# Copyright The Royal Society of Chemistry, 1999 # CCDC Number: 186/1334 data_clagpm _audit_creation_date 98-09-17 _audit_creation_method from_xtal_archive_file_using_CIFIO _audit_update_record ? _chemical_compound_source ? #ActaC _chemical_name_systematic ? #ActaC _chemical_name_common ? #ActaC _chemical_formula_analytical C9_H27_Ag4_Cl4_P3 #ActaC _chemical_formula_moiety ? #ActaC _chemical_formula_structural [Ag4Cl4(PMe3)3] #ActaC _chemical_formula_sum C9_H27_Ag4_Cl4_P3 #ActaC _chemical_formula_weight 801.53 #ActaC _chemical_melting_point ? #ActaC _computing_data_collection 'Enraf-Nonius Software' #ActaC _computing_cell_refinement 'Enraf-Nonius Software' #ActaC _computing_data_reduction xtal_DIFDAT_ABSORB_SORTRF_ADDREF #ActaC _computing_structure_solution xtal #ActaC _computing_structure_refinement xtal_CRYLSQ #ActaC _computing_molecular_graphics xtal #ActaC _computing_publication_material xtal_BONDLA_CIFIO #ActaC _cell_length_a 18.160(6) #ActaC _cell_length_b 18.160(6) #ActaC _cell_length_c 11.900(5) #ActaC _cell_angle_alpha 90.00000 #ActaC _cell_angle_beta 90.00000 #ActaC _cell_angle_gamma 120.0000 #ActaC _cell_volume 3399(3) #ActaC _cell_formula_units_Z 6 #ActaC _cell_measurement_temperature 293 #ActaC _cell_measurement_reflns_used 8 #ActaC _cell_measurement_theta_min 17.4 #ActaC _cell_measurement_theta_max 21.0 #ActaC _cell_special_details #ActaC ; ? ; _symmetry_cell_setting trigonal #ActaC _symmetry_space_group_name_H-M R3c #ActaC _symmetry_space_group_name_Hall R_3_-2"c #ActaC loop_ _symmetry_equiv_pos_as_xyz #ActaC +x,+y,+z -y,+x-y,+z -y,-x,1/2+z -x+y,-x,+z +x,+x-y,1/2+z -x+y,+y,1/2+z 2/3+x,1/3+y,1/3+z 1/3+x,2/3+y,2/3+z 2/3-y,1/3+x-y,1/3+z 1/3-y,2/3+x-y,2/3+z 2/3-y,1/3-x,5/6+z 1/3-y,2/3-x,1/6+z 2/3-x+y,1/3-x,1/3+z 1/3-x+y,2/3-x,2/3+z 2/3+x,1/3+x-y,5/6+z 1/3+x,2/3+x-y,1/6+z 2/3-x+y,1/3+y,5/6+z 1/3-x+y,2/3+y,1/6+z _exptl_crystal_description needle #ActaC _exptl_crystal_preparation ? _exptl_crystal_colour colourless #ActaC _exptl_crystal_size_max 0.21 #ActaC _exptl_crystal_size_mid 0.08 #ActaC _exptl_crystal_size_min 0.04 #ActaC _exptl_crystal_density_diffrn 2.35 #ActaC _exptl_crystal_density_meas ? #ActaC _exptl_crystal_density_method ? #ActaC _exptl_crystal_F_000 2292 #ActaC _exptl_absorpt_process_details ? _exptl_absorpt_coefficient_mu 4.1 #ActaC _exptl_absorpt_correction_type gaussian #ActaC _exptl_absorpt_correction_T_min 0.72 #ActaC _exptl_absorpt_correction_T_max 0.84 #ActaC _exptl_special_details #ActaC ; ? ; _diffrn_special_details ; ? ; _diffrn_ambient_temperature 293 #ActaC _diffrn_radiation_wavelength 0.71073 #ActaC _diffrn_radiation_type Mo-K\a #ActaC _diffrn_radiation_source 'sealed tube' #ActaC _diffrn_radiation_monochromator graphite #ActaC _diffrn_radiation_detector 'single counter' #ActaC _diffrn_measurement_device CAD4 #ActaC _diffrn_measurement_method 2theta-theta #ActaC _diffrn_standards_number 8 #ActaC _diffrn_standards_interval_count ? #ActaC _diffrn_standards_interval_time 3600 #ActaC _diffrn_standards_decay_% 0 #ActaC loop_ _diffrn_standard_refln_index_h #ActaC _diffrn_standard_refln_index_k #ActaC _diffrn_standard_refln_index_l #ActaC 4 4 4 -4 -4 -4 8 0 0 -8 0 0 0 8 0 0 -8 0 0 0 8 0 0 -8 loop_ _diffrn_attenuator_code _diffrn_attenuator_scale ? ? _diffrn_reflns_number 5218 #ActaC _diffrn_reflns_av_R_equivalents .065 #ActaC _diffrn_reflns_av_sigmaI/netI 0 #ActaC _diffrn_reflns_limit_h_min -12 #ActaC _diffrn_reflns_limit_h_max 0 #ActaC _diffrn_reflns_limit_k_min -12 #ActaC _diffrn_reflns_limit_k_max 23 #ActaC _diffrn_reflns_limit_l_min -11 #ActaC _diffrn_reflns_limit_l_max 15 #ActaC _diffrn_reflns_theta_min 2.24 #ActaC _diffrn_reflns_theta_max 27.5 #ActaC _diffrn_reflns_reduction_process equatorial_monochr_Lp #ActaC loop_ _atom_type_symbol #ActaC _atom_type_description #ActaC _atom_type_oxidation_number _atom_type_number_in_cell _atom_type_scat_dispersion_real #ActaC _atom_type_scat_dispersion_imag #ActaC _atom_type_scat_source #ActaC C ? 0 54 .002 .002 Int._Tables_Vol_IV_Tables_2.2B_and_2.3.1 H ? 0 162 0 0 Int._Tables_Vol_IV_Tables_2.2B_and_2.3.1 Ag ? 0 24 -1.085 1.101 Int._Tables_Vol_IV_Tables_2.2B_and_2.3.1 P ? 0 18 .09 .095 Int._Tables_Vol_IV_Tables_2.2B_and_2.3.1 Cl ? 0 24 .132 .159 Int._Tables_Vol_IV_Tables_2.2B_and_2.3.1 loop_ _atom_site_label #ActaC _atom_site_fract_x #ActaC _atom_site_fract_y #ActaC _atom_site_fract_z #ActaC _atom_site_U_iso_or_equiv #ActaC _atom_site_thermal_displace_type #ActaC _atom_site_calc_flag #ActaC _atom_site_calc_attached_atom #ActaC Ag1 .47249(6) .68167(5) .50000 .0571(6) Uani ? ? Ag2 .33330 .66666 .17591(17) .0691(10) Uani ? ? Cl1 .33337 .66653 .3917(4) .045(2) Uani ? ? Cl2 .4885(2) .7936(2) .6265(3) .0569(18) Uani ? ? P .5053(2) .58147(19) .4236(3) .0394(16) Uani ? ? C1 .5974(8) .6183(7) .3379(13) .058(7) Uani ? ? C2 .4215(8) .5056(8) .3318(12) .064(8) Uani ? ? C3 .5167(7) .5140(7) .5236(11) .057(7) Uani ? ? H1a .64757 .65640 .36050 .14000 Uiso ? ? H1b .58801 .64316 .25969 .14000 Uiso ? ? H1c .61106 .57561 .28998 .14000 Uiso ? ? H2a .41173 .54504 .27429 .15500 Uiso ? ? H2b .36656 .48452 .37469 .15500 Uiso ? ? H2c .43059 .47219 .30136 .15500 Uiso ? ? H3a .47582 .48283 .56717 .15000 Uiso ? ? H3b .57185 .55036 .56784 .15000 Uiso ? ? H3c .53797 .47265 .49073 .15000 Uiso ? ? loop_ _atom_site_aniso_label #ActaC _atom_site_aniso_U_11 #ActaC _atom_site_aniso_U_22 #ActaC _atom_site_aniso_U_33 #ActaC _atom_site_aniso_U_12 #ActaC _atom_site_aniso_U_13 #ActaC _atom_site_aniso_U_23 #ActaC Ag1 .0576(7) .0485(7) .0731(7) .0326(7) .0095(6) -.0063(6) Ag2 .0791(9) .0791(9) .0489(11) .0396(4) .00000 .00000 Cl1 .049(2) .049(2) .038(3) .0244(10) .00000 .00000 Cl2 .058(2) .051(2) .062(2) .0280(18) -.0052(17) -.0157(18) P .0392(18) .0337(18) .045(2) .0180(16) .0007(15) -.0043(15) C1 .061(9) .051(8) .080(10) .041(8) .014(8) .000(8) C2 .048(8) .050(9) .082(10) .016(7) -.008(7) -.009(7) C3 .066(9) .060(8) .055(9) .039(7) .014(7) .013(7) _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens ? _refine_special_details sfls:_F____sigma_weight______full_matrix _refine_ls_structure_factor_coef F #ActaC _refine_ls_matrix_type full #ActaC _refine_ls_weighting_scheme sigma #ActaC _refine_ls_hydrogen_treatment noref #ActaC _refine_ls_extinction_method Zachariasen #ActaC _refine_ls_extinction_coef 2301(115) #ActaC _refine_ls_extinction_expression Eq22_p292_"Cryst._Comp."_Munksgaard_1970 _refine_ls_abs_structure_details none #ActaC _refine_ls_abs_structure_Flack 0 #ActaC _refine_ls_number_reflns 530 #ActaC _refine_ls_number_parameters 61 #ActaC _refine_ls_number_restraints 0 #ActaC _refine_ls_number_constraints 0 #ActaC _refine_ls_R_factor_all .07 #ActaC _refine_ls_R_factor_obs .034 #ActaC _refine_ls_wR_factor_all .025 #ActaC _refine_ls_wR_factor_obs .021 #ActaC _refine_ls_goodness_of_fit_all 1.333 #ActaC _refine_ls_goodness_of_fit_obs 1.482 #ActaC _refine_ls_shift/esd_max .072 #ActaC _refine_ls_shift/esd_mean .004 #ActaC _refine_diff_density_min -.994 #ActaC _refine_diff_density_max 1.342 #ActaC _geom_special_details ? #ActaC loop_ _geom_bond_atom_site_label_1 #ActaC _geom_bond_atom_site_label_2 #ActaC _geom_bond_distance #ActaC _geom_bond_site_symmetry_1 #ActaC _geom_bond_site_symmetry_2 #ActaC _geom_bond_publ_flag #ActaC Ag1 Cl1 2.725(2) . . ? Ag1 Cl2 2.428(3) . . ? Ag1 P 2.362(3) . . ? Ag2 Cl1 2.568(5) . . ? Ag2 Cl2 2.665(4) . 3_664 ? Ag2 Cl2 2.666(4) . 5_564 ? Ag2 Cl2 2.665(4) . 6_554 ? P C1 1.780(13) . . ? P C2 1.819(13) . . ? P C3 1.793(13) . . ? C1 H1a .866(12) . . ? C1 H1b 1.085(14) . . ? C1 H1c 1.086(13) . . ? C2 H2a 1.069(13) . . ? C2 H2b 1.011(13) . . ? C2 H2c .790(13) . . ? C3 H3a .848(12) . . ? C3 H3b 1.027(12) . . ? C3 H3c 1.075(12) . . ? loop_ _geom_contact_atom_site_label_1 #ActaC _geom_contact_atom_site_label_2 #ActaC _geom_contact_distance #ActaC _geom_contact_site_symmetry_1 #ActaC _geom_contact_site_symmetry_2 #ActaC _geom_contact_publ_flag #ActaC Ag1 Ag2 3.1866(17) . 3_665 ? Ag1 Cl2 3.415(5) . 4_565 ? Ag2 Cl1 3.382(5) . 3_664 ? P H1a 2.361(3) . . ? P H1b 2.373(3) . . ? P H2a 2.315(3) . . ? P H2b 2.313(3) . . ? P H2c 2.281(3) . . ? P H3a 2.336(3) . . ? P H3b 2.325(3) . . ? C1 C2 2.803(17) . . ? C1 C3 2.801(19) . . ? C2 C3 2.820(19) . . ? loop_ _geom_angle_atom_site_label_1 #ActaC _geom_angle_atom_site_label_2 #ActaC _geom_angle_atom_site_label_3 #ActaC _geom_angle #ActaC _geom_angle_site_symmetry_1 #ActaC _geom_angle_site_symmetry_2 #ActaC _geom_angle_site_symmetry_3 #ActaC _geom_angle_publ_flag #ActaC Cl1 Ag1 Cl2 95.41(12) . . . ? Cl1 Ag1 P 108.59(10) . . . ? Cl2 Ag1 P 155.97(14) . . . ? Cl1 Ag2 Cl2 102.71(8) . . 3_664 ? Cl1 Ag2 Cl2 102.69(8) . . 5_564 ? Cl1 Ag2 Cl2 102.81(8) . . 6_554 ? Cl2 Ag2 Cl2 115.28(13) 3_664 . 5_564 ? Cl2 Ag2 Cl2 115.30(13) 3_664 . 6_554 ? Cl2 Ag2 Cl2 115.27(11) 5_564 . 6_554 ? Ag1 Cl1 Ag2 118.27(8) . . . ? Ag1 Cl1 Ag1 99.47(11) . . 2_665 ? Ag1 Cl1 Ag1 99.56(11) . . 4_565 ? Ag2 Cl1 Ag1 118.10(8) . . 2_665 ? Ag2 Cl1 Ag1 118.23(8) . . 4_565 ? Ag1 Cl1 Ag1 99.46(11) 2_665 . 4_565 ? Ag1 Cl2 Ag2 77.31(9) . . 3_665 ? Ag1 P C1 118.9(5) . . . ? Ag1 P C2 112.2(6) . . . ? Ag1 P C3 115.5(5) . . . ? C1 P C2 102.3(6) . . . ? C1 P C3 103.3(7) . . . ? C2 P C3 102.6(6) . . . ? P C1 H1a 122.5(13) . . . ? P C1 H1b 109.5(11) . . . ? P C1 H1c 122.7(8) . . . ? H1a C1 H1b 104.8(11) . . . ? H1a C1 H1c 102.1(14) . . . ? H1b C1 H1c 89.2(11) . . . ? P C2 H2a 103.5(8) . . . ? P C2 H2b 106.1(10) . . . ? P C2 H2c 116.2(13) . . . ? H2a C2 H2b 96.4(14) . . . ? H2a C2 H2c 112.9(15) . . . ? H2b C2 H2c 119.1(12) . . . ? P C3 H3a 120.0(14) . . . ? P C3 H3b 108.0(8) . . . ? P C3 H3c 116.1(10) . . . ? H3a C3 H3b 111.3(14) . . . ? H3a C3 H3c 104.9(12) . . . ? H3b C3 H3c 93.4(12) . . . ? loop_ _geom_torsion_atom_site_label_1 #ActaC _geom_torsion_atom_site_label_2 #ActaC _geom_torsion_atom_site_label_3 #ActaC _geom_torsion_atom_site_label_4 #ActaC _geom_torsion #ActaC _geom_torsion_site_symmetry_1 #ActaC _geom_torsion_site_symmetry_2 #ActaC _geom_torsion_site_symmetry_3 #ActaC _geom_torsion_site_symmetry_4 #ActaC _geom_torsion_publ_flag #ActaC ? ? ? ? ? ? ? ? ? ? _reflns_limit_h_min -12 _reflns_limit_h_max 0 _reflns_limit_k_min -12 _reflns_limit_k_max 23 _reflns_limit_l_min -11 _reflns_limit_l_max 15 _reflns_number_total 878 #ActaC _reflns_number_observed 530 #ActaC _reflns_observed_criterion refl_observed_if_I____>3.000_sigma(I___) _reflns_d_resolution_high .77 _reflns_d_resolution_low 9.064 loop_ _reflns_scale_group_code _reflns_scale_meas_F ? 