# Electronic Supplementary Material (ESI) for Journal of Materials Chemistry C.
# This journal is © The Royal Society of Chemistry 2024

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_Dy
_database_code_depnum_ccdc_archive 'CCDC 2325208'
loop_
_audit_author_name
_audit_author_address
'Xiaotong Wang'
;Nankai university
China
;
_audit_update_record             
;
2024-05-05 deposited with the CCDC.	2024-05-10 downloaded from the CCDC.
;
_audit_creation_date             2024-01-02
_audit_creation_method           
;
Olex2 1.5
(compiled 2023.08.24 svn.re1ec1418 for OlexSys, GUI svn.r6817)
;
_shelx_SHELXL_version_number     2014/7
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         'C30 H24 Dy F18 N2 O9'
_chemical_formula_sum            'C30 H24 Dy F18 N2 O9'
_chemical_formula_weight         1061.01
_chemical_absolute_configuration ?
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0030 0.0020 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Dy Dy -0.1890 4.4100 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0170 0.0100 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0060 0.0030 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0110 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           4
_space_group_name_H-M_alt        'P 21'
_space_group_name_Hall           'P 2yb'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y+1/2, -z'

_cell_length_a                   22.297(2)
_cell_length_b                   16.6711(16)
_cell_length_c                   23.000(2)
_cell_angle_alpha                90
_cell_angle_beta                 116.697(2)
_cell_angle_gamma                90
_cell_volume                     7638.0(12)
_cell_formula_units_Z            8
_cell_measurement_reflns_used    24132
_cell_measurement_temperature    113
_cell_measurement_theta_max      27.5
_cell_measurement_theta_min      3.0
_shelx_estimated_absorpt_T_max   0.679
_shelx_estimated_absorpt_T_min   0.420
_exptl_absorpt_coefficient_mu    2.097
_exptl_absorpt_correction_type   Multi-scan
_exptl_absorpt_correction_T_max  1.000
_exptl_absorpt_correction_T_min  0.846
_exptl_absorpt_process_details   sadabs
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            red
_exptl_crystal_density_diffrn    1.845
_exptl_crystal_density_meas      .
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             4144
_exptl_crystal_size_max          0.5
_exptl_crystal_size_mid          0.3
_exptl_crystal_size_min          0.2
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0249
_diffrn_reflns_av_unetI/netI     0.0300
_diffrn_reflns_Laue_measured_fraction_full 0.997
_diffrn_reflns_Laue_measured_fraction_max 0.996
_diffrn_reflns_limit_h_max       28
_diffrn_reflns_limit_h_min       -28
_diffrn_reflns_limit_k_max       21
_diffrn_reflns_limit_k_min       -21
_diffrn_reflns_limit_l_max       29
_diffrn_reflns_limit_l_min       -29
_diffrn_reflns_number            98872
_diffrn_reflns_point_group_measured_fraction_full 0.998
_diffrn_reflns_point_group_measured_fraction_max 0.996
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         27.542
_diffrn_reflns_theta_min         3.009
_diffrn_ambient_temperature      113
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 0.997
_diffrn_measured_fraction_theta_max 0.996
_diffrn_measurement_device_type  'Rigaku Pilatus 200K'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   ?
_diffrn_source_current           24.0
_diffrn_source_power             1.2
_diffrn_source_voltage           50.0
_reflns_Friedel_coverage         0.934
_reflns_Friedel_fraction_full    0.998
_reflns_Friedel_fraction_max     0.996
_reflns_number_gt                32997
_reflns_number_total             34384
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       'CrystalClear (Rigaku Inc., 2008)'
_computing_data_collection       'CrystalClear (Rigaku Inc., 2008)'
_computing_data_reduction        'CrystalClear (Rigaku Inc., 2008)'
_computing_molecular_graphics    'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_structure_refinement  'XL  (Sheldrick, 2008)'
_computing_structure_solution    'XL  (Sheldrick, 2008)'
_refine_diff_density_max         5.989
_refine_diff_density_min         -1.553
_refine_diff_density_rms         0.139
_refine_ls_abs_structure_details 
;
 Refined as an inversion twin.
;
_refine_ls_abs_structure_Flack   0.305(7)
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.047
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     2182
_refine_ls_number_reflns         34384
_refine_ls_number_restraints     73
_refine_ls_R_factor_all          0.0408
_refine_ls_R_factor_gt           0.0385
_refine_ls_restrained_S_all      1.065
_refine_ls_shift/su_max          0.005
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0610P)²+13.1362P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0964
_refine_ls_wR_factor_ref         0.0979
_refine_special_details          
;
 Refined as a 2-component inversion twin.
;
_olex2_refinement_description    
;
1. Twinned data refinement
 Scales: 0.695(7)
 0.305(7)
2. Fixed Uiso
 At 1.2 times of:
  All C(H) groups, All C(H,H) groups
 At 1.5 times of:
  All C(H,H,H) groups
3. Uiso/Uaniso restraints and constraints
Uanis(C25) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.01
Uanis(F52) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.01
Uanis(C29) \\sim Ueq, Uanis(C26) \\sim Ueq: with sigma of 0.01 and sigma for
terminal atoms of 0.01
Uanis(C28) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.01
Uanis(F2) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.01
Uanis(F6) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.01
Uanis(F22) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.01
Uanis(F34) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.01
Uanis(F36) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(F40) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(F24) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02
4.a Secondary CH2 refined with riding coordinates:
 C17(H17A,H17B), C47(H47A,H47B), C77(H77A,H77B), C107(H10D,H10E)
4.b Aromatic/amide H refined with riding coordinates:
 C20(H20), C13(H13), C8(H8), C3(H3), C19(H19), C21(H21), C22(H22), C43(H43),
 C51(H51), C33(H33), C38(H38), C49(H49), C50(H50), C52(H52), C82(H82), C80(H80),
  C81(H81), C73(H73), C79(H79), C63(H63), C68(H68), C109(H109), C93(H93),
 C103(H103), C98(H98), C112(H112), C110(H110), C111(H111)
4.c Idealised Me refined as rotating group:
 C16(H16A,H16B,H16C), C26(H26A,H26B,H26C), C25(H25A,H25B,H25C), C58(H58A,H58B,
 H58C), C60(H60A,H60B,H60C), C46(H46A,H46B,H46C), C55(H55A,H55B,H55C), C57(H57A,
 H57B,H57C), C90(H90A,H90B,H90C), C88(H88A,H88B,H88C), C76(H76A,H76B,H76C),
 C87(H87A,H87B,H87C), C85(H85A,H85B,H85C), C117(H11A,H11B,H11C), C115(H11D,H11E,
 H11F), C120(H12A,H12B,H12C), C106(H10A,H10B,H10C), C118(H11G,H11H,H11I),
 C28(H28A,H28B,H28C), C30(H30A,H30B,H30C)
;
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Dy1 Dy 0.00166(2) 0.25937(2) -0.48948(2) 0.02502(8) Uani 1 1 d . . . . .
F1 F -0.1001(5) 0.1319(6) -0.7477(3) 0.086(3) Uani 1 1 d . . . . .
F2 F -0.0172(6) 0.2077(5) -0.7152(5) 0.091(3) Uani 1 1 d . U . . .
F3 F -0.0055(3) 0.0916(4) -0.6738(3) 0.0467(14) Uani 1 1 d . . . . .
F4 F -0.2598(3) 0.1944(4) -0.6720(4) 0.067(2) Uani 1 1 d . . . . .
F5 F -0.2475(3) 0.3181(4) -0.6731(4) 0.0628(19) Uani 1 1 d . . . . .
F6 F -0.2341(3) 0.2606(7) -0.5862(3) 0.079(2) Uani 1 1 d . U . . .
F7 F 0.2189(3) 0.1832(5) -0.4782(3) 0.0596(18) Uani 1 1 d . . . . .
F8 F 0.2569(3) 0.2709(5) -0.4030(4) 0.0624(18) Uani 1 1 d . . . . .
F9 F 0.2723(3) 0.1453(4) -0.3779(3) 0.0569(17) Uani 1 1 d . . . . .
F10 F 0.1698(4) 0.1231(5) -0.2396(3) 0.0651(19) Uani 1 1 d . . . . .
F11 F 0.1259(4) 0.2401(4) -0.2444(3) 0.070(2) Uani 1 1 d . . . . .
F12 F 0.0638(4) 0.1350(5) -0.2733(3) 0.067(2) Uani 1 1 d . . . . .
F13 F 0.1781(3) 0.3981(4) -0.3135(3) 0.0545(16) Uani 1 1 d . . . . .
F14 F 0.1215(3) 0.5070(3) -0.3453(3) 0.0457(14) Uani 1 1 d . . . . .
F15 F 0.1264(3) 0.4452(5) -0.2616(3) 0.065(2) Uani 1 1 d . . . . .
F16 F -0.1680(2) 0.3485(4) -0.4226(2) 0.0461(14) Uani 1 1 d . . . . .
F17 F -0.1051(2) 0.3979(4) -0.3290(2) 0.0410(12) Uani 1 1 d . . . . .
F18 F -0.1122(3) 0.2700(4) -0.3423(3) 0.0492(15) Uani 1 1 d . . . . .
O7 O -0.0893(3) 0.4733(5) -0.6399(3) 0.0435(16) Uani 1 1 d . . . . .
O9 O -0.0506(3) 0.1347(3) -0.5020(3) 0.0383(14) Uani 1 1 d . . . . .
O1 O -0.0122(3) 0.2078(3) -0.5909(3) 0.0342(14) Uani 1 1 d . . . . .
O8 O 0.0198(3) 0.3646(4) -0.5498(3) 0.0361(14) Uani 1 1 d . . . . .
O5 O 0.0623(3) 0.3599(4) -0.4156(3) 0.0284(12) Uani 1 1 d . . . . .
O6 O -0.0624(3) 0.2996(3) -0.4377(3) 0.0269(11) Uani 1 1 d . . . . .
O3 O 0.1108(3) 0.2224(4) -0.4642(3) 0.0352(13) Uani 1 1 d . . . . .
O4 O 0.0487(3) 0.1976(4) -0.3850(4) 0.0373(15) Uani 1 1 d . . . . .
N1 N 0.0440(3) 0.4366(4) -0.5400(3) 0.0257(14) Uani 1 1 d . . . . .
N2 N -0.0572(3) 0.0639(4) -0.4819(3) 0.0260(14) Uani 1 1 d . . . . .
C7 C 0.1614(4) 0.2001(5) -0.4137(5) 0.036(2) Uani 1 1 d . . . . .
C20 C -0.1770(5) 0.4959(7) -0.5399(6) 0.053(3) Uani 1 1 d . . . . .
H20 H -0.2197 0.4929 -0.5423 0.064 Uiso 1 1 calc R U . . .
C1 C -0.0447(7) 0.1547(7) -0.6946(5) 0.052(3) Uani 1 1 d . . . . .
C2 C -0.0624(6) 0.1915(5) -0.6422(5) 0.036(2) Uani 1 1 d . . . . .
C5 C -0.2234(4) 0.2540(6) -0.6364(4) 0.0317(17) Uani 1 1 d . . . . .
C11 C 0.1220(4) 0.4330(6) -0.3196(4) 0.0356(19) Uani 1 1 d . . . . .
C12 C 0.0600(4) 0.3867(5) -0.3656(4) 0.0277(16) Uani 1 1 d . . . . .
C13 C 0.0077(4) 0.3806(5) -0.3494(4) 0.0255(15) Uani 1 1 d . . . . .
H13 H 0.0115 0.4053 -0.3116 0.031 Uiso 1 1 calc R U . . .
C14 C -0.0509(4) 0.3385(5) -0.3882(4) 0.0243(15) Uani 1 1 d . . . . .
C15 C -0.1095(4) 0.3394(5) -0.3699(4) 0.0303(17) Uani 1 1 d . . . . .
C6 C 0.2287(5) 0.1988(7) -0.4178(5) 0.044(2) Uani 1 1 d . . . . .
C4 C -0.1473(4) 0.2458(5) -0.6163(4) 0.0278(17) Uani 1 1 d . . . . .
C8 C 0.1648(5) 0.1808(6) -0.3541(5) 0.038(2) Uani 1 1 d . . . . .
H8 H 0.2057 0.1661 -0.3199 0.046 Uiso 1 1 calc R U . . .
C9 C 0.1068(5) 0.1830(6) -0.3445(5) 0.037(2) Uani 1 1 d . . . . .
C10 C 0.1161(5) 0.1686(7) -0.2744(5) 0.046(2) Uani 1 1 d . . . . .
C16 C -0.1007(7) 0.4151(9) -0.7390(6) 0.066(3) Uani 1 1 d . . . . .
H16A H -0.1319 0.3955 -0.7811 0.098 Uiso 1 1 calc R U . . .
H16B H -0.0680 0.3744 -0.7165 0.098 Uiso 1 1 calc R U . . .
H16C H -0.0785 0.4620 -0.7441 0.098 Uiso 1 1 calc R U . . .
C17 C -0.1382(6) 0.4365(7) -0.6999(5) 0.051(3) Uani 1 1 d . . . . .
H17A H -0.1745 0.4736 -0.7240 0.061 Uiso 1 1 calc R U . . .
H17B H -0.1571 0.3887 -0.6904 0.061 Uiso 1 1 calc R U . . .
C3 C -0.1291(5) 0.2010(5) -0.6569(4) 0.0346(19) Uani 1 1 d . . . . .
H3 H -0.1621 0.1774 -0.6942 0.041 Uiso 1 1 calc R U . . .
C19 C -0.1688(5) 0.4800(6) -0.5944(6) 0.047(2) Uani 1 1 d . . . . .
H19 H -0.2057 0.4673 -0.6335 0.057 Uiso 1 1 calc R U . . .
C21 C -0.1232(6) 0.5164(7) -0.4813(6) 0.052(3) Uani 1 1 d . . . . .
H21 H -0.1302 0.5276 -0.4452 0.062 Uiso 1 1 calc R U . . .
C22 C -0.0594(5) 0.5203(7) -0.4763(4) 0.038(2) Uani 1 1 d . . . . .
H22 H -0.0233 0.5352 -0.4373 0.046 Uiso 1 1 calc R U . . .
C18 C -0.1043(5) 0.4830(6) -0.5905(5) 0.039(2) Uani 1 1 d . . . . .
C26 C 0.0763(9) 0.4650(13) -0.6237(8) 0.105(6) Uani 1 1 d . U . . .
H26A H 0.0375 0.4313 -0.6441 0.157 Uiso 1 1 calc R U . . .
H26B H 0.1091 0.4493 -0.6378 0.157 Uiso 1 1 calc R U . . .
H26C H 0.0637 0.5199 -0.6356 0.157 Uiso 1 1 calc R U . . .
C25 C 0.1518(10) 0.3947(11) -0.5323(12) 0.121(6) Uani 1 1 d . U . . .
H25A H 0.1670 0.3779 -0.4880 0.181 Uiso 1 1 calc R U . . .
H25B H 0.1894 0.4121 -0.5387 0.181 Uiso 1 1 calc R U . . .
H25C H 0.1301 0.3506 -0.5609 0.181 Uiso 1 1 calc R U . . .
