# Supplementary Information (SI) for Inorganic Chemistry Frontiers.
# This journal is © the Partner Organisations 2024

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
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data_20201220al_0m
_database_code_depnum_ccdc_archive 'CCDC 2356757'
loop_
_audit_author_name
_audit_author_address
AgPt
;XPU
China
;
_audit_update_record             
;
2024-05-21 deposited with the CCDC.	2024-07-18 downloaded from the CCDC.
;
_audit_creation_date             2024-05-20
_audit_creation_method           
;
Olex2 1.5
(compiled 2024.02.16 svn.r378c4104 for OlexSys, GUI svn.r6928)
;
_shelx_SHELXL_version_number     2018/3
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         'C148 H142 Ag16 Cl2 P8 Pt S6, 2(C H2 Cl2)'
_chemical_formula_sum            'C150 H146 Ag16 Cl6 P8 Pt S6'
_chemical_formula_weight         4522.49
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0137 0.0067 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag 0.0782 3.3823 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.3281 0.5435 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.2543 0.3332 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -5.3886 5.5592 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.2925 0.4295 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_H-M_alt        'P -1'
_space_group_name_Hall           '-P 1'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'

_cell_length_a                   18.450(6)
_cell_length_b                   18.992(6)
_cell_length_c                   29.482(9)
_cell_angle_alpha                75.225(11)
_cell_angle_beta                 73.008(10)
_cell_angle_gamma                64.526(11)
_cell_volume                     8819(5)
_cell_formula_units_Z            2
_cell_measurement_reflns_used    9822
_cell_measurement_temperature    150.00
_cell_measurement_theta_max      55.219
_cell_measurement_theta_min      3.989
_shelx_estimated_absorpt_T_max   0.324
_shelx_estimated_absorpt_T_min   0.263
_exptl_absorpt_coefficient_mu    12.134
_exptl_absorpt_correction_T_max  0.7508
_exptl_absorpt_correction_T_min  0.1921
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
;
SADABS-2016/2 (Bruker,2016/2) was used for absorption correction.
wR2(int) was 0.1803 before and 0.1005 after correction.
The Ratio of minimum to maximum transmission is 0.2559.
The λ/2 correction factor is Not present.
;
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            ?
_exptl_crystal_density_diffrn    1.703
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       block
_exptl_crystal_F_000             4388
_exptl_crystal_size_max          0.15
_exptl_crystal_size_mid          0.13
_exptl_crystal_size_min          0.12
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0909
_diffrn_reflns_av_unetI/netI     0.0831
_diffrn_reflns_Laue_measured_fraction_full 0.996
_diffrn_reflns_Laue_measured_fraction_max 0.985
_diffrn_reflns_limit_h_max       22
_diffrn_reflns_limit_h_min       -22
_diffrn_reflns_limit_k_max       23
_diffrn_reflns_limit_k_min       -23
_diffrn_reflns_limit_l_max       36
_diffrn_reflns_limit_l_min       -35
_diffrn_reflns_number            127207
_diffrn_reflns_point_group_measured_fraction_full 0.996
_diffrn_reflns_point_group_measured_fraction_max 0.985
_diffrn_reflns_theta_full        53.594
_diffrn_reflns_theta_max         55.334
_diffrn_reflns_theta_min         2.267
_diffrn_ambient_temperature      150.00
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 0.996
_diffrn_measured_fraction_theta_max 0.985
_diffrn_measurement_device_type  'Bruker D8 VENTURE'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_type           GaK\a
_diffrn_radiation_wavelength     1.34139
_diffrn_source                   ?
_diffrn_source_current           2.86
_diffrn_source_power             0.19985679999999997
_diffrn_source_voltage           69.88
_diffrn_standards_number         0
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                23883
_reflns_number_total             33557
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 Structure factors included contributions from the .fab file.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       'SAINT V8.38A (Bruker, 2018)'
_computing_data_collection       ?
_computing_data_reduction        'SAINT V8.38A (Bruker, 2018)'
_computing_molecular_graphics    'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_structure_refinement  'olex2.refine 1.5 (Bourhis et al., 2015)'
_computing_structure_solution    'olex2.solve 1.5 (Bourhis et al., 2015)'
_refine_diff_density_max         3.499
_refine_diff_density_min         -3.135
_refine_diff_density_rms         0.267
_refine_ls_extinction_coef       0.00022(2)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     'SHELXL-2018/3 (Sheldrick 2018)'
_refine_ls_goodness_of_fit_ref   1.093
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1691
_refine_ls_number_reflns         33557
_refine_ls_number_restraints     3316
_refine_ls_R_factor_all          0.1073
_refine_ls_R_factor_gt           0.0847
_refine_ls_restrained_S_all      1.060
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.1690P)²+2.7847P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.2419
_refine_ls_wR_factor_ref         0.2624
_refine_special_details          ?
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H) groups, All C(H,H) groups
 At 1.5 times of:
  All C(H,H,H) groups
2. Restrained distances
 C7-C6 = C8-C7
 1.5 with sigma of 0.02
 C23-C22
 1.5 with sigma of 0.02
 H40b-H37
 2 with sigma of 0.02
 C6-C1 \\sim C2-C1 \\sim C3-C2 \\sim C96-C95 \\sim C4-C3 \\sim C5-C4 \\sim C6-C5
 with sigma of 0.02
 C89-C88 \\sim C88-C87 \\sim C92-C87 \\sim C92-C91 \\sim C91-C90 \\sim C90-C89
 with sigma of 0.02
3. Uiso/Uaniso restraints and constraints
C1 \\sim C2 \\sim C3 \\sim C4 \\sim C5 \\sim C6 \\sim C7 \\sim C8 \\sim C9
\\sim C10 \\sim C11 \\sim C12 \\sim C13 \\sim C14 \\sim C15 \\sim C16 \\sim C17
\\sim C18 \\sim C19 \\sim C20 \\sim C21 \\sim C22 \\sim C23 \\sim C24 \\sim C25
\\sim C26 \\sim C27 \\sim C28 \\sim C29 \\sim C30 \\sim C31 \\sim C32 \\sim C33
\\sim C34 \\sim C35 \\sim C36 \\sim C37 \\sim C38 \\sim C39 \\sim C40 \\sim C41
\\sim C42 \\sim C43 \\sim C44 \\sim C45 \\sim C46 \\sim C47 \\sim C48 \\sim C49
\\sim C50 \\sim C51 \\sim C52 \\sim C53 \\sim C54 \\sim C55 \\sim C56 \\sim C57
\\sim C58 \\sim C59 \\sim C60 \\sim C61 \\sim C62 \\sim C63 \\sim C64 \\sim C65
\\sim C66 \\sim C67 \\sim C68 \\sim C69 \\sim C70 \\sim C71 \\sim C72 \\sim C73
\\sim C74 \\sim C75 \\sim C76 \\sim C77 \\sim C78 \\sim C79 \\sim C80 \\sim C81
\\sim C82 \\sim C83 \\sim C84 \\sim C85 \\sim C86 \\sim C87 \\sim C88 \\sim C89
\\sim C90 \\sim C91 \\sim C92 \\sim C93 \\sim C94 \\sim C95 \\sim C96 \\sim C97
\\sim C98 \\sim C99 \\sim C100 \\sim C101 \\sim C102 \\sim C103 \\sim C104
\\sim C105 \\sim C106 \\sim C107 \\sim C108 \\sim C109 \\sim C110 \\sim C111
\\sim C112 \\sim C113 \\sim C114 \\sim C115 \\sim C116 \\sim C117 \\sim C118
\\sim C119 \\sim C120 \\sim C121 \\sim C122 \\sim C123 \\sim C124 \\sim C125
\\sim C126 \\sim C127 \\sim C128 \\sim C129 \\sim C130 \\sim C131 \\sim C132
\\sim C133 \\sim C134 \\sim C135 \\sim C136 \\sim C137 \\sim C138 \\sim C139
\\sim C140 \\sim C141 \\sim C142 \\sim C145 \\sim C146 \\sim C147 \\sim C148
\\sim C149 \\sim C150 \\sim C144 \\sim C143: within 3.8A with sigma of 0.015
and sigma for terminal atoms of 0.03 within 3.8A
4.a Secondary CH2 refined with riding coordinates:
 C7(H7a,H7b), C15(H15a,H15b), C23(H23a,H23b), C31(H31a,H31b), C39(H39a,H39b),
 C47(H47a,H47b), C61(H61a,H61b), C86(H86a,H86b), C111(H11a,H11b), C136(H13a,
 H13b), C144(H14a,H14b), C143(H14c,H14d)
4.b Aromatic/amide H refined with riding coordinates:
 C2(H2), C3(H3), C4(H4), C5(H5), C10(H10), C11(H11), C12(H12), C13(H13),
 C18(H18), C19(H19), C20(H20), C21(H21), C26(H26), C27(H27), C28(H28), C29(H29),
  C34(H34), C35(H35), C36(H36), C37(H37), C42(H42), C43(H43), C44(H44),
 C45(H45), C50(H50), C51(H51), C52(H52), C53(H53), C54(H54), C56(H56), C57(H57),
  C58(H58), C59(H59), C60(H60), C63(H63), C64(H64), C65(H65), C66(H66),
 C67(H67), C69(H69), C70(H70), C71(H71), C72(H72), C73(H73), C75(H75), C76(H76),
  C77(H77), C78(H78), C79(H79), C81(H81), C82(H82), C83(H83), C84(H84),
 C85(H85), C88(H88), C89(H89), C90(H90), C91(H91), C92(H92), C94(H94), C95(H95),
  C96(H96), C97(H97), C98(H98), C100(H100), C101(H101), C102(H102), C103(H103),
 C104(H104), C106(H106), C107(H107), C108(H108), C109(H109), C110(H110),
 C113(H113), C114(H114), C115(H115), C116(H116), C117(H117), C119(H119),
 C120(H120), C121(H121), C122(H122), C123(H123), C125(H125), C126(H126),
 C127(H127), C128(H128), C129(H129), C131(H131), C132(H132), C133(H133),
 C134(H134), C135(H135), C138(H138), C139(H139), C140(H140), C141(H141),
 C142(H142), C145(H145), C146(H146), C147(H147), C148(H148), C150(H150)
4.c Idealised Me refined as rotating group:
 C8(H8a,H8b,H8c), C16(H16a,H16b,H16c), C24(H24a,H24b,H24c), C32(H32a,H32b,
 H32c), C40(H40a,H40b,H40c), C48(H48a,H48b,H48c)
;
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     iterative
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Pt1 Pt 0.35243(3) 0.79688(2) 0.26999(2) 0.03693(14) Uani 1 1 d . . . . .
Ag1 Ag 0.49888(5) 0.81737(5) 0.24687(2) 0.0449(2) Uani 1 1 d . . . . .
Cl1 Cl 0.1966(2) 0.8288(2) 0.44355(9) 0.0682(8) Uani 1 1 d . . . . .
S1 S 0.5901(2) 0.8785(2) 0.24908(10) 0.0621(8) Uani 1 1 d . . . . .
P1 P 0.53869(18) 0.83215(18) 0.40581(9) 0.0478(7) Uani 1 1 d . . . . .
C1 C 0.6834(10) 0.8111(11) 0.2631(6) 0.101(3) Uani 1 1 d D U . . .
Ag2 Ag 0.50026(5) 0.89810(5) 0.33094(3) 0.0527(2) Uani 1 1 d . . . . .
Cl2 Cl 0.18957(19) 0.8979(2) 0.13638(9) 0.0623(8) Uani 1 1 d . . . . .
S2 S 0.37900(18) 1.02707(16) 0.31555(9) 0.0479(6) Uani 1 1 d . . . . .
P2 P 0.54426(19) 0.67371(18) 0.39327(10) 0.0494(7) Uani 1 1 d . . . . .
C2 C 0.7017(10) 0.7297(10) 0.2689(7) 0.109(4) Uani 1 1 d D U . . .
H2 H 0.663367 0.712141 0.264592 0.131 Uiso 1 1 calc R U . . .
Ag3 Ag 0.29041(5) 1.07683(5) 0.24747(3) 0.0513(2) Uani 1 1 d . . . . .
S3 S 0.5837(2) 0.5377(2) 0.22437(11) 0.0670(8) Uani 1 1 d . . . . .
P3 P 0.1598(2) 1.17376(17) 0.27990(10) 0.0501(7) Uani 1 1 d . . . . .
C3 C 0.7772(10) 0.6735(12) 0.2811(7) 0.114(4) Uani 1 1 d D U . . .
H3 H 0.790640 0.618872 0.282527 0.137 Uiso 1 1 calc R U . . .
Ag4 Ag 0.35503(5) 0.91360(4) 0.30631(2) 0.04210(19) Uani 1 1 d . . . . .
S4 S 0.36062(19) 0.56021(17) 0.21099(9) 0.0502(7) Uani 1 1 d . . . . .
P4 P 0.08453(17) 1.04863(17) 0.29863(9) 0.0455(6) Uani 1 1 d . . . . .
C4 C 0.8316(11) 0.6978(12) 0.2909(7) 0.116(4) Uani 1 1 d D U . . .
H4 H 0.876840 0.663219 0.305363 0.139 Uiso 1 1 calc R U . . .
Ag5 Ag 0.35741(5) 0.92903(5) 0.20718(2) 0.0431(2) Uani 1 1 d . . . . .
S5 S 0.3574(2) 0.52761(18) 0.36623(10) 0.0569(7) Uani 1 1 d . . . . .
P5 P 0.53741(19) 0.78378(18) 0.09822(9) 0.0487(7) Uani 1 1 d . . . . .
C5 C 0.8120(11) 0.7789(11) 0.2771(8) 0.124(4) Uani 1 1 d D U . . .
H5 H 0.856140 0.794134 0.274122 0.149 Uiso 1 1 calc R U . . .
Ag6 Ag 0.21169(5) 0.93248(5) 0.28124(2) 0.04167(19) Uani 1 1 d . . . . .
S6 S 0.38104(19) 1.04822(18) 0.16694(9) 0.0521(7) Uani 1 1 d . . . . .
P6 P 0.5301(2) 0.63327(18) 0.08374(9) 0.0511(7) Uani 1 1 d . . . . .
C6 C 0.7392(10) 0.8435(11) 0.2666(8) 0.121(4) Uani 1 1 d D U . . .
Ag7 Ag 0.27010(5) 0.81442(5) 0.36232(2) 0.04281(19) Uani 1 1 d . . . . .
P7 P 0.14150(18) 0.58987(18) 0.29624(9) 0.0484(7) Uani 1 1 d . . . . .
C7 C 0.7275(12) 0.9318(12) 0.2421(7) 0.132(5) Uani 1 1 d D U . . .
H7A H 0.779183 0.941058 0.232861 0.159 Uiso 1 1 calc R U . . .
H7B H 0.699981 0.950047 0.214646 0.159 Uiso 1 1 calc R U . . .
Ag8 Ag 0.44812(5) 0.74325(5) 0.33836(2) 0.0429(2) Uani 1 1 d . . . . .
P8 P 0.07509(18) 0.76502(18) 0.31052(10) 0.0471(6) Uani 1 1 d . . . . .
C8 C 0.6737(15) 0.9632(17) 0.2855(8) 0.170(7) Uani 1 1 d D U . . .
H8A H 0.666588 1.018246 0.282859 0.254 Uiso 1 1 calc R U . . .
H8B H 0.698183 0.931995 0.313245 0.254 Uiso 1 1 calc R U . . .
H8C H 0.620205 0.960628 0.289779 0.254 Uiso 1 1 calc R U . . .
Ag9 Ag 0.44457(5) 0.77855(5) 0.17702(2) 0.0435(2) Uani 1 1 d . . . . .
C9 C 0.3147(9) 1.0535(7) 0.3719(4) 0.058(2) Uani 1 1 d . U . . .
Ag10 Ag 0.49365(5) 0.66298(5) 0.25515(2) 0.0446(2) Uani 1 1 d . . . . .
C10 C 0.2496(9) 1.0333(7) 0.3924(4) 0.060(2) Uani 1 1 d . U . . .
H10 H 0.241270 0.999508 0.377296 0.072 Uiso 1 1 calc R U . . .
Ag11 Ag 0.35385(5) 0.66070(5) 0.33061(2) 0.04251(19) Uani 1 1 d . . . . .
C11 C 0.1934(10) 1.0585(8) 0.4341(4) 0.068(3) Uani 1 1 d . U . . .
H11 H 0.146491 1.045243 0.446840 0.082 Uiso 1 1 calc R U . . .
Ag12 Ag 0.20792(5) 0.77469(5) 0.29609(2) 0.04206(19) Uani 1 1 d . . . . .
C12 C 0.2119(10) 1.1061(8) 0.4565(4) 0.074(3) Uani 1 1 d . U . . .
H12 H 0.176388 1.124979 0.485197 0.089 Uiso 1 1 calc R U . . .
Ag13 Ag 0.34591(5) 0.68401(5) 0.23230(2) 0.0428(2) Uani 1 1 d . . . . .
C13 C 0.2794(10) 1.1245(8) 0.4372(4) 0.072(2) Uani 1 1 d . U . . .
H13 H 0.289518 1.155658 0.453390 0.087 Uiso 1 1 calc R U . . .
Ag14 Ag 0.48736(6) 0.59213(5) 0.16806(3) 0.0526(2) Uani 1 1 d . . . . .
C14 C 0.3357(9) 1.0995(8) 0.3941(4) 0.065(2) Uani 1 1 d . U . . .
Ag15 Ag 0.27522(5) 0.57432(5) 0.30281(3) 0.0519(2) Uani 1 1 d . . . . .
