# Electronic Supplementary Material (ESI) for Journal of Materials Chemistry C.
# This journal is © The Royal Society of Chemistry 2023

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
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data_cu_20211021li_czu_th_0m
_database_code_depnum_ccdc_archive 'CCDC 2157705'
loop_
_audit_author_name
_audit_author_address
'Xiaoqin yang'
;Hunan University of Science and Technology
China
;
_audit_update_record             
;
2022-03-10 deposited with the CCDC.	2023-08-18 downloaded from the CCDC.
;
_audit_creation_date             2021-10-25
_audit_creation_method           
;
Olex2 1.5
(compiled 2021.10.07 svn.r9718050b for OlexSys, GUI svn.r6410)
;
_shelx_SHELXL_version_number     2018/3
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         'C48 H28 N8 O2 Pt2 S2, 2(C H Cl3)'
_chemical_formula_sum            'C50 H30 Cl6 N8 O2 Pt2 S2'
_chemical_formula_weight         1441.82
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.3639 0.7018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -4.5932 6.9264 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.3331 0.5567 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_H-M_alt        'P -1'
_space_group_name_Hall           '-P 1'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'

_cell_length_a                   13.5533(3)
_cell_length_b                   19.4177(4)
_cell_length_c                   20.0115(4)
_cell_angle_alpha                106.9470(10)
_cell_angle_beta                 97.2750(10)
_cell_angle_gamma                101.9880(10)
_cell_volume                     4828.33(18)
_cell_formula_units_Z            4
_cell_measurement_reflns_used    9647
_cell_measurement_temperature    193.00
_cell_measurement_theta_max      68.22
_cell_measurement_theta_min      2.46
_shelx_estimated_absorpt_T_max   0.316
_shelx_estimated_absorpt_T_min   0.267
_exptl_absorpt_coefficient_mu    14.969
_exptl_absorpt_correction_T_max  0.7531
_exptl_absorpt_correction_T_min  0.3588
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
;
SADABS-2016/2 (Bruker,2016/2) was used for absorption correction.
wR2(int) was 0.1277 before and 0.0710 after correction.
The Ratio of minimum to maximum transmission is 0.4764.
The λ/2 correction factor is Not present.
;
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            ?
_exptl_crystal_density_diffrn    1.983
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       BLOCK
_exptl_crystal_F_000             2768
_exptl_crystal_size_max          0.12
_exptl_crystal_size_mid          0.1
_exptl_crystal_size_min          0.1
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0531
_diffrn_reflns_av_unetI/netI     0.0460
_diffrn_reflns_Laue_measured_fraction_full 0.996
_diffrn_reflns_Laue_measured_fraction_max 0.993
_diffrn_reflns_limit_h_max       16
_diffrn_reflns_limit_h_min       -16
_diffrn_reflns_limit_k_max       23
_diffrn_reflns_limit_k_min       -23
_diffrn_reflns_limit_l_max       24
_diffrn_reflns_limit_l_min       -24
_diffrn_reflns_number            66363
_diffrn_reflns_point_group_measured_fraction_full 0.996
_diffrn_reflns_point_group_measured_fraction_max 0.993
_diffrn_reflns_theta_full        67.679
_diffrn_reflns_theta_max         68.280
_diffrn_reflns_theta_min         2.356
_diffrn_ambient_temperature      193.00
_diffrn_detector_area_resol_mean 7.41
_diffrn_detector_type            'Bruker PHOTON III'
_diffrn_measured_fraction_theta_full 0.996
_diffrn_measured_fraction_theta_max 0.993
_diffrn_measurement_device       'three-circle diffractometer'
_diffrn_measurement_device_type  'Bruker D8 VENTURE PHOTON III'
_diffrn_measurement_method       'ω and φ shutterless scans'
_diffrn_measurement_specimen_support 'nylon loop'
_diffrn_radiation_type           CuK\a
_diffrn_radiation_wavelength     1.54178
_diffrn_source                   ?
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                15999
_reflns_number_total             17586
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       
;
SAINT V8.40B (Bruker, 2019)
;
_computing_data_collection       'Bruker BIS V6.2.14'
_computing_data_reduction        
;
SAINT V8.40B (Bruker, 2019)
;
_computing_molecular_graphics    'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_structure_refinement  'SHELXL 2018/3 (Sheldrick, 2015)'
_computing_structure_solution    'olex2.solve 1.5 (Bourhis et al., 2015)'
_refine_diff_density_max         1.436
_refine_diff_density_min         -1.500
_refine_diff_density_rms         0.167
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.039
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1271
_refine_ls_number_reflns         17586
_refine_ls_number_restraints     10
_refine_ls_R_factor_all          0.0385
_refine_ls_R_factor_gt           0.0351
_refine_ls_restrained_S_all      1.047
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0467P)²+14.2796P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0941
_refine_ls_wR_factor_ref         0.0963
_refine_special_details          ?
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H) groups
2. Restrained distances
 H03F-H02J
 2.1 with sigma of 0.02
 H025-H02M
 2.1 with sigma of 0.02
 H01K-H01G
 2.1 with sigma of 0.02
 H01G-H01K
 2.1 with sigma of 0.02
3. Uiso/Uaniso restraints and constraints
C9A \\sim C9B: within 2A with sigma of 0.01 and sigma for terminal atoms of
0.02 within 2A
4. Others
 Sof(C9B)=Sof(H9B)=1-FVAR(1)
 Sof(C9A)=Sof(H9A)=FVAR(1)
5.a Ternary CH refined with riding coordinates:
 C03T(H03T), C03V(H03V), C03U(H03U), C9A(H9A), C9B(H9B)
5.b Aromatic/amide H refined with riding coordinates:
 C01C(H01C), C01E(H01E), C01G(H01G), C01K(H01K), C01P(H01P), C01W(H01W),
 C02H(H02H), C02L(H02L), C02M(H02M), C02P(H02P), C02Q(H02Q), C02R(H02R),
 C02T(H02T), C02V(H02V), C02W(H02W), C02X(H02X), C02Z(H02Z), C03D(H03D),
 C03G(H03G), C03L(H03L), C03M(H03M), C03N(H03N), C03R(H03R), C03S(H03S),
 C025(H025), C031(H031), C033(H033), C037(H037), C01A(H01A), C01M(H01M),
 C01Q(H01Q), C01X(H01X), C01Y(H01Y), C02A(H02A), C02J(H02J), C02O(H02O),
 C02U(H02U), C03A(H03A), C03B(H03B), C03C(H03C), C03E(H03E), C03F(H03F),
 C03H(H03H), C03I(H03I), C03J(H03J), C03K(H03K), C03O(H03O), C03P(H03P),
 C03Q(H03Q), C020(H020), C023(H023), C032(H032), C034(H034), C036(H036),
 C038(H038), C039(H039)
;
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     iterative
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Pt1 Pt 0.88293(2) 0.19136(2) 0.34482(2) 0.01990(6) Uani 1 1 d . . . . .
Pt2 Pt 0.68419(2) 0.23353(2) 0.36433(2) 0.01883(6) Uani 1 1 d . . . . .
S1 S 0.82973(10) 0.08552(7) 0.37493(7) 0.0282(3) Uani 1 1 d . . . . .
S2 S 0.72845(10) 0.27130(7) 0.48681(6) 0.0270(2) Uani 1 1 d . . . . .
O00K O 0.9103(3) 0.29563(19) 0.56838(17) 0.0263(7) Uani 1 1 d . . . . .
O00M O 0.6468(3) 0.01959(18) 0.39083(17) 0.0245(7) Uani 1 1 d . . . . .
N1 N 1.0157(3) 0.2676(2) 0.4946(2) 0.0283(9) Uani 1 1 d . . . . .
N2 N 0.9151(3) 0.2537(2) 0.4550(2) 0.0246(8) Uani 1 1 d . . . . .
N3 N 0.9299(3) 0.2806(2) 0.3123(2) 0.0240(8) Uani 1 1 d . . . . .
N4 N 1.0525(4) 0.5430(3) 0.4313(3) 0.0537(14) Uani 1 1 d . . . . .
N5 N 0.6443(3) 0.1224(2) 0.3674(2) 0.0240(8) Uani 1 1 d . . . . .
N6 N 0.5445(3) 0.0906(2) 0.3747(2) 0.0249(8) Uani 1 1 d . . . . .
N7 N 0.6474(3) 0.2076(2) 0.2565(2) 0.0224(8) Uani 1 1 d . . . . .
N16 N 0.5851(4) -0.0204(3) 0.0656(3) 0.0474(13) Uani 1 1 d . . . . .
C01B C 0.6257(4) 0.2480(3) 0.1543(3) 0.0242(10) Uani 1 1 d . . . . .
C01C C 0.9666(4) 0.3511(3) 0.3595(3) 0.0258(10) Uani 1 1 d . . . . .
H01C H 0.978611 0.358289 0.409123 0.031 Uiso 1 1 calc R U . . .
C01E C 0.6252(4) 0.1350(3) 0.2127(2) 0.0235(10) Uani 1 1 d . . . . .
H01E H 0.618463 0.096192 0.233132 0.028 Uiso 1 1 calc R U . . .
C01G C 0.7236(4) 0.4063(3) 0.2739(3) 0.0273(10) Uani 1 1 d . . . . .
H01G H 0.715325 0.407656 0.226453 0.033 Uiso 1 1 calc DR U . . .
C01H C 0.6105(4) 0.1730(3) 0.1084(3) 0.0265(10) Uani 1 1 d . . . . .
C01J C 0.6125(4) 0.1173(3) 0.1408(3) 0.0272(10) Uani 1 1 d . . . . .
C01K C 0.6034(4) 0.2995(3) 0.1205(3) 0.0332(12) Uani 1 1 d . . . . .
