# Electronic Supplementary Material (ESI) for Dalton Transactions.
# This journal is © The Royal Society of Chemistry 2023

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_namoioh
_database_code_depnum_ccdc_archive 'CCDC 2296933'
loop_
_audit_author_name
_audit_author_address
'Liu hongming'
;Guangxi University
China
;
_audit_update_record             
;
2023-09-23 deposited with the CCDC.	2023-12-06 downloaded from the CCDC.
;
_audit_creation_date             2023-03-17
_audit_creation_method           
;
Olex2 1.5
(compiled 2021.11.18 svn.ra9532c28 for OlexSys, GUI svn.r6429)
;
_shelx_SHELXL_version_number     2018/3
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         'H2 I Mo Na O7'
_chemical_formula_sum            'H2 I Mo Na O7'
_chemical_formula_weight         359.85
_chemical_absolute_configuration ?
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
I I -0.4742 1.8119 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Mo Mo -1.6832 0.6857 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Na Na 0.0362 0.0249 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           7
_space_group_name_H-M_alt        'P 1 c 1'
_space_group_name_Hall           'P -2yc'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'x, -y, z+1/2'

_cell_length_a                   10.9278(9)
_cell_length_b                   7.7836(6)
_cell_length_c                   7.2784(6)
_cell_angle_alpha                90
_cell_angle_beta                 99.345(8)
_cell_angle_gamma                90
_cell_volume                     610.87(9)
_cell_formula_units_Z            4
_cell_measurement_temperature    296(2)
_cell_measurement_reflns_used    1351
_cell_measurement_theta_min      4.4990
_cell_measurement_theta_max      28.7980
_shelx_estimated_absorpt_T_max   0.713
_shelx_estimated_absorpt_T_min   0.390
_exptl_absorpt_coefficient_mu    7.252
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  0.51066
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   ?
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            colourless
_exptl_crystal_colour_primary    colourless
_exptl_crystal_density_diffrn    3.913
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       plate
_exptl_crystal_F_000             656
_exptl_crystal_size_max          0.16
_exptl_crystal_size_mid          0.13
_exptl_crystal_size_min          0.05
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0395
_diffrn_reflns_av_unetI/netI     0.0774
_diffrn_reflns_Laue_measured_fraction_full 0.997
_diffrn_reflns_Laue_measured_fraction_max 0.997
_diffrn_reflns_limit_h_max       12
_diffrn_reflns_limit_h_min       -13
_diffrn_reflns_limit_k_max       9
_diffrn_reflns_limit_k_min       -9
_diffrn_reflns_limit_l_max       8
_diffrn_reflns_limit_l_min       -8
_diffrn_reflns_number            2458
_diffrn_reflns_point_group_measured_fraction_full 0.756
_diffrn_reflns_point_group_measured_fraction_max 0.750
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         25.681
_diffrn_reflns_theta_min         3.779
_diffrn_ambient_temperature      296(2)
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 0.997
_diffrn_measured_fraction_theta_max 0.997
_diffrn_measurement_device_type  'multiwire proportional'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   ?
_reflns_Friedel_coverage         0.497
_reflns_Friedel_fraction_full    0.514
_reflns_Friedel_fraction_max     0.500
_reflns_number_gt                1543
_reflns_number_total             1740
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences. Completness statistics refer to single and
 composite reflections containing twin component 1 only.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       ?
_computing_data_collection       ?
_computing_data_reduction        ?
_computing_molecular_graphics    'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_structure_refinement  'SHELXL 2018/3 (Sheldrick, 2015)'
_computing_structure_solution    'SHELXT 2018/2 (Sheldrick, 2018)'
_refine_diff_density_max         5.065
_refine_diff_density_min         -3.049
_refine_diff_density_rms         0.417
_refine_ls_abs_structure_details 
;
 Refined as an inversion twin.
;
_refine_ls_abs_structure_Flack   -0.02(10)
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.067
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     182
_refine_ls_number_reflns         1740
_refine_ls_number_restraints     56
_refine_ls_R_factor_all          0.0639
_refine_ls_R_factor_gt           0.0573
_refine_ls_restrained_S_all      1.054
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0512P)²+20.2291P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1338
_refine_ls_wR_factor_ref         0.1407
_refine_special_details          
;
 Refined as a 2-component inversion twin.
