# Electronic Supplementary Material (ESI) for Dalton Transactions.
# This journal is © The Royal Society of Chemistry 2023

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_ex_wk1
_database_code_depnum_ccdc_archive 'CCDC 2251721'
loop_
_audit_author_name
_audit_author_address
Wadepohl
;Uni Heidelberg
Germany
;
_audit_update_record             
;
2023-03-26 deposited with the CCDC.	2023-10-18 downloaded from the CCDC.
;
_audit_creation_date             2017-05-15

_audit_block_code                ex_wk1
_audit_block_refno               2883
_audit_block_usercomment         'W. Keller SeB11'


_audit_creation_method           
;
Olex2 1.2
(compiled Mar 28 2017 19:34:44 for OlexSys, GUI svn.r5337)
;
_chemical_name_systematic        ?
_chemical_name_common            ?
_chemical_formula_moiety         'B11 Cl11 Se'
_chemical_formula_sum            'B11 Cl11 Se'
_chemical_properties_physical    'air-sensitive, moisture-sensitive'
_chemical_formula_weight         587.82
_symmetry_cell_setting           monoclinic
#_space_group_name_H-M_alt       'P 21'
#_space_group_IT_number          4
_chemical_absolute_configuration ad
_chemical_melting_point          ?
_exptl_crystal_description       irregular
_exptl_crystal_colour            colourless
_diffrn_ambient_temperature      120(1)
_chemical_oxdiff_formula         'Se1 B11 Cl11'
_chemical_oxdiff_usercomment     'W. Keller SeB11'
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Se Se -0.0929 2.2259 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           4
_space_group_name_H-M_alt        'P 1 21 1'
_space_group_name_Hall           'P 2yb'
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z'

_cell_length_a                   8.85030(9)
_cell_length_b                   26.9786(2)
_cell_length_c                   9.14388(9)
_cell_angle_alpha                90
_cell_angle_beta                 118.7986(14)
_cell_angle_gamma                90
_cell_volume                     1913.24(4)
_cell_formula_units_Z            4
_cell_measurement_reflns_used    67816
_cell_measurement_temperature    120(1)
_cell_measurement_theta_max      32.1390
_cell_measurement_theta_min      2.5430
_shelx_estimated_absorpt_T_max   0.722
_shelx_estimated_absorpt_T_min   0.722
_exptl_absorpt_coefficient_mu    3.479
_exptl_absorpt_correction_T_max  1.000
_exptl_absorpt_correction_T_min  0.205
_exptl_absorpt_correction_type   gaussian
_exptl_absorpt_process_details   
;
CrysAlisPro 1.171.38.46 (Rigaku Oxford Diffraction, 2015)
Numerical absorption correction based on gaussian integration over
 a multifaceted crystal model (Busing & Levy, 1957).
Empirical absorption correction using spherical harmonics,
 implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_absorpt_special_details   ?
_exptl_crystal_colour_primary    colourless
_exptl_crystal_density_diffrn    2.041
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_F_000             1104
loop_
_exptl_crystal_face_index_h
_exptl_crystal_face_index_k
_exptl_crystal_face_index_l
_exptl_crystal_face_perp_dist
-6 33 2 0.1827
12 11 -4 0.1473
6 -19 5 0.2029
-12 -10 5 0.1521
10 2 -12 0.1710
11 12 -9 0.1617
10 21 -3 0.1449
3 35 -5 0.1834
2 36 2 0.1628
5 -15 7 0.1941
-3 36 1 0.1722
-2 20 11 0.2055
1 -6 11 0.1626
7 -9 -12 0.1831
12 7 -8 0.1553
-10 -18 9 0.1734
-8 26 0 0.1672
-12 5 6 0.1650
-8 -19 -3 0.1198
8 19 3 0.1198
-2 -38 2 0.1652
2 38 -2 0.1652
-5 -6 13 0.1647
5 -33 0 0.2098
5 28 -8 0.1948
-9 -25 6 0.1731
_exptl_crystal_size_max          0.398
_exptl_crystal_size_mid          0.391
_exptl_crystal_size_min          0.240
loop_
_exptl_oxdiff_crystal_face_indexfrac_h
_exptl_oxdiff_crystal_face_indexfrac_k
_exptl_oxdiff_crystal_face_indexfrac_l
_exptl_oxdiff_crystal_face_x
_exptl_oxdiff_crystal_face_y
_exptl_oxdiff_crystal_face_z
-5.9997 32.9988 2.0000 -0.1692 0.4042 0.8947
11.9996 10.9999 -4.0000 -0.7542 -0.6796 -0.0899
5.9997 -18.9994 4.9999 -0.4494 -0.0348 -0.8821
-11.9996 -9.9999 5.0000 0.6800 0.7307 0.0697
9.9996 2.0003 -11.9999 -0.0069 -1.0066 0.1338
10.9997 11.9999 -8.9999 -0.3986 -0.8833 0.1857
9.9997 20.9995 -3.0000 -0.8164 -0.5301 0.1721
3.0000 34.9990 -5.0000 -0.4062 -0.3136 0.8586
2.0001 35.9988 1.9999 -0.7705 0.0757 0.6262
4.9998 -14.9996 6.9998 -0.5562 0.1124 -0.8366
-2.9997 35.9988 1.0000 -0.3613 0.2347 0.8777
-1.9998 19.9992 10.9998 -0.8040 0.6605 0.0593
1.0000 -6.0000 10.9998 -0.6445 0.4919 -0.6400
6.9997 -8.9994 -11.9998 0.3587 -0.8999 0.0166
11.9996 7.0001 -7.9999 -0.4575 -0.8840 -0.0089
-9.9997 -17.9997 8.9999 0.4139 0.8316 -0.3599
-7.9996 25.9991 0.0001 0.1898 0.3770 0.9085
-11.9996 4.9996 6.0000 0.4072 0.8052 0.3584
-7.9998 -18.9994 -2.9999 1.0082 0.1535 0.0424
7.9998 18.9994 2.9999 -1.0082 -0.1535 -0.0424
-2.0001 -37.9988 2.0000 0.5589 0.1187 -0.8397
2.0001 37.9988 -2.0000 -0.5589 -0.1187 0.8397
-4.9998 -6.0001 12.9998 -0.3455 0.8409 -0.4736
4.9997 -32.9989 -0.0000 0.1191 -0.2637 -0.9375
4.9999 27.9993 -7.9999 -0.2666 -0.5570 0.7475
-8.9998 -24.9994 6.0000 0.6233 0.6299 -0.4292

_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0359
_diffrn_reflns_av_unetI/netI     0.0206
_diffrn_reflns_Laue_measured_fraction_full 1.000
_diffrn_reflns_Laue_measured_fraction_max 0.981
_diffrn_reflns_limit_h_max       13
_diffrn_reflns_limit_h_min       -13
_diffrn_reflns_limit_k_max       40
_diffrn_reflns_limit_k_min       -40
_diffrn_reflns_limit_l_max       13
_diffrn_reflns_limit_l_min       -13
_diffrn_reflns_number            121819
_diffrn_reflns_point_group_measured_fraction_full 1.000
_diffrn_reflns_point_group_measured_fraction_max 0.963
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         32.365
_diffrn_reflns_theta_min         2.542
_diffrn_ambient_environment      'perfluoro polyether oil / N~2~'
_diffrn_detector                 'CCD plate'
_diffrn_detector_area_resol_mean 7.9621
_diffrn_detector_type            Eos
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 0.981
_diffrn_measurement_details      
;
List of Runs (angles in degrees, time in seconds):

  # Type    Start    End  Width  tₑₓₚ   ω     θ     κ     φ   Frames
#--------------------------------------------------------------------------
  1  ω     -3.00  97.00   0.50    2.00    --   27.02  77.00-180.00  200
  2  ω    -42.00  48.00   0.50    2.00    --   27.02 -57.00  60.00  180
  3  ω      7.00  96.00   0.50    2.00    --   27.02  57.00  30.00  178
  4  ω    -43.00  57.00   0.50    2.00    --   27.02 -77.00 -30.00  200
  5  ω     -3.00  97.00   0.50    2.00    --   27.02  77.00  90.00  200
  6  ω    -43.00  57.00   0.50    2.00    --   27.02 -77.00-120.00  200
  7  ω     -3.00  97.00   0.50    2.00    --   27.02  77.00 -60.00  200
  8  ω    -20.00  69.00   0.50    2.00    --   27.02 -99.00-180.00  178
  9  ω      2.00  99.00   0.50    2.00    --   27.02  38.00 -60.00  194
 10  ω    -17.00 100.00   0.50    2.00    --   27.02  19.00-180.00  234
 11  ω     -3.00  97.00   0.50    2.00    --   27.02  77.00   0.00  200
 12  ω    -20.00  69.00   0.50    2.00    --   27.02 -99.00-120.00  178
 13  ω      7.00  96.00   0.50    2.00    --   27.02  57.00 -90.00  178
 14  ω    -20.00  69.00   0.50    2.00    --   27.02 -99.00  60.00  178
 15  ω      7.00  96.00   0.50    2.00    --   27.02  57.00 -30.00  178
 16  ω    -46.00 100.00   0.50    2.00    --   27.02   0.00-180.00  292
 17  ω    -46.00 100.00   0.50    2.00    --   27.02   0.00-150.00  292
 18  ω    -46.00 100.00   0.50    2.00    --   27.02   0.00-120.00  292
 19  ω    -46.00 100.00   0.50    2.00    --   27.02   0.00 -90.00  292
 20  ω      7.00  96.00   0.50    2.00    --   27.02  57.00-180.00  178
 21  ω    -46.00 100.00   0.50    2.00    --   27.02   0.00 -30.00  292
 22  ω    -46.00  40.00   0.50    2.00    --   27.02   0.00   0.00  172
 23  ω    -46.00 100.00   0.50    2.00    --   27.02   0.00 -60.00  292
 24  φ    -60.00 210.00   0.50    0.10   0.00   0.00   0.00    --   540
;
_diffrn_measurement_device       'four-circle diffractometer'
_diffrn_measurement_device_type  'Agilent SuperNova, Dual, Cu at zero, Eos'
_diffrn_measurement_method       'ω and φ scans'
_diffrn_orient_matrix_type       
'CrysAlisPro convention (1999,Acta A55,543-557)'
_diffrn_orient_matrix_UB_11      -0.0698392000
_diffrn_orient_matrix_UB_12      -0.0141894000
_diffrn_orient_matrix_UB_13      -0.0599872000
_diffrn_orient_matrix_UB_21      -0.0416928000
_diffrn_orient_matrix_UB_22      0.0016730000
_diffrn_orient_matrix_UB_23      0.0494210000
_diffrn_orient_matrix_UB_31      -0.0418417000
_diffrn_orient_matrix_UB_32      0.0220712000
_diffrn_orient_matrix_UB_33      -0.0423406000
_diffrn_radiation_monochromator  mirror
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   'microfocus X-Ray tube'
_diffrn_source_type              'Agilent SuperNova (Mo) X-ray Source'
_reflns_Friedel_coverage         0.927
_reflns_Friedel_fraction_full    1.000
_reflns_Friedel_fraction_max     0.944
_reflns_number_gt                12843
_reflns_number_total             13175
_reflns_odcompleteness_completeness 99.97
_reflns_odcompleteness_iscentric 1
_reflns_odcompleteness_theta     30.44
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       'CrysAlisPro 1.171.38.46 (Rigaku OD, 2015)'
_computing_data_collection       'CrysAlisPro 1.171.38.46 (Rigaku OD, 2015)'
_computing_data_reduction        'CrysAlisPro 1.171.38.46 (Rigaku OD, 2015)'
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  
'encif (Wadepohl, 2009-17); encifer 1.5.2 (CCDC, 2016)'
_computing_structure_refinement  'ShelXL (Sheldrick, 2015)'
_shelxl_version_number           2016/6
_computing_structure_solution    'SUPERFLIP (Palatinus, 2007-2009)'
_refine_diff_density_max         0.448
_refine_diff_density_min         -0.353
_refine_diff_density_rms         0.061
_refine_ls_abs_structure_details 
;
 Flack x determined using 5881 quotients [(I+)-(I-)]/[(I+)+(I-)]
 (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259).
;
_refine_ls_abs_structure_Flack   0.0035(14)
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.085
_refine_ls_hydrogen_treatment    undef
_refine_ls_matrix_type           full
_refine_ls_number_parameters     415
_refine_ls_number_reflns         13175
_refine_ls_number_restraints     1
_refine_ls_R_factor_all          0.0203
_refine_ls_R_factor_gt           0.0190
_refine_ls_restrained_S_all      1.085
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0153P)²+0.4254P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0384
_refine_ls_wR_factor_ref         0.0387
_refine_special_details          ?