H01K H 0.602354 0.347700 0.149342 0.040 Uiso 1 1 calc DR U . . .
C01L C 1.0078(4) 0.2921(3) 0.5597(3) 0.0273(10) Uani 1 1 d . . . . .
C01O C 0.7024(4) 0.0790(3) 0.3773(2) 0.0228(9) Uani 1 1 d . . . . .
C01P C 0.7554(4) 0.4028(3) 0.4118(3) 0.0269(10) Uani 1 1 d . . . . .
H01P H 0.767861 0.402781 0.459595 0.032 Uiso 1 1 calc R U . . .
C01R C 0.9865(4) 0.4115(3) 0.3372(3) 0.0301(11) Uani 1 1 d . . . . .
C01S C 0.9600(4) 0.4027(3) 0.2636(3) 0.0333(12) Uani 1 1 d . . . . .
C01W C 0.8394(4) 0.0629(3) 0.2050(3) 0.0328(12) Uani 1 1 d . . . . .
H01W H 0.826005 0.029195 0.230924 0.039 Uiso 1 1 calc R U . . .
C02B C 0.8554(4) 0.2717(3) 0.5000(2) 0.0234(10) Uani 1 1 d . . . . .
C02F C 0.4684(4) -0.0219(3) 0.4026(2) 0.0264(10) Uani 1 1 d . . . . .
C02H C 0.8342(4) 0.0351(3) 0.1317(3) 0.0396(13) Uani 1 1 d . . . . .
H02H H 0.815907 -0.017223 0.108141 0.048 Uiso 1 1 calc R U . . .
C02I C 0.9160(4) 0.3295(3) 0.2150(3) 0.0293(11) Uani 1 1 d . . . . .
C02K C 1.0899(4) 0.3132(3) 0.6226(3) 0.0337(12) Uani 1 1 d . . . . .
C02L C 0.3740(4) -0.0045(3) 0.4086(3) 0.0343(12) Uani 1 1 d . . . . .
H02L H 0.363524 0.040349 0.402554 0.041 Uiso 1 1 calc R U . . .
C02M C 0.8802(4) 0.1581(3) 0.1268(3) 0.0357(12) Uani 1 1 d . . . . .
H02M H 0.896842 0.190717 0.100211 0.043 Uiso 1 1 calc DR U . . .
C02N C 0.5963(4) 0.0405(3) 0.0982(3) 0.0336(12) Uani 1 1 d . . . . .
C02P C 0.5923(4) 0.1573(3) 0.0342(3) 0.0368(12) Uani 1 1 d . . . . .
H02P H 0.588462 0.108607 0.003891 0.044 Uiso 1 1 calc R U . . .
C02Q C 0.2958(5) -0.0532(4) 0.4233(3) 0.0425(14) Uani 1 1 d . . . . .
H02Q H 0.231366 -0.041799 0.427014 0.051 Uiso 1 1 calc R U . . .
C02R C 0.5837(5) 0.2825(4) 0.0491(3) 0.0404(13) Uani 1 1 d . . . . .
H02R H 0.572128 0.319213 0.028550 0.048 Uiso 1 1 calc R U . . .
C02T C 0.4829(5) -0.0872(3) 0.4121(3) 0.0349(12) Uani 1 1 d . . . . .
H02T H 0.547062 -0.099065 0.408655 0.042 Uiso 1 1 calc R U . . .
C02V C 1.1906(5) 0.3174(4) 0.6131(3) 0.0487(16) Uani 1 1 d . . . . .
H02V H 1.205431 0.308662 0.566623 0.058 Uiso 1 1 calc R U . . .
C02W C 0.3117(5) -0.1180(3) 0.4326(3) 0.0405(14) Uani 1 1 d . . . . .
H02W H 0.258430 -0.151021 0.443187 0.049 Uiso 1 1 calc R U . . .
C02X C 0.9706(5) 0.4649(4) 0.2392(4) 0.0482(16) Uani 1 1 d . . . . .
H02X H 1.004420 0.513616 0.270863 0.058 Uiso 1 1 calc R U . . .
C02Y C 1.0245(4) 0.4846(3) 0.3897(3) 0.0389(13) Uani 1 1 d . . . . .
C02Z C 0.4046(5) -0.1350(3) 0.4266(3) 0.0426(14) Uani 1 1 d . . . . .
H02Z H 0.414768 -0.180008 0.432436 0.051 Uiso 1 1 calc R U . . .
C03D C 0.8555(4) 0.0829(4) 0.0931(3) 0.0404(14) Uani 1 1 d . . . . .
H03D H 0.852834 0.063538 0.043290 0.048 Uiso 1 1 calc R U . . .
C03G C 1.0687(5) 0.3283(4) 0.6905(3) 0.0456(15) Uani 1 1 d . . . . .
H03G H 1.000315 0.326672 0.697306 0.055 Uiso 1 1 calc R U . . .
C03L C 1.2693(5) 0.3346(4) 0.6715(4) 0.0556(18) Uani 1 1 d . . . . .
H03L H 1.338076 0.336939 0.665108 0.067 Uiso 1 1 calc R U . . .
C03M C 0.8813(6) 0.3827(5) 0.1215(4) 0.059(2) Uani 1 1 d . . . . .
H03M H 0.852697 0.376380 0.073579 0.070 Uiso 1 1 calc R U . . .
C03N C 1.2474(6) 0.3481(4) 0.7388(4) 0.061(2) Uani 1 1 d . . . . .
H03N H 1.301194 0.358997 0.778705 0.074 Uiso 1 1 calc R U . . .
C03R C 1.1489(6) 0.3461(5) 0.7488(4) 0.061(2) Uani 1 1 d . . . . .
H03R H 1.134948 0.356742 0.795552 0.074 Uiso 1 1 calc R U . . .
C03S C 0.9314(6) 0.4539(5) 0.1689(4) 0.062(2) Uani 1 1 d . . . . .
H03S H 0.938422 0.495398 0.152255 0.075 Uiso 1 1 calc R U . . .
C010 C 0.8817(4) 0.1883(3) 0.2001(3) 0.0269(10) Uani 1 1 d . . . . .
C012 C 0.6951(4) 0.3373(3) 0.2857(2) 0.0211(9) Uani 1 1 d . . . . .
C014 C 0.8641(4) 0.1394(3) 0.2409(3) 0.0251(10) Uani 1 1 d . . . . .
C016 C 0.7136(4) 0.3348(3) 0.3565(2) 0.0220(9) Uani 1 1 d . . . . .
C017 C 0.9090(4) 0.2672(3) 0.2409(3) 0.0259(10) Uani 1 1 d . . . . .
C018 C 0.6534(3) 0.2638(3) 0.2301(2) 0.0205(9) Uani 1 1 d . . . . .
C021 C 0.5502(4) 0.0311(3) 0.3887(3) 0.0251(10) Uani 1 1 d . . . . .
C025 C 0.8735(5) 0.3227(4) 0.1440(3) 0.0433(15) Uani 1 1 d . . . . .
H025 H 0.838626 0.274692 0.111373 0.052 Uiso 1 1 calc DR U . . .
C031 C 0.7787(4) 0.4694(3) 0.3988(3) 0.0321(11) Uani 1 1 d . . . . .
H031 H 0.805856 0.514595 0.437483 0.039 Uiso 1 1 calc R U . . .
C033 C 0.7629(4) 0.4711(3) 0.3294(3) 0.0327(12) Uani 1 1 d . . . . .
H033 H 0.779436 0.517255 0.320684 0.039 Uiso 1 1 calc R U . . .
C037 C 0.5802(5) 0.2108(4) 0.0050(3) 0.0446(15) Uani 1 1 d . . . . .
H037 H 0.569346 0.199622 -0.045266 0.054 Uiso 1 1 calc R U . . .
Pt3 Pt 0.35065(2) 0.26432(2) 0.12946(2) 0.01976(6) Uani 1 1 d . . . . .
Pt4 Pt 0.15250(2) 0.30377(2) 0.16228(2) 0.02135(6) Uani 1 1 d . . . . .
S3 S 0.28211(10) 0.21736(7) 0.00973(6) 0.0276(3) Uani 1 1 d . . . . .
S4 S 0.18394(10) 0.41130(7) 0.13230(7) 0.0309(3) Uani 1 1 d . . . . .
O00N O 0.0998(3) 0.20334(19) -0.06358(17) 0.0265(7) Uani 1 1 d . . . . .
O00O O 0.3602(3) 0.48233(19) 0.11157(18) 0.0277(7) Uani 1 1 d . . . . .
N8 N 0.1327(3) 0.2132(2) 0.1948(2) 0.0233(8) Uani 1 1 d . . . . .
N9 N 0.4141(3) 0.2969(2) 0.2354(2) 0.0249(9) Uani 1 1 d . . . . .
N10 N 0.3693(3) 0.3753(2) 0.1245(2) 0.0270(9) Uani 1 1 d . . . . .
N11 N 0.4661(3) 0.4110(2) 0.1153(2) 0.0280(9) Uani 1 1 d . . . . .
N12 N 0.1034(3) 0.2452(2) 0.0509(2) 0.0250(9) Uani 1 1 d . . . . .
N13 N 0.0042(3) 0.2385(2) 0.0150(2) 0.0265(9) Uani 1 1 d . . . . .
N14 N 0.5656(5) 0.5327(3) 0.4118(3) 0.0552(15) Uani 1 1 d . . . . .
N15 N 0.0463(5) -0.0474(3) 0.0685(3) 0.0569(15) Uani 1 1 d . . . . .
C01A C 0.1067(4) 0.1430(3) 0.1461(3) 0.0254(10) Uani 1 1 d . . . . .
H01A H 0.093216 0.137050 0.096715 0.030 Uiso 1 1 calc R U . . .