;
_olex2_refinement_description    
;
1. Twinned data refinement
 Scales: 1.02(10)
 -0.02(10)
2. Fixed Uiso
 At 1.5 times of:
  All O(H,H) groups
3. Uiso/Uaniso restraints and constraints
Uanis(O4) \\sim Ueq, Uanis(O6) \\sim Ueq, Uanis(O7) \\sim Ueq, Uanis(O9) \\sim
Ueq, Uanis(O11) \\sim Ueq, Uanis(O2) \\sim Ueq, Uanis(O1) \\sim Ueq, Uanis(O5)
\\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.005
Uanis(O14) \\sim Ueq: with sigma of 0.006 and sigma for terminal atoms of 0.003
4.a Secondary CH2 refined with riding coordinates:
 O1(H1A,H1B), O2(H2A,H2B)
;
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     dual
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
I1 I 0.51889(19) 0.2668(3) 0.3298(2) 0.0120(6) Uani 1 1 d . . . . .
I2 I 0.47941(19) 0.7669(3) 0.3198(2) 0.0122(6) Uani 1 1 d . . . . .
Mo1 Mo 0.7678(3) 0.4999(3) 0.5652(4) 0.0071(6) Uani 1 1 d . . . . .
Mo2 Mo 0.2306(3) 0.9980(3) 0.4339(4) 0.0074(6) Uani 1 1 d . . . . .
Na1 Na 0.7505(15) -0.019(3) 0.600(2) 0.047(6) Uani 1 1 d . . . . .
Na2 Na 0.2479(16) 0.469(3) 0.469(2) 0.041(5) Uani 1 1 d . . . . .
O1 O 0.887(2) 0.003(3) 0.374(4) 0.023(6) Uani 1 1 d . U . . .
H1A H 0.938776 0.104583 0.394370 0.035 Uiso 1 1 calc R U . . .
H1B H 0.940203 -0.097920 0.376805 0.035 Uiso 1 1 calc R U . . .
O2 O 0.112(2) 0.494(3) 0.684(4) 0.027(6) Uani 1 1 d . U . . .
H2A H 0.062171 0.391098 0.686382 0.040 Uiso 1 1 calc R U . . .
H2B H 0.057685 0.592309 0.656664 0.040 Uiso 1 1 calc R U . . .
O3 O 0.599(3) 0.060(4) 0.342(3) 0.028(7) Uani 1 1 d . . . . .
O4 O 0.383(2) 0.211(3) 0.420(3) 0.020(5) Uani 1 1 d . U . . .
O5 O 0.596(2) 0.342(3) 0.560(3) 0.017(5) Uani 1 1 d . U . . .
O6 O 0.863(2) 0.332(3) 0.626(3) 0.022(5) Uani 1 1 d . U . . .
O7 O 0.724(2) 0.562(3) 0.805(3) 0.015(5) Uani 1 1 d . U . . .
O8 O 0.870(2) 0.661(3) 0.558(4) 0.032(6) Uani 1 1 d . . . . .
O9 O 0.611(2) 0.712(3) 0.468(4) 0.027(6) Uani 1 1 d . U . . .
O10 O 0.398(3) 0.564(3) 0.287(4) 0.031(7) Uani 1 1 d . . . . .
O11 O 0.402(2) 0.842(3) 0.515(3) 0.021(5) Uani 1 1 d . U . . .
O12 O 0.136(2) 0.829(3) 0.448(3) 0.024(6) Uani 1 1 d . . . . .
O13 O 0.128(2) 1.160(3) 0.378(4) 0.028(6) Uani 1 1 d . . . . .
O14 O 0.276(2) 0.946(3) 0.194(3) 0.012(5) Uani 1 1 d . U . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
I1 O3 1.83(3) . ?
I1 O4 1.77(2) . ?
I1 O5 1.84(2) . ?
I2 O9 1.70(3) . ?
I2 O10 1.81(3) . ?
I2 O11 1.86(2) . ?
Mo1 O5 2.24(2) . ?
Mo1 O6 1.68(3) . ?
Mo1 O7 1.95(2) . ?
Mo1 O7 1.94(2) 2_564 ?
Mo1 O8 1.68(3) . ?
Mo1 O9 2.40(2) . ?
Mo2 Na2 3.68(2) 1_565 ?
Mo2 O4 2.36(2) 1_565 ?
Mo2 O11 2.23(2) . ?