C27 C 0.1079(5) 0.4558(6) -0.5455(6) 0.047(3) Uani 1 1 d . . . . .
C23 C -0.0496(4) 0.5018(5) -0.5300(4) 0.0265(15) Uani 1 1 d . . . . .
C24 C 0.0173(4) 0.5012(5) -0.5274(4) 0.0295(17) Uani 1 1 d . . . . .
Dy2 Dy -0.48339(2) 0.02489(2) 0.50024(2) 0.01403(7) Uani 1 1 d . . . . .
F19 F -0.4087(3) -0.0625(4) 0.7652(2) 0.0429(14) Uani 1 1 d . . . . .
F20 F -0.4859(3) -0.1303(3) 0.6914(3) 0.0434(14) Uani 1 1 d . . . . .
F21 F -0.5028(3) -0.0064(4) 0.7052(3) 0.0454(14) Uani 1 1 d . . . . .
F22 F -0.2286(3) -0.0220(6) 0.7175(3) 0.081(3) Uani 1 1 d . U . . .
F23 F -0.2372(3) 0.0471(4) 0.6386(4) 0.067(2) Uani 1 1 d . . . . .
F24 F -0.2504(3) -0.0779(6) 0.6301(5) 0.107(4) Uani 1 1 d . U . . .
F25 F -0.7088(3) -0.0157(4) 0.4822(3) 0.0464(14) Uani 1 1 d . . . . .
F26 F -0.7274(3) 0.0834(3) 0.4161(3) 0.0466(14) Uani 1 1 d . . . . .
F27 F -0.7639(2) -0.0344(4) 0.3792(3) 0.0454(14) Uani 1 1 d . . . . .
F28 F -0.6095(3) 0.2724(3) 0.3551(3) 0.0383(12) Uani 1 1 d . . . . .
F29 F -0.6667(2) 0.1639(4) 0.3250(3) 0.0427(13) Uani 1 1 d . . . . .
F30 F -0.6175(3) 0.2098(4) 0.2703(3) 0.0499(16) Uani 1 1 d . . . . .
F31 F -0.6293(3) 0.0077(3) 0.2460(2) 0.0431(13) Uani 1 1 d . . . . .
F32 F -0.6434(3) -0.1178(3) 0.2565(2) 0.0444(13) Uani 1 1 d . . . . .
F33 F -0.5447(3) -0.0731(4) 0.2815(2) 0.0431(13) Uani 1 1 d . . . . .
F34 F -0.3262(3) 0.1117(7) 0.4131(4) 0.090(3) Uani 1 1 d . U . . .
F35 F -0.3961(3) 0.1409(5) 0.3186(3) 0.067(2) Uani 1 1 d . . . . .
F36 F -0.3830(5) 0.0212(5) 0.3497(5) 0.102(3) Uani 1 1 d . U . . .
O17 O -0.4750(3) 0.1374(3) 0.5664(2) 0.0206(10) Uani 1 1 d . . . . .
O10 O -0.4800(3) -0.0191(3) 0.5991(2) 0.0199(10) Uani 1 1 d . . . . .
O11 O -0.3703(2) 0.0198(4) 0.5754(2) 0.0202(10) Uani 1 1 d . . . . .
O16 O -0.3673(3) 0.2464(4) 0.6268(3) 0.0278(13) Uani 1 1 d . . . . .
O18 O -0.4512(2) -0.1089(3) 0.5099(2) 0.0207(10) Uani 1 1 d . . . . .
O14 O -0.5469(2) 0.1290(3) 0.4270(2) 0.0202(10) Uani 1 1 d . . . . .
O12 O -0.5950(2) 0.0005(3) 0.4742(2) 0.0198(10) Uani 1 1 d . . . . .
O15 O -0.4225(2) 0.0688(3) 0.4465(2) 0.0211(10) Uani 1 1 d . . . . .
O13 O -0.5328(3) -0.0350(3) 0.3950(2) 0.0227(11) Uani 1 1 d . . . . .
N3 N -0.5058(3) 0.2039(3) 0.5571(3) 0.0176(12) Uani 1 1 d . . . . .
N4 N -0.4584(3) -0.1767(4) 0.4799(3) 0.0194(12) Uani 1 1 d . . . . .
C42 C -0.5482(4) 0.1511(4) 0.3739(3) 0.0198(14) Uani 1 1 d . . . . .
C39 C -0.5920(4) -0.0402(5) 0.3537(4) 0.0229(15) Uani 1 1 d . . . . .
C35 C -0.2630(4) -0.0143(5) 0.6543(4) 0.0269(16) Uani 1 1 d . . . . .
C43 C -0.4998(4) 0.1397(5) 0.3526(3) 0.0221(14) Uani 1 1 d . . . . .
H43 H -0.5074 0.1579 0.3116 0.027 Uiso 1 1 calc R U . . .
C51 C -0.3865(4) 0.3114(5) 0.4461(4) 0.0296(18) Uani 1 1 d . . . . .
H51 H -0.3917 0.3262 0.4051 0.036 Uiso 1 1 calc R U . . .
C58 C -0.3857(4) -0.1401(5) 0.4290(4) 0.0314(18) Uani 1 1 d . . . . .
H58A H -0.4251 -0.1195 0.3930 0.047 Uiso 1 1 calc R U . . .
H58B H -0.3555 -0.1612 0.4133 0.047 Uiso 1 1 calc R U . . .
H58C H -0.3639 -0.0977 0.4595 0.047 Uiso 1 1 calc R U . . .
C59 C -0.4057(4) -0.2071(5) 0.4627(4) 0.0219(15) Uani 1 1 d . . . . .
C60 C -0.3469(4) -0.2331(5) 0.5261(4) 0.0304(17) Uani 1 1 d . . . . .
H60A H -0.3291 -0.1873 0.5539 0.046 Uiso 1 1 calc R U . . .
H60B H -0.3126 -0.2562 0.5170 0.046 Uiso 1 1 calc R U . . .
H60C H -0.3619 -0.2721 0.5473 0.046 Uiso 1 1 calc R U . . .
C31 C -0.4577(4) -0.0578(5) 0.7049(4) 0.0254(16) Uani 1 1 d . . . . .
C32 C -0.4332(4) -0.0335(4) 0.6546(3) 0.0182(14) Uani 1 1 d . . . . .
C33 C -0.3644(4) -0.0312(5) 0.6744(3) 0.0236(15) Uani 1 1 d . . . . .
H33 H -0.3348 -0.0466 0.7164 0.028 Uiso 1 1 calc R U . . .
C34 C -0.3395(4) -0.0057(4) 0.6312(4) 0.0209(14) Uani 1 1 d . . . . .
C41 C -0.6109(4) 0.1992(5) 0.3296(4) 0.0278(17) Uani 1 1 d . . . . .
C44 C -0.4390(4) 0.1005(5) 0.3927(4) 0.0232(15) Uani 1 1 d . . . . .
C45 C -0.3862(4) 0.0941(6) 0.3666(4) 0.0347(19) Uani 1 1 d . . . . .
C36 C -0.7122(4) 0.0045(6) 0.4248(4) 0.0311(18) Uani 1 1 d . . . . .
C37 C -0.6458(4) -0.0107(4) 0.4218(4) 0.0217(14) Uani 1 1 d . . . . .
C38 C -0.6500(4) -0.0310(6) 0.3613(4) 0.0272(17) Uani 1 1 d . . . . .
H38 H -0.6918 -0.0384 0.3259 0.033 Uiso 1 1 calc R U . . .
C40 C -0.6025(4) -0.0567(5) 0.2838(4) 0.0276(17) Uani 1 1 d . . . . .
C46 C -0.3182(5) 0.1866(6) 0.7314(4) 0.039(2) Uani 1 1 d . . . . .
H46A H -0.3536 0.1476 0.7149 0.059 Uiso 1 1 calc R U . . .
H46B H -0.3312 0.2306 0.7501 0.059 Uiso 1 1 calc R U . . .
H46C H -0.2782 0.1623 0.7640 0.059 Uiso 1 1 calc R U . . .
C47 C -0.3048(4) 0.2169(6) 0.6766(4) 0.0340(18) Uani 1 1 d . . . . .
H47A H -0.2717 0.2595 0.6920 0.041 Uiso 1 1 calc R U . . .
H47B H -0.2879 0.1738 0.6598 0.041 Uiso 1 1 calc R U . . .
C48 C -0.3711(4) 0.2646(5) 0.5680(4) 0.0250(15) Uani 1 1 d . . . . .
C49 C -0.3146(4) 0.2708(6) 0.5562(4) 0.033(2) Uani 1 1 d . . . . .
H49 H -0.2719 0.2587 0.5886 0.040 Uiso 1 1 calc R U . . .
C50 C -0.3239(4) 0.2955(6) 0.4945(4) 0.0338(19) Uani 1 1 d . . . . .
H50 H -0.2869 0.3012 0.4863 0.041 Uiso 1 1 calc R U . . .
C52 C -0.4423(4) 0.3059(4) 0.4570(4) 0.0243(16) Uani 1 1 d . . . . .
H52 H -0.4844 0.3197 0.4244 0.029 Uiso 1 1 calc R U . . .
C53 C -0.4350(4) 0.2796(4) 0.5175(3) 0.0180(14) Uani 1 1 d . . . . .
C55 C -0.5990(4) 0.1464(5) 0.5740(5) 0.0298(17) Uani 1 1 d . . . . .
H55A H -0.6219 0.1322 0.5288 0.045 Uiso 1 1 calc R U . . .
H55B H -0.6314 0.1577 0.5898 0.045 Uiso 1 1 calc R U . . .
H55C H -0.5709 0.1027 0.5984 0.045 Uiso 1 1 calc R U . . .
C56 C -0.5563(4) 0.2197(5) 0.5822(4) 0.0219(14) Uani 1 1 d . . . . .
C57 C -0.5161(5) 0.2412(6) 0.6535(4) 0.035(2) Uani 1 1 d . . . . .
H57A H -0.4877 0.1969 0.6763 0.053 Uiso 1 1 calc R U . . .
H57B H -0.5462 0.2527 0.6719 0.053 Uiso 1 1 calc R U . . .
H57C H -0.4890 0.2875 0.6575 0.053 Uiso 1 1 calc R U . . .
C54 C -0.4917(3) 0.2703(4) 0.5311(3) 0.0149(13) Uani 1 1 d . . . . .
Dy3 Dy -0.50793(2) 0.72255(2) 0.00778(2) 0.01546(7) Uani 1 1 d . . . . .
F37 F -0.3140(3) 0.8358(4) 0.2581(3) 0.0566(16) Uani 1 1 d . . . . .
F38 F -0.3734(4) 0.7329(4) 0.2510(3) 0.0528(16) Uani 1 1 d . . . . .
F39 F -0.4196(3) 0.8479(4) 0.2282(3) 0.0557(17) Uani 1 1 d . . . . .
F40 F -0.6078(6) 0.7266(5) 0.1613(6) 0.110(4) Uani 1 1 d . U . . .
F41 F -0.5929(4) 0.6080(5) 0.1918(4) 0.084(3) Uani 1 1 d . . . . .
F42 F -0.6640(4) 0.6419(10) 0.0984(4) 0.136(5) Uani 1 1 d . . . . .
F43 F -0.3755(3) 0.5309(5) 0.2334(3) 0.0639(19) Uani 1 1 d . . . . .
F44 F -0.3282(3) 0.5784(4) 0.1780(3) 0.0537(17) Uani 1 1 d . . . . .
F45 F -0.3870(3) 0.4710(4) 0.1471(3) 0.0483(15) Uani 1 1 d . . . . .
F46 F -0.2303(3) 0.7983(5) 0.1037(3) 0.0599(18) Uani 1 1 d . . . . .
F47 F -0.2594(3) 0.6759(4) 0.0796(4) 0.0608(18) Uani 1 1 d . . . . .
F48 F -0.2922(3) 0.7639(4) 0.0048(3) 0.0450(13) Uani 1 1 d . . . . .
F49 F -0.5049(3) 0.7482(4) -0.2063(3) 0.0527(16) Uani 1 1 d . . . . .
F50 F -0.5124(3) 0.8721(3) -0.1869(2) 0.0422(13) Uani 1 1 d . . . . .
F51 F -0.5965(3) 0.8103(4) -0.2596(2) 0.0482(15) Uani 1 1 d . . . . .
F52 F -0.7696(3) 0.7635(7) -0.2021(3) 0.092(3) Uani 1 1 d . U . . .
F53 F -0.7469(3) 0.8019(4) -0.1076(3) 0.0576(18) Uani 1 1 d . . . . .
F54 F -0.7535(3) 0.6800(5) -0.1268(5) 0.083(3) Uani 1 1 d . . . . .
O27 O -0.5206(3) 0.6144(3) -0.0626(2) 0.0211(10) Uani 1 1 d . . . . .
O23 O -0.5681(3) 0.6836(3) 0.0642(3) 0.0247(11) Uani 1 1 d . . . . .
O24 O -0.4479(3) 0.6164(3) 0.0776(3) 0.0231(11) Uani 1 1 d . . . . .
O19 O -0.4503(3) 0.7798(3) 0.1134(3) 0.0257(12) Uani 1 1 d . . . . .
O20 O -0.3983(2) 0.7471(3) 0.0259(3) 0.0240(11) Uani 1 1 d . . . . .
O22 O -0.6222(2) 0.7228(4) -0.0636(2) 0.0216(10) Uani 1 1 d . . . . .
O21 O -0.5174(3) 0.7695(3) -0.0936(2) 0.0198(10) Uani 1 1 d . . . . .
O25 O -0.3679(3) 1.0025(4) 0.1292(3) 0.0286(12) Uani 1 1 d . . . . .
O26 O -0.5423(3) 0.8552(3) 0.0002(3) 0.0259(11) Uani 1 1 d . . . . .
N5 N -0.5377(3) 0.9239(4) 0.0263(3) 0.0208(12) Uani 1 1 d . . . . .
N6 N -0.4919(3) 0.5458(3) -0.0563(3) 0.0199(13) Uani 1 1 d . . . . .
C89 C -0.4417(4) 0.5282(6) -0.0821(4) 0.0285(16) Uani 1 1 d . . . . .
C90 C -0.4845(5) 0.5125(6) -0.1552(4) 0.041(2) Uani 1 1 d . . . . .
H90A H -0.5123 0.4663 -0.1609 0.061 Uiso 1 1 calc R U . . .
H90B H -0.4556 0.5029 -0.1752 0.061 Uiso 1 1 calc R U . . .
H90C H -0.5123 0.5583 -0.1750 0.061 Uiso 1 1 calc R U . . .
C88 C -0.3959(5) 0.6016(6) -0.0709(5) 0.040(2) Uani 1 1 d . . . . .
H88A H -0.4226 0.6472 -0.0931 0.060 Uiso 1 1 calc R U . . .
H88B H -0.3641 0.5906 -0.0874 0.060 Uiso 1 1 calc R U . . .
H88C H -0.3723 0.6128 -0.0251 0.060 Uiso 1 1 calc R U . . .
C76 C -0.3154(5) 1.0404(6) 0.2398(4) 0.043(2) Uani 1 1 d . . . . .