C01D C 0.1879(4) 0.3039(3) 0.3075(3) 0.0328(12) Uani 1 1 d . . . . .
C01F C 0.4071(3) 0.2429(3) 0.2655(2) 0.0215(9) Uani 1 1 d . . . . .
C01I C 0.0057(4) 0.2134(3) -0.0510(3) 0.0267(10) Uani 1 1 d . . . . .
C01M C 0.3984(5) 0.2113(3) 0.3783(3) 0.0359(13) Uani 1 1 d . . . . .
H01M H 0.361452 0.161303 0.352281 0.043 Uiso 1 1 calc R U . . .
C01N C 0.4275(4) 0.2625(3) 0.3417(3) 0.0279(11) Uani 1 1 d . . . . .
C01Q C 0.3871(4) 0.1028(3) 0.2272(3) 0.0275(10) Uani 1 1 d . . . . .
H01Q H 0.411728 0.105146 0.274600 0.033 Uiso 1 1 calc R U . . .
C01T C 0.1496(4) 0.2247(3) 0.2656(3) 0.0303(11) Uani 1 1 d . . . . .
C01U C 0.0996(4) 0.0813(3) 0.1666(3) 0.0321(11) Uani 1 1 d . . . . .
C01X C 0.3244(4) 0.0966(3) 0.0870(3) 0.0278(10) Uani 1 1 d . . . . .
H01X H 0.304775 0.093651 0.038799 0.033 Uiso 1 1 calc R U . . .
C01Y C 0.6277(5) 0.5108(3) 0.0827(3) 0.0377(13) Uani 1 1 d . . . . .
H01Y H 0.638625 0.464505 0.084342 0.045 Uiso 1 1 calc R U . . .
C01Z C 0.4747(4) 0.3383(3) 0.3834(3) 0.0298(11) Uani 1 1 d . . . . .
C02A C 0.3599(4) 0.0354(3) 0.1724(3) 0.0320(11) Uani 1 1 d . . . . .
H02A H 0.362468 -0.009054 0.182708 0.038 Uiso 1 1 calc R U . . .
C02C C 0.1120(4) 0.0886(4) 0.2399(3) 0.0387(13) Uani 1 1 d . . . . .
C02D C 0.5355(4) 0.5279(3) 0.0943(3) 0.0296(11) Uani 1 1 d . . . . .
C02E C 0.4567(4) 0.4723(3) 0.1075(3) 0.0268(10) Uani 1 1 d . . . . .
C02G C 0.1581(4) 0.2239(2) 0.0027(2) 0.0216(9) Uani 1 1 d . . . . .
C02J C 0.2271(4) 0.3341(4) 0.3819(3) 0.0451(16) Uani 1 1 d . . . . .
H02J H 0.229944 0.300928 0.408414 0.054 Uiso 1 1 calc DR U . . .
C02O C 0.3289(4) 0.0321(3) 0.1025(3) 0.0325(11) Uani 1 1 d . . . . .
H02O H 0.310722 -0.014456 0.065122 0.039 Uiso 1 1 calc R U . . .
C02S C 0.1292(4) 0.1609(4) 0.2897(3) 0.0361(13) Uani 1 1 d . . . . .
C02U C -0.1782(5) 0.1904(4) -0.1011(3) 0.0483(16) Uani 1 1 d . . . . .
H02U H -0.191990 0.198340 -0.054411 0.058 Uiso 1 1 calc R U . . .
C03A C 0.2587(5) 0.4566(4) 0.3776(3) 0.0509(18) Uani 1 1 d . . . . .
H03A H 0.279361 0.508888 0.401401 0.061 Uiso 1 1 calc R U . . .
C03B C 0.4240(6) 0.2344(4) 0.4517(3) 0.0509(17) Uani 1 1 d . . . . .
H03B H 0.404628 0.199671 0.475759 0.061 Uiso 1 1 calc R U . . .
C03C C -0.2583(6) 0.1736(4) -0.1591(4) 0.0580(18) Uani 1 1 d . . . . .
H03C H -0.327050 0.168972 -0.152029 0.070 Uiso 1 1 calc R U . . .
C03E C -0.0595(5) 0.1848(4) -0.1800(3) 0.0426(14) Uani 1 1 d . . . . .
H03E H 0.008863 0.188655 -0.187787 0.051 Uiso 1 1 calc R U . . .
C03F C 0.1203(5) 0.1650(5) 0.3608(3) 0.055(2) Uani 1 1 d . . . . .
H03F H 0.121606 0.211592 0.394208 0.066 Uiso 1 1 calc DR U . . .
C03H C 0.1011(5) 0.0252(4) 0.2626(4) 0.0569(18) Uani 1 1 d . . . . .
H03H H 0.093017 -0.022828 0.229217 0.068 Uiso 1 1 calc R U . . .
C03I C 0.1100(5) 0.1043(6) 0.3820(4) 0.068(3) Uani 1 1 d . . . . .
H03I H 0.107856 0.109072 0.430334 0.081 Uiso 1 1 calc R U . . .
C03J C -0.2388(6) 0.1637(4) -0.2259(3) 0.0534(18) Uani 1 1 d . . . . .
H03J H -0.293706 0.153693 -0.264810 0.064 Uiso 1 1 calc R U . . .
C03K C 0.4774(6) 0.3072(4) 0.4912(3) 0.0533(19) Uani 1 1 d . . . . .
H03K H 0.497261 0.321048 0.541547 0.064 Uiso 1 1 calc R U . . .
C03O C 0.2605(5) 0.4081(4) 0.4165(3) 0.054(2) Uani 1 1 d . . . . .
H03O H 0.284777 0.426744 0.466694 0.064 Uiso 1 1 calc R U . . .
C03P C -0.1404(6) 0.1682(4) -0.2374(3) 0.0539(18) Uani 1 1 d . . . . .
H03P H -0.127460 0.160062 -0.284306 0.065 Uiso 1 1 calc R U . . .
C03Q C 0.1025(6) 0.0339(7) 0.3325(5) 0.079(3) Uani 1 1 d . . . . .
H03Q H 0.098338 -0.008011 0.348378 0.095 Uiso 1 1 calc R U . . .
C013 C 0.3781(4) 0.1681(3) 0.2123(2) 0.0234(10) Uani 1 1 d . . . . .
C015 C 0.3480(3) 0.1660(3) 0.1408(2) 0.0202(9) Uani 1 1 d . . . . .
C019 C 0.1916(4) 0.3532(3) 0.2672(3) 0.0328(12) Uani 1 1 d . . . . .
C020 C 0.4519(4) 0.3704(3) 0.2755(3) 0.0291(11) Uani 1 1 d . . . . .
H020 H 0.453177 0.407208 0.252825 0.035 Uiso 1 1 calc R U . . .
C022 C 0.4877(4) 0.3920(3) 0.3470(3) 0.0300(11) Uani 1 1 d . . . . .
C023 C 0.2271(4) 0.4291(3) 0.3047(3) 0.0394(13) Uani 1 1 d . . . . .
H023 H 0.229722 0.463193 0.278828 0.047 Uiso 1 1 calc R U . . .
C024 C -0.0783(4) 0.1955(3) -0.1122(3) 0.0326(11) Uani 1 1 d . . . . .
C026 C 0.3092(4) 0.4193(3) 0.1227(2) 0.0240(10) Uani 1 1 d . . . . .
C030 C 0.5309(4) 0.4697(3) 0.3846(3) 0.0397(13) Uani 1 1 d . . . . .
C032 C 0.7044(5) 0.5619(4) 0.0686(3) 0.0469(15) Uani 1 1 d . . . . .
H032 H 0.767739 0.550608 0.060590 0.056 Uiso 1 1 calc R U . . .
C034 C 0.5191(5) 0.5957(3) 0.0921(3) 0.0403(13) Uani 1 1 d . . . . .
H034 H 0.456394 0.607685 0.100736 0.048 Uiso 1 1 calc R U . . .
C035 C 0.0720(5) 0.0095(4) 0.1120(4) 0.0416(14) Uani 1 1 d . . . . .
C036 C 0.5016(5) 0.3588(4) 0.4582(3) 0.0445(15) Uani 1 1 d . . . . .
H036 H 0.536615 0.408842 0.485620 0.053 Uiso 1 1 calc R U . . .
C038 C 0.6875(6) 0.6288(4) 0.0663(3) 0.0522(18) Uani 1 1 d . . . . .
H038 H 0.739798 0.663814 0.057111 0.063 Uiso 1 1 calc R U . . .
C039 C 0.5957(6) 0.6456(4) 0.0771(3) 0.0499(17) Uani 1 1 d . . . . .
H039 H 0.584512 0.691531 0.074360 0.060 Uiso 1 1 calc R U . . .
Cl Cl 0.5910(3) 0.80989(16) 0.25769(15) 0.1065(10) Uani 1 1 d . . . . .
Cl0A Cl 0.54785(17) 0.93447(12) 0.21993(10) 0.0690(5) Uani 1 1 d . . . . .
Cl0C Cl 0.6931(2) 0.85978(12) 0.15770(11) 0.0799(6) Uani 1 1 d . . . . .
C03T C 0.6445(7) 0.8883(5) 0.2337(4) 0.068(2) Uani 1 1 d . . . . .
H03T H 0.701521 0.923158 0.273407 0.081 Uiso 1 1 calc R U . . .
Cl0B Cl 0.79408(16) -0.09765(15) 0.43389(11) 0.0765(6) Uani 1 1 d . . . . .
Cl0E Cl 0.8859(2) -0.13304(17) 0.31120(12) 0.0943(8) Uani 1 1 d . . . . .
Cl09 Cl 1.00774(15) -0.09806(12) 0.45071(11) 0.0670(5) Uani 1 1 d . . . . .