Mo2 O12 1.68(2) . ?
Mo2 O13 1.69(2) . ?
Mo2 O14 1.93(2) . ?
Mo2 O14 1.93(2) 2_575 ?
Na1 Na1 3.652(4) 2_554 ?
Na1 Na1 3.652(4) 2 ?
Na1 O1 2.40(3) . ?
Na1 O1 2.30(3) 2 ?
Na1 O3 2.62(3) 2 ?
Na1 O3 2.37(3) . ?
Na1 O6 2.99(3) . ?
Na1 O8 2.85(3) 1_545 ?
Na1 O9 2.68(3) 1_545 ?
Na2 Na2 3.671(6) 2_565 ?
Na2 Na2 3.671(6) 2_564 ?
Na2 O2 2.36(3) 2_564 ?
Na2 O2 2.33(3) . ?
Na2 O4 2.56(3) . ?
Na2 O10 2.62(3) 2_565 ?
Na2 O10 2.39(4) . ?
Na2 O13 2.77(3) 1_545 ?
O1 H1A 0.9700 . ?
O1 H1B 0.9700 . ?
O2 H2A 0.9700 . ?
O2 H2B 0.9700 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O3 I1 O5 95.1(11) . . ?
O4 I1 O3 100.9(12) . . ?
O4 I1 O5 91.9(10) . . ?
O9 I2 O10 102.1(12) . . ?
O9 I2 O11 92.2(11) . . ?
O10 I2 O11 95.6(12) . . ?
O5 Mo1 O9 79.4(9) . . ?
O6 Mo1 O5 93.3(10) . . ?
O6 Mo1 O7 96.3(11) . 2_564 ?
O6 Mo1 O7 100.9(11) . . ?
O6 Mo1 O9 172.5(10) . . ?
O7 Mo1 O5 79.8(9) . . ?
O7 Mo1 O5 76.9(9) 2_564 . ?
O7 Mo1 O7 151.7(13) 2_564 . ?
O7 Mo1 O9 80.0(9) . . ?
O7 Mo1 O9 80.2(9) 2_564 . ?
O8 Mo1 O5 165.0(10) . . ?
O8 Mo1 O6 101.6(13) . . ?
O8 Mo1 O7 96.0(12) . . ?
O8 Mo1 O7 102.4(12) . 2_564 ?
O8 Mo1 O9 85.7(10) . . ?
O4 Mo2 Na2 43.7(6) 1_565 1_565 ?
O11 Mo2 Na2 119.5(7) . 1_565 ?
O11 Mo2 O4 79.9(9) . 1_565 ?
O12 Mo2 Na2 143.0(9) . 1_565 ?
O12 Mo2 O4 172.9(11) . 1_565 ?
O12 Mo2 O11 93.1(11) . . ?
O12 Mo2 O13 102.1(13) . . ?
O12 Mo2 O14 98.2(10) . . ?
O12 Mo2 O14 100.2(11) . 2_575 ?
O13 Mo2 Na2 45.5(9) . 1_565 ?
O13 Mo2 O4 85.0(10) . 1_565 ?
O13 Mo2 O11 164.7(11) . . ?
O13 Mo2 O14 101.3(11) . . ?
O13 Mo2 O14 97.1(11) . 2_575 ?
O14 Mo2 Na2 72.8(7) 2_575 1_565 ?
O14 Mo2 Na2 104.7(7) . 1_565 ?
O14 Mo2 O4 79.2(9) 2_575 1_565 ?
O14 Mo2 O4 79.6(9) . 1_565 ?
O14 Mo2 O11 78.0(9) 2_575 . ?
O14 Mo2 O11 78.2(9) . . ?
O14 Mo2 O14 150.5(13) 2_575 . ?
Na1 Na1 Na1 170.5(14) 2 2_554 ?
O1 Na1 Na1 139.2(7) 2 2_554 ?
O1 Na1 Na1 40.0(7) 2 2 ?
O1 Na1 Na1 140.9(9) . 2 ?
O1 Na1 Na1 38.0(8) . 2_554 ?
O1 Na1 O1 101.6(12) 2 . ?
O1 Na1 O3 177.1(14) . 2 ?
O1 Na1 O3 160.9(15) 2 . ?
O1 Na1 O3 79.3(10) 2 2 ?
O1 Na1 O6 71.5(9) . . ?