H76A H -0.3398 1.0900 0.2294 0.064 Uiso 1 1 calc R U . . .
H76B H -0.2732 1.0477 0.2777 0.064 Uiso 1 1 calc R U . . .
H76C H -0.3410 0.9999 0.2484 0.064 Uiso 1 1 calc R U . . .
C69 C -0.4460(4) 0.5929(4) 0.1309(4) 0.0231(15) Uani 1 1 d . . . . .
C82 C -0.4427(4) 0.9464(5) -0.0407(4) 0.0231(16) Uani 1 1 d . . . . .
H82 H -0.4853 0.9357 -0.0739 0.028 Uiso 1 1 calc R U . . .
C72 C -0.5659(4) 0.7789(4) -0.1477(4) 0.0214(15) Uani 1 1 d . . . . .
C66 C -0.6049(5) 0.6543(6) 0.1422(5) 0.038(2) Uani 1 1 d . . . . .
C61 C -0.3738(5) 0.8029(5) 0.2229(4) 0.037(2) Uani 1 1 d . . . . .
C80 C -0.3238(4) 0.9561(6) -0.0030(4) 0.0333(18) Uani 1 1 d . . . . .
H80 H -0.2867 0.9531 -0.0113 0.040 Uiso 1 1 calc R U . . .
C87 C -0.6511(4) 0.9743(6) -0.0235(6) 0.046(3) Uani 1 1 d . . . . .
H87A H -0.6403 1.0205 -0.0419 0.069 Uiso 1 1 calc R U . . .
H87B H -0.6903 0.9853 -0.0175 0.069 Uiso 1 1 calc R U . . .
H87C H -0.6597 0.9294 -0.0523 0.069 Uiso 1 1 calc R U . . .
C67 C -0.5519(4) 0.6473(5) 0.1164(4) 0.0252(15) Uani 1 1 d . . . . .
C70 C -0.3828(5) 0.5426(5) 0.1730(5) 0.037(2) Uani 1 1 d . . . . .
C84 C -0.4924(4) 0.9795(4) 0.0342(3) 0.0192(14) Uani 1 1 d . . . . .
C64 C -0.3441(4) 0.7627(5) 0.0756(4) 0.0270(16) Uani 1 1 d . . . . .
C78 C -0.3701(4) 0.9847(5) 0.0709(4) 0.0233(15) Uani 1 1 d . . . . .
C81 C -0.3860(4) 0.9390(6) -0.0521(4) 0.033(2) Uani 1 1 d . . . . .
H81 H -0.3908 0.9227 -0.0927 0.040 Uiso 1 1 calc R U . . .
C77 C -0.3030(4) 1.0147(6) 0.1837(4) 0.0334(18) Uani 1 1 d . . . . .
H77A H -0.2783 1.0558 0.1736 0.040 Uiso 1 1 calc R U . . .
H77B H -0.2771 0.9654 0.1941 0.040 Uiso 1 1 calc R U . . .
C73 C -0.6348(4) 0.7711(5) -0.1657(4) 0.0262(17) Uani 1 1 d . . . . .
H73 H -0.6662 0.7828 -0.2081 0.031 Uiso 1 1 calc R U . . .
C79 C -0.3145(4) 0.9778(6) 0.0590(4) 0.0318(18) Uani 1 1 d . . . . .
H79 H -0.2716 0.9876 0.0920 0.038 Uiso 1 1 calc R U . . .
C83 C -0.4348(4) 0.9693(5) 0.0197(3) 0.0209(14) Uani 1 1 d . . . . .
C86 C -0.5927(4) 0.9549(5) 0.0417(5) 0.0324(19) Uani 1 1 d . . . . .
C71 C -0.5453(4) 0.8036(5) -0.2013(4) 0.0277(17) Uani 1 1 d . . . . .
C63 C -0.3353(4) 0.7820(5) 0.1373(4) 0.0294(17) Uani 1 1 d . . . . .
H63 H -0.2921 0.7901 0.1702 0.035 Uiso 1 1 calc R U . . .
C68 C -0.4936(4) 0.6051(5) 0.1533(4) 0.0264(16) Uani 1 1 d . . . . .
H68 H -0.4863 0.5846 0.1936 0.032 Uiso 1 1 calc R U . . .
C62 C -0.3893(4) 0.7896(5) 0.1514(4) 0.0279(17) Uani 1 1 d . . . . .
C85 C -0.6108(6) 0.8900(6) 0.0772(7) 0.057(3) Uani 1 1 d . . . . .
H85A H -0.6242 0.8424 0.0509 0.086 Uiso 1 1 calc R U . . .
H85B H -0.6472 0.9082 0.0854 0.086 Uiso 1 1 calc R U . . .
H85C H -0.5726 0.8783 0.1178 0.086 Uiso 1 1 calc R U . . .
C74 C -0.6563(4) 0.7461(5) -0.1202(4) 0.0250(17) Uani 1 1 d . . . . .
C75 C -0.7319(4) 0.7478(6) -0.1407(4) 0.035(2) Uani 1 1 d . . . . .
C65 C -0.2811(4) 0.7503(6) 0.0649(5) 0.038(2) Uani 1 1 d . . . . .
Dy4 Dy 0.00142(2) 0.42161(2) 0.00743(2) 0.01722(7) Uani 1 1 d . . . . .
F55 F -0.2049(3) 0.5225(5) 0.0174(3) 0.070(2) Uani 1 1 d . . . . .
F56 F -0.1607(3) 0.5490(4) 0.1191(4) 0.0598(18) Uani 1 1 d . . . . .
F57 F -0.1711(3) 0.4277(3) 0.0871(4) 0.0547(16) Uani 1 1 d . . . . .
F58 F 0.0720(3) 0.6855(4) 0.1495(4) 0.0574(17) Uani 1 1 d . . . . .
F59 F 0.1392(3) 0.5879(4) 0.1903(3) 0.0514(15) Uani 1 1 d . . . . .
F60 F 0.0678(4) 0.6169(6) 0.2262(3) 0.079(3) Uani 1 1 d . . . . .
F61 F 0.0168(4) 0.2935(6) 0.2067(3) 0.090(3) Uani 1 1 d . . . . .
F62 F 0.0617(4) 0.4077(5) 0.2443(3) 0.075(2) Uani 1 1 d . . . . .
F63 F 0.1211(4) 0.3025(5) 0.2681(3) 0.0643(19) Uani 1 1 d . . . . .
F64 F 0.2410(2) 0.3647(4) 0.0786(3) 0.0422(13) Uani 1 1 d . . . . .
F65 F 0.2520(3) 0.4627(4) 0.1439(3) 0.0494(15) Uani 1 1 d . . . . .
F66 F 0.2738(3) 0.3422(4) 0.1799(3) 0.0499(15) Uani 1 1 d . . . . .
F67 F 0.0806(3) 0.2653(4) -0.1296(3) 0.0558(17) Uani 1 1 d . . . . .
F68 F 0.0856(5) 0.3834(5) -0.1601(5) 0.092(3) Uani 1 1 d . . . . .
F69 F 0.0095(4) 0.3037(5) -0.2217(3) 0.075(2) Uani 1 1 d . . . . .
F70 F -0.1999(3) 0.3982(5) -0.2543(3) 0.0576(17) Uani 1 1 d . . . . .
F71 F -0.2184(3) 0.4578(3) -0.1818(3) 0.0460(13) Uani 1 1 d . . . . .
F72 F -0.2142(3) 0.3287(4) -0.1837(3) 0.0600(18) Uani 1 1 d . . . . .
O35 O 0.0135(2) 0.5266(3) -0.0562(2) 0.0227(10) Uani 1 1 d . . . . .
O32 O 0.0310(3) 0.3657(3) -0.0702(3) 0.0236(11) Uani 1 1 d . . . . .
O33 O -0.0970(2) 0.4183(3) -0.0897(3) 0.0259(10) Uani 1 1 d . . . . .
O31 O 0.1175(2) 0.3997(3) 0.0605(2) 0.0229(11) Uani 1 1 d . . . . .
O28 O -0.0857(3) 0.4645(3) 0.0297(3) 0.0266(11) Uani 1 1 d . . . . .
O29 O 0.0417(3) 0.5321(4) 0.0786(3) 0.0272(11) Uani 1 1 d . . . . .
O30 O 0.0270(3) 0.3691(3) 0.1108(3) 0.0278(12) Uani 1 1 d . . . . .
O34 O -0.0913(3) 0.6271(4) -0.1555(3) 0.0323(13) Uani 1 1 d . . . . .
O36 O -0.0392(3) 0.2904(3) -0.0058(3) 0.0297(12) Uani 1 1 d . . . . .
N7 N 0.0379(3) 0.5985(4) -0.0437(3) 0.0188(12) Uani 1 1 d . . . . .
N8 N -0.0500(3) 0.2224(4) 0.0146(3) 0.0233(12) Uani 1 1 d . . . . .
C91 C -0.1571(5) 0.5011(5) 0.0748(5) 0.0366(19) Uani 1 1 d . . . . .
C116 C 0.1030(4) 0.6201(4) -0.0442(4) 0.0228(15) Uani 1 1 d . . . . .
C94 C 0.0245(5) 0.5577(5) 0.1212(4) 0.0306(17) Uani 1 1 d . . . . .
C117 C 0.1531(4) 0.5534(5) -0.0158(5) 0.0359(19) Uani 1 1 d . . . . .
H11A H 0.1569 0.5391 0.0262 0.054 Uiso 1 1 calc R U . . .
H11B H 0.1960 0.5708 -0.0113 0.054 Uiso 1 1 calc R U . . .
H11C H 0.1384 0.5076 -0.0440 0.054 Uiso 1 1 calc R U . . .
C115 C 0.0852(4) 0.6330(6) -0.1160(4) 0.038(2) Uani 1 1 d . . . . .
H11D H 0.0640 0.5857 -0.1403 0.057 Uiso 1 1 calc R U . . .
H11E H 0.1254 0.6437 -0.1202 0.057 Uiso 1 1 calc R U . . .
H11F H 0.0551 0.6777 -0.1326 0.057 Uiso 1 1 calc R U . . .
C109 C -0.1813(4) 0.6489(5) -0.1249(4) 0.0337(18) Uani 1 1 d . . . . .
H109 H -0.2145 0.6347 -0.1658 0.040 Uiso 1 1 calc R U . . .
C95 C 0.0766(5) 0.6115(6) 0.1733(5) 0.042(2) Uani 1 1 d . . . . .
C93 C -0.0362(4) 0.5452(5) 0.1232(4) 0.0306(18) Uani 1 1 d . . . . .
H93 H -0.0421 0.5658 0.1579 0.037 Uiso 1 1 calc R U . . .
C120 C -0.1479(5) 0.2658(6) 0.0296(6) 0.046(2) Uani 1 1 d . . . . .
H12A H -0.1188 0.2753 0.0748 0.069 Uiso 1 1 calc R U . . .
H12B H -0.1915 0.2505 0.0244 0.069 Uiso 1 1 calc R U . . .
H12C H -0.1515 0.3139 0.0052 0.069 Uiso 1 1 calc R U . . .
C104 C -0.1112(4) 0.3972(4) -0.1463(4) 0.0241(15) Uani 1 1 d . . . . .
C96 C 0.0698(5) 0.3385(6) 0.2205(4) 0.041(2) Uani 1 1 d . . . . .
C103 C -0.0677(4) 0.3696(5) -0.1703(4) 0.0333(18) Uani 1 1 d . . . . .
H103 H -0.0845 0.3595 -0.2146 0.040 Uiso 1 1 calc R U . . .
C106 C -0.0995(5) 0.5864(7) -0.2569(5) 0.047(2) Uani 1 1 d . . . . .
H10A H -0.1282 0.5880 -0.3029 0.071 Uiso 1 1 calc R U . . .
H10B H -0.0828 0.5328 -0.2444 0.071 Uiso 1 1 calc R U . . .
H10C H -0.0625 0.6225 -0.2463 0.071 Uiso 1 1 calc R U . . .
C105 C -0.1862(4) 0.3952(5) -0.1923(4) 0.0366(19) Uani 1 1 d . . . . .
C101 C 0.0445(5) 0.3265(6) -0.1608(4) 0.037(2) Uani 1 1 d . . . . .
C92 C -0.0877(4) 0.5031(5) 0.0750(4) 0.0283(16) Uani 1 1 d . . . . .
C98 C 0.1449(4) 0.3550(5) 0.1667(4) 0.0282(16) Uani 1 1 d . . . . .
H98 H 0.1800 0.3387 0.2059 0.034 Uiso 1 1 calc R U . . .
C114 C 0.0060(4) 0.6621(5) -0.0355(4) 0.0206(14) Uani 1 1 d . . . . .
C113 C -0.0647(3) 0.6654(4) -0.0482(4) 0.0212(14) Uani 1 1 d . . . . .
C112 C -0.0830(4) 0.6910(5) -0.0012(4) 0.0295(17) Uani 1 1 d . . . . .
H112 H -0.0501 0.7061 0.0396 0.035 Uiso 1 1 calc R U . . .
C102 C 0.0002(4) 0.3568(5) -0.1300(4) 0.0276(16) Uani 1 1 d . . . . .
C110 C -0.1985(4) 0.6738(6) -0.0762(5) 0.0367(19) Uani 1 1 d . . . . .
H110 H -0.2436 0.6765 -0.0854 0.044 Uiso 1 1 calc R U . . .
C99 C 0.1586(4) 0.3791(5) 0.1163(4) 0.0254(15) Uani 1 1 d . . . . .
C111 C -0.1501(4) 0.6944(5) -0.0148(5) 0.036(2) Uani 1 1 d . . . . .
H111 H -0.1624 0.7104 0.0170 0.043 Uiso 1 1 calc R U . . .
C97 C 0.0796(4) 0.3546(5) 0.1598(4) 0.0269(16) Uani 1 1 d . . . . .
C100 C 0.2324(4) 0.3871(6) 0.1298(4) 0.0333(18) Uani 1 1 d . . . . .
C119 C -0.1191(4) 0.1990(5) 0.0048(5) 0.0281(17) Uani 1 1 d . . . . .
C107 C -0.1387(5) 0.6111(6) -0.2210(4) 0.040(2) Uani 1 1 d . . . . .
H10D H -0.1650 0.6588 -0.2407 0.048 Uiso 1 1 calc R U . . .
H10E H -0.1690 0.5685 -0.2225 0.048 Uiso 1 1 calc R U . . .
C108 C -0.1140(4) 0.6457(5) -0.1113(4) 0.0285(16) Uani 1 1 d . . . . .
C118 C -0.1619(4) 0.1853(6) -0.0684(5) 0.042(2) Uani 1 1 d . . . . .
H11G H -0.1625 0.2334 -0.0916 0.063 Uiso 1 1 calc R U . . .
H11H H -0.2069 0.1718 -0.0767 0.063 Uiso 1 1 calc R U . . .
H11I H -0.1431 0.1423 -0.0826 0.063 Uiso 1 1 calc R U . . .
C29 C -0.1182(6) 0.0419(6) -0.4736(8) 0.062(3) Uani 1 1 d . U . . .