C03V C 0.9026(7) -0.0835(6) 0.4005(5) 0.072(2) Uani 1 1 d . . . . .
H03V H 0.921376 -0.029664 0.404670 0.086 Uiso 1 1 calc R U . . .
Cl0D Cl 0.4355(2) 0.57807(16) 0.29014(14) 0.0933(7) Uani 1 1 d . . . . .
Cl1 Cl 0.3793(4) 0.69024(18) 0.2410(2) 0.1349(13) Uani 1 1 d . . . . .
Cl6 Cl 0.2647(3) 0.63459(16) 0.33360(14) 0.1076(10) Uani 1 1 d . . . . .
C03U C 0.3335(9) 0.6127(5) 0.2647(4) 0.078(3) Uani 1 1 d . . . . .
H03U H 0.285740 0.573573 0.222243 0.093 Uiso 1 1 calc R U . . .
Cl3 Cl 0.1042(3) 0.6287(2) 0.17658(17) 0.1232(11) Uani 1 1 d . . . . .
Cl4 Cl 0.2081(2) 0.5916(2) 0.05901(15) 0.1089(10) Uani 1 1 d . . . . .
Cl5 Cl -0.0022(2) 0.59894(17) 0.03530(17) 0.1031(8) Uani 1 1 d . . . . .
C9A C 0.112(3) 0.633(2) 0.0977(18) 0.081(6) Uani 0.284(19) 1 d . U P A 1
H9A H 0.135504 0.687102 0.103909 0.098 Uiso 0.284(19) 1 calc R U P A 1
C9B C 0.0920(12) 0.5749(10) 0.0857(8) 0.088(4) Uani 0.716(19) 1 d . U P A 2
H9B H 0.068672 0.520838 0.080075 0.106 Uiso 0.716(19) 1 calc R U P A 2


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Pt1 Pt2 3.0124(3) . ?
Pt1 S1 2.3071(12) . ?
Pt1 N2 2.122(4) . ?
Pt1 N3 2.033(4) . ?
Pt1 C014 1.986(5) . ?
Pt2 S2 2.3028(11) . ?
Pt2 N5 2.133(4) . ?
Pt2 N7 2.037(4) . ?
Pt2 C016 1.979(5) . ?
S1 C01O 1.711(5) . ?
S2 C02B 1.706(5) . ?
O00K C01L 1.367(6) . ?
O00K C02B 1.368(5) . ?
O00M C01O 1.359(6) . ?
O00M C021 1.371(6) . ?
N1 N2 1.417(6) . ?
N1 C01L 1.277(7) . ?
N2 C02B 1.305(6) . ?
N3 C01C 1.363(6) . ?
N3 C017 1.357(6) . ?
N4 C02Y 1.146(8) . ?
N5 N6 1.411(6) . ?
N5 C01O 1.305(6) . ?
N6 C021 1.282(6) . ?
N7 C01E 1.372(6) . ?
N7 C018 1.338(6) . ?
N16 C02N 1.140(7) . ?
C01B C01H 1.435(7) . ?
C01B C01K 1.420(7) . ?
C01B C018 1.438(6) . ?
C01C H01C 0.9500 . ?
C01C C01R 1.359(7) . ?
C01E H01E 0.9500 . ?
C01E C01J 1.357(7) . ?
C01G H01G 0.9500 . ?
C01G C012 1.413(7) . ?
C01G C033 1.362(7) . ?
C01H C01J 1.417(7) . ?
C01H C02P 1.404(7) . ?
C01J C02N 1.440(7) . ?
C01K H01K 0.9500 . ?
C01K C02R 1.347(8) . ?
C01L C02K 1.464(7) . ?
C01P H01P 0.9500 . ?
C01P C016 1.402(7) . ?
C01P C031 1.375(7) . ?
C01R C01S 1.422(8) . ?
C01R C02Y 1.440(8) . ?
C01S C02I 1.419(8) . ?
C01S C02X 1.419(8) . ?
C01W H01W 0.9500 . ?
C01W C02H 1.395(8) . ?
C01W C014 1.394(7) . ?
C02F C02L 1.400(8) . ?
C02F C02T 1.385(7) . ?
C02F C021 1.460(7) . ?
C02H H02H 0.9500 . ?
C02H C03D 1.380(9) . ?
C02I C017 1.439(7) . ?
C02I C025 1.422(8) . ?
C02K C02V 1.390(9) . ?
C02K C03G 1.384(8) . ?
C02L H02L 0.9500 . ?
C02L C02Q 1.389(8) . ?
C02M H02M 0.9500 . ?
C02M C03D 1.366(8) . ?
C02M C010 1.407(7) . ?
C02P H02P 0.9500 . ?
C02P C037 1.359(9) . ?
C02Q H02Q 0.9500 . ?
C02Q C02W 1.381(9) . ?
C02R H02R 0.9500 . ?
C02R C037 1.401(9) . ?
C02T H02T 0.9500 . ?
C02T C02Z 1.377(8) . ?
C02V H02V 0.9500 . ?
C02V C03L 1.389(8) . ?
C02W H02W 0.9500 . ?
C02W C02Z 1.377(9) . ?
C02X H02X 0.9500 . ?
C02X C03S 1.376(10) . ?
C02Z H02Z 0.9500 . ?
C03D H03D 0.9500 . ?
C03G H03G 0.9500 . ?
C03G C03R 1.396(9) . ?
C03L H03L 0.9500 . ?
C03L C03N 1.378(11) . ?
C03M H03M 0.9500 . ?
C03M C03S 1.397(12) . ?
C03M C025 1.356(9) . ?
C03N H03N 0.9500 . ?
C03N C03R 1.370(11) . ?
C03R H03R 0.9500 . ?
C03S H03S 0.9500 . ?
C010 C014 1.427(7) . ?
C010 C017 1.453(7) . ?
C012 C016 1.424(7) . ?
C012 C018 1.474(6) . ?
C025 H025 0.9500 . ?
C031 H031 0.9500 . ?
C031 C033 1.388(8) . ?
C033 H033 0.9500 . ?
C037 H037 0.9500 . ?
Pt3 Pt4 3.0395(3) . ?
Pt3 S3 2.2904(12) . ?
Pt3 N9 2.040(4) . ?
Pt3 N10 2.150(4) . ?
Pt3 C015 1.980(5) . ?
Pt4 S4 2.3082(13) . ?
Pt4 N8 2.025(4) . ?
Pt4 N12 2.130(4) . ?
Pt4 C019 1.986(5) . ?
S3 C02G 1.703(5) . ?
S4 C026 1.712(5) . ?
O00N C01I 1.373(6) . ?
O00N C02G 1.356(6) . ?
O00O C02E 1.370(6) . ?
O00O C026 1.368(6) . ?
N8 C01A 1.367(6) . ?
N8 C01T 1.350(6) . ?
N9 C01F 1.346(6) . ?
N9 C020 1.367(6) . ?
N10 N11 1.413(6) . ?
N10 C026 1.302(6) . ?
N11 C02E 1.274(7) . ?
N12 N13 1.404(6) . ?
N12 C02G 1.314(6) . ?
N13 C01I 1.272(6) . ?
N14 C030 1.150(8) . ?
N15 C035 1.141(8) . ?
C01A H01A 0.9500 . ?
C01A C01U 1.366(7) . ?
C01D C01T 1.465(8) . ?
C01D C02J 1.415(7) . ?
C01D C019 1.416(8) . ?
C01F C01N 1.435(7) . ?
C01F C013 1.467(7) . ?
C01I C024 1.466(7) . ?
C01M H01M 0.9500 . ?
C01M C01N 1.419(8) . ?
C01M C03B 1.379(8) . ?
C01N C01Z 1.424(7) . ?
C01Q H01Q 0.9500 . ?
C01Q C02A 1.384(7) . ?
C01Q C013 1.409(7) . ?
C01T C02S 1.444(8) . ?
C01U C02C 1.416(8) . ?
C01U C035 1.439(9) . ?
C01X H01X 0.9500 . ?
C01X C02O 1.385(7) . ?
C01X C015 1.402(7) . ?
C01Y H01Y 0.9500 . ?
C01Y C02D 1.387(8) . ?
C01Y C032 1.399(8) . ?
C01Z C022 1.432(8) . ?
C01Z C036 1.409(7) . ?
C02A H02A 0.9500 . ?
C02A C02O 1.388(8) . ?
C02C C02S 1.417(9) . ?
C02C C03H 1.419(8) . ?
C02D C02E 1.461(7) . ?
C02D C034 1.391(8) . ?
C02J H02J 0.9500 . ?
C02J C03O 1.350(10) . ?
C02O H02O 0.9500 . ?
C02S C03F 1.423(7) . ?
C02U H02U 0.9500 . ?
C02U C03C 1.395(9) . ?
C02U C024 1.388(9) . ?
C03A H03A 0.9500 . ?
C03A C03O 1.387(11) . ?
C03A C023 1.376(8) . ?
C03B H03B 0.9500 . ?
C03B C03K 1.388(11) . ?
C03C H03C 0.9500 . ?
C03C C03J 1.362(10) . ?
C03E H03E 0.9500 . ?
C03E C03P 1.394(8) . ?
C03E C024 1.378(8) . ?
C03F H03F 0.9500 . ?
C03F C03I 1.352(11) . ?
C03H H03H 0.9500 . ?
C03H C03Q 1.357(11) . ?
C03I H03I 0.9500 . ?
C03I C03Q 1.409(14) . ?
C03J H03J 0.9500 . ?
C03J C03P 1.371(11) . ?
C03K H03K 0.9500 . ?
C03K C036 1.362(10) . ?
C03O H03O 0.9500 . ?
C03P H03P 0.9500 . ?
C03Q H03Q 0.9500 . ?