12.7704 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_meas _refln_F_calc _refln_F_sigma _refln_observed_status _refln_scale_group_code -12 17 10 38.046 43.639 11.807 < 1 -12 18 9 29.485 26.280 11.306 < 1 -12 19 8 59.116 54.024 8.017 o 1 -12 20 7 33.832 27.401 11.558 < 1 -12 21 6 46.212 41.938 10.522 < 1 -12 22 5 51.939 50.850 9.980 < 1 -11 13 12 19.764 18.086 9.605 < 1 -11 14 11 36.568 24.783 11.085 < 1 -11 15 10 26.060 20.791 10.416 < 1 -11 16 9 25.823 28.638 10.369 < 1 -11 17 8 44.641 54.169 9.917 < 1 -11 18 7 31.687 49.793 11.048 < 1 -11 19 6 69.892 58.868 5.927 o 1 -11 19 9 39.765 25.800 11.376 < 1 -11 20 5 26.663 32.708 10.373 < 1 -11 20 8 36.775 35.687 11.782 < 1 -11 21 4 40.171 29.049 10.192 < 1 -11 21 7 35.489 47.119 13.773 < 1 -11 22 0 84.861 81.113 7.327 o 1 -11 22 3 24.908 32.210 10.232 < 1 -11 23 -1 30.721 27.206 11.219 < 1 -11 23 2 43.372 40.401 11.119 < 1 -10 12 11 36.138 39.408 11.005 < 1 -10 13 10 45.560 35.732 8.941 < 1 -10 14 9 55.779 55.660 6.942 o 1 -10 14 12 29.780 16.163 11.300 < 1 -10 15 8 37.775 37.194 9.781 < 1 -10 15 11 36.166 42.348 11.639 < 1 -10 16 7 52.441 41.729 6.555 o 1 -10 16 10 69.496 62.104 6.458 o 1 -10 17 6 30.561 30.066 10.015 < 1 -10 17 9 59.359 51.235 6.612 o 1 -10 18 5 54.543 53.288 6.384 o 1 -10 18 8 42.683 36.971 10.515 < 1 -10 19 4 99.907 95.912 4.303 o 1 -10 19 7 37.671 43.198 10.751 < 1 -10 20 0 20.765 29.821 10.118 < 1 -10 20 3 36.533 42.411 10.286 < 1 -10 20 6 26.074 4.120 10.342 < 1 -10 21 -1 36.378 46.101 10.822 < 1 -10 21 2 64.062 52.672 6.286 o 1 -10 21 5 61.460 57.104 6.958 o 1 -10 22 -2 31.499 27.791 11.072 < 1 -10 22 1 39.806 47.816 10.857 < 1 -10 22 4 25.910 6.276 10.840 < 1 -10 23 -3 46.343 55.096 11.500 < 1 -10 23 0 46.889 41.534 10.511 < 1 -10 23 3 35.554 45.649 11.920 < 1 -9 11 10 93.436 88.723 4.344 o 1 -9 12 9 61.089 61.652 5.918 o 1 -9 12 12 24.092 29.371 10.436 < 1 -9 13 8 105.736 101.245 3.742 o 1 -9 13 11 58.019 67.130 7.494 o 1 -9 14 7 75.286 73.020 4.817 o 1 -9 14 10 27.638 41.096 10.646 < 1 -9 15 6 100.018 102.684 3.746 o 1 -9 15 9 32.058 32.260 10.613 < 1 -9 16 5 65.061 76.177 5.313 o 1 -9 16 8 49.392 43.365 7.400 o 1 -9 16 11 27.718 28.554 11.042 < 1 -9 17 4 66.037 67.454 5.201 o 1 -9 17 7 28.382 17.272 10.065 < 1 -9 17 10 54.763 57.427 8.243 o 1 -9 18 0 65.763 62.232 6.855 o 1 -9 18 3 46.167 29.837 6.810 o 1 -9 18 6 22.327 20.602 9.710 < 1 -9 18 9 45.546 32.213 10.287 < 1 -9 19 -1 24.023 16.285 9.398 < 1 -9 19 2 63.473 55.783 5.692 o 1 -9 19 5 23.300 27.016 9.597 < 1 -9 19 8 63.682 53.527 7.113 o 1 -9 20 -2 29.920 21.314 10.060 < 1 -9 20 1 39.571 39.479 9.819 < 1 -9 20 4 75.757 77.675 5.582 o 1 -9 20 7 31.039 20.962 11.048 < 1 -9 21 -3 78.031 66.506 5.561 o 1 -9 21 0 21.189 28.970 8.771 < 1 -9 21 3 42.566 54.154 10.516 < 1 -9 21 6 45.058 65.576 11.369 < 1 -9 22 -4 41.175 16.806 10.614 < 1 -9 22 -1 49.939 60.441 9.408 < 1 -9 22 2 58.225 36.971 7.012 o 1 -9 22 5 28.290 34.826 11.227 < 1 -9 23 -2 28.015 8.878 11.036 < 1 -9 23 1 58.363 54.299 8.063 o 1 -8 10 9 48.190 37.774 5.923 o 1 -8 11 8 118.189 116.755 3.111 o 1 -8 11 11 21.613 15.030 9.206 < 1 -8 12 7 69.178 70.543 4.371 o 1 -8 12 10 23.960 17.720 9.809 < 1 -8 12 13 37.055 21.548 11.788 < 1 -8 13 6 139.742 142.903 2.728 o 1 -8 13 9 80.123 72.838 4.810 o 1 -8 13 12 50.696 36.302 9.594 < 1 -8 14 5 124.770 123.059 2.842 o 1 -8 14 8 86.851 92.372 4.632 o 1 -8 14 11 56.294 41.338 7.258 o 1 -8 15 4 120.598 119.587 2.945 o 1 -8 15 7 41.610 32.250 8.277 < 1 -8 15 10 72.670 78.373 6.101 o 1 -8 16 0 145.047 146.306 3.848 o 1 -8 16 3 104.502 105.368 3.279 o 1 -8 16 6 130.037 131.619 3.352 o 1 -8 16 9 19.401 15.966 9.181 < 1 -8 17 -1 47.093 48.715 6.347 o 1 -8 17 2 37.096 31.384 8.765 < 1 -8 17 5 48.157 45.594 6.808 o 1 -8 17 8 23.789 26.769 9.946 < 1 -8 18 -2 105.478 109.437 3.772 o 1 -8 18 1 14.802 20.948 7.924 < 1 -8 18 4 30.011 26.259 10.073 < 1 -8 18 7 27.743 37.464 10.412 < 1 -8 19 -3 20.674 13.136 9.379 < 1 -8 19 0 119.072 118.089 3.624 o 1 -8 19 3 39.556 36.259 9.084 < 1 -8 19 6 78.689 79.147 5.439 o 1 -8 19 9 24.928 19.014 10.815 < 1 -8 20 -4 80.683 84.144 5.433 o 1 -8 20 -1 24.010 34.053 9.591 < 1 -8 20 2 89.304 94.212 4.765 o 1 -8 20 5 48.959 43.034 8.810 < 1 -8 20 8 73.096 64.982 6.716 o 1 -8 21 -5 68.785 57.849 6.480 o 1 -8 21 -2 34.435 33.251 10.750 < 1 -8 21 1 54.216 44.330 7.154 o 1 -8 21 4 35.035 35.183 11.119 < 1 -8 22 -3 22.450 40.773 9.798 < 1 -8 22 0 37.658 31.123 10.543 < 1 -8 22 3 20.902 21.083 9.290 < 1 -8 23 -1 21.777 15.926 9.572 < 1 -8 23 2 22.293 22.934 9.935 < 1 -7 0 14 31.561 10.667 13.268 < 1 -7 9 8 129.539 130.406 2.749 o 1 -7 10 7 108.248 115.272 2.933 o 1 -7 10 10 20.711 3.576 8.612 < 1 -7 11 6 166.458 170.291 2.387 o 1 -7 11 9 64.593 70.310 5.205 o 1 -7 11 12 22.650 14.343 9.385 < 1 -7 12 5 116.526 116.721 2.715 o 1 -7 12 8 155.601 151.364 2.823 o 1 -7 12 11 20.808 20.234 9.090 < 1 -7 13 4 20.794 26.778 8.336 < 1 -7 13 7 86.177 79.171 3.585 o 1 -7 13 10 35.990 43.209 10.368 < 1 -7 14 0 208.826 204.308 3.045 o 1 -7 14 3 28.497 36.250 8.232 < 1 -7 14 6 125.085 125.963 3.056 o 1 -7 14 9 31.271 14.037 10.188 < 1 -7 14 12 20.027 29.915 8.467 < 1 -7 15 -1 97.082 97.584 3.176 o 1 -7 15 2 114.834 121.894 3.035 o 1 -7 15 5 58.130 58.430 5.150 o 1 -7 15 8 80.024 77.966 4.951 o 1 -7 15 11 44.625 37.105 10.079 < 1 -7 16 -2 86.824 91.713 3.701 o 1 -7 16 1 74.759 80.326 4.134 o 1 -7 16 4 58.502 55.142 5.065 o 1 -7 16 7 70.205 65.225 5.051 o 1 -7 16 10 27.644 38.565 10.585 < 1 -7 17 -3 65.909 76.081 5.483 o 1 -7 17 0 132.770 135.959 2.984 o 1 -7 17 3 99.818 103.404 3.717 o 1 -7 17 6 89.583 86.640 4.356 o 1 -7 17 9 58.614 45.395 7.002 o 1 -7 18 -4 107.610 104.419 3.786 o 1 -7 18 -1 37.691 33.432 9.237 < 1 -7 18 2 120.222 123.532 3.448 o 1 -7 18 5 65.811 57.860 5.737 o 1 -7 18 8 81.803 75.309 5.470 o 1 -7 19 -5 29.057 25.688 10.577 < 1 -7 19 -2 136.138 133.727 3.422 o 1 -7 19 1 23.550 38.899 9.626 < 1 -7 19 4 57.142 53.998 6.712 o 1 -7 19 7 28.410 28.546 10.650 < 1 -7 20 -6 47.447 39.030 9.435 < 1 -7 20 -3 45.744 46.035 9.077 < 1 -7 20 0 41.039 57.558 10.023 < 1 -7 20 3 24.511 2.355 9.924 < 1 -7 20 6 59.610 62.059 7.135 o 1 -7 21 -4 29.084 35.960 10.980 < 1 -7 21 -1 18.084 11.093 8.265 < 1 -7 21 2 34.086 22.196 10.454 < 1 -7 21 5 24.937 12.276 10.523 < 1 -7 22 -2 25.904 15.179 10.713 < 1 -7 22 1 28.051 12.209 10.876 < 1 -7 22 4 42.294 12.712 10.839 < 1 -7 23 0 46.076 43.133 17.928 < 1 -6 -2 14 32.437 26.478 11.743 < 1 -6 -1 13 36.266 36.303 10.793 < 1 -6 0 12 54.099 48.807 11.372 < 1 -6 8 7 60.144 60.372 3.863 o 1 -6 9 6 140.725 140.013 2.373 o 1 -6 9 9 100.005 100.998 3.519 o 1 -6 10 5 156.039 157.708 2.215 o 1 -6 10 8 189.086 188.107 2.430 o 1 -6 10 11 94.202 98.305 4.416 o 1 -6 11 4 176.016 175.743 2.156 o 1 -6 11 7 96.958 103.627 3.332 o 1 -6 11 10 47.513 47.506 6.916 o 1 -6 11 13 37.160 43.457 11.626 < 1 -6 12 0 15.917 7.619 7.323 < 1 -6 12 3 87.454 81.912 2.930 o 1 -6 12 6 80.765 83.427 3.595 o 1 -6 12 9 54.570 51.262 6.243 o 1 -6 12 12 31.366 18.194 10.937 < 1 -6 13 -1 46.601 48.270 4.441 o 1 -6 13 2 55.828 51.240 4.106 o 1 -6 13 5 83.283 78.845 3.457 o 1 -6 13 8 19.887 13.139 8.181 < 1 -6 13 11 19.166 7.943 9.181 < 1 -6 14 -2 96.001 93.899 3.070 o 1 -6 14 1 65.457 68.875 3.972 o 1 -6 14 4 105.379 106.683 3.047 o 1 -6 14 7 80.869 71.125 4.350 o 1 -6 14 10 37.497 43.116 10.545 < 1 -6 15 -3 152.613 149.992 2.560 o 1 -6 15 0 230.496 225.677 2.273 o 1 -6 15 3 153.476 151.474 2.576 o 1 -6 15 6 86.605 85.915 4.133 o 1 -6 15 9 36.213 44.428 10.724 < 1 -6 16 -4 89.068 93.641 3.914 o 1 -6 16 -1 110.827 113.832 3.051 o 1 -6 16 2 58.833 56.956 4.746 o 1 -6 16 5 120.549 116.560 3.304 o 1 -6 16 8 67.294 63.081 5.708 o 1 -6 16 11 31.708 29.855 11.511 < 1 -6 17 -5 56.431 48.373 6.284 o 1 -6 17 -2 67.331 66.937 4.976 o 1 -6 17 1 80.909 85.606 4.183 o 1 -6 17 4 31.411 32.279 9.776 < 1 -6 17 7 68.875 65.769 5.754 o 1 -6 17 10 47.625 23.076 9.637 < 1 -6 18 -6 38.407 29.602 9.917 < 1 -6 18 -3 38.268 28.184 9.380 < 1 -6 18 0 109.225 109.741 3.527 o 1 -6 18 3 22.788 43.651 8.724 < 1 -6 18 6 65.303 64.026 5.949 o 1 -6 18 9 29.826 27.433 11.083 < 1 -6 19 -7 26.767 16.909 10.480 < 1 -6 19 -4 98.754 90.792 4.164 o 1 -6 19 -1 40.310 43.733 9.180 < 1 -6 19 2 42.505 63.295 9.968 < 1 -6 19 5 34.951 42.726 10.331 < 1 -6 19 8 61.450 57.370 7.552 o 1 -6 20 -5 22.088 33.211 9.668 < 1 -6 20 -2 35.523 45.605 10.709 < 1 -6 20 1 60.571 41.555 5.962 o 1 -6 20 4 36.581 37.345 10.419 < 1 -6 20 7 37.814 13.516 11.062 < 1 -6 21 -6 37.857 40.083 11.662 < 1 -6 21 -3 36.045 38.367 11.005 < 1 -6 21 0 65.156 59.789 6.174 o 1 -6 21 3 50.275 48.518 8.954 < 1 -6 21 6 26.233 14.379 11.098 < 1 -6 22 -4 26.191 26.829 10.946 < 1 -6 22 -1 51.607 46.948 9.751 < 1 -6 22 2 22.316 29.522 9.731 < 1 -5 -4 14 32.163 47.763 11.641 < 1 -5 -3 13 31.776 16.700 11.142 < 1 -5 -2 12 32.238 30.388 10.453 < 1 -5 -1 11 29.807 36.416 10.064 < 1 -5 -1 14 51.593 40.246 9.262 < 1 -5 0 10 52.716 44.180 7.448 o 1 -5 7 6 147.215 148.622 2.131 o 1 -5 8 5 242.861 247.035 1.925 o 1 -5 8 8 103.796 101.920 2.994 o 1 -5 9 4 204.192 205.366 1.847 o 1 -5 9 7 152.917 147.899 2.423 o 1 -5 9 10 86.587 84.238 4.182 o 1 -5 10 0 87.308 85.775 3.231 o 1 -5 10 3 318.140 318.926 2.004 o 1 -5 10 6 71.575 79.124 3.550 o 1 -5 10 9 72.070 88.325 4.864 o 1 -5 10 12 22.079 5.491 9.827 < 1 -5 11 -1 244.679 245.733 1.924 o 1 -5 11 2 158.426 156.818 2.023 o 1 -5 11 5 127.792 130.628 2.520 o 1 -5 11 8 117.726 119.729 3.195 o 1 -5 11 11 42.538 44.369 9.489 < 1 -5 12 -2 241.260 244.407 2.044 o 