C28 C -0.1478(8) 0.1042(9) -0.4569(10) 0.093(5) Uani 1 1 d . U . . .
H28A H -0.1189 0.1208 -0.4131 0.139 Uiso 1 1 calc R U . . .
H28B H -0.1901 0.0868 -0.4597 0.139 Uiso 1 1 calc R U . . .
H28C H -0.1549 0.1483 -0.4861 0.139 Uiso 1 1 calc R U . . .
C30 C -0.1758(7) 0.0280(11) -0.5507(8) 0.084(4) Uani 1 1 d . . . . .
H30A H -0.1743 0.0721 -0.5769 0.127 Uiso 1 1 calc R U . . .
H30B H -0.2196 0.0251 -0.5525 0.127 Uiso 1 1 calc R U . . .
H30C H -0.1665 -0.0211 -0.5670 0.127 Uiso 1 1 calc R U . . .
O2 O -0.1101(3) 0.2801(3) -0.5651(3) 0.0290(12) Uani 1 1 d . . . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Dy1 O9 2.337(6) . ?
Dy1 O1 2.373(6) . ?
Dy1 O8 2.381(6) . ?
Dy1 O5 2.337(6) . ?
Dy1 O6 2.332(5) . ?
Dy1 O3 2.317(6) . ?
Dy1 O4 2.381(7) . ?
Dy1 O2 2.337(6) . ?
F1 C1 1.344(15) . ?
F2 C1 1.281(13) . ?
F3 C1 1.313(12) . ?
F4 C5 1.310(10) . ?
F5 C5 1.318(11) . ?
F6 C5 1.284(10) . ?
F7 C6 1.332(12) . ?
F8 C6 1.327(13) . ?
F9 C6 1.334(13) . ?
F10 C10 1.337(12) . ?
F11 C10 1.345(13) . ?
F12 C10 1.304(13) . ?
F13 C11 1.328(11) . ?
F14 C11 1.366(11) . ?
F15 C11 1.309(11) . ?
F16 C15 1.331(9) . ?
F17 C15 1.329(10) . ?
F18 C15 1.333(11) . ?
O7 C17 1.456(11) . ?
O7 C18 1.333(12) . ?
O9 N2 1.300(9) . ?
O1 C2 1.237(12) . ?
O8 N1 1.294(8) . ?
O5 C12 1.258(10) . ?
O6 C14 1.233(9) . ?
O3 C7 1.258(11) . ?
O4 C9 1.232(12) . ?
N1 C27 1.517(10) . ?
N1 C24 1.324(11) . ?
N2 C24 1.328(11) 2_544 ?
N2 C29 1.501(12) . ?
C7 C6 1.546(12) . ?
C7 C8 1.378(13) . ?
C20 H20 0.9300 . ?
C20 C19 1.371(16) . ?
C20 C21 1.385(17) . ?
C1 C2 1.556(13) . ?
C2 C3 1.378(14) . ?
C5 C4 1.550(12) . ?
C11 C12 1.519(12) . ?
C12 C13 1.378(11) . ?
C13 H13 0.9300 . ?
C13 C14 1.395(11) . ?
C14 C15 1.542(10) . ?
C4 C3 1.392(12) . ?
C4 O2 1.234(10) . ?
C8 H8 0.9300 . ?
C8 C9 1.407(12) . ?
C9 C10 1.550(14) . ?
C16 H16A 0.9600 . ?
C16 H16B 0.9600 . ?
C16 H16C 0.9600 . ?
C16 C17 1.520(17) . ?
C17 H17A 0.9700 . ?
C17 H17B 0.9700 . ?
C3 H3 0.9300 . ?
C19 H19 0.9300 . ?
C19 C18 1.401(13) . ?
C21 H21 0.9300 . ?
C21 C22 1.377(13) . ?
C22 H22 0.9300 . ?
C22 C23 1.381(12) . ?
C18 C23 1.414(12) . ?
C26 H26A 0.9600 . ?
C26 H26B 0.9600 . ?
C26 H26C 0.9600 . ?
C26 C27 1.62(2) . ?
C25 H25A 0.9600 . ?
C25 H25B 0.9600 . ?
C25 H25C 0.9600 . ?
C25 C27 1.35(2) . ?
C27 C29 1.488(14) 2_554 ?
C23 C24 1.466(11) . ?
C24 N2 1.328(11) 2_554 ?
Dy2 O17 2.368(5) . ?
Dy2 O10 2.357(5) . ?
Dy2 O11 2.333(5) . ?
Dy2 O18 2.323(5) . ?
Dy2 O14 2.390(5) . ?
Dy2 O12 2.318(5) . ?
Dy2 O15 2.327(5) . ?
Dy2 O13 2.383(5) . ?
F19 C31 1.327(9) . ?
F20 C31 1.334(9) . ?
F21 C31 1.323(9) . ?
F22 C35 1.310(10) . ?
F23 C35 1.303(10) . ?
F24 C35 1.285(11) . ?
F25 C36 1.332(10) . ?
F26 C36 1.350(11) . ?
F27 C36 1.327(10) . ?
F28 C41 1.348(10) . ?
F29 C41 1.335(10) . ?
F30 C41 1.316(10) . ?
F31 C40 1.340(9) . ?
F32 C40 1.323(9) . ?
F33 C40 1.341(10) . ?
F34 C45 1.315(12) . ?
F35 C45 1.286(10) . ?
F36 C45 1.287(13) . ?
O17 N3 1.271(8) . ?
O10 C32 1.256(8) . ?
O11 C34 1.228(9) . ?
O16 C47 1.436(10) . ?
O16 C48 1.351(9) . ?
O18 N4 1.296(8) . ?
O14 C42 1.262(8) . ?
O12 C37 1.243(9) . ?
O15 C44 1.239(9) . ?
O13 C39 1.236(9) . ?
N3 C56 1.502(9) . ?
N3 C54 1.359(9) . ?
N4 C59 1.488(9) . ?
N4 C54 1.354(9) 2_446 ?
C42 C43 1.385(10) . ?
C42 C41 1.535(10) . ?
C39 C38 1.390(11) . ?
C39 C40 1.541(10) . ?
C35 C34 1.550(10) . ?
C43 H43 0.9300 . ?
C43 C44 1.411(10) . ?
C51 H51 0.9300 . ?
C51 C50 1.364(13) . ?
C51 C52 1.378(11) . ?
C58 H58A 0.9600 . ?
C58 H58B 0.9600 . ?
C58 H58C 0.9600 . ?
C58 C59 1.536(10) . ?
C59 C60 1.521(11) . ?
C59 C56 1.576(11) 2_446 ?
C60 H60A 0.9600 . ?
C60 H60B 0.9600 . ?
C60 H60C 0.9600 . ?
C31 C32 1.539(10) . ?
C32 C33 1.390(10) . ?
C33 H33 0.9300 . ?
C33 C34 1.404(10) . ?
C44 C45 1.549(10) . ?
C36 C37 1.534(10) . ?
C37 C38 1.394(11) . ?
C38 H38 0.9300 . ?
C46 H46A 0.9600 . ?
C46 H46B 0.9600 . ?
C46 H46C 0.9600 . ?
C46 C47 1.504(12) . ?
C47 H47A 0.9700 . ?
C47 H47B 0.9700 . ?
C48 C49 1.406(11) . ?
C48 C53 1.398(11) . ?
C49 H49 0.9300 . ?
C49 C50 1.401(12) . ?
C50 H50 0.9300 . ?
C52 H52 0.9300 . ?
C52 C53 1.396(10) . ?
C53 C54 1.441(9) . ?
C55 H55A 0.9600 . ?
C55 H55B 0.9600 . ?
C55 H55C 0.9600 . ?
C55 C56 1.508(11) . ?
C56 C59 1.576(11) 2_456 ?
C56 C57 1.517(11) . ?
C57 H57A 0.9600 . ?
C57 H57B 0.9600 . ?
C57 H57C 0.9600 . ?
C54 N4 1.354(9) 2_456 ?
Dy3 O27 2.353(5) . ?
Dy3 O23 2.340(5) . ?
Dy3 O24 2.360(5) . ?
Dy3 O19 2.378(5) . ?
Dy3 O20 2.325(5) . ?
Dy3 O22 2.330(5) . ?
Dy3 O21 2.377(5) . ?
Dy3 O26 2.321(5) . ?
F37 C61 1.328(10) . ?
F38 C61 1.331(11) . ?
F39 C61 1.316(11) . ?
F40 C66 1.295(13) . ?
F41 C66 1.301(11) . ?
F42 C66 1.266(13) . ?
F43 C70 1.338(11) . ?
F44 C70 1.313(11) . ?
F45 C70 1.319(11) . ?
F46 C65 1.346(11) . ?
F47 C65 1.318(11) . ?
F48 C65 1.310(12) . ?
F49 C71 1.332(10) . ?
F50 C71 1.316(10) . ?
F51 C71 1.318(9) . ?
F52 C75 1.305(11) . ?
F53 C75 1.318(11) . ?
F54 C75 1.323(12) . ?
O27 N6 1.286(8) . ?
O23 C67 1.243(9) . ?
O24 C69 1.270(9) . ?
O19 C62 1.253(10) . ?
O20 C64 1.264(9) . ?
O22 C74 1.239(9) . ?
O21 C72 1.237(9) . ?
O25 C78 1.352(9) . ?
O25 C77 1.442(9) . ?
O26 N5 1.275(8) . ?
N5 C84 1.322(10) . ?
N5 C86 1.511(9) . ?
N6 C89 1.512(9) . ?
N6 C84 1.329(9) 2_445 ?
C89 C90 1.538(12) . ?
C89 C88 1.540(12) . ?
C89 C86 1.518(13) 2_445 ?
C90 H90A 0.9600 . ?
C90 H90B 0.9600 . ?
C90 H90C 0.9600 . ?
C88 H88A 0.9600 . ?
C88 H88B 0.9600 . ?
C88 H88C 0.9600 . ?
C76 H76A 0.9600 . ?
C76 H76B 0.9600 . ?
C76 H76C 0.9600 . ?
C76 C77 1.499(12) . ?
C69 C70 1.549(11) . ?
C69 C68 1.389(11) . ?
C82 H82 0.9300 . ?
C82 C81 1.406(11) . ?
C82 C83 1.374(10) . ?
C72 C73 1.406(11) . ?
C72 C71 1.553(10) . ?
C66 C67 1.546(11) . ?
C61 C62 1.536(12) . ?
C80 H80 0.9300 . ?
C80 C81 1.368(12) . ?
C80 C79 1.395(12) . ?
C87 H87A 0.9600 . ?
C87 H87B 0.9600 . ?
C87 H87C 0.9600 . ?
C87 C86 1.514(14) . ?
C67 C68 1.384(11) . ?
C84 N6 1.329(9) 2_455 ?
C84 C83 1.474(10) . ?
C64 C63 1.379(12) . ?
C64 C65 1.544(11) . ?
C78 C79 1.389(11) . ?
C78 C83 1.418(10) . ?
C81 H81 0.9300 . ?
C77 H77A 0.9700 . ?
C77 H77B 0.9700 . ?
C73 H73 0.9300 . ?
C73 C74 1.397(11) . ?
C79 H79 0.9300 . ?
C86 C89 1.518(13) 2_455 ?
C86 C85 1.516(12) . ?
C63 H63 0.9300 . ?
C63 C62 1.387(13) . ?
C68 H68 0.9300 . ?
C85 H85A 0.9600 . ?
C85 H85B 0.9600 . ?
C85 H85C 0.9600 . ?
C74 C75 1.533(11) . ?
Dy4 O35 2.373(5) . ?
Dy4 O32 2.355(5) . ?
Dy4 O33 2.324(5) . ?
Dy4 O31 2.342(5) . ?
Dy4 O28 2.333(5) . ?
Dy4 O29 2.357(6) . ?
Dy4 O30 2.351(5) . ?
Dy4 O36 2.334(5) . ?
F55 C91 1.319(11) . ?
F56 C91 1.326(10) . ?
F57 C91 1.323(10) . ?
F58 C95 1.335(13) . ?
F59 C95 1.328(12) . ?
F60 C95 1.321(11) . ?
F61 C96 1.312(12) . ?
F62 C96 1.323(12) . ?
F63 C96 1.320(12) . ?
F64 C100 1.330(10) . ?
F65 C100 1.326(11) . ?
F66 C100 1.335(10) . ?
F67 C101 1.298(11) . ?
F68 C101 1.313(12) . ?
F69 C101 1.316(11) . ?
F70 C105 1.317(10) . ?
F71 C105 1.349(11) . ?
F72 C105 1.331(10) . ?
O35 N7 1.295(8) . ?
O32 C102 1.239(10) . ?
O33 C104 1.245(9) . ?
O31 C99 1.244(9) . ?
O28 C92 1.243(10) . ?
O29 C94 1.275(10) . ?
O30 C97 1.232(10) . ?
O34 C107 1.424(10) . ?
O34 C108 1.359(9) . ?
O36 N8 1.292(8) . ?
N7 C116 1.500(8) . ?
N7 C114 1.336(9) . ?
N8 C114 1.334(10) 2_545 ?
N8 C119 1.505(10) . ?
C91 C92 1.544(11) . ?
C116 C117 1.502(11) . ?
C116 C115 1.531(11) . ?
C116 C119 1.545(11) 2 ?
C94 C95 1.529(13) . ?
C94 C93 1.390(12) . ?
C117 H11A 0.9600 . ?
C117 H11B 0.9600 . ?
C117 H11C 0.9600 . ?
C115 H11D 0.9600 . ?
C115 H11E 0.9600 . ?
C115 H11F 0.9600 . ?
C109 H109 0.9300 . ?
C109 C110 1.399(13) . ?
C109 C108 1.390(11) . ?
C93 H93 0.9300 . ?
C93 C92 1.378(12) . ?
C120 H12A 0.9600 . ?
C120 H12B 0.9600 . ?
C120 H12C 0.9600 . ?
C120 C119 1.517(11) . ?
C104 C103 1.391(11) . ?
C104 C105 1.525(11) . ?
C96 C97 1.531(11) . ?
C103 H103 0.9300 . ?
C103 C102 1.391(12) . ?
C106 H10A 0.9600 . ?
C106 H10B 0.9600 . ?
C106 H10C 0.9600 . ?
C106 C107 1.503(13) . ?
C101 C102 1.539(11) . ?
C98 H98 0.9300 . ?
C98 C99 1.385(10) . ?
C98 C97 1.392(12) . ?
C114 N8 1.334(10) 2 ?
C114 C113 1.470(9) . ?
C113 C112 1.383(11) . ?
C113 C108 1.410(11) . ?
C112 H112 0.9300 . ?
C112 C111 1.385(11) . ?
C110 H110 0.9300 . ?
C110 C111 1.380(14) . ?
C99 C100 1.538(11) . ?
C111 H111 0.9300 . ?
C119 C116 1.545(11) 2_545 ?
C119 C118 1.534(14) . ?
C107 H10D 0.9700 . ?
C107 H10E 0.9700 . ?
C118 H11G 0.9600 . ?
C118 H11H 0.9600 . ?
C118 H11I 0.9600 . ?