C013 C015 1.424(6) . ?
C019 C023 1.390(8) . ?
C020 H020 0.9500 . ?
C020 C022 1.360(7) . ?
C022 C030 1.429(8) . ?
C023 H023 0.9500 . ?
C032 H032 0.9500 . ?
C032 C038 1.378(10) . ?
C034 H034 0.9500 . ?
C034 C039 1.392(9) . ?
C036 H036 0.9500 . ?
C038 H038 0.9500 . ?
C038 C039 1.378(11) . ?
C039 H039 0.9500 . ?
Cl C03T 1.769(9) . ?
Cl0A C03T 1.770(9) . ?
Cl0C C03T 1.724(8) . ?
C03T H03T 1.0000 . ?
Cl0B C03V 1.695(9) . ?
Cl0E C03V 1.725(9) . ?
Cl09 C03V 1.757(9) . ?
C03V H03V 1.0000 . ?
Cl0D C03U 1.740(11) . ?
Cl1 C03U 1.726(9) . ?
Cl6 C03U 1.760(9) . ?
C03U H03U 1.0000 . ?
Cl3 C9A 1.62(3) . ?
Cl3 C9B 1.780(15) . ?
Cl4 C9A 1.80(4) . ?
Cl4 C9B 1.724(16) . ?
Cl5 C9A 1.74(4) . ?
Cl5 C9B 1.750(16) . ?
C9A H9A 1.0000 . ?
C9B H9B 1.0000 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
S1 Pt1 Pt2 91.66(3) . . ?
N2 Pt1 Pt2 77.81(11) . . ?
N2 Pt1 S1 88.02(12) . . ?
N3 Pt1 Pt2 89.84(11) . . ?
N3 Pt1 S1 176.55(11) . . ?
N3 Pt1 N2 95.33(16) . . ?
C014 Pt1 Pt2 105.08(13) . . ?
C014 Pt1 S1 96.19(16) . . ?
C014 Pt1 N2 174.78(18) . . ?
C014 Pt1 N3 80.43(19) . . ?
S2 Pt2 Pt1 93.21(3) . . ?
N5 Pt2 Pt1 79.93(11) . . ?
N5 Pt2 S2 86.65(11) . . ?
N7 Pt2 Pt1 87.67(11) . . ?
N7 Pt2 S2 176.10(12) . . ?
N7 Pt2 N5 97.24(15) . . ?
C016 Pt2 Pt1 102.07(13) . . ?
C016 Pt2 S2 96.18(14) . . ?
C016 Pt2 N5 176.41(18) . . ?
C016 Pt2 N7 79.93(17) . . ?
C01O S1 Pt1 104.09(16) . . ?
C02B S2 Pt2 101.81(16) . . ?
C01L O00K C02B 103.5(4) . . ?
C01O O00M C021 103.9(4) . . ?
C01L N1 N2 104.7(4) . . ?
N1 N2 Pt1 118.2(3) . . ?
C02B N2 Pt1 132.2(3) . . ?
C02B N2 N1 108.1(4) . . ?
C01C N3 Pt1 121.9(3) . . ?
C017 N3 Pt1 115.8(3) . . ?
C017 N3 C01C 121.7(4) . . ?
N6 N5 Pt2 120.3(3) . . ?
C01O N5 Pt2 130.6(3) . . ?
C01O N5 N6 107.8(4) . . ?
C021 N6 N5 105.4(4) . . ?
C01E N7 Pt2 120.6(3) . . ?
C018 N7 Pt2 117.8(3) . . ?
C018 N7 C01E 121.5(4) . . ?
C01H C01B C018 118.5(4) . . ?
C01K C01B C01H 116.0(4) . . ?
C01K C01B C018 125.4(5) . . ?
N3 C01C H01C 119.1 . . ?
C01R C01C N3 121.7(5) . . ?
C01R C01C H01C 119.1 . . ?
N7 C01E H01E 119.3 . . ?
C01J C01E N7 121.4(5) . . ?
C01J C01E H01E 119.3 . . ?
C012 C01G H01G 119.5 . . ?
C033 C01G H01G 119.5 . . ?
C033 C01G C012 121.0(5) . . ?
C01J C01H C01B 117.5(4) . . ?
C02P C01H C01B 119.5(5) . . ?
C02P C01H C01J 123.0(5) . . ?
C01E C01J C01H 120.5(5) . . ?
C01E C01J C02N 118.7(5) . . ?
C01H C01J C02N 120.8(5) . . ?
C01B C01K H01K 118.8 . . ?
C02R C01K C01B 122.5(5) . . ?
C02R C01K H01K 118.8 . . ?
O00K C01L C02K 119.6(4) . . ?
N1 C01L O00K 113.7(4) . . ?
N1 C01L C02K 126.7(5) . . ?
O00M C01O S1 118.6(3) . . ?
N5 C01O S1 131.1(4) . . ?
N5 C01O O00M 110.3(4) . . ?
C016 C01P H01P 119.1 . . ?
C031 C01P H01P 119.1 . . ?
C031 C01P C016 121.9(5) . . ?
C01C C01R C01S 120.0(5) . . ?
C01C C01R C02Y 119.0(5) . . ?
C01S C01R C02Y 120.7(5) . . ?
C02I C01S C01R 118.1(5) . . ?
C02I C01S C02X 120.2(5) . . ?
C02X C01S C01R 121.6(6) . . ?
C02H C01W H01W 119.5 . . ?
C014 C01W H01W 119.5 . . ?
C014 C01W C02H 121.1(6) . . ?
O00K C02B S2 118.5(3) . . ?
N2 C02B S2 131.4(4) . . ?
N2 C02B O00K 110.0(4) . . ?
C02L C02F C021 118.6(5) . . ?
C02T C02F C02L 119.4(5) . . ?
C02T C02F C021 121.9(5) . . ?
C01W C02H H02H 119.7 . . ?
C03D C02H C01W 120.6(6) . . ?
C03D C02H H02H 119.7 . . ?
C01S C02I C017 119.1(5) . . ?
C01S C02I C025 117.3(5) . . ?
C025 C02I C017 123.4(5) . . ?
C02V C02K C01L 118.8(5) . . ?
C03G C02K C01L 121.2(5) . . ?
C03G C02K C02V 120.0(5) . . ?
C02F C02L H02L 120.1 . . ?
C02Q C02L C02F 119.8(5) . . ?
C02Q C02L H02L 120.1 . . ?
C03D C02M H02M 119.3 . . ?
C03D C02M C010 121.4(5) . . ?
C010 C02M H02M 119.3 . . ?
N16 C02N C01J 178.5(6) . . ?
C01H C02P H02P 119.5 . . ?
C037 C02P C01H 121.0(5) . . ?
C037 C02P H02P 119.5 . . ?
C02L C02Q H02Q 120.1 . . ?
C02W C02Q C02L 119.9(6) . . ?
C02W C02Q H02Q 120.1 . . ?
C01K C02R H02R 119.9 . . ?
C01K C02R C037 120.2(5) . . ?
C037 C02R H02R 119.9 . . ?
C02F C02T H02T 119.9 . . ?
C02Z C02T C02F 120.2(6) . . ?
C02Z C02T H02T 119.9 . . ?
C02K C02V H02V 120.0 . . ?
C03L C02V C02K 119.9(6) . . ?
C03L C02V H02V 120.0 . . ?
C02Q C02W H02W 119.9 . . ?
C02Z C02W C02Q 120.2(5) . . ?
C02Z C02W H02W 119.9 . . ?
C01S C02X H02X 120.5 . . ?
C03S C02X C01S 119.1(7) . . ?
C03S C02X H02X 120.5 . . ?
N4 C02Y C01R 178.4(6) . . ?
C02T C02Z C02W 120.5(6) . . ?
C02T C02Z H02Z 119.7 . . ?
C02W C02Z H02Z 119.7 . . ?
C02H C03D H03D 120.2 . . ?
C02M C03D C02H 119.7(5) . . ?
C02M C03D H03D 120.2 . . ?
C02K C03G H03G 120.3 . . ?
C02K C03G C03R 119.4(7) . . ?
C03R C03G H03G 120.3 . . ?
C02V C03L H03L 120.1 . . ?
C03N C03L C02V 119.8(7) . . ?
C03N C03L H03L 120.1 . . ?
C03S C03M H03M 120.0 . . ?
C025 C03M H03M 120.0 . . ?
C025 C03M C03S 119.9(7) . . ?
C03L C03N H03N 119.7 . . ?
C03R C03N C03L 120.6(6) . . ?
C03R C03N H03N 119.7 . . ?
C03G C03R H03R 119.9 . . ?
C03N C03R C03G 120.3(7) . . ?
C03N C03R H03R 119.9 . . ?
C02X C03S C03M 121.3(6) . . ?
C02X C03S H03S 119.4 . . ?
C03M C03S H03S 119.4 . . ?
C02M C010 C014 119.1(5) . . ?
C02M C010 C017 125.5(5) . . ?
C014 C010 C017 115.1(4) . . ?
C01G C012 C016 119.5(4) . . ?
C01G C012 C018 125.9(4) . . ?
C016 C012 C018 114.5(4) . . ?
C01W C014 Pt1 128.0(4) . . ?
C01W C014 C010 117.9(5) . . ?
C010 C014 Pt1 114.0(4) . . ?
C01P C016 Pt2 127.5(4) . . ?
C01P C016 C012 117.3(4) . . ?
C012 C016 Pt2 115.1(3) . . ?
N3 C017 C02I 118.7(5) . . ?
N3 C017 C010 112.8(4) . . ?
C02I C017 C010 128.5(5) . . ?
N7 C018 C01B 119.6(4) . . ?
N7 C018 C012 112.5(4) . . ?