C15 C 0.4081(10) 1.1209(8) 0.3742(5) 0.073(3) Uani 1 1 d . U . . .
H15A H 0.399540 1.155103 0.343060 0.087 Uiso 1 1 calc R U . . .
H15B H 0.455550 1.071590 0.366678 0.087 Uiso 1 1 calc R U . . .
Ag16 Ag 0.26421(5) 0.84761(5) 0.19959(2) 0.0438(2) Uani 1 1 d . . . . .
C16 C 0.4355(14) 1.1612(13) 0.4002(7) 0.116(5) Uani 1 1 d . U . . .
H16A H 0.480572 1.175316 0.378826 0.174 Uiso 1 1 calc R U . . .
H16B H 0.454329 1.125291 0.428619 0.174 Uiso 1 1 calc R U . . .
H16C H 0.389385 1.209025 0.410176 0.174 Uiso 1 1 calc R U . . .
C17 C 0.6778(11) 0.5516(12) 0.1853(6) 0.099(3) Uani 1 1 d . U . . .
C18 C 0.6874(12) 0.6197(13) 0.1869(6) 0.107(4) Uani 1 1 d . U . . .
H18 H 0.648239 0.656443 0.207509 0.129 Uiso 1 1 calc R U . . .
C19 C 0.7585(12) 0.6323(13) 0.1564(6) 0.106(3) Uani 1 1 d . U . . .
H19 H 0.767778 0.676912 0.158173 0.127 Uiso 1 1 calc R U . . .
C20 C 0.8121(12) 0.5832(13) 0.1255(7) 0.111(4) Uani 1 1 d . U . . .
H20 H 0.854275 0.596523 0.102589 0.133 Uiso 1 1 calc R U . . .
C21 C 0.8057(12) 0.5180(13) 0.1272(6) 0.107(4) Uani 1 1 d . U . . .
H21 H 0.849004 0.480005 0.108843 0.129 Uiso 1 1 calc R U . . .
C22 C 0.7343(13) 0.4984(12) 0.1564(7) 0.114(4) Uani 1 1 d D U . . .
C23 C 0.7257(12) 0.4247(11) 0.1557(7) 0.111(4) Uani 1 1 d D U . . .
H23A H 0.680151 0.436669 0.140066 0.133 Uiso 1 1 calc R U . . .
H23B H 0.713404 0.398084 0.188929 0.133 Uiso 1 1 calc R U . . .
C24 C 0.8044(15) 0.3726(15) 0.1286(8) 0.153(7) Uani 1 1 d . U . . .
H24A H 0.813448 0.397339 0.095091 0.230 Uiso 1 1 calc R U . . .
H24B H 0.801953 0.321550 0.130155 0.230 Uiso 1 1 calc R U . . .
H24C H 0.849708 0.364781 0.142825 0.230 Uiso 1 1 calc R U . . .
C25 C 0.2914(9) 0.5941(8) 0.1714(4) 0.062(2) Uani 1 1 d . U . . .
C26 C 0.2298(8) 0.6697(8) 0.1699(4) 0.060(2) Uani 1 1 d . U . . .
H26 H 0.224908 0.703986 0.190136 0.072 Uiso 1 1 calc R U . . .
C27 C 0.1759(9) 0.6956(9) 0.1396(4) 0.066(2) Uani 1 1 d . U . . .
H27 H 0.135139 0.747666 0.138410 0.079 Uiso 1 1 calc R U . . .
C28 C 0.1816(10) 0.6455(9) 0.1109(5) 0.073(2) Uani 1 1 d . U . . .
H28 H 0.142220 0.661330 0.091702 0.088 Uiso 1 1 calc R U . . .
C29 C 0.2443(9) 0.5727(8) 0.1103(4) 0.068(2) Uani 1 1 d . U . . .
H29 H 0.250941 0.540754 0.088157 0.082 Uiso 1 1 calc R U . . .
C30 C 0.2979(9) 0.5444(8) 0.1406(4) 0.062(2) Uani 1 1 d . U . . .
C31 C 0.3680(10) 0.4633(8) 0.1388(4) 0.072(3) Uani 1 1 d . U . . .
H31A H 0.419227 0.469395 0.137522 0.086 Uiso 1 1 calc R U . . .
H31B H 0.357186 0.428889 0.169222 0.086 Uiso 1 1 calc R U . . .
C32 C 0.3832(11) 0.4207(9) 0.0978(5) 0.085(4) Uani 1 1 d . U . . .
H32A H 0.386520 0.456439 0.067366 0.128 Uiso 1 1 calc R U . . .
H32B H 0.338058 0.403832 0.102209 0.128 Uiso 1 1 calc R U . . .
H32C H 0.434984 0.374487 0.097225 0.128 Uiso 1 1 calc R U . . .
C33 C 0.2875(8) 0.5406(8) 0.4247(4) 0.064(2) Uani 1 1 d . U . . .
C34 C 0.2524(9) 0.6116(9) 0.4416(4) 0.071(2) Uani 1 1 d . U . . .
H34 H 0.263829 0.654623 0.420914 0.085 Uiso 1 1 calc R U . . .
C35 C 0.2015(10) 0.6260(9) 0.4863(5) 0.075(3) Uani 1 1 d . U . . .
H35 H 0.178903 0.675844 0.496829 0.090 Uiso 1 1 calc R U . . .
C36 C 0.1867(10) 0.5608(9) 0.5140(5) 0.080(3) Uani 1 1 d . U . . .
H36 H 0.150819 0.566515 0.544621 0.095 Uiso 1 1 calc R U . . .
C37 C 0.2227(9) 0.4865(9) 0.4989(4) 0.070(2) Uani 1 1 d . U . . .
H37 H 0.212493 0.442837 0.519450 0.083 Uiso 1 1 calc DR U . . .
C38 C 0.2720(9) 0.4775(9) 0.4546(5) 0.071(2) Uani 1 1 d . U . . .
C39 C 0.3109(10) 0.3967(9) 0.4373(5) 0.077(3) Uani 1 1 d . U . . .
H39A H 0.298120 0.403266 0.405696 0.092 Uiso 1 1 calc R U . . .
H39B H 0.371308 0.376867 0.432840 0.092 Uiso 1 1 calc R U . . .
C40 C 0.2804(12) 0.3357(10) 0.4722(6) 0.099(5) Uani 1 1 d . U . . .
H40A H 0.222651 0.350036 0.472132 0.149 Uiso 1 1 calc R U . . .
H40B H 0.285743 0.334268 0.504529 0.149 Uiso 1 1 calc DR U . . .
H40C H 0.313262 0.283560 0.462246 0.149 Uiso 1 1 calc R U . . .
C41 C 0.3155(9) 1.1035(8) 0.1261(4) 0.063(2) Uani 1 1 d . U . . .
C42 C 0.2646(9) 1.0727(8) 0.1172(4) 0.068(2) Uani 1 1 d . U . . .
H42 H 0.265669 1.021865 0.132513 0.081 Uiso 1 1 calc R U . . .
C43 C 0.2122(10) 1.1185(9) 0.0852(5) 0.081(3) Uani 1 1 d . U . . .
H43 H 0.176233 1.098805 0.080230 0.097 Uiso 1 1 calc R U . . .
C44 C 0.2112(10) 1.1880(9) 0.0619(5) 0.080(3) Uani 1 1 d . U . . .
H44 H 0.176021 1.216579 0.039877 0.096 Uiso 1 1 calc R U . . .
C45 C 0.2588(10) 1.2180(10) 0.0690(5) 0.086(3) Uani 1 1 d . U . . .
H45 H 0.256657 1.268119 0.051496 0.103 Uiso 1 1 calc R U . . .
C46 C 0.3145(10) 1.1786(9) 0.1023(5) 0.073(3) Uani 1 1 d . U . . .
C47 C 0.3683(10) 1.2119(8) 0.1084(5) 0.074(3) Uani 1 1 d . U . . .
H47A H 0.380020 1.247283 0.078700 0.089 Uiso 1 1 calc R U . . .
H47B H 0.421074 1.168721 0.113679 0.089 Uiso 1 1 calc R U . . .
C48 C 0.3291(11) 1.2594(10) 0.1518(5) 0.090(4) Uani 1 1 d . U . . .
H48A H 0.274655 1.299065 0.148191 0.134 Uiso 1 1 calc R U . . .
H48B H 0.364262 1.285592 0.152622 0.134 Uiso 1 1 calc R U . . .
H48C H 0.324053 1.223138 0.181813 0.134 Uiso 1 1 calc R U . . .
C49 C 0.6044(8) 0.8694(8) 0.4194(4) 0.060(2) Uani 1 1 d . U . . .
C50 C 0.6853(10) 0.8416(10) 0.4050(6) 0.090(3) Uani 1 1 d . U . . .
H50 H 0.712310 0.796226 0.389300 0.108 Uiso 1 1 calc R U . . .
C51 C 0.7335(10) 0.8798(10) 0.4128(6) 0.092(3) Uani 1 1 d . U . . .
H51 H 0.791066 0.861343 0.400402 0.110 Uiso 1 1 calc R U . . .
C52 C 0.6960(10) 0.9419(10) 0.4379(6) 0.082(3) Uani 1 1 d . U . . .
H52 H 0.726979 0.965557 0.444757 0.099 Uiso 1 1 calc R U . . .
C53 C 0.6167(11) 0.9677(11) 0.4521(6) 0.094(3) Uani 1 1 d . U . . .
H53 H 0.589585 1.011333 0.469260 0.113 Uiso 1 1 calc R U . . .
C54 C 0.5708(10) 0.9338(10) 0.4429(6) 0.084(3) Uani 1 1 d . U . . .
H54 H 0.512816 0.956186 0.453369 0.100 Uiso 1 1 calc R U . . .
C55 C 0.4633(8) 0.8302(8) 0.4609(4) 0.061(2) Uani 1 1 d . U . . .
C56 C 0.3807(9) 0.8699(8) 0.4595(4) 0.065(2) Uani 1 1 d . U . . .
H56 H 0.365306 0.896698 0.429752 0.078 Uiso 1 1 calc R U . . .
C57 C 0.3200(9) 0.8712(8) 0.5010(4) 0.069(3) Uani 1 1 d . U . . .
H57 H 0.263541 0.897677 0.499638 0.083 Uiso 1 1 calc R U . . .
C58 C 0.3429(9) 0.8337(8) 0.5438(5) 0.070(3) Uani 1 1 d . U . . .
H58 H 0.302054 0.832797 0.572176 0.084 Uiso 1 1 calc R U . . .
C59 C 0.4258(9) 0.7968(8) 0.5461(5) 0.071(3) Uani 1 1 d . U . . .
H59 H 0.441348 0.773111 0.576126 0.085 Uiso 1 1 calc R U . . .
C60 C 0.4853(9) 0.7950(8) 0.5043(4) 0.066(2) Uani 1 1 d . U . . .
H60 H 0.541745 0.769199 0.505751 0.080 Uiso 1 1 calc R U . . .
C61 C 0.6015(8) 0.7281(7) 0.4030(4) 0.060(2) Uani 1 1 d . U . . .
H61A H 0.621170 0.703303 0.433282 0.072 Uiso 1 1 calc R U . . .
H61B H 0.650113 0.723261 0.376493 0.072 Uiso 1 1 calc R U . . .
C62 C 0.4976(8) 0.6402(7) 0.4541(4) 0.0571(19) Uani 1 1 d . U . . .
C63 C 0.4132(8) 0.6667(8) 0.4659(4) 0.064(2) Uani 1 1 d . U . . .
H63 H 0.382405 0.697979 0.441976 0.077 Uiso 1 1 calc R U . . .
C64 C 0.3723(9) 0.6483(8) 0.5123(4) 0.069(2) Uani 1 1 d . U . . .
H64 H 0.313996 0.669305 0.521022 0.082 Uiso 1 1 calc R U . . .
C65 C 0.4200(9) 0.5980(8) 0.5455(4) 0.070(3) Uani 1 1 d . U . . .
H65 H 0.394352 0.583660 0.577452 0.084 Uiso 1 1 calc R U . . .
C66 C 0.5069(9) 0.5682(8) 0.5314(4) 0.068(3) Uani 1 1 d . U . . .
H66 H 0.539049 0.532407 0.553749 0.082 Uiso 1 1 calc R U . . .
C67 C 0.5447(8) 0.5899(8) 0.4868(4) 0.063(2) Uani 1 1 d . U . . .
H67 H 0.602866 0.570801 0.477958 0.075 Uiso 1 1 calc R U . . .
C68 C 0.6262(9) 0.5846(8) 0.3726(4) 0.065(2) Uani 1 1 d . U . . .
C69 C 0.6159(10) 0.5449(8) 0.3421(5) 0.075(3) Uani 1 1 d . U . . .
H69 H 0.563710 0.562832 0.334337 0.090 Uiso 1 1 calc R U . . .
C70 C 0.6763(11) 0.4838(10) 0.3240(5) 0.087(3) Uani 1 1 d . U . . .
H70 H 0.665692 0.461807 0.302262 0.104 Uiso 1 1 calc R U . . .
C71 C 0.7507(11) 0.4506(10) 0.3335(5) 0.088(3) Uani 1 1 d . U . . .
H71 H 0.791582 0.404789 0.320836 0.105 Uiso 1 1 calc R U . . .
C72 C 0.7650(11) 0.4873(10) 0.3635(6) 0.089(3) Uani 1 1 d . U . . .
H72 H 0.817221 0.466467 0.371634 0.107 Uiso 1 1 calc R U . . .
C73 C 0.7030(10) 0.5549(10) 0.3816(5) 0.083(3) Uani 1 1 d . U . . .
H73 H 0.714929 0.580380 0.400705 0.099 Uiso 1 1 calc R U . . .
C74 C 0.1034(8) 1.2505(7) 0.2378(4) 0.0583(19) Uani 1 1 d . U . . .
C75 C 0.0284(9) 1.3155(8) 0.2564(5) 0.070(2) Uani 1 1 d . U . . .
H75 H 0.011756 1.318482 0.289752 0.085 Uiso 1 1 calc R U . . .
C76 C -0.0175(10) 1.3719(9) 0.2248(5) 0.076(3) Uani 1 1 d . U . . .
H76 H -0.059829 1.419106 0.235004 0.091 Uiso 1 1 calc R U . . .
C77 C -0.0014(10) 1.3592(8) 0.1780(5) 0.074(3) Uani 1 1 d . U . . .
H77 H -0.037611 1.393829 0.157402 0.089 Uiso 1 1 calc R U . . .
C78 C 0.0644(9) 1.2987(9) 0.1617(5) 0.074(3) Uani 1 1 d . U . . .
H78 H 0.077660 1.294520 0.128600 0.089 Uiso 1 1 calc R U . . .
C79 C 0.1147(9) 1.2413(8) 0.1913(4) 0.065(2) Uani 1 1 d . U . . .
H79 H 0.156930 1.195455 0.179334 0.078 Uiso 1 1 calc R U . . .
C80 C 0.1708(10) 1.2299(8) 0.3177(5) 0.068(2) Uani 1 1 d . U . . .
C81 C 0.1131(11) 1.2606(8) 0.3548(5) 0.075(3) Uani 1 1 d . U . . .
H81 H 0.063700 1.251605 0.363016 0.090 Uiso 1 1 calc R U . . .
C82 C 0.1226(12) 1.3076(9) 0.3833(5) 0.087(3) Uani 1 1 d . U . . .
H82 H 0.081961 1.328310 0.410115 0.105 Uiso 1 1 calc R U . . .
C83 C 0.1950(12) 1.3194(9) 0.3682(5) 0.085(3) Uani 1 1 d . U . . .
H83 H 0.203601 1.350298 0.385296 0.102 Uiso 1 1 calc R U . . .
C84 C 0.2577(12) 1.2881(9) 0.3287(5) 0.087(3) Uani 1 1 d . U . . .
H84 H 0.307355 1.296858 0.319751 0.104 Uiso 1 1 calc R U . . .
C85 C 0.2431(10) 1.2441(8) 0.3036(5) 0.075(2) Uani 1 1 d . U . . .
H85 H 0.282998 1.223381 0.276519 0.090 Uiso 1 1 calc R U . . .
C86 C 0.0894(8) 1.1319(7) 0.3208(4) 0.056(2) Uani 1 1 d . U . . .
H86A H 0.033831 1.174090 0.325997 0.067 Uiso 1 1 calc R U . . .
H86B H 0.106215 1.111650 0.352145 0.067 Uiso 1 1 calc R U . . .
C87 C 0.0370(7) 1.0979(7) 0.2483(4) 0.060(2) Uani 1 1 d D U . . .
C88 C -0.0360(8) 1.1660(7) 0.2511(4) 0.067(2) Uani 1 1 d D U . . .
H88 H -0.059895 1.187400 0.280270 0.080 Uiso 1 1 calc R U . . .
C89 C -0.0739(9) 1.2024(8) 0.2123(4) 0.075(3) Uani 1 1 d D U . . .
H89 H -0.119253 1.251616 0.211796 0.091 Uiso 1 1 calc R U . . .
C90 C -0.0379(6) 1.1587(7) 0.1739(4) 0.055(2) Uani 1 1 d D U . . .
H90 H -0.068419 1.175194 0.149463 0.066 Uiso 1 1 calc R U . . .
C91 C 0.0327(8) 1.0977(8) 0.1673(5) 0.073(2) Uani 1 1 d D U . . .
H91 H 0.057448 1.078362 0.137439 0.088 Uiso 1 1 calc R U . . .
C92 C 0.0675(8) 1.0646(8) 0.2066(3) 0.061(2) Uani 1 1 d D U . . .
