      0.0000718   1196.18640   7424.29395
  6970.0      0.0000717   1194.63391   7256.46777
  6421.0      0.0000779   1193.08606   6505.82813
  5442.0      0.0000919   1191.54285   5417.24072
  4339.0      0.0001152   1190.00427   4316.38184
  3298.0      0.0001516   1188.47046   3384.50806
  2693.0      0.0001857   1186.94153   2691.46533
  2242.0      0.0002230   1185.41736   2226.85571
  1876.0      0.0002665   1183.89819   1939.37524
  1766.0      0.0002831   1182.38379   1769.65100
  1662.0      0.0003008   1180.87439   1669.56177
  1661.0      0.0003010   1179.36987   1595.31165
  1645.0      0.0003040   1177.87073   1554.50671
  1587.0      0.0003151   1176.37646   1525.23608
  1645.0      0.0003040   1174.88782   1504.13025
  1638.0      0.0003053   1173.40405   1488.75317
  1670.0      0.0002994   1171.92542   1478.03943
  1836.0      0.0002723   1170.45227   1471.39966
  1950.0      0.0002564   1168.98438   1468.54260
  2010.0      0.0002488   1167.52197   1469.43896
  2113.0      0.0002366   1166.06506   1474.37830
  2059.0      0.0002428   1164.61340   1484.15442
  2015.0      0.0002481   1163.16736   1500.46863
  1902.0      0.0002629   1161.72705   1526.67566
  1857.0      0.0002693   1160.29211   1568.94067
  1749.0      0.0002859   1158.86292   1639.29358
  1841.0      0.0002716   1157.43921   1749.68262
  1970.0      0.0002538   1156.02136   1921.99744
  2189.0      0.0002284   1154.60901   2172.28687
  2561.0      0.0001952   1153.20264   2509.08081
  2846.0      0.0001757   1151.80200   2919.30078
  3459.0      0.0001446   1150.40747   3383.29224
  3869.0      0.0001292   1149.01855   3828.32666
  4126.0      0.0001212   1147.63538   4178.39063
  4285.0      0.0001167   1146.25842   4362.73438
  4260.0      0.0001174   1144.88721   4346.89404
  4130.0      0.0001211   1143.52209   4207.60889
  4012.0      0.0001246   1142.16296   4131.03516
  4119.0      0.0001214   1140.80981   4298.97314
  4516.0      0.0001107   1139.46313   4818.83936
  5507.0      0.0000908   1138.12219   5684.06006
  6708.0      0.0000745   1136.78735   6744.94482
  7462.0      0.0000670   1135.45874   7714.99707
  8149.0      0.0000614   1134.13623   8238.38184
  7997.0      0.0000625   1132.81995   8055.62305
  7338.0      0.0000681   1131.50989   7188.84619
  5973.0      0.0000837   1130.20605   5980.45703
  4535.0      0.0001103   1128.90857   4787.24072
  3521.0      0.0001420   1127.61731   3819.90869
  2961.0      0.0001689   1126.33252   3153.89307
  2728.0      0.0001833   1125.05371   2778.32983
  2515.0      0.0001988   1123.78137   2649.64282
  2710.0      0.0001845   1122.51538   2738.18359
  3026.0      0.0001652   1121.25574   3056.97705
  3564.0      0.0001403   1120.00256   3668.77148
  4428.0      0.0001129   1118.75574   4671.72607
  6187.0      0.0000808   1117.51550   6164.33350
  8088.0      0.0000618   1116.28149   8193.16406
  10542.0     0.0000474   1115.05396   10678.15723
  13162.0     0.0000380   1113.83289   13386.33984
  15844.0     0.0000316   1112.61816   15950.88086
  17884.0     0.0000280   1111.41003   17940.36328
  19393.0     0.0000258   1110.20825   19118.06641
  19429.0     0.0000257   1109.01318   19429.46680
  18657.0     0.0000268   1107.82471   18761.02148
  16876.0     0.0000296   1106.64246   17028.63867
  14856.0     0.0000337   1105.46667   14604.66016
  12538.0     0.0000399   1104.29761   12234.58301
  10799.0     0.0000463   1103.13489   10480.77539
  9694.0      0.0000516   1101.97876   9507.13770
  9172.0      0.0000545   1100.82910   9124.36035
  8838.0      0.0000566   1099.68604   8928.53809
  8569.0      0.0000583   1098.54956   8470.83203
  7626.0      0.0000656   1097.41968   7537.53369
  6359.0      0.0000786   1096.29639   6279.86182
  5048.0      0.0000990   1095.17932   4995.44727
  4033.0      0.0001240   1094.06897   3899.83203
  3021.0      0.0001655   1092.96509   3086.78638
  2442.0      0.0002048   1091.86780   2558.65649
  2232.0      0.0002240   1090.77698   2267.36548
  2006.0      0.0002493   1089.69275   2150.07568
  1961.0      0.0002550   1088.61511   2147.21313
  1987.0      0.0002516   1087.54382   2203.52319
  2029.0      0.0002464   1086.47913   2258.82495
  2094.0      0.0002388   1085.42090   2274.91626
  2021.0      0.0002474   1084.36914   2221.62256
  1985.0      0.0002519   1083.32385   2123.32959
  1940.0      0.0002577   1082.28516   2039.08582
  1981.0      0.0002524   1081.25281   2028.52405
  2035.0      0.0002457   1080.22717   2134.37451
  2298.0      0.0002176   1079.20776   2376.37207
  2738.0      0.0001826   1078.19495   2742.16528
  3114.0      0.0001606   1077.18835   3177.88867
  3483.0      0.0001436   1076.18823   3588.17432
  3790.0      0.0001319   1075.19458   3852.50415
  3802.0      0.0001315   1074.20740   3874.65234
  3673.0      0.0001361   1073.22644   3649.67383
  3253.0      0.0001537   1072.25183   3258.05249
  2835.0      0.0001764   1071.28369   2808.23047
  2440.0      0.0002049   1070.32190   2401.81836
  2122.0      0.0002356   1069.36621   2104.67261
  1962.0      0.0002548   1068.41699   1940.59827
  1800.0      0.0002778   1067.47388   1902.88062
  1985.0      0.0002519   1066.53723   1965.58301
  2109.0      0.0002371   1065.60669   2089.56152
  2259.0      0.0002213   1064.68237   2226.88965
  2294.0      0.0002180   1063.76440   2331.60205
  2379.0      0.0002102   1062.85254   2376.55273
  2417.0      0.0002069   1061.94666   2386.41992
  2437.0      0.0002052   1061.04712   2436.91699
  2636.0      0.0001897   1060.15356   2605.38110
  2892.0      0.0001729   1059.26611   2916.25757
  3383.0      0.0001478   1058.38464   3328.63306
  3763.0      0.0001329   1057.50940   3726.94897
  4019.0      0.0001244   1056.64014   3959.38892
  3906.0      0.0001280   1055.77686   3920.59399
  3624.0      0.0001380   1054.91956   3654.46118