1 -5 12 1 83.229 82.526 2.870 o 1 -5 12 4 159.994 160.768 2.290 o 1 -5 12 7 24.176 28.933 8.845 < 1 -5 12 10 78.145 72.467 4.993 o 1 -5 12 13 19.906 11.543 9.726 < 1 -5 13 -3 109.269 111.125 2.871 o 1 -5 13 0 196.259 205.682 2.146 o 1 -5 13 3 209.571 213.056 2.196 o 1 -5 13 6 65.916 61.129 4.556 o 1 -5 13 9 41.587 45.801 9.169 < 1 -5 13 12 37.907 15.809 11.061 < 1 -5 14 -4 45.685 38.562 5.254 o 1 -5 14 -1 152.810 147.361 2.344 o 1 -5 14 2 91.846 97.142 3.083 o 1 -5 14 5 174.474 176.519 2.574 o 1 -5 14 8 26.121 13.702 9.717 < 1 -5 14 11 55.052 51.157 7.806 o 1 -5 15 -5 62.487 62.522 5.013 o 1 -5 15 -2 63.622 68.845 4.270 o 1 -5 15 1 149.693 150.734 2.508 o 1 -5 15 4 115.716 111.531 2.989 o 1 -5 15 7 26.968 38.479 9.533 < 1 -5 15 10 25.172 21.940 10.215 < 1 -5 16 -6 37.803 29.472 9.508 < 1 -5 16 -3 28.472 38.125 9.368 < 1 -5 16 0 76.396 72.259 3.955 o 1 -5 16 3 97.409 99.824 3.460 o 1 -5 16 6 30.408 29.371 9.828 < 1 -5 16 9 37.833 22.949 10.566 < 1 -5 17 -7 28.477 36.211 10.478 < 1 -5 17 -4 51.827 60.222 6.827 o 1 -5 17 -1 104.180 104.899 3.559 o 1 -5 17 2 91.357 97.474 3.972 o 1 -5 17 5 39.573 46.035 9.620 < 1 -5 17 8 40.273 37.356 10.102 < 1 -5 18 -8 55.614 36.103 7.375 o 1 -5 18 -5 42.507 36.269 8.626 < 1 -5 18 -2 60.845 58.114 5.777 o 1 -5 18 1 99.094 90.663 3.869 o 1 -5 18 4 60.204 57.147 6.177 o 1 -5 18 7 19.664 18.196 8.757 < 1 -5 19 -6 45.083 53.450 10.036 < 1 -5 19 -3 21.714 5.103 8.889 < 1 -5 19 0 39.801 53.728 9.984 < 1 -5 19 3 40.713 30.909 9.252 < 1 -5 19 6 33.908 20.945 10.788 < 1 -5 20 -7 34.920 39.997 11.934 < 1 -5 20 -4 35.294 37.421 10.855 < 1 -5 20 -1 39.115 34.202 10.061 < 1 -5 20 2 39.381 36.469 10.032 < 1 -5 20 5 45.350 43.346 9.948 < 1 -5 21 -5 62.308 64.446 7.709 o 1 -5 21 -2 60.846 66.371 7.223 o 1 -5 21 1 50.212 60.192 9.371 < 1 -5 21 4 50.442 37.441 9.590 < 1 -5 22 -3 60.205 69.064 8.359 o 1 -5 22 0 65.834 49.465 6.996 o 1 -5 22 3 32.313 42.488 11.351 < 1 -4 -5 13 36.500 39.334 11.298 < 1 -4 -4 12 25.246 12.855 10.157 < 1 -4 -3 11 59.338 62.802 5.685 o 1 -4 -3 14 54.617 53.426 7.879 o 1 -4 -2 10 66.442 71.014 4.794 o 1 -4 -2 13 44.063 31.728 9.639 < 1 -4 -1 9 128.127 131.841 2.807 o 1 -4 -1 12 34.891 45.145 10.442 < 1 -4 -1 15 34.852 5.591 11.771 < 1 -4 0 8 262.196 261.497 3.037 o 1 -4 0 14 74.852 60.052 7.842 o 1 -4 6 5 414.325 419.637 2.156 o 1 -4 7 4 208.916 212.196 1.745 o 1 -4 7 7 35.933 42.587 7.143 < 1 -4 8 0 14.825 4.444 6.314 < 1 -4 8 3 121.667 117.482 1.826 o 1 -4 8 6 100.602 104.430 2.578 o 1 -4 8 9 56.490 50.314 4.825 o 1 -4 9 -1 216.061 218.165 1.706 o 1 -4 9 2 186.403 187.741 1.765 o 1 -4 9 5 271.105 275.872 2.027 o 1 -4 9 8 105.527 105.278 3.134 o 1 -4 9 11 58.192 56.365 6.386 o 1 -4 10 -2 320.280 324.419 1.968 o 1 -4 10 1 289.749 286.646 1.888 o 1 -4 10 4 256.702 259.904 1.996 o 1 -4 10 7 83.829 83.114 3.527 o 1 -4 10 10 108.668 101.797 3.672 o 1 -4 10 13 61.729 44.386 6.872 o 1 -4 11 -3 51.154 53.364 4.113 o 1 -4 11 0 163.145 166.747 1.955 o 1 -4 11 3 143.464 138.907 2.173 o 1 -4 11 6 95.223 93.783 3.126 o 1 -4 11 9 38.925 17.511 8.562 < 1 -4 11 12 27.664 7.678 10.521 < 1 -4 12 -4 107.195 110.785 2.766 o 1 -4 12 -1 59.375 62.774 3.688 o 1 -4 12 2 131.748 132.336 2.340 o 1 -4 12 5 122.210 125.767 2.743 o 1 -4 12 8 90.595 88.937 3.848 o 1 -4 12 11 30.593 23.286 10.574 < 1 -4 13 -5 190.609 188.211 2.397 o 1 -4 13 -2 159.572 160.160 2.351 o 1 -4 13 1 118.676 123.303 2.626 o 1 -4 13 4 183.048 181.182 2.331 o 1 -4 13 7 108.852 103.684 3.275 o 1 -4 13 10 56.918 47.611 6.470 o 1 -4 14 -6 50.629 59.269 6.291 o 1 -4 14 -3 185.332 187.090 2.410 o 1 -4 14 0 152.650 154.918 2.362 o 1 -4 14 3 124.292 122.426 2.790 o 1 -4 14 6 37.913 36.873 8.306 < 1 -4 14 9 62.482 65.389 6.229 o 1 -4 14 12 27.947 2.269 11.158 < 1 -4 15 -7 26.245 32.732 9.810 < 1 -4 15 -4 66.049 70.171 4.485 o 1 -4 15 -1 86.684 79.488 3.498 o 1 -4 15 2 20.147 14.229 8.008 < 1 -4 15 5 24.272 18.960 8.858 < 1 -4 15 8 29.518 9.020 10.123 < 1 -4 15 11 41.842 26.186 10.835 < 1 -4 16 -8 25.872 31.936 10.153 < 1 -4 16 -5 54.120 53.491 6.557 o 1 -4 16 -2 64.120 66.190 4.850 o 1 -4 16 1 36.673 52.663 8.801 < 1 -4 16 4 102.547 103.909 3.598 o 1 -4 16 7 28.963 39.102 10.308 < 1 -4 16 10 42.455 41.103 10.835 < 1 -4 17 -9 44.279 43.455 10.859 < 1 -4 17 -6 30.323 16.294 10.376 < 1 -4 17 -3 140.982 139.820 3.192 o 1 -4 17 0 85.477 85.956 4.157 o 1 -4 17 3 89.447 91.481 4.280 o 1 -4 17 6 17.227 10.085 8.410 < 1 -4 17 9 27.080 34.708 10.862 < 1 -4 18 -7 30.188 47.767 10.889 < 1 -4 18 -4 39.107 34.530 9.755 < 1 -4 18 -1 88.987 87.146 4.314 o 1 -4 18 2 74.409 70.818 5.042 o 1 -4 18 5 31.178 24.709 10.265 < 1 -4 18 8 35.851 24.063 11.008 < 1 -4 19 -8 33.582 34.184 11.663 < 1 -4 19 -5 37.979 45.052 10.651 < 1 -4 19 -2 88.950 89.878 4.721 o 1 -4 19 1 20.286 13.777 8.945 < 1 -4 19 4 52.465 54.419 8.913 < 1 -4 19 7 25.509 20.923 10.622 < 1 -4 20 -6 56.289 43.778 8.055 o 1 -4 20 -3 56.469 47.730 7.064 o 1 -4 20 0 52.823 53.848 7.422 o 1 -4 20 3 88.933 83.612 4.906 o 1 -4 20 6 25.381 26.700 