H92 H 0.114578 1.016717 0.205244 0.073 Uiso 1 1 calc R U . . .
C93 C 0.0077(8) 1.0245(8) 0.3496(4) 0.062(2) Uani 1 1 d . U . . .
C94 C 0.0368(10) 0.9798(8) 0.3887(5) 0.074(3) Uani 1 1 d . U . . .
H94 H 0.093459 0.962279 0.388538 0.089 Uiso 1 1 calc R U . . .
C95 C -0.0149(8) 0.9592(9) 0.4290(5) 0.079(3) Uani 1 1 d D U . . .
H95 H 0.006054 0.927307 0.456461 0.095 Uiso 1 1 calc R U . . .
C96 C -0.0976(8) 0.9852(8) 0.4292(5) 0.075(3) Uani 1 1 d D U . . .
H96 H -0.134504 0.974004 0.457400 0.089 Uiso 1 1 calc R U . . .
C97 C -0.1250(9) 1.0269(8) 0.3888(5) 0.070(3) Uani 1 1 d . U . . .
H97 H -0.180341 1.040006 0.387614 0.084 Uiso 1 1 calc R U . . .
C98 C -0.0743(9) 1.0506(8) 0.3495(5) 0.065(2) Uani 1 1 d . U . . .
H98 H -0.095509 1.084628 0.322617 0.078 Uiso 1 1 calc R U . . .
C99 C 0.4853(8) 0.8563(7) 0.0521(4) 0.0565(19) Uani 1 1 d . U . . .
C100 C 0.4019(8) 0.8893(7) 0.0619(4) 0.060(2) Uani 1 1 d . U . . .
H100 H 0.371369 0.875251 0.092227 0.072 Uiso 1 1 calc R U . . .
C101 C 0.3624(9) 0.9438(8) 0.0270(4) 0.069(2) Uani 1 1 d . U . . .
H101 H 0.304091 0.966790 0.033455 0.083 Uiso 1 1 calc R U . . .
C102 C 0.4053(9) 0.9655(8) -0.0167(4) 0.069(3) Uani 1 1 d . U . . .
H102 H 0.377239 1.001579 -0.040801 0.082 Uiso 1 1 calc R U . . .
C103 C 0.4877(9) 0.9349(8) -0.0251(4) 0.065(3) Uani 1 1 d . U . . .
H103 H 0.517299 0.952474 -0.054707 0.078 Uiso 1 1 calc R U . . .
C104 C 0.5303(8) 0.8795(8) 0.0074(4) 0.058(2) Uani 1 1 d . U . . .
H104 H 0.588584 0.857082 0.000288 0.070 Uiso 1 1 calc R U . . .
C105 C 0.6189(9) 0.8135(8) 0.0965(4) 0.065(2) Uani 1 1 d . U . . .
C106 C 0.6021(9) 0.8715(8) 0.1234(4) 0.064(2) Uani 1 1 d . U . . .
H106 H 0.548107 0.894481 0.141546 0.077 Uiso 1 1 calc R U . . .
C107 C 0.6621(9) 0.8968(9) 0.1244(5) 0.071(3) Uani 1 1 d . U . . .
H107 H 0.649289 0.934933 0.144044 0.085 Uiso 1 1 calc R U . . .
C108 C 0.7410(9) 0.8662(9) 0.0966(5) 0.069(2) Uani 1 1 d . U . . .
H108 H 0.782485 0.882984 0.096919 0.083 Uiso 1 1 calc R U . . .
C109 C 0.7572(10) 0.8106(10) 0.0684(5) 0.083(3) Uani 1 1 d . U . . .
H109 H 0.810187 0.790730 0.048477 0.099 Uiso 1 1 calc R U . . .
C110 C 0.6998(9) 0.7836(9) 0.0682(5) 0.074(2) Uani 1 1 d . U . . .
H110 H 0.713919 0.744476 0.049030 0.089 Uiso 1 1 calc R U . . .
C111 C 0.5946(8) 0.6910(7) 0.0732(4) 0.059(2) Uani 1 1 d . U . . .
H11A H 0.642809 0.658903 0.088030 0.071 Uiso 1 1 calc R U . . .
H11B H 0.614839 0.702808 0.038257 0.071 Uiso 1 1 calc R U . . .
C112 C 0.4540(8) 0.6912(8) 0.0470(4) 0.058(2) Uani 1 1 d . U . . .
C113 C 0.3726(8) 0.7145(8) 0.0678(4) 0.059(2) Uani 1 1 d . U . . .
H113 H 0.355967 0.696525 0.100739 0.071 Uiso 1 1 calc R U . . .
C114 C 0.3137(9) 0.7645(8) 0.0409(4) 0.067(2) Uani 1 1 d . U . . .
H114 H 0.257231 0.783358 0.056112 0.081 Uiso 1 1 calc R U . . .
C115 C 0.3370(9) 0.7864(8) -0.0072(4) 0.065(2) Uani 1 1 d . U . . .
H115 H 0.297088 0.818919 -0.025950 0.078 Uiso 1 1 calc R U . . .
C116 C 0.4225(9) 0.7594(8) -0.0287(4) 0.067(3) Uani 1 1 d . U . . .
H116 H 0.440795 0.773306 -0.062089 0.081 Uiso 1 1 calc R U . . .
C117 C 0.4752(9) 0.7150(8) -0.0012(4) 0.061(2) Uani 1 1 d . U . . .
H117 H 0.531972 0.698248 -0.015714 0.073 Uiso 1 1 calc R U . . .
C118 C 0.5937(9) 0.5464(8) 0.0532(4) 0.065(2) Uani 1 1 d . U . . .
C119 C 0.5555(10) 0.5018(8) 0.0482(5) 0.068(2) Uani 1 1 d . U . . .
H119 H 0.497796 0.517723 0.059463 0.082 Uiso 1 1 calc R U . . .
C120 C 0.5990(10) 0.4340(9) 0.0271(5) 0.074(3) Uani 1 1 d . U . . .
H120 H 0.571382 0.405641 0.021655 0.089 Uiso 1 1 calc R U . . .
C121 C 0.6824(10) 0.4088(9) 0.0143(5) 0.073(3) Uani 1 1 d . U . . .
H121 H 0.713826 0.360332 0.001963 0.088 Uiso 1 1 calc R U . . .
C122 C 0.7213(10) 0.4540(9) 0.0192(5) 0.079(3) Uani 1 1 d . U . . .
H122 H 0.779388 0.436151 0.010271 0.095 Uiso 1 1 calc R U . . .
C123 C 0.6774(9) 0.5231(9) 0.0367(5) 0.071(2) Uani 1 1 d . U . . .
H123 H 0.704237 0.555498 0.037586 0.085 Uiso 1 1 calc R U . . .
C124 C 0.1424(8) 0.5362(8) 0.2511(4) 0.059(2) Uani 1 1 d . U . . .
C125 C 0.1975(9) 0.4618(8) 0.2495(4) 0.067(2) Uani 1 1 d . U . . .
H125 H 0.236422 0.441261 0.269446 0.081 Uiso 1 1 calc R U . . .
C126 C 0.2004(10) 0.4134(9) 0.2203(5) 0.074(3) Uani 1 1 d . U . . .
H126 H 0.241358 0.361601 0.218800 0.088 Uiso 1 1 calc R U . . .
C127 C 0.1410(10) 0.4445(8) 0.1939(5) 0.071(3) Uani 1 1 d . U . . .
H127 H 0.140534 0.411863 0.174457 0.086 Uiso 1 1 calc R U . . .
C128 C 0.0838(10) 0.5173(9) 0.1934(5) 0.072(2) Uani 1 1 d . U . . .
H128 H 0.044973 0.536912 0.173479 0.086 Uiso 1 1 calc R U . . .
C129 C 0.0833(9) 0.5662(8) 0.2252(4) 0.065(2) Uani 1 1 d . U . . .
H129 H 0.042330 0.617769 0.227432 0.078 Uiso 1 1 calc R U . . .
C130 C 0.0831(8) 0.5512(8) 0.3510(4) 0.0575(19) Uani 1 1 d . U . . .
C131 C 0.0162(8) 0.5395(8) 0.3501(4) 0.060(2) Uani 1 1 d . U . . .
H131 H -0.001382 0.552395 0.320682 0.072 Uiso 1 1 calc R U . . .
C132 C -0.0276(9) 0.5087(8) 0.3916(4) 0.069(3) Uani 1 1 d . U . . .
H132 H -0.075824 0.502894 0.390752 0.083 Uiso 1 1 calc R U . . .
C133 C 0.0000(9) 0.4869(9) 0.4334(4) 0.071(3) Uani 1 1 d . U . . .
H133 H -0.026174 0.461533 0.461155 0.086 Uiso 1 1 calc R U . . .
C134 C 0.0672(9) 0.5023(8) 0.4352(4) 0.070(2) Uani 1 1 d . U . . .
H134 H 0.085185 0.490362 0.464318 0.084 Uiso 1 1 calc R U . . .
C135 C 0.1064(8) 0.5353(8) 0.3933(4) 0.060(2) Uani 1 1 d . U . . .
H135 H 0.150980 0.547213 0.394145 0.071 Uiso 1 1 calc R U . . .
C136 C 0.0751(8) 0.6904(7) 0.2793(4) 0.057(2) Uani 1 1 d . U . . .
H13A H 0.018241 0.692999 0.285905 0.068 Uiso 1 1 calc R U . . .
H13B H 0.091692 0.705201 0.244263 0.068 Uiso 1 1 calc R U . . .
C137 C 0.0225(8) 0.7482(7) 0.3716(4) 0.0548(19) Uani 1 1 d . U . . .
C138 C -0.0454(9) 0.7287(8) 0.3841(4) 0.066(2) Uani 1 1 d . U . . .
H138 H -0.065839 0.725241 0.359051 0.080 Uiso 1 1 calc R U . . .
C139 C -0.0862(10) 0.7138(9) 0.4312(5) 0.080(3) Uani 1 1 d . U . . .
H139 H -0.132395 0.699863 0.438459 0.096 Uiso 1 1 calc R U . . .
C140 C -0.0562(10) 0.7204(9) 0.4662(5) 0.076(3) Uani 1 1 d . U . . .
H140 H -0.082402 0.710412 0.498644 0.091 Uiso 1 1 calc R U . . .
C141 C 0.0115(10) 0.7412(9) 0.4566(5) 0.078(3) Uani 1 1 d . U . . .
H141 H 0.030729 0.745111 0.482057 0.093 Uiso 1 1 calc R U . . .
C142 C 0.0504(9) 0.7563(8) 0.4087(4) 0.066(2) Uani 1 1 d . U . . .
H142 H 0.095512 0.771922 0.401456 0.080 Uiso 1 1 calc R U . . .
C145 C -0.0254(9) 0.9417(9) 0.2105(5) 0.074(3) Uani 1 1 d . U . . .
H145 H -0.010842 0.955594 0.176720 0.089 Uiso 1 1 calc R U . . .
C146 C -0.0999(8) 0.9898(8) 0.2366(5) 0.066(2) Uani 1 1 d . U . . .
H146 H -0.134655 1.037243 0.220763 0.079 Uiso 1 1 calc R U . . .
C147 C -0.1213(9) 0.9688(9) 0.2831(5) 0.073(3) Uani 1 1 d . U . . .
H147 H -0.172848 1.000623 0.300067 0.088 Uiso 1 1 calc R U . . .
C148 C -0.0709(8) 0.9012(8) 0.3086(5) 0.065(2) Uani 1 1 d . U . . .
H148 H -0.086726 0.888522 0.342316 0.078 Uiso 1 1 calc R U . . .
C149 C 0.0028(8) 0.8532(7) 0.2832(4) 0.058(2) Uani 1 1 d . U . . .
C150 C 0.0254(9) 0.8763(8) 0.2330(5) 0.066(2) Uani 1 1 d . U . . .
H150 H 0.076660 0.845291 0.215252 0.079 Uiso 1 1 calc R U . . .
Cl5 Cl 0.0217(3) 0.8279(4) 0.55489(15) 0.1127(15) Uani 1 1 d . . . . .
Cl6 Cl 0.1497(4) 0.7376(4) 0.60753(19) 0.153(2) Uani 1 1 d . . . . .
C144 C 0.1157(11) 0.8121(10) 0.5651(5) 0.089(5) Uani 1 1 d . . . . .
H14A H 0.157016 0.802566 0.534790 0.107 Uiso 1 1 calc R U . . .
H14B H 0.111434 0.860881 0.573919 0.107 Uiso 1 1 calc R U . . .
Cl3 Cl 0.5792(5) 1.1061(5) 0.1550(2) 0.159(2) Uani 1 1 d . . . . .
Cl4 Cl 0.4855(7) 1.1855(6) 0.2370(3) 0.214(4) Uani 1 1 d . . . . .
C143 C 0.5131(14) 1.1024(13) 0.2099(7) 0.118(7) Uani 1 1 d . . . . .
H14C H 0.539868 1.053982 0.231201 0.141 Uiso 1 1 calc R U . . .
H14D H 0.463064 1.099994 0.205589 0.141 Uiso 1 1 calc R U . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Pt1 Ag1 2.7585(11) . ?
Pt1 Ag4 2.7194(10) . ?
Pt1 Ag5 2.7321(11) . ?
Pt1 Ag6 2.7685(12) . ?
Pt1 Ag7 2.7274(11) . ?
Pt1 Ag8 2.7756(10) . ?
Pt1 Ag9 2.7890(11) . ?
Pt1 Ag10 2.7657(12) . ?
Pt1 Ag11 2.7378(11) . ?
Pt1 Ag12 2.7350(11) . ?
Pt1 Ag13 2.7128(10) . ?
Pt1 Ag16 2.7369(10) . ?
Ag1 S1 2.442(3) . ?
Ag1 Ag2 3.2409(13) . ?
Ag1 Ag4 2.8632(13) . ?
Ag1 Ag5 2.9047(13) . ?
Ag1 Ag8 2.8026(12) . ?
Ag1 Ag9 2.8992(11) . ?
Ag1 Ag10 2.9207(14) . ?
Cl1 Ag7 2.401(3) . ?
S1 C1 1.739(17) . ?
S1 Ag2 2.510(3) . ?
P1 Ag2 2.384(3) . ?
P1 C49 1.816(10) . ?
P1 C55 1.807(13) . ?
P1 C61 1.820(13) . ?
C1 C2 1.408(14) . ?
C1 C6 1.446(13) . ?
Ag2 S2 2.554(3) . ?
Ag2 Ag4 2.8538(13) . ?
Cl2 Ag16 2.396(3) . ?
S2 Ag3 2.686(3) . ?
S2 Ag4 2.471(3) . ?
S2 C9 1.784(12) . ?
P2 Ag8 2.467(3) . ?
P2 C61 1.879(11) . ?
P2 C62 1.831(12) . ?
P2 C68 1.818(15) . ?
C2 H2 0.9500 . ?
C2 C3 1.424(14) . ?
Ag3 P3 2.417(3) . ?
Ag3 Ag4 3.0543(14) . ?
Ag3 Ag5 2.9454(14) . ?
Ag3 S6 2.507(3) . ?
S3 Ag10 2.462(4) . ?
S3 Ag14 2.501(3) . ?
S3 C17 1.866(19) . ?
P3 C74 1.809(12) . ?
P3 C80 1.829(12) . ?
P3 C86 1.805(12) . ?
C3 H3 0.9500 . ?
C3 C4 1.393(14) . ?
Ag4 Ag5 2.8509(13) . ?
Ag4 Ag6 2.8035(13) . ?
Ag4 Ag7 2.8582(12) . ?
Ag4 Ag8 2.9865(14) . ?
S4 Ag13 2.470(3) . ?
S4 Ag14 2.557(3) . ?
S4 Ag15 2.720(3) . ?
S4 C25 1.785(13) . ?
P4 Ag6 2.461(3) . ?
P4 C86 1.904(10) . ?
P4 C87 1.787(11) . ?
P4 C93 1.854(13) . ?
C4 H4 0.9500 . ?
C4 C5 1.399(14) . ?
Ag5 Ag6 2.9137(13) . ?
Ag5 S6 2.429(3) . ?
Ag5 Ag9 2.8376(14) . ?
Ag5 Ag16 2.8438(11) . ?
S5 Ag11 2.457(3) . ?
S5 Ag15 2.498(3) . ?
S5 C33 1.829(13) . ?
P5 Ag9 2.458(3) . ?
P5 C99 1.828(12) . ?
P5 C105 1.804(12) . ?
P5 C111 1.837(13) . ?
C5 H5 0.9500 . ?
C5 C6 1.426(14) . ?
Ag6 Ag7 2.9320(12) . ?
Ag6 Ag12 2.9444(14) . ?
Ag6 Ag16 2.9333(12) . ?
S6 C41 1.768(13) . ?
P6 Ag14 2.409(3) . ?
P6 C111 1.856(11) . ?
P6 C112 1.819(13) . ?
P6 C118 1.840(14) . ?
C6 C7 1.595(17) . ?
Ag7 Ag8 2.9028(15) . ?
Ag7 Ag11 2.9073(14) . ?
Ag7 Ag12 2.9162(11) . ?
P7 Ag15 2.416(3) . ?
P7 C124 1.864(11) . ?
P7 C130 1.834(11) . ?
P7 C136 1.804(13) . ?
C7 H7A 0.9900 . ?
C7 H7B 0.9900 . ?
C7 C8 1.456(17) . ?
Ag8 Ag10 2.9410(12) . ?
Ag8 Ag11 2.8803(11) . ?
