# Electronic Supplementary Material (ESI) for Dalton Transactions # This journal is © The Royal Society of Chemistry 2012 data_global _journal_name_full 'Dalton Trans.' _journal_coden_cambridge 0222 _journal_year ? _journal_volume ? _journal_page_first ? _publ_contact_author_name 'Stefano Zacchini' _publ_contact_author_email stefano.zacchini@unibo.it loop_ _publ_author_name S.Zacchini C.Femoni M.Iapalucci G.Longoni S.Fedi 'F.F.de Biani' data_p21c _database_code_depnum_ccdc_archive 'CCDC 846297' #TrackingRef '- ni17_P21C.CIF' _audit_creation_method SHELXL-97 _chemical_name_systematic ; ? ; _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'C63.96 H88 N4 Ni16.96 O25.30' _chemical_formula_weight 2313.46 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ni Ni 0.3393 1.1124 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _symmetry_cell_setting Monoclinic _symmetry_space_group_name_H-M P2(1)/c loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' _cell_length_a 38.2056(15) _cell_length_b 14.5054(6) _cell_length_c 22.9812(9) _cell_angle_alpha 90.00 _cell_angle_beta 93.9820(10) _cell_angle_gamma 90.00 _cell_volume 12705.1(9) _cell_formula_units_Z 6 _cell_measurement_temperature 293(2) _cell_measurement_reflns_used 6783 _cell_measurement_theta_min 2.298 _cell_measurement_theta_max 20.589 _exptl_crystal_description prism _exptl_crystal_colour black _exptl_crystal_size_max 0.23 _exptl_crystal_size_mid 0.16 _exptl_crystal_size_min 0.12 _exptl_crystal_density_meas ? _exptl_crystal_density_diffrn 1.814 _exptl_crystal_density_method 'not measured' _exptl_crystal_F_000 7062 _exptl_absorpt_coefficient_mu 3.740 _exptl_absorpt_correction_type empirical _exptl_absorpt_correction_T_min 0.4800 _exptl_absorpt_correction_T_max 0.6624 _exptl_absorpt_process_details ? _exptl_special_details ; ? ; _diffrn_ambient_temperature 293(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_radiation_source 'fine-focus sealed tube' _diffrn_radiation_monochromator graphite _diffrn_measurement_device_type 'CCD area detector' _diffrn_measurement_method 'phi and omega scans' _diffrn_detector_area_resol_mean ? _diffrn_standards_number ? _diffrn_standards_interval_count ? _diffrn_standards_interval_time ? _diffrn_standards_decay_% ? _diffrn_reflns_number 120260 _diffrn_reflns_av_R_equivalents 0.0825 _diffrn_reflns_av_sigmaI/netI 0.0664 _diffrn_reflns_limit_h_min -45 _diffrn_reflns_limit_h_max 45 _diffrn_reflns_limit_k_min -17 _diffrn_reflns_limit_k_max 17 _diffrn_reflns_limit_l_min -27 _diffrn_reflns_limit_l_max 27 _diffrn_reflns_theta_min 1.50 _diffrn_reflns_theta_max 25.03 _reflns_number_total 22439 _reflns_number_gt 11198 _reflns_threshold_expression >2sigma(I) _computing_data_collection ? _computing_cell_refinement ? _computing_data_reduction ? _computing_structure_solution 'SHELXS-97 (Sheldrick, 1990)' _computing_structure_refinement 'SHELXL-97 (Sheldrick, 1997)' _computing_molecular_graphics ? _computing_publication_material ? _refine_special_details ; Refinement of F^2^ against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F^2^, conventional R-factors R are based on F, with F set to zero for negative F^2^. The threshold expression of F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F^2^ are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger. ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'calc w=1/[\s^2^(Fo^2^)+(0.1332P)^2^+53.4584P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef ? _refine_ls_number_reflns 22439 _refine_ls_number_parameters 1268 _refine_ls_number_restraints 2731 _refine_ls_R_factor_all 0.1564 _refine_ls_R_factor_gt 0.0791 _refine_ls_wR_factor_ref 0.2728 _refine_ls_wR_factor_gt 0.2182 _refine_ls_goodness_of_fit_ref 1.036 _refine_ls_restrained_S_all 1.148 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_symmetry_multiplicity _atom_site_calc_flag _atom_site_refinement_flags _atom_site_disorder_assembly _atom_site_disorder_group Ni1 Ni 0.28614(4) 0.37989(10) 0.18726(7) 0.0530(4) Uani 1 1 d . A . Ni2 Ni 0.34009(4) 0.30271(11) 0.17901(8) 0.0595(4) Uani 1 1 d . . . Ni3 Ni 0.34506(5) 0.37118(11) 0.06145(8) 0.0624(5) Uani 1 1 d U A . Ni4 Ni 0.29253(5) 0.45615(11) 0.06414(7) 0.0595(4) Uani 1 1 d . . . Ni5 Ni 0.26728(5) 0.47918(12) 0.26366(8) 0.0635(5) Uani 1 1 d U . . Ni6 Ni 0.32419(4) 0.41348(12) 0.29224(7) 0.0606(4) Uani 1 1 d . A . Ni7 Ni 0.38105(5) 0.38561(13) 0.25782(8) 0.0694(5) Uani 1 1 d U A . Ni8 Ni 0.37770(4) 0.44053(12) 0.15307(7) 0.0607(4) Uani 1 1 d U A . Ni9 Ni 0.39125(5) 0.50005(14) 0.05201(9) 