C01B C018 C012 127.8(4) . . ?
O00M C021 C02F 119.7(4) . . ?
N6 C021 O00M 112.6(4) . . ?
N6 C021 C02F 127.8(5) . . ?
C02I C025 H025 119.1 . . ?
C03M C025 C02I 121.9(7) . . ?
C03M C025 H025 119.1 . . ?
C01P C031 H031 119.8 . . ?
C01P C031 C033 120.4(5) . . ?
C033 C031 H031 119.8 . . ?
C01G C033 C031 119.9(5) . . ?
C01G C033 H033 120.1 . . ?
C031 C033 H033 120.1 . . ?
C02P C037 C02R 120.0(5) . . ?
C02P C037 H037 120.0 . . ?
C02R C037 H037 120.0 . . ?
S3 Pt3 Pt4 91.37(3) . . ?
N9 Pt3 Pt4 91.50(11) . . ?
N9 Pt3 S3 174.77(12) . . ?
N9 Pt3 N10 95.49(16) . . ?
N10 Pt3 Pt4 75.61(11) . . ?
N10 Pt3 S3 89.46(12) . . ?
C015 Pt3 Pt4 108.20(12) . . ?
C015 Pt3 S3 95.07(14) . . ?
C015 Pt3 N9 79.87(17) . . ?
C015 Pt3 N10 173.96(17) . . ?
S4 Pt4 Pt3 95.34(3) . . ?
N8 Pt4 Pt3 83.43(11) . . ?
N8 Pt4 S4 175.99(12) . . ?
N8 Pt4 N12 96.99(15) . . ?
N12 Pt4 Pt3 80.54(12) . . ?
N12 Pt4 S4 86.55(11) . . ?
C019 Pt4 Pt3 101.08(15) . . ?
C019 Pt4 S4 96.62(18) . . ?
C019 Pt4 N8 79.9(2) . . ?
C019 Pt4 N12 176.3(2) . . ?
C02G S3 Pt3 105.06(15) . . ?
C026 S4 Pt4 100.16(17) . . ?
C02G O00N C01I 103.6(4) . . ?
C026 O00O C02E 103.6(4) . . ?
C01A N8 Pt4 120.6(3) . . ?
C01T N8 Pt4 117.9(4) . . ?
C01T N8 C01A 121.5(4) . . ?
C01F N9 Pt3 116.6(3) . . ?
C01F N9 C020 121.4(4) . . ?
C020 N9 Pt3 121.7(3) . . ?
N11 N10 Pt3 116.9(3) . . ?
C026 N10 Pt3 135.5(3) . . ?
C026 N10 N11 107.3(4) . . ?
C02E N11 N10 106.0(4) . . ?
N13 N12 Pt4 121.1(3) . . ?
C02G N12 Pt4 129.6(3) . . ?
C02G N12 N13 107.9(4) . . ?
C01I N13 N12 105.4(4) . . ?
N8 C01A H01A 119.1 . . ?
C01U C01A N8 121.7(5) . . ?
C01U C01A H01A 119.1 . . ?
C02J C01D C01T 126.2(6) . . ?
C02J C01D C019 118.5(6) . . ?
C019 C01D C01T 115.1(4) . . ?
N9 C01F C01N 119.7(4) . . ?
N9 C01F C013 112.4(4) . . ?
C01N C01F C013 127.9(4) . . ?
O00N C01I C024 118.6(4) . . ?
N13 C01I O00N 113.2(4) . . ?
N13 C01I C024 128.2(5) . . ?
C01N C01M H01M 120.1 . . ?
C03B C01M H01M 120.1 . . ?
C03B C01M C01N 119.8(6) . . ?
C01M C01N C01F 123.7(5) . . ?
C01M C01N C01Z 117.7(5) . . ?
C01Z C01N C01F 118.5(5) . . ?
C02A C01Q H01Q 120.2 . . ?
C02A C01Q C013 119.7(5) . . ?
C013 C01Q H01Q 120.2 . . ?
N8 C01T C01D 112.1(5) . . ?
N8 C01T C02S 118.6(5) . . ?
C02S C01T C01D 129.3(5) . . ?
C01A C01U C02C 119.9(5) . . ?
C01A C01U C035 118.1(5) . . ?
C02C C01U C035 121.8(5) . . ?
C02O C01X H01X 119.1 . . ?
C02O C01X C015 121.7(5) . . ?
C015 C01X H01X 119.1 . . ?
C02D C01Y H01Y 120.1 . . ?
C02D C01Y C032 119.8(6) . . ?
C032 C01Y H01Y 120.1 . . ?
C01N C01Z C022 117.6(4) . . ?
C036 C01Z C01N 120.1(5) . . ?
C036 C01Z C022 122.2(5) . . ?
C01Q C02A H02A 119.7 . . ?
C01Q C02A C02O 120.5(5) . . ?
C02O C02A H02A 119.7 . . ?
C01U C02C C02S 117.9(5) . . ?
C01U C02C C03H 121.1(6) . . ?
C02S C02C C03H 120.9(6) . . ?
C01Y C02D C02E 118.0(5) . . ?
C01Y C02D C034 120.4(5) . . ?
C034 C02D C02E 121.6(5) . . ?
O00O C02E C02D 120.7(4) . . ?
N11 C02E O00O 112.6(4) . . ?
N11 C02E C02D 126.7(5) . . ?
O00N C02G S3 118.0(3) . . ?
N12 C02G S3 132.1(4) . . ?
N12 C02G O00N 109.9(4) . . ?
C01D C02J H02J 118.8 . . ?
C03O C02J C01D 122.5(6) . . ?
C03O C02J H02J 118.8 . . ?
C01X C02O C02A 120.1(5) . . ?
C01X C02O H02O 120.0 . . ?
C02A C02O H02O 120.0 . . ?
C02C C02S C01T 119.2(5) . . ?
C02C C02S C03F 116.6(6) . . ?
C03F C02S C01T 124.2(6) . . ?
C03C C02U H02U 120.3 . . ?
C024 C02U H02U 120.3 . . ?
C024 C02U C03C 119.3(6) . . ?
C03O C03A H03A 119.9 . . ?
C023 C03A H03A 119.9 . . ?
C023 C03A C03O 120.1(6) . . ?
C01M C03B H03B 119.3 . . ?
C01M C03B C03K 121.4(6) . . ?
C03K C03B H03B 119.3 . . ?
C02U C03C H03C 119.7 . . ?
C03J C03C C02U 120.6(7) . . ?
C03J C03C H03C 119.7 . . ?
C03P C03E H03E 119.9 . . ?
C024 C03E H03E 119.9 . . ?
C024 C03E C03P 120.3(6) . . ?
C02S C03F H03F 119.2 . . ?
C03I C03F C02S 121.6(8) . . ?
C03I C03F H03F 119.2 . . ?
C02C C03H H03H 120.4 . . ?
C03Q C03H C02C 119.2(8) . . ?
C03Q C03H H03H 120.4 . . ?
C03F C03I H03I 119.9 . . ?
C03F C03I C03Q 120.2(7) . . ?
C03Q C03I H03I 119.9 . . ?
C03C C03J H03J 119.8 . . ?
C03C C03J C03P 120.5(6) . . ?
C03P C03J H03J 119.8 . . ?
C03B C03K H03K 119.8 . . ?
C036 C03K C03B 120.3(5) . . ?
C036 C03K H03K 119.8 . . ?
C02J C03O C03A 118.9(5) . . ?
C02J C03O H03O 120.6 . . ?
C03A C03O H03O 120.6 . . ?
C03E C03P H03P 120.1 . . ?
C03J C03P C03E 119.7(6) . . ?
C03J C03P H03P 120.1 . . ?
C03H C03Q C03I 120.9(7) . . ?
C03H C03Q H03Q 119.5 . . ?
C03I C03Q H03Q 119.5 . . ?
C01Q C013 C01F 124.6(4) . . ?
C01Q C013 C015 120.5(4) . . ?
C015 C013 C01F 114.6(4) . . ?
C01X C015 Pt3 127.8(4) . . ?
C01X C015 C013 117.4(4) . . ?
C013 C015 Pt3 114.8(3) . . ?
C01D C019 Pt4 114.8(4) . . ?
C023 C019 Pt4 127.8(5) . . ?
C023 C019 C01D 117.2(5) . . ?
N9 C020 H020 119.2 . . ?
C022 C020 N9 121.5(5) . . ?
C022 C020 H020 119.2 . . ?
C020 C022 C01Z 120.0(5) . . ?
C020 C022 C030 118.2(5) . . ?
C030 C022 C01Z 121.7(5) . . ?
C03A C023 C019 122.6(7) . . ?
C03A C023 H023 118.7 . . ?
C019 C023 H023 118.7 . . ?
C02U C024 C01I 119.2(5) . . ?
C03E C024 C01I 121.2(5) . . ?
C03E C024 C02U 119.6(5) . . ?
O00O C026 S4 118.0(3) . . ?
N10 C026 S4 131.6(4) . . ?
N10 C026 O00O 110.4(4) . . ?
N14 C030 C022 176.8(7) . . ?
C01Y C032 H032 120.3 . . ?
C038 C032 C01Y 119.5(7) . . ?
C038 C032 H032 120.3 . . ?
C02D C034 H034 120.4 . . ?
C02D C034 C039 119.2(6) . . ?
C039 C034 H034 120.4 . . ?
N15 C035 C01U 177.4(7) . . ?
C01Z C036 H036 119.9 . . ?
C03K C036 C01Z 120.2(6) . . ?
C03K C036 H036 119.9 . . ?
C032 C038 H038 119.6 . . ?
C032 C038 C039 120.8(6) . . ?
C039 C038 H038 119.6 . . ?
C034 C039 H039 119.8 . . ?