P8 Ag12 2.441(3) . ?
P8 C136 1.877(11) . ?
P8 C137 1.799(11) . ?
P8 C149 1.803(13) . ?
C8 H8A 0.9800 . ?
C8 H8B 0.9800 . ?
C8 H8C 0.9800 . ?
Ag9 Ag10 2.8062(12) . ?
Ag9 Ag13 2.9629(12) . ?
Ag9 Ag14 3.3435(16) . ?
Ag9 Ag16 2.9382(15) . ?
C9 C10 1.345(17) . ?
C9 C14 1.440(14) . ?
Ag10 Ag11 2.8804(13) . ?
Ag10 Ag13 2.8361(13) . ?
Ag10 Ag14 3.2386(13) . ?
C10 H10 0.9500 . ?
C10 C11 1.396(18) . ?
Ag11 Ag12 2.9044(13) . ?
Ag11 Ag13 2.8559(13) . ?
Ag11 Ag15 2.9827(11) . ?
C11 H11 0.9500 . ?
C11 C12 1.437(18) . ?
Ag12 Ag13 2.8401(13) . ?
Ag12 Ag16 2.9310(12) . ?
C12 H12 0.9500 . ?
C12 C13 1.36(2) . ?
Ag13 Ag14 2.8849(13) . ?
Ag13 Ag15 2.9844(12) . ?
Ag13 Ag16 2.8545(14) . ?
C13 H13 0.9500 . ?
C13 C14 1.425(19) . ?
C14 C15 1.478(19) . ?
C15 H15A 0.9900 . ?
C15 H15B 0.9900 . ?
C15 C16 1.51(2) . ?
C16 H16A 0.9800 . ?
C16 H16B 0.9800 . ?
C16 H16C 0.9800 . ?
C17 C18 1.39(3) . ?
C17 C22 1.36(2) . ?
C18 H18 0.9500 . ?
C18 C19 1.43(2) . ?
C19 H19 0.9500 . ?
C19 C20 1.34(3) . ?
C20 H20 0.9500 . ?
C20 C21 1.28(3) . ?
C21 H21 0.9500 . ?
C21 C22 1.49(3) . ?
C22 C23 1.482(17) . ?
C23 H23A 0.9900 . ?
C23 H23B 0.9900 . ?
C23 C24 1.49(3) . ?
C24 H24A 0.9800 . ?
C24 H24B 0.9800 . ?
C24 H24C 0.9800 . ?
C25 C26 1.396(19) . ?
C25 C30 1.418(15) . ?
C26 H26 0.9500 . ?
C26 C27 1.381(17) . ?
C27 H27 0.9500 . ?
C27 C28 1.380(17) . ?
C28 H28 0.9500 . ?
C28 C29 1.37(2) . ?
C29 H29 0.9500 . ?
C29 C30 1.370(18) . ?
C30 C31 1.53(2) . ?
C31 H31A 0.9900 . ?
C31 H31B 0.9900 . ?
C31 C32 1.515(17) . ?
C32 H32A 0.9800 . ?
C32 H32B 0.9800 . ?
C32 H32C 0.9800 . ?
C33 C34 1.37(2) . ?
C33 C38 1.380(17) . ?
C34 H34 0.9500 . ?
C34 C35 1.390(19) . ?
C35 H35 0.9500 . ?
C35 C36 1.386(19) . ?
C36 H36 0.9500 . ?
C36 C37 1.40(2) . ?
C37 H37 0.9500 . ?
C37 C38 1.359(19) . ?
C38 C39 1.54(2) . ?
C39 H39A 0.9900 . ?
C39 H39B 0.9900 . ?
C39 C40 1.527(19) . ?
C40 H40A 0.9800 . ?
C40 H40B 0.9800 . ?
C40 H40C 0.9800 . ?
C41 C42 1.412(18) . ?
C41 C46 1.414(18) . ?
C42 H42 0.9500 . ?
C42 C43 1.402(18) . ?
C43 H43 0.9500 . ?
C43 C44 1.32(2) . ?
C44 H44 0.9500 . ?
C44 C45 1.32(2) . ?
C45 H45 0.9500 . ?
C45 C46 1.46(2) . ?
C46 C47 1.46(2) . ?
C47 H47A 0.9900 . ?
C47 H47B 0.9900 . ?
C47 C48 1.57(2) . ?
C48 H48A 0.9800 . ?
C48 H48B 0.9800 . ?
C48 H48C 0.9800 . ?
C49 C50 1.32(2) . ?
C49 C54 1.375(19) . ?
C50 H50 0.9500 . ?
C50 C51 1.46(2) . ?
C51 H51 0.9500 . ?
C51 C52 1.37(2) . ?
C52 H52 0.9500 . ?
C52 C53 1.30(2) . ?
C53 H53 0.9500 . ?
C53 C54 1.38(2) . ?
C54 H54 0.9500 . ?
C55 C56 1.386(19) . ?
C55 C60 1.373(17) . ?
C56 H56 0.9500 . ?
C56 C57 1.396(18) . ?
C57 H57 0.9500 . ?
C57 C58 1.367(18) . ?
C58 H58 0.9500 . ?
C58 C59 1.40(2) . ?
C59 H59 0.9500 . ?
C59 C60 1.387(18) . ?
C60 H60 0.9500 . ?
C61 H61A 0.9900 . ?
C61 H61B 0.9900 . ?
C62 C63 1.377(18) . ?
C62 C67 1.378(16) . ?
C63 H63 0.9500 . ?
C63 C64 1.395(17) . ?
C64 H64 0.9500 . ?
C64 C65 1.397(18) . ?
C65 H65 0.9500 . ?
C65 C66 1.42(2) . ?
C66 H66 0.9500 . ?
C66 C67 1.350(18) . ?
C67 H67 0.9500 . ?
C68 C69 1.408(17) . ?
C68 C73 1.361(19) . ?
C69 H69 0.9500 . ?
C69 C70 1.31(2) . ?
C70 H70 0.9500 . ?
C70 C71 1.32(2) . ?
C71 H71 0.9500 . ?
C71 C72 1.39(2) . ?
C72 H72 0.9500 . ?
C72 C73 1.40(2) . ?
C73 H73 0.9500 . ?
C74 C75 1.47(2) . ?
C74 C79 1.371(16) . ?
C75 H75 0.9500 . ?
C75 C76 1.381(18) . ?
C76 H76 0.9500 . ?
C76 C77 1.385(19) . ?
C77 H77 0.9500 . ?
C77 C78 1.33(2) . ?
C78 H78 0.9500 . ?
C78 C79 1.388(18) . ?
C79 H79 0.9500 . ?
C80 C81 1.34(2) . ?
C80 C85 1.40(2) . ?
C81 H81 0.9500 . ?
C81 C82 1.460(19) . ?
C82 H82 0.9500 . ?
C82 C83 1.37(2) . ?
C83 H83 0.9500 . ?
C83 C84 1.42(2) . ?
C84 H84 0.9500 . ?
C84 C85 1.393(19) . ?
C85 H85 0.9500 . ?
C86 H86A 0.9900 . ?
C86 H86B 0.9900 . ?
C87 C88 1.408(12) . ?
C87 C92 1.384(11) . ?
C88 H88 0.9500 . ?
C88 C89 1.385(12) . ?
C89 H89 0.9500 . ?
C89 C90 1.408(12) . ?
C90 H90 0.9500 . ?
C90 C91 1.321(12) . ?
C91 H91 0.9500 . ?
C91 C92 1.367(11) . ?
C92 H92 0.9500 . ?
C93 C94 1.345(18) . ?
C93 C98 1.375(18) . ?
C94 H94 0.9500 . ?
C94 C95 1.376(19) . ?
C95 H95 0.9500 . ?
C95 C96 1.386(13) . ?
C96 H96 0.9500 . ?
C96 C97 1.353(19) . ?
C97 H97 0.9500 . ?
C97 C98 1.373(18) . ?
C98 H98 0.9500 . ?
C99 C100 1.359(18) . ?
C99 C104 1.412(16) . ?
C100 H100 0.9500 . ?
C100 C101 1.382(17) . ?
C101 H101 0.9500 . ?
C101 C102 1.367(18) . ?
C102 H102 0.9500 . ?
C102 C103 1.343(19) . ?
C103 H103 0.9500 . ?
C103 C104 1.364(17) . ?
C104 H104 0.9500 . ?
C105 C106 1.395(17) . ?
C105 C110 1.43(2) . ?
C106 H106 0.9500 . ?
C106 C107 1.393(17) . ?
C107 H107 0.9500 . ?
C107 C108 1.40(2) . ?
C108 H108 0.9500 . ?
C108 C109 1.39(2) . ?
C109 H109 0.9500 . ?
C109 C110 1.362(18) . ?
C110 H110 0.9500 . ?
C111 H11A 0.9900 . ?
C111 H11B 0.9900 . ?
C112 C113 1.361(18) . ?
C112 C117 1.369(16) . ?
C113 H113 0.9500 . ?
C113 C114 1.393(18) . ?
C114 H114 0.9500 . ?
C114 C115 1.366(17) . ?
C115 H115 0.9500 . ?
C115 C116 1.429(19) . ?
C116 H116 0.9500 . ?
C116 C117 1.311(17) . ?
C117 H117 0.9500 . ?
C118 C119 1.369(17) . ?
C118 C123 1.378(19) . ?
C119 H119 0.9500 . ?
C119 C120 1.385(19) . ?
C120 H120 0.9500 . ?
C120 C121 1.36(2) . ?
C121 H121 0.9500 . ?
C121 C122 1.389(19) . ?
C122 H122 0.9500 . ?
C122 C123 1.35(2) . ?
C123 H123 0.9500 . ?
C124 C125 1.343(19) . ?
C124 C129 1.350(17) . ?
C125 H125 0.9500 . ?
C125 C126 1.387(16) . ?
C126 H126 0.9500 . ?
C126 C127 1.37(2) . ?
C127 H127 0.9500 . ?
C127 C128 1.33(2) . ?
C128 H128 0.9500 . ?
C128 C129 1.474(16) . ?
C129 H129 0.9500 . ?
C130 C131 1.354(15) . ?
C130 C135 1.357(15) . ?
C131 H131 0.9500 . ?
C131 C132 1.398(16) . ?
C132 H132 0.9500 . ?
C132 C133 1.370(17) . ?
C133 H133 0.9500 . ?
C133 C134 1.409(18) . ?
C134 H134 0.9500 . ?
C134 C135 1.383(17) . ?
C135 H135 0.9500 . ?
C136 H13A 0.9900 . ?
C136 H13B 0.9900 . ?
C137 C138 1.380(16) . ?
C137 C142 1.403(15) . ?
C138 H138 0.9500 . ?
C138 C139 1.395(18) . ?
C139 H139 0.9500 . ?
C139 C140 1.356(19) . ?
C140 H140 0.9500 . ?
C140 C141 1.40(2) . ?
C141 H141 0.9500 . ?
C141 C142 1.403(18) . ?
C142 H142 0.9500 . ?
C145 H145 0.9500 . ?
C145 C146 1.41(2) . ?
C145 C150 1.342(19) . ?
C146 H146 0.9500 . ?
C146 C147 1.318(19) . ?
C147 H147 0.9500 . ?
C147 C148 1.402(19) . ?
C148 H148 0.9500 . ?
C148 C149 1.387(18) . ?
C149 C150 1.423(17) . ?
C150 H150 0.9500 . ?
Cl5 C144 1.732(19) . ?
Cl6 C144 1.658(17) . ?
C144 H14A 0.9900 . ?
C144 H14B 0.9900 . ?
Cl3 C143 1.73(2) . ?
Cl4 C143 1.76(2) . ?
C143 H14C 0.9900 . ?
C143 H14D 0.9900 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Ag1 Pt1 Ag6 115.75(4) . . ?
Ag1 Pt1 Ag8 60.85(3) . . ?
Ag1 Pt1 Ag9 63.01(2) . . ?
Ag1 Pt1 Ag10 63.84(3) . . ?
Ag4 Pt1 Ag1 63.02(3) . . ?
Ag4 Pt1 Ag5 63.06(3) . . ?
Ag4 Pt1 Ag6 61.43(3) . . ?
Ag4 Pt1 Ag7 63.30(3) . . ?
Ag4 Pt1 Ag8 65.83(3) . . ?
Ag4 Pt1 Ag9 114.65(3) . . ?
Ag4 Pt1 Ag10 119.31(3) . . ?
Ag4 Pt1 Ag11 118.12(3) . . ?
Ag4 Pt1 Ag12 116.27(3) . . ?
Ag4 Pt1 Ag16 115.00(3) . . ?
Ag5 Pt1 Ag1 63.88(3) . . ?
Ag5 Pt1 Ag6 63.97(3) . . ?
Ag5 Pt1 Ag8 116.56(3) . . ?
Ag5 Pt1 Ag9 61.85(3) . . ?
Ag5 Pt1 Ag10 114.40(3) . . ?
Ag5 Pt1 Ag11 177.50(3) . . ?
Ag5 Pt1 Ag12 117.65(3) . . ?
Ag5 Pt1 Ag16 62.66(3) . . ?
Ag6 Pt1 Ag8 117.65(3) . . ?
Ag6 Pt1 Ag9 117.23(3) . . ?
Ag7 Pt1 Ag1 113.77(3) . . ?
Ag7 Pt1 Ag5 117.93(3) . . ?
Ag7 Pt1 Ag6 64.48(3) . . ?
Ag7 Pt1 Ag8 63.66(3) . . ?
Ag7 Pt1 Ag9 176.69(2) . . ?
Ag7 Pt1 Ag10 117.61(3) . . ?
Ag7 Pt1 Ag11 64.28(3) . . ?
Ag7 Pt1 Ag12 64.53(2) . . ?
Ag7 Pt1 Ag16 118.84(4) . . ?
Ag8 Pt1 Ag9 113.27(3) . . ?
Ag10 Pt1 Ag6 177.91(2) . . ?
Ag10 Pt1 Ag8 64.11(3) . . ?
Ag10 Pt1 Ag9 60.69(3) . . ?
Ag11 Pt1 Ag1 114.41(3) . . ?
Ag11 Pt1 Ag6 118.50(3) . . ?
Ag11 Pt1 Ag8 62.99(3) . . ?
Ag11 Pt1 Ag9 115.88(3) . . ?
Ag11 Pt1 Ag10 63.12(3) . . ?
Ag12 Pt1 Ag1 178.03(2) . . ?
Ag12 Pt1 Ag6 64.69(3) . . ?
Ag12 Pt1 Ag8 117.19(3) . . ?
Ag12 Pt1 Ag9 118.67(3) . . ?
Ag12 Pt1 Ag10 115.81(3) . . ?
Ag12 Pt1 Ag11 64.11(3) . . ?
Ag12 Pt1 Ag16 64.78(3) . . ?
Ag13 Pt1 Ag1 117.92(3) . . ?
Ag13 Pt1 Ag4 178.14(3) . . ?
Ag13 Pt1 Ag5 115.68(3) . . ?
Ag13 Pt1 Ag6 116.88(3) . . ?
Ag13 Pt1 Ag7 116.99(3) . . ?
Ag13 Pt1 Ag8 116.01(3) . . ?
Ag13 Pt1 Ag9 65.15(3) . . ?
Ag13 Pt1 Ag10 62.34(3) . . ?
Ag13 Pt1 Ag11 63.19(3) . . ?
Ag13 Pt1 Ag12 62.84(3) . . ?
Ag13 Pt1 Ag16 63.17(3) . . ?
Ag16 Pt1 Ag1 117.19(3) . . ?
Ag16 Pt1 Ag6 64.39(3) . . ?
Ag16 Pt1 Ag8 177.50(3) . . ?
Ag16 Pt1 Ag9 64.23(3) . . ?
Ag16 Pt1 Ag10 113.82(3) . . ?
Ag16 Pt1 Ag11 117.68(3) . . ?
Pt1 Ag1 Ag2 107.54(3) . . ?
Pt1 Ag1 Ag4 57.82(3) . . ?
Pt1 Ag1 Ag5 57.62(3) . . ?
Pt1 Ag1 Ag8 59.88(2) . . ?
Pt1 Ag1 Ag9 59.01(3) . . ?
Pt1 Ag1 Ag10 58.20(2) . . ?
S1 Ag1 Pt1 154.98(9) . . ?
S1 Ag1 Ag2 50.03(7) . . ?
S1 Ag1 Ag4 97.17(9) . . ?
S1 Ag1 Ag5 112.47(9) . . ?
S1 Ag1 Ag8 110.85(7) . . ?
S1 Ag1 Ag9 139.23(7) . . ?
S1 Ag1 Ag10 141.44(10) . . ?
Ag4 Ag1 Ag2 55.33(3) . . ?
Ag4 Ag1 Ag5 59.24(3) . . ?
Ag4 Ag1 Ag9 107.15(4) . . ?
Ag4 Ag1 Ag10 109.85(4) . . ?
Ag5 Ag1 Ag2 104.95(4) . . ?
Ag5 Ag1 Ag10 104.99(3) . . ?
Ag8 Ag1 Ag2 68.18(3) . . ?
Ag8 Ag1 Ag4 63.61(3) . . ?
Ag8 Ag1 Ag5 110.34(4) . . ?
Ag8 Ag1 Ag9 109.18(4) . . ?
Ag8 Ag1 Ag10 61.80(3) . . ?
Ag9 Ag1 Ag2 162.11(4) . . ?
Ag9 Ag1 Ag5 58.54(3) . . ?
Ag9 Ag1 Ag10 57.65(3) . . ?
Ag10 Ag1 Ag2 127.90(3) . . ?