0.0800(6) Uani 1 1 d U . . Ni10 Ni 0.33811(6) 0.57308(13) 0.01528(8) 0.0753(5) Uani 1 1 d U A . Ni11 Ni 0.28023(6) 0.61841(12) 0.04589(8) 0.0743(5) Uani 1 1 d U A . Ni12 Ni 0.27705(4) 0.54542(11) 0.15359(7) 0.0559(4) Uani 1 1 d . A . Ni13 Ni 0.36221(5) 0.55485(13) 0.24198(9) 0.0713(5) Uani 1 1 d U . . Ni14 Ni 0.30582(5) 0.62120(11) 0.24792(8) 0.0633(5) Uani 1 1 d U A . Ni15 Ni 0.31580(5) 0.68952(11) 0.13512(8) 0.0647(5) Uani 1 1 d . . . Ni16 Ni 0.37078(5) 0.62253(12) 0.12198(9) 0.0714(5) Uani 1 1 d . A . C1 C 0.2462(4) 0.3696(10) 0.2313(7) 0.076(3) Uani 1 1 d U A . C2 C 0.2941(4) 0.2586(9) 0.1641(6) 0.065(3) Uani 1 1 d U A . C3 C 0.2994(4) 0.3399(10) 0.0313(6) 0.072(3) Uani 1 1 d U A . C4 C 0.2591(5) 0.5129(12) 0.0115(8) 0.098(4) Uani 1 1 d U A . C5 C 0.2341(4) 0.5315(10) 0.2962(6) 0.0720(17) Uani 1 1 d U B . C6 C 0.2929(4) 0.4086(12) 0.3424(7) 0.087(3) Uani 1 1 d U A . C7 C 0.3614(5) 0.3609(13) 0.3330(7) 0.098(4) Uani 1 1 d U . . C8 C 0.4196(4) 0.3319(12) 0.2736(7) 0.0834(18) Uani 1 1 d U . . C9 C 0.4323(5) 0.4685(12) 0.0364(7) 0.0902(18) Uani 1 1 d U A . C10 C 0.3756(6) 0.5452(15) -0.0239(10) 0.120(5) Uani 1 1 d U A . C11 C 0.3133(5) 0.6346(10) -0.0347(7) 0.0824(18) Uani 1 1 d U . . C12 C 0.2532(5) 0.7058(11) 0.0295(7) 0.0866(18) Uani 1 1 d U . . C13 C 0.2559(4) 0.4250(11) 0.1183(7) 0.083(3) Uani 1 1 d U A . C14 C 0.4048(4) 0.5588(11) 0.2591(8) 0.0875(18) Uani 1 1 d U A . C15 C 0.3494(5) 0.6667(11) 0.2753(7) 0.089(4) Uani 1 1 d U A . C16 C 0.3606(4) 0.7412(10) 0.1484(7) 0.082(3) Uani 1 1 d U A . O1 O 0.2219(3) 0.3219(7) 0.2371(5) 0.087(3) Uani 1 1 d U . . O2 O 0.2794(2) 0.1901(6) 0.1494(4) 0.075(2) Uani 1 1 d U . . O3 O 0.2847(3) 0.2811(7) 0.0044(4) 0.081(2) Uani 1 1 d U . . O4 O 0.2367(3) 0.4896(8) -0.0263(5) 0.104(3) Uani 1 1 d U . . O5 O 0.2114(3) 0.5700(8) 0.3176(5) 0.100(3) Uani 1 1 d U . . O6 O 0.2781(3) 0.3912(8) 0.3841(5) 0.097(3) Uani 1 1 d U . . O7 O 0.3742(3) 0.3352(9) 0.3775(5) 0.106(3) Uani 1 1 d U A . O8 O 0.4458(3) 0.2905(9) 0.2848(6) 0.120(3) Uani 1 1 d U A . O9 O 0.4602(4) 0.4441(9) 0.0241(6) 0.123(3) Uani 1 1 d U . . O10 O 0.3892(4) 0.5475(10) -0.0692(6) 0.129(4) Uani 1 1 d U . . O11 O 0.3017(3) 0.6679(8) -0.0802(5) 0.101(3) Uani 1 1 d U A . O12 O 0.2351(4) 0.7707(9) 0.0151(6) 0.120(3) Uani 1 1 d U A . O13 O 0.2280(3) 0.3927(7) 0.1034(5) 0.090(3) Uani 1 1 d U . . O14 O 0.4365(4) 0.5649(9) 0.2737(6) 0.124(3) Uani 1 1 d U . . O15 O 0.3623(3) 0.7316(7) 0.2994(5) 0.100(3) Uani 1 1 d U . . O16 O 0.3738(3) 0.8101(7) 0.1649(4) 0.087(3) Uani 1 1 d U . . C17 C 0.4161(8) 0.624(3) 0.1303(19) 0.129(7) Uiso 0.62(2) 1 d PDU A 1 O17 O 0.4467(7) 0.6326(17) 0.1345(12) 0.130(6) Uiso 0.62(2) 1 d PDU A 1 C17' C 0.4143(13) 0.638(5) 0.104(3) 0.129(7) Uiso 0.38(2) 1 d PDU A 2 O17' O 0.4412(11) 0.674(3) 0.095(2) 0.131(7) Uiso 0.38(2) 1 d PDU A 2 C18 C 0.2802(4) 0.7051(10) 0.2744(6) 0.0721(17) Uani 1 1 d U . . O18 O 0.2636(3) 0.7591(8) 0.2991(5) 0.100(3) Uani 1 1 d U A . C19 C 0.296(2) 0.795(3) 0.150(5) 0.090(5) Uiso 0.299(6) 1 d PDU A 1 O19 O 0.3012(11) 0.875(3) 0.1572(18) 0.092(5) Uiso 0.299(6) 1 d PDU A 1 C20 C 0.2369(15) 0.601(4) 0.167(3) 0.100(2) Uiso 0.299(6) 1 d PDU A 1 O20 O 0.2169(11) 0.661(3) 0.1768(18) 0.107(4) Uiso 0.299(6) 1 d PDU A 1 Ni17 Ni 0.25720(9) 0.7020(2) 0.15710(17) 0.1022(14) Uani 0.701(6) 1 d PU A 2 C21 C 0.2227(6) 0.7748(18) 0.1618(12) 0.105(2) Uiso 0.701(6) 1 d PDU A 2 O21 O 0.1969(5) 0.8179(14) 0.1667(9) 0.127(5) Uiso 0.701(6) 1 d PDU A 2 C19' C 0.2902(10) 0.7916(15) 0.143(2) 0.089(5) Uiso 0.701(6) 1 d PDU A 2 O19' O 0.2838(5) 0.8713(13) 0.1394(8) 0.103(4) Uiso 0.701(6) 1 d PDU A 2 C20' C 0.2331(5) 0.590(2) 0.1496(13) 0.099(3) Uiso 0.701(6) 1 d PDU A 2 O20' O 0.2031(5) 0.5674(12) 0.1439(8) 0.108(4) Uiso 0.701(6) 1 d PDU A 2 C22 C 0.3389(3) 0.4329(8) 0.2077(5) 0.052(2) Uani 1 1 d U A . C23 C 0.3132(3) 0.4974(8) 0.2195(5) 0.052(2) Uani 1 1 d U A . C24 C 0.3217(3) 0.5705(8) 0.0996(5) 0.054(2) Uani 1 1 d U A . C25 C 0.3456(3) 0.4991(8) 0.0931(5) 0.053(2) Uani 1 1 d U A . C26 C 0.3645(12) 0.2046(19) 0.1700(15) 0.090(5) Uiso 0.698(5) 1 d PDU B 1 O26 O 0.3765(5) 0.1298(14) 0.1704(8) 0.099(4) Uiso 0.698(5) 1 d PDU B 1 C27 C 0.3702(6) 0.2804(14) 0.0414(10) 0.0676(18) Uiso 0.698(5) 1 d PDU A 1 O27 O 0.3900(4) 0.2255(11) 0.0241(8) 0.092(3) Uiso 0.698(5) 1 d PDU A 1 C28 C 0.4188(5) 0.3815(16) 0.1525(11) 0.083(2) Uiso 0.698(5) 1 d PDU A 1 O28 O 0.4457(4) 0.3424(11) 0.1508(7) 0.091(3) Uiso 0.698(5) 1 d PDU A 1 Ni18 Ni 0.39364(18) 0.2969(5) 0.1271(3) 0.086(2) Uani 0.302(5) 1 d PU A 2 C26' C 0.367(3) 0.205(5) 0.182(4) 