_olex2_refinement_description    
;
;
_atom_sites_solution_hydrogens   .
_atom_sites_solution_primary     iterative
_atom_sites_solution_secondary   difmap
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Se1 Se -0.48192(3) -0.20829(2) -0.14030(3) 0.01436(4) Uani 1 1 d . . . . .
Cl2 Cl -0.46588(8) -0.18691(2) -0.48517(7) 0.02333(11) Uani 1 1 d . . . . .
Cl3 Cl -0.09195(8) -0.22999(2) -0.07889(8) 0.02400(11) Uani 1 1 d . . . . .
Cl4 Cl -0.21567(7) -0.21353(2) 0.25919(7) 0.02379(11) Uani 1 1 d . . . . .
Cl5 Cl -0.66046(7) -0.16063(2) 0.06671(7) 0.02094(11) Uani 1 1 d . . . . .
Cl6 Cl -0.82061(7) -0.14318(2) -0.39152(7) 0.02388(12) Uani 1 1 d . . . . .
Cl7 Cl -0.09735(8) -0.10798(2) -0.24971(7) 0.02223(11) Uani 1 1 d . . . . .
Cl8 Cl 0.05561(7) -0.12246(3) 0.19606(7) 0.02658(13) Uani 1 1 d . . . . .
Cl9 Cl -0.28453(8) -0.08241(2) 0.28677(7) 0.02374(12) Uani 1 1 d . . . . .
Cl10 Cl -0.64775(9) -0.03995(2) -0.10573(8) 0.02743(13) Uani 1 1 d . . . . .
Cl11 Cl -0.53267(9) -0.05666(2) -0.43877(7) 0.02654(12) Uani 1 1 d . . . . .
Cl12 Cl -0.20769(9) -0.01783(2) -0.02963(8) 0.02734(13) Uani 1 1 d . . . . .
B2 B -0.4216(3) -0.16025(10) -0.2949(3) 0.0159(4) Uani 1 1 d . . . . .
B3 B -0.2275(3) -0.18227(10) -0.0859(3) 0.0158(4) Uani 1 1 d . . . . .
B4 B -0.2904(3) -0.17355(9) 0.0885(3) 0.0156(4) Uani 1 1 d . . . . .
B5 B -0.5200(3) -0.14630(9) -0.0109(3) 0.0149(4) Uani 1 1 d . . . . .
B6 B -0.6022(3) -0.13784(10) -0.2472(3) 0.0164(4) Uani 1 1 d . . . . .
B7 B -0.2395(3) -0.12265(9) -0.1722(3) 0.0153(4) Uani 1 1 d . . . . .
B8 B -0.1630(3) -0.13008(10) 0.0492(3) 0.0159(4) Uani 1 1 d . . . . .
B9 B -0.3323(3) -0.10947(10) 0.0923(3) 0.0160(4) Uani 1 1 d . . . . .
B10 B -0.5122(3) -0.08877(10) -0.1009(3) 0.0167(4) Uani 1 1 d . . . . .
B11 B -0.4555(3) -0.09703(9) -0.2659(3) 0.0157(4) Uani 1 1 d . . . . .
B12 B -0.2963(3) -0.07811(9) -0.0612(3) 0.0172(5) Uani 1 1 d . . . . .
Se51 Se -0.81247(3) -0.45883(2) -0.28634(3) 0.01478(4) Uani 1 1 d . . . . .
Cl52 Cl -0.44585(7) -0.45909(2) -0.29031(7) 0.02277(11) Uani 1 1 d . . . . .
Cl53 Cl -0.51240(7) -0.40962(2) 0.05892(6) 0.01999(10) Uani 1 1 d . . . . .
Cl54 Cl -0.98965(7) -0.39851(2) -0.09694(7) 0.01990(10) Uani 1 1 d . . . . .
Cl55 Cl -1.21861(7) -0.44158(2) -0.54279(7) 0.02120(11) Uani 1 1 d . . . . .
Cl56 Cl -0.88806(8) -0.47820(2) -0.66615(7) 0.02556(12) Uani 1 1 d . . . . .
Cl57 Cl -0.40440(7) -0.32832(2) -0.19372(7) 0.01809(10) Uani 1 1 d . . . . .
Cl58 Cl -0.73057(7) -0.29205(2) -0.07303(7) 0.01918(10) Uani 1 1 d . . . . .
Cl59 Cl -1.15616(7) -0.30973(2) -0.43817(7) 0.02107(10) Uani 1 1 d . . . . .
Cl60 Cl -1.09193(7) -0.35653(2) -0.77906(6) 0.02250(11) Uani 1 1 d . . . . .
Cl61 Cl -0.62915(8) -0.36826(2) -0.62812(7) 0.02373(12) Uani 1 1 d . . . . .
Cl62 Cl -0.79583(7) -0.26591(2) -0.49220(7) 0.02029(10) Uani 1 1 d . . . . .
B52 B -0.6217(3) -0.42147(9) -0.3300(3) 0.0151(4) Uani 1 1 d . . . . .
B53 B -0.6549(3) -0.39608(9) -0.1483(3) 0.0146(4) Uani 1 1 d . . . . .
B54 B -0.9016(3) -0.39018(9) -0.2295(3) 0.0140(4) Uani 1 1 d . . . . .
B55 B -1.0198(3) -0.41154(9) -0.4599(3) 0.0150(4) Uani 1 1 d . . . . .
B56 B -0.8481(3) -0.43083(10) -0.5231(3) 0.0165(4) Uani 1 1 d . . . . .
B57 B -0.6085(3) -0.35762(9) -0.2790(3) 0.0141(4) Uani 1 1 d . . . . .
B58 B -0.7694(3) -0.33962(9) -0.2207(3) 0.0139(4) Uani 1 1 d . . . . .
B59 B -0.9805(3) -0.34824(9) -0.4008(3) 0.0144(4) Uani 1 1 d . . . . .
B60 B -0.9488(3) -0.37174(9) -0.5694(3) 0.0145(4) Uani 1 1 d . . . . .
B61 B -0.7192(3) -0.37746(9) -0.4950(3) 0.0148(4) Uani 1 1 d . . . . .
B62 B -0.8021(3) -0.32698(9) -0.4271(3) 0.0134(4) Uani 1 1 d . . . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Se1 B2 2.166(2) . ?
Se1 B3 2.175(2) . ?
Se1 B4 2.171(2) . ?
Se1 B5 2.166(2) . ?
Se1 B6 2.168(3) . ?
Cl2 B2 1.744(2) . ?
Cl3 B3 1.740(3) . ?
Cl4 B4 1.744(2) . ?
Cl5 B5 1.746(2) . ?
Cl6 B6 1.744(3) . ?
Cl7 B7 1.761(2) . ?
Cl8 B8 1.757(2) . ?
Cl9 B9 1.775(2) . ?
Cl10 B10 1.767(3) . ?
Cl11 B11 1.764(2) . ?
Cl12 B12 1.768(3) . ?
B2 B3 1.947(3) . ?
B2 B6 1.945(3) . ?
B2 B7 1.773(3) . ?
B2 B11 1.774(4) . ?
B3 B4 1.940(3) . ?
B3 B7 1.772(4) . ?
B3 B8 1.776(4) . ?
B4 B5 1.928(3) . ?
B4 B8 1.779(3) . ?
B4 B9 1.772(4) . ?
B5 B6 1.933(3) . ?
B5 B9 1.769(4) . ?
B5 B10 1.773(4) . ?
B6 B10 1.775(4) . ?
B6 B11 1.772(4) . ?
B7 B8 1.810(3) . ?
B7 B11 1.814(4) . ?
B7 B12 1.794(3) . ?
B8 B9 1.810(3) . ?
B8 B12 1.797(4) . ?
B9 B10 1.805(4) . ?
B9 B12 1.794(3) . ?
B10 B11 1.819(3) . ?
B10 B12 1.789(4) . ?
B11 B12 1.791(4) . ?
Se51 B52 2.162(2) . ?
Se51 B53 2.170(3) . ?
Se51 B54 2.172(2) . ?
Se51 B55 2.170(2) . ?
Se51 B56 2.168(2) . ?
Cl52 B52 1.744(2) . ?
Cl53 B53 1.736(2) . ?
Cl54 B54 1.742(2) . ?
Cl55 B55 1.744(2) . ?
Cl56 B56 1.739(2) . ?
Cl57 B57 1.772(2) . ?
Cl58 B58 1.772(2) . ?
Cl59 B59 1.761(2) . ?
Cl60 B60 1.763(2) . ?
Cl61 B61 1.764(2) . ?
Cl62 B62 1.762(2) . ?
B52 B53 1.946(3) . ?
B52 B56 1.946(3) . ?
B52 B57 1.774(4) . ?
B52 B61 1.782(3) . ?
B53 B54 1.945(3) . ?
B53 B57 1.774(3) . ?
B53 B58 1.772(4) . ?
B54 B55 1.935(3) . ?
B54 B58 1.774(3) . ?
B54 B59 1.780(3) . ?
B55 B56 1.940(3) . ?
B55 B59 1.774(4) . ?
B55 B60 1.777(3) . ?
B56 B60 1.775(4) . ?
B56 B61 1.777(4) . ?
B57 B58 1.811(3) . ?
B57 B61 1.812(3) . ?
B57 B62 1.794(3) . ?
B58 B59 1.814(3) . ?
B58 B62 1.799(3) . ?
B59 B60 1.810(3) . ?
B59 B62 1.802(3) . ?
B60 B61 1.812(3) . ?
B60 B62 1.791(3) . ?
B61 B62 1.794(3) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
B2 Se1 B3 53.31(9) . . ?
B2 Se1 B4 92.71(9) . . ?
B2 Se1 B5 92.67(9) . . ?
B2 Se1 B6 53.33(9) . . ?
B4 Se1 B3 53.03(9) . . ?
B5 Se1 B3 92.42(9) . . ?
B5 Se1 B4 52.78(9) . . ?
B5 Se1 B6 52.96(9) . . ?
B6 Se1 B3 92.83(10) . . ?
B6 Se1 B4 92.41(10) . . ?
Cl2 B2 Se1 113.38(13) . . ?
Cl2 B2 B3 121.42(16) . . ?
Cl2 B2 B6 122.54(15) . . ?
Cl2 B2 B7 124.49(16) . . ?
Cl2 B2 B11 124.96(16) . . ?
B3 B2 Se1 63.59(10) . . ?
B6 B2 Se1 63.38(10) . . ?
B6 B2 B3 107.85(15) . . ?
B7 B2 Se1 111.35(14) . . ?
B7 B2 B3 56.66(13) . . ?
B7 B2 B6 105.96(16) . . ?
B7 B2 B11 61.51(14) . . ?
B11 B2 Se1 111.41(13) . . ?
B11 B2 B3 106.22(16) . . ?
B11 B2 B6 56.69(13) . . ?
Cl3 B3 Se1 112.89(13) . . ?
Cl3 B3 B2 121.91(15) . . ?
Cl3 B3 B4 121.67(16) . . ?
Cl3 B3 B7 125.48(16) . . ?
Cl3 B3 B8 125.17(16) . . ?
B2 B3 Se1 63.10(10) . . ?
B4 B3 Se1 63.36(10) . . ?
B4 B3 B2 107.64(15) . . ?
B7 B3 Se1 110.97(14) . . ?
B7 B3 B2 56.70(13) . . ?
B7 B3 B4 106.07(16) . . ?
B7 B3 B8 61.36(14) . . ?
B8 B3 Se1 111.42(14) . . ?
B8 B3 B2 106.07(17) . . ?
B8 B3 B4 57.01(13) . . ?
Cl4 B4 Se1 112.27(13) . . ?
Cl4 B4 B3 121.70(16) . . ?
Cl4 B4 B5 121.14(15) . . ?
Cl4 B4 B8 125.75(17) . . ?
Cl4 B4 B9 125.34(16) . . ?
B3 B4 Se1 63.60(10) . . ?
B5 B4 Se1 63.50(10) . . ?
B5 B4 B3 108.25(15) . . ?
B8 B4 Se1 111.50(14) . . ?
B8 B4 B3 56.85(13) . . ?
B8 B4 B5 106.25(17) . . ?
B9 B4 Se1 111.51(15) . . ?
B9 B4 B3 106.25(16) . . ?
B9 B4 B5 56.93(14) . . ?
B9 B4 B8 61.29(14) . . ?
Cl5 B5 Se1 112.31(13) . . ?
Cl5 B5 B4 121.25(15) . . ?
Cl5 B5 B6 121.50(16) . . ?