  3401.0      0.0001470   1054.06799   3322.97559
  3064.0      0.0001632   1053.22253   3098.58447
  2956.0      0.0001691   1052.38293   3036.34912
  2972.0      0.0001682   1051.54907   3094.32568
  3027.0      0.0001652   1050.72107   3156.44507
  2962.0      0.0001688   1049.89893   3096.63696
  2732.0      0.0001830   1049.08276   2866.99731
  2374.0      0.0002106   1048.27209   2529.24097
  2020.0      0.0002475   1047.46716   2183.04517
  1725.0      0.0002899   1046.66785   1899.12793
  1714.0      0.0002917   1045.87415   1705.65088
  1560.0      0.0003205   1045.08618   1597.80701
  1517.0      0.0003296   1044.30371   1554.15930
  1506.0      0.0003320   1043.52698   1551.56262
  1593.0      0.0003139   1042.75562   1573.96265
  1619.0      0.0003088   1041.98975   1616.12976
  1714.0      0.0002917   1041.22937   1685.74231
  1802.0      0.0002775   1040.47437   1804.71582
  2095.0      0.0002387   1039.72461   2011.79102
  2470.0      0.0002024   1038.98035   2365.59619
  3125.0      0.0001600   1038.24133   2941.25659
  4071.0      0.0001228   1037.50757   3812.62598
  5191.0      0.0000963   1036.77930   5015.98975
  6534.0      0.0000765   1036.05603   6498.72900
  8097.0      0.0000618   1035.33789   8068.95508
  9320.0      0.0000536   1034.62488   9388.79297
  9950.0      0.0000503   1033.91699   10037.19141
  9540.0      0.0000524   1033.21411   9788.40137
  8517.0      0.0000587   1032.51636   8755.16113
  7194.0      0.0000695   1031.82336   7408.90869
  6149.0      0.0000813   1031.13550   6205.44189
  5334.0      0.0000937   1030.45264   5421.32813
  4974.0      0.0001005   1029.77441   5164.75000
  5310.0      0.0000942   1029.10095   5414.12988
  6229.0      0.0000803   1028.43237   6056.51514
  7179.0      0.0000696   1027.76855   6915.18213
  7812.0      0.0000640   1027.10925   7741.08496
  8557.0      0.0000584   1026.45496   8220.36426
  8103.0      0.0000617   1025.80493   8071.37256
  7341.0      0.0000681   1025.15967   7248.60400
  6023.0      0.0000830   1024.51892   6024.32715
  4614.0      0.0001084   1023.88251   4746.57813
  3312.0      0.0001510   1023.25061   3643.35571
  2467.0      0.0002027   1022.62323   2809.83618
  2049.0      0.0002440   1022.00000   2242.70288
  1765.0      0.0002833   1021.38129   1890.21497
  1586.0      0.0003153   1020.76666   1684.31433
  1509.0      0.0003313   1020.15649   1572.97241
  1506.0      0.0003320   1019.55035   1518.02722
  1509.0      0.0003313   1018.94830   1498.43188
  1480.0      0.0003378   1018.35046   1505.12378
  1535.0      0.0003257   1017.75659   1529.65405
  1619.0      0.0003088   1017.16675   1564.26221
  1624.0      0.0003079   1016.58081   1601.73804
  1748.0      0.0002860   1015.99884   1640.62671
  1707.0      0.0002929   1015.42084   1695.43323
  1817.0      0.0002752   1014.84662   1797.18872
  2045.0      0.0002445   1014.27612   1987.80457
  2379.0      0.0002102   1013.70941   2297.93262
  2697.0      0.0001854   1013.14636   2725.23755
  3161.0      0.0001582   1012.58698   3229.35571
  3663.0      0.0001365   1012.03107   3707.09570
  4008.0      0.0001248   1011.47894   4023.58545
  3992.0      0.0001253   1010.93011   4059.13770
  3706.0      0.0001349   1010.38495   3797.80054
  3429.0      0.0001458   1009.84308   3351.12085
  2865.0      0.0001745   1009.30457   2865.00146
  2361.0      0.0002118   1008.76941   2452.77905
  2184.0      0.0002289   1008.23755   2171.20825
  1989.0      0.0002514   1007.70892   2022.09070
  1973.0      0.0002534   1007.18347   1969.63965
  1941.0      0.0002576   1006.66107   1958.49268
  1960.0      0.0002551   1006.14203   1932.88098
  1817.0      0.0002752   1005.62573   1854.64502
  1691.0      0.0002957   1005.11261   1731.73962
  1573.0      0.0003179   1004.60248   1585.94934
  1463.0      0.0003418   1004.09503   1449.38074
  1323.0      0.000378    1003.59064   1337.31104
  1204.0      0.000415    1003.08899   1254.07141
  1174.0      0.000426    1002.59015   1200.90479
  1149.0      0.000435    1002.09399   1163.73804
  1026.0      0.000487    1001.60065   1139.95166
  1052.0      0.000475    1001.10980   1124.35278
  1077.0      0.000464    1000.62146   1113.53784
  1134.0      0.000441    1000.13586   1105.54407
  1106.0      0.000452    999.65265    1099.50305
  1106.0      0.000452    999.17181    1094.56152
  1037.0      0.000482    998.69354    1090.60254
  1086.0      0.000460    998.21741    1087.46643
  1106.0      0.000452    997.74390    1085.10669
  1102.0      0.000454    997.27240    1083.36353
  1070.0      0.000467    996.80322    1084.13696
  1075.0      0.000465    996.33618    1083.70251
  1036.0      0.000483    995.87128    1083.91235
  988.0       0.000506    995.40845    1084.80652
  1031.0      0.000485    994.94763    1086.45410
  984.0       0.000508    994.48889    1088.95886
  1039.0      0.000481    994.03204    1092.47253
  1034.0      0.000484    993.57709    1097.22058
  1067.0      0.000469    993.12402    1105.28442
  1039.0      0.000481    992.67273    1113.96802
  1070.0      0.000467    992.22321    1126.36572
  1079.0      0.000463    991.77539    1145.69263
  1132.0      0.000442    991.32935    1178.89172
  1184.0      0.000422    990.88495    1239.48157
  1346.0      0.000371    990.44196    1354.24207
  1465.0      0.0003413   990.00073    1545.39905
  1801.0      0.0002776   989.56097    1846.41040
  2297.0      0.0002177   989.12262    2266.53101
  2690.0      0.0001859   988.68567    2763.81909
  3245.0      0.0001541   988.25018    3256.94897
  3617.0      0.0001382   987.81592    3595.55713
  3578.0      0.0001397   987.38306    3645.50244
  3337.0      0.0001498   986.95135    3377.06470
  2938.0      0.0001702   986.52106    2906.05737
  2333.0      0.0002143   986.09174    2394.87500
  1950.0      0.0002564   985.66357    1956.85901