10.477 < 1 -4 21 -4 38.897 16.901 11.104 < 1 -4 21 -1 59.079 68.671 7.729 o 1 -4 21 2 31.339 16.146 11.089 < 1 -4 21 5 32.656 38.724 12.301 < 1 -4 22 1 55.925 44.991 8.032 o 1 -3 -7 13 23.719 17.865 9.683 < 1 -3 -6 12 27.958 39.769 10.349 < 1 -3 -5 11 39.031 49.410 9.705 < 1 -3 -5 14 40.093 36.469 11.265 < 1 -3 -4 10 96.729 90.970 3.532 o 1 -3 -4 13 28.176 36.828 10.538 < 1 -3 -3 9 113.616 112.198 3.003 o 1 -3 -3 12 25.776 18.976 9.756 < 1 -3 -2 8 271.028 274.244 2.158 o 1 -3 -2 11 139.933 137.590 3.022 o 1 -3 -2 14 43.441 49.316 10.682 < 1 -3 -1 7 150.673 149.026 2.071 o 1 -3 -1 10 93.695 87.112 3.434 o 1 -3 -1 13 25.246 45.078 10.210 < 1 -3 0 6 280.359 278.405 2.670 o 1 -3 0 12 46.196 38.559 10.534 < 1 -3 5 4 387.681 394.615 1.969 o 1 -3 6 0 31.767 27.444 4.242 o 1 -3 6 3 470.102 473.866 2.171 o 1 -3 6 6 114.627 111.111 2.163 o 1 -3 7 -1 179.715 183.072 1.564 o 1 -3 7 2 245.501 243.685 1.656 o 1 -3 7 5 31.503 35.164 6.330 < 1 -3 7 8 98.239 98.182 3.047 o 1 -3 8 -2 186.309 184.197 1.695 o 1 -3 8 1 136.828 136.595 1.680 o 1 -3 8 4 159.611 159.346 1.865 o 1 -3 8 7 73.789 78.819 3.419 o 1 -3 8 10 87.422 90.245 4.014 o 1 -3 9 -3 308.870 313.643 1.944 o 1 -3 9 0 301.149 297.269 1.849 o 1 -3 9 3 312.796 311.501 1.958 o 1 -3 9 6 45.015 50.206 5.306 o 1 -3 9 9 53.399 52.436 5.686 o 1 -3 9 12 31.070 33.055 10.738 < 1 -3 10 -4 114.225 118.874 2.387 o 1 -3 10 -1 145.979 148.053 1.893 o 1 -3 10 2 170.560 170.955 1.886 o 1 -3 10 5 205.816 207.316 2.076 o 1 -3 10 8 82.717 82.213 3.820 o 1 -3 10 11 25.993 29.254 9.779 < 1 -3 11 -5 54.682 50.360 4.347 o 1 -3 11 -2 206.784 206.827 1.971 o 1 -3 11 1 36.542 34.783 5.132 o 1 -3 11 4 201.759 199.516 2.102 o 1 -3 11 7 94.186 94.984 3.394 o 1 -3 11 10 95.819 96.751 4.314 o 1 -3 11 13 36.718 16.487 11.655 < 1 -3 12 -6 47.725 54.578 5.693 o 1 -3 12 -3 183.084 184.908 2.158 o 1 -3 12 0 188.127 193.131 2.077 o 1 -3 12 3 165.334 166.549 2.251 o 1 -3 12 6 27.065 40.569 8.930 < 1 -3 12 9 31.365 41.951 10.133 < 1 -3 12 12 22.225 36.138 9.905 < 1 -3 13 -7 128.117 129.680 3.170 o 1 -3 13 -4 108.745 107.164 2.880 o 1 -3 13 -1 159.585 166.111 2.373 o 1 -3 13 2 132.406 133.038 2.491 o 1 -3 13 5 201.582 201.294 2.379 o 1 -3 13 8 34.263 32.221 9.760 < 1 -3 13 11 56.638 47.374 7.376 o 1 -3 14 -8 76.932 70.429 4.792 o 1 -3 14 -5 113.994 116.444 3.082 o 1 -3 14 -2 154.002 151.894 2.481 o 1 -3 14 1 98.523 98.562 3.114 o 1 -3 14 4 78.250 84.071 4.042 o 1 -3 14 7 66.445 69.307 5.343 o 1 -3 14 10 54.146 48.574 7.376 o 1 -3 15 -9 28.577 32.546 10.469 < 1 -3 15 -6 76.446 66.852 4.565 o 1 -3 15 -3 122.334 116.478 2.915 o 1 -3 15 0 80.195 75.194 3.704 o 1 -3 15 3 97.761 101.617 3.438 o 1 -3 15 6 57.130 55.226 6.056 o 1 -3 15 9 16.130 10.713 7.562 < 1 -3 16 -10 23.594 12.071 10.156 < 1 -3 16 -7 54.783 48.580 7.421 o 1 -3 16 -4 28.880 24.354 9.719 < 1 -3 16 -1 149.754 142.314 2.679 o 1 -3 16 2 72.767 70.951 4.219 o 1 -3 16 5 100.053 85.022 3.737 o 1 -3 16 8 33.247 14.257 10.519 < 1 -3 17 -8 56.560 60.932 7.667 o 1 -3 17 -5 98.648 95.612 4.232 o 1 -3 17 -2 60.176 55.702 5.892 o 1 -3 17 1 129.499 129.966 3.295 o 1 -3 17 4 106.536 111.845 3.940 o 1 -3 17 7 44.230 44.344 9.497 < 1 -3 18 -6 36.515 45.666 11.171 < 1 -3 18 -3 41.355 48.356 9.997 < 1 -3 18 0 76.058 70.295 4.940 o 1 -3 18 3 55.624 53.728 6.475 o 1 -3 18 6 27.304 34.182 10.159 < 1 -3 19 -7 42.354 32.150 10.863 < 1 -3 19 -4 27.952 36.950 10.618 < 1 -3 19 -1 31.421 39.279 10.512 < 1 -3 19 2 28.141 31.460 10.188 < 1 -3 19 5 23.202 24.564 10.099 < 1 -3 20 -5 34.910 30.936 11.638 < 1 -3 20 -2 26.291 24.839 10.328 < 1 -3 20 1 44.201 35.770 9.787 < 1 -3 20 4 60.122 43.084 6.806 o 1 -3 21 -3 57.371 49.281 7.977 o 1 -3 21 0 51.342 48.131 9.446 < 1 -3 21 3 26.062 21.324 10.520 < 1 -2 -9 13 25.466 25.618 10.814 < 1 -2 -8 12 50.554 38.214 8.880 < 1 -2 -7 11 57.127 56.901 6.211 o 1 -2 -7 14 24.548 5.854 10.341 < 1 -2 -6 10 56.743 47.817 5.487 o 1 -2 -6 13 60.795 53.571 6.746 o 1 -2 -5 9 66.872 56.595 4.221 o 1 -2 -5 12 40.177 18.581 9.774 < 1 -2 -4 8 156.418 160.591 2.395 o 1 -2 -4 11 67.542 62.826 5.232 o 1 -2 -4 14 59.194 62.300 7.376 o 1 -2 -3 7 196.794 198.384 2.015 o 1 -2 -3 10 76.473 78.116 4.191 o 1 -2 -3 13 60.238 64.424 6.793 o 1 -2 -2 6 158.651 155.594 1.869 o 1 -2 -2 9 118.663 114.237 2.840 o 1 -2 -2 12 29.843 31.149 10.198 < 1 -2 -2 15 60.520 22.083 7.648 o 1 -2 -1 5 181.902 180.607 1.673 o 1 -2 -1 8 144.734 145.464 2.283 o 1 -2 -1 11 77.892 81.601 4.371 o 1 -2 -1 14 58.778 59.547 7.317 o 1 -2 0 4 214.733 211.865 2.160 o 1 -2 0 10 167.560 172.837 3.554 o 1 -2 4 0 89.449 81.234 1.869 o 1 -2 4 3 618.893 626.878 2.491 o 1 -2 5 -1 401.447 400.493 1.818 o 1 -2 5 2 322.712 327.620 1.688 o 1 -2 5 5 409.718 408.956 2.124 o 1 -2 6 -2 362.237 361.128 1.841 o 1 -2 6 1 373.732 361.264 1.831 o 1 -2 6 4 282.426 282.118 1.795 o 1 -2 6 7 203.107 199.790 2.059 o 1 -2 7 -3 149.647 153.726 1.682 o 1 -2 7 0 310.710 311.718 1.741 o 1 -2 7 3 265.483 265.253 1.764 o 1 -2 7 6 143.636 141.420 2.132 o 1 -2 7 9 53.304 61.884 