Supplementary Material (ESI) for Dalton Transactions This journal is (c) The Royal Society of Chemistry 2001 Table S3a. Anisotropic displacement parameters for Cu(glygly)(OH2)2.H2O at 293 K from spherical atom model. The anisotropic displacement factor exponent takes the form: -2.(pi)^2[h^2.a*^2.U11 + ... + 2.k.l.b*.c*.U23] Atom U11 U22 U33 U12 U13 U23 CuA 0.0194(2) 0.0320(2) 0.0209(2) -0.0005(1) 0.0068(1) 0.0046(1) O1A 0.0222(9) 0.045(1) 0.0233(9) 0.0034(8) 0.0075(7) 0.0101(8) O2A 0.024(1) 0.062(2) 0.026(1) 0.0034(9) 0.0039(8) 0.013(1) O3A 0.028(1) 0.043(1) 0.0223(9) -0.0008(9) 0.0081(8) 0.0104(9) O4A 0.022(1) 0.039(1) 0.036(1) 0.0025(9) 0.0093(9) 0.0130(9) O5A 0.025(1) 0.029(1) 0.042(1) 0.003(1) 0.0068(9) 0.0022(9) O6A 0.043(1) 0.043(1) 0.035(1) 0.010(1) 0.018(1) 0.015(1) N1A 0.022(1) 0.031(1) 0.022(1) -0.0004(9) 0.0067(8) 0.0030(9) N2A 0.024(1) 0.051(2) 0.032(1) -0.004(1) 0.005(1) 0.010(1) C1A 0.025(1) 0.030(1) 0.021(1) 0.003(1) 0.007(1) 0.001(1) C2A 0.019(1) 0.029(2) 0.024(1) 0.002(1) 0.007(1) 0.004(1) C3A 0.025(1) 0.025(1) 0.021(1) -0.000(1) 0.007(1) 0.000(1) C4A 0.029(2) 0.043(2) 0.023(1) -0.001(1) 0.002(1) 0.007(1) CuB 0.0230(2) 0.0340(2) 0.0180(2) -0.0032(1) 0.0052(1) 0.0024(1) O1B 0.0248(9) 0.047(1) 0.0198(9) -0.0079(9) 0.0059(7) 0.0033(8) O2B 0.028(1) 0.055(1) 0.0207(9) -0.0099(9) 0.0023(8) 0.0031(9) O3B 0.027(1) 0.049(1) 0.031(1) -0.0113(9) 0.0121(8) -0.0067(9) O4B 0.038(1) 0.038(1) 0.022(1) -0.009(1) 0.0029(9) 0.008(1) O5B 0.050(1) 0.040(2) 0.033(1) 0.014(1) 0.015(1) 0.007(1) O6B 0.028(1) 0.056(1) 0.032(1) -0.006(1) 0.0102(9) -0.006(1) N1B 0.023(1) 0.032(1) 0.020(1) -0.0016(9) 0.0051(8) 0.0022(9) N2B 0.028(1) 0.038(2) 0.020(1) 0.002(1) 0.0039(9) 0.001(1) C1B 0.023(1) 0.027(1) 0.021(1) 0.001(1) 0.006(1) 0.001(1) C2B 0.024(1) 0.030(2) 0.020(1) -0.001(1) 0.008(1) 0.003(1) C3B 0.022(1) 0.026(1) 0.026(1) 0.001(1) 0.008(1) -0.004(1) C4B 0.022(1) 0.042(2) 0.026(1) 0.001(1) 0.002(1) -0.007(1)