  1557.0      0.0003211   985.23651    1639.18677
  1431.0      0.0003494   984.81055    1440.11621
  1304.0      0.000383    984.38550    1333.99683
  1293.0      0.000387    983.96149    1293.26404
  1225.0      0.000408    983.53839    1296.59058
  1286.0      0.000389    983.11621    1351.31519
  1455.0      0.0003436   982.69482    1461.80640
  1645.0      0.0003040   982.27423    1640.08789
  1972.0      0.0002535   981.85443    1888.17029
  2278.0      0.0002195   981.43542    2184.70117
  2664.0      0.0001877   981.01697    2480.99805
  2794.0      0.0001790   980.59924    2717.99292
  3006.0      0.0001663   980.18213    2871.73169
  3307.0      0.0001512   979.76556    3015.52222
  3534.0      0.0001415   979.34967    3280.17676
  4034.0      0.0001239   978.93420    3777.26831
  4940.0      0.0001012   978.51923    4486.79346
  5624.0      0.0000889   978.10461    5224.27490
  6119.0      0.0000817   977.69043    5692.81787
  5819.0      0.0000859   977.27661    5615.72070
  5145.0      0.0000972   976.86310    4982.37988
  4086.0      0.0001224   976.44995    4059.58008
  3070.0      0.0001629   976.03699    3146.07275
  2316.0      0.0002159   975.62427    2419.62939
  1919.0      0.0002606   975.21179    1931.16431
  1642.0      0.0003045   974.79932    1647.93628
  1532.0      0.0003264   974.38702    1506.17603
  1523.0      0.0003283   973.97485    1457.75012
  1436.0      0.0003482   973.56281    1449.18152
  1559.0      0.0003207   973.15057    1475.42737
  1596.0      0.0003133   972.73859    1537.82507
  1652.0      0.0003027   972.32648    1655.82642
  1978.0      0.0002528   971.91418    1867.51514
  2364.0      0.0002115   971.50195    2232.41748
  2888.0      0.0001731   971.08954    2824.53296
  3845.0      0.0001300   970.67688    3707.60425
  5052.0      0.0000990   970.26410    4891.12451
  6537.0      0.0000765   969.85101    6279.20020
  8066.0      0.0000620   969.43781    7637.80078
  8878.0      0.0000563   969.02435    8623.52637
  8984.0      0.0000557   968.61041    8903.21484
  8546.0      0.0000585   968.19635    8367.27441
  7177.0      0.0000697   967.78174    7239.56982
  5741.0      0.0000871   967.36682    5904.47070
  4265.0      0.0001172   966.95142    4658.63232
  3278.0      0.0001525   966.53577    3648.22827
  2721.0      0.0001838   966.11957    2916.72461
  2278.0      0.0002195   965.70282    2450.37964
  2234.0      0.0002238   965.28571    2213.86719
  2228.0      0.0002244   964.86786    2182.21558
  2320.0      0.0002155   964.44952    2358.39111
  2746.0      0.0001821   964.03064    2771.88721
  3476.0      0.0001438   963.61108    3457.85889
  4477.0      0.0001117   963.19098    4419.09717
  5580.0      0.0000896   962.77008    5579.07617
  6709.0      0.0000745   962.34869    6744.09766
  7770.0      0.0000644   961.92664    7612.03174
  7895.0      0.0000633   961.50366    7869.96191
  7416.0      0.0000674   961.08008    7389.64697
  6505.0      0.0000769   960.65570    6373.60645
  5355.0      0.0000934   960.23053    5187.00391
  4020.0      0.0001244   959.80457    4112.56396
  3199.0      0.0001563   959.37775    3284.54810
  2674.0      0.0001870   958.95026    2720.12915
  2371.0      0.0002109   958.52179    2364.23511
  2162.0      0.0002313   958.09253    2143.44946
  2010.0      0.0002488   957.66235    2009.72266
  2034.0      0.0002458   957.23126    1953.69263
  2120.0      0.0002358   956.79926    1986.97009
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  2534.0      0.0001973   955.93237    2355.74292
  2797.0      0.0001788   955.49750    2652.37549
  3042.0      0.0001644   955.06177    2946.20361
  3367.0      0.0001485   954.62494    3164.18970
  3310.0      0.0001511   954.18707    3285.48779
  3504.0      0.0001427   953.74829    3407.29175
  3908.0      0.0001279   953.30829    3732.15527
  4709.0      0.0001062   952.86743    4499.12646
  6217.0      0.0000804   952.42548    5924.31494
  8347.0      0.0000599   951.98242    8132.63477
  11367.0     0.0000440   951.53839    11041.38184
  14504.0     0.0000345   951.09314    14261.56055
  17495.0     0.0000286   950.64691    17095.03125
  19038.0     0.0000263   950.19952    18737.56836
  18895.0     0.0000265   949.75092    18691.98438
  17350.0     0.0000288   949.30133    17115.00586
  14633.0     0.0000342   948.85052    14679.92871
  11604.0     0.0000431   948.39862    12038.20020
  9428.0      0.0000530   947.94550    9511.84863
  7389.0      0.0000677   947.49133    7265.55420
  5649.0      0.0000885   947.03607    5416.26367
  4306.0      0.0001161   946.57941    4009.62842
  3259.0      0.0001534   946.12170    3012.58911
  2554.0      0.0001958   945.66284    2352.11694
  2247.0      0.0002225   945.20276    1942.12183
  1882.0      0.0002657   944.74152    1700.01550
  1652.0      0.0003027   944.27899    1559.69299
  1562.0      0.0003201   943.81543    1476.93689
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  1773.0      0.0002820   907.02368    1710.67065
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  2043.0      0.0002447   904.88489    1993.87830
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  4020.0      0.0001244   900.59344    3975.06982
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  1438.0      0.0003477   897.36841    1512.42957
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  2722.0      0.0001837   885.05859    2576.75854
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  984.0       0.000508    878.74457    1058.98889
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  942.0       0.000531    877.18524    984.75085
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  935.0       0.000535    876.15070    965.05389
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  921.0       0.000543    875.12067    957.24835