Ag1 S1 Ag2 81.75(9) . . ?
C1 S1 Ag1 113.7(5) . . ?
C1 S1 Ag2 101.6(6) . . ?
C49 P1 Ag2 111.1(4) . . ?
C49 P1 C61 104.3(6) . . ?
C55 P1 Ag2 122.0(4) . . ?
C55 P1 C49 104.2(5) . . ?
C55 P1 C61 103.1(6) . . ?
C61 P1 Ag2 110.6(4) . . ?
C2 C1 S1 119.5(10) . . ?
C2 C1 C6 123.9(15) . . ?
C6 C1 S1 116.6(13) . . ?
S1 Ag2 Ag1 48.22(6) . . ?
S1 Ag2 S2 103.78(11) . . ?
S1 Ag2 Ag4 95.86(7) . . ?
P1 Ag2 Ag1 126.75(8) . . ?
P1 Ag2 S1 126.53(11) . . ?
P1 Ag2 S2 127.62(10) . . ?
P1 Ag2 Ag4 124.15(7) . . ?
S2 Ag2 Ag1 96.05(6) . . ?
S2 Ag2 Ag4 54.02(6) . . ?
Ag4 Ag2 Ag1 55.60(3) . . ?
Ag2 S2 Ag3 130.08(10) . . ?
Ag4 S2 Ag2 69.19(8) . . ?
Ag4 S2 Ag3 72.51(7) . . ?
C9 S2 Ag2 108.5(4) . . ?
C9 S2 Ag3 110.9(4) . . ?
C9 S2 Ag4 104.1(4) . . ?
C61 P2 Ag8 117.5(4) . . ?
C62 P2 Ag8 114.6(4) . . ?
C62 P2 C61 103.7(5) . . ?
C68 P2 Ag8 112.1(4) . . ?
C68 P2 C61 103.0(6) . . ?
C68 P2 C62 104.5(6) . . ?
C1 C2 H2 119.8 . . ?
C1 C2 C3 120.4(17) . . ?
C3 C2 H2 119.8 . . ?
S2 Ag3 Ag4 50.49(6) . . ?
S2 Ag3 Ag5 98.57(7) . . ?
P3 Ag3 S2 105.44(9) . . ?
P3 Ag3 Ag4 119.13(7) . . ?
P3 Ag3 Ag5 140.01(7) . . ?
P3 Ag3 S6 138.25(10) . . ?
Ag5 Ag3 Ag4 56.71(3) . . ?
S6 Ag3 S2 111.24(10) . . ?
S6 Ag3 Ag4 99.71(8) . . ?
S6 Ag3 Ag5 52.15(7) . . ?
Ag10 S3 Ag14 81.46(11) . . ?
C17 S3 Ag10 106.9(6) . . ?
C17 S3 Ag14 102.2(5) . . ?
C74 P3 Ag3 117.6(4) . . ?
C74 P3 C80 102.6(5) . . ?
C80 P3 Ag3 111.9(5) . . ?
C86 P3 Ag3 114.0(4) . . ?
C86 P3 C74 107.0(6) . . ?
C86 P3 C80 101.9(6) . . ?
C2 C3 H3 119.6 . . ?
C4 C3 C2 120.7(18) . . ?
C4 C3 H3 119.6 . . ?
Pt1 Ag4 Ag1 59.16(3) . . ?
Pt1 Ag4 Ag2 120.86(4) . . ?
Pt1 Ag4 Ag3 113.81(4) . . ?
Pt1 Ag4 Ag5 58.69(2) . . ?
Pt1 Ag4 Ag6 60.15(2) . . ?
Pt1 Ag4 Ag7 58.49(3) . . ?
Pt1 Ag4 Ag8 57.99(3) . . ?
Ag1 Ag4 Ag3 107.47(4) . . ?
Ag1 Ag4 Ag8 57.21(3) . . ?
Ag2 Ag4 Ag1 69.07(3) . . ?
Ag2 Ag4 Ag3 107.01(3) . . ?
Ag2 Ag4 Ag7 118.80(4) . . ?
Ag2 Ag4 Ag8 71.32(3) . . ?
S2 Ag4 Pt1 163.47(7) . . ?
S2 Ag4 Ag1 108.42(8) . . ?
S2 Ag4 Ag2 56.79(7) . . ?
S2 Ag4 Ag3 57.01(7) . . ?
S2 Ag4 Ag5 106.56(6) . . ?
S2 Ag4 Ag6 121.98(8) . . ?
S2 Ag4 Ag7 138.00(7) . . ?
S2 Ag4 Ag8 126.85(7) . . ?
Ag5 Ag4 Ag1 61.11(3) . . ?
Ag5 Ag4 Ag2 117.56(3) . . ?
Ag5 Ag4 Ag3 59.72(3) . . ?
Ag5 Ag4 Ag7 110.05(3) . . ?
Ag5 Ag4 Ag8 106.74(3) . . ?
Ag6 Ag4 Ag1 111.37(4) . . ?
Ag6 Ag4 Ag2 178.68(4) . . ?
Ag6 Ag4 Ag3 71.67(3) . . ?
Ag6 Ag4 Ag5 62.03(3) . . ?
Ag6 Ag4 Ag7 62.37(3) . . ?
Ag6 Ag4 Ag8 109.98(3) . . ?
Ag7 Ag4 Ag1 106.86(4) . . ?
Ag7 Ag4 Ag3 129.91(4) . . ?
Ag7 Ag4 Ag8 59.51(3) . . ?
Ag8 Ag4 Ag3 164.49(3) . . ?
Ag13 S4 Ag14 70.02(7) . . ?
Ag13 S4 Ag15 70.02(7) . . ?
Ag14 S4 Ag15 128.46(10) . . ?
C25 S4 Ag13 102.8(4) . . ?
C25 S4 Ag14 109.4(4) . . ?
C25 S4 Ag15 110.1(4) . . ?
C86 P4 Ag6 118.6(4) . . ?
C87 P4 Ag6 113.6(4) . . ?
C87 P4 C86 103.2(5) . . ?
C87 P4 C93 108.5(6) . . ?
C93 P4 Ag6 112.5(4) . . ?
C93 P4 C86 99.0(5) . . ?
C3 C4 H4 123.9 . . ?
C3 C4 C5 112.3(17) . . ?
C5 C4 H4 123.9 . . ?
Pt1 Ag5 Ag1 58.50(3) . . ?
Pt1 Ag5 Ag3 116.93(4) . . ?
Pt1 Ag5 Ag4 58.25(3) . . ?
Pt1 Ag5 Ag6 58.62(3) . . ?
Pt1 Ag5 Ag9 60.06(3) . . ?
Pt1 Ag5 Ag16 58.75(3) . . ?
Ag1 Ag5 Ag3 109.34(3) . . ?
Ag1 Ag5 Ag6 107.12(4) . . ?
Ag4 Ag5 Ag1 59.66(3) . . ?
Ag4 Ag5 Ag3 63.57(3) . . ?
Ag4 Ag5 Ag6 58.19(3) . . ?
Ag6 Ag5 Ag3 71.80(3) . . ?
S6 Ag5 Pt1 164.12(7) . . ?
S6 Ag5 Ag1 109.42(8) . . ?
S6 Ag5 Ag3 54.59(7) . . ?
S6 Ag5 Ag4 107.52(7) . . ?
S6 Ag5 Ag6 122.18(8) . . ?
S6 Ag5 Ag9 125.51(8) . . ?
S6 Ag5 Ag16 136.89(7) . . ?
Ag9 Ag5 Ag1 60.63(3) . . ?
Ag9 Ag5 Ag3 169.90(4) . . ?
Ag9 Ag5 Ag4 109.19(4) . . ?
Ag9 Ag5 Ag6 111.16(3) . . ?
Ag9 Ag5 Ag16 62.28(3) . . ?
Ag16 Ag5 Ag1 109.35(4) . . ?
Ag16 Ag5 Ag3 125.63(4) . . ?
Ag16 Ag5 Ag4 107.82(3) . . ?
Ag16 Ag5 Ag6 61.24(3) . . ?
Ag11 S5 Ag15 74.01(8) . . ?
C33 S5 Ag11 104.2(4) . . ?
C33 S5 Ag15 109.0(4) . . ?
C99 P5 Ag9 112.9(4) . . ?
C99 P5 C111 106.3(5) . . ?
C105 P5 Ag9 114.6(4) . . ?
C105 P5 C99 102.9(6) . . ?
C105 P5 C111 101.8(6) . . ?
C111 P5 Ag9 116.7(4) . . ?
C4 C5 H5 113.4 . . ?
C4 C5 C6 133.1(18) . . ?
C6 C5 H5 113.4 . . ?
Pt1 Ag6 Ag4 58.42(3) . . ?
Pt1 Ag6 Ag5 57.41(3) . . ?
Pt1 Ag6 Ag7 57.08(3) . . ?
Pt1 Ag6 Ag12 57.11(3) . . ?
Pt1 Ag6 Ag16 57.28(3) . . ?
Ag4 Ag6 Ag5 59.78(3) . . ?
Ag4 Ag6 Ag7 59.73(3) . . ?
Ag4 Ag6 Ag12 107.37(3) . . ?
Ag4 Ag6 Ag16 106.65(4) . . ?
P4 Ag6 Pt1 175.09(7) . . ?
P4 Ag6 Ag4 120.37(7) . . ?
P4 Ag6 Ag5 126.77(7) . . ?
P4 Ag6 Ag7 118.02(7) . . ?
P4 Ag6 Ag12 120.90(7) . . ?
P4 Ag6 Ag16 126.43(7) . . ?
Ag5 Ag6 Ag7 106.31(4) . . ?
Ag5 Ag6 Ag12 105.97(3) . . ?
Ag5 Ag6 Ag16 58.20(3) . . ?
Ag7 Ag6 Ag12 59.50(3) . . ?
Ag7 Ag6 Ag16 106.65(4) . . ?
Ag16 Ag6 Ag12 59.82(3) . . ?
Ag5 S6 Ag3 73.26(8) . . ?
C41 S6 Ag3 104.2(4) . . ?
C41 S6 Ag5 111.2(4) . . ?
C111 P6 Ag14 111.6(4) . . ?
C112 P6 Ag14 120.2(4) . . ?
C112 P6 C111 104.9(6) . . ?
C112 P6 C118 102.7(6) . . ?
C118 P6 Ag14 110.0(4) . . ?
C118 P6 C111 106.4(6) . . ?
C1 C6 C7 119.3(15) . . ?
C5 C6 C1 107.5(15) . . ?
C5 C6 C7 129.0(15) . . ?
Pt1 Ag7 Ag4 58.21(3) . . ?
Pt1 Ag7 Ag6 58.44(3) . . ?
Pt1 Ag7 Ag8 58.98(2) . . ?
Pt1 Ag7 Ag11 58.03(2) . . ?
Pt1 Ag7 Ag12 57.86(3) . . ?
Cl1 Ag7 Pt1 179.21(8) . . ?
Cl1 Ag7 Ag4 122.54(9) . . ?
Cl1 Ag7 Ag6 121.60(9) . . ?
Cl1 Ag7 Ag8 121.44(8) . . ?
Cl1 Ag7 Ag11 121.47(9) . . ?
Cl1 Ag7 Ag12 121.40(8) . . ?
Ag4 Ag7 Ag6 57.90(3) . . ?
Ag4 Ag7 Ag8 62.44(3) . . ?
Ag4 Ag7 Ag11 108.55(4) . . ?
Ag4 Ag7 Ag12 106.68(3) . . ?
Ag8 Ag7 Ag6 108.78(3) . . ?
Ag8 Ag7 Ag11 59.44(3) . . ?
Ag8 Ag7 Ag12 107.86(4) . . ?
Ag11 Ag7 Ag6 108.27(4) . . ?
Ag11 Ag7 Ag12 59.83(3) . . ?
Ag12 Ag7 Ag6 60.46(3) . . ?
C124 P7 Ag15 115.1(4) . . ?
C130 P7 Ag15 114.4(4) . . ?
C130 P7 C124 101.7(5) . . ?
C136 P7 Ag15 114.4(4) . . ?
C136 P7 C124 103.6(5) . . ?
C136 P7 C130 106.3(6) . . ?
C6 C7 H7A 113.3 . . ?
C6 C7 H7B 113.3 . . ?
H7A C7 H7B 110.6 . . ?
C8 C7 C6 92.1(19) . . ?
C8 C7 H7A 113.3 . . ?
C8 C7 H7B 113.3 . . ?
Pt1 Ag8 Ag1 59.27(3) . . ?
Pt1 Ag8 Ag4 56.18(2) . . ?
Pt1 Ag8 Ag7 57.36(3) . . ?
Pt1 Ag8 Ag10 57.78(3) . . ?
Pt1 Ag8 Ag11 57.87(3) . . ?
Ag1 Ag8 Ag4 59.18(3) . . ?
Ag1 Ag8 Ag7 107.28(3) . . ?
Ag1 Ag8 Ag10 61.07(3) . . ?
Ag1 Ag8 Ag11 108.78(3) . . ?
P2 Ag8 Pt1 169.94(8) . . ?
P2 Ag8 Ag1 120.31(8) . . ?
P2 Ag8 Ag4 133.32(7) . . ?
P2 Ag8 Ag7 128.31(8) . . ?
P2 Ag8 Ag10 112.58(8) . . ?
P2 Ag8 Ag11 115.91(7) . . ?
Ag7 Ag8 Ag4 58.05(3) . . ?
Ag7 Ag8 Ag10 107.05(3) . . ?
Ag10 Ag8 Ag4 105.99(4) . . ?
Ag11 Ag8 Ag4 105.83(4) . . ?
Ag11 Ag8 Ag7 60.36(3) . . ?
Ag11 Ag8 Ag10 59.30(3) . . ?
C136 P8 Ag12 114.7(4) . . ?
C137 P8 Ag12 118.3(4) . . ?
C137 P8 C136 106.0(5) . . ?
C137 P8 C149 105.1(6) . . ?
C149 P8 Ag12 111.2(4) . . ?
C149 P8 C136 99.5(5) . . ?
C7 C8 H8A 109.5 . . ?
C7 C8 H8B 109.5 . . ?
C7 C8 H8C 109.5 . . ?
H8A C8 H8B 109.5 . . ?
H8A C8 H8C 109.5 . . ?
H8B C8 H8C 109.5 . . ?
Pt1 Ag9 Ag1 57.98(3) . . ?
Pt1 Ag9 Ag5 58.09(3) . . ?
Pt1 Ag9 Ag10 59.25(3) . . ?
Pt1 Ag9 Ag13 56.18(2) . . ?
Pt1 Ag9 Ag14 104.45(3) . . ?
Pt1 Ag9 Ag16 57.02(2) . . ?
Ag1 Ag9 Ag13 106.20(3) . . ?
Ag1 Ag9 Ag14 122.09(3) . . ?
Ag1 Ag9 Ag16 106.93(4) . . ?
Ag5 Ag9 Ag1 60.83(3) . . ?
Ag5 Ag9 Ag13 105.23(4) . . ?
Ag5 Ag9 Ag14 159.22(3) . . ?
Ag5 Ag9 Ag16 58.96(3) . . ?
P5 Ag9 Pt1 166.67(7) . . ?
P5 Ag9 Ag1 110.04(7) . . ?
P5 Ag9 Ag5 112.18(8) . . ?
P5 Ag9 Ag10 122.43(8) . . ?
P5 Ag9 Ag13 137.00(7) . . ?
P5 Ag9 Ag14 86.78(7) . . ?
P5 Ag9 Ag16 128.13(8) . . ?
Ag10 Ag9 Ag1 61.56(3) . . ?
Ag10 Ag9 Ag5 109.94(4) . . ?
Ag10 Ag9 Ag13 58.82(3) . . ?
Ag10 Ag9 Ag14 62.84(3) . . ?
Ag10 Ag9 Ag16 106.73(3) . . ?
Ag13 Ag9 Ag14 54.04(3) . . ?
Ag16 Ag9 Ag13 57.86(3) . . ?
Ag16 Ag9 Ag14 103.02(3) . . ?
C10 C9 S2 122.6(8) . . ?
C10 C9 C14 121.6(11) . . ?
C14 C9 S2 115.9(10) . . ?
Pt1 Ag10 Ag1 57.96(3) . . ?
Pt1 Ag10 Ag8 58.11(3) . . ?
Pt1 Ag10 Ag9 60.07(3) . . ?
Pt1 Ag10 Ag11 57.97(3) . . ?
Pt1 Ag10 Ag13 57.91(3) . . ?
Pt1 Ag10 Ag14 107.79(3) . . ?
Ag1 Ag10 Ag8 57.12(3) . . ?
Ag1 Ag10 Ag14 125.05(3) . . ?
S3 Ag10 Pt1 156.46(8) . . ?
S3 Ag10 Ag1 137.12(10) . . ?
S3 Ag10 Ag8 142.26(7) . . ?
S3 Ag10 Ag9 107.95(8) . . ?
S3 Ag10 Ag11 116.55(9) . . ?
S3 Ag10 Ag13 98.92(8) . . ?
S3 Ag10 Ag14 49.79(7) . . ?
Ag8 Ag10 Ag14 163.58(4) . . ?
Ag9 Ag10 Ag1 60.79(3) . . ?
Ag9 Ag10 Ag8 107.90(4) . . ?
Ag9 Ag10 Ag11 110.90(4) . . ?
Ag9 Ag10 Ag13 63.35(3) . . ?
Ag9 Ag10 Ag14 66.72(3) . . ?
Ag11 Ag10 Ag1 105.59(3) . . ?