0.092(5) Uiso 0.302(5) 1 d PDU A 2 O26' O 0.3817(11) 0.138(3) 0.1986(18) 0.095(5) Uiso 0.302(5) 1 d PDU A 2 C27' C 0.3738(16) 0.299(3) 0.030(2) 0.074(3) Uiso 0.302(5) 1 d PDU A 2 O27' O 0.3802(10) 0.240(3) -0.0028(16) 0.082(4) Uiso 0.302(5) 1 d PDU A 2 C28' C 0.4205(8) 0.430(3) 0.151(2) 0.0684(18) Uiso 0.302(5) 1 d PDU A 2 O28' O 0.4498(7) 0.441(2) 0.1689(15) 0.083(4) Uiso 0.302(5) 1 d PDU A 2 C29 C 0.4318(12) 0.249(4) 0.122(2) 0.089(3) Uiso 0.302(5) 1 d PDU A 2 O29 O 0.4581(10) 0.209(3) 0.1137(16) 0.106(6) Uiso 0.302(5) 1 d PDU A 2 Ni21 Ni 0.01654(6) -0.06203(14) 0.09663(9) 0.0839(6) Uani 1 1 d . . . Ni22 Ni -0.01117(5) 0.07913(18) 0.11548(9) 0.0882(6) Uani 1 1 d . D . Ni23 Ni -0.06848(5) 0.01201(15) 0.04181(8) 0.0790(6) Uani 1 1 d U . . Ni24 Ni -0.02302(5) 0.12861(14) 0.00663(9) 0.0752(5) Uani 1 1 d . . . Ni25 Ni 0.02960(6) 0.20079(15) 0.07469(10) 0.0946(7) Uani 1 1 d U . . Ni26 Ni 0.04382(5) 0.12914(14) -0.01661(9) 0.0766(6) Uani 1 1 d . . . Ni27 Ni 0.06813(5) 0.07239(13) 0.09283(8) 0.0713(5) Uani 1 1 d . D . Ni28 Ni 0.07780(5) -0.08328(14) 0.06271(9) 0.0769(5) Uani 1 1 d U . . C31 C 0.1091(4) -0.1627(12) 0.0632(8) 0.0925(18) Uani 1 1 d U . . C32 C -0.0102(5) -0.0279(14) 0.1591(9) 0.109(4) Uani 1 1 d U D . C33 C 0.0165(5) 0.2959(13) 0.1035(9) 0.1062(19) Uani 1 1 d U D . C34 C 0.0752(5) 0.1828(14) 0.1239(9) 0.111(4) Uani 1 1 d U D . C35 C 0.0751(4) 0.1067(12) -0.0729(7) 0.093(4) Uani 1 1 d U . . C36 C 0.1045(5) 0.0069(14) 0.1175(9) 0.108(4) Uani 1 1 d U . . O31 O 0.1312(4) -0.2201(10) 0.0606(6) 0.131(3) Uani 1 1 d U D . O32 O -0.0209(4) -0.0587(9) 0.2028(6) 0.117(4) Uani 1 1 d U . . O33 O 0.0067(4) 0.3632(10) 0.1313(7) 0.139(3) Uani 1 1 d DU . . O34 O 0.0940(4) 0.2379(9) 0.1492(6) 0.118(4) Uani 1 1 d U . . O35 O 0.0912(3) 0.1423(8) -0.1088(5) 0.099(3) Uani 1 1 d U D . O36 O 0.1303(3) -0.0069(9) 0.1497(6) 0.114(3) Uani 1 1 d U D . C37 C 0.0029(11) 0.191(2) -0.0669(17) 0.115(6) Uiso 0.50 1 d PDU . -1 O37 O 0.0031(7) 0.2604(17) -0.0937(11) 0.108(6) Uiso 0.50 1 d PDU C -1 C38 C 0.0569(10) -0.140(2) 0.1299(15) 0.106(8) Uiso 0.50 1 d PDU D -1 O38 O 0.0649(7) -0.1975(18) 0.1651(11) 0.112(7) Uiso 0.50 1 d PDU D -1 C39 C 0.0586(14) 0.249(3) 0.015(2) 0.139(7) Uiso 0.50 1 d PDU D -1 O39 O 0.0754(8) 0.311(2) -0.0014(14) 0.137(7) Uiso 0.50 1 d PDU D -1 C38' C -0.0196(11) 0.163(2) -0.1172(18) 0.118(6) Uiso 0.50 1 d PDU . -2 O38' O -0.0239(7) 0.239(2) -0.1354(12) 0.124(6) Uiso 0.50 1 d PDU E -2 C39' C 0.0478(14) 0.247(3) -0.005(2) 0.140(7) Uiso 0.50 1 d PDU D -2 O39' O 0.0529(9) 0.324(3) -0.0189(15) 0.146(7) Uiso 0.50 1 d PDU D -2 C41 C 0.0399(3) 0.0003(9) 0.0264(6) 0.063(3) Uani 1 1 d U . . C42 C 0.0186(3) 0.0642(9) 0.0500(6) 0.063(3) Uani 1 1 d U D . C43 C -0.1009(8) 0.082(2) 0.0754(17) 0.091(3) Uiso 0.567(7) 1 d PDU D 1 O43 O -0.1260(6) 0.1232(16) 0.0878(10) 0.107(4) Uiso 0.567(7) 1 d PDU D 1 C44 C -0.0387(15) 0.146(3) 0.158(3) 0.148(8) Uiso 0.567(7) 1 d PDU D 1 O44 O -0.0499(8) 0.211(2) 0.1813(15) 0.152(8) Uiso 0.567(7) 1 d PDU D 1 C45 C -0.0437(17) 0.235(3) 0.015(3) 0.110(6) Uiso 0.567(7) 1 d PDU D 1 O45 O -0.0608(7) 0.3020(18) 0.0213(11) 0.119(6) Uiso 0.567(7) 1 d PDU D 1 Ni29 Ni -0.06658(19) 0.1621(5) 0.0713(3) 0.134(3) Uani 0.433(7) 1 d PU D 2 C43' C -0.0985(10) 0.054(3) 0.082(2) 0.0853(19) Uiso 0.433(7) 1 d PDU D 2 O43' O -0.1229(7) 0.057(2) 0.1110(12) 0.100(4) Uiso 0.433(7) 1 d PDU D 2 C44' C -0.029(2) 0.153(5) 0.162(3) 0.148(8) Uiso 0.433(7) 1 d PDU D 2 O44' O -0.0382(11) 0.183(3) 0.2063(18) 0.149(8) Uiso 0.433(7) 1 d PDU D 2 C45' C -0.041(2) 0.238(3) 0.006(4) 0.110(6) Uiso 0.433(7) 1 d PDU D 2 O45' O -0.0435(8) 0.316(2) -0.0087(14) 0.110(6) Uiso 0.433(7) 1 d PDU D 2 C46 C -0.0898(13) 0.240(3) 0.094(2) 0.137(4) Uiso 0.433(7) 1 d PDU D 2 O46 O -0.1068(7) 0.298(2) 0.1140(15) 0.149(7) Uiso 0.433(7) 1 d PDU D 2 N1 N 0.2856(3) 0.0645(7) 0.3144(4) 0.074(3) Uani 1 1 d D . . C101 C 0.2597(4) -0.0104(11) 0.3154(8) 0.132(6) Uiso 1 1 d DU . . H10A H 0.2452 -0.0004 0.3479 0.159 Uiso 1 1 calc R . . H10B H 0.2720 -0.0683 0.3221 0.159 Uiso 1 1 calc R . . C102 C 0.2357(5) -0.0188(15) 0.2593(8) 0.137(6) Uiso 1 1 d DU . . H10C H 0.2198 -0.0694 0.2629 0.205 Uiso 1 1 calc R . . H10D H 0.2497 -0.0296 0.2269 0.205 Uiso 1 1 calc R . . H10E H 0.2226 0.0372 0.2531 0.205 Uiso 1 1 calc R . . C103 C 0.2680(4) 0.1542(9) 0.3054(7) 0.118(5) Uiso 1 1 d DU . . H10F H 0.2558 0.1553 0.2670 0.142 Uiso 1 1 calc R . . H10G H 0.2855 0.2027 0.3069 0.142 Uiso 1 1 calc R . . C104 C 0.2416(5) 0.1739(14) 0.3515(8) 0.127(6) Uiso 1 1 d DU . . H10H H 0.2305 0.2324 0.3435 