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  966.0       0.000518    872.56549    968.25159
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  929.0       0.000538    848.86230    962.46307
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  943.0       0.000530    848.04480    982.05927
  974.0       0.000513    847.63989    995.17859
  974.0       0.000513    847.23743    1011.06635
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  4523.0      0.0001105   834.26996    4418.62256
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  6716.0      0.0000744   831.19287    5894.82813
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  2509.0      0.0001993   820.11041    2452.57715
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  1789.0      0.0002795   820.06873    1688.39478
  1612.0      0.0003102   820.06000    1527.59937
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  1130.0      0.000442    820.06976    1076.69800
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  1094.0      0.000457    820.11084    1136.58557
  1188.0      0.000421    820.12933    1197.93506
  1293.0      0.000387    820.15015    1287.39734
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  1686.0      0.0002966   820.22662    1716.05176
  1860.0      0.0002688   820.25665    1871.71802
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  2880.0      0.0001736   733.49420    2685.57251
  3042.0      0.0001644   733.13336    2986.56860
  3282.0      0.0001523   732.77179    3179.76270
  3143.0      0.0001591   732.40967    3220.61035
  3038.0      0.0001646   732.04688    3105.20166
  2746.0      0.0001821   731.68341    2866.49390
  2493.0      0.0002006   731.31934    2563.19531
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  1873.0      0.0002670   729.85663    1737.01514
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  1972.0      0.0002535   729.12146    1841.40930
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  2291.0      0.0002182   728.38367    2333.06860
  2576.0      0.0001941   728.01385    2710.06885
  3016.0      0.0001658   727.64337    3134.91968
  3399.0      0.0001471   727.27240    3552.10986
  3766.0      0.0001328   726.90070    3869.57593
  3926.0      0.0001274   726.52832    3994.46606
  3851.0      0.0001298   726.15540    3888.30493
  3665.0      0.0001364   725.78186    3596.00366
  3183.0      0.0001571   725.40765    3205.99976
  2765.0      0.0001808   725.03284    2801.46021
  2330.0      0.0002146   724.65735    2443.41333
  2135.0      0.0002342   724.28143    2162.45923
  1882.0      0.0002657   723.90479    1966.60449
  1820.0      0.0002747   723.52753    1838.00525
  1786.0      0.0002800   723.14966    1754.34424
  1675.0      0.0002985   722.77124    1678.21326
  1650.0      0.0003030   722.39215    1588.67017
  1587.0      0.0003151   722.01251    1484.63867
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  1454.0      0.0003439   721.25146    1276.91260
  1354.0      0.000369    720.87012    1195.70691
  1334.0      0.000375    720.48804    1139.17432
  1248.0      0.000401    720.10547    1108.26172
  1172.0      0.000427    719.72229    1106.90491
  1179.0      0.000424    719.33856    1139.25562
  1248.0      0.000401    718.95422    1211.80505
  1300.0      0.000385    718.56940    1331.88623
  1437.0      0.0003479   718.18390    1506.01941
  1651.0      0.0003028   717.79797    1734.60022
  2012.0      0.0002485   717.41138    2008.35986
  2283.0      0.0002190   717.02429    2303.30762
  2546.0      0.0001964   716.63660    2577.89331
  2821.0      0.0001772   716.24835    2779.80713
  2836.0      0.0001763   715.85956    2872.93018
  2907.0      0.0001720   715.47028    2861.49585
  2758.0      0.0001813   715.08044    2774.01929
  2555.0      0.0001957   714.69012    2633.63330
  2432.0      0.0002056   714.29919    2456.45605
  2310.0      0.0002165   713.90784    2264.16235
  2181.0      0.0002293   713.51587    2081.28760
  1941.0      0.0002576   713.12341    1924.68091
  1955.0      0.0002558   712.73041    1802.71472
  1871.0      0.0002672   712.33698    1722.31409
  1876.0      0.0002665   711.94299    1693.86633
  1923.0      0.0002600   711.54852    1729.45947
  2025.0      0.0002469   711.15363    1840.18823
  2234.0      0.0002238   710.75818    2028.65710
  2427.0      0.0002060   710.36224    2299.96729
  2766.0      0.0001808   709.96582    2644.84229
  3039.0      0.0001645   709.56891    3045.14502
  3377.0      0.0001481   709.17157    3479.62573
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  4556.0      0.0001097   708.37549    4407.55371
  5052.0      0.0000990   707.97681    4864.12598
  5384.0      0.0000929   707.57764    5236.32227
  5485.0      0.0000912   707.17804    5446.60693
  5566.0      0.0000898   706.77795    5462.72266
  5111.0      0.0000978   706.37750    5301.24902
  4752.0      0.0001052   705.97662    4984.09180
  4336.0      0.0001153   705.57526    4531.32764
  3942.0      0.0001268   705.17352    3992.17896
  3514.0      0.0001423   704.77142    3444.46924
  3022.0      0.0001655   704.36884    2958.21533
  2714.0      0.0001842   703.96588    2575.05347
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  2277.0      0.0002196   702.75464    2093.04346
  2259.0      0.0002213   702.35022    2089.68823
  2276.0      0.0002197   701.94531    2108.86890
  2227.0      0.0002245   701.54010    2119.14624
  2141.0      0.0002335   701.13458    2101.43481
  2113.0      0.0002366   700.72864    2045.50879
  1950.0      0.0002564   700.32239    1948.16272
  1805.0      0.0002770   699.91577    1819.10095
  1647.0      0.0003036   699.50879    1678.65125
  1448.0      0.0003453   699.10156    1548.04590
  1385.0      0.000361    698.69391    1441.08618
  1271.0      0.000393    698.28601    1363.52136
  1265.0      0.000395    697.87793    1315.09949