C29 C27 1.488(14) 2_544 ?
C29 C28 1.374(17) . ?
C29 C30 1.67(2) . ?
C28 H28A 0.9600 . ?
C28 H28B 0.9600 . ?
C28 H28C 0.9600 . ?
C30 H30A 0.9600 . ?
C30 H30B 0.9600 . ?
C30 H30C 0.9600 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O9 Dy1 O1 73.7(2) . . ?
O9 Dy1 O8 142.1(2) . . ?
O9 Dy1 O5 145.3(2) . . ?
O9 Dy1 O4 73.1(2) . . ?
O9 Dy1 O2 74.5(2) . . ?
O1 Dy1 O8 71.0(2) . . ?
O1 Dy1 O4 129.8(2) . . ?
O5 Dy1 O1 138.71(19) . . ?
O5 Dy1 O8 72.6(2) . . ?
O5 Dy1 O4 74.2(2) . . ?
O5 Dy1 O2 120.7(2) . . ?
O6 Dy1 O9 86.1(2) . . ?
O6 Dy1 O1 140.1(2) . . ?
O6 Dy1 O8 112.9(2) . . ?
O6 Dy1 O5 73.15(19) . . ?
O6 Dy1 O4 72.7(2) . . ?
O6 Dy1 O2 69.16(18) . . ?
O3 Dy1 O9 101.8(2) . . ?
O3 Dy1 O1 78.9(2) . . ?
O3 Dy1 O8 84.7(2) . . ?
O3 Dy1 O5 79.0(2) . . ?
O3 Dy1 O6 139.8(2) . . ?
O3 Dy1 O4 72.3(2) . . ?
O3 Dy1 O2 151.01(19) . . ?
O4 Dy1 O8 142.5(2) . . ?
O2 Dy1 O1 72.4(2) . . ?
O2 Dy1 O8 82.0(2) . . ?
O2 Dy1 O4 130.9(2) . . ?
C18 O7 C17 119.4(8) . . ?
N2 O9 Dy1 153.3(6) . . ?
C2 O1 Dy1 132.7(6) . . ?
N1 O8 Dy1 138.6(5) . . ?
C12 O5 Dy1 132.2(5) . . ?
C14 O6 Dy1 134.5(5) . . ?
C7 O3 Dy1 135.6(6) . . ?
C9 O4 Dy1 133.3(6) . . ?
O8 N1 C27 121.1(6) . . ?
O8 N1 C24 126.6(7) . . ?
C24 N1 C27 112.2(6) . . ?
O9 N2 C24 126.7(7) . 2_544 ?
O9 N2 C29 121.4(7) . . ?
C24 N2 C29 111.6(7) 2_544 . ?
O3 C7 C6 116.2(8) . . ?
O3 C7 C8 127.9(8) . . ?
C8 C7 C6 115.9(9) . . ?
C19 C20 H20 119.1 . . ?
C19 C20 C21 121.7(9) . . ?
C21 C20 H20 119.1 . . ?
F1 C1 C2 111.5(10) . . ?
F2 C1 F1 104.9(10) . . ?
F2 C1 F3 109.7(10) . . ?
F2 C1 C2 110.2(9) . . ?
F3 C1 F1 107.1(9) . . ?
F3 C1 C2 113.1(8) . . ?
O1 C2 C1 112.8(9) . . ?
O1 C2 C3 128.7(8) . . ?
C3 C2 C1 118.5(9) . . ?
F4 C5 F5 104.8(7) . . ?
F4 C5 C4 114.1(7) . . ?
F5 C5 C4 109.9(7) . . ?
F6 C5 F4 108.2(8) . . ?
F6 C5 F5 108.5(9) . . ?
F6 C5 C4 111.0(7) . . ?
F13 C11 F14 105.5(7) . . ?
F13 C11 C12 111.7(8) . . ?
F14 C11 C12 109.3(7) . . ?
F15 C11 F13 108.9(8) . . ?
F15 C11 F14 106.3(8) . . ?
F15 C11 C12 114.6(7) . . ?
O5 C12 C11 114.8(7) . . ?
O5 C12 C13 127.5(7) . . ?
C13 C12 C11 117.7(7) . . ?
C12 C13 H13 119.1 . . ?
C12 C13 C14 121.8(7) . . ?
C14 C13 H13 119.1 . . ?
O6 C14 C13 127.0(7) . . ?
O6 C14 C15 113.9(7) . . ?
C13 C14 C15 119.1(7) . . ?
F16 C15 F18 107.3(7) . . ?
F16 C15 C14 110.9(6) . . ?
F17 C15 F16 106.9(7) . . ?
F17 C15 F18 107.6(7) . . ?
F17 C15 C14 113.5(7) . . ?
F18 C15 C14 110.3(7) . . ?
F7 C6 F9 108.4(8) . . ?
F7 C6 C7 110.8(8) . . ?
F8 C6 F7 106.3(9) . . ?
F8 C6 F9 108.3(8) . . ?
F8 C6 C7 109.5(8) . . ?
F9 C6 C7 113.3(9) . . ?
C3 C4 C5 117.1(7) . . ?
O2 C4 C5 114.9(7) . . ?
O2 C4 C3 128.0(8) . . ?
C7 C8 H8 119.8 . . ?
C7 C8 C9 120.5(9) . . ?
C9 C8 H8 119.8 . . ?
O4 C9 C8 127.9(9) . . ?
O4 C9 C10 115.0(8) . . ?
C8 C9 C10 117.1(9) . . ?
F10 C10 F11 107.4(9) . . ?
F10 C10 C9 112.1(8) . . ?
F11 C10 C9 108.1(9) . . ?
F12 C10 F10 108.3(10) . . ?
F12 C10 F11 108.2(8) . . ?
F12 C10 C9 112.5(9) . . ?
H16A C16 H16B 109.5 . . ?
H16A C16 H16C 109.5 . . ?
H16B C16 H16C 109.5 . . ?
C17 C16 H16A 109.5 . . ?
C17 C16 H16B 109.5 . . ?
C17 C16 H16C 109.5 . . ?
O7 C17 C16 106.3(9) . . ?
O7 C17 H17A 110.5 . . ?
O7 C17 H17B 110.5 . . ?
C16 C17 H17A 110.5 . . ?
C16 C17 H17B 110.5 . . ?
H17A C17 H17B 108.7 . . ?
C2 C3 C4 120.3(8) . . ?
C2 C3 H3 119.9 . . ?
C4 C3 H3 119.9 . . ?
C20 C19 H19 120.4 . . ?
C20 C19 C18 119.2(10) . . ?
C18 C19 H19 120.4 . . ?
C20 C21 H21 119.9 . . ?
C22 C21 C20 120.2(10) . . ?
C22 C21 H21 119.9 . . ?
C21 C22 H22 120.4 . . ?
C21 C22 C23 119.2(9) . . ?
C23 C22 H22 120.4 . . ?
O7 C18 C19 125.9(9) . . ?
O7 C18 C23 115.5(8) . . ?
C19 C18 C23 118.6(9) . . ?
H26A C26 H26B 109.5 . . ?
H26A C26 H26C 109.5 . . ?
H26B C26 H26C 109.5 . . ?
C27 C26 H26A 109.5 . . ?
C27 C26 H26B 109.5 . . ?
C27 C26 H26C 109.5 . . ?
H25A C25 H25B 109.5 . . ?
H25A C25 H25C 109.5 . . ?
H25B C25 H25C 109.5 . . ?
C27 C25 H25A 109.5 . . ?
C27 C25 H25B 109.5 . . ?
C27 C25 H25C 109.5 . . ?
N1 C27 C26 99.0(9) . . ?
C25 C27 N1 115.7(11) . . ?
C25 C27 C26 103.3(14) . . ?
C25 C27 C29 131.4(13) . 2_554 ?
C29 C27 N1 101.9(7) 2_554 . ?
C29 C27 C26 99.8(12) 2_554 . ?
C22 C23 C18 121.1(8) . . ?
C22 C23 C24 122.1(8) . . ?
C18 C23 C24 116.7(7) . . ?
N1 C24 N2 109.9(7) . 2_554 ?
N1 C24 C23 123.2(7) . . ?
N2 C24 C23 126.7(8) 2_554 . ?
O17 Dy2 O14 74.26(17) . . ?
O17 Dy2 O13 148.39(18) . . ?
O10 Dy2 O17 70.63(18) . . ?
O10 Dy2 O14 131.19(18) . . ?
O10 Dy2 O13 130.5(2) . . ?
O11 Dy2 O17 78.78(18) . . ?
O11 Dy2 O10 73.62(17) . . ?
O11 Dy2 O14 130.52(18) . . ?
O11 Dy2 O13 126.18(18) . . ?
O18 Dy2 O17 140.09(17) . . ?
O18 Dy2 O10 74.56(18) . . ?
O18 Dy2 O11 73.14(19) . . ?
O18 Dy2 O14 145.51(17) . . ?
O18 Dy2 O15 97.15(18) . . ?
O18 Dy2 O13 71.12(18) . . ?
O12 Dy2 O17 94.05(17) . . ?
O12 Dy2 O10 76.14(17) . . ?
O12 Dy2 O11 149.61(17) . . ?
O12 Dy2 O18 96.05(18) . . ?
O12 Dy2 O14 73.65(17) . . ?
O12 Dy2 O15 137.08(17) . . ?
O12 Dy2 O13 73.24(18) . . ?
O15 Dy2 O17 101.28(18) . . ?
O15 Dy2 O10 146.78(17) . . ?
O15 Dy2 O11 73.20(17) . . ?
O15 Dy2 O14 72.47(17) . . ?
O15 Dy2 O13 72.87(19) . . ?
O13 Dy2 O14 74.40(18) . . ?
N3 O17 Dy2 134.6(4) . . ?
C32 O10 Dy2 133.8(5) . . ?
C34 O11 Dy2 134.2(5) . . ?
C48 O16 C47 118.6(6) . . ?
N4 O18 Dy2 145.8(4) . . ?
C42 O14 Dy2 130.1(5) . . ?
C37 O12 Dy2 133.0(5) . . ?
C44 O15 Dy2 133.0(5) . . ?
C39 O13 Dy2 131.0(5) . . ?
O17 N3 C56 122.0(6) . . ?
O17 N3 C54 124.7(6) . . ?
C54 N3 C56 112.8(6) . . ?
O18 N4 C59 121.1(6) . . ?
O18 N4 C54 124.2(6) . 2_446 ?
C54 N4 C59 114.2(6) 2_446 . ?
O14 C42 C43 128.2(7) . . ?
O14 C42 C41 114.4(6) . . ?
C43 C42 C41 117.3(6) . . ?
O13 C39 C38 129.1(7) . . ?
O13 C39 C40 115.0(7) . . ?
C38 C39 C40 115.9(7) . . ?
F22 C35 C34 113.2(7) . . ?
F23 C35 F22 105.8(7) . . ?
F23 C35 C34 112.8(7) . . ?
F24 C35 F22 105.5(9) . . ?
F24 C35 F23 108.6(9) . . ?
F24 C35 C34 110.4(7) . . ?
C42 C43 H43 119.8 . . ?
C42 C43 C44 120.3(6) . . ?
C44 C43 H43 119.8 . . ?
C50 C51 H51 119.5 . . ?
C50 C51 C52 121.0(7) . . ?
C52 C51 H51 119.5 . . ?
H58A C58 H58B 109.5 . . ?
H58A C58 H58C 109.5 . . ?
H58B C58 H58C 109.5 . . ?
C59 C58 H58A 109.5 . . ?
C59 C58 H58B 109.5 . . ?
C59 C58 H58C 109.5 . . ?
N4 C59 C58 109.2(6) . . ?
N4 C59 C60 106.6(6) . . ?
N4 C59 C56 100.4(5) . 2_446 ?
C58 C59 C56 115.2(6) . 2_446 ?
C60 C59 C58 111.8(7) . . ?
C60 C59 C56 112.7(7) . 2_446 ?
C59 C60 H60A 109.5 . . ?
C59 C60 H60B 109.5 . . ?
C59 C60 H60C 109.5 . . ?
H60A C60 H60B 109.5 . . ?
H60A C60 H60C 109.5 . . ?
H60B C60 H60C 109.5 . . ?
F19 C31 F20 105.6(6) . . ?
F19 C31 C32 113.5(7) . . ?
F20 C31 C32 110.8(6) . . ?
F21 C31 F19 107.6(6) . . ?
F21 C31 F20 107.9(7) . . ?
F21 C31 C32 111.2(6) . . ?
O10 C32 C31 113.6(6) . . ?
O10 C32 C33 128.2(7) . . ?
C33 C32 C31 118.2(6) . . ?
C32 C33 H33 119.8 . . ?
C32 C33 C34 120.4(7) . . ?
C34 C33 H33 119.8 . . ?
O11 C34 C35 113.7(7) . . ?
O11 C34 C33 129.1(7) . . ?
C33 C34 C35 117.0(6) . . ?
F28 C41 C42 110.3(7) . . ?
F29 C41 F28 105.8(7) . . ?
F29 C41 C42 111.2(6) . . ?
F30 C41 F28 107.4(7) . . ?
F30 C41 F29 108.1(7) . . ?
F30 C41 C42 113.7(7) . . ?
O15 C44 C43 128.1(7) . . ?
O15 C44 C45 115.0(7) . . ?
C43 C44 C45 116.9(6) . . ?
F34 C45 C44 109.9(7) . . ?
F35 C45 F34 106.5(8) . . ?
F35 C45 F36 109.0(9) . . ?
F35 C45 C44 115.1(7) . . ?
F36 C45 F34 106.3(9) . . ?
F36 C45 C44 109.6(7) . . ?
F25 C36 F26 106.9(7) . . ?
F25 C36 C37 112.1(6) . . ?
F26 C36 C37 109.7(6) . . ?
F27 C36 F25 107.7(7) . . ?
F27 C36 F26 106.8(7) . . ?
F27 C36 C37 113.4(7) . . ?
O12 C37 C36 114.2(7) . . ?
O12 C37 C38 128.9(7) . . ?
C38 C37 C36 116.8(7) . . ?
C39 C38 C37 120.2(7) . . ?
C39 C38 H38 119.9 . . ?
C37 C38 H38 119.9 . . ?
F31 C40 F33 107.1(7) . . ?
F31 C40 C39 110.4(7) . . ?
F32 C40 F31 107.2(6) . . ?
F32 C40 F33 107.1(7) . . ?
F32 C40 C39 112.4(7) . . ?
F33 C40 C39 112.3(6) . . ?
H46A C46 H46B 109.5 . . ?
H46A C46 H46C 109.5 . . ?
H46B C46 H46C 109.5 . . ?
C47 C46 H46A 109.5 . . ?
C47 C46 H46B 109.5 . . ?
C47 C46 H46C 109.5 . . ?
O16 C47 C46 107.3(7) . . ?
O16 C47 H47A 110.2 . . ?
O16 C47 H47B 110.2 . . ?
C46 C47 H47A 110.2 . . ?
C46 C47 H47B 110.2 . . ?
H47A C47 H47B 108.5 . . ?
O16 C48 C49 123.4(7) . . ?
O16 C48 C53 116.9(7) . . ?