Cl5 B5 B9 125.25(16) . . ?
Cl5 B5 B10 125.22(16) . . ?
B4 B5 Se1 63.72(10) . . ?
B4 B5 B6 108.42(15) . . ?
B6 B5 Se1 63.55(10) . . ?
B9 B5 Se1 111.83(14) . . ?
B9 B5 B4 57.09(13) . . ?
B9 B5 B6 106.33(16) . . ?
B9 B5 B10 61.28(15) . . ?
B10 B5 Se1 111.80(13) . . ?
B10 B5 B4 106.56(17) . . ?
B10 B5 B6 57.04(13) . . ?
Cl6 B6 Se1 113.16(14) . . ?
Cl6 B6 B2 122.40(15) . . ?
Cl6 B6 B5 121.28(15) . . ?
Cl6 B6 B10 124.28(17) . . ?
Cl6 B6 B11 125.09(17) . . ?
B2 B6 Se1 63.29(11) . . ?
B5 B6 Se1 63.49(10) . . ?
B5 B6 B2 107.85(15) . . ?
B10 B6 Se1 111.68(14) . . ?
B10 B6 B2 106.40(17) . . ?
B10 B6 B5 56.95(13) . . ?
B11 B6 Se1 111.40(14) . . ?
B11 B6 B2 56.78(13) . . ?
B11 B6 B5 106.41(17) . . ?
B11 B6 B10 61.70(14) . . ?
Cl7 B7 B2 118.81(15) . . ?
Cl7 B7 B3 118.82(16) . . ?
Cl7 B7 B8 121.35(16) . . ?
Cl7 B7 B11 121.29(16) . . ?
Cl7 B7 B12 121.77(16) . . ?
B2 B7 B8 112.36(17) . . ?
B2 B7 B11 59.27(14) . . ?
B2 B7 B12 108.91(17) . . ?
B3 B7 B2 66.65(15) . . ?
B3 B7 B8 59.43(14) . . ?
B3 B7 B11 112.31(17) . . ?
B3 B7 B12 109.20(16) . . ?
B8 B7 B11 108.15(16) . . ?
B12 B7 B8 59.81(14) . . ?
B12 B7 B11 59.53(14) . . ?
Cl8 B8 B3 119.41(16) . . ?
Cl8 B8 B4 119.63(16) . . ?
Cl8 B8 B7 121.51(15) . . ?
Cl8 B8 B9 121.31(16) . . ?
Cl8 B8 B12 121.42(17) . . ?
B3 B8 B4 66.14(14) . . ?
B3 B8 B7 59.21(14) . . ?
B3 B8 B9 111.88(17) . . ?
B3 B8 B12 108.88(17) . . ?
B4 B8 B7 111.53(17) . . ?
B4 B8 B9 59.16(14) . . ?
B4 B8 B12 108.63(17) . . ?
B9 B8 B7 107.86(17) . . ?
B12 B8 B7 59.65(14) . . ?
B12 B8 B9 59.64(14) . . ?
Cl9 B9 B8 121.47(16) . . ?
Cl9 B9 B10 121.68(16) . . ?
Cl9 B9 B12 122.94(16) . . ?
B4 B9 Cl9 118.03(16) . . ?
B4 B9 B8 59.55(14) . . ?
B4 B9 B10 112.13(17) . . ?
B4 B9 B12 109.10(16) . . ?
B5 B9 Cl9 118.35(15) . . ?
B5 B9 B4 65.97(14) . . ?
B5 B9 B8 111.98(17) . . ?
B5 B9 B10 59.48(14) . . ?
B5 B9 B12 108.81(17) . . ?
B10 B9 B8 108.34(16) . . ?
B12 B9 B8 59.82(14) . . ?
B12 B9 B10 59.60(14) . . ?
Cl10 B10 B5 119.11(15) . . ?
Cl10 B10 B6 118.97(17) . . ?
Cl10 B10 B9 121.55(16) . . ?
Cl10 B10 B11 121.70(16) . . ?
Cl10 B10 B12 122.08(17) . . ?
B5 B10 B6 66.01(15) . . ?
B5 B10 B9 59.24(14) . . ?
B5 B10 B11 111.44(17) . . ?
B5 B10 B12 108.85(17) . . ?
B6 B10 B9 111.78(18) . . ?
B6 B10 B11 59.07(14) . . ?
B6 B10 B12 108.68(17) . . ?
B9 B10 B11 107.93(17) . . ?
B12 B10 B9 59.88(14) . . ?
B12 B10 B11 59.53(13) . . ?
Cl11 B11 B2 118.69(15) . . ?
Cl11 B11 B6 119.00(17) . . ?
Cl11 B11 B7 121.57(15) . . ?
Cl11 B11 B10 121.70(16) . . ?
Cl11 B11 B12 122.05(16) . . ?
B2 B11 B7 59.22(14) . . ?
B2 B11 B10 112.09(17) . . ?
B2 B11 B12 109.00(17) . . ?
B6 B11 B2 66.52(14) . . ?
B6 B11 B7 111.85(17) . . ?
B6 B11 B10 59.22(14) . . ?
B6 B11 B12 108.69(16) . . ?
B7 B11 B10 107.71(16) . . ?
B12 B11 B7 59.69(14) . . ?
B12 B11 B10 59.39(14) . . ?
Cl12 B12 B7 119.04(16) . . ?
Cl12 B12 B8 120.44(17) . . ?
Cl12 B12 B9 122.54(16) . . ?
Cl12 B12 B10 121.85(17) . . ?
Cl12 B12 B11 119.78(16) . . ?
B7 B12 B8 60.54(14) . . ?
B9 B12 B7 109.30(17) . . ?
B9 B12 B8 60.54(14) . . ?
B10 B12 B7 109.93(17) . . ?
B10 B12 B8 109.66(17) . . ?
B10 B12 B9 60.52(14) . . ?
B10 B12 B11 61.08(14) . . ?
B11 B12 B7 60.78(14) . . ?
B11 B12 B8 109.74(17) . . ?
B11 B12 B9 109.67(17) . . ?
B52 Se51 B53 53.38(9) . . ?
B52 Se51 B54 93.02(9) . . ?
B52 Se51 B55 92.94(9) . . ?
B52 Se51 B56 53.40(9) . . ?
B53 Se51 B54 53.23(9) . . ?
B55 Se51 B53 92.69(9) . . ?
B55 Se51 B54 52.91(9) . . ?
B56 Se51 B53 93.01(9) . . ?
B56 Se51 B54 92.71(9) . . ?
B56 Se51 B55 53.13(9) . . ?
Cl52 B52 Se51 112.84(13) . . ?
Cl52 B52 B53 120.91(15) . . ?
Cl52 B52 B56 122.61(15) . . ?
Cl52 B52 B57 124.85(16) . . ?
Cl52 B52 B61 125.71(15) . . ?
B53 B52 Se51 63.51(10) . . ?
B56 B52 Se51 63.45(10) . . ?
B56 B52 B53 107.93(15) . . ?
B57 B52 Se51 111.26(13) . . ?
B57 B52 B53 56.74(13) . . ?
B57 B52 B56 105.87(16) . . ?
B57 B52 B61 61.27(14) . . ?
B61 B52 Se51 111.37(14) . . ?
B61 B52 B53 106.13(16) . . ?
B61 B52 B56 56.73(13) . . ?
Cl53 B53 Se51 113.33(13) . . ?
Cl53 B53 B52 121.95(15) . . ?
Cl53 B53 B54 121.69(15) . . ?
Cl53 B53 B57 125.22(16) . . ?
Cl53 B53 B58 124.95(16) . . ?
B52 B53 Se51 63.11(10) . . ?
B54 B53 Se51 63.44(10) . . ?
B54 B53 B52 107.84(15) . . ?
B57 B53 Se51 110.91(14) . . ?
B57 B53 B52 56.73(13) . . ?
B57 B53 B54 106.06(16) . . ?
B58 B53 Se51 111.20(14) . . ?
B58 B53 B52 106.15(16) . . ?
B58 B53 B54 56.78(13) . . ?
B58 B53 B57 61.43(14) . . ?
Cl54 B54 Se51 113.09(13) . . ?
Cl54 B54 B53 121.34(15) . . ?
Cl54 B54 B55 122.05(15) . . ?
Cl54 B54 B58 125.03(16) . . ?
Cl54 B54 B59 125.23(16) . . ?
B53 B54 Se51 63.33(10) . . ?
B55 B54 Se51 63.48(10) . . ?
B55 B54 B53 108.06(15) . . ?
B58 B54 Se51 111.02(13) . . ?
B58 B54 B53 56.67(13) . . ?
B58 B54 B55 106.10(15) . . ?
B58 B54 B59 61.41(14) . . ?
B59 B54 Se51 111.41(13) . . ?
B59 B54 B53 106.26(16) . . ?
B59 B54 B55 56.89(13) . . ?
Cl55 B55 Se51 111.43(13) . . ?
Cl55 B55 B54 120.99(14) . . ?
Cl55 B55 B56 121.14(15) . . ?
Cl55 B55 B59 126.06(16) . . ?
Cl55 B55 B60 126.34(16) . . ?
B54 B55 Se51 63.60(10) . . ?
B54 B55 B56 108.31(15) . . ?
B56 B55 Se51 63.38(10) . . ?
B59 B55 Se51 111.73(14) . . ?
B59 B55 B54 57.15(13) . . ?
B59 B55 B56 106.38(16) . . ?
B59 B55 B60 61.28(14) . . ?
B60 B55 Se51 111.29(14) . . ?
B60 B55 B54 106.33(16) . . ?
B60 B55 B56 56.86(13) . . ?
Cl56 B56 Se51 111.97(13) . . ?
Cl56 B56 B52 121.71(16) . . ?
Cl56 B56 B55 121.10(16) . . ?
Cl56 B56 B60 125.71(16) . . ?
Cl56 B56 B61 126.03(16) . . ?
B52 B56 Se51 63.15(10) . . ?
B55 B56 Se51 63.49(10) . . ?
B55 B56 B52 107.87(15) . . ?
B60 B56 Se51 111.45(14) . . ?
B60 B56 B52 106.20(16) . . ?
B60 B56 B55 56.94(13) . . ?
B60 B56 B61 61.35(14) . . ?
B61 B56 Se51 111.32(14) . . ?
B61 B56 B52 56.98(13) . . ?
B61 B56 B55 106.26(16) . . ?
Cl57 B57 B52 118.25(15) . . ?
Cl57 B57 B53 118.82(15) . . ?
Cl57 B57 B58 122.01(16) . . ?
Cl57 B57 B61 120.87(15) . . ?
Cl57 B57 B62 121.82(16) . . ?
B52 B57 B53 66.53(14) . . ?
B52 B57 B58 112.10(17) . . ?
B52 B57 B61 59.59(13) . . ?
B52 B57 B62 109.33(17) . . ?
B53 B57 B58 59.23(13) . . ?
B53 B57 B61 112.50(17) . . ?
B53 B57 B62 109.35(16) . . ?
B58 B57 B61 108.14(16) . . ?
B62 B57 B58 59.88(13) . . ?
B62 B57 B61 59.67(13) . . ?
Cl58 B58 B54 118.21(14) . . ?
Cl58 B58 B57 121.83(15) . . ?
Cl58 B58 B59 121.40(16) . . ?
Cl58 B58 B62 122.43(16) . . ?
B53 B58 Cl58 118.16(15) . . ?
B53 B58 B54 66.55(14) . . ?
B53 B58 B57 59.34(13) . . ?
B53 B58 B59 112.49(17) . . ?
B53 B58 B62 109.20(16) . . ?
B54 B58 B57 112.07(17) . . ?
B54 B58 B59 59.46(13) . . ?
B54 B58 B62 109.21(16) . . ?
B57 B58 B59 108.08(16) . . ?
B62 B58 B57 59.59(13) . . ?
B62 B58 B59 59.81(13) . . ?
Cl59 B59 B54 118.76(15) . . ?
Cl59 B59 B55 118.89(16) . . ?
Cl59 B59 B58 121.84(16) . . ?
Cl59 B59 B60 121.73(15) . . ?
Cl59 B59 B62 122.34(16) . . ?
B54 B59 B58 59.13(13) . . ?
B54 B59 B60 111.78(17) . . ?
B54 B59 B62 108.83(16) . . ?
B55 B59 B54 65.95(14) . . ?
B55 B59 B58 111.41(17) . . ?
B55 B59 B60 59.43(13) . . ?
B55 B59 B62 108.76(16) . . ?
B60 B59 B58 107.68(16) . . ?
B62 B59 B58 59.67(13) . . ?