  1232.0      0.000406    697.46942    1286.11938
  1265.0      0.000395    697.06061    1270.02722
  1208.0      0.000414    696.65149    1259.70972
  1242.0      0.000403    696.24213    1250.81958
  1192.0      0.000419    695.83252    1243.44177
  1232.0      0.000406    695.42261    1246.89966
  1320.0      0.000379    695.01245    1277.70764
  1348.0      0.000371    694.60211    1356.23914
  1440.0      0.0003472   694.19147    1504.31555
  1725.0      0.0002899   693.78058    1740.00696
  2055.0      0.0002433   693.36945    2071.18091
  2392.0      0.0002090   692.95807    2492.89819
  2919.0      0.0001713   692.54657    2976.43628
  3468.0      0.0001442   692.13477    3463.92065
  3783.0      0.0001322   691.72278    3868.69702
  3971.0      0.0001259   691.31061    4100.26758
  4060.0      0.0001232   690.89832    4115.42969
  3886.0      0.0001287   690.48584    3941.06934
  3579.0      0.0001397   690.07312    3636.06934
  3307.0      0.0001512   689.66022    3249.39990
  2984.0      0.0001676   689.24719    2826.67358
  2407.0      0.0002077   688.83398    2412.43506
  2078.0      0.0002406   688.42072    2046.62756
  1710.0      0.0002924   688.00720    1751.64026
  1530.0      0.0003268   687.59369    1530.55225
  1353.0      0.000370    687.17999    1386.10657
  1233.0      0.000406    686.76624    1308.08386
  1269.0      0.000394    686.35229    1288.56018
  1299.0      0.000385    685.93823    1323.67725
  1384.0      0.000361    685.52417    1410.23962
  1461.0      0.0003422   685.10999    1548.18201
  1689.0      0.0002960   684.69568    1736.49817
  2026.0      0.0002468   684.28149    1976.49182
  2230.0      0.0002242   683.86707    2265.18335
  2666.0      0.0001875   683.45264    2593.11743
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  3313.0      0.0001509   682.62366    3230.14307
  3540.0      0.0001412   682.20929    3444.56885
  3549.0      0.0001409   681.79462    3554.03491
  3478.0      0.0001438   681.38013    3561.98438
  3461.0      0.0001445   680.96552    3470.41309
  3117.0      0.0001604   680.55103    3285.92944
  3016.0      0.0001658   680.13641    3041.82227
  2836.0      0.0001763   679.72198    2801.72217
  2600.0      0.0001923   679.30743    2620.47437
  2473.0      0.0002022   678.89307    2530.55664
  2486.0      0.0002011   678.47876    2534.69287
  2488.0      0.0002010   678.06433    2609.56152
  2638.0      0.0001895   677.65015    2707.39014
  2707.0      0.0001847   677.23584    2773.47607
  2738.0      0.0001826   676.82184    2767.26221
  2664.0      0.0001877   676.40771    2674.83179
  2503.0      0.0001998   675.99390    2501.72363
  2412.0      0.0002073   675.58014    2269.71045
  2134.0      0.0002343   675.16632    2014.13184
  1871.0      0.0002672   674.75287    1771.11450
  1610.0      0.0003106   674.33929    1564.55408
  1416.0      0.000353    673.92609    1407.32434
  1342.0      0.000373    673.51282    1302.24951
  1247.0      0.000401    673.09985    1246.09607
  1268.0      0.000394    672.68695    1230.61389
  1256.0      0.000398    672.27435    1243.74084
  1317.0      0.000380    671.86194    1271.09277
  1371.0      0.000365    671.44952    1296.11072
  1344.0      0.000372    671.03754    1310.89795
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  1383.0      0.000362    670.21393    1317.61133
  1342.0      0.000373    669.80243    1313.68237
  1367.0      0.000366    669.39124    1302.23364
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  1313.0      0.000381    668.56952    1266.77356
  1310.0      0.000382    668.15918    1267.47839
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  1545.0      0.0003236   666.92926    1498.20020
  1664.0      0.0003005   666.51996    1647.16553
  1864.0      0.0002682   666.11084    1798.55176
  1933.0      0.0002587   665.70215    1916.48975
  2048.0      0.0002441   665.29382    1973.42749
  1985.0      0.0002519   664.88562    1971.39722
  2018.0      0.0002478   664.47797    1938.82483
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  1840.0      0.0002717   662.85040    1986.30432
  1924.0      0.0002599   662.44427    2052.21826
  2010.0      0.0002488   662.03882    2118.19775
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  2227.0      0.0002245   661.22876    2287.29028
  2330.0      0.0002146   660.82446    2429.83862
  2512.0      0.0001990   660.42047    2620.79541
  2784.0      0.0001796   660.01697    2842.50293
  2963.0      0.0001687   659.61377    3065.67407
  3034.0      0.0001648   659.21124    3259.89575
  3283.0      0.0001523   658.80896    3416.95142
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  3563.0      0.0001403   658.00604    3621.24438
  3543.0      0.0001411   657.60516    3637.64429
  3494.0      0.0001431   657.20496    3579.68994
  3337.0      0.0001498   656.80505    3459.80786
  3183.0      0.0001571   656.40582    3291.11816
  2989.0      0.0001673   656.00696    3069.38647
  2698.0      0.0001853   655.60870    2786.70288
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  1969.0      0.0002539   654.81372    2121.83789
  1694.0      0.0002952   654.41711    1820.76672
  1487.0      0.0003362   654.02087    1578.52783
  1293.0      0.000387    653.62537    1405.17761
  1216.0      0.000411    653.23029    1297.57007
  1181.0      0.000423    652.83594    1243.95093
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  1180.0      0.000424    651.26404    1231.14392
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  1205.0      0.000415    650.48181    1191.50696
  1153.0      0.000434    650.09167    1177.09631
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  1448.0      0.0003453   648.53735    1453.40393
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  2257.0      0.0002215   647.37866    2269.81104