C53 C48 C49 119.6(7) . . ?
C48 C49 H49 120.7 . . ?
C50 C49 C48 118.6(8) . . ?
C50 C49 H49 120.7 . . ?
C51 C50 C49 121.0(7) . . ?
C51 C50 H50 119.5 . . ?
C49 C50 H50 119.5 . . ?
C51 C52 H52 120.3 . . ?
C51 C52 C53 119.5(8) . . ?
C53 C52 H52 120.3 . . ?
C48 C53 C54 117.8(6) . . ?
C52 C53 C48 120.1(7) . . ?
C52 C53 C54 122.0(7) . . ?
H55A C55 H55B 109.5 . . ?
H55A C55 H55C 109.5 . . ?
H55B C55 H55C 109.5 . . ?
C56 C55 H55A 109.5 . . ?
C56 C55 H55B 109.5 . . ?
C56 C55 H55C 109.5 . . ?
N3 C56 C59 99.2(5) . 2_456 ?
N3 C56 C55 110.5(6) . . ?
N3 C56 C57 106.0(6) . . ?
C55 C56 C59 115.0(6) . 2_456 ?
C55 C56 C57 111.0(7) . . ?
C57 C56 C59 114.1(7) . 2_456 ?
C56 C57 H57A 109.5 . . ?
C56 C57 H57B 109.5 . . ?
C56 C57 H57C 109.5 . . ?
H57A C57 H57B 109.5 . . ?
H57A C57 H57C 109.5 . . ?
H57B C57 H57C 109.5 . . ?
N3 C54 C53 125.7(6) . . ?
N4 C54 N3 106.2(6) 2_456 . ?
N4 C54 C53 128.1(6) 2_456 . ?
O27 Dy3 O24 75.50(18) . . ?
O27 Dy3 O19 148.47(19) . . ?
O27 Dy3 O21 69.34(17) . . ?
O23 Dy3 O27 104.31(19) . . ?
O23 Dy3 O24 72.88(18) . . ?
O23 Dy3 O19 74.13(19) . . ?
O23 Dy3 O21 144.59(18) . . ?
O24 Dy3 O19 74.03(19) . . ?
O24 Dy3 O21 133.44(18) . . ?
O20 Dy3 O27 92.82(19) . . ?
O20 Dy3 O23 140.26(19) . . ?
O20 Dy3 O24 77.33(18) . . ?
O20 Dy3 O19 72.79(19) . . ?
O20 Dy3 O22 148.79(18) . . ?
O20 Dy3 O21 74.98(18) . . ?
O22 Dy3 O27 76.22(19) . . ?
O22 Dy3 O23 70.90(18) . . ?
O22 Dy3 O24 126.0(2) . . ?
O22 Dy3 O19 129.56(19) . . ?
O22 Dy3 O21 73.81(18) . . ?
O21 Dy3 O19 129.71(19) . . ?
O26 Dy3 O27 138.13(19) . . ?
O26 Dy3 O23 93.1(2) . . ?
O26 Dy3 O24 146.36(19) . . ?
O26 Dy3 O19 72.7(2) . . ?
O26 Dy3 O20 97.51(19) . . ?
O26 Dy3 O22 74.1(2) . . ?
O26 Dy3 O21 74.44(19) . . ?
N6 O27 Dy3 134.7(5) . . ?
C67 O23 Dy3 132.8(5) . . ?
C69 O24 Dy3 130.6(5) . . ?
C62 O19 Dy3 133.2(5) . . ?
C64 O20 Dy3 134.4(5) . . ?
C74 O22 Dy3 134.5(5) . . ?
C72 O21 Dy3 132.8(5) . . ?
C78 O25 C77 117.9(6) . . ?
N5 O26 Dy3 150.0(5) . . ?
O26 N5 C84 126.0(6) . . ?
O26 N5 C86 121.1(6) . . ?
C84 N5 C86 112.2(6) . . ?
O27 N6 C89 123.2(6) . . ?
O27 N6 C84 125.4(6) . 2_445 ?
C84 N6 C89 111.0(6) 2_445 . ?
N6 C89 C90 104.9(6) . . ?
N6 C89 C88 109.5(7) . . ?
N6 C89 C86 100.1(6) . 2_445 ?
C90 C89 C88 111.0(7) . . ?
C86 C89 C90 115.2(8) 2_445 . ?
C86 C89 C88 115.0(7) 2_445 . ?
C89 C90 H90A 109.5 . . ?
C89 C90 H90B 109.5 . . ?
C89 C90 H90C 109.5 . . ?
H90A C90 H90B 109.5 . . ?
H90A C90 H90C 109.5 . . ?
H90B C90 H90C 109.5 . . ?
C89 C88 H88A 109.5 . . ?
C89 C88 H88B 109.5 . . ?
C89 C88 H88C 109.5 . . ?
H88A C88 H88B 109.5 . . ?
H88A C88 H88C 109.5 . . ?
H88B C88 H88C 109.5 . . ?
H76A C76 H76B 109.5 . . ?
H76A C76 H76C 109.5 . . ?
H76B C76 H76C 109.5 . . ?
C77 C76 H76A 109.5 . . ?
C77 C76 H76B 109.5 . . ?
C77 C76 H76C 109.5 . . ?
O24 C69 C70 113.4(7) . . ?
O24 C69 C68 127.9(7) . . ?
C68 C69 C70 118.7(7) . . ?
C81 C82 H82 120.1 . . ?
C83 C82 H82 120.1 . . ?
C83 C82 C81 119.7(7) . . ?
O21 C72 C73 129.1(7) . . ?
O21 C72 C71 113.3(7) . . ?
C73 C72 C71 117.6(7) . . ?
F40 C66 F41 106.1(9) . . ?
F40 C66 C67 111.3(8) . . ?
F41 C66 C67 113.7(8) . . ?
F42 C66 F40 103.2(11) . . ?
F42 C66 F41 109.4(10) . . ?
F42 C66 C67 112.5(8) . . ?
F37 C61 F38 106.2(7) . . ?
F37 C61 C62 113.2(8) . . ?
F38 C61 C62 110.0(7) . . ?
F39 C61 F37 108.4(8) . . ?
F39 C61 F38 106.9(8) . . ?
F39 C61 C62 111.7(7) . . ?
C81 C80 H80 119.1 . . ?
C81 C80 C79 121.8(7) . . ?
C79 C80 H80 119.1 . . ?
H87A C87 H87B 109.5 . . ?
H87A C87 H87C 109.5 . . ?
H87B C87 H87C 109.5 . . ?
C86 C87 H87A 109.5 . . ?
C86 C87 H87B 109.5 . . ?
C86 C87 H87C 109.5 . . ?
O23 C67 C66 113.2(7) . . ?
O23 C67 C68 128.7(7) . . ?
C68 C67 C66 118.1(7) . . ?
F43 C70 C69 112.3(8) . . ?
F44 C70 F43 107.5(8) . . ?
F44 C70 F45 109.1(9) . . ?
F44 C70 C69 110.8(7) . . ?
F45 C70 F43 106.7(8) . . ?
F45 C70 C69 110.3(7) . . ?
N5 C84 N6 108.6(6) . 2_455 ?
N5 C84 C83 125.3(7) . . ?
N6 C84 C83 126.1(7) 2_455 . ?
O20 C64 C63 128.0(7) . . ?
O20 C64 C65 113.3(8) . . ?
C63 C64 C65 118.4(7) . . ?
O25 C78 C79 125.2(7) . . ?
O25 C78 C83 115.8(6) . . ?
C79 C78 C83 119.0(7) . . ?
C82 C81 H81 120.3 . . ?
C80 C81 C82 119.4(8) . . ?
C80 C81 H81 120.3 . . ?
O25 C77 C76 106.7(7) . . ?
O25 C77 H77A 110.4 . . ?
O25 C77 H77B 110.4 . . ?
C76 C77 H77A 110.4 . . ?
C76 C77 H77B 110.4 . . ?
H77A C77 H77B 108.6 . . ?
C72 C73 H73 119.9 . . ?
C74 C73 C72 120.2(7) . . ?
C74 C73 H73 119.9 . . ?
C80 C79 H79 120.4 . . ?
C78 C79 C80 119.2(7) . . ?
C78 C79 H79 120.4 . . ?
C82 C83 C84 122.2(7) . . ?
C82 C83 C78 120.8(7) . . ?
C78 C83 C84 117.0(6) . . ?
N5 C86 C89 100.3(6) . 2_455 ?
N5 C86 C87 105.6(7) . . ?
N5 C86 C85 108.9(7) . . ?
C87 C86 C89 114.0(7) . 2_455 ?
C87 C86 C85 111.5(9) . . ?
C85 C86 C89 115.4(9) . 2_455 ?
F49 C71 C72 109.7(7) . . ?
F50 C71 F49 107.6(7) . . ?
F50 C71 F51 108.2(7) . . ?
F50 C71 C72 111.1(6) . . ?
F51 C71 F49 106.3(7) . . ?
F51 C71 C72 113.6(7) . . ?
C64 C63 H63 119.1 . . ?
C64 C63 C62 121.7(8) . . ?
C62 C63 H63 119.1 . . ?
C69 C68 H68 119.6 . . ?
C67 C68 C69 120.7(7) . . ?
C67 C68 H68 119.6 . . ?
O19 C62 C61 114.7(8) . . ?
O19 C62 C63 127.4(8) . . ?
C63 C62 C61 117.6(8) . . ?
C86 C85 H85A 109.5 . . ?
C86 C85 H85B 109.5 . . ?
C86 C85 H85C 109.5 . . ?
H85A C85 H85B 109.5 . . ?
H85A C85 H85C 109.5 . . ?
H85B C85 H85C 109.5 . . ?
O22 C74 C73 128.8(7) . . ?
O22 C74 C75 113.5(7) . . ?
C73 C74 C75 117.7(7) . . ?
F52 C75 F53 106.3(8) . . ?
F52 C75 F54 107.8(9) . . ?
F52 C75 C74 114.9(8) . . ?
F53 C75 F54 103.4(8) . . ?
F53 C75 C74 111.4(7) . . ?
F54 C75 C74 112.3(7) . . ?
F46 C65 C64 111.7(8) . . ?
F47 C65 F46 106.6(8) . . ?
F47 C65 C64 109.9(8) . . ?
F48 C65 F46 107.4(8) . . ?
F48 C65 F47 107.9(8) . . ?
F48 C65 C64 113.0(7) . . ?
O32 Dy4 O35 71.13(18) . . ?
O32 Dy4 O29 133.38(18) . . ?
O33 Dy4 O35 75.22(18) . . ?
O33 Dy4 O32 74.15(18) . . ?
O33 Dy4 O31 147.36(18) . . ?
O33 Dy4 O28 72.45(19) . . ?
O33 Dy4 O29 125.9(2) . . ?
O33 Dy4 O30 131.16(19) . . ?
O33 Dy4 O36 73.1(2) . . ?
O31 Dy4 O35 91.77(17) . . ?
O31 Dy4 O32 73.32(18) . . ?
O31 Dy4 O29 76.90(19) . . ?
O31 Dy4 O30 72.91(18) . . ?
O28 Dy4 O35 104.23(18) . . ?
O28 Dy4 O32 146.28(18) . . ?
O28 Dy4 O31 140.19(18) . . ?
O28 Dy4 O29 72.71(19) . . ?
O28 Dy4 O30 74.92(19) . . ?
O28 Dy4 O36 90.20(19) . . ?
O29 Dy4 O35 74.85(19) . . ?
O30 Dy4 O35 148.79(19) . . ?
O30 Dy4 O32 126.57(19) . . ?
O30 Dy4 O29 75.2(2) . . ?
O36 Dy4 O35 139.08(19) . . ?
O36 Dy4 O32 75.78(19) . . ?
O36 Dy4 O31 101.2(2) . . ?
O36 Dy4 O29 145.8(2) . . ?
O36 Dy4 O30 71.7(2) . . ?
N7 O35 Dy4 134.3(4) . . ?
C102 O32 Dy4 133.2(5) . . ?
C104 O33 Dy4 134.4(5) . . ?
C99 O31 Dy4 135.2(5) . . ?
C92 O28 Dy4 133.6(5) . . ?
C94 O29 Dy4 130.0(5) . . ?
C97 O30 Dy4 134.2(5) . . ?
C108 O34 C107 119.1(7) . . ?
N8 O36 Dy4 154.2(5) . . ?
O35 N7 C116 122.1(6) . . ?
O35 N7 C114 124.7(6) . . ?
C114 N7 C116 112.9(6) . . ?
O36 N8 C114 124.5(6) . 2_545 ?
O36 N8 C119 121.2(6) . . ?
C114 N8 C119 113.4(6) 2_545 . ?
F55 C91 F56 107.8(8) . . ?
F55 C91 F57 107.5(9) . . ?
F55 C91 C92 110.8(7) . . ?
F56 C91 C92 113.0(8) . . ?
F57 C91 F56 106.9(7) . . ?
F57 C91 C92 110.6(7) . . ?
N7 C116 C117 110.6(6) . . ?
N7 C116 C115 105.0(6) . . ?
N7 C116 C119 99.8(5) . 2 ?
C117 C116 C115 110.8(7) . . ?
C117 C116 C119 116.4(7) . 2 ?
C115 C116 C119 113.1(7) . 2 ?
O29 C94 C95 114.5(8) . . ?
O29 C94 C93 127.5(8) . . ?
C93 C94 C95 118.0(8) . . ?
C116 C117 H11A 109.5 . . ?
C116 C117 H11B 109.5 . . ?
C116 C117 H11C 109.5 . . ?
H11A C117 H11B 109.5 . . ?
H11A C117 H11C 109.5 . . ?
H11B C117 H11C 109.5 . . ?
C116 C115 H11D 109.5 . . ?
C116 C115 H11E 109.5 . . ?
C116 C115 H11F 109.5 . . ?
H11D C115 H11E 109.5 . . ?
H11D C115 H11F 109.5 . . ?
H11E C115 H11F 109.5 . . ?
C110 C109 H109 120.4 . . ?
C108 C109 H109 120.4 . . ?
C108 C109 C110 119.2(8) . . ?
F58 C95 C94 109.3(8) . . ?
F59 C95 F58 105.7(8) . . ?
F59 C95 C94 112.7(8) . . ?
F60 C95 F58 107.3(9) . . ?
F60 C95 F59 108.7(9) . . ?
F60 C95 C94 112.8(8) . . ?
C94 C93 H93 119.3 . . ?
C92 C93 C94 121.4(8) . . ?
C92 C93 H93 119.3 . . ?
H12A C120 H12B 109.5 . . ?
H12A C120 H12C 109.5 . . ?
H12B C120 H12C 109.5 . . ?
C119 C120 H12A 109.5 . . ?
C119 C120 H12B 109.5 . . ?
C119 C120 H12C 109.5 . . ?
O33 C104 C103 127.7(7) . . ?
O33 C104 C105 114.7(7) . . ?
C103 C104 C105 117.4(7) . . ?
F61 C96 F62 108.9(10) . . ?
F61 C96 F63 106.9(9) . . ?
F61 C96 C97 111.2(8) . . ?