O1 Na1 O6 71.9(9) 2 . ?
O1 Na1 O8 69.1(9) . 1_545 ?
O1 Na1 O8 84.1(10) 2 1_545 ?
O1 Na1 O9 127.5(12) 2 1_545 ?
O1 Na1 O9 101.2(11) . 1_545 ?
O3 Na1 Na1 130.9(9) . 2 ?
O3 Na1 Na1 45.8(7) . 2_554 ?
O3 Na1 Na1 40.4(7) 2 2 ?
O3 Na1 Na1 141.4(7) 2 2_554 ?
O3 Na1 O1 82.7(11) . . ?
O3 Na1 O3 97.4(11) . 2 ?
O3 Na1 O6 92.3(11) . . ?
O3 Na1 O6 111.4(11) 2 . ?
O3 Na1 O8 114.6(12) . 1_545 ?
O3 Na1 O8 108.4(11) 2 1_545 ?
O3 Na1 O9 76.1(9) 2 1_545 ?
O3 Na1 O9 68.7(11) . 1_545 ?
O6 Na1 Na1 85.5(8) . 2_554 ?
O6 Na1 Na1 85.8(9) . 2 ?
O8 Na1 Na1 104.6(9) 1_545 2 ?
O8 Na1 Na1 83.8(9) 1_545 2_554 ?
O8 Na1 O6 127.9(9) 1_545 . ?
O9 Na1 Na1 78.5(8) 1_545 2_554 ?
O9 Na1 Na1 109.2(9) 1_545 2 ?
O9 Na1 O6 160.6(10) 1_545 . ?
O9 Na1 O8 61.5(9) 1_545 1_545 ?
Na2 Na2 Mo2 94.0(7) 2_564 1_545 ?
Na2 Na2 Mo2 101.1(7) 2_565 1_545 ?
Na2 Na2 Na2 164.8(13) 2_565 2_564 ?
O2 Na2 Mo2 95.7(9) . 1_545 ?
O2 Na2 Mo2 92.4(8) 2_564 1_545 ?
O2 Na2 Na2 38.3(8) 2_564 2_564 ?
O2 Na2 Na2 38.9(8) . 2_565 ?
O2 Na2 Na2 138.8(9) 2_564 2_565 ?
O2 Na2 Na2 139.1(8) . 2_564 ?
O2 Na2 O2 101.6(12) . 2_564 ?
O2 Na2 O4 127.3(12) . . ?
O2 Na2 O4 105.5(11) 2_564 . ?
O2 Na2 O10 82.1(11) 2_564 . ?
O2 Na2 O10 178.6(13) 2_564 2_565 ?
O2 Na2 O10 77.9(11) . 2_565 ?
O2 Na2 O10 156.3(13) . . ?
O2 Na2 O13 84.6(10) . 1_545 ?
O2 Na2 O13 71.9(9) 2_564 1_545 ?
O4 Na2 Mo2 39.7(6) . 1_545 ?
O4 Na2 Na2 82.5(8) . 2_564 ?
O4 Na2 Na2 109.7(9) . 2_565 ?
O4 Na2 O10 75.8(9) . 2_565 ?
O4 Na2 O13 62.9(9) . 1_545 ?
O10 Na2 Mo2 88.9(8) 2_565 1_545 ?
O10 Na2 Mo2 107.6(9) . 1_545 ?
O10 Na2 Na2 40.4(8) 2_565 2_565 ?
O10 Na2 Na2 45.3(8) . 2_564 ?
O10 Na2 Na2 142.0(8) 2_565 2_564 ?
O10 Na2 Na2 128.4(10) . 2_565 ?
O10 Na2 O4 72.6(9) . . ?
O10 Na2 O10 97.8(12) . 2_565 ?
O10 Na2 O13 118.5(11) . 1_545 ?
O10 Na2 O13 109.3(11) 2_565 1_545 ?
O13 Na2 Mo2 25.9(6) 1_545 1_545 ?
O13 Na2 Na2 106.1(9) 1_545 2_565 ?
O13 Na2 Na2 87.2(8) 1_545 2_564 ?
Na1 O1 Na1 102.0(12) 2_554 . ?
Na1 O1 H1A 111.4 2_554 . ?
Na1 O1 H1A 111.4 . . ?
Na1 O1 H1B 111.4 . . ?