Ag11 Ag10 Ag8 59.30(3) . . ?
Ag11 Ag10 Ag14 107.05(3) . . ?
Ag13 Ag10 Ag1 109.03(3) . . ?
Ag13 Ag10 Ag8 107.35(3) . . ?
Ag13 Ag10 Ag11 59.94(3) . . ?
Ag13 Ag10 Ag14 56.24(3) . . ?
C9 C10 H10 117.7 . . ?
C9 C10 C11 124.6(11) . . ?
C11 C10 H10 117.7 . . ?
Pt1 Ag11 Ag7 57.69(3) . . ?
Pt1 Ag11 Ag8 59.15(3) . . ?
Pt1 Ag11 Ag10 58.91(3) . . ?
Pt1 Ag11 Ag12 57.90(3) . . ?
Pt1 Ag11 Ag13 57.98(3) . . ?
Pt1 Ag11 Ag15 114.33(3) . . ?
S5 Ag11 Pt1 165.44(7) . . ?
S5 Ag11 Ag7 134.57(8) . . ?
S5 Ag11 Ag8 130.99(7) . . ?
S5 Ag11 Ag10 114.04(9) . . ?
S5 Ag11 Ag12 117.91(8) . . ?
S5 Ag11 Ag13 107.54(7) . . ?
S5 Ag11 Ag15 53.61(7) . . ?
Ag7 Ag11 Ag15 125.81(4) . . ?
Ag8 Ag11 Ag7 60.20(3) . . ?
Ag8 Ag11 Ag10 61.40(3) . . ?
Ag8 Ag11 Ag12 108.79(4) . . ?
Ag8 Ag11 Ag15 168.73(3) . . ?
Ag10 Ag11 Ag7 108.56(3) . . ?
Ag10 Ag11 Ag12 107.33(4) . . ?
Ag10 Ag11 Ag15 107.55(4) . . ?
Ag12 Ag11 Ag7 60.23(3) . . ?
Ag12 Ag11 Ag15 71.23(4) . . ?
Ag13 Ag11 Ag7 107.18(3) . . ?
Ag13 Ag11 Ag8 108.48(3) . . ?
Ag13 Ag11 Ag10 59.26(3) . . ?
Ag13 Ag11 Ag12 59.08(3) . . ?
Ag13 Ag11 Ag15 61.44(3) . . ?
C10 C11 H11 122.5 . . ?
C10 C11 C12 114.9(13) . . ?
C12 C11 H11 122.5 . . ?
Pt1 Ag12 Ag6 58.21(2) . . ?
Pt1 Ag12 Ag7 57.61(3) . . ?
Pt1 Ag12 Ag11 57.99(3) . . ?
Pt1 Ag12 Ag13 58.20(3) . . ?
Pt1 Ag12 Ag16 57.64(2) . . ?
Ag7 Ag12 Ag6 60.04(3) . . ?
Ag7 Ag12 Ag16 107.13(4) . . ?
P8 Ag12 Pt1 173.20(7) . . ?
P8 Ag12 Ag6 118.27(8) . . ?
P8 Ag12 Ag7 126.87(7) . . ?
P8 Ag12 Ag11 128.10(8) . . ?
P8 Ag12 Ag13 120.74(7) . . ?
P8 Ag12 Ag16 115.69(7) . . ?
Ag11 Ag12 Ag6 108.01(3) . . ?
Ag11 Ag12 Ag7 59.93(3) . . ?
Ag11 Ag12 Ag16 106.80(4) . . ?
Ag13 Ag12 Ag6 107.68(4) . . ?
Ag13 Ag12 Ag7 107.36(4) . . ?
Ag13 Ag12 Ag11 59.61(3) . . ?
Ag13 Ag12 Ag16 59.27(3) . . ?
Ag16 Ag12 Ag6 59.90(3) . . ?
C11 C12 H12 119.4 . . ?
C13 C12 C11 121.1(12) . . ?
C13 C12 H12 119.4 . . ?
Pt1 Ag13 Ag9 58.67(3) . . ?
Pt1 Ag13 Ag10 59.74(2) . . ?
Pt1 Ag13 Ag11 58.83(2) . . ?
Pt1 Ag13 Ag12 58.96(3) . . ?
Pt1 Ag13 Ag14 120.44(4) . . ?
Pt1 Ag13 Ag15 115.05(4) . . ?
Pt1 Ag13 Ag16 58.83(3) . . ?
S4 Ag13 Pt1 166.69(7) . . ?
S4 Ag13 Ag9 124.15(7) . . ?
S4 Ag13 Ag10 109.47(8) . . ?
S4 Ag13 Ag11 109.93(7) . . ?
S4 Ag13 Ag12 124.10(8) . . ?
S4 Ag13 Ag14 56.39(7) . . ?
S4 Ag13 Ag15 58.92(7) . . ?
S4 Ag13 Ag16 134.48(7) . . ?
Ag9 Ag13 Ag15 166.45(3) . . ?
Ag10 Ag13 Ag9 57.83(3) . . ?
Ag10 Ag13 Ag11 60.80(3) . . ?
Ag10 Ag13 Ag12 110.36(4) . . ?
Ag10 Ag13 Ag14 68.95(4) . . ?
Ag10 Ag13 Ag15 108.68(4) . . ?
Ag10 Ag13 Ag16 108.22(3) . . ?
Ag11 Ag13 Ag9 107.20(3) . . ?
Ag11 Ag13 Ag14 118.16(4) . . ?
Ag11 Ag13 Ag15 61.37(3) . . ?
Ag12 Ag13 Ag9 109.92(4) . . ?
Ag12 Ag13 Ag11 61.31(3) . . ?
Ag12 Ag13 Ag14 179.31(3) . . ?
Ag12 Ag13 Ag15 72.08(4) . . ?
Ag12 Ag13 Ag16 61.95(3) . . ?
Ag14 Ag13 Ag9 69.73(4) . . ?
Ag14 Ag13 Ag15 108.11(4) . . ?
Ag16 Ag13 Ag9 60.64(3) . . ?
Ag16 Ag13 Ag11 110.25(3) . . ?
Ag16 Ag13 Ag14 118.13(4) . . ?
Ag16 Ag13 Ag15 128.41(4) . . ?
C12 C13 H13 118.3 . . ?
C12 C13 C14 123.5(12) . . ?
C14 C13 H13 118.3 . . ?
S3 Ag14 S4 107.49(11) . . ?
S3 Ag14 Ag9 92.61(8) . . ?
S3 Ag14 Ag10 48.75(8) . . ?
S3 Ag14 Ag13 96.74(9) . . ?
S4 Ag14 Ag9 108.35(7) . . ?
S4 Ag14 Ag10 96.21(6) . . ?
S4 Ag14 Ag13 53.58(7) . . ?
P6 Ag14 S3 122.19(12) . . ?
P6 Ag14 S4 128.41(10) . . ?
P6 Ag14 Ag9 83.84(8) . . ?
P6 Ag14 Ag10 125.94(8) . . ?
P6 Ag14 Ag13 125.98(9) . . ?
Ag10 Ag14 Ag9 50.44(2) . . ?
Ag13 Ag14 Ag9 56.23(3) . . ?
Ag13 Ag14 Ag10 54.81(3) . . ?
C9 C14 C15 123.8(12) . . ?
C13 C14 C9 114.2(12) . . ?
C13 C14 C15 122.0(11) . . ?
S4 Ag15 Ag11 99.84(6) . . ?
S4 Ag15 Ag13 51.07(6) . . ?
S5 Ag15 S4 116.81(10) . . ?
S5 Ag15 Ag11 52.38(7) . . ?
S5 Ag15 Ag13 102.71(7) . . ?
P7 Ag15 S4 101.28(9) . . ?
P7 Ag15 S5 137.98(10) . . ?
P7 Ag15 Ag11 139.79(8) . . ?
P7 Ag15 Ag13 115.28(8) . . ?
Ag11 Ag15 Ag13 57.19(3) . . ?
C14 C15 H15A 106.4 . . ?
C14 C15 H15B 106.4 . . ?
C14 C15 C16 123.7(13) . . ?
H15A C15 H15B 106.5 . . ?
C16 C15 H15A 106.4 . . ?
C16 C15 H15B 106.4 . . ?
Pt1 Ag16 Ag5 58.59(3) . . ?
Pt1 Ag16 Ag6 58.33(3) . . ?
Pt1 Ag16 Ag9 58.74(3) . . ?
Pt1 Ag16 Ag12 57.58(3) . . ?
Pt1 Ag16 Ag13 58.00(2) . . ?
Cl2 Ag16 Pt1 176.84(8) . . ?
Cl2 Ag16 Ag5 118.25(8) . . ?
Cl2 Ag16 Ag6 120.68(9) . . ?
Cl2 Ag16 Ag9 120.13(8) . . ?
Cl2 Ag16 Ag12 125.00(8) . . ?
Cl2 Ag16 Ag13 124.53(8) . . ?
Ag5 Ag16 Ag6 60.55(3) . . ?
Ag5 Ag16 Ag9 58.76(3) . . ?
Ag5 Ag16 Ag12 108.18(3) . . ?
Ag5 Ag16 Ag13 107.98(4) . . ?
Ag6 Ag16 Ag9 107.81(3) . . ?
Ag12 Ag16 Ag6 60.28(3) . . ?
Ag12 Ag16 Ag9 108.11(3) . . ?
Ag13 Ag16 Ag6 107.60(4) . . ?
Ag13 Ag16 Ag9 61.51(3) . . ?
Ag13 Ag16 Ag12 58.78(3) . . ?
C15 C16 H16A 109.5 . . ?
C15 C16 H16B 109.5 . . ?
C15 C16 H16C 109.5 . . ?
H16A C16 H16B 109.5 . . ?
H16A C16 H16C 109.5 . . ?
H16B C16 H16C 109.5 . . ?
C18 C17 S3 116.6(13) . . ?
C22 C17 S3 122.1(16) . . ?
C22 C17 C18 121.3(19) . . ?
C17 C18 H18 121.2 . . ?
C17 C18 C19 117.5(18) . . ?
C19 C18 H18 121.2 . . ?
C18 C19 H19 119.0 . . ?
C20 C19 C18 122(2) . . ?
C20 C19 H19 119.0 . . ?
C19 C20 H20 120.4 . . ?
C21 C20 C19 119(2) . . ?
C21 C20 H20 120.4 . . ?
C20 C21 H21 118.2 . . ?
C20 C21 C22 124(2) . . ?
C22 C21 H21 118.2 . . ?
C17 C22 C21 115.8(18) . . ?
C17 C22 C23 121.4(19) . . ?
C23 C22 C21 122.8(17) . . ?
C22 C23 H23A 110.1 . . ?
C22 C23 H23B 110.1 . . ?
C22 C23 C24 108.0(18) . . ?
H23A C23 H23B 108.4 . . ?
C24 C23 H23A 110.1 . . ?
C24 C23 H23B 110.1 . . ?
C23 C24 H24A 109.5 . . ?
C23 C24 H24B 109.5 . . ?
C23 C24 H24C 109.5 . . ?
H24A C24 H24B 109.5 . . ?
H24A C24 H24C 109.5 . . ?
H24B C24 H24C 109.5 . . ?
C26 C25 S4 121.3(9) . . ?
C26 C25 C30 118.3(11) . . ?
C30 C25 S4 120.4(11) . . ?
C25 C26 H26 119.4 . . ?
C27 C26 C25 121.2(11) . . ?
C27 C26 H26 119.4 . . ?
C26 C27 H27 120.2 . . ?
C28 C27 C26 119.7(14) . . ?
C28 C27 H27 120.2 . . ?
C27 C28 H28 120.3 . . ?
C29 C28 C27 119.5(13) . . ?
C29 C28 H28 120.3 . . ?
C28 C29 H29 118.8 . . ?
C28 C29 C30 122.3(12) . . ?
C30 C29 H29 118.8 . . ?
C25 C30 C31 119.9(11) . . ?
C29 C30 C25 118.8(13) . . ?
C29 C30 C31 121.2(10) . . ?
C30 C31 H31A 108.0 . . ?
C30 C31 H31B 108.0 . . ?
H31A C31 H31B 107.2 . . ?
C32 C31 C30 117.3(12) . . ?
C32 C31 H31A 108.0 . . ?
C32 C31 H31B 108.0 . . ?
C31 C32 H32A 109.5 . . ?
C31 C32 H32B 109.5 . . ?
C31 C32 H32C 109.5 . . ?
H32A C32 H32B 109.5 . . ?
H32A C32 H32C 109.5 . . ?
H32B C32 H32C 109.5 . . ?
C34 C33 S5 121.7(9) . . ?
C34 C33 C38 117.8(12) . . ?
C38 C33 S5 120.5(11) . . ?
C33 C34 H34 117.2 . . ?
C33 C34 C35 125.6(13) . . ?
C35 C34 H34 117.2 . . ?
C34 C35 H35 123.1 . . ?
C36 C35 C34 113.8(14) . . ?
C36 C35 H35 123.1 . . ?
C35 C36 H36 118.6 . . ?
C35 C36 C37 122.7(14) . . ?
C37 C36 H36 118.6 . . ?
C36 C37 H37 120.1 . . ?
C38 C37 C36 119.7(12) . . ?
C38 C37 H37 120.1 . . ?
C33 C38 C39 119.4(12) . . ?
C37 C38 C33 120.4(14) . . ?
C37 C38 C39 120.3(12) . . ?
C38 C39 H39A 109.0 . . ?
C38 C39 H39B 109.0 . . ?
H39A C39 H39B 107.8 . . ?
C40 C39 C38 112.8(13) . . ?
C40 C39 H39A 109.0 . . ?
C40 C39 H39B 109.0 . . ?
C39 C40 H40A 109.5 . . ?
C39 C40 H40B 109.5 . . ?
C39 C40 H40C 109.5 . . ?
H40A C40 H40B 109.5 . . ?
H40A C40 H40C 109.5 . . ?
H40B C40 H40C 109.5 . . ?
C42 C41 S6 120.1(9) . . ?
C42 C41 C46 120.1(12) . . ?
C46 C41 S6 119.8(10) . . ?
C41 C42 H42 120.6 . . ?
C43 C42 C41 118.8(13) . . ?
C43 C42 H42 120.6 . . ?
C42 C43 H43 118.8 . . ?
C44 C43 C42 122.3(15) . . ?
C44 C43 H43 118.8 . . ?
C43 C44 H44 119.8 . . ?
C45 C44 C43 120.4(14) . . ?
C45 C44 H44 119.8 . . ?
C44 C45 H45 118.2 . . ?
C44 C45 C46 123.6(14) . . ?
C46 C45 H45 118.2 . . ?
C41 C46 C45 114.8(13) . . ?
C41 C46 C47 122.5(13) . . ?
C47 C46 C45 122.6(13) . . ?
C46 C47 H47A 109.2 . . ?
C46 C47 H47B 109.2 . . ?
C46 C47 C48 111.9(13) . . ?
H47A C47 H47B 107.9 . . ?
C48 C47 H47A 109.2 . . ?
C48 C47 H47B 109.2 . . ?
C47 C48 H48A 109.5 . . ?
C47 C48 H48B 109.5 . . ?
C47 C48 H48C 109.5 . . ?
H48A C48 H48B 109.5 . . ?
H48A C48 H48C 109.5 . . ?
H48B C48 H48C 109.5 . . ?
C50 C49 P1 123.8(11) . . ?
C50 C49 C54 115.6(12) . . ?
C54 C49 P1 120.4(11) . . ?
C49 C50 H50 119.6 . . ?
C49 C50 C51 120.8(15) . . ?
C51 C50 H50 119.6 . . ?
C50 C51 H51 119.9 . . ?
C52 C51 C50 120.1(15) . . ?
C52 C51 H51 119.9 . . ?
C51 C52 H52 121.1 . . ?
C53 C52 C51 117.9(15) . . ?
C53 C52 H52 121.1 . . ?
C52 C53 H53 119.0 . . ?
C52 C53 C54 122.0(17) . . ?
C54 C53 H53 119.0 . . ?
C49 C54 C53 123.5(15) . . ?
C49 C54 H54 118.3 . . ?
C53 C54 H54 118.3 . . ?
C56 C55 P1 118.7(10) . . ?
C60 C55 P1 122.0(11) . . ?
C60 C55 C56 119.1(12) . . ?
C55 C56 H56 119.4 . . ?
C55 C56 C57 121.1(12) . . ?
C57 C56 H56 119.4 . . ?
C56 C57 H57 120.5 . . ?
C58 C57 C56 119.0(14) . . ?
C58 C57 H57 120.5 . . ?
C57 C58 H58 119.7 . . ?
C57 C58 C59 120.5(13) . . ?
C59 C58 H58 119.7 . . ?
C58 C59 H59 120.2 . . ?
C60 C59 C58 119.6(13) . . ?
C60 C59 H59 120.2 . . ?
C55 C60 C59 120.5(13) . . ?
C55 C60 H60 119.7 . . ?
C59 C60 H60 119.7 . . ?
P1 C61 P2 112.7(6) . . ?
P1 C61 H61A 109.0 . . ?
P1 C61 H61B 109.0 . . ?
P2 C61 H61A 109.0 . . ?
P2 C61 H61B 109.0 . . ?
H61A C61 H61B 107.8 . . ?
C63 C62 P2 117.2(9) . . ?
C63 C62 C67 121.2(11) . . ?
C67 C62 P2 121.6(10) . . ?
C62 C63 H63 119.5 . . ?
C62 C63 C64 121.0(12) . . ?
C64 C63 H63 119.5 . . ?
C63 C64 H64 121.2 . . ?