F62 C96 C97 109.0(8) . . ?
F63 C96 F62 106.4(8) . . ?
F63 C96 C97 114.2(8) . . ?
C104 C103 H103 119.0 . . ?
C102 C103 C104 122.0(8) . . ?
C102 C103 H103 119.0 . . ?
H10A C106 H10B 109.5 . . ?
H10A C106 H10C 109.5 . . ?
H10B C106 H10C 109.5 . . ?
C107 C106 H10A 109.5 . . ?
C107 C106 H10B 109.5 . . ?
C107 C106 H10C 109.5 . . ?
F70 C105 F71 106.5(7) . . ?
F70 C105 F72 107.2(8) . . ?
F70 C105 C104 113.5(8) . . ?
F71 C105 C104 111.4(7) . . ?
F72 C105 F71 107.0(8) . . ?
F72 C105 C104 110.8(7) . . ?
F67 C101 F68 107.8(9) . . ?
F67 C101 F69 106.6(8) . . ?
F67 C101 C102 111.6(7) . . ?
F68 C101 F69 107.5(8) . . ?
F68 C101 C102 110.3(8) . . ?
F69 C101 C102 112.8(8) . . ?
O28 C92 C91 113.5(7) . . ?
O28 C92 C93 127.4(7) . . ?
C93 C92 C91 119.1(7) . . ?
C99 C98 H98 119.4 . . ?
C99 C98 C97 121.3(7) . . ?
C97 C98 H98 119.4 . . ?
N7 C114 C113 126.4(7) . . ?
N8 C114 N7 107.2(6) 2 . ?
N8 C114 C113 126.4(7) 2 . ?
C112 C113 C114 121.5(7) . . ?
C112 C113 C108 120.5(7) . . ?
C108 C113 C114 117.8(7) . . ?
C113 C112 H112 119.9 . . ?
C113 C112 C111 120.3(8) . . ?
C111 C112 H112 119.9 . . ?
O32 C102 C103 128.0(7) . . ?
O32 C102 C101 113.6(7) . . ?
C103 C102 C101 118.4(7) . . ?
C109 C110 H110 119.3 . . ?
C111 C110 C109 121.5(8) . . ?
C111 C110 H110 119.3 . . ?
O31 C99 C98 127.4(7) . . ?
O31 C99 C100 114.2(7) . . ?
C98 C99 C100 118.3(7) . . ?
C112 C111 H111 120.3 . . ?
C110 C111 C112 119.4(8) . . ?
C110 C111 H111 120.3 . . ?
O30 C97 C96 113.7(8) . . ?
O30 C97 C98 128.3(7) . . ?
C98 C97 C96 117.9(8) . . ?
F64 C100 F66 106.8(8) . . ?
F64 C100 C99 111.3(6) . . ?
F65 C100 F64 108.7(7) . . ?
F65 C100 F66 107.4(7) . . ?
F65 C100 C99 109.6(7) . . ?
F66 C100 C99 112.8(7) . . ?
N8 C119 C116 100.3(6) . 2_545 ?
N8 C119 C120 109.3(7) . . ?
N8 C119 C118 107.0(7) . . ?
C120 C119 C116 115.5(7) . 2_545 ?
C120 C119 C118 111.2(8) . . ?
C118 C119 C116 112.5(7) . 2_545 ?
O34 C107 C106 107.2(7) . . ?
O34 C107 H10D 110.3 . . ?
O34 C107 H10E 110.3 . . ?
C106 C107 H10D 110.3 . . ?
C106 C107 H10E 110.3 . . ?
H10D C107 H10E 108.5 . . ?
O34 C108 C109 124.6(8) . . ?
O34 C108 C113 116.3(7) . . ?
C109 C108 C113 119.1(7) . . ?
C119 C118 H11G 109.5 . . ?
C119 C118 H11H 109.5 . . ?
C119 C118 H11I 109.5 . . ?
H11G C118 H11H 109.5 . . ?
H11G C118 H11I 109.5 . . ?
H11H C118 H11I 109.5 . . ?
N2 C29 C30 102.0(10) . . ?
C27 C29 N2 104.1(8) 2_544 . ?
C27 C29 C30 97.1(11) 2_544 . ?
C28 C29 N2 115.3(10) . . ?
C28 C29 C27 132.5(12) . 2_544 ?
C28 C29 C30 99.5(13) . . ?
C29 C28 H28A 109.5 . . ?
C29 C28 H28B 109.5 . . ?
C29 C28 H28C 109.5 . . ?
H28A C28 H28B 109.5 . . ?
H28A C28 H28C 109.5 . . ?
H28B C28 H28C 109.5 . . ?
C29 C30 H30A 109.5 . . ?
C29 C30 H30B 109.5 . . ?
C29 C30 H30C 109.5 . . ?
H30A C30 H30B 109.5 . . ?
H30A C30 H30C 109.5 . . ?
H30B C30 H30C 109.5 . . ?
C4 O2 Dy1 132.5(5) . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Dy1 O9 N2 C24 -71.5(14) . . . 2_544 ?
Dy1 O9 N2 C29 115.8(12) . . . . ?
Dy1 O1 C2 C1 -177.2(5) . . . . ?
Dy1 O1 C2 C3 2.1(14) . . . . ?
Dy1 O8 N1 C27 113.6(9) . . . . ?
Dy1 O8 N1 C24 -69.3(12) . . . . ?
Dy1 O5 C12 C11 161.3(6) . . . . ?
Dy1 O5 C12 C13 -20.8(13) . . . . ?
Dy1 O6 C14 C13 8.1(13) . . . . ?
Dy1 O6 C14 C15 -172.5(5) . . . . ?
Dy1 O3 C7 C6 -167.5(6) . . . . ?
Dy1 O3 C7 C8 8.6(15) . . . . ?
Dy1 O4 C9 C8 -17.6(15) . . . . ?
Dy1 O4 C9 C10 160.1(7) . . . . ?
F1 C1 C2 O1 175.2(9) . . . . ?
F1 C1 C2 C3 -4.1(13) . . . . ?
F2 C1 C2 O1 -68.8(12) . . . . ?
F2 C1 C2 C3 111.9(12) . . . . ?
F3 C1 C2 O1 54.5(12) . . . . ?
F3 C1 C2 C3 -124.9(11) . . . . ?
F4 C5 C4 C3 26.7(11) . . . . ?
F4 C5 C4 O2 -152.9(8) . . . . ?
F5 C5 C4 C3 -90.6(9) . . . . ?
F5 C5 C4 O2 89.8(9) . . . . ?
F6 C5 C4 C3 149.3(9) . . . . ?
F6 C5 C4 O2 -30.3(11) . . . . ?
F13 C11 C12 O5 -41.0(11) . . . . ?
F13 C11 C12 C13 140.9(8) . . . . ?
F14 C11 C12 O5 75.3(10) . . . . ?
F14 C11 C12 C13 -102.8(9) . . . . ?
F15 C11 C12 O5 -165.4(8) . . . . ?
F15 C11 C12 C13 16.4(12) . . . . ?
O7 C18 C23 C22 174.2(9) . . . . ?
O7 C18 C23 C24 -5.3(12) . . . . ?
O9 N2 C29 C27 176.3(9) . . . 2_544 ?
O9 N2 C29 C28 -30.9(18) . . . . ?
O9 N2 C29 C30 75.8(11) . . . . ?
O1 C2 C3 C4 11.8(15) . . . . ?
O8 N1 C27 C26 81.5(12) . . . . ?
O8 N1 C27 C25 -28.0(18) . . . . ?
O8 N1 C27 C29 -176.4(9) . . . 2_554 ?
O8 N1 C24 N2 177.9(7) . . . 2_554 ?
O8 N1 C24 C23 -7.2(13) . . . . ?
O5 C12 C13 C14 2.9(14) . . . . ?
O6 C14 C15 F16 -41.8(10) . . . . ?
O6 C14 C15 F17 -162.1(7) . . . . ?
O6 C14 C15 F18 77.0(9) . . . . ?
O3 C7 C6 F7 -30.6(12) . . . . ?
O3 C7 C6 F8 86.4(10) . . . . ?
O3 C7 C6 F9 -152.7(8) . . . . ?
O3 C7 C8 C9 1.5(16) . . . . ?
O4 C9 C10 F10 154.7(9) . . . . ?
O4 C9 C10 F11 -87.0(11) . . . . ?
O4 C9 C10 F12 32.4(12) . . . . ?
C7 C8 C9 O4 3.4(16) . . . . ?
C7 C8 C9 C10 -174.2(9) . . . . ?
C20 C19 C18 O7 -176.1(10) . . . . ?
C20 C19 C18 C23 0.6(15) . . . . ?
C20 C21 C22 C23 -1.4(17) . . . . ?
C1 C2 C3 C4 -169.0(8) . . . . ?
C5 C4 C3 C2 179.7(8) . . . . ?
C5 C4 O2 Dy1 155.6(5) . . . . ?
C11 C12 C13 C14 -179.2(8) . . . . ?
C12 C13 C14 O6 3.8(13) . . . . ?
C12 C13 C14 C15 -175.6(8) . . . . ?
C13 C14 C15 F16 137.7(8) . . . . ?
C13 C14 C15 F17 17.3(11) . . . . ?
C13 C14 C15 F18 -103.5(8) . . . . ?
C6 C7 C8 C9 177.6(9) . . . . ?
C8 C7 C6 F7 152.8(9) . . . . ?
C8 C7 C6 F8 -90.3(11) . . . . ?
C8 C7 C6 F9 30.7(12) . . . . ?
C8 C9 C10 F10 -27.3(14) . . . . ?
C8 C9 C10 F11 90.9(10) . . . . ?
C8 C9 C10 F12 -149.7(9) . . . . ?
C17 O7 C18 C19 -17.1(15) . . . . ?
C17 O7 C18 C23 166.1(8) . . . . ?
C3 C4 O2 Dy1 -23.9(13) . . . . ?
C19 C20 C21 C22 -0.8(18) . . . . ?
C19 C18 C23 C22 -2.9(14) . . . . ?
C19 C18 C23 C24 177.6(8) . . . . ?
C21 C20 C19 C18 1.2(17) . . . . ?
C21 C22 C23 C18 3.3(15) . . . . ?
C21 C22 C23 C24 -177.3(9) . . . . ?
C22 C23 C24 N1 119.9(10) . . . . ?
C22 C23 C24 N2 -66.1(12) . . . 2_554 ?
C18 O7 C17 C16 -166.2(10) . . . . ?
C18 C23 C24 N1 -60.6(11) . . . . ?
C18 C23 C24 N2 113.4(10) . . . 2_554 ?
C27 N1 C24 N2 -4.8(10) . . . 2_554 ?
C27 N1 C24 C23 170.0(8) . . . . ?
C24 N1 C27 C26 -95.9(11) . . . . ?
C24 N1 C27 C25 154.5(14) . . . . ?
C24 N1 C27 C29 6.1(12) . . . 2_554 ?
C24 N2 C29 C27 2.6(13) 2_544 . . 2_544 ?
C24 N2 C29 C28 155.4(13) 2_544 . . . ?
C24 N2 C29 C30 -97.9(10) 2_544 . . . ?
Dy2 O17 N3 C56 105.0(7) . . . . ?
Dy2 O17 N3 C54 -83.1(8) . . . . ?
Dy2 O10 C32 C31 177.3(5) . . . . ?
Dy2 O10 C32 C33 -3.8(12) . . . . ?
Dy2 O11 C34 C35 165.3(5) . . . . ?
Dy2 O11 C34 C33 -11.2(13) . . . . ?
Dy2 O18 N4 C59 104.6(8) . . . . ?
Dy2 O18 N4 C54 -83.9(10) . . . 2_446 ?
Dy2 O14 C42 C43 -22.2(11) . . . . ?
Dy2 O14 C42 C41 160.1(5) . . . . ?
Dy2 O12 C37 C36 -159.6(5) . . . . ?
Dy2 O12 C37 C38 16.8(12) . . . . ?
Dy2 O15 C44 C43 18.3(12) . . . . ?
Dy2 O15 C44 C45 -160.3(6) . . . . ?
Dy2 O13 C39 C38 -18.3(13) . . . . ?
Dy2 O13 C39 C40 159.7(5) . . . . ?
F19 C31 C32 O10 -171.5(6) . . . . ?
F19 C31 C32 C33 9.5(10) . . . . ?
F20 C31 C32 O10 69.9(9) . . . . ?
F20 C31 C32 C33 -109.1(8) . . . . ?
F21 C31 C32 O10 -50.1(9) . . . . ?
F21 C31 C32 C33 131.0(7) . . . . ?
F22 C35 C34 O11 164.0(8) . . . . ?
F22 C35 C34 C33 -19.1(11) . . . . ?
F23 C35 C34 O11 43.8(10) . . . . ?
F23 C35 C34 C33 -139.3(8) . . . . ?
F24 C35 C34 O11 -77.9(10) . . . . ?
F24 C35 C34 C33 99.0(10) . . . . ?
F25 C36 C37 O12 -34.2(10) . . . . ?
F25 C36 C37 C38 148.9(8) . . . . ?
F26 C36 C37 O12 84.5(8) . . . . ?
F26 C36 C37 C38 -92.5(9) . . . . ?
F27 C36 C37 O12 -156.3(7) . . . . ?
F27 C36 C37 C38 26.8(11) . . . . ?
O17 N3 C56 C59 -161.0(6) . . . 2_456 ?
O17 N3 C56 C55 -39.9(9) . . . . ?
O17 N3 C56 C57 80.5(8) . . . . ?
O17 N3 C54 N4 170.7(6) . . . 2_456 ?
O17 N3 C54 C53 -8.2(11) . . . . ?
O10 C32 C33 C34 4.3(13) . . . . ?
O16 C48 C49 C50 -175.6(8) . . . . ?
O16 C48 C53 C52 174.2(7) . . . . ?
O16 C48 C53 C54 -3.3(10) . . . . ?
O18 N4 C59 C58 -49.1(9) . . . . ?
O18 N4 C59 C60 71.8(8) . . . . ?
O18 N4 C59 C56 -170.6(6) . . . 2_446 ?
O14 C42 C43 C44 -1.7(13) . . . . ?
O14 C42 C41 F28 70.5(8) . . . . ?
O14 C42 C41 F29 -46.5(9) . . . . ?
O14 C42 C41 F30 -168.8(7) . . . . ?
O12 C37 C38 C39 -0.9(14) . . . . ?
O15 C44 C45 F34 -45.4(11) . . . . ?
O15 C44 C45 F35 -165.7(8) . . . . ?
O15 C44 C45 F36 71.1(11) . . . . ?
O13 C39 C38 C37 2.2(14) . . . . ?
O13 C39 C40 F31 -111.2(8) . . . . ?
O13 C39 C40 F32 129.1(8) . . . . ?
O13 C39 C40 F33 8.2(10) . . . . ?
C42 C43 C44 O15 4.5(13) . . . . ?
C42 C43 C44 C45 -176.9(7) . . . . ?
C43 C42 C41 F28 -107.4(8) . . . . ?
C43 C42 C41 F29 135.5(8) . . . . ?
C43 C42 C41 F30 13.2(11) . . . . ?