  2632.0      0.0001900   646.99371    2622.76440
  2964.0      0.0001687   646.60962    2958.69702
  3210.0      0.0001558   646.22607    3232.01245
  3420.0      0.0001462   645.84344    3417.08789
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  3606.0      0.0001387   645.08008    3548.02905
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  3438.0      0.0001454   644.31970    3472.08276
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  3057.0      0.0001636   641.68243    3191.16528
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  3026.0      0.0001652   640.93604    3073.72949
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  2216.0      0.0002256   639.08447    2169.65112
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  1035.0      0.000483    635.08685    980.11414
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  991.0       0.000505    634.37170    950.58936
  966.0       0.000518    634.01563    940.38055
  933.0       0.000536    633.66028    938.87244
  969.0       0.000516    633.30609    948.81329
  974.0       0.000513    632.95282    973.30829
  997.0       0.000502    632.60034    1014.03070
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  1186.0      0.000422    631.89844    1141.62549
  1165.0      0.000429    631.54901    1217.94421
  1250.0      0.000400    631.20050    1295.79028
  1365.0      0.000366    630.85303    1359.49170
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  1421.0      0.000352    629.81653    1389.22461
  1378.0      0.000363    629.47296    1367.60388
  1398.0      0.000358    629.13049    1351.16663
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  1441.0      0.0003470   627.09698    1450.28406
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  4027.0      0.0001242   623.79230    4100.39551
  4591.0      0.0001089   623.46771    4403.56836
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  4916.0      0.0001017   622.82196    4684.41748
  4778.0      0.0001046   622.50073    4544.90137
  4418.0      0.0001132   622.18060    4228.19336
  3959.0      0.0001263   621.86163    3825.74927
  3589.0      0.0001393   621.54382    3436.38672
  2992.0      0.0001671   621.22705    3126.12866
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  2711.0      0.0001844   620.28363    2727.04199
  2683.0      0.0001864   619.97131    2655.75171
  2621.0      0.0001908   619.66028    2564.72461
  2442.0      0.0002048   619.35040    2455.45581
  2294.0      0.0002180   619.04163    2336.32983
  2119.0      0.0002360   618.73401    2209.54126
  1984.0      0.0002520   618.42749    2070.35303
  1868.0      0.0002677   618.12225    1912.83313
  1711.0      0.0002922   617.81805    1741.00989
  1492.0      0.0003351   617.51514    1569.21204
  1379.0      0.000363    617.21326    1417.42432
  1272.0      0.000393    616.91272    1304.27271
  1261.0      0.000397    616.61328    1243.05481
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  1310.0      0.000382    616.01788    1300.89026
  1349.0      0.000371    615.72192    1415.04480
  1542.0      0.0003243   615.42725    1568.97083
  1665.0      0.0003003   615.13367    1738.04297
  1912.0      0.0002615   614.84143    1888.68518
  1958.0      0.0002554   614.55017    1983.12915
  1993.0      0.0002509   614.26025    1999.33240
  2029.0      0.0002464   613.97162    1947.27954
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  972.0       0.000514    606.38281    962.26715
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  1082.0      0.000462    604.09589    1082.23059
  1046.0      0.000478    604.04657    1085.02771
  1064.0      0.000470    603.99524    1075.82996
  968.0       0.000517    603.94196    1053.58923
  992.0       0.000504    603.88654    1020.25562
  935.0       0.000535    603.82922    981.94409
  870.0       0.000575    603.76990    942.99988
  868.0       0.000576    603.70850    908.25635
  892.0       0.000561    603.64508    881.12115
  847.0       0.000590    603.57971    864.07764
  859.0       0.000582    603.51233    858.90747
  875.0       0.000571    603.44287    867.16077
  872.0       0.000573    603.37146    890.04596
  920.0       0.000543    603.29797    929.44702
  975.0       0.000513    603.22253    986.21521
  1057.0      0.000473    603.14502    1061.36926
  1191.0      0.000420    603.06555    1154.68701
  1323.0      0.000378    602.98401    1264.17700
  1448.0      0.0003453   602.90045    1385.27576
  1535.0      0.0003257   602.81494    1511.63257
  1728.0      0.0002894   602.72742    1635.27307
  1803.0      0.0002773   602.63788    1747.94739
  1809.0      0.0002764   602.54633    1843.96216
  1902.0      0.0002629   602.45276    1921.67126
  1990.0      0.0002513   602.35718    1984.26794
  1996.0      0.0002505   602.25964    2035.72229
  2097.0      0.0002384   602.16016    2078.86011
  2149.0      0.0002327   602.05859    2114.73486
  2121.0      0.0002357   601.95508    2143.41821
  2161.0      0.0002314   601.84955    2164.59961
  2078.0      0.0002406   601.74207    2177.15552
  2056.0      0.0002432   601.63257    2179.36548
  2125.0      0.0002353   601.52118    2170.93921
  2051.0      0.0002438   601.40771    2154.21899
  2060.0      0.0002427   601.29236    2133.49194
  2019.0      0.0002476   601.17505    2111.54102
  2092.0      0.0002390   601.05579    2087.45361
  2041.0      0.0002450   600.93451    2056.56738
  2040.0      0.0002451   600.81128    2014.81714
  2037.0      0.0002455   600.68622    1962.24060
  2010.0      0.0002488   600.55914    1903.68530
  1937.0      0.0002581   600.43011    1845.55176
  1838.0      0.0002720   600.29919    1792.30176
  1777.0      0.0002814   600.16632    1745.58411
  1768.0      0.0002828   600.03162    1704.27722
  1721.0      0.0002905   599.89496    1669.46411
  1654.0      0.0003023   599.75635    1645.06824