0.190 Uiso 1 1 calc R . . H10I H 0.2536 0.1751 0.3895 0.190 Uiso 1 1 calc R . . H10J H 0.2240 0.1263 0.3501 0.190 Uiso 1 1 calc R . . C105 C 0.3055(5) 0.0640(12) 0.3718(6) 0.131(6) Uiso 1 1 d DU . . H10K H 0.3163 0.0039 0.3776 0.158 Uiso 1 1 calc R . . H10L H 0.2891 0.0720 0.4018 0.158 Uiso 1 1 calc R . . C106 C 0.3341(5) 0.1379(13) 0.3802(9) 0.132(6) Uiso 1 1 d DU . . H10M H 0.3457 0.1321 0.4185 0.199 Uiso 1 1 calc R . . H10N H 0.3237 0.1979 0.3760 0.199 Uiso 1 1 calc R . . H10O H 0.3509 0.1298 0.3514 0.199 Uiso 1 1 calc R . . C107 C 0.3084(4) 0.0527(11) 0.2660(7) 0.119(5) Uiso 1 1 d DU . . H10P H 0.3233 0.1066 0.2646 0.142 Uiso 1 1 calc R . . H10Q H 0.2937 0.0510 0.2299 0.142 Uiso 1 1 calc R . . C108 C 0.3318(5) -0.0329(11) 0.2682(9) 0.121(5) Uiso 1 1 d DU . . H10R H 0.3448 -0.0350 0.2340 0.182 Uiso 1 1 calc R . . H10S H 0.3175 -0.0872 0.2697 0.182 Uiso 1 1 calc R . . H10T H 0.3478 -0.0304 0.3024 0.182 Uiso 1 1 calc R . . N2 N 0.1877(3) 0.1456(8) 0.0152(5) 0.086(4) Uani 1 1 d D . . C201 C 0.1735(6) 0.0524(11) 0.0228(10) 0.273(15) Uiso 1 1 d DU . . H20A H 0.1589 0.0361 -0.0120 0.328 Uiso 1 1 calc RD . . H20B H 0.1586 0.0530 0.0553 0.328 Uiso 1 1 calc R . . C202 C 0.2017(8) -0.0221(12) 0.0338(17) 0.278(15) Uiso 1 1 d DU . . H20C H 0.1906 -0.0813 0.0364 0.417 Uiso 1 1 calc R . . H20D H 0.2151 -0.0092 0.0697 0.417 Uiso 1 1 calc RD . . H20E H 0.2169 -0.0225 0.0023 0.417 Uiso 1 1 calc R . . C203 C 0.2076(4) 0.1499(15) -0.0368(7) 0.180(8) Uiso 1 1 d DU . . H20F H 0.2285 0.1125 -0.0296 0.216 Uiso 1 1 calc R . . H20G H 0.2152 0.2131 -0.0414 0.216 Uiso 1 1 calc RD . . C204 C 0.1890(6) 0.1186(18) -0.0950(8) 0.176(8) Uiso 1 1 d DU . . H20H H 0.2049 0.1237 -0.1254 0.264 Uiso 1 1 calc R . . H20I H 0.1689 0.1568 -0.1041 0.264 Uiso 1 1 calc R . . H20J H 0.1817 0.0556 -0.0918 0.264 Uiso 1 1 calc RD . . C205 C 0.1554(5) 0.2020(15) 0.0109(12) 0.221(11) Uiso 1 1 d DU . . H20K H 0.1451 0.2019 0.0483 0.266 Uiso 1 1 calc R . . H20L H 0.1386 0.1744 -0.0176 0.266 Uiso 1 1 calc R . . C206 C 0.1623(6) 0.3023(14) -0.0071(14) 0.225(11) Uiso 1 1 d DU . . H20M H 0.1406 0.3361 -0.0090 0.338 Uiso 1 1 calc R . . H20N H 0.1718 0.3030 -0.0446 0.338 Uiso 1 1 calc RD . . H20O H 0.1786 0.3303 0.0212 0.338 Uiso 1 1 calc R . . C207 C 0.2102(5) 0.1751(14) 0.0663(7) 0.163(7) Uiso 1 1 d DU . . H20P H 0.2205 0.2344 0.0580 0.196 Uiso 1 1 calc R . . H20Q H 0.2292 0.1311 0.0729 0.196 Uiso 1 1 calc RD . . C208 C 0.1904(6) 0.1833(17) 0.1222(8) 0.161(7) Uiso 1 1 d DU . . H20R H 0.2066 0.1992 0.1544 0.242 Uiso 1 1 calc R . . H20S H 0.1794 0.1254 0.1299 0.242 Uiso 1 1 calc R . . H20T H 0.1728 0.2304 0.1170 0.242 Uiso 1 1 calc R . . N3 N 0.5423(3) 0.4488(9) 0.2161(6) 0.112(5) Uani 1 1 d D . . C301 C 0.5635(7) 0.399(3) 0.2618(13) 0.169(7) Uiso 0.497(14) 1 d PDU F 1 H30A H 0.5797 0.4423 0.2817 0.202 Uiso 0.497(14) 1 calc PR F 1 H30B H 0.5772 0.3522 0.2439 0.202 Uiso 0.497(14) 1 calc PR F 1 C302 C 0.5410(12) 0.354(4) 0.3068(17) 0.169(8) Uiso 0.497(14) 1 d PDU F 1 H30C H 0.5560 0.3216 0.3352 0.253 Uiso 0.497(14) 1 calc PR F 1 H30D H 0.5249 0.3113 0.2874 0.253 Uiso 0.497(14) 1 calc PR F 1 H30E H 0.5281 0.4005 0.3258 0.253 Uiso 0.497(14) 1 calc PR F 1 C303 C 0.5135(6) 0.501(2) 0.2401(17) 0.165(7) Uiso 0.497(14) 1 d PDU F 1 H30F H 0.5010 0.4597 0.2646 0.198 Uiso 0.497(14) 1 calc PR F 1 H30G H 0.4973 0.5194 0.2079 0.198 Uiso 0.497(14) 1 calc PR F 1 C304 C 0.5238(13) 0.587(3) 0.276(2) 0.167(8) Uiso 0.497(14) 1 d PDU F 1 H30H H 0.5032 0.6150 0.2895 0.251 Uiso 0.497(14) 1 calc PR F 1 H30I H 0.5354 0.6301 0.2518 0.251 Uiso 0.497(14) 1 calc PR F 1 H30J H 0.5395 0.5700 0.3086 0.251 Uiso 0.497(14) 1 calc PR F 1 C305 C 0.5655(7) 0.513(2) 0.1871(15) 0.166(7) Uiso 0.497(14) 1 d PDU F 1 H30K H 0.5856 0.4797 0.1745 0.199 Uiso 0.497(14) 1 calc PR F 1 H30L H 0.5740 0.5600 0.2147 0.199 Uiso 0.497(14) 1 calc PR F 1 C306 C 0.5461(14) 0.560(3) 0.1342(19) 0.167(8) Uiso 0.497(14) 1 d PDU F 1 H30M H 0.5619 0.5999 0.1158 0.251 Uiso 0.497(14) 1 calc PR F 1 H30N H 0.5267 0.5946 0.1468 0.251 Uiso 0.497(14) 1 calc PR F 1 H30O H 0.5376 0.5133 0.1069 0.251 Uiso 0.497(14) 1 calc PR F 1 C307 C 0.5273(8) 0.384(2) 0.1717(15) 0.168(7) Uiso 0.497(14) 1 d PDU F 1 H30P H 0.5218 0.4173 0.1356 0.202 Uiso 0.497(14) 1 calc PR F 1 H30Q H 0.5057 0.3589 0.1845 0.202 Uiso 0.497(14) 1 calc PR F 1 C308 C 0.5525(13) 0.305(3) 0.160(2) 0.168(8) Uiso 0.497(14) 1 d PDU F 1 H30R H 0.5420 0.2654 0.1301 0.252 Uiso 0.497(14) 1 calc PR F 1 H30S H 0.5570 0.2694 0.1953 0.252 Uiso 0.497(14) 1 calc PR F 1 H30T H 0.5741 0.3291 0.1480 0.252 