5.351 o 1 -2 8 -4 196.873 201.289 1.848 o 1 -2 8 -1 190.735 192.534 1.651 o 1 -2 8 2 105.199 107.048 1.989 o 1 -2 8 5 116.545 116.409 2.290 o 1 -2 8 8 60.721 61.583 4.277 o 1 -2 8 11 64.660 65.697 5.556 o 1 -2 9 -5 146.892 146.666 2.160 o 1 -2 9 -2 133.208 132.627 1.906 o 1 -2 9 1 179.533 179.841 1.778 o 1 -2 9 4 225.229 222.220 1.892 o 1 -2 9 7 32.941 50.624 8.215 < 1 -2 9 10 84.840 92.829 4.407 o 1 -2 9 13 35.383 34.568 11.271 < 1 -2 10 -6 153.995 154.177 2.382 o 1 -2 10 -3 124.489 122.550 2.172 o 1 -2 10 0 256.431 251.595 1.891 o 1 -2 10 3 79.489 75.816 2.793 o 1 -2 10 6 93.103 94.042 3.034 o 1 -2 10 9 72.973 70.556 4.552 o 1 -2 10 12 37.421 31.854 10.514 < 1 -2 11 -7 19.840 39.588 7.664 < 1 -2 11 -4 86.057 86.150 3.139 o 1 -2 11 -1 153.554 155.713 2.130 o 1 -2 11 2 213.462 214.737 2.014 o 1 -2 11 5 96.361 97.250 3.040 o 1 -2 11 8 63.091 64.108 5.216 o 1 -2 11 11 59.176 44.913 6.465 o 1 -2 12 -8 102.218 98.431 3.734 o 1 -2 12 -5 149.368 146.936 2.564 o 1 -2 12 -2 107.301 107.986 2.697 o 1 -2 12 1 154.350 151.924 2.164 o 1 -2 12 4 151.466 146.894 2.390 o 1 -2 12 7 111.804 106.054 3.203 o 1 -2 12 10 52.087 53.403 6.645 o 1 -2 13 -9 57.791 62.749 6.692 o 1 -2 13 -6 30.327 38.795 9.026 < 1 -2 13 -3 121.195 124.785 2.793 o 1 -2 13 0 87.440 92.015 3.105 o 1 -2 13 3 146.948 146.215 2.493 o 1 -2 13 6 61.240 64.834 5.021 o 1 -2 13 9 47.023 55.442 8.874 < 1 -2 13 12 21.766 18.092 9.811 < 1 -2 14 -10 46.933 37.558 9.280 < 1 -2 14 -7 71.608 72.036 5.317 o 1 -2 14 -4 97.857 105.341 3.345 o 1 -2 14 -1 88.717 90.234 3.469 o 1 -2 14 2 106.997 101.619 3.007 o 1 -2 14 5 64.730 63.152 4.735 o 1 -2 14 8 25.362 12.510 9.823 < 1 -2 14 11 57.098 38.579 7.510 o 1 -2 15 -11 27.249 32.406 11.085 < 1 -2 15 -8 69.397 65.541 5.662 o 1 -2 15 -5 143.289 140.842 3.084 o 1 -2 15 -2 81.116 77.535 4.026 o 1 -2 15 1 105.968 104.001 3.245 o 1 -2 15 4 51.736 50.585 5.920 o 1 -2 15 7 51.227 49.672 6.744 o 1 -2 15 10 32.620 41.589 11.250 < 1 -2 16 -9 43.637 46.755 10.882 < 1 -2 16 -6 84.364 79.380 4.883 o 1 -2 16 -3 146.282 137.369 2.985 o 1 -2 16 0 163.151 166.734 2.796 o 1 -2 16 3 146.080 140.886 2.938 o 1 -2 16 6 38.418 41.975 9.956 < 1 -2 16 9 43.049 52.302 10.585 < 1 -2 17 -7 63.977 67.809 6.856 o 1 -2 17 -4 20.003 10.773 9.384 < 1 -2 17 -1 48.932 55.003 7.052 o 1 -2 17 2 59.882 64.961 5.780 o 1 -2 17 5 93.643 93.029 4.467 o 1 -2 17 8 28.589 13.579 10.540 < 1 -2 18 -8 35.474 12.575 11.574 < 1 -2 18 -5 52.760 26.769 6.894 o 1 -2 18 -2 32.875 2.752 10.210 < 1 -2 18 1 56.683 55.832 6.316 o 1 -2 18 4 47.687 46.230 8.569 < 1 -2 18 7 42.157 44.390 10.672 < 1 -2 19 -6 29.614 16.553 11.177 < 1 -2 19 -3 36.964 35.635 10.662 < 1 -2 19 0 25.760 26.674 9.950 < 1 -2 19 3 22.887 13.411 9.779 < 1 -2 19 6 23.325 25.183 9.880 < 1 -2 20 -4 72.040 71.485 6.705 o 1 -2 20 -1 26.712 18.786 10.418 < 1 -2 20 2 32.291 35.478 10.980 < 1 -2 20 5 45.274 36.162 10.266 < 1 -2 21 -2 33.385 26.046 11.526 < 1 -2 21 1 25.613 19.776 10.689 < 1 -1 -10 12 24.655 12.601 10.231 < 1 -1 -9 11 22.738 7.382 9.668 < 1 -1 -8 10 123.758 126.900 3.386 o 1 -1 -8 13 23.524 21.127 10.214 < 1 -1 -7 9 38.619 26.912 7.659 < 1 -1 -7 12 73.546 75.330 5.782 o 1 -1 -6 8 114.002 109.179 2.725 o 1 -1 -6 11 64.737 63.681 5.510 o 1 -1 -6 14 23.675 16.827 10.134 < 1 -1 -5 7 156.931 157.359 2.163 o 1 -1 -5 10 103.645 99.480 3.246 o 1 -1 -5 13 21.050 14.595 9.081 < 1 -1 -4 6 107.729 108.542 2.117 o 1 -1 -4 9 74.131 75.730 3.761 o 1 -1 -4 12 20.860 18.089 8.934 < 1 -1 -4 15 23.708 25.175 10.369 < 1 -1 -3 5 300.189 299.056 1.818 o 1 -1 -3 8 214.291 210.293 2.122 o 1 -1 -3 11 60.071 52.755 5.257 o 1 -1 -3 14 69.948 65.906 6.430 o 1 -1 -2 4 240.365 239.645 1.571 o 1 -1 -2 7 63.168 63.450 3.255 o 1 -1 -2 10 140.976 142.760 2.785 o 1 -1 -2 13 62.227 50.070 6.241 o 1 -1 -1 3 132.943 131.288 1.331 o 1 -1 -1 6 303.774 303.335 1.882 o 1 -1 -1 9 29.813 18.430 7.866 < 1 -1 -1 12 31.348 52.859 10.058 < 1 -1 -1 15 32.914 7.490 11.678 < 1 -1 0 2 477.734 474.740 2.677 o 1 -1 0 8 231.637 233.824 2.920 o 1 -1 0 14 38.975 18.230 12.762 < 1 -1 2 0 619.815 621.801 2.908 o 1 -1 3 -1 318.230 314.931 1.482 o 1 -1 3 2 352.387 347.212 1.654 o 1 -1 4 -2 297.659 293.975 1.538 o 1 -1 4 1 263.667 257.185 1.413 o 1 -1 4 4 318.337 318.524 1.776 o 1 -1 5 -3 341.578 340.938 1.791 o 1 -1 5 0 319.318 319.425 1.635 o 1 -1 5 3 185.176 184.780 1.528 o 1 -1 5 6 155.497 152.763 1.952 o 1 -1 6 -4 183.124 187.720 1.701 o 1 -1 6 -1 97.611 98.427 1.692 o 1 -1 6 2 266.241 265.133 1.633 o 1 -1 6 5 224.756 225.772 1.832 o 1 -1 6 8 116.637 114.340 2.728 o 1 -1 7 -5 69.434 67.913 2.851 o 1 -1 7 -2 303.204 304.355 1.783 o 1 -1 7 1 153.051 154.415 1.611 o 1 -1 7 4 86.124 90.090 2.453 o 1 -1 7 7 25.994 34.330 7.890 < 1 -1 7 10 128.893 130.502 3.022 o 1 -1 8 -6 289.793 298.771 2.110 o 1 -1 8 -3 208.307 206.478 1.774 o 1 -1 8 0 675.110 685.595 2.797 o 1 -1 8 3 261.129 256.673 1.858 o 1 -1 8 6 262.894 262.915 2.071 o 1 -1 8 9 23.121 31.009 8.685 < 1 -1 8 12 85.738 74.280 4.993 o 1 -1 9 -7 28.505 12.069 