  1617.0      0.0003092   599.61584    1635.14563
  1615.0      0.0003096   599.47357    1644.35242
  1670.0      0.0002994   599.32928    1672.89661
  1726.0      0.0002897   599.18323    1717.06494
  1778.0      0.0002812   599.03522    1767.64954
  1903.0      0.0002627   598.88538    1813.32886
  1874.0      0.0002668   598.73376    1841.97693
  1965.0      0.0002545   598.58020    1842.94934
  1917.0      0.0002608   598.42487    1809.69653
  1846.0      0.0002709   598.26764    1743.18115
  1662.0      0.0003008   598.10864    1652.82800
  1537.0      0.0003253   597.94775    1552.94092
  1392.0      0.000359    597.78516    1457.53857
  1421.0      0.000352    597.62079    1377.47498
  1284.0      0.000389    597.45459    1319.36902
  1262.0      0.000396    597.28662    1285.60010
  1306.0      0.000383    597.11682    1275.01929
  1298.0      0.000385    596.94537    1284.35803
  1324.0      0.000378    596.77209    1309.82385
  1344.0      0.000372    596.59717    1348.64319
  1399.0      0.000357    596.42047    1399.88635
  1533.0      0.0003262   596.24200    1464.11780
  1579.0      0.0003167   596.06195    1541.96875
  1690.0      0.0002959   595.88007    1633.05896
  1830.0      0.0002732   595.69659    1734.26123
  1914.0      0.0002612   595.51135    1841.94434
  2047.0      0.0002443   595.32452    1953.28101
  2099.0      0.0002382   595.13599    2067.57788
  2250.0      0.0002222   594.94586    2184.66821
  2319.0      0.0002156   594.75415    2300.57202
  2492.0      0.0002006   594.56073    2408.81812
  2509.0      0.0001993   594.36578    2493.71313
  2620.0      0.0001908   594.16913    2536.82593
  2584.0      0.0001935   593.97101    2521.79834
  2502.0      0.0001998   593.77124    2442.20239
  2372.0      0.0002108   593.56995    2306.56689
  2172.0      0.0002302   593.36707    2133.12305
  1903.0      0.0002627   593.16272    1943.67175
  1708.0      0.0002927   592.95685    1756.68018
  1556.0      0.0003213   592.74933    1585.41321
  1309.0      0.000382    592.54053    1437.26782
  1316.0      0.000380    592.33008    1315.49023
  1249.0      0.000400    592.11823    1219.39368
  1122.0      0.000446    591.90491    1145.21216
  1071.0      0.000467    591.69019    1087.62695
  1059.0      0.000472    591.47400    1041.37378
  1022.0      0.000489    591.25641    1002.57440
  959.0       0.000521    591.03741    969.08594
  973.0       0.000514    590.81696    940.28943
  928.0       0.000539    590.59521    916.79822
  836.0       0.000598    590.37213    899.78937
  897.0       0.000557    590.14764    890.61609
  899.0       0.000556    589.92181    890.42731
  893.0       0.000560    589.69476    899.42755
  861.0       0.000581    589.46637    917.66248
  1008.0      0.000496    589.23663    944.38586
  932.0       0.000536    589.00574    978.14697
  1022.0      0.000489    588.77344    1016.99347
  1042.0      0.000480    588.53998    1057.53650
  1114.0      0.000449    588.30524    1096.80127
  1088.0      0.000460    588.06940    1131.88013
  1177.0      0.000425    587.83228    1160.88037
  1223.0      0.000409    587.59399    1182.84167
  1193.0      0.000419    587.35461    1197.02344
  1173.0      0.000426    587.11395    1203.27344
  1192.0      0.000419    586.87225    1200.13037
  1141.0      0.000438    586.62939    1188.49609
  1224.0      0.000408    586.38550    1170.96216
  1144.0      0.000437    586.14044    1152.46997
  1131.0      0.000442    585.89435    1139.55640
  1095.0      0.000457    585.64722    1139.23999
  1116.0      0.000448    585.39899    1157.73352
  1183.0      0.000423    585.14978    1201.85168
  1333.0      0.000375    584.89960    1274.58044
  1494.0      0.0003347   584.64838    1377.24756
  1513.0      0.0003305   584.39618    1507.09558
  1697.0      0.0002946   584.14307    1656.72168
  1828.0      0.0002735   583.88898    1813.60229
  2037.0      0.0002455   583.63403    1961.15173
  2071.0      0.0002414   583.37811    2080.51294
  2108.0      0.0002372   583.12134    2154.27686
  2182.0      0.0002291   582.86371    2171.33984
  2086.0      0.0002397   582.60510    2129.91211
  1949.0      0.0002565   582.34583    2039.83643
  1818.0      0.0002750   582.08563    1918.81018
  1693.0      0.0002953   581.82465    1787.00696
  1574.0      0.0003177   581.56281    1662.21851
  1509.0      0.0003313   581.30035    1556.15540
  1514.0      0.0003303   581.03711    1473.85693
  1442.0      0.0003467   580.77301    1414.73669
  1425.0      0.000351    580.50842    1373.12024
  1379.0      0.000363    580.24286    1341.47375
  1393.0      0.000359    579.97681    1313.18274
  1382.0      0.000362    579.70996    1284.75415
  1319.0      0.000379    579.44263    1255.68250
  1229.0      0.000407    579.17456    1226.93787
  1171.0      0.000427    578.90582    1199.97754
  1167.0      0.000428    578.63660    1176.26379
  1158.0      0.000432    578.36670    1156.36182
  1146.0      0.000436    578.09631    1141.77185
  1169.0      0.000428    577.82526    1133.80127
  1161.0      0.000431    577.55383    1133.81763
  1241.0      0.000403    577.28180    1142.77600
  1225.0      0.000408    577.00934    1161.34363
  1209.0      0.000414    576.73645    1189.03784
  1304.0      0.000383    576.46295    1224.25623
  1307.0      0.000383    576.18915    1264.46704
  1332.0      0.000375    575.91486    1305.60315
  1462.0      0.0003420   575.64020    1343.11841
  1403.0      0.000356    575.36505    1373.04797
  1525.0      0.0003279   575.08966    1393.63721
  1453.0      0.0003441   574.81378    1407.08191
  1451.0      0.0003446   574.53766    1418.65686
  1397.0      0.000358    574.26123    1433.97949
  1415.0      0.000353    573.98450    1457.19165
  1469.0      0.0003404   573.70746    1488.49512
  1475.0      0.0003390   573.43011    1524.57129