Uiso 0.497(14) 1 calc PR F 1 C3A1 C 0.5175(7) 0.386(2) 0.2435(17) 0.165(7) Uiso 0.503(14) 1 d PDU F 2 H3A1 H 0.5011 0.3611 0.2135 0.198 Uiso 0.503(14) 1 calc PR F 2 H3A2 H 0.5042 0.4212 0.2703 0.198 Uiso 0.503(14) 1 calc PR F 2 C3A2 C 0.5364(12) 0.306(3) 0.277(2) 0.170(8) Uiso 0.503(14) 1 d PDU F 2 H3A3 H 0.5194 0.2678 0.2935 0.254 Uiso 0.503(14) 1 calc PR F 2 H3A4 H 0.5523 0.3309 0.3068 0.254 Uiso 0.503(14) 1 calc PR F 2 H3A5 H 0.5492 0.2709 0.2500 0.254 Uiso 0.503(14) 1 calc PR F 2 C3A3 C 0.5687(7) 0.390(2) 0.1899(15) 0.168(7) Uiso 0.503(14) 1 d PDU F 2 H3A6 H 0.5774 0.3456 0.2189 0.202 Uiso 0.503(14) 1 calc PR F 2 H3A7 H 0.5883 0.4290 0.1809 0.202 Uiso 0.503(14) 1 calc PR F 2 C3A4 C 0.5558(13) 0.338(3) 0.1342(17) 0.168(8) Uiso 0.503(14) 1 d PDU F 2 H3A8 H 0.5747 0.3017 0.1208 0.252 Uiso 0.503(14) 1 calc PR F 2 H3A9 H 0.5480 0.3813 0.1045 0.252 Uiso 0.503(14) 1 calc PR F 2 H3AX H 0.5367 0.2981 0.1425 0.252 Uiso 0.503(14) 1 calc PR F 2 C3A5 C 0.5241(6) 0.504(2) 0.1704(15) 0.166(7) Uiso 0.503(14) 1 d PDU F 2 H3AY H 0.5024 0.5266 0.1846 0.199 Uiso 0.503(14) 1 calc PR F 2 H3AZ H 0.5181 0.4648 0.1371 0.199 Uiso 0.503(14) 1 calc PR F 2 C3A6 C 0.5451(13) 0.587(3) 0.150(2) 0.168(8) Uiso 0.503(14) 1 d PDU F 2 H3AA H 0.5305 0.6232 0.1229 0.252 Uiso 0.503(14) 1 calc PR F 2 H3AB H 0.5652 0.5654 0.1309 0.252 Uiso 0.503(14) 1 calc PR F 2 H3AC H 0.5528 0.6243 0.1828 0.252 Uiso 0.503(14) 1 calc PR F 2 C3A7 C 0.5607(8) 0.505(3) 0.2621(14) 0.169(7) Uiso 0.503(14) 1 d PDU F 2 H3AD H 0.5745 0.5513 0.2437 0.203 Uiso 0.503(14) 1 calc PR F 2 H3AE H 0.5768 0.4655 0.2851 0.203 Uiso 0.503(14) 1 calc PR F 2 C3A8 C 0.5367(13) 0.553(3) 0.3031(18) 0.169(8) Uiso 0.503(14) 1 d PDU F 2 H3AF H 0.5506 0.5885 0.3315 0.253 Uiso 0.503(14) 1 calc PR F 2 H3AG H 0.5234 0.5080 0.3227 0.253 Uiso 0.503(14) 1 calc PR F 2 H3AH H 0.5209 0.5937 0.2810 0.253 Uiso 0.503(14) 1 calc PR F 2 N4 N 0.1077(4) 0.5357(10) 0.1807(7) 0.117(5) Uani 1 1 d D . . C401 C 0.1343(7) 0.469(2) 0.2029(10) 0.263(14) Uiso 1 1 d DU . . H40A H 0.1570 0.4987 0.2045 0.316 Uiso 1 1 calc RD . . H40B H 0.1349 0.4189 0.1747 0.316 Uiso 1 1 calc RD . . C402 C 0.1297(9) 0.426(2) 0.2625(11) 0.259(14) Uiso 1 1 d DU . . H40C H 0.1478 0.3810 0.2710 0.388 Uiso 1 1 calc R . . H40D H 0.1072 0.3966 0.2623 0.388 Uiso 1 1 calc R . . H40E H 0.1313 0.4733 0.2917 0.388 Uiso 1 1 calc R . . C403 C 0.1036(8) 0.6146(18) 0.2197(14) 0.311(17) Uiso 1 1 d DU . . H40F H 0.0980 0.5914 0.2576 0.373 Uiso 1 1 calc RD . . H40G H 0.0837 0.6510 0.2044 0.373 Uiso 1 1 calc RD . . C404 C 0.1354(9) 0.677(2) 0.2281(17) 0.308(17) Uiso 1 1 d DU . . H40H H 0.1350 0.7088 0.2648 0.463 Uiso 1 1 calc R . . H40I H 0.1348 0.7220 0.1971 0.463 Uiso 1 1 calc R . . H40J H 0.1564 0.6414 0.2276 0.463 Uiso 1 1 calc RD . . C405 C 0.1197(7) 0.568(2) 0.1246(10) 0.44(3) Uiso 1 1 d DU . . H40K H 0.1446 0.5807 0.1296 0.531 Uiso 1 1 calc RD . . H40L H 0.1078 0.6251 0.1141 0.531 Uiso 1 1 calc RD . . C406 C 0.1131(10) 0.499(3) 0.0745(8) 0.44(3) Uiso 1 1 d DU . . H40M H 0.1228 0.5230 0.0401 0.664 Uiso 1 1 calc RD . . H40N H 0.0884 0.4898 0.0670 0.664 Uiso 1 1 calc R . . H40O H 0.1242 0.4414 0.0849 0.664 Uiso 1 1 calc RD . . C407 C 0.0728(6) 0.494(2) 0.1749(18) 0.45(3) Uiso 1 1 d DU . . H40P H 0.0666 0.4737 0.2131 0.535 Uiso 1 1 calc RD . . H40Q H 0.0738 0.4392 0.1505 0.535 Uiso 1 1 calc R . . C408 C 0.0438(6) 0.557(3) 0.149(2) 0.44(3) Uiso 1 1 d DU . . H40R H 0.0272 0.5219 0.1247 0.667 Uiso 1 1 calc R . . H40S H 0.0540 0.6039 0.1255 0.667 Uiso 1 1 calc RD . . H40T H 0.0321 0.5861 0.1796 0.667 Uiso 1 1 calc R . . N5 N 0.0789(3) 0.4213(9) 0.8124(6) 0.099(4) Uani 1 1 d D . . C501 C 0.0911(7) 0.457(2) 0.8701(8) 0.256(13) Uiso 1 1 d DU . . H50A H 0.1072 0.5074 0.8651 0.307 Uiso 1 1 calc R . . H50B H 0.1041 0.4085 0.8914 0.307 Uiso 1 1 calc R . . C502 C 0.0618(8) 0.490(2) 0.9068(13) 0.249(13) Uiso 1 1 d DU . . H50C H 0.0717 0.5131 0.9436 0.374 Uiso 1 1 calc R . . H50D H 0.0462 0.4401 0.9135 0.374 Uiso 1 1 calc R . . H50E H 0.0490 0.5388 0.8865 0.374 Uiso 1 1 calc R . . C503 C 0.0588(6) 0.4904(16) 0.7778(13) 0.281(15) Uiso 1 1 d DU . . H50F H 0.0360 0.4973 0.7938 0.338 Uiso 1 1 calc R . . H50G H 0.0547 0.4674 0.7383 0.338 Uiso 1 1 calc R . . C504 C 0.0758(8) 0.5852(14) 0.7754(16) 0.276(15) Uiso 1 1 d DU . . H50H H 0.0611 0.6254 0.7513 0.414 Uiso 1 1 calc R . . H50I H 0.0983 0.5796 0.7593 0.414 Uiso 1 1 calc RD . . H50J H 0.0789 0.6102 0.8141 0.414 Uiso 1 1 calc R . . C505 C 0.1102(6) 0.3961(16) 0.7822(10) 0.231(12) Uiso 1 1 d DU . . H50K H 0.1233 0.4517 0.7750 0.277 Uiso 