B62 B59 B60 59.47(13) . . ?
Cl60 B60 B55 119.30(16) . . ?
Cl60 B60 B56 118.92(16) . . ?
Cl60 B60 B59 121.32(16) . . ?
Cl60 B60 B61 121.10(15) . . ?
Cl60 B60 B62 121.50(16) . . ?
B55 B60 B59 59.29(13) . . ?
B55 B60 B61 111.98(17) . . ?
B55 B60 B62 109.11(16) . . ?
B56 B60 B55 66.20(14) . . ?
B56 B60 B59 112.18(16) . . ?
B56 B60 B61 59.37(14) . . ?
B56 B60 B62 109.09(17) . . ?
B59 B60 B61 108.42(16) . . ?
B62 B60 B59 60.03(13) . . ?
B62 B60 B61 59.70(13) . . ?
Cl61 B61 B52 118.85(16) . . ?
Cl61 B61 B56 119.08(15) . . ?
Cl61 B61 B57 121.58(16) . . ?
Cl61 B61 B60 121.77(16) . . ?
Cl61 B61 B62 121.87(16) . . ?
B52 B61 B57 59.13(14) . . ?
B52 B61 B60 111.87(16) . . ?
B52 B61 B62 108.95(16) . . ?
B56 B61 B52 66.29(14) . . ?
B56 B61 B57 111.67(16) . . ?
B56 B61 B60 59.28(14) . . ?
B56 B61 B62 108.91(16) . . ?
B57 B61 B60 107.68(16) . . ?
B62 B61 B57 59.67(13) . . ?
B62 B61 B60 59.57(13) . . ?
Cl62 B62 B57 120.79(16) . . ?
Cl62 B62 B58 121.08(16) . . ?
Cl62 B62 B59 121.00(16) . . ?
Cl62 B62 B60 120.99(15) . . ?
Cl62 B62 B61 120.56(15) . . ?
B57 B62 B58 60.54(13) . . ?
B57 B62 B59 109.41(16) . . ?
B57 B62 B61 60.67(13) . . ?
B58 B62 B59 60.52(13) . . ?
B60 B62 B57 109.40(17) . . ?
B60 B62 B58 109.17(16) . . ?
B60 B62 B59 60.50(13) . . ?
B60 B62 B61 60.73(14) . . ?
B61 B62 B58 109.47(16) . . ?
B61 B62 B59 109.61(17) . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Se1 B2 B7 Cl7 145.22(14) . . . . ?
Se1 B2 B7 B3 34.01(14) . . . . ?
Se1 B2 B7 B8 -5.0(2) . . . . ?
Se1 B2 B7 B11 -103.52(15) . . . . ?
Se1 B2 B7 B12 -69.33(19) . . . . ?
Se1 B2 B11 Cl11 -144.94(13) . . . . ?
Se1 B2 B11 B6 -33.55(14) . . . . ?
Se1 B2 B11 B7 103.42(15) . . . . ?
Se1 B2 B11 B10 5.3(2) . . . . ?
Se1 B2 B11 B12 69.15(18) . . . . ?
Se1 B3 B7 Cl7 -144.94(13) . . . . ?
Se1 B3 B7 B2 -33.75(13) . . . . ?
Se1 B3 B7 B8 103.67(15) . . . . ?
Se1 B3 B7 B11 5.1(2) . . . . ?
Se1 B3 B7 B12 69.17(19) . . . . ?
Se1 B3 B8 Cl8 145.81(13) . . . . ?
Se1 B3 B8 B4 34.01(14) . . . . ?
Se1 B3 B8 B7 -102.93(16) . . . . ?
Se1 B3 B8 B9 -4.6(2) . . . . ?
Se1 B3 B8 B12 -68.57(18) . . . . ?
Se1 B4 B8 Cl8 -145.60(14) . . . . ?
Se1 B4 B8 B3 -34.11(14) . . . . ?
Se1 B4 B8 B7 5.0(2) . . . . ?
Se1 B4 B8 B9 103.51(16) . . . . ?
Se1 B4 B8 B12 68.85(19) . . . . ?
Se1 B4 B9 Cl9 144.60(13) . . . . ?
Se1 B4 B9 B5 34.02(13) . . . . ?
Se1 B4 B9 B8 -103.49(15) . . . . ?
Se1 B4 B9 B10 -4.6(2) . . . . ?
Se1 B4 B9 B12 -68.65(19) . . . . ?
Se1 B5 B9 Cl9 -144.30(14) . . . . ?
Se1 B5 B9 B4 -34.18(13) . . . . ?
Se1 B5 B9 B8 4.7(2) . . . . ?
Se1 B5 B9 B10 103.70(15) . . . . ?
Se1 B5 B9 B12 68.93(19) . . . . ?
Se1 B5 B10 Cl10 144.82(14) . . . . ?
Se1 B5 B10 B6 33.78(14) . . . . ?
Se1 B5 B10 B9 -103.73(16) . . . . ?
Se1 B5 B10 B11 -5.0(2) . . . . ?
Se1 B5 B10 B12 -68.84(19) . . . . ?
Se1 B6 B10 Cl10 -144.96(13) . . . . ?
Se1 B6 B10 B5 -33.73(14) . . . . ?
Se1 B6 B10 B9 5.0(2) . . . . ?
Se1 B6 B10 B11 103.41(16) . . . . ?
Se1 B6 B10 B12 69.15(19) . . . . ?
Se1 B6 B11 Cl11 144.47(13) . . . . ?
Se1 B6 B11 B2 33.51(14) . . . . ?
Se1 B6 B11 B7 -5.7(2) . . . . ?
Se1 B6 B11 B10 -103.86(16) . . . . ?
Se1 B6 B11 B12 -69.66(19) . . . . ?
Cl2 B2 B7 Cl7 3.5(3) . . . . ?
Cl2 B2 B7 B3 -107.8(2) . . . . ?
Cl2 B2 B7 B8 -146.81(18) . . . . ?
Cl2 B2 B7 B11 114.7(2) . . . . ?
Cl2 B2 B7 B12 148.90(18) . . . . ?
Cl2 B2 B11 Cl11 -2.4(3) . . . . ?
Cl2 B2 B11 B6 109.0(2) . . . . ?
Cl2 B2 B11 B7 -114.0(2) . . . . ?
Cl2 B2 B11 B10 147.93(17) . . . . ?
Cl2 B2 B11 B12 -148.27(17) . . . . ?
Cl3 B3 B7 Cl7 -3.2(3) . . . . ?
Cl3 B3 B7 B2 108.0(2) . . . . ?
Cl3 B3 B7 B8 -114.6(2) . . . . ?
Cl3 B3 B7 B11 146.82(17) . . . . ?
Cl3 B3 B7 B12 -149.13(18) . . . . ?
Cl3 B3 B8 Cl8 3.8(3) . . . . ?
Cl3 B3 B8 B4 -108.0(2) . . . . ?
Cl3 B3 B8 B7 115.1(2) . . . . ?
Cl3 B3 B8 B9 -146.54(17) . . . . ?
Cl3 B3 B8 B12 149.46(17) . . . . ?
Cl4 B4 B8 Cl8 -3.8(3) . . . . ?
Cl4 B4 B8 B3 107.6(2) . . . . ?
Cl4 B4 B8 B7 146.73(18) . . . . ?
Cl4 B4 B8 B9 -114.7(2) . . . . ?
Cl4 B4 B8 B12 -149.39(17) . . . . ?
Cl4 B4 B9 Cl9 3.4(3) . . . . ?
Cl4 B4 B9 B5 -107.1(2) . . . . ?
Cl4 B4 B9 B8 115.4(2) . . . . ?
Cl4 B4 B9 B10 -145.73(17) . . . . ?
Cl4 B4 B9 B12 150.20(17) . . . . ?
Cl5 B5 B9 Cl9 -2.7(3) . . . . ?
Cl5 B5 B9 B4 107.4(2) . . . . ?
Cl5 B5 B9 B8 146.33(17) . . . . ?
Cl5 B5 B9 B10 -114.7(2) . . . . ?
Cl5 B5 B9 B12 -149.48(17) . . . . ?
Cl5 B5 B10 Cl10 3.3(3) . . . . ?
Cl5 B5 B10 B6 -107.7(2) . . . . ?
Cl5 B5 B10 B9 114.8(2) . . . . ?
Cl5 B5 B10 B11 -146.55(18) . . . . ?
Cl5 B5 B10 B12 149.65(17) . . . . ?
Cl6 B6 B10 Cl10 -3.4(3) . . . . ?
Cl6 B6 B10 B5 107.8(2) . . . . ?
Cl6 B6 B10 B9 146.51(17) . . . . ?
Cl6 B6 B10 B11 -115.0(2) . . . . ?
Cl6 B6 B10 B12 -149.30(17) . . . . ?
Cl6 B6 B11 Cl11 2.1(3) . . . . ?
Cl6 B6 B11 B2 -108.8(2) . . . . ?
Cl6 B6 B11 B7 -148.00(17) . . . . ?
Cl6 B6 B11 B10 113.8(2) . . . . ?
Cl6 B6 B11 B12 148.00(18) . . . . ?
Cl7 B7 B8 Cl8 0.6(3) . . . . ?
Cl7 B7 B8 B3 -107.2(2) . . . . ?
Cl7 B7 B8 B4 -149.37(17) . . . . ?
Cl7 B7 B8 B9 147.50(17) . . . . ?
Cl7 B7 B8 B12 111.0(2) . . . . ?
Cl7 B7 B11 Cl11 0.3(3) . . . . ?
Cl7 B7 B11 B2 107.15(19) . . . . ?
Cl7 B7 B11 B6 149.55(17) . . . . ?
Cl7 B7 B11 B10 -147.24(17) . . . . ?
Cl7 B7 B11 B12 -110.9(2) . . . . ?
Cl7 B7 B12 Cl12 0.3(3) . . . . ?
Cl7 B7 B12 B8 -110.3(2) . . . . ?
Cl7 B7 B12 B9 -147.57(17) . . . . ?
Cl7 B7 B12 B10 147.75(17) . . . . ?
Cl7 B7 B12 B11 110.15(19) . . . . ?
Cl8 B8 B9 Cl9 -1.9(3) . . . . ?
Cl8 B8 B9 B4 -108.1(2) . . . . ?
Cl8 B8 B9 B5 -149.82(17) . . . . ?
Cl8 B8 B9 B10 146.49(17) . . . . ?
Cl8 B8 B9 B12 110.5(2) . . . . ?
Cl8 B8 B12 Cl12 2.3(3) . . . . ?
Cl8 B8 B12 B7 110.62(19) . . . . ?
Cl8 B8 B12 B9 -110.36(19) . . . . ?
Cl8 B8 B12 B10 -147.04(16) . . . . ?
Cl8 B8 B12 B11 147.64(16) . . . . ?
Cl9 B9 B10 Cl10 0.9(3) . . . . ?
Cl9 B9 B10 B5 -106.49(19) . . . . ?
Cl9 B9 B10 B6 -148.13(16) . . . . ?
Cl9 B9 B10 B11 148.77(16) . . . . ?
Cl9 B9 B10 B12 112.3(2) . . . . ?
Cl9 B9 B12 Cl12 0.8(3) . . . . ?
Cl9 B9 B12 B7 147.27(17) . . . . ?
Cl9 B9 B12 B8 110.0(2) . . . . ?
Cl9 B9 B12 B10 -110.2(2) . . . . ?
Cl9 B9 B12 B11 -147.82(17) . . . . ?
Cl10 B10 B11 Cl11 0.1(3) . . . . ?
Cl10 B10 B11 B2 -149.17(17) . . . . ?
Cl10 B10 B11 B6 -107.1(2) . . . . ?
Cl10 B10 B11 B7 147.59(17) . . . . ?
Cl10 B10 B11 B12 111.2(2) . . . . ?
Cl10 B10 B12 Cl12 -1.6(3) . . . . ?
Cl10 B10 B12 B7 -148.01(17) . . . . ?
Cl10 B10 B12 B8 147.20(16) . . . . ?
Cl10 B10 B12 B9 110.5(2) . . . . ?
Cl10 B10 B12 B11 -110.5(2) . . . . ?
Cl11 B11 B12 Cl12 -1.7(3) . . . . ?
Cl11 B11 B12 B7 -110.46(19) . . . . ?
Cl11 B11 B12 B8 -147.38(16) . . . . ?
Cl11 B11 B12 B9 147.87(17) . . . . ?
Cl11 B11 B12 B10 110.5(2) . . . . ?
B2 B3 B7 Cl7 -111.20(18) . . . . ?
B2 B3 B7 B8 137.42(16) . . . . ?