C038 C039 C034 120.3(6) . . ?
C038 C039 H039 119.8 . . ?
Cl C03T Cl0A 109.0(5) . . ?
Cl C03T H03T 109.1 . . ?
Cl0A C03T H03T 109.1 . . ?
Cl0C C03T Cl 109.5(4) . . ?
Cl0C C03T Cl0A 110.9(5) . . ?
Cl0C C03T H03T 109.1 . . ?
Cl0B C03V Cl0E 113.6(5) . . ?
Cl0B C03V Cl09 112.8(5) . . ?
Cl0B C03V H03V 106.2 . . ?
Cl0E C03V Cl09 111.1(5) . . ?
Cl0E C03V H03V 106.2 . . ?
Cl09 C03V H03V 106.2 . . ?
Cl0D C03U Cl6 111.0(5) . . ?
Cl0D C03U H03U 108.5 . . ?
Cl1 C03U Cl0D 109.8(6) . . ?
Cl1 C03U Cl6 110.6(4) . . ?
Cl1 C03U H03U 108.5 . . ?
Cl6 C03U H03U 108.5 . . ?
Cl3 C9A Cl4 115(2) . . ?
Cl3 C9A Cl5 116(2) . . ?
Cl3 C9A H9A 105.7 . . ?
Cl4 C9A H9A 105.7 . . ?
Cl5 C9A Cl4 108(2) . . ?
Cl5 C9A H9A 105.7 . . ?
Cl3 C9B H9B 109.1 . . ?
Cl4 C9B Cl3 110.7(9) . . ?
Cl4 C9B Cl5 111.5(8) . . ?
Cl4 C9B H9B 109.1 . . ?
Cl5 C9B Cl3 107.3(9) . . ?
Cl5 C9B H9B 109.1 . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Pt1 S1 C01O O00M 177.3(3) . . . . ?
Pt1 S1 C01O N5 -2.1(5) . . . . ?
Pt1 N2 C02B S2 -17.0(7) . . . . ?
Pt1 N2 C02B O00K 164.3(3) . . . . ?
Pt1 N3 C01C C01R -172.1(4) . . . . ?
Pt1 N3 C017 C02I 164.7(3) . . . . ?
Pt1 N3 C017 C010 -15.4(5) . . . . ?
Pt2 S2 C02B O00K 176.6(3) . . . . ?
Pt2 S2 C02B N2 -2.0(5) . . . . ?
Pt2 N5 N6 C021 -167.8(3) . . . . ?
Pt2 N5 C01O S1 -14.1(7) . . . . ?
Pt2 N5 C01O O00M 166.5(3) . . . . ?
Pt2 N7 C01E C01J -172.1(4) . . . . ?
Pt2 N7 C018 C01B -178.5(3) . . . . ?
Pt2 N7 C018 C012 4.8(5) . . . . ?
O00K C01L C02K C02V -172.8(5) . . . . ?
O00K C01L C02K C03G 7.6(8) . . . . ?
N1 N2 C02B S2 177.4(4) . . . . ?
N1 N2 C02B O00K -1.3(5) . . . . ?
N1 C01L C02K C02V 9.5(9) . . . . ?
N1 C01L C02K C03G -170.2(6) . . . . ?
N2 N1 C01L O00K 0.5(6) . . . . ?
N2 N1 C01L C02K 178.4(5) . . . . ?
N3 C01C C01R C01S 5.9(8) . . . . ?
N3 C01C C01R C02Y 179.6(5) . . . . ?
N5 N6 C021 O00M -0.6(5) . . . . ?
N5 N6 C021 C02F 178.7(5) . . . . ?
N6 N5 C01O S1 179.4(4) . . . . ?
N6 N5 C01O O00M 0.0(5) . . . . ?
N7 C01E C01J C01H -7.2(7) . . . . ?
N7 C01E C01J C02N 175.8(4) . . . . ?
C01B C01H C01J C01E 2.1(7) . . . . ?
C01B C01H C01J C02N 179.1(5) . . . . ?
C01B C01H C02P C037 -5.7(8) . . . . ?
C01B C01K C02R C037 2.8(9) . . . . ?
C01C N3 C017 C02I -6.4(7) . . . . ?
C01C N3 C017 C010 173.6(4) . . . . ?
C01C C01R C01S C02I -2.0(7) . . . . ?
C01C C01R C01S C02X 174.1(5) . . . . ?
C01E N7 C018 C01B 6.4(6) . . . . ?
C01E N7 C018 C012 -170.3(4) . . . . ?
C01G C012 C016 Pt2 -173.5(3) . . . . ?
C01G C012 C016 C01P 3.1(7) . . . . ?
C01G C012 C018 N7 170.9(4) . . . . ?
C01G C012 C018 C01B -5.5(8) . . . . ?
C01H C01B C01K C02R -9.4(8) . . . . ?
C01H C01B C018 N7 -11.1(6) . . . . ?
C01H C01B C018 C012 165.0(4) . . . . ?
C01H C02P C037 C02R -1.3(9) . . . . ?
C01J C01H C02P C037 173.0(5) . . . . ?
C01K C01B C01H C01J -168.1(4) . . . . ?
C01K C01B C01H C02P 10.6(7) . . . . ?
C01K C01B C018 N7 163.3(5) . . . . ?
C01K C01B C018 C012 -20.6(8) . . . . ?
C01K C02R C037 C02P 2.8(10) . . . . ?
C01L O00K C02B S2 -177.3(3) . . . . ?
C01L O00K C02B N2 1.5(5) . . . . ?
C01L N1 N2 Pt1 -167.5(3) . . . . ?
C01L N1 N2 C02B 0.5(5) . . . . ?
C01L C02K C02V C03L -177.6(6) . . . . ?
C01L C02K C03G C03R 178.1(6) . . . . ?
C01O O00M C021 N6 0.6(5) . . . . ?
C01O O00M C021 C02F -178.7(4) . . . . ?
C01O N5 N6 C021 0.4(5) . . . . ?
C01P C031 C033 C01G 0.3(8) . . . . ?
C01R C01S C02I C017 -5.7(7) . . . . ?
C01R C01S C02I C025 169.2(5) . . . . ?
C01R C01S C02X C03S -171.5(6) . . . . ?
C01S C02I C017 N3 9.9(7) . . . . ?
C01S C02I C017 C010 -170.0(5) . . . . ?
C01S C02I C025 C03M 5.1(8) . . . . ?
C01S C02X C03S C03M 0.1(11) . . . . ?
C01W C02H C03D C02M -1.0(8) . . . . ?
C02B O00K C01L N1 -1.3(6) . . . . ?
C02B O00K C01L C02K -179.3(4) . . . . ?
C02F C02L C02Q C02W 0.5(9) . . . . ?
C02F C02T C02Z C02W -0.8(9) . . . . ?
C02H C01W C014 Pt1 -176.5(4) . . . . ?
C02H C01W C014 C010 1.3(7) . . . . ?
C02I C01S C02X C03S 4.5(9) . . . . ?
C02K C02V C03L C03N -0.8(11) . . . . ?
C02K C03G C03R C03N -0.3(12) . . . . ?
C02L C02F C02T C02Z 0.7(8) . . . . ?
C02L C02F C021 O00M 172.5(4) . . . . ?
C02L C02F C021 N6 -6.7(8) . . . . ?
C02L C02Q C02W C02Z -0.7(9) . . . . ?
C02M C010 C014 Pt1 174.0(4) . . . . ?
C02M C010 C014 C01W -4.1(7) . . . . ?
C02M C010 C017 N3 -163.9(5) . . . . ?
C02M C010 C017 C02I 16.1(8) . . . . ?
C02P C01H C01J C01E -176.6(5) . . . . ?
C02P C01H C01J C02N 0.4(8) . . . . ?
C02Q C02W C02Z C02T 0.8(9) . . . . ?
C02T C02F C02L C02Q -0.6(8) . . . . ?
C02T C02F C021 O00M -5.5(7) . . . . ?
C02T C02F C021 N6 175.3(5) . . . . ?
C02V C02K C03G C03R -1.5(10) . . . . ?
C02V C03L C03N C03R -1.1(12) . . . . ?
C02X C01S C02I C017 178.1(5) . . . . ?
C02X C01S C02I C025 -6.9(7) . . . . ?
C02Y C01R C01S C02I -175.6(5) . . . . ?
C02Y C01R C01S C02X 0.5(8) . . . . ?
C03D C02M C010 C014 4.5(8) . . . . ?
C03D C02M C010 C017 178.6(5) . . . . ?
C03G C02K C02V C03L 2.1(10) . . . . ?
C03L C03N C03R C03G 1.6(13) . . . . ?
C03S C03M C025 C02I -0.6(10) . . . . ?
C010 C02M C03D C02H -1.9(8) . . . . ?
C012 C01G C033 C031 2.3(8) . . . . ?
C014 C01W C02H C03D 1.3(8) . . . . ?
C014 C010 C017 N3 10.5(6) . . . . ?
C014 C010 C017 C02I -169.6(5) . . . . ?
C016 C01P C031 C033 -1.1(8) . . . . ?
C016 C012 C018 N7 -4.4(6) . . . . ?
C016 C012 C018 C01B 179.2(4) . . . . ?
C017 N3 C01C C01R -1.6(7) . . . . ?
C017 C02I C025 C03M 179.8(6) . . . . ?
C017 C010 C014 Pt1 -0.7(5) . . . . ?
C017 C010 C014 C01W -178.8(4) . . . . ?
C018 N7 C01E C01J 2.8(7) . . . . ?
C018 C01B C01H C01J 6.8(7) . . . . ?
C018 C01B C01H C02P -174.4(5) . . . . ?
C018 C01B C01K C02R 176.1(5) . . . . ?
C018 C012 C016 Pt2 2.1(5) . . . . ?