1 1 calc RD . . H50L H 0.1027 0.3694 0.7447 0.277 Uiso 1 1 calc R . . C506 C 0.1341(7) 0.329(2) 0.8157(13) 0.228(12) Uiso 1 1 d DU . . H50M H 0.1543 0.3164 0.7941 0.342 Uiso 1 1 calc R . . H50N H 0.1217 0.2720 0.8213 0.342 Uiso 1 1 calc R . . H50O H 0.1416 0.3543 0.8530 0.342 Uiso 1 1 calc R . . C507 C 0.0557(6) 0.3428(14) 0.8213(9) 0.195(9) Uiso 1 1 d DU . . H50P H 0.0343 0.3669 0.8362 0.234 Uiso 1 1 calc R . . H50Q H 0.0669 0.3046 0.8518 0.234 Uiso 1 1 calc R . . C508 C 0.0449(7) 0.2803(16) 0.7700(10) 0.178(9) Uiso 1 1 d DU . . H50R H 0.0301 0.2320 0.7827 0.267 Uiso 1 1 calc R . . H50S H 0.0655 0.2539 0.7550 0.267 Uiso 1 1 calc R . . H50T H 0.0325 0.3157 0.7399 0.267 Uiso 1 1 calc R . . N6 N 0.3555(3) 0.9367(7) -0.0077(5) 0.102(5) Uani 1 1 d D . . C601 C 0.3348(9) 0.962(2) 0.0417(11) 0.136(8) Uiso 0.506(12) 1 d PDU G 1 H60A H 0.3501 0.9628 0.0772 0.163 Uiso 0.506(12) 1 calc PR G 1 H60B H 0.3169 0.9158 0.0461 0.163 Uiso 0.506(12) 1 calc PR G 1 C602 C 0.3172(14) 1.057(3) 0.034(2) 0.137(9) Uiso 0.506(12) 1 d PDU G 1 H60C H 0.3046 1.0707 0.0676 0.205 Uiso 0.506(12) 1 calc PR G 1 H60D H 0.3011 1.0559 -0.0001 0.205 Uiso 0.506(12) 1 calc PR G 1 H60E H 0.3347 1.1031 0.0294 0.205 Uiso 0.506(12) 1 calc PR G 1 C603 C 0.3866(6) 0.998(2) -0.0073(14) 0.148(7) Uiso 0.506(12) 1 d PDU G 1 H60F H 0.3788 1.0608 -0.0122 0.178 Uiso 0.506(12) 1 calc PR G 1 H60G H 0.3999 0.9821 -0.0405 0.178 Uiso 0.506(12) 1 calc PR G 1 C604 C 0.4111(10) 0.991(4) 0.0481(17) 0.152(7) Uiso 0.506(12) 1 d PDU G 1 H60H H 0.4306 1.0322 0.0450 0.229 Uiso 0.506(12) 1 calc PRD G 1 H60I H 0.4195 0.9291 0.0529 0.229 Uiso 0.506(12) 1 calc PR G 1 H60J H 0.3985 1.0083 0.0812 0.229 Uiso 0.506(12) 1 calc PR G 1 C605 C 0.3669(9) 0.8410(13) 0.0034(16) 0.151(8) Uiso 0.506(12) 1 d PDU G 1 H60K H 0.3465 0.8017 -0.0048 0.181 Uiso 0.506(12) 1 calc PR G 1 H60L H 0.3734 0.8356 0.0448 0.181 Uiso 0.506(12) 1 calc PR G 1 C606 C 0.3968(10) 0.801(3) -0.029(2) 0.155(8) Uiso 0.506(12) 1 d PDU G 1 H60M H 0.4011 0.7383 -0.0168 0.233 Uiso 0.506(12) 1 calc PR G 1 H60N H 0.4177 0.8367 -0.0206 0.233 Uiso 0.506(12) 1 calc PR G 1 H60O H 0.3906 0.8021 -0.0703 0.233 Uiso 0.506(12) 1 calc PR G 1 C607 C 0.3380(8) 0.952(2) -0.0654(9) 0.145(6) Uiso 0.506(12) 1 d PDU G 1 H60P H 0.3552 0.9464 -0.0944 0.174 Uiso 0.506(12) 1 calc PR G 1 H60Q H 0.3288 1.0142 -0.0674 0.174 Uiso 0.506(12) 1 calc PR G 1 C608 C 0.3081(9) 0.884(3) -0.0801(18) 0.139(7) Uiso 0.506(12) 1 d PDU G 1 H60R H 0.2978 0.8968 -0.1186 0.209 Uiso 0.506(12) 1 calc PR G 1 H60S H 0.2906 0.8905 -0.0523 0.209 Uiso 0.506(12) 1 calc PR G 1 H60T H 0.3171 0.8222 -0.0788 0.209 Uiso 0.506(12) 1 calc PR G 1 C6A1 C 0.3420(10) 1.0324(14) -0.0031(14) 0.135(8) Uiso 0.494(12) 1 d PDU G 2 H6A1 H 0.3258 1.0448 -0.0365 0.162 Uiso 0.494(12) 1 calc PR G 2 H6A2 H 0.3615 1.0751 -0.0045 0.162 Uiso 0.494(12) 1 calc PR G 2 C6A2 C 0.3233(15) 1.050(3) 0.0529(18) 0.137(9) Uiso 0.494(12) 1 d PDU G 2 H6A3 H 0.3150 1.1125 0.0530 0.206 Uiso 0.494(12) 1 calc PR G 2 H6A4 H 0.3394 1.0400 0.0862 0.206 Uiso 0.494(12) 1 calc PR G 2 H6A5 H 0.3038 1.0086 0.0543 0.206 Uiso 0.494(12) 1 calc PR G 2 C6A3 C 0.3241(7) 0.875(2) -0.0130(15) 0.136(8) Uiso 0.494(12) 1 d PDU G 2 H6A6 H 0.3132 0.8756 0.0238 0.163 Uiso 0.494(12) 1 calc PR G 2 H6A7 H 0.3320 0.8126 -0.0195 0.163 Uiso 0.494(12) 1 calc PR G 2 C6A4 C 0.2964(9) 0.900(3) -0.0615(17) 0.136(8) Uiso 0.494(12) 1 d PDU G 2 H6A8 H 0.2772 0.8573 -0.0610 0.203 Uiso 0.494(12) 1 calc PR G 2 H6A9 H 0.3066 0.8965 -0.0985 0.203 Uiso 0.494(12) 1 calc PR G 2 H6AX H 0.2881 0.9613 -0.0554 0.203 Uiso 0.494(12) 1 calc PR G 2 C6A5 C 0.3721(10) 0.936(2) -0.0637(11) 0.147(6) Uiso 0.494(12) 1 d PDU G 2 H6AY H 0.3895 0.9842 -0.0639 0.177 Uiso 0.494(12) 1 calc PR G 2 H6AZ H 0.3545 0.9471 -0.0953 0.177 Uiso 0.494(12) 1 calc PR G 2 C6A6 C 0.3899(12) 0.842(3) -0.0735(19) 0.156(7) Uiso 0.494(12) 1 d PDU G 2 H6AA H 0.4005 0.8430 -0.1101 0.234 Uiso 0.494(12) 1 calc PR G 2 H6AB H 0.3726 0.7939 -0.0740 0.234 Uiso 0.494(12) 1 calc PR G 2 H6AC H 0.4075 0.8309 -0.0425 0.234 Uiso 0.494(12) 1 calc PR G 2 C6A7 C 0.3771(9) 0.905(2) 0.0424(13) 0.150(8) Uiso 0.494(12) 1 d PDU G 2 H6AD H 0.3906 0.8526 0.0304 0.180 Uiso 0.494(12) 1 calc PR G 2 H6AE H 0.3617 0.8830 0.0713 0.180 Uiso 0.494(12) 1 calc PR G 2 C6A8 C 0.4025(11) 0.975(3) 0.0718(18) 0.152(8) Uiso 0.494(12) 1 d PDU G 2 H6AF H 0.4150 0.9467 0.1049 0.228 Uiso 0.494(12) 1 calc PR G 2 H6AG H 0.3896 1.0271 0.0845 0.228 Uiso 0.494(12) 1 calc PR G 2 H6AH H 0.4189 0.9947 0.0446 0.228 Uiso 0.494(12) 1 calc PR G 2 C701 C 0.1645(7) 