B2 B3 B7 B11 38.86(15) . . . . ?
B2 B3 B7 B12 102.92(18) . . . . ?
B2 B3 B8 Cl8 -147.31(15) . . . . ?
B2 B3 B8 B4 100.89(16) . . . . ?
B2 B3 B8 B7 -36.05(14) . . . . ?
B2 B3 B8 B9 62.3(2) . . . . ?
B2 B3 B8 B12 -1.7(2) . . . . ?
B2 B6 B10 Cl10 147.82(15) . . . . ?
B2 B6 B10 B5 -100.94(17) . . . . ?
B2 B6 B10 B9 -62.3(2) . . . . ?
B2 B6 B10 B11 36.20(15) . . . . ?
B2 B6 B10 B12 1.9(2) . . . . ?
B2 B6 B11 Cl11 110.96(19) . . . . ?
B2 B6 B11 B7 -39.17(15) . . . . ?
B2 B6 B11 B10 -137.37(17) . . . . ?
B2 B6 B11 B12 -103.17(18) . . . . ?
B2 B7 B8 Cl8 149.98(18) . . . . ?
B2 B7 B8 B3 42.20(17) . . . . ?
B2 B7 B8 B4 0.0(2) . . . . ?
B2 B7 B8 B9 -63.1(2) . . . . ?
B2 B7 B8 B12 -99.57(19) . . . . ?
B2 B7 B11 Cl11 -106.8(2) . . . . ?
B2 B7 B11 B6 42.40(17) . . . . ?
B2 B7 B11 B10 105.62(18) . . . . ?
B2 B7 B11 B12 141.92(17) . . . . ?
B2 B7 B12 Cl12 -143.98(17) . . . . ?
B2 B7 B12 B8 105.42(18) . . . . ?
B2 B7 B12 B9 68.2(2) . . . . ?
B2 B7 B12 B10 3.5(2) . . . . ?
B2 B7 B12 B11 -34.08(16) . . . . ?
B2 B11 B12 Cl12 142.79(17) . . . . ?
B2 B11 B12 B7 34.08(16) . . . . ?
B2 B11 B12 B8 -2.8(2) . . . . ?
B2 B11 B12 B9 -67.6(2) . . . . ?
B2 B11 B12 B10 -104.97(18) . . . . ?
B3 B2 B7 Cl7 111.21(19) . . . . ?
B3 B2 B7 B8 -39.05(16) . . . . ?
B3 B2 B7 B11 -137.53(16) . . . . ?
B3 B2 B7 B12 -103.34(18) . . . . ?
B3 B2 B11 Cl11 147.61(15) . . . . ?
B3 B2 B11 B6 -101.00(16) . . . . ?
B3 B2 B11 B7 35.98(14) . . . . ?
B3 B2 B11 B10 -62.1(2) . . . . ?
B3 B2 B11 B12 1.7(2) . . . . ?
B3 B4 B8 Cl8 -111.5(2) . . . . ?
B3 B4 B8 B7 39.09(16) . . . . ?
B3 B4 B8 B9 137.62(17) . . . . ?
B3 B4 B8 B12 102.97(18) . . . . ?
B3 B4 B9 Cl9 -147.91(15) . . . . ?
B3 B4 B9 B5 101.50(16) . . . . ?
B3 B4 B9 B8 -36.00(15) . . . . ?
B3 B4 B9 B10 62.9(2) . . . . ?
B3 B4 B9 B12 -1.2(2) . . . . ?
B3 B7 B8 Cl8 107.8(2) . . . . ?
B3 B7 B8 B4 -42.16(17) . . . . ?
B3 B7 B8 B9 -105.30(18) . . . . ?
B3 B7 B8 B12 -141.77(18) . . . . ?
B3 B7 B11 Cl11 -148.92(17) . . . . ?
B3 B7 B11 B2 -42.07(16) . . . . ?
B3 B7 B11 B6 0.3(2) . . . . ?
B3 B7 B11 B10 63.5(2) . . . . ?
B3 B7 B11 B12 99.85(18) . . . . ?
B3 B7 B12 Cl12 144.95(17) . . . . ?
B3 B7 B12 B8 34.35(16) . . . . ?
B3 B7 B12 B9 -2.9(2) . . . . ?
B3 B7 B12 B10 -67.6(2) . . . . ?
B3 B7 B12 B11 -105.16(18) . . . . ?
B3 B8 B9 Cl9 147.84(17) . . . . ?
B3 B8 B9 B4 41.63(17) . . . . ?
B3 B8 B9 B5 -0.1(2) . . . . ?
B3 B8 B9 B10 -63.8(2) . . . . ?
B3 B8 B9 B12 -99.73(19) . . . . ?
B3 B8 B12 Cl12 -142.53(16) . . . . ?
B3 B8 B12 B7 -34.18(16) . . . . ?
B3 B8 B12 B9 104.84(18) . . . . ?
B3 B8 B12 B10 68.2(2) . . . . ?
B3 B8 B12 B11 2.8(2) . . . . ?
B4 B3 B7 Cl7 147.96(15) . . . . ?
B4 B3 B7 B2 -100.84(16) . . . . ?
B4 B3 B7 B8 36.58(15) . . . . ?
B4 B3 B7 B11 -62.0(2) . . . . ?
B4 B3 B7 B12 2.1(2) . . . . ?
B4 B3 B8 Cl8 111.80(19) . . . . ?
B4 B3 B8 B7 -136.95(17) . . . . ?
B4 B3 B8 B9 -38.58(16) . . . . ?
B4 B3 B8 B12 -102.59(18) . . . . ?
B4 B5 B9 Cl9 -110.12(19) . . . . ?
B4 B5 B9 B8 38.90(16) . . . . ?
B4 B5 B9 B10 137.87(16) . . . . ?
B4 B5 B9 B12 103.10(18) . . . . ?
B4 B5 B10 Cl10 -147.42(16) . . . . ?
B4 B5 B10 B6 101.54(17) . . . . ?
B4 B5 B10 B9 -35.98(15) . . . . ?
B4 B5 B10 B11 62.7(2) . . . . ?
B4 B5 B10 B12 -1.1(2) . . . . ?
B4 B8 B9 Cl9 106.2(2) . . . . ?
B4 B8 B9 B5 -41.71(17) . . . . ?
B4 B8 B9 B10 -105.40(19) . . . . ?
B4 B8 B9 B12 -141.35(18) . . . . ?
B4 B8 B12 Cl12 147.09(16) . . . . ?
B4 B8 B12 B7 -104.57(18) . . . . ?
B4 B8 B12 B9 34.46(16) . . . . ?
B4 B8 B12 B10 -2.2(2) . . . . ?
B4 B8 B12 B11 -67.5(2) . . . . ?
B4 B9 B10 Cl10 148.80(17) . . . . ?
B4 B9 B10 B5 41.41(16) . . . . ?
B4 B9 B10 B6 -0.2(2) . . . . ?
B4 B9 B10 B11 -63.3(2) . . . . ?
B4 B9 B10 B12 -99.84(18) . . . . ?
B4 B9 B12 Cl12 -143.99(18) . . . . ?
B4 B9 B12 B7 2.5(2) . . . . ?
B4 B9 B12 B8 -34.73(17) . . . . ?
B4 B9 B12 B10 105.02(19) . . . . ?
B4 B9 B12 B11 67.4(2) . . . . ?
B5 B4 B8 Cl8 147.03(16) . . . . ?
B5 B4 B8 B3 -101.49(17) . . . . ?
B5 B4 B8 B7 -62.4(2) . . . . ?
B5 B4 B8 B9 36.14(15) . . . . ?
B5 B4 B8 B12 1.5(2) . . . . ?
B5 B4 B9 Cl9 110.59(18) . . . . ?
B5 B4 B9 B8 -137.50(17) . . . . ?
B5 B4 B9 B10 -38.59(15) . . . . ?
B5 B4 B9 B12 -102.66(18) . . . . ?
B5 B6 B10 Cl10 -111.24(19) . . . . ?
B5 B6 B10 B9 38.68(15) . . . . ?
B5 B6 B10 B11 137.14(17) . . . . ?
B5 B6 B10 B12 102.88(18) . . . . ?
B5 B6 B11 Cl11 -148.14(15) . . . . ?
B5 B6 B11 B2 100.90(17) . . . . ?
B5 B6 B11 B7 61.7(2) . . . . ?
B5 B6 B11 B10 -36.47(15) . . . . ?
B5 B6 B11 B12 -2.3(2) . . . . ?
B5 B9 B10 Cl10 107.4(2) . . . . ?
B5 B9 B10 B6 -41.64(17) . . . . ?
B5 B9 B10 B11 -104.74(19) . . . . ?
B5 B9 B10 B12 -141.25(17) . . . . ?
B5 B9 B12 Cl12 145.72(18) . . . . ?
B5 B9 B12 B7 -67.8(2) . . . . ?
B5 B9 B12 B8 -105.03(19) . . . . ?
B5 B9 B12 B10 34.72(16) . . . . ?
B5 B9 B12 B11 -2.9(2) . . . . ?
B5 B10 B11 Cl11 149.06(18) . . . . ?
B5 B10 B11 B2 -0.2(3) . . . . ?
B5 B10 B11 B6 41.89(18) . . . . ?
B5 B10 B11 B7 -63.5(2) . . . . ?
B5 B10 B11 B12 -99.89(19) . . . . ?
B5 B10 B12 Cl12 -146.74(17) . . . . ?
B5 B10 B12 B7 66.8(2) . . . . ?
B5 B10 B12 B8 2.1(2) . . . . ?
B5 B10 B12 B9 -34.63(16) . . . . ?
B5 B10 B12 B11 104.32(19) . . . . ?
B6 B2 B7 Cl7 -147.64(16) . . . . ?
B6 B2 B7 B3 101.15(16) . . . . ?
B6 B2 B7 B8 62.1(2) . . . . ?
B6 B2 B7 B11 -36.38(15) . . . . ?
B6 B2 B7 B12 -2.2(2) . . . . ?
B6 B2 B11 Cl11 -111.4(2) . . . . ?
B6 B2 B11 B7 136.97(16) . . . . ?
B6 B2 B11 B10 38.90(16) . . . . ?
B6 B2 B11 B12 102.70(17) . . . . ?
B6 B5 B9 Cl9 148.19(16) . . . . ?
B6 B5 B9 B4 -101.68(16) . . . . ?
B6 B5 B9 B8 -62.8(2) . . . . ?
B6 B5 B9 B10 36.19(15) . . . . ?
B6 B5 B9 B12 1.4(2) . . . . ?
B6 B5 B10 Cl10 111.0(2) . . . . ?
B6 B5 B10 B9 -137.52(17) . . . . ?
B6 B5 B10 B11 -38.82(16) . . . . ?
B6 B5 B10 B12 -102.62(18) . . . . ?
B6 B10 B11 Cl11 107.2(2) . . . . ?
B6 B10 B11 B2 -42.09(17) . . . . ?
B6 B10 B11 B7 -105.34(19) . . . . ?
B6 B10 B11 B12 -141.78(18) . . . . ?
B6 B10 B12 Cl12 143.02(17) . . . . ?
B6 B10 B12 B7 -3.4(2) . . . . ?
B6 B10 B12 B8 -68.2(2) . . . . ?
B6 B10 B12 B9 -104.87(19) . . . . ?
B6 B10 B12 B11 34.08(16) . . . . ?
B6 B11 B12 Cl12 -146.38(17) . . . . ?
B6 B11 B12 B7 104.92(19) . . . . ?
B6 B11 B12 B8 68.0(2) . . . . ?
B6 B11 B12 B9 3.2(2) . . . . ?
B6 B11 B12 B10 -34.14(17) . . . . ?
B7 B2 B11 Cl11 111.63(18) . . . . ?
B7 B2 B11 B6 -136.97(16) . . . . ?
B7 B2 B11 B10 -98.08(19) . . . . ?
B7 B2 B11 B12 -34.27(16) . . . . ?
B7 B3 B8 Cl8 -111.26(18) . . . . ?
B7 B3 B8 B4 136.95(17) . . . . ?
B7 B3 B8 B9 98.36(19) . . . . ?
B7 B3 B8 B12 34.36(16) . . . . ?
B7 B8 B9 Cl9 -148.91(17) . . . . ?
B7 B8 B9 B4 104.88(19) . . . . ?
B7 B8 B9 B5 63.2(2) . . . . ?
B7 B8 B9 B10 -0.5(2) . . . . ?
B7 B8 B9 B12 -36.48(16) . . . . ?
B7 B8 B12 Cl12 -108.35(19) . . . . ?
B7 B8 B12 B9 139.03(18) . . . . ?