C018 C012 C016 C01P 178.7(4) . . . . ?
C021 O00M C01O S1 -179.8(3) . . . . ?
C021 O00M C01O N5 -0.3(5) . . . . ?
C021 C02F C02L C02Q -178.6(5) . . . . ?
C021 C02F C02T C02Z 178.6(5) . . . . ?
C025 C02I C017 N3 -164.7(5) . . . . ?
C025 C02I C017 C010 15.4(8) . . . . ?
C025 C03M C03S C02X -2.1(11) . . . . ?
C031 C01P C016 Pt2 175.5(4) . . . . ?
C031 C01P C016 C012 -0.7(7) . . . . ?
C033 C01G C012 C016 -4.0(7) . . . . ?
C033 C01G C012 C018 -179.0(5) . . . . ?
Pt3 S3 C02G O00N 176.6(3) . . . . ?
Pt3 S3 C02G N12 -4.3(5) . . . . ?
Pt3 N9 C01F C01N -165.5(3) . . . . ?
Pt3 N9 C01F C013 14.6(5) . . . . ?
Pt3 N9 C020 C022 175.5(4) . . . . ?
Pt3 N10 N11 C02E 174.3(3) . . . . ?
Pt3 N10 C026 S4 7.3(8) . . . . ?
Pt3 N10 C026 O00O -173.2(3) . . . . ?
Pt4 S4 C026 O00O -173.5(3) . . . . ?
Pt4 S4 C026 N10 5.9(5) . . . . ?
Pt4 N8 C01A C01U 175.6(4) . . . . ?
Pt4 N8 C01T C01D -4.3(5) . . . . ?
Pt4 N8 C01T C02S 175.9(3) . . . . ?
Pt4 N12 N13 C01I 168.3(3) . . . . ?
Pt4 N12 C02G S3 14.5(7) . . . . ?
Pt4 N12 C02G O00N -166.4(3) . . . . ?
Pt4 C019 C023 C03A -175.4(4) . . . . ?
O00N C01I C024 C02U 166.7(5) . . . . ?
O00N C01I C024 C03E -14.3(8) . . . . ?
N8 C01A C01U C02C 4.6(8) . . . . ?
N8 C01A C01U C035 -179.8(5) . . . . ?
N8 C01T C02S C02C 12.3(7) . . . . ?
N8 C01T C02S C03F -164.7(5) . . . . ?
N9 C01F C01N C01M 164.0(5) . . . . ?
N9 C01F C01N C01Z -12.6(7) . . . . ?
N9 C01F C013 C01Q 165.2(4) . . . . ?
N9 C01F C013 C015 -9.1(6) . . . . ?
N9 C020 C022 C01Z -7.8(8) . . . . ?
N9 C020 C022 C030 176.8(5) . . . . ?
N10 N11 C02E O00O 0.8(6) . . . . ?
N10 N11 C02E C02D -178.3(5) . . . . ?
N11 N10 C026 S4 -178.4(4) . . . . ?
N11 N10 C026 O00O 1.0(5) . . . . ?
N12 N13 C01I O00N -1.0(6) . . . . ?
N12 N13 C01I C024 179.4(5) . . . . ?
N13 N12 C02G S3 -179.2(4) . . . . ?
N13 N12 C02G O00N 0.0(5) . . . . ?
N13 C01I C024 C02U -13.6(9) . . . . ?
N13 C01I C024 C03E 165.3(6) . . . . ?
C01A N8 C01T C01D 173.4(4) . . . . ?
C01A N8 C01T C02S -6.4(7) . . . . ?
C01A C01U C02C C02S 1.5(8) . . . . ?
C01A C01U C02C C03H 177.6(5) . . . . ?
C01D C01T C02S C02C -167.5(5) . . . . ?
C01D C01T C02S C03F 15.5(8) . . . . ?
C01D C02J C03O C03A -1.6(9) . . . . ?
C01D C019 C023 C03A 0.6(8) . . . . ?
C01F N9 C020 C022 2.6(7) . . . . ?
C01F C01N C01Z C022 7.4(7) . . . . ?
C01F C01N C01Z C036 -176.2(5) . . . . ?
C01F C013 C015 Pt3 -0.6(5) . . . . ?
C01F C013 C015 C01X 176.9(4) . . . . ?
C01I O00N C02G S3 178.8(3) . . . . ?
C01I O00N C02G N12 -0.6(5) . . . . ?
C01M C01N C01Z C022 -169.4(5) . . . . ?
C01M C01N C01Z C036 7.0(7) . . . . ?
C01M C03B C03K C036 3.2(10) . . . . ?
C01N C01F C013 C01Q -14.6(8) . . . . ?
C01N C01F C013 C015 171.0(4) . . . . ?
C01N C01M C03B C03K 0.4(9) . . . . ?
C01N C01Z C022 C020 2.5(7) . . . . ?
C01N C01Z C022 C030 177.7(5) . . . . ?
C01N C01Z C036 C03K -3.6(8) . . . . ?
C01Q C02A C02O C01X -0.4(8) . . . . ?
C01Q C013 C015 Pt3 -175.2(4) . . . . ?
C01Q C013 C015 C01X 2.3(7) . . . . ?
C01T N8 C01A C01U -2.1(7) . . . . ?
C01T C01D C02J C03O -179.7(5) . . . . ?
C01T C01D C019 Pt4 -3.7(6) . . . . ?
C01T C01D C019 C023 179.8(5) . . . . ?
C01T C02S C03F C03I -174.2(6) . . . . ?
C01U C02C C02S C01T -9.7(8) . . . . ?
C01U C02C C02S C03F 167.5(5) . . . . ?
C01U C02C C03H C03Q -172.9(6) . . . . ?
C01Y C02D C02E O00O -172.8(5) . . . . ?
C01Y C02D C02E N11 6.2(8) . . . . ?
C01Y C02D C034 C039 0.9(8) . . . . ?
C01Y C032 C038 C039 -0.6(9) . . . . ?
C02A C01Q C013 C01F -178.3(5) . . . . ?
C02A C01Q C013 C015 -4.3(7) . . . . ?
C02C C02S C03F C03I 8.8(8) . . . . ?
C02C C03H C03Q C03I 2.8(11) . . . . ?
C02D C01Y C032 C038 -0.1(9) . . . . ?
C02D C034 C039 C038 -1.5(9) . . . . ?
C02E O00O C026 S4 179.0(3) . . . . ?
C02E O00O C026 N10 -0.5(5) . . . . ?
C02E C02D C034 C039 -177.9(5) . . . . ?
C02G O00N C01I N13 1.0(5) . . . . ?
C02G O00N C01I C024 -179.3(4) . . . . ?
C02G N12 N13 C01I 0.6(5) . . . . ?
C02J C01D C01T N8 -170.2(5) . . . . ?
C02J C01D C01T C02S 9.6(9) . . . . ?
C02J C01D C019 Pt4 172.0(4) . . . . ?
C02J C01D C019 C023 -4.5(7) . . . . ?
C02O C01X C015 Pt3 177.8(4) . . . . ?
C02O C01X C015 C013 0.7(7) . . . . ?
C02S C02C C03H C03Q 3.1(10) . . . . ?
C02S C03F C03I C03Q -3.3(10) . . . . ?
C02U C03C C03J C03P 1.8(12) . . . . ?
C03B C01M C01N C01F 177.9(5) . . . . ?
C03B C01M C01N C01Z -5.4(8) . . . . ?
C03B C03K C036 C01Z -1.6(10) . . . . ?
C03C C02U C024 C01I 179.8(6) . . . . ?
C03C C02U C024 C03E 0.8(10) . . . . ?
C03C C03J C03P C03E -1.6(11) . . . . ?
C03F C03I C03Q C03H -2.7(12) . . . . ?
C03H C02C C02S C01T 174.1(5) . . . . ?
C03H C02C C02S C03F -8.7(8) . . . . ?
C03O C03A C023 C019 3.0(9) . . . . ?
C03P C03E C024 C01I -179.6(6) . . . . ?
C03P C03E C024 C02U -0.6(10) . . . . ?
C013 C01F C01N C01M -16.1(8) . . . . ?
C013 C01F C01N C01Z 167.2(4) . . . . ?
C013 C01Q C02A C02O 3.3(8) . . . . ?
C015 C01X C02O C02A -1.7(8) . . . . ?
C019 C01D C01T N8 5.2(6) . . . . ?
C019 C01D C01T C02S -175.1(5) . . . . ?
C019 C01D C02J C03O 5.1(8) . . . . ?
C020 N9 C01F C01N 7.8(7) . . . . ?
C020 N9 C01F C013 -172.1(4) . . . . ?
C022 C01Z C036 C03K 172.7(5) . . . . ?
C023 C03A C03O C02J -2.5(9) . . . . ?
C024 C02U C03C C03J -1.4(11) . . . . ?
C024 C03E C03P C03J 1.0(11) . . . . ?
C026 O00O C02E N11 -0.3(5) . . . . ?
C026 O00O C02E C02D 178.9(4) . . . . ?
C026 N10 N11 C02E -1.1(5) . . . . ?
C032 C01Y C02D C02E 178.8(5) . . . . ?
C032 C01Y C02D C034 -0.1(8) . . . . ?
C032 C038 C039 C034 1.4(10) . . . . ?
C034 C02D C02E O00O 6.0(7) . . . . ?
C034 C02D C02E N11 -175.0(5) . . . . ?
C035 C01U C02C C02S -173.9(5) . . . . ?
C035 C01U C02C C03H 2.2(9) . . . . ?
C036 C01Z C022 C020 -173.9(5) . . . . ?
C036 C01Z C022 C030 1.3(8) . . . . ?

_olex2_submission_special_instructions 'No special instructions were received'