0.611(2) 0.9604(9) 0.231(10) Uiso 1 1 d DU . . H70A H 0.1522 0.5553 0.9680 0.346 Uiso 1 1 calc R . . H70B H 0.1491 0.6629 0.9640 0.346 Uiso 1 1 calc R . . H70C H 0.1844 0.6173 0.9879 0.346 Uiso 1 1 calc R . . C702 C 0.1768(6) 0.6082(16) 0.8990(10) 0.227(10) Uiso 1 1 d DU . . C703 C 0.1938(8) 0.6957(17) 0.8787(14) 0.225(10) Uiso 1 1 d DU . . H70D H 0.2001 0.6880 0.8392 0.337 Uiso 1 1 calc R . . H70E H 0.2146 0.7084 0.9035 0.337 Uiso 1 1 calc R . . H70F H 0.1777 0.7462 0.8805 0.337 Uiso 1 1 calc R . . O704 O 0.1719(6) 0.5404(16) 0.8693(10) 0.219(9) Uiso 1 1 d D . . C801 C 0.5410(12) 0.859(4) 0.060(3) 0.52(3) Uiso 1 1 d DU . . H80A H 0.5388 0.9083 0.0875 0.775 Uiso 1 1 calc R . . H80B H 0.5618 0.8680 0.0396 0.775 Uiso 1 1 calc R . . H80C H 0.5426 0.8013 0.0806 0.775 Uiso 1 1 calc R . . C802 C 0.5089(12) 0.858(3) 0.0168(18) 0.52(3) Uiso 1 1 d DU . . C803 C 0.5027(15) 0.761(3) -0.0068(18) 0.52(3) Uiso 1 1 d DU . . H80D H 0.4794 0.7562 -0.0251 0.780 Uiso 1 1 calc R . . H80E H 0.5053 0.7172 0.0248 0.780 Uiso 1 1 calc R . . H80F H 0.5194 0.7470 -0.0348 0.780 Uiso 1 1 calc R . . O804 O 0.4836(13) 0.885(3) 0.041(2) 0.55(4) Uiso 1 1 d D . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Ni1 0.0515(9) 0.0474(9) 0.0600(10) -0.0035(7) 0.0030(7) -0.0048(7) Ni2 0.0571(10) 0.0545(10) 0.0670(11) -0.0049(8) 0.0046(8) 0.0034(8) Ni3 0.0700(11) 0.0558(10) 0.0611(10) -0.0062(8) 0.0017(8) 0.0027(8) Ni4 0.0664(11) 0.0516(9) 0.0591(10) -0.0075(8) -0.0058(8) 0.0001(8) Ni5 0.0673(11) 0.0581(10) 0.0671(11) -0.0040(8) 0.0181(9) -0.0004(8) Ni6 0.0628(10) 0.0677(11) 0.0513(10) 0.0034(8) 0.0032(8) -0.0061(8) Ni7 0.0619(11) 0.0821(12) 0.0627(11) 0.0028(9) -0.0056(9) 0.0086(9) Ni8 0.0492(9) 0.0748(11) 0.0582(10) -0.0004(8) 0.0045(7) -0.0040(8) Ni9 0.0847(13) 0.0829(13) 0.0760(13) -0.0044(10) 0.0301(11) -0.0118(11) Ni10 0.1053(15) 0.0662(11) 0.0542(11) 0.0040(9) 0.0035(10) -0.0145(10) Ni11 0.1000(14) 0.0558(10) 0.0644(11) 0.0024(9) -0.0126(10) 0.0103(10) Ni12 0.0544(9) 0.0535(9) 0.0597(10) 0.0033(8) 0.0024(8) 0.0017(7) Ni13 0.0619(11) 0.0720(12) 0.0800(12) -0.0166(10) 0.0054(9) -0.0192(9) Ni14 0.0794(12) 0.0505(9) 0.0596(10) -0.0049(8) 0.0023(9) -0.0048(8) Ni15 0.0824(12) 0.0493(9) 0.0637(11) -0.0032(8) 0.0140(9) -0.0091(9) Ni16 0.0714(12) 0.0634(11) 0.0789(13) -0.0114(9) 0.0011(10) -0.0132(9) C1 0.064(7) 0.068(7) 0.098(8) -0.003(6) 0.023(6) -0.011(5) C2 0.073(7) 0.051(6) 0.071(6) -0.007(5) 0.005(6) -0.008(5) C3 0.077(7) 0.068(7) 0.067(7) -0.013(6) -0.008(6) -0.003(6) C4 0.100(5) 0.096(5) 0.096(5) -0.002(4) -0.004(4) 0.004(4) C5 0.074(3) 0.069(3) 0.075(3) -0.002(3) 0.019(3) 0.003(3) C6 0.091(8) 0.107(8) 0.064(7) -0.005(7) 0.021(6) -0.020(7) C7 0.108(9) 0.123(9) 0.062(7) 0.030(7) -0.006(7) -0.009(8) C8 0.073(3) 0.097(3) 0.079(3) 0.005(3) -0.006(3) 0.013(3) C9 0.090(3) 0.096(3) 0.088(3) -0.004(3) 0.033(3) -0.007(3) C10 0.123(6) 0.125(6) 0.113(6) 0.000(5) 0.020(4) -0.006(4) C11 0.114(3) 0.070(3) 0.062(3) 0.004(3) -0.001(3) -0.010(3) C12 0.110(3) 0.068(3) 0.079(3) 0.003(3) -0.014(3) 0.014(3) C13 0.061(7) 0.092(8) 0.093(8) 0.015(6) -0.016(6) -0.013(6) C14 0.074(3) 0.090(3) 0.097(3) -0.017(3) 0.001(3) -0.017(3) C15 0.119(9) 0.073(7) 0.077(8) -0.019(6) 0.006(7) -0.029(7) C16 0.106(8) 0.065(7) 0.075(7) -0.005(6) 0.008(6) -0.026(6) O1 0.075(6) 0.081(6) 0.106(7) -0.006(5) 0.024(5) -0.018(5) O2 0.083(6) 0.056(5) 0.087(6) -0.010(5) 0.003(5) -0.009(4) O3 0.085(6) 0.076(6) 0.079(6) -0.017(5) -0.005(5) -0.007(5) O4 0.107(5) 0.103(5) 0.101(5) -0.003(4) -0.009(4) 0.005(4) O5 0.100(4) 0.098(4) 0.103(4) -0.004(4) 0.024(4) 0.008(4) O6 0.098(7) 0.118(7) 0.075(6) 0.003(6) 0.016(5) -0.016(6) O7 0.114(8) 0.136(8) 0.068(6) 0.030(6) -0.007(6) -0.007(7) O8 0.111(5) 0.130(5) 0.118(5) 0.007(4) 0.000(4) 0.018(4) O9 0.118(5) 0.130(5) 0.124(5) -0.002(4) 0.025(4) 0.005(4) O10 0.132(5) 0.137(5) 0.119(5) 0.002(4) 0.020(4) -0.005(4) O11 0.124(4) 0.088(4) 0.089(4) 0.002(4) -0.006(4) -0.002(4) O12 0.130(5) 0.110(5) 0.117(5) 0.001(4) -0.008(4) 0.017(4) O13 0.067(6) 0.100(7) 0.099(7) 0.012(5) -0.022(5) -0.014(5) O14 0.108(5) 0.128(5) 0.134(5) -0.014(4) -0.003(4) -0.010(4) O15 0.127(8) 0.082(7) 0.090(7) -0.023(5) -0.002(6) -0.029(6) O16 0.109(7) 0.067(6) 0.087(6) -0.009(5) 0.008(5) -0.026(5) C18 0.086(3) 0.061(3) 0.069(3) -0.009(3) 0.004(3) 0.000(3) O18 0.107(4) 0.092(4) 0.100(4) -0.012(4) 0.007(4) 0.009(4) Ni17 0.0900(19) 0.0806(18) 0.137(2) -0.0046(15) 0.0141(15) 0.0144(14) C22 0.052(5) 0.055(5) 0.050(5) -0.003(4) 0.007(4) -0.006(4) C23 0.052(5) 0.054(5) 0.050(5) -0.004(4) 0.006(4) -0.007(4) C24 