B7 B8 B12 B10 102.35(18) . . . . ?
B7 B8 B12 B11 37.02(16) . . . . ?
B7 B11 B12 Cl12 108.71(19) . . . . ?
B7 B11 B12 B8 -36.92(16) . . . . ?
B7 B11 B12 B9 -101.67(19) . . . . ?
B7 B11 B12 B10 -139.05(18) . . . . ?
B8 B3 B7 Cl7 111.39(19) . . . . ?
B8 B3 B7 B2 -137.42(16) . . . . ?
B8 B3 B7 B11 -98.56(18) . . . . ?
B8 B3 B7 B12 -34.50(16) . . . . ?
B8 B4 B9 Cl9 -111.91(19) . . . . ?
B8 B4 B9 B5 137.50(17) . . . . ?
B8 B4 B9 B10 98.91(18) . . . . ?
B8 B4 B9 B12 34.84(16) . . . . ?
B8 B7 B11 Cl11 147.44(17) . . . . ?
B8 B7 B11 B2 -105.72(18) . . . . ?
B8 B7 B11 B6 -63.3(2) . . . . ?
B8 B7 B11 B10 -0.1(2) . . . . ?
B8 B7 B11 B12 36.21(16) . . . . ?
B8 B7 B12 Cl12 110.6(2) . . . . ?
B8 B7 B12 B9 -37.23(17) . . . . ?
B8 B7 B12 B10 -101.91(18) . . . . ?
B8 B7 B12 B11 -139.51(17) . . . . ?
B8 B9 B10 Cl10 -147.41(17) . . . . ?
B8 B9 B10 B5 105.21(19) . . . . ?
B8 B9 B10 B6 63.6(2) . . . . ?
B8 B9 B10 B11 0.5(2) . . . . ?
B8 B9 B10 B12 -36.05(16) . . . . ?
B8 B9 B12 Cl12 -109.3(2) . . . . ?
B8 B9 B12 B7 37.23(17) . . . . ?
B8 B9 B12 B10 139.75(18) . . . . ?
B8 B9 B12 B11 102.13(19) . . . . ?
B9 B4 B8 Cl8 110.89(19) . . . . ?
B9 B4 B8 B3 -137.62(17) . . . . ?
B9 B4 B8 B7 -98.54(19) . . . . ?
B9 B4 B8 B12 -34.66(16) . . . . ?
B9 B5 B10 Cl10 -111.44(19) . . . . ?
B9 B5 B10 B6 137.52(17) . . . . ?
B9 B5 B10 B11 98.70(19) . . . . ?
B9 B5 B10 B12 34.90(16) . . . . ?
B9 B8 B12 Cl12 112.63(19) . . . . ?
B9 B8 B12 B7 -139.03(18) . . . . ?
B9 B8 B12 B10 -36.68(16) . . . . ?
B9 B8 B12 B11 -102.00(18) . . . . ?
B9 B10 B11 Cl11 -147.71(17) . . . . ?
B9 B10 B11 B2 63.0(2) . . . . ?
B9 B10 B11 B6 105.12(19) . . . . ?
B9 B10 B11 B7 -0.2(2) . . . . ?
B9 B10 B11 B12 -36.66(17) . . . . ?
B9 B10 B12 Cl12 -112.1(2) . . . . ?
B9 B10 B12 B7 101.48(19) . . . . ?
B9 B10 B12 B8 36.69(16) . . . . ?
B9 B10 B12 B11 138.95(18) . . . . ?
B10 B5 B9 Cl9 112.00(19) . . . . ?
B10 B5 B9 B4 -137.87(16) . . . . ?
B10 B5 B9 B8 -98.97(18) . . . . ?
B10 B5 B9 B12 -34.77(16) . . . . ?
B10 B6 B11 Cl11 -111.67(19) . . . . ?
B10 B6 B11 B2 137.37(17) . . . . ?
B10 B6 B11 B7 98.21(18) . . . . ?
B10 B6 B11 B12 34.20(17) . . . . ?
B10 B9 B12 Cl12 111.0(2) . . . . ?
B10 B9 B12 B7 -102.52(19) . . . . ?
B10 B9 B12 B8 -139.75(18) . . . . ?
B10 B9 B12 B11 -37.62(17) . . . . ?
B10 B11 B12 Cl12 -112.2(2) . . . . ?
B10 B11 B12 B7 139.05(18) . . . . ?
B10 B11 B12 B8 102.13(18) . . . . ?
B10 B11 B12 B9 37.38(17) . . . . ?
B11 B2 B7 Cl7 -111.26(19) . . . . ?
B11 B2 B7 B3 137.53(16) . . . . ?
B11 B2 B7 B8 98.48(18) . . . . ?
B11 B2 B7 B12 34.19(16) . . . . ?
B11 B6 B10 Cl10 111.63(19) . . . . ?
B11 B6 B10 B5 -137.14(17) . . . . ?
B11 B6 B10 B9 -98.46(18) . . . . ?
B11 B6 B10 B12 -34.26(16) . . . . ?
B11 B7 B8 Cl8 -146.55(17) . . . . ?
B11 B7 B8 B3 105.68(18) . . . . ?
B11 B7 B8 B4 63.5(2) . . . . ?
B11 B7 B8 B9 0.4(2) . . . . ?
B11 B7 B8 B12 -36.09(16) . . . . ?
B11 B7 B12 Cl12 -109.9(2) . . . . ?
B11 B7 B12 B8 139.51(17) . . . . ?
B11 B7 B12 B9 102.28(19) . . . . ?
B11 B7 B12 B10 37.60(16) . . . . ?
B11 B10 B12 Cl12 108.9(2) . . . . ?
B11 B10 B12 B7 -37.47(16) . . . . ?
B11 B10 B12 B8 -102.26(18) . . . . ?
B11 B10 B12 B9 -138.95(18) . . . . ?
B12 B7 B8 Cl8 -110.5(2) . . . . ?
B12 B7 B8 B3 141.77(18) . . . . ?
B12 B7 B8 B4 99.61(19) . . . . ?
B12 B7 B8 B9 36.47(16) . . . . ?
B12 B7 B11 Cl11 111.2(2) . . . . ?
B12 B7 B11 B2 -141.92(17) . . . . ?
B12 B7 B11 B6 -99.52(19) . . . . ?
B12 B7 B11 B10 -36.31(16) . . . . ?
B12 B8 B9 Cl9 -112.4(2) . . . . ?
B12 B8 B9 B4 141.35(18) . . . . ?
B12 B8 B9 B5 99.64(19) . . . . ?
B12 B8 B9 B10 35.95(17) . . . . ?
B12 B9 B10 Cl10 -111.4(2) . . . . ?
B12 B9 B10 B5 141.25(17) . . . . ?
B12 B9 B10 B6 99.61(19) . . . . ?
B12 B9 B10 B11 36.51(16) . . . . ?
B12 B10 B11 Cl11 -111.0(2) . . . . ?
B12 B10 B11 B2 99.68(19) . . . . ?
B12 B10 B11 B6 141.78(18) . . . . ?
B12 B10 B11 B7 36.44(17) . . . . ?
Se51 B52 B57 Cl57 145.45(12) . . . . ?
Se51 B52 B57 B53 34.15(14) . . . . ?
Se51 B52 B57 B58 -4.7(2) . . . . ?
Se51 B52 B57 B61 -103.45(15) . . . . ?
Se51 B52 B57 B62 -69.18(18) . . . . ?
Se51 B52 B61 Cl61 -145.18(13) . . . . ?
Se51 B52 B61 B56 -33.82(14) . . . . ?
Se51 B52 B61 B57 103.27(15) . . . . ?
Se51 B52 B61 B60 5.1(2) . . . . ?
Se51 B52 B61 B62 69.09(19) . . . . ?
Se51 B53 B57 Cl57 -144.42(13) . . . . ?
Se51 B53 B57 B52 -33.92(14) . . . . ?
Se51 B53 B57 B58 103.46(15) . . . . ?
Se51 B53 B57 B61 5.1(2) . . . . ?
Se51 B53 B57 B62 69.37(19) . . . . ?
Se51 B53 B58 Cl58 144.80(12) . . . . ?
Se51 B53 B58 B54 34.17(13) . . . . ?
Se51 B53 B58 B57 -102.99(15) . . . . ?
Se51 B53 B58 B59 -4.7(2) . . . . ?
Se51 B53 B58 B62 -69.05(18) . . . . ?
Se51 B54 B58 Cl58 -144.63(13) . . . . ?
Se51 B54 B58 B53 -34.09(13) . . . . ?
Se51 B54 B58 B57 5.0(2) . . . . ?
Se51 B54 B58 B59 103.65(15) . . . . ?
Se51 B54 B58 B62 69.12(18) . . . . ?
Se51 B54 B59 Cl59 145.10(13) . . . . ?
Se51 B54 B59 B55 34.08(14) . . . . ?
Se51 B54 B59 B58 -103.01(15) . . . . ?
Se51 B54 B59 B60 -4.8(2) . . . . ?
Se51 B54 B59 B62 -68.62(18) . . . . ?
Se51 B55 B59 Cl59 -145.04(13) . . . . ?
Se51 B55 B59 B54 -34.21(13) . . . . ?
Se51 B55 B59 B58 4.7(2) . . . . ?
Se51 B55 B59 B60 103.14(15) . . . . ?
Se51 B55 B59 B62 68.60(17) . . . . ?
Se51 B55 B60 Cl60 145.05(13) . . . . ?
Se51 B55 B60 B56 34.03(14) . . . . ?
Se51 B55 B60 B59 -103.86(15) . . . . ?
Se51 B55 B60 B61 -4.8(2) . . . . ?
Se51 B55 B60 B62 -69.00(19) . . . . ?
Se51 B56 B60 Cl60 -145.66(13) . . . . ?
Se51 B56 B60 B55 -34.11(14) . . . . ?
Se51 B56 B60 B59 4.4(2) . . . . ?
Se51 B56 B60 B61 103.32(16) . . . . ?
Se51 B56 B60 B62 68.95(18) . . . . ?
Se51 B56 B61 Cl61 144.73(14) . . . . ?
Se51 B56 B61 B52 33.71(14) . . . . ?
Se51 B56 B61 B57 -5.3(2) . . . . ?
Se51 B56 B61 B60 -103.53(15) . . . . ?
Se51 B56 B61 B62 -69.26(19) . . . . ?
Cl52 B52 B57 Cl57 4.3(3) . . . . ?
Cl52 B52 B57 B53 -106.97(19) . . . . ?
Cl52 B52 B57 B58 -145.86(17) . . . . ?
Cl52 B52 B57 B61 115.4(2) . . . . ?
Cl52 B52 B57 B62 149.70(16) . . . . ?
Cl52 B52 B61 Cl61 -2.6(3) . . . . ?
Cl52 B52 B61 B56 108.8(2) . . . . ?
Cl52 B52 B61 B57 -114.1(2) . . . . ?
Cl52 B52 B61 B60 147.76(17) . . . . ?
Cl52 B52 B61 B62 -148.29(17) . . . . ?
Cl53 B53 B57 Cl57 -2.3(3) . . . . ?
Cl53 B53 B57 B52 108.2(2) . . . . ?
Cl53 B53 B57 B58 -114.5(2) . . . . ?
Cl53 B53 B57 B61 147.17(17) . . . . ?
Cl53 B53 B57 B62 -148.55(17) . . . . ?
Cl53 B53 B58 Cl58 2.7(3) . . . . ?
Cl53 B53 B58 B54 -107.96(19) . . . . ?
Cl53 B53 B58 B57 114.9(2) . . . . ?
Cl53 B53 B58 B59 -146.79(17) . . . . ?
Cl53 B53 B58 B62 148.82(17) . . . . ?
Cl54 B54 B58 Cl58 -3.1(3) . . . . ?
Cl54 B54 B58 B53 107.4(2) . . . . ?
Cl54 B54 B58 B57 146.55(17) . . . . ?
Cl54 B54 B58 B59 -114.9(2) . . . . ?
Cl54 B54 B58 B62 -149.38(17) . . . . ?
Cl54 B54 B59 Cl59 2.7(3) . . . . ?
Cl54 B54 B59 B55 -108.4(2) . . . . ?
Cl54 B54 B59 B58 114.5(2) . . . . ?
Cl54 B54 B59 B60 -147.28(17) . . . . ?
Cl54 B54 B59 B62 148.93(17) . . . . ?
Cl55 B55 B59 Cl59 -4.1(3) . . . . ?
Cl55 B55 B59 B54 106.74(19) . . . . ?
Cl55 B55 B59 B58 145.63(16) . . . . ?
Cl55 B55 B59 B60 -115.9(2) . . . . ?