C63 C64 C65 117.6(13) . . ?
C65 C64 H64 121.2 . . ?
C64 C65 H65 120.2 . . ?
C64 C65 C66 119.7(12) . . ?
C66 C65 H65 120.2 . . ?
C65 C66 H66 119.4 . . ?
C67 C66 C65 121.2(12) . . ?
C67 C66 H66 119.4 . . ?
C62 C67 H67 120.5 . . ?
C66 C67 C62 119.0(13) . . ?
C66 C67 H67 120.5 . . ?
C69 C68 P2 121.2(10) . . ?
C73 C68 P2 123.8(10) . . ?
C73 C68 C69 114.8(14) . . ?
C68 C69 H69 119.0 . . ?
C70 C69 C68 122.1(14) . . ?
C70 C69 H69 119.0 . . ?
C69 C70 H70 117.4 . . ?
C69 C70 C71 125.2(15) . . ?
C71 C70 H70 117.4 . . ?
C70 C71 H71 122.2 . . ?
C70 C71 C72 115.5(16) . . ?
C72 C71 H71 122.2 . . ?
C71 C72 H72 119.7 . . ?
C71 C72 C73 120.7(15) . . ?
C73 C72 H72 119.7 . . ?
C68 C73 C72 121.6(14) . . ?
C68 C73 H73 119.2 . . ?
C72 C73 H73 119.2 . . ?
C75 C74 P3 118.9(9) . . ?
C79 C74 P3 122.3(10) . . ?
C79 C74 C75 116.7(11) . . ?
C74 C75 H75 120.3 . . ?
C76 C75 C74 119.3(12) . . ?
C76 C75 H75 120.3 . . ?
C75 C76 H76 120.3 . . ?
C75 C76 C77 119.5(15) . . ?
C77 C76 H76 120.3 . . ?
C76 C77 H77 119.8 . . ?
C78 C77 C76 120.3(13) . . ?
C78 C77 H77 119.8 . . ?
C77 C78 H78 118.8 . . ?
C77 C78 C79 122.4(13) . . ?
C79 C78 H78 118.8 . . ?
C74 C79 C78 120.2(14) . . ?
C74 C79 H79 119.9 . . ?
C78 C79 H79 119.9 . . ?
C81 C80 P3 124.1(12) . . ?
C81 C80 C85 120.2(12) . . ?
C85 C80 P3 115.6(11) . . ?
C80 C81 H81 118.6 . . ?
C80 C81 C82 122.7(15) . . ?
C82 C81 H81 118.6 . . ?
C81 C82 H82 122.6 . . ?
C83 C82 C81 114.8(15) . . ?
C83 C82 H82 122.6 . . ?
C82 C83 H83 118.0 . . ?
C82 C83 C84 124.1(14) . . ?
C84 C83 H83 118.0 . . ?
C83 C84 H84 121.5 . . ?
C85 C84 C83 117.0(16) . . ?
C85 C84 H84 121.5 . . ?
C80 C85 H85 119.4 . . ?
C84 C85 C80 121.1(15) . . ?
C84 C85 H85 119.4 . . ?
P3 C86 P4 113.3(6) . . ?
P3 C86 H86A 108.9 . . ?
P3 C86 H86B 108.9 . . ?
P4 C86 H86A 108.9 . . ?
P4 C86 H86B 108.9 . . ?
H86A C86 H86B 107.7 . . ?
C88 C87 P4 122.0(8) . . ?
C92 C87 P4 119.6(9) . . ?
C92 C87 C88 118.1(11) . . ?
C87 C88 H88 119.2 . . ?
C89 C88 C87 121.6(12) . . ?
C89 C88 H88 119.2 . . ?
C88 C89 H89 123.6 . . ?
C88 C89 C90 112.8(11) . . ?
C90 C89 H89 123.6 . . ?
C89 C90 H90 115.8 . . ?
C91 C90 C89 128.5(10) . . ?
C91 C90 H90 115.8 . . ?
C90 C91 H91 122.5 . . ?
C90 C91 C92 114.9(12) . . ?
C92 C91 H91 122.5 . . ?
C87 C92 H92 118.6 . . ?
C91 C92 C87 122.8(12) . . ?
C91 C92 H92 118.6 . . ?
C94 C93 P4 115.5(11) . . ?
C94 C93 C98 120.3(12) . . ?
C98 C93 P4 124.3(10) . . ?
C93 C94 H94 119.7 . . ?
C93 C94 C95 120.6(14) . . ?
C95 C94 H94 119.7 . . ?
C94 C95 H95 120.2 . . ?
C94 C95 C96 119.6(13) . . ?
C96 C95 H95 120.2 . . ?
C95 C96 H96 120.5 . . ?
C97 C96 C95 119.1(13) . . ?
C97 C96 H96 120.5 . . ?
C96 C97 H97 119.5 . . ?
C96 C97 C98 121.1(13) . . ?
C98 C97 H97 119.5 . . ?
C93 C98 H98 120.4 . . ?
C97 C98 C93 119.1(13) . . ?
C97 C98 H98 120.4 . . ?
C100 C99 P5 118.7(9) . . ?
C100 C99 C104 120.2(11) . . ?
C104 C99 P5 121.1(10) . . ?
C99 C100 H100 120.6 . . ?
C99 C100 C101 118.8(12) . . ?
C101 C100 H100 120.6 . . ?
C100 C101 H101 119.3 . . ?
C102 C101 C100 121.5(14) . . ?
C102 C101 H101 119.3 . . ?
C101 C102 H102 120.5 . . ?
C103 C102 C101 118.9(13) . . ?
C103 C102 H102 120.5 . . ?
C102 C103 H103 118.8 . . ?
C102 C103 C104 122.3(12) . . ?
C104 C103 H103 118.8 . . ?
C99 C104 H104 120.9 . . ?
C103 C104 C99 118.2(12) . . ?
C103 C104 H104 120.9 . . ?
C106 C105 P5 118.6(10) . . ?
C106 C105 C110 116.7(11) . . ?
C110 C105 P5 124.7(10) . . ?
C105 C106 H106 119.0 . . ?
C107 C106 C105 121.9(13) . . ?
C107 C106 H106 119.0 . . ?
C106 C107 H107 119.9 . . ?
C106 C107 C108 120.1(12) . . ?
C108 C107 H107 119.9 . . ?
C107 C108 H108 120.9 . . ?
C109 C108 C107 118.1(11) . . ?
C109 C108 H108 120.9 . . ?
C108 C109 H109 118.8 . . ?
C110 C109 C108 122.3(15) . . ?
C110 C109 H109 118.8 . . ?
C105 C110 H110 119.7 . . ?
C109 C110 C105 120.7(13) . . ?
C109 C110 H110 119.7 . . ?
P5 C111 P6 111.9(7) . . ?
P5 C111 H11A 109.2 . . ?
P5 C111 H11B 109.2 . . ?
P6 C111 H11A 109.2 . . ?
P6 C111 H11B 109.2 . . ?
H11A C111 H11B 107.9 . . ?
C113 C112 P6 119.6(9) . . ?
C113 C112 C117 117.9(12) . . ?
C117 C112 P6 122.4(10) . . ?
C112 C113 H113 119.8 . . ?
C112 C113 C114 120.3(11) . . ?
C114 C113 H113 119.8 . . ?
C113 C114 H114 119.9 . . ?
C115 C114 C113 120.1(13) . . ?
C115 C114 H114 119.9 . . ?
C114 C115 H115 120.7 . . ?
C114 C115 C116 118.7(12) . . ?
C116 C115 H115 120.7 . . ?
C115 C116 H116 120.8 . . ?
C117 C116 C115 118.3(11) . . ?
C117 C116 H116 120.8 . . ?
C112 C117 H117 117.8 . . ?
C116 C117 C112 124.5(13) . . ?
C116 C117 H117 117.8 . . ?
C119 C118 P6 117.6(11) . . ?
C119 C118 C123 119.0(13) . . ?
C123 C118 P6 123.3(10) . . ?
C118 C119 H119 119.3 . . ?
C118 C119 C120 121.5(14) . . ?
C120 C119 H119 119.3 . . ?
C119 C120 H120 120.7 . . ?
C121 C120 C119 118.5(13) . . ?
C121 C120 H120 120.7 . . ?
C120 C121 H121 120.1 . . ?
C120 C121 C122 119.9(14) . . ?
C122 C121 H121 120.1 . . ?
C121 C122 H122 119.6 . . ?
C123 C122 C121 120.8(15) . . ?
C123 C122 H122 119.6 . . ?
C118 C123 H123 120.1 . . ?
C122 C123 C118 119.8(13) . . ?
C122 C123 H123 120.1 . . ?
C125 C124 P7 117.6(9) . . ?
C125 C124 C129 120.1(11) . . ?
C129 C124 P7 121.7(11) . . ?
C124 C125 H125 118.3 . . ?
C124 C125 C126 123.4(13) . . ?
C126 C125 H125 118.3 . . ?
C125 C126 H126 122.0 . . ?
C127 C126 C125 116.0(14) . . ?
C127 C126 H126 122.0 . . ?
C126 C127 H127 117.6 . . ?
C128 C127 C126 124.7(12) . . ?
C128 C127 H127 117.6 . . ?
C127 C128 H128 121.5 . . ?
C127 C128 C129 117.0(13) . . ?
C129 C128 H128 121.5 . . ?
C124 C129 C128 118.7(13) . . ?
C124 C129 H129 120.7 . . ?
C128 C129 H129 120.7 . . ?
C131 C130 P7 121.1(9) . . ?
C131 C130 C135 119.3(11) . . ?
C135 C130 P7 119.5(8) . . ?
C130 C131 H131 119.4 . . ?
C130 C131 C132 121.2(11) . . ?
C132 C131 H131 119.4 . . ?
C131 C132 H132 120.4 . . ?
C133 C132 C131 119.2(12) . . ?
C133 C132 H132 120.4 . . ?
C132 C133 H133 120.1 . . ?
C132 C133 C134 119.8(12) . . ?
C134 C133 H133 120.1 . . ?
C133 C134 H134 120.9 . . ?
C135 C134 C133 118.2(11) . . ?
C135 C134 H134 120.9 . . ?
C130 C135 C134 121.9(11) . . ?
C130 C135 H135 119.0 . . ?
C134 C135 H135 119.0 . . ?
P7 C136 P8 115.1(6) . . ?
P7 C136 H13A 108.5 . . ?
P7 C136 H13B 108.5 . . ?
P8 C136 H13A 108.5 . . ?
P8 C136 H13B 108.5 . . ?
H13A C136 H13B 107.5 . . ?
C138 C137 P8 123.3(8) . . ?
C138 C137 C142 117.5(11) . . ?
C142 C137 P8 119.2(9) . . ?
C137 C138 H138 117.8 . . ?
C137 C138 C139 124.3(12) . . ?
C139 C138 H138 117.8 . . ?
C138 C139 H139 121.8 . . ?
C140 C139 C138 116.3(14) . . ?
C140 C139 H139 121.8 . . ?
C139 C140 H140 118.5 . . ?
C139 C140 C141 123.1(13) . . ?
C141 C140 H140 118.5 . . ?
C140 C141 H141 120.6 . . ?
C140 C141 C142 118.9(13) . . ?
C142 C141 H141 120.6 . . ?
C137 C142 H142 120.1 . . ?
C141 C142 C137 119.8(12) . . ?
C141 C142 H142 120.1 . . ?
C146 C145 H145 119.8 . . ?
C150 C145 H145 119.8 . . ?
C150 C145 C146 120.4(14) . . ?
C145 C146 H146 120.2 . . ?
C147 C146 C145 119.6(14) . . ?
C147 C146 H146 120.2 . . ?
C146 C147 H147 118.7 . . ?
C146 C147 C148 122.6(15) . . ?
C148 C147 H147 118.7 . . ?
C147 C148 H148 120.8 . . ?
C149 C148 C147 118.3(13) . . ?
C149 C148 H148 120.8 . . ?
C148 C149 P8 123.9(10) . . ?
C148 C149 C150 118.8(12) . . ?
C150 C149 P8 117.3(10) . . ?
C145 C150 C149 120.3(14) . . ?
C145 C150 H150 119.9 . . ?
C149 C150 H150 119.9 . . ?
Cl5 C144 H14A 108.4 . . ?
Cl5 C144 H14B 108.4 . . ?
Cl6 C144 Cl5 115.5(10) . . ?
Cl6 C144 H14A 108.4 . . ?
Cl6 C144 H14B 108.4 . . ?
H14A C144 H14B 107.5 . . ?
Cl3 C143 Cl4 111.4(9) . . ?
Cl3 C143 H14C 109.4 . . ?
Cl3 C143 H14D 109.4 . . ?
Cl4 C143 H14C 109.4 . . ?
Cl4 C143 H14D 109.4 . . ?
H14C C143 H14D 108.0 . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Ag1 S1 C1 C2 3.9(18) . . . . ?
Ag1 S1 C1 C6 -177.9(13) . . . . ?
S1 C1 C2 C3 -179.0(15) . . . . ?
S1 C1 C6 C5 -178.7(15) . . . . ?
S1 C1 C6 C7 -19(3) . . . . ?
P1 C49 C50 C51 173.4(12) . . . . ?
P1 C49 C54 C53 -176.3(13) . . . . ?
P1 C55 C56 C57 -179.2(10) . . . . ?
P1 C55 C60 C59 177.9(10) . . . . ?
C1 C2 C3 C4 5(3) . . . . ?
C1 C6 C7 C8 90(2) . . . . ?
Ag2 S1 C1 C2 89.9(16) . . . . ?
Ag2 S1 C1 C6 -91.9(15) . . . . ?
Ag2 P1 C49 C50 -87.5(14) . . . . ?
Ag2 P1 C49 C54 87.3(12) . . . . ?
Ag2 P1 C55 C56 -1.5(12) . . . . ?
Ag2 P1 C55 C60 -177.3(9) . . . . ?
Ag2 P1 C61 P2 -64.4(7) . . . . ?
Ag2 S2 C9 C10 -93.7(11) . . . . ?
Ag2 S2 C9 C14 87.5(10) . . . . ?
S2 C9 C10 C11 -174.0(10) . . . . ?
S2 C9 C14 C13 175.5(10) . . . . ?
S2 C9 C14 C15 -3.5(17) . . . . ?
P2 C62 C63 C64 -175.8(10) . . . . ?
P2 C62 C67 C66 178.9(9) . . . . ?
P2 C68 C69 C70 174.9(13) . . . . ?
P2 C68 C73 C72 -177.7(12) . . . . ?
C2 C1 C6 C5 -1(3) . . . . ?
C2 C1 C6 C7 158.6(19) . . . . ?
C2 C3 C4 C5 -13(3) . . . . ?
Ag3 S2 C9 C10 55.1(12) . . . . ?
Ag3 S2 C9 C14 -123.7(9) . . . . ?
Ag3 P3 C74 C75 -173.2(8) . . . . ?
Ag3 P3 C74 C79 23.8(12) . . . . ?
Ag3 P3 C80 C81 -150.2(11) . . . . ?
Ag3 P3 C80 C85 33.8(11) . . . . ?
Ag3 P3 C86 P4 -44.5(7) . . . . ?
Ag3 S6 C41 C42 -83.2(11) . . . . ?
Ag3 S6 C41 C46 97.0(11) . . . . ?
S3 C17 C18 C19 -178.8(13) . . . . ?
S3 C17 C22 C21 179.7(13) . . . . ?
S3 C17 C22 C23 -2(3) . . . . ?
P3 C74 C75 C76 -176.4(10) . . . . ?
P3 C74 C79 C78 173.7(10) . . . . ?
P3 C80 C81 C82 -177.8(10) . . . . ?
P3 C80 C85 C84 178.2(11) . . . . ?
C3 C4 C5 C6 18(4) . . . . ?
Ag4 S2 C9 C10 -21.3(12) . . . . ?
Ag4 S2 C9 C14 159.9(9) . . . . ?
S4 C25 C26 C27 -179.5(9) . . . . ?
S4 C25 C30 C29 -179.3(9) . . . . ?
S4 C25 C30 C31 -4.0(16) . . . . ?
P4 C87 C88 C89 -178.0(10) . . . . ?
P4 C87 C92 C91 177.9(10) . . . . ?
P4 C93 C94 C95 179.0(11) . . . . ?
P4 C93 C98 C97 178.0(10) . . . . ?
C4 C5 C6 C1 -11(4) . . . . ?
C4 C5 C6 C7 -168(2) . . . . ?
Ag5 S6 C41 C42 -6.0(12) . . . . ?
Ag5 S6 C41 C46 174.2(10) . . . . ?
S5 C33 C34 C35 -177.1(11) . . . . ?
S5 C33 C38 C37 177.3(10) . . . . ?
S5 C33 C38 C39 -3.0(17) . . . . ?
P5 C99 C100 C101 -179.6(9) . . . . ?
P5 C99 C104 C103 -178.8(9) . . . . ?
P5 C105 C106 C107 179.1(10) . . . . ?
P5 C105 C110 C109 178.7(11) . . . . ?
C5 C6 C7 C8 -115(3) . . . . ?
Ag6 P4 C87 C88 -179.5(9) . . . . ?
Ag6 P4 C87 C92 7.0(11) . . . . ?
Ag6 P4 C93 C94 46.8(11) . . . . ?
Ag6 P4 C93 C98 -134.7(11) . . . . ?
S6 C41 C42 C43 178.9(11) . . . . ?
S6 C41 C46 C45 179.2(10) . . . . ?
S6 C41 C46 C47 2.6(19) . . . . ?