Na1 O1 H1B 111.4 2_554 . ?
H1A O1 H1B 109.2 . . ?
Na2 O2 Na2 102.8(12) . 2_565 ?
Na2 O2 H2A 111.2 2_565 . ?
Na2 O2 H2A 111.2 . . ?
Na2 O2 H2B 111.2 2_565 . ?
Na2 O2 H2B 111.2 . . ?
H2A O2 H2B 109.1 . . ?
I1 O3 Na1 122.3(15) . . ?
I1 O3 Na1 115.1(13) . 2_554 ?
Na1 O3 Na1 93.8(10) . 2_554 ?
I1 O4 Mo2 146.0(11) . 1_545 ?
I1 O4 Na2 113.3(11) . . ?
Mo2 O4 Na2 96.7(9) 1_545 . ?
I1 O5 Mo1 116.7(10) . . ?
Mo1 O6 Na1 117.5(12) . . ?
Mo1 O7 Mo1 139.3(13) 2_565 . ?
Mo1 O8 Na1 109.3(12) . 1_565 ?
I2 O9 Mo1 147.9(13) . . ?
I2 O9 Na1 113.7(11) . 1_565 ?
Mo1 O9 Na1 95.3(10) . 1_565 ?
I2 O10 Na2 124.5(14) . . ?
I2 O10 Na2 115.2(14) . 2_564 ?
Na2 O10 Na2 94.3(11) . 2_564 ?
I2 O11 Mo2 115.9(11) . . ?
Mo2 O13 Na2 108.6(12) . 1_565 ?
Mo2 O14 Mo2 140.9(13) 2_574 . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
O3 I1 O4 Mo2 -37(3) . . . 1_545 ?
O3 I1 O4 Na2 173.0(12) . . . . ?
O3 I1 O5 Mo1 93.2(14) . . . . ?
O4 I1 O3 Na1 153.4(13) . . . 2_554 ?
O4 I1 O3 Na1 -94.2(16) . . . . ?
O4 I1 O5 Mo1 -165.7(12) . . . . ?
O4 Mo2 O13 Na2 -21.3(10) 1_565 . . 1_565 ?
O5 I1 O3 Na1 -113.7(14) . . . 2_554 ?
O5 I1 O3 Na1 -1.3(16) . . . . ?
O5 I1 O4 Mo2 -133(2) . . . 1_545 ?
O5 I1 O4 Na2 77.4(13) . . . . ?
O5 Mo1 O6 Na1 12.2(12) . . . . ?
O5 Mo1 O8 Na1 17(5) . . . 1_565 ?
O6 Mo1 O8 Na1 -158.1(12) . . . 1_565 ?
O7 Mo1 O6 Na1 -65.0(12) 2_564 . . . ?
O7 Mo1 O6 Na1 92.4(12) . . . . ?
O7 Mo1 O8 Na1 102.7(12) 2_564 . . 1_565 ?
O7 Mo1 O8 Na1 -55.7(13) . . . 1_565 ?
O8 Mo1 O6 Na1 -169.1(13) . . . . ?
O9 I2 O10 Na2 92.3(18) . . . . ?
O9 I2 O10 Na2 -152.7(13) . . . 2_564 ?
O9 I2 O11 Mo2 166.2(13) . . . . ?
O9 Mo1 O8 Na1 23.7(11) . . . 1_565 ?
O10 I2 O9 Mo1 35(3) . . . . ?
O10 I2 O9 Na1 -171.8(12) . . . 1_565 ?
O10 I2 O11 Mo2 -91.3(14) . . . . ?
O11 I2 O9 Mo1 132(2) . . . . ?
O11 I2 O9 Na1 -75.5(12) . . . 1_565 ?
O11 I2 O10 Na2 113.9(14) . . . 2_564 ?
O11 I2 O10 Na2 -1.2(18) . . . . ?
O11 Mo2 O13 Na2 -13(5) . . . 1_565 ?
O12 Mo2 O13 Na2 159.3(11) . . . 1_565 ?
O14 Mo2 O13 Na2 -99.6(11) . . . 1_565 ?
O14 Mo2 O13 Na2 57.2(11) 2_575 . . 1_565 ?

_olex2_submission_special_instructions 'No special instructions were received'
loop_
_twin_individual_id
_twin_individual_mass_fraction_refined
1 1.02(10)
2 -0.02(10)