  1590.0      0.0003145   573.15265    1558.91736
  1636.0      0.0003056   572.87482    1582.94812
  1587.0      0.0003151   572.59680    1588.03613
  1570.0      0.0003185   572.31873    1568.57288
  1519.0      0.0003292   572.04022    1524.96216
  1502.0      0.0003329   571.76172    1463.70496
  1408.0      0.000355    571.48297    1394.76025
  1318.0      0.000379    571.20422    1328.40894
  1202.0      0.000416    570.92523    1273.99341
  1243.0      0.000402    570.64624    1238.18188
  1235.0      0.000405    570.36707    1224.94019
  1251.0      0.000400    570.08795    1234.65173
  1283.0      0.000390    569.80878    1265.50842
  1343.0      0.000372    569.52948    1313.06494
  1452.0      0.0003444   569.25031    1370.95447
  1446.0      0.0003458   568.97095    1431.47339
  1518.0      0.0003294   568.69177    1486.66077
  1512.0      0.0003307   568.41254    1529.73083
  1579.0      0.0003167   568.13342    1555.48462
  1595.0      0.0003135   567.85431    1567.39380
  1584.0      0.0003157   567.57532    1567.02881
  1621.0      0.0003085   567.29651    1565.28186
  1585.0      0.0003155   567.01764    1569.09729
  1508.0      0.0003316   566.73907    1584.65173
  1542.0      0.0003243   566.46051    1616.01965
  1564.0      0.0003197   566.18225    1664.87146
  1604.0      0.0003117   565.90399    1730.79028
  1749.0      0.0002859   565.62610    1810.09778
  1802.0      0.0002775   565.34839    1895.48010
  1935.0      0.0002584   565.07080    1975.06116
  2034.0      0.0002458   564.79364    2034.98132
  2035.0      0.0002457   564.51648    2061.71509
  2061.0      0.0002426   564.23975    2046.87244
  1976.0      0.0002530   563.96326    1990.35803
  1924.0      0.0002599   563.68713    1899.90906
  1702.0      0.0002938   563.41119    1788.23071
  1666.0      0.0003001   563.13574    1667.22058
  1465.0      0.0003413   562.86060    1546.09607
  1451.0      0.0003446   562.58569    1431.09631
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  1147.0      0.000436    561.76355    1154.08386
  1080.0      0.000463    561.49023    1087.72766
  1086.0      0.000460    561.21741    1033.15955
  999.0       0.000501    560.94495    990.03546
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  996.0       0.000502    560.13062    928.03955
  906.0       0.000552    559.86023    930.63068
  983.0       0.000509    559.59015    943.17535
  1027.0      0.000487    559.32068    964.57227
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  684.0       0.000731    368.62921    672.85748
  663.0       0.000754    368.28702    674.44366
  711.0       0.000703    367.93866    675.40851
  639.0       0.000782    367.58392    675.60236
  709.0       0.000705    367.22333    674.98389
  640.0       0.000781    366.85660    673.51373
  728.0       0.000687    366.48425    671.23901
  704.0       0.000710    366.10623    668.01050
  676.0       0.000740    365.72305    663.65680
  743.0       0.000673    365.33478    658.06110
  648.0       0.000772    364.94159    651.30835
  662.0       0.000755    364.54416    643.51501
  646.0       0.000774    364.14249    635.28729
  661.0       0.000756    363.73727    627.10852
  640.0       0.000781    363.32874    619.58105
  619.0       0.000808    362.91766    613.21588
  627.0       0.000797    362.50427    608.49023
  618.0       0.000809    362.08942    605.81372
  658.0       0.000760    361.67371    605.54578
  709.0       0.000705    361.25757    607.98950
  605.0       0.000826    360.84213    613.41132
  670.0       0.000746    360.42801    622.00513
  658.0       0.000760    360.01624    633.96118
  644.0       0.000776    359.60757    649.25714
  691.0       0.000724    359.20340    667.90582
  696.0       0.000718    358.80460    689.54041
  728.0       0.000687    358.41226    714.14948
  729.0       0.000686    358.02802    740.90820
  715.0       0.000699    357.65298    768.88306
  758.0       0.000660    357.28882    796.83954
  797.0       0.000627    356.93695    823.37036
  840.0       0.000595    356.59933    846.64539
  850.0       0.000588    356.27744    865.10632
  836.0       0.000598    355.97357    877.31580
  841.0       0.000595    355.68961    882.23700
  835.0       0.000599    355.42767    879.38922
  882.0       0.000567    355.19025    868.93951
  855.0       0.000585    354.97971    851.69611
  867.0       0.000577    354.79886    828.98969
  777.0       0.000644    354.65030    802.46045
  763.0       0.000655    354.53717    773.83228
  705.0       0.000709    354.46255    744.73761
  665.0       0.000752    354.42987    716.61023
  678.0       0.000737    354.44250    690.63617
  611.0       0.000818    354.50436    667.72247
  637.0       0.000785    354.61935    648.48480
  646.0       0.000774    354.79166    633.24976
  629.0       0.000795    355.02560    622.07379
  616.0       0.000812    355.32617    614.77570
  645.0       0.000775    355.69788    610.97729
  631.0       0.000792    356.14615    610.16345
  599.0       0.000835    356.67667    611.67114
  611.0       0.000818    357.29483    614.78778
  627.0       0.000797    358.00717    618.74103
  646.0       0.000774    358.81961    622.75415
  651.0       0.000768    359.73956    626.12537
  635.0       0.000787    360.77332    628.31793
  671.0      .            .            .
_pd_meas_number_of_points              5750
_pd_proc_number_of_points              5750

_reflns_number_total                   1601
_reflns_limit_h_min                    0
_reflns_limit_h_max                    6
_reflns_limit_k_min                    0
_reflns_limit_k_max                    31
_reflns_limit_l_min                    -7
_reflns_limit_l_max                    7
_reflns_d_resolution_high              0.890
_reflns_d_resolution_low               13.949
#--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--#