P6 C112 C113 C114 174.5(9) . . . . ?
P6 C112 C117 C116 -177.1(10) . . . . ?
P6 C118 C119 C120 -177.9(10) . . . . ?
P6 C118 C123 C122 172.9(11) . . . . ?
C6 C1 C2 C3 3(3) . . . . ?
P7 C124 C125 C126 174.8(10) . . . . ?
P7 C124 C129 C128 -174.4(9) . . . . ?
P7 C130 C131 C132 178.8(11) . . . . ?
P7 C130 C135 C134 -176.6(11) . . . . ?
Ag8 P2 C61 P1 38.4(8) . . . . ?
Ag8 P2 C62 C63 -9.8(11) . . . . ?
Ag8 P2 C62 C67 169.5(8) . . . . ?
Ag8 P2 C68 C69 -24.4(13) . . . . ?
Ag8 P2 C68 C73 149.9(12) . . . . ?
P8 C137 C138 C139 178.6(12) . . . . ?
P8 C137 C142 C141 -178.2(11) . . . . ?
P8 C149 C150 C145 -179.4(10) . . . . ?
Ag9 P5 C99 C100 -11.3(10) . . . . ?
Ag9 P5 C99 C104 167.0(8) . . . . ?
Ag9 P5 C105 C106 -37.3(12) . . . . ?
Ag9 P5 C105 C110 144.7(11) . . . . ?
Ag9 P5 C111 P6 40.5(7) . . . . ?
C9 C10 C11 C12 -3.1(19) . . . . ?
C9 C14 C15 C16 -172.8(15) . . . . ?
Ag10 S3 C17 C18 10.7(15) . . . . ?
Ag10 S3 C17 C22 -169.1(14) . . . . ?
C10 C9 C14 C13 -3.3(18) . . . . ?
C10 C9 C14 C15 177.7(13) . . . . ?
C10 C11 C12 C13 0.4(19) . . . . ?
Ag11 S5 C33 C34 -5.8(11) . . . . ?
Ag11 S5 C33 C38 177.9(9) . . . . ?
C11 C12 C13 C14 1(2) . . . . ?
Ag12 P8 C136 P7 61.3(7) . . . . ?
Ag12 P8 C137 C138 -168.8(10) . . . . ?
Ag12 P8 C137 C142 12.2(13) . . . . ?
Ag12 P8 C149 C148 -119.8(9) . . . . ?
Ag12 P8 C149 C150 56.8(9) . . . . ?
C12 C13 C14 C9 1(2) . . . . ?
C12 C13 C14 C15 179.7(14) . . . . ?
Ag13 S4 C25 C26 -17.9(11) . . . . ?
Ag13 S4 C25 C30 162.1(9) . . . . ?
C13 C14 C15 C16 8(2) . . . . ?
Ag14 S3 C17 C18 95.4(13) . . . . ?
Ag14 S3 C17 C22 -84.4(16) . . . . ?
Ag14 S4 C25 C26 -90.9(10) . . . . ?
Ag14 S4 C25 C30 89.1(10) . . . . ?
Ag14 P6 C111 P5 -63.8(7) . . . . ?
Ag14 P6 C112 C113 3.2(11) . . . . ?
Ag14 P6 C112 C117 -179.1(8) . . . . ?
Ag14 P6 C118 C119 70.6(11) . . . . ?
Ag14 P6 C118 C123 -107.3(11) . . . . ?
C14 C9 C10 C11 5(2) . . . . ?
Ag15 S4 C25 C26 55.3(10) . . . . ?
Ag15 S4 C25 C30 -124.7(9) . . . . ?
Ag15 S5 C33 C34 -83.4(11) . . . . ?
Ag15 S5 C33 C38 100.2(10) . . . . ?
Ag15 P7 C124 C125 43.7(11) . . . . ?
Ag15 P7 C124 C129 -145.1(9) . . . . ?
Ag15 P7 C130 C131 -165.2(10) . . . . ?
Ag15 P7 C130 C135 16.0(12) . . . . ?
Ag15 P7 C136 P8 -43.2(7) . . . . ?
C17 C18 C19 C20 3(3) . . . . ?
C17 C22 C23 C24 -168.6(18) . . . . ?
C18 C17 C22 C21 0(3) . . . . ?
C18 C17 C22 C23 178.0(18) . . . . ?
C18 C19 C20 C21 -9(3) . . . . ?
C19 C20 C21 C22 10(3) . . . . ?
C20 C21 C22 C17 -6(3) . . . . ?
C20 C21 C22 C23 176(2) . . . . ?
C21 C22 C23 C24 9(3) . . . . ?
C22 C17 C18 C19 1(3) . . . . ?
C25 C26 C27 C28 1.5(19) . . . . ?
C25 C30 C31 C32 -166.6(12) . . . . ?
C26 C25 C30 C29 0.7(18) . . . . ?
C26 C25 C30 C31 176.0(11) . . . . ?
C26 C27 C28 C29 -5(2) . . . . ?
C27 C28 C29 C30 6(2) . . . . ?
C28 C29 C30 C25 -4.2(19) . . . . ?
C28 C29 C30 C31 -179.3(12) . . . . ?
C29 C30 C31 C32 8.6(18) . . . . ?
C30 C25 C26 C27 0.5(18) . . . . ?
C33 C34 C35 C36 -1(2) . . . . ?
C33 C38 C39 C40 -173.8(12) . . . . ?
C34 C33 C38 C37 0.9(19) . . . . ?
C34 C33 C38 C39 -179.5(12) . . . . ?
C34 C35 C36 C37 2(2) . . . . ?
C35 C36 C37 C38 -2(2) . . . . ?
C36 C37 C38 C33 1(2) . . . . ?
C36 C37 C38 C39 -179.2(13) . . . . ?
C37 C38 C39 C40 5.9(19) . . . . ?
C38 C33 C34 C35 -1(2) . . . . ?
C41 C42 C43 C44 3(2) . . . . ?
C41 C46 C47 C48 -88.3(17) . . . . ?
C42 C41 C46 C45 -0.6(19) . . . . ?
C42 C41 C46 C47 -177.2(13) . . . . ?
C42 C43 C44 C45 -2(2) . . . . ?
C43 C44 C45 C46 0(2) . . . . ?
C44 C45 C46 C41 1(2) . . . . ?
C44 C45 C46 C47 178.1(15) . . . . ?
C45 C46 C47 C48 95.3(16) . . . . ?
C46 C41 C42 C43 -1.3(19) . . . . ?
C49 P1 C55 C56 125.0(10) . . . . ?
C49 P1 C55 C60 -50.8(12) . . . . ?
C49 P1 C61 P2 176.1(6) . . . . ?
C49 C50 C51 C52 4(3) . . . . ?
C50 C49 C54 C53 -1(2) . . . . ?
C50 C51 C52 C53 -3(3) . . . . ?
C51 C52 C53 C54 1(3) . . . . ?
C52 C53 C54 C49 2(3) . . . . ?
C54 C49 C50 C51 -2(2) . . . . ?
C55 P1 C49 C50 139.4(14) . . . . ?
C55 P1 C49 C54 -45.7(13) . . . . ?
C55 P1 C61 P2 67.6(7) . . . . ?
C55 C56 C57 C58 1.2(19) . . . . ?
C56 C55 C60 C59 2.1(19) . . . . ?
C56 C57 C58 C59 2(2) . . . . ?
C57 C58 C59 C60 -3(2) . . . . ?
C58 C59 C60 C55 1(2) . . . . ?
C60 C55 C56 C57 -3.3(19) . . . . ?
C61 P1 C49 C50 31.7(14) . . . . ?
C61 P1 C49 C54 -153.5(12) . . . . ?
C61 P1 C55 C56 -126.4(10) . . . . ?
C61 P1 C55 C60 57.8(11) . . . . ?
C61 P2 C62 C63 119.5(10) . . . . ?
C61 P2 C62 C67 -61.2(11) . . . . ?
C61 P2 C68 C69 -151.6(11) . . . . ?
C61 P2 C68 C73 22.7(14) . . . . ?
C62 P2 C61 P1 -89.2(7) . . . . ?
C62 P2 C68 C69 100.2(11) . . . . ?
C62 P2 C68 C73 -85.4(13) . . . . ?
C62 C63 C64 C65 -4.1(19) . . . . ?
C63 C62 C67 C66 -1.9(19) . . . . ?
C63 C64 C65 C66 0.5(19) . . . . ?
C64 C65 C66 C67 2(2) . . . . ?
C65 C66 C67 C62 -1.8(19) . . . . ?
C67 C62 C63 C64 4.9(19) . . . . ?
C68 P2 C61 P1 162.1(6) . . . . ?
C68 P2 C62 C63 -132.8(10) . . . . ?
C68 P2 C62 C67 46.5(11) . . . . ?
C68 C69 C70 C71 3(3) . . . . ?
C69 C68 C73 C72 -3(2) . . . . ?
C69 C70 C71 C72 -3(3) . . . . ?
C70 C71 C72 C73 0(2) . . . . ?
C71 C72 C73 C68 3(3) . . . . ?
C73 C68 C69 C70 0(2) . . . . ?
C74 P3 C80 C81 82.8(13) . . . . ?
C74 P3 C80 C85 -93.2(11) . . . . ?
C74 P3 C86 P4 87.4(7) . . . . ?
C74 C75 C76 C77 12(2) . . . . ?
C75 C74 C79 C78 10.4(18) . . . . ?
C75 C76 C77 C78 -9(2) . . . . ?
C76 C77 C78 C79 7(2) . . . . ?
C77 C78 C79 C74 -8(2) . . . . ?
C79 C74 C75 C76 -12.5(18) . . . . ?
C80 P3 C74 C75 -49.9(11) . . . . ?
C80 P3 C74 C79 147.1(11) . . . . ?
C80 P3 C86 P4 -165.3(7) . . . . ?
C80 C81 C82 C83 2(2) . . . . ?
C81 C80 C85 C84 2(2) . . . . ?
C81 C82 C83 C84 -1(2) . . . . ?
C82 C83 C84 C85 1(2) . . . . ?
C83 C84 C85 C80 -2(2) . . . . ?
C85 C80 C81 C82 -2(2) . . . . ?
C86 P3 C74 C75 57.0(10) . . . . ?
C86 P3 C74 C79 -106.0(11) . . . . ?
C86 P3 C80 C81 -28.0(14) . . . . ?
C86 P3 C80 C85 156.1(10) . . . . ?
C86 P4 C87 C88 -49.8(11) . . . . ?
C86 P4 C87 C92 136.8(10) . . . . ?
C86 P4 C93 C94 -79.4(11) . . . . ?
C86 P4 C93 C98 99.1(12) . . . . ?
C87 P4 C93 C94 173.3(10) . . . . ?
C87 P4 C93 C98 -8.2(13) . . . . ?
C87 C88 C89 C90 7.8(18) . . . . ?
C88 C87 C92 C91 4.2(18) . . . . ?
C88 C89 C90 C91 -13(2) . . . . ?
C89 C90 C91 C92 13(2) . . . . ?
C90 C91 C92 C87 -7.8(18) . . . . ?
C92 C87 C88 C89 -4.4(18) . . . . ?
C93 P4 C87 C88 54.6(11) . . . . ?
C93 P4 C87 C92 -118.8(10) . . . . ?
C93 C94 C95 C96 0(2) . . . . ?
C94 C93 C98 C97 -4(2) . . . . ?
C94 C95 C96 C97 4(2) . . . . ?
C95 C96 C97 C98 -7(2) . . . . ?
C96 C97 C98 C93 7(2) . . . . ?
C98 C93 C94 C95 0(2) . . . . ?
C99 P5 C105 C106 85.6(11) . . . . ?
C99 P5 C105 C110 -92.4(13) . . . . ?
C99 P5 C111 P6 -86.4(7) . . . . ?
C99 C100 C101 C102 -0.7(19) . . . . ?
C100 C99 C104 C103 -0.5(17) . . . . ?
C100 C101 C102 C103 -2(2) . . . . ?
C101 C102 C103 C104 4(2) . . . . ?
C102 C103 C104 C99 -2.5(19) . . . . ?
C104 C99 C100 C101 2.0(17) . . . . ?
C105 P5 C99 C100 -135.5(10) . . . . ?
C105 P5 C99 C104 42.8(11) . . . . ?
C105 P5 C111 P6 166.2(6) . . . . ?
C105 C106 C107 C108 2(2) . . . . ?
C106 C105 C110 C109 1(2) . . . . ?
C106 C107 C108 C109 0(2) . . . . ?
C107 C108 C109 C110 -2(2) . . . . ?
C108 C109 C110 C105 2(2) . . . . ?
C110 C105 C106 C107 -3(2) . . . . ?
C111 P5 C99 C100 117.9(10) . . . . ?
C111 P5 C99 C104 -63.8(10) . . . . ?
C111 P5 C105 C106 -164.4(10) . . . . ?
C111 P5 C105 C110 17.6(13) . . . . ?
C111 P6 C112 C113 -123.4(10) . . . . ?
C111 P6 C112 C117 54.4(11) . . . . ?
C111 P6 C118 C119 -168.4(10) . . . . ?
C111 P6 C118 C123 13.7(13) . . . . ?
C112 P6 C111 P5 67.9(7) . . . . ?
C112 P6 C118 C119 -58.5(11) . . . . ?
C112 P6 C118 C123 123.6(12) . . . . ?
C112 C113 C114 C115 4.2(19) . . . . ?
C113 C112 C117 C116 0.7(19) . . . . ?
C113 C114 C115 C116 -2.3(19) . . . . ?
C114 C115 C116 C117 -0.4(19) . . . . ?
C115 C116 C117 C112 1(2) . . . . ?
C117 C112 C113 C114 -3.4(18) . . . . ?
C118 P6 C111 P5 176.2(6) . . . . ?
C118 P6 C112 C113 125.6(10) . . . . ?
C118 P6 C112 C117 -56.6(11) . . . . ?
C118 C119 C120 C121 5(2) . . . . ?
C119 C118 C123 C122 -5(2) . . . . ?
C119 C120 C121 C122 -5(2) . . . . ?
C120 C121 C122 C123 0(2) . . . . ?
C121 C122 C123 C118 5(2) . . . . ?
C123 C118 C119 C120 0(2) . . . . ?
C124 P7 C130 C131 -40.5(13) . . . . ?
C124 P7 C130 C135 140.6(11) . . . . ?
C124 P7 C136 P8 -169.3(6) . . . . ?
C124 C125 C126 C127 -3(2) . . . . ?
C125 C124 C129 C128 -3.5(19) . . . . ?
C125 C126 C127 C128 2(2) . . . . ?
C126 C127 C128 C129 -2(2) . . . . ?
C127 C128 C129 C124 2.9(19) . . . . ?
C129 C124 C125 C126 3(2) . . . . ?
C130 P7 C124 C125 -80.5(11) . . . . ?
C130 P7 C124 C129 90.7(11) . . . . ?
C130 P7 C136 P8 83.9(7) . . . . ?
C130 C131 C132 C133 -3(2) . . . . ?
C131 C130 C135 C134 4(2) . . . . ?
C131 C132 C133 C134 6(2) . . . . ?
C132 C133 C134 C135 -4(2) . . . . ?
C133 C134 C135 C130 -2(2) . . . . ?
C135 C130 C131 C132 -2(2) . . . . ?
C136 P7 C124 C125 169.4(10) . . . . ?
C136 P7 C124 C129 -19.4(12) . . . . ?
C136 P7 C130 C131 67.6(12) . . . . ?
C136 P7 C130 C135 -111.2(11) . . . . ?
C136 P8 C137 C138 -38.5(13) . . . . ?
C136 P8 C137 C142 142.6(11) . . . . ?
C136 P8 C149 C148 118.9(10) . . . . ?
C136 P8 C149 C150 -64.5(9) . . . . ?
C137 P8 C136 P7 -71.1(8) . . . . ?
C137 P8 C149 C148 9.4(10) . . . . ?
C137 P8 C149 C150 -174.0(8) . . . . ?
C137 C138 C139 C140 1(2) . . . . ?
C138 C137 C142 C141 3(2) . . . . ?
C138 C139 C140 C141 0(2) . . . . ?
C139 C140 C141 C142 0(2) . . . . ?
C140 C141 C142 C137 -2(2) . . . . ?
C142 C137 C138 C139 -2(2) . . . . ?
C145 C146 C147 C148 2.6(19) . . . . ?
C146 C145 C150 C149 2.6(19) . . . . ?
C146 C147 C148 C149 -2.7(18) . . . . ?
C147 C148 C149 P8 179.2(8) . . . . ?
C147 C148 C149 C150 2.5(16) . . . . ?
C148 C149 C150 C145 -2.6(17) . . . . ?
C149 P8 C136 P7 -180.0(7) . . . . ?
C149 P8 C137 C138 66.3(12) . . . . ?
C149 P8 C137 C142 -112.6(11) . . . . ?
C150 C145 C146 C147 -2.6(19) . . . . ?

_smtbx_masks_special_details     ?
loop_
_smtbx_masks_void_nr
_smtbx_masks_void_average_x
_smtbx_masks_void_average_y
_smtbx_masks_void_average_z
_smtbx_masks_void_volume
_smtbx_masks_void_count_electrons
_smtbx_masks_void_content
1 0.000 -0.292 0.000 1991.3 290.0 ?
2 0.207 0.351 0.589 16.7 1.2 ?
3 0.793 0.649 0.411 16.7 1.2 ?

_smtbx_masks_void_probe_radius   1.2
_smtbx_masks_void_truncation_radius 1.2
_olex2_submission_special_instructions 'No special instructions were received'