Cl55 B55 B59 B62 -150.45(16) . . . . ?
Cl55 B55 B60 Cl60 4.4(3) . . . . ?
Cl55 B55 B60 B56 -106.6(2) . . . . ?
Cl55 B55 B60 B59 115.5(2) . . . . ?
Cl55 B55 B60 B61 -145.52(17) . . . . ?
Cl55 B55 B60 B62 150.33(17) . . . . ?
Cl56 B56 B60 Cl60 -4.6(3) . . . . ?
Cl56 B56 B60 B55 106.9(2) . . . . ?
Cl56 B56 B60 B59 145.43(17) . . . . ?
Cl56 B56 B60 B61 -115.6(2) . . . . ?
Cl56 B56 B60 B62 -150.02(17) . . . . ?
Cl56 B56 B61 Cl61 3.4(3) . . . . ?
Cl56 B56 B61 B52 -107.6(2) . . . . ?
Cl56 B56 B61 B57 -146.56(18) . . . . ?
Cl56 B56 B61 B60 115.2(2) . . . . ?
Cl56 B56 B61 B62 149.43(17) . . . . ?
Cl57 B57 B58 Cl58 -0.7(3) . . . . ?
Cl57 B57 B58 B53 -106.82(19) . . . . ?
Cl57 B57 B58 B54 -149.13(16) . . . . ?
Cl57 B57 B58 B59 147.26(16) . . . . ?
Cl57 B57 B58 B62 110.87(19) . . . . ?
Cl57 B57 B61 Cl61 -0.2(3) . . . . ?
Cl57 B57 B61 B52 106.78(19) . . . . ?
Cl57 B57 B61 B56 148.90(17) . . . . ?
Cl57 B57 B61 B60 -147.86(16) . . . . ?
Cl57 B57 B61 B62 -111.2(2) . . . . ?
Cl57 B57 B62 Cl62 -0.5(3) . . . . ?
Cl57 B57 B62 B58 -111.18(19) . . . . ?
Cl57 B57 B62 B59 -148.21(16) . . . . ?
Cl57 B57 B62 B60 147.23(16) . . . . ?
Cl57 B57 B62 B61 109.66(18) . . . . ?
Cl58 B58 B59 Cl59 0.3(3) . . . . ?
Cl58 B58 B59 B54 -106.44(18) . . . . ?
Cl58 B58 B59 B55 -148.34(16) . . . . ?
Cl58 B58 B59 B60 148.30(16) . . . . ?
Cl58 B58 B59 B62 111.83(19) . . . . ?
Cl58 B58 B62 Cl62 0.3(3) . . . . ?
Cl58 B58 B62 B57 110.58(19) . . . . ?
Cl58 B58 B62 B59 -110.15(19) . . . . ?
Cl58 B58 B62 B60 -147.45(16) . . . . ?
Cl58 B58 B62 B61 147.78(16) . . . . ?
Cl59 B59 B60 Cl60 0.6(3) . . . . ?
Cl59 B59 B60 B55 -107.13(19) . . . . ?
Cl59 B59 B60 B56 -148.62(17) . . . . ?
Cl59 B59 B60 B61 147.75(17) . . . . ?
Cl59 B59 B60 B62 111.4(2) . . . . ?
Cl59 B59 B62 Cl62 0.1(3) . . . . ?
Cl59 B59 B62 B57 147.71(16) . . . . ?
Cl59 B59 B62 B58 110.7(2) . . . . ?
Cl59 B59 B62 B60 -110.44(19) . . . . ?
Cl59 B59 B62 B61 -147.50(16) . . . . ?
Cl60 B60 B61 Cl61 -0.1(3) . . . . ?
Cl60 B60 B61 B52 -149.46(17) . . . . ?
Cl60 B60 B61 B56 -107.4(2) . . . . ?
Cl60 B60 B61 B57 147.43(17) . . . . ?
Cl60 B60 B61 B62 110.75(19) . . . . ?
Cl60 B60 B62 Cl62 0.0(3) . . . . ?
Cl60 B60 B62 B57 -147.64(16) . . . . ?
Cl60 B60 B62 B58 147.81(16) . . . . ?
Cl60 B60 B62 B59 110.51(19) . . . . ?
Cl60 B60 B62 B61 -110.09(18) . . . . ?
Cl61 B61 B62 Cl62 0.0(3) . . . . ?
Cl61 B61 B62 B57 -110.53(19) . . . . ?
Cl61 B61 B62 B58 -147.67(16) . . . . ?
Cl61 B61 B62 B59 147.68(16) . . . . ?
Cl61 B61 B62 B60 110.72(19) . . . . ?
B52 B53 B57 Cl57 -110.49(19) . . . . ?
B52 B53 B57 B58 137.38(17) . . . . ?
B52 B53 B57 B61 39.01(16) . . . . ?
B52 B53 B57 B62 103.29(18) . . . . ?
B52 B53 B58 Cl58 -148.32(15) . . . . ?
B52 B53 B58 B54 101.05(16) . . . . ?
B52 B53 B58 B57 -36.11(15) . . . . ?
B52 B53 B58 B59 62.2(2) . . . . ?
B52 B53 B58 B62 -2.2(2) . . . . ?
B52 B56 B60 Cl60 147.37(15) . . . . ?
B52 B56 B60 B55 -101.08(16) . . . . ?
B52 B56 B60 B59 -62.6(2) . . . . ?
B52 B56 B60 B61 36.35(14) . . . . ?
B52 B56 B60 B62 2.0(2) . . . . ?
B52 B56 B61 Cl61 111.02(19) . . . . ?
B52 B56 B61 B57 -38.96(16) . . . . ?
B52 B56 B61 B60 -137.24(16) . . . . ?
B52 B56 B61 B62 -102.97(17) . . . . ?
B52 B57 B58 Cl58 148.22(16) . . . . ?
B52 B57 B58 B53 42.09(17) . . . . ?
B52 B57 B58 B54 -0.2(2) . . . . ?
B52 B57 B58 B59 -63.8(2) . . . . ?
B52 B57 B58 B62 -100.22(18) . . . . ?
B52 B57 B61 Cl61 -107.0(2) . . . . ?
B52 B57 B61 B56 42.12(17) . . . . ?
B52 B57 B61 B60 105.36(18) . . . . ?
B52 B57 B61 B62 142.00(17) . . . . ?
B52 B57 B62 Cl62 -144.37(16) . . . . ?
B52 B57 B62 B58 104.92(18) . . . . ?
B52 B57 B62 B59 67.9(2) . . . . ?
B52 B57 B62 B60 3.3(2) . . . . ?
B52 B57 B62 B61 -34.24(15) . . . . ?
B52 B61 B62 Cl62 144.46(16) . . . . ?
B52 B61 B62 B57 33.97(16) . . . . ?
B52 B61 B62 B58 -3.2(2) . . . . ?
B52 B61 B62 B59 -67.8(2) . . . . ?
B52 B61 B62 B60 -104.78(18) . . . . ?
B53 B52 B57 Cl57 111.30(18) . . . . ?
B53 B52 B57 B58 -38.90(15) . . . . ?
B53 B52 B57 B61 -137.60(17) . . . . ?
B53 B52 B57 B62 -103.33(17) . . . . ?
B53 B52 B61 Cl61 147.49(16) . . . . ?
B53 B52 B61 B56 -101.16(16) . . . . ?
B53 B52 B61 B57 35.94(15) . . . . ?
B53 B52 B61 B60 -62.2(2) . . . . ?
B53 B52 B61 B62 1.8(2) . . . . ?
B53 B54 B58 Cl58 -110.55(18) . . . . ?
B53 B54 B58 B57 39.13(15) . . . . ?
B53 B54 B58 B59 137.74(16) . . . . ?
B53 B54 B58 B62 103.21(17) . . . . ?
B53 B54 B59 Cl59 -147.73(15) . . . . ?
B53 B54 B59 B55 101.26(16) . . . . ?
B53 B54 B59 B58 -35.83(15) . . . . ?
B53 B54 B59 B60 62.3(2) . . . . ?
B53 B54 B59 B62 -1.4(2) . . . . ?
B53 B57 B58 Cl58 106.12(19) . . . . ?
B53 B57 B58 B54 -42.31(16) . . . . ?
B53 B57 B58 B59 -105.92(18) . . . . ?
B53 B57 B58 B62 -142.31(18) . . . . ?
B53 B57 B61 Cl61 -149.03(17) . . . . ?
B53 B57 B61 B52 -42.03(17) . . . . ?
B53 B57 B61 B56 0.1(2) . . . . ?
B53 B57 B61 B60 63.3(2) . . . . ?
B53 B57 B61 B62 99.97(18) . . . . ?
B53 B57 B62 Cl62 144.54(16) . . . . ?
B53 B57 B62 B58 33.83(16) . . . . ?
B53 B57 B62 B59 -3.2(2) . . . . ?
B53 B57 B62 B60 -67.8(2) . . . . ?
B53 B57 B62 B61 -105.33(18) . . . . ?
B53 B58 B59 Cl59 148.68(16) . . . . ?
B53 B58 B59 B54 41.90(16) . . . . ?
B53 B58 B59 B55 0.0(2) . . . . ?
B53 B58 B59 B60 -63.4(2) . . . . ?
B53 B58 B59 B62 -99.84(18) . . . . ?
B53 B58 B62 Cl62 -144.08(16) . . . . ?
B53 B58 B62 B57 -33.84(16) . . . . ?
B53 B58 B62 B59 105.43(19) . . . . ?
B53 B58 B62 B60 68.1(2) . . . . ?
B53 B58 B62 B61 3.4(2) . . . . ?
B54 B53 B57 Cl57 148.42(15) . . . . ?
B54 B53 B57 B52 -101.09(17) . . . . ?
B54 B53 B57 B58 36.29(15) . . . . ?
B54 B53 B57 B61 -62.1(2) . . . . ?
B54 B53 B57 B62 2.2(2) . . . . ?
B54 B53 B58 Cl58 110.63(17) . . . . ?
B54 B53 B58 B57 -137.16(16) . . . . ?
B54 B53 B58 B59 -38.82(15) . . . . ?
B54 B53 B58 B62 -103.22(17) . . . . ?
B54 B55 B59 Cl59 -110.83(18) . . . . ?
B54 B55 B59 B58 38.88(15) . . . . ?
B54 B55 B59 B60 137.35(17) . . . . ?
B54 B55 B59 B62 102.81(17) . . . . ?
B54 B55 B60 Cl60 -147.47(16) . . . . ?
B54 B55 B60 B56 101.51(17) . . . . ?
B54 B55 B60 B59 -36.38(15) . . . . ?
B54 B55 B60 B61 62.6(2) . . . . ?
B54 B55 B60 B62 -1.5(2) . . . . ?
B54 B58 B59 Cl59 106.78(19) . . . . ?
B54 B58 B59 B55 -41.90(16) . . . . ?
B54 B58 B59 B60 -105.26(18) . . . . ?
B54 B58 B59 B62 -141.74(17) . . . . ?
B54 B58 B62 Cl62 144.88(16) . . . . ?
B54 B58 B62 B57 -104.88(18) . . . . ?
B54 B58 B62 B59 34.39(16) . . . . ?
B54 B58 B62 B60 -2.9(2) . . . . ?
B54 B58 B62 B61 -67.7(2) . . . . ?
B54 B59 B60 Cl60 149.53(16) . . . . ?
B54 B59 B60 B55 41.78(17) . . . . ?
B54 B59 B60 B56 0.3(2) . . . . ?
B54 B59 B60 B61 -63.3(2) . . . . ?
B54 B59 B60 B62 -99.66(18) . . . . ?
B54 B59 B62 Cl62 -144.78(16) . . . . ?
B54 B59 B62 B57 2.9(2) . . . . ?
B54 B59 B62 B58 -34.17(16) . . . . ?
B54 B59 B62 B60 104.72(18) . . . . ?
B54 B59 B62 B61 67.7(2) . . . . ?
B55 B54 B58 Cl58 148.13(15) . . . . ?
B55 B54 B58 B53 -101.32(16) . . . . ?
B55 B54 B58 B57 -62.2(2) . . . . ?
B55 B54 B58 B59 36.41(15) . . . . ?
B55 B54 B58 B62 1.9(2) . . . . ?
B55 B54 B59 Cl59 111.01(19) . . . . ?
B55 B54 B59 B58 -137.09(16) . . . . ?
B55 B54 B59 B60 -38.92(16) . . . . ?
B55 B54 B59 B62 -102.70(18) . . . . ?
B55 B56 B60 Cl60 -111.55(18) . . . . ?