7.980 < 1 -1 9 -4 138.249 139.900 2.117 o 1 -1 9 -1 86.828 87.945 2.369 o 1 -1 9 2 228.547 226.267 1.834 o 1 -1 9 5 26.505 32.603 7.846 < 1 -1 9 8 71.191 73.191 4.225 o 1 -1 9 11 35.625 47.675 10.187 < 1 -1 9 14 30.600 8.435 11.700 < 1 -1 10 -8 30.706 34.148 8.783 < 1 -1 10 -5 54.325 66.286 4.324 o 1 -1 10 -2 49.503 51.908 3.721 o 1 -1 10 1 85.914 89.309 2.608 o 1 -1 10 4 79.435 82.887 3.042 o 1 -1 10 7 37.132 42.728 7.378 < 1 -1 10 10 77.289 65.759 4.625 o 1 -1 10 13 28.023 27.210 11.047 < 1 -1 11 -9 24.892 34.751 9.447 < 1 -1 11 -6 90.045 84.904 3.291 o 1 -1 11 -3 115.398 114.406 2.471 o 1 -1 11 0 217.221 214.065 1.987 o 1 -1 11 3 113.961 109.751 2.562 o 1 -1 11 6 155.783 161.671 2.521 o 1 -1 11 9 37.489 39.651 9.421 < 1 -1 11 12 18.905 14.251 8.218 < 1 -1 12 -10 55.345 63.857 7.710 o 1 -1 12 -7 65.931 67.807 4.905 o 1 -1 12 -4 246.116 248.694 2.279 o 1 -1 12 -1 87.254 85.307 3.013 o 1 -1 12 2 204.809 202.524 2.136 o 1 -1 12 5 65.672 69.058 4.328 o 1 -1 12 8 185.249 183.670 2.745 o 1 -1 12 11 35.080 21.397 10.961 < 1 -1 13 -11 22.432 22.903 9.655 < 1 -1 13 -8 62.140 62.018 5.882 o 1 -1 13 -5 96.076 98.037 3.423 o 1 -1 13 -2 143.440 146.023 2.521 o 1 -1 13 1 120.983 123.434 2.685 o 1 -1 13 4 83.079 72.545 3.398 o 1 -1 13 7 28.443 35.224 9.655 < 1 -1 13 10 36.945 17.580 10.458 < 1 -1 14 -9 34.461 2.535 10.589 < 1 -1 14 -6 64.590 61.140 5.287 o 1 -1 14 -3 99.553 103.255 3.404 o 1 -1 14 0 78.474 70.510 3.671 o 1 -1 14 3 72.332 71.402 4.179 o 1 -1 14 6 77.659 86.015 4.665 o 1 -1 14 9 33.711 41.828 10.617 < 1 -1 15 -10 27.430 16.751 11.034 < 1 -1 15 -7 56.656 55.100 6.578 o 1 -1 15 -4 78.367 75.812 4.341 o 1 -1 15 -1 53.338 46.925 5.672 o 1 -1 15 2 55.304 61.857 5.559 o 1 -1 15 5 79.529 81.672 4.534 o 1 -1 15 8 55.813 55.531 7.064 o 1 -1 16 -8 53.028 50.967 7.826 o 1 -1 16 -5 92.194 84.835 4.288 o 1 -1 16 -2 79.375 75.505 4.276 o 1 -1 16 1 75.476 60.181 4.295 o 1 -1 16 4 55.027 64.062 6.454 o 1 -1 16 7 52.771 53.479 7.466 o 1 -1 16 10 28.595 36.202 11.174 < 1 -1 17 -9 46.676 29.298 10.517 < 1 -1 17 -6 45.295 42.214 9.695 < 1 -1 17 -3 25.388 15.074 9.889 < 1 -1 17 0 74.617 85.479 5.019 o 1 -1 17 3 85.921 84.925 4.499 o 1 -1 17 6 46.412 38.719 8.992 < 1 -1 17 9 24.495 21.549 10.121 < 1 -1 18 -7 21.034 22.999 9.826 < 1 -1 18 -4 67.956 48.567 6.136 o 1 -1 18 -1 35.424 17.171 10.156 < 1 -1 18 2 77.430 67.774 5.025 o 1 -1 18 5 26.178 34.369 10.259 < 1 -1 19 -5 35.411 26.229 11.439 < 1 -1 19 -2 57.024 69.053 7.811 o 1 -1 19 1 35.795 37.706 10.576 < 1 -1 19 4 60.958 61.671 7.118 o 1 -1 20 -3 40.258 2.549 10.793 < 1 -1 20 0 35.565 54.098 11.518 < 1 -1 20 3 29.332 27.012 11.064 < 1 0 -12 12 21.135 11.036 10.733 < 1 0 -10 10 155.075 153.007 4.455 o 1 0 -9 12 64.942 65.104 9.269 o 1 0 -8 8 166.169 168.704 3.546 o 1 0 -8 14 32.424 5.053 13.140 < 1 0 -7 10 92.272 101.123 5.426 o 1 0 -6 6 253.318 256.664 2.761 o 1 0 -6 12 25.396 33.385 10.576 < 1 0 -5 8 34.433 43.917 9.611 < 1 0 -5 14 43.357 63.632 13.786 < 1 0 -4 4 396.769 393.511 2.791 o 1 0 -4 10 141.179 138.132 3.938 o 1 0 -3 6 37.876 43.804 6.626 < 1 0 -3 12 37.322 28.476 12.253 < 1 0 -2 2 383.366 380.050 2.417 o 1 0 -2 8 39.140 17.991 7.509 < 1 0 -2 14 31.161 39.545 12.339 < 1 0 -1 4 309.173 306.182 2.337 o 1 0 -1 10 146.347 147.020 3.607 o 1 0 0 6 532.906 523.412 5.867 o 1 0 0 12 165.035 156.145 6.801 o 1 0 3 0 45.118 40.495 2.776 o 1 0 4 2 543.586 535.897 3.196 o 1 0 5 -2 96.145 100.335 2.384 o 1 0 5 4 114.829 106.814 2.572 o 1 0 6 0 580.081 570.595 3.442 o 1 0 6 6 313.461 314.551 2.904 o 1 0 7 -4 279.059 278.228 2.644 o 1 0 7 2 317.171 316.509 2.594 o 1 0 7 8 227.418 226.872 3.180 o 1 0 8 -2 318.465 324.017 2.702 o 1 0 8 4 273.742 281.208 2.763 o 1 0 8 10 127.396 125.306 4.629 o 1 0 9 -6 176.964 179.550 3.229 o 1 0 9 0 362.252 365.265 2.917 o 1 0 9 6 245.065 248.069 3.056 o 1 0 9 12 38.122 22.206 12.650 < 1 0 10 -4 158.067 157.636 3.110 o 1 0 10 2 215.684 222.102 2.845 o 1 0 10 8 137.824 134.999 4.048 o 1 0 11 -8 148.108 154.920 4.250 o 1 0 11 -2 264.205 263.271 2.945 o 1 0 11 4 130.756 129.693 3.335 o 1 0 11 10 65.957 50.495 7.861 o 1 0 12 -6 137.556 137.700 3.960 o 1 0 12 0 206.959 214.457 3.093 o 1 0 12 6 165.777 165.959 3.624 o 1 0 12 12 50.699 57.370 13.961 < 1 0 13 -10 27.836 33.242 11.335 < 1 0 13 -4 125.370 122.169 4.043 o 1 0 13 2 98.527 92.433 4.289 o 1 0 13 8 104.129 93.165 5.432 o 1 0 14 -8 33.380 23.399 12.000 < 1 0 14 -2 93.383 90.638 5.042 o 1 0 14 4 28.347 29.031 10.891 < 1 0 14 10 72.287 79.899 8.458 o 1 0 15 -6 113.566 112.855 5.344 o 1 0 15 0 167.196 156.105 3.721 o 1 0 15 6 80.464 75.548 6.711 o 1 0 16 -4 40.585 53.109 12.222 < 1 0 16 2 48.749 52.634 10.598 < 1 0 16 8 28.363 19.922 12.025 < 1 0 17 -8 55.679 27.589 12.458 < 1 0 17 -2 61.837 46.249 7.769 o 1 0 17 4 42.871 9.812 11.544 < 1 0 18 -6 36.455 57.118 13.532 < 1 0 18 0 104.147 96.969 5.705 o 1 0 18 6 87.481 86.483 7.646 o 1 0 19 -4 90.045 92.184 7.941 o 1 0 19 2 96.712 93.785 6.666 o 1 0 20 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