C43 C44 C45 F34 135.8(9) . . . . ?
C43 C44 C45 F35 15.6(12) . . . . ?
C43 C44 C45 F36 -107.6(10) . . . . ?
C51 C52 C53 C48 4.6(11) . . . . ?
C51 C52 C53 C54 -178.0(7) . . . . ?
C31 C32 C33 C34 -176.9(7) . . . . ?
C32 C33 C34 O11 3.4(13) . . . . ?
C32 C33 C34 C35 -173.0(7) . . . . ?
C41 C42 C43 C44 176.0(7) . . . . ?
C36 C37 C38 C39 175.5(8) . . . . ?
C38 C39 C40 F31 67.1(9) . . . . ?
C38 C39 C40 F32 -52.6(10) . . . . ?
C38 C39 C40 F33 -173.5(7) . . . . ?
C40 C39 C38 C37 -175.8(7) . . . . ?
C47 O16 C48 C49 -12.3(12) . . . . ?
C47 O16 C48 C53 169.2(7) . . . . ?
C48 O16 C47 C46 -169.2(7) . . . . ?
C48 C49 C50 C51 -1.7(14) . . . . ?
C48 C53 C54 N3 -53.1(10) . . . . ?
C48 C53 C54 N4 128.2(8) . . . 2_456 ?
C49 C48 C53 C52 -4.4(12) . . . . ?
C49 C48 C53 C54 178.1(7) . . . . ?
C50 C51 C52 C53 -3.4(12) . . . . ?
C52 C51 C50 C49 2.0(14) . . . . ?
C52 C53 C54 N3 129.4(8) . . . . ?
C52 C53 C54 N4 -49.2(10) . . . 2_456 ?
C53 C48 C49 C50 2.9(13) . . . . ?
C56 N3 C54 N4 -16.8(8) . . . 2_456 ?
C56 N3 C54 C53 164.3(6) . . . . ?
C54 N3 C56 C59 26.2(7) . . . 2_456 ?
C54 N3 C56 C55 147.4(6) . . . . ?
C54 N3 C56 C57 -92.3(7) . . . . ?
C54 N4 C59 C58 138.6(7) 2_446 . . . ?
C54 N4 C59 C60 -100.5(7) 2_446 . . . ?
C54 N4 C59 C56 17.2(8) 2_446 . . 2_446 ?
Dy3 O27 N6 C89 -104.8(7) . . . . ?
Dy3 O27 N6 C84 83.8(9) . . . 2_445 ?
Dy3 O23 C67 C66 165.4(6) . . . . ?
Dy3 O23 C67 C68 -12.8(13) . . . . ?
Dy3 O24 C69 C70 -159.2(5) . . . . ?
Dy3 O24 C69 C68 23.0(12) . . . . ?
Dy3 O19 C62 C61 -160.1(5) . . . . ?
Dy3 O19 C62 C63 13.1(13) . . . . ?
Dy3 O20 C64 C63 -10.4(13) . . . . ?
Dy3 O20 C64 C65 163.5(5) . . . . ?
Dy3 O22 C74 C73 10.7(14) . . . . ?
Dy3 O22 C74 C75 -168.3(5) . . . . ?
Dy3 O21 C72 C73 6.6(12) . . . . ?
Dy3 O21 C72 C71 -174.2(5) . . . . ?
Dy3 O26 N5 C84 81.8(11) . . . . ?
Dy3 O26 N5 C86 -108.5(10) . . . . ?
F37 C61 C62 O19 -161.4(8) . . . . ?
F37 C61 C62 C63 24.7(11) . . . . ?
F38 C61 C62 O19 79.9(10) . . . . ?
F38 C61 C62 C63 -94.0(10) . . . . ?
F39 C61 C62 O19 -38.7(11) . . . . ?
F39 C61 C62 C63 147.4(8) . . . . ?
F40 C66 C67 O23 -69.1(11) . . . . ?
F40 C66 C67 C68 109.3(10) . . . . ?
F41 C66 C67 O23 171.2(9) . . . . ?
F41 C66 C67 C68 -10.4(13) . . . . ?
F42 C66 C67 O23 46.2(13) . . . . ?
F42 C66 C67 C68 -135.4(11) . . . . ?
O27 N6 C89 C90 -79.8(9) . . . . ?
O27 N6 C89 C88 39.3(10) . . . . ?
O27 N6 C89 C86 160.6(7) . . . 2_445 ?
O23 C67 C68 C69 -5.5(14) . . . . ?
O24 C69 C70 F43 168.7(8) . . . . ?
O24 C69 C70 F44 48.4(10) . . . . ?
O24 C69 C70 F45 -72.5(9) . . . . ?
O24 C69 C68 C67 -0.1(13) . . . . ?
O20 C64 C63 C62 -2.6(14) . . . . ?
O20 C64 C65 F46 152.2(8) . . . . ?
O20 C64 C65 F47 -89.6(10) . . . . ?
O20 C64 C65 F48 30.9(11) . . . . ?
O22 C74 C75 F52 -172.9(9) . . . . ?
O22 C74 C75 F53 66.2(11) . . . . ?
O22 C74 C75 F54 -49.2(11) . . . . ?
O21 C72 C73 C74 -3.3(13) . . . . ?
O21 C72 C71 F49 58.3(9) . . . . ?
O21 C72 C71 F50 -60.5(9) . . . . ?
O21 C72 C71 F51 177.2(7) . . . . ?
O25 C78 C79 C80 177.5(8) . . . . ?
O25 C78 C83 C82 -176.4(7) . . . . ?
O25 C78 C83 C84 3.9(10) . . . . ?
O26 N5 C84 N6 173.1(7) . . . 2_455 ?
O26 N5 C84 C83 -6.0(12) . . . . ?
O26 N5 C86 C89 170.0(7) . . . 2_455 ?
O26 N5 C86 C87 -71.3(9) . . . . ?
O26 N5 C86 C85 48.5(11) . . . . ?
N5 C84 C83 C82 56.2(11) . . . . ?
N5 C84 C83 C78 -124.1(8) . . . . ?
N6 C84 C83 C82 -122.7(9) 2_455 . . . ?
N6 C84 C83 C78 56.9(10) 2_455 . . . ?
C72 C73 C74 O22 -5.6(14) . . . . ?
C72 C73 C74 C75 173.3(7) . . . . ?
C66 C67 C68 C69 176.3(8) . . . . ?
C70 C69 C68 C67 -177.8(7) . . . . ?
C84 N5 C86 C89 -19.1(9) . . . 2_455 ?
C84 N5 C86 C87 99.6(8) . . . . ?
C84 N5 C86 C85 -140.6(8) . . . . ?
C84 N6 C89 C90 92.8(8) 2_445 . . . ?
C84 N6 C89 C88 -148.1(7) 2_445 . . . ?
C84 N6 C89 C86 -26.9(8) 2_445 . . 2_445 ?
C64 C63 C62 O19 1.0(14) . . . . ?
C64 C63 C62 C61 174.0(8) . . . . ?
C78 O25 C77 C76 175.1(7) . . . . ?
C81 C82 C83 C84 178.8(7) . . . . ?
C81 C82 C83 C78 -0.8(12) . . . . ?
C81 C80 C79 C78 -1.9(15) . . . . ?
C77 O25 C78 C79 -0.5(12) . . . . ?
C77 O25 C78 C83 177.0(7) . . . . ?
C73 C72 C71 F49 -122.4(8) . . . . ?
C73 C72 C71 F50 118.8(8) . . . . ?
C73 C72 C71 F51 -3.5(11) . . . . ?
C73 C74 C75 F52 8.1(13) . . . . ?
C73 C74 C75 F53 -112.9(9) . . . . ?
C73 C74 C75 F54 131.7(9) . . . . ?
C79 C80 C81 C82 2.4(14) . . . . ?
C79 C78 C83 C82 1.3(12) . . . . ?
C79 C78 C83 C84 -178.4(7) . . . . ?
C83 C82 C81 C80 -1.0(13) . . . . ?
C83 C78 C79 C80 0.1(13) . . . . ?
C86 N5 C84 N6 2.6(9) . . . 2_455 ?
C86 N5 C84 C83 -176.5(7) . . . . ?
C71 C72 C73 C74 177.5(7) . . . . ?
C63 C64 C65 F46 -33.3(12) . . . . ?
C63 C64 C65 F47 84.9(10) . . . . ?
C63 C64 C65 F48 -154.5(8) . . . . ?
C68 C69 C70 F43 -13.3(11) . . . . ?
C68 C69 C70 F44 -133.5(9) . . . . ?
C68 C69 C70 F45 105.6(9) . . . . ?
C65 C64 C63 C62 -176.3(8) . . . . ?
Dy4 O35 N7 C116 108.2(7) . . . . ?
Dy4 O35 N7 C114 -78.8(9) . . . . ?
Dy4 O32 C102 C103 -8.7(13) . . . . ?
Dy4 O32 C102 C101 172.2(5) . . . . ?
Dy4 O33 C104 C103 -2.7(12) . . . . ?
Dy4 O33 C104 C105 171.7(5) . . . . ?
Dy4 O31 C99 C98 5.9(13) . . . . ?
Dy4 O31 C99 C100 -170.2(5) . . . . ?
Dy4 O28 C92 C91 -167.8(5) . . . . ?
Dy4 O28 C92 C93 12.0(12) . . . . ?
Dy4 O29 C94 C95 159.8(6) . . . . ?
Dy4 O29 C94 C93 -23.5(13) . . . . ?
Dy4 O30 C97 C96 166.5(6) . . . . ?
Dy4 O30 C97 C98 -10.3(14) . . . . ?
Dy4 O36 N8 C114 -85.2(12) . . . 2_545 ?
Dy4 O36 N8 C119 106.6(12) . . . . ?
F55 C91 C92 O28 -52.3(10) . . . . ?
F55 C91 C92 C93 127.8(9) . . . . ?
F56 C91 C92 O28 -173.4(7) . . . . ?
F56 C91 C92 C93 6.8(11) . . . . ?
F57 C91 C92 O28 66.8(10) . . . . ?
F57 C91 C92 C93 -113.0(9) . . . . ?
F61 C96 C97 O30 41.6(12) . . . . ?
F61 C96 C97 C98 -141.3(10) . . . . ?
F62 C96 C97 O30 -78.4(10) . . . . ?
F62 C96 C97 C98 98.7(10) . . . . ?
F63 C96 C97 O30 162.7(8) . . . . ?
F63 C96 C97 C98 -20.1(12) . . . . ?
F67 C101 C102 O32 48.5(11) . . . . ?
F67 C101 C102 C103 -130.7(9) . . . . ?
F68 C101 C102 O32 -71.3(10) . . . . ?
F68 C101 C102 C103 109.5(10) . . . . ?
F69 C101 C102 O32 168.5(8) . . . . ?
F69 C101 C102 C103 -10.7(12) . . . . ?
O35 N7 C116 C117 -38.6(9) . . . . ?
O35 N7 C116 C115 81.1(8) . . . . ?
O35 N7 C116 C119 -161.7(6) . . . 2 ?
O35 N7 C114 N8 171.5(6) . . . 2 ?
O35 N7 C114 C113 -9.4(11) . . . . ?
O33 C104 C103 C102 4.7(14) . . . . ?
O33 C104 C105 F70 159.6(7) . . . . ?
O33 C104 C105 F71 39.5(10) . . . . ?
O33 C104 C105 F72 -79.6(10) . . . . ?
O31 C99 C100 F64 -39.7(10) . . . . ?
O31 C99 C100 F65 80.6(9) . . . . ?
O31 C99 C100 F66 -159.7(7) . . . . ?
O29 C94 C95 F58 80.1(10) . . . . ?
O29 C94 C95 F59 -37.1(11) . . . . ?
O29 C94 C95 F60 -160.6(9) . . . . ?
O29 C94 C93 C92 -2.0(14) . . . . ?
O36 N8 C119 C116 -173.6(6) . . . 2_545 ?
O36 N8 C119 C120 -51.7(10) . . . . ?
O36 N8 C119 C118 68.9(9) . . . . ?
N7 C114 C113 C112 126.4(8) . . . . ?
N7 C114 C113 C108 -57.0(10) . . . . ?
N8 C114 C113 C112 -54.7(11) 2 . . . ?
N8 C114 C113 C108 121.9(8) 2 . . . ?
C116 N7 C114 N8 -14.9(8) . . . 2 ?
C116 N7 C114 C113 164.2(7) . . . . ?
C94 C93 C92 O28 8.5(13) . . . . ?
C94 C93 C92 C91 -171.7(8) . . . . ?
C109 C110 C111 C112 0.5(14) . . . . ?
C95 C94 C93 C92 174.5(8) . . . . ?
C93 C94 C95 F58 -96.9(9) . . . . ?
C93 C94 C95 F59 145.9(8) . . . . ?
C93 C94 C95 F60 22.4(13) . . . . ?
C104 C103 C102 O32 1.2(14) . . . . ?
C104 C103 C102 C101 -179.8(8) . . . . ?
C103 C104 C105 F70 -25.4(11) . . . . ?
C103 C104 C105 F71 -145.6(8) . . . . ?
C103 C104 C105 F72 95.4(9) . . . . ?
C105 C104 C103 C102 -169.6(8) . . . . ?
C98 C99 C100 F64 143.9(8) . . . . ?
C98 C99 C100 F65 -95.9(9) . . . . ?
C98 C99 C100 F66 23.8(11) . . . . ?
C114 N7 C116 C117 147.6(7) . . . . ?
C114 N7 C116 C115 -92.8(8) . . . . ?
C114 N7 C116 C119 24.5(8) . . . 2 ?
C114 N8 C119 C116 17.0(8) 2_545 . . 2_545 ?
C114 N8 C119 C120 138.9(8) 2_545 . . . ?
C114 N8 C119 C118 -100.6(8) 2_545 . . . ?
C114 C113 C112 C111 179.3(7) . . . . ?
C114 C113 C108 O34 -1.5(11) . . . . ?
C114 C113 C108 C109 -179.5(7) . . . . ?
C113 C112 C111 C110 -1.6(13) . . . . ?
C112 C113 C108 O34 175.1(7) . . . . ?
C112 C113 C108 C109 -2.9(12) . . . . ?
C110 C109 C108 O34 -176.0(8) . . . . ?
C110 C109 C108 C113 1.8(13) . . . . ?
C99 C98 C97 O30 5.1(14) . . . . ?
C99 C98 C97 C96 -171.6(8) . . . . ?
C97 C98 C99 O31 -2.8(14) . . . . ?
C97 C98 C99 C100 173.1(8) . . . . ?
C107 O34 C108 C109 1.5(13) . . . . ?
C107 O34 C108 C113 -176.4(8) . . . . ?
C108 O34 C107 C106 -175.7(8) . . . . ?
C108 C109 C110 C111 -0.7(14) . . . . ?
C108 C113 C112 C111 2.8(12) . . . . ?
O2 C4 C3 C2 -0.8(14) . . . . ?

_olex2_submission_special_instructions 'No special instructions were received'
loop_
_twin_individual_id
_twin_individual_mass_fraction_refined
1 0.695(7)
2 0.305(7)