B55 B56 B60 B59 38.51(16) . . . . ?
B55 B56 B60 B61 137.43(16) . . . . ?
B55 B56 B60 B62 103.06(17) . . . . ?
B55 B56 B61 Cl61 -147.93(15) . . . . ?
B55 B56 B61 B52 101.05(16) . . . . ?
B55 B56 B61 B57 62.1(2) . . . . ?
B55 B56 B61 B60 -36.20(14) . . . . ?
B55 B56 B61 B62 -1.9(2) . . . . ?
B55 B59 B60 Cl60 107.75(19) . . . . ?
B55 B59 B60 B56 -41.50(17) . . . . ?
B55 B59 B60 B61 -105.13(19) . . . . ?
B55 B59 B60 B62 -141.44(17) . . . . ?
B55 B59 B62 Cl62 145.02(16) . . . . ?
B55 B59 B62 B57 -67.3(2) . . . . ?
B55 B59 B62 B58 -104.36(18) . . . . ?
B55 B59 B62 B60 34.53(16) . . . . ?
B55 B59 B62 B61 -2.5(2) . . . . ?
B55 B60 B61 Cl61 149.15(17) . . . . ?
B55 B60 B61 B52 -0.2(2) . . . . ?
B55 B60 B61 B56 41.87(17) . . . . ?
B55 B60 B61 B57 -63.3(2) . . . . ?
B55 B60 B61 B62 -99.97(18) . . . . ?
B55 B60 B62 Cl62 -145.07(16) . . . . ?
B55 B60 B62 B57 67.3(2) . . . . ?
B55 B60 B62 B58 2.7(2) . . . . ?
B55 B60 B62 B59 -34.56(16) . . . . ?
B55 B60 B62 B61 104.85(18) . . . . ?
B56 B52 B57 Cl57 -147.38(14) . . . . ?
B56 B52 B57 B53 101.32(16) . . . . ?
B56 B52 B57 B58 62.42(19) . . . . ?
B56 B52 B57 B61 -36.28(14) . . . . ?
B56 B52 B57 B62 -2.0(2) . . . . ?
B56 B52 B61 Cl61 -111.35(19) . . . . ?
B56 B52 B61 B57 137.10(16) . . . . ?
B56 B52 B61 B60 38.97(16) . . . . ?
B56 B52 B61 B62 102.91(18) . . . . ?
B56 B55 B59 Cl59 147.64(15) . . . . ?
B56 B55 B59 B54 -101.53(16) . . . . ?
B56 B55 B59 B58 -62.65(19) . . . . ?
B56 B55 B59 B60 35.82(15) . . . . ?
B56 B55 B59 B62 1.3(2) . . . . ?
B56 B55 B60 Cl60 111.01(19) . . . . ?
B56 B55 B60 B59 -137.89(17) . . . . ?
B56 B55 B60 B61 -38.88(16) . . . . ?
B56 B55 B60 B62 -103.04(18) . . . . ?
B56 B60 B61 Cl61 107.28(19) . . . . ?
B56 B60 B61 B52 -42.05(17) . . . . ?
B56 B60 B61 B57 -105.16(18) . . . . ?
B56 B60 B61 B62 -141.84(17) . . . . ?
B56 B60 B62 Cl62 144.32(16) . . . . ?
B56 B60 B62 B57 -3.3(2) . . . . ?
B56 B60 B62 B58 -67.9(2) . . . . ?
B56 B60 B62 B59 -105.16(18) . . . . ?
B56 B60 B62 B61 34.24(15) . . . . ?
B56 B61 B62 Cl62 -144.92(16) . . . . ?
B56 B61 B62 B57 104.59(18) . . . . ?
B56 B61 B62 B58 67.4(2) . . . . ?
B56 B61 B62 B59 2.8(2) . . . . ?
B56 B61 B62 B60 -34.16(16) . . . . ?
B57 B52 B61 Cl61 111.55(19) . . . . ?
B57 B52 B61 B56 -137.10(16) . . . . ?
B57 B52 B61 B60 -98.13(18) . . . . ?
B57 B52 B61 B62 -34.18(16) . . . . ?
B57 B53 B58 Cl58 -112.21(18) . . . . ?
B57 B53 B58 B54 137.16(16) . . . . ?
B57 B53 B58 B59 98.33(18) . . . . ?
B57 B53 B58 B62 33.94(16) . . . . ?
B57 B58 B59 Cl59 -147.78(16) . . . . ?
B57 B58 B59 B54 105.44(18) . . . . ?
B57 B58 B59 B55 63.5(2) . . . . ?
B57 B58 B59 B60 0.2(2) . . . . ?
B57 B58 B59 B62 -36.29(16) . . . . ?
B57 B58 B62 Cl62 -110.24(19) . . . . ?
B57 B58 B62 B59 139.27(18) . . . . ?
B57 B58 B62 B60 101.98(18) . . . . ?
B57 B58 B62 B61 37.20(16) . . . . ?
B57 B61 B62 Cl62 110.49(19) . . . . ?
B57 B61 B62 B58 -37.15(15) . . . . ?
B57 B61 B62 B59 -101.79(17) . . . . ?
B57 B61 B62 B60 -138.75(17) . . . . ?
B58 B53 B57 Cl57 112.12(18) . . . . ?
B58 B53 B57 B52 -137.38(17) . . . . ?
B58 B53 B57 B61 -98.37(18) . . . . ?
B58 B53 B57 B62 -34.09(16) . . . . ?
B58 B54 B59 Cl59 -111.90(19) . . . . ?
B58 B54 B59 B55 137.09(16) . . . . ?
B58 B54 B59 B60 98.17(18) . . . . ?
B58 B54 B59 B62 34.39(15) . . . . ?
B58 B57 B61 Cl61 147.52(17) . . . . ?
B58 B57 B61 B52 -105.48(18) . . . . ?
B58 B57 B61 B56 -63.4(2) . . . . ?
B58 B57 B61 B60 -0.1(2) . . . . ?
B58 B57 B61 B62 36.52(16) . . . . ?
B58 B57 B62 Cl62 110.71(19) . . . . ?
B58 B57 B62 B59 -37.03(16) . . . . ?
B58 B57 B62 B60 -101.59(18) . . . . ?
B58 B57 B62 B61 -139.17(17) . . . . ?
B58 B59 B60 Cl60 -147.37(16) . . . . ?
B58 B59 B60 B55 104.88(18) . . . . ?
B58 B59 B60 B56 63.4(2) . . . . ?
B58 B59 B60 B61 -0.3(2) . . . . ?
B58 B59 B60 B62 -36.56(16) . . . . ?
B58 B59 B62 Cl62 -110.62(19) . . . . ?
B58 B59 B62 B57 37.04(16) . . . . ?
B58 B59 B62 B60 138.89(18) . . . . ?
B58 B59 B62 B61 101.83(18) . . . . ?
B59 B54 B58 Cl58 111.72(18) . . . . ?
B59 B54 B58 B53 -137.74(16) . . . . ?
B59 B54 B58 B57 -98.60(18) . . . . ?
B59 B54 B58 B62 -34.53(16) . . . . ?
B59 B55 B60 Cl60 -111.10(19) . . . . ?
B59 B55 B60 B56 137.89(17) . . . . ?
B59 B55 B60 B61 99.01(18) . . . . ?
B59 B55 B60 B62 34.85(16) . . . . ?
B59 B58 B62 Cl62 110.49(19) . . . . ?
B59 B58 B62 B57 -139.27(18) . . . . ?
B59 B58 B62 B60 -37.29(16) . . . . ?
B59 B58 B62 B61 -102.07(18) . . . . ?
B59 B60 B61 Cl61 -147.33(16) . . . . ?
B59 B60 B61 B52 63.3(2) . . . . ?
B59 B60 B61 B56 105.38(18) . . . . ?
B59 B60 B61 B57 0.2(2) . . . . ?
B59 B60 B61 B62 -36.45(16) . . . . ?
B59 B60 B62 Cl62 -110.52(19) . . . . ?
B59 B60 B62 B57 101.86(17) . . . . ?
B59 B60 B62 B58 37.30(16) . . . . ?
B59 B60 B62 B61 139.40(17) . . . . ?
B60 B55 B59 Cl59 111.82(18) . . . . ?
B60 B55 B59 B54 -137.35(17) . . . . ?
B60 B55 B59 B58 -98.47(18) . . . . ?
B60 B55 B59 B62 -34.55(15) . . . . ?
B60 B56 B61 Cl61 -111.74(19) . . . . ?
B60 B56 B61 B52 137.24(16) . . . . ?
B60 B56 B61 B57 98.28(18) . . . . ?
B60 B56 B61 B62 34.28(15) . . . . ?
B60 B59 B62 Cl62 110.50(18) . . . . ?
B60 B59 B62 B57 -101.85(18) . . . . ?
B60 B59 B62 B58 -138.89(18) . . . . ?
B60 B59 B62 B61 -37.05(16) . . . . ?
B60 B61 B62 Cl62 -110.76(18) . . . . ?
B60 B61 B62 B57 138.75(17) . . . . ?
B60 B61 B62 B58 101.60(18) . . . . ?
B60 B61 B62 B59 36.96(15) . . . . ?
B61 B52 B57 Cl57 -111.10(17) . . . . ?
B61 B52 B57 B53 137.60(17) . . . . ?
B61 B52 B57 B58 98.70(18) . . . . ?
B61 B52 B57 B62 34.27(15) . . . . ?
B61 B56 B60 Cl60 111.01(18) . . . . ?
B61 B56 B60 B55 -137.43(16) . . . . ?
B61 B56 B60 B59 -98.92(18) . . . . ?
B61 B56 B60 B62 -34.37(15) . . . . ?
B61 B57 B58 Cl58 -148.00(16) . . . . ?
B61 B57 B58 B53 105.88(18) . . . . ?
B61 B57 B58 B54 63.6(2) . . . . ?
B61 B57 B58 B59 0.0(2) . . . . ?
B61 B57 B58 B62 -36.43(16) . . . . ?
B61 B57 B62 Cl62 -110.13(18) . . . . ?
B61 B57 B62 B58 139.17(17) . . . . ?
B61 B57 B62 B59 102.14(18) . . . . ?
B61 B57 B62 B60 37.57(15) . . . . ?
B61 B60 B62 Cl62 110.08(18) . . . . ?
B61 B60 B62 B57 -37.55(15) . . . . ?
B61 B60 B62 B58 -102.10(18) . . . . ?
B61 B60 B62 B59 -139.40(17) . . . . ?
B62 B57 B58 Cl58 -111.57(19) . . . . ?
B62 B57 B58 B53 142.31(18) . . . . ?
B62 B57 B58 B54 100.00(18) . . . . ?
B62 B57 B58 B59 36.39(16) . . . . ?
B62 B57 B61 Cl61 111.0(2) . . . . ?
B62 B57 B61 B52 -142.00(17) . . . . ?
B62 B57 B61 B56 -99.88(19) . . . . ?
B62 B57 B61 B60 -36.64(16) . . . . ?
B62 B58 B59 Cl59 -111.48(19) . . . . ?
B62 B58 B59 B54 141.74(17) . . . . ?
B62 B58 B59 B55 99.84(18) . . . . ?
B62 B58 B59 B60 36.48(16) . . . . ?
B62 B59 B60 Cl60 -110.81(19) . . . . ?
B62 B59 B60 B55 141.44(17) . . . . ?
B62 B59 B60 B56 99.94(19) . . . . ?
B62 B59 B60 B61 36.31(16) . . . . ?
B62 B60 B61 Cl61 -110.9(2) . . . . ?
B62 B60 B61 B52 99.79(18) . . . . ?
B62 B60 B61 B56 141.84(17) . . . . ?
B62 B60 B61 B57 36.68(16) . . . . ?

_olex2_submission_special_instructions 'No special instructions were received'
_oxdiff_exptl_absorpt_empirical_details 
;
Empirical correction (ABSPACK) includes:
- Absorption correction using spherical harmonics
- Frame scaling
- Detector area scaling
;
_oxdiff_exptl_absorpt_empirical_full_max 1.147
_oxdiff_exptl_absorpt_empirical_full_min 0.866
_cell_oxdiff_length_a            8.84944(7)
_cell_oxdiff_length_b            26.97772(16)
_cell_oxdiff_length_c            9.14550(7)
_cell_oxdiff_angle_alpha         90.0118(6)
_cell_oxdiff_angle_beta          118.8034(8)
_cell_oxdiff_angle_gamma         89.9469(6)
_cell_oxdiff_volume              1913.24(2)
_cell_oxdiff_measurement_reflns_used 67816
_diffrn_measurement_specimen_support 'polyimid foil'