0.062(6) 0.054(5) 0.045(5) 0.002(4) -0.001(4) -0.009(4) C25 0.062(6) 0.053(5) 0.044(5) 0.001(4) 0.000(4) -0.009(4) Ni18 0.085(3) 0.084(3) 0.093(3) 0.0153(19) 0.0337(19) 0.0250(19) Ni21 0.1034(16) 0.0842(14) 0.0666(12) 0.0022(10) 0.0228(11) -0.0302(12) Ni22 0.0712(13) 0.1283(18) 0.0657(12) -0.0156(12) 0.0089(10) -0.0040(12) Ni23 0.0759(12) 0.0937(13) 0.0692(11) -0.0064(10) 0.0178(9) -0.0153(10) Ni24 0.0668(12) 0.0803(13) 0.0776(13) -0.0122(10) 0.0001(10) -0.0013(10) Ni25 0.1056(16) 0.0771(14) 0.1005(16) -0.0161(12) 0.0038(13) -0.0011(12) Ni26 0.0734(12) 0.0799(13) 0.0775(13) 0.0095(10) 0.0134(10) -0.0217(10) Ni27 0.0660(11) 0.0759(12) 0.0715(12) -0.0010(10) 0.0016(9) -0.0176(9) Ni28 0.0677(12) 0.0839(13) 0.0793(13) -0.0016(10) 0.0075(10) -0.0015(10) C31 0.084(3) 0.098(3) 0.095(3) -0.004(3) 0.003(3) 0.007(3) C32 0.112(6) 0.115(6) 0.100(6) 0.003(4) 0.014(4) -0.011(4) C33 0.117(3) 0.088(3) 0.113(3) -0.019(3) 0.005(3) 0.001(3) C34 0.115(6) 0.110(6) 0.110(6) -0.002(4) 0.006(4) -0.014(4) C35 0.088(7) 0.106(7) 0.086(7) 0.024(6) 0.018(6) -0.024(6) C36 0.090(7) 0.126(7) 0.109(8) 0.005(7) 0.009(7) -0.006(7) O31 0.128(5) 0.131(5) 0.132(5) -0.006(4) -0.004(4) 0.016(4) O32 0.121(5) 0.125(5) 0.108(5) 0.005(4) 0.019(4) -0.011(4) O33 0.145(5) 0.126(5) 0.146(5) -0.017(4) 0.008(4) 0.003(4) O34 0.121(5) 0.114(5) 0.117(5) -0.006(4) 0.003(4) -0.017(4) O35 0.095(5) 0.110(5) 0.095(5) 0.015(4) 0.020(4) -0.014(4) O36 0.102(5) 0.124(5) 0.114(5) 0.002(4) 0.005(4) -0.004(5) C41 0.053(6) 0.071(7) 0.067(6) 0.006(5) 0.009(5) -0.017(5) C42 0.052(6) 0.071(7) 0.067(6) 0.006(5) 0.008(5) -0.016(5) Ni29 0.125(4) 0.125(4) 0.155(4) -0.021(3) 0.033(3) -0.001(3) N1 0.104(9) 0.065(7) 0.054(7) 0.008(6) 0.012(6) 0.010(7) N2 0.062(7) 0.094(9) 0.101(10) 0.001(8) 0.011(7) -0.015(7) N3 0.076(9) 0.124(12) 0.134(13) 0.012(10) -0.012(9) -0.011(8) N4 0.095(11) 0.091(10) 0.162(16) -0.003(10) 0.000(10) 0.003(8) N5 0.094(10) 0.103(10) 0.099(10) 0.019(9) -0.005(8) -0.003(8) N6 0.147(13) 0.059(8) 0.102(11) 0.011(7) 0.019(10) -0.012(8) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Ni1 C2 1.868(13) . ? Ni1 C1 1.893(14) . ? Ni1 C13 2.006(15) . ? Ni1 C23 2.101(12) . ? Ni1 C22 2.177(12) . ? Ni1 Ni2 2.364(2) . ? Ni1 Ni5 2.419(2) . ? Ni1 Ni12 2.539(2) . ? Ni1 Ni6 2.772(2) . ? Ni2 C26 1.72(2) . ? Ni2 C26' 1.74(5) . ? Ni2 C2 1.880(14) . ? Ni2 C22 2.002(12) . ? Ni2 Ni18 2.440(7) . ? Ni2 Ni8 2.557(2) . ? Ni2 Ni7 2.604(2) . ? Ni2 Ni3 2.897(2) . ? Ni3 C27 1.711(18) . ? Ni3 C27' 1.71(4) . ? Ni3 C3 1.886(14) . ? Ni3 C25 1.993(12) . ? Ni3 Ni4 2.360(2) . ? Ni3 Ni18 2.548(7) . ? Ni3 Ni8 2.576(2) . ? Ni3 Ni9 2.590(3) . ? Ni4 C3 1.873(14) . ? Ni4 C4 1.887(18) . ? Ni4 C13 1.988(16) . ? Ni4 C24 2.127(12) . ? Ni4 C25 2.179(12) . ? Ni4 Ni11 2.431(2) . ? Ni4 Ni12 2.534(2) . ? Ni4 Ni10 2.728(3) . ? Ni5 C5 1.694(14) . ? Ni5 C1 1.908(15) . ? Ni5 C23 2.104(12) . ? Ni5 C6 2.244(17) . ? Ni5 Ni6 2.423(2) . ? Ni5 Ni14 2.572(2) . ? Ni5 Ni12 2.755(2) . ? Ni6 C6 1.719(15) . ? Ni6 C7 1.817(18) . ? Ni6 C22 2.078(12) . ? Ni6 C23 2.088(12) . ? Ni6 Ni7 2.397(3) . ? Ni6 Ni13 2.808(2) . ? Ni7 C8 1.682(16) . ? Ni7 C7 1.964(17) . ? Ni7 C22 2.033(12) . ? Ni7 Ni8 2.531(2) . ? Ni7 Ni13 2.577(3) . ? Ni8 C28' 1.64(3) . ? Ni8 C28 1.788(17) . ? Ni8 C25 1.974(12) . ? Ni8 C22 2.012(11) . ? Ni8 Ni18 2.262(7) . ? Ni8 Ni9 2.564(3) . ? Ni8 Ni13 2.728(2) . ? Ni8 Ni16 2.743(3) . ? Ni9 C9 1.696(17) . ? Ni9 C10 1.92(2) . ? Ni9 C25 2.042(12) . ? Ni9 Ni10 2.391(3) . ? Ni9 C17' 2.47(7) . ? Ni9 Ni16 2.555(3) . ? Ni10 C11 1.692(16) . ? Ni10 C10 1.79(2) . ? Ni10 C24 2.077(12) . ? Ni10 C25 2.088(12) . ? Ni10 Ni11 2.456(3) . ? Ni10 Ni16 2.768(3) . ? Ni11 C12 1.661(16) . ? Ni11 C4 1.879(18) . ? Ni11 C24 2.059(12) . ? Ni11 C11 2.326(16) . ? Ni11 Ni15 2.594(3) . ? Ni11 Ni12 2.702(2) . ? Ni12 C20 1.78(5) . ? Ni12 C20' 1.79(2) . ? Ni12 C13 2.068(16) . ? Ni12 C23 2.096(12) . ? Ni12 C24 2.208(12) . ? Ni12 Ni17 2.397(4) . ? Ni12 Ni14 2.605(2) . ? Ni12 Ni15 2.613(2) . ? Ni13 C14 1.646(16) . ? Ni13 C15 1.874(16) . ? Ni13 C23 2.082(12) . ? Ni13 C22 2.108(12) . ? Ni13 Ni14 2.372(3) . ? Ni13 Ni16 2.967(3) . ? Ni14 C18 1.702(15) . ? Ni14 C15 1.859(17) . ? Ni14 C23 1.938(12) . ? Ni14 Ni15 2.826(2) . ? Ni14 Ni17 2.939(4) . ? Ni15 C19 1.75(7) . ? Ni15 C19' 1.79(3) . ? Ni15 C16 1.874(16) . ? Ni15 C24 1.930(12) . ? Ni15 Ni17 2.336(4) . ? Ni15 Ni16 2.353(3) . ? Ni16 C17 1.73(3) . ? Ni16 C17' 1.75(5) . ? Ni16 C16 1.875(16) . ? Ni16 C24 2.055(12) . ? Ni16 C25 2.118(12) . ? C1 O1 1.175(15) . ? C2 O2 1.179(14) . ? C3 O3 1.173(15) . ? C4 O4 1.225(19) . ? C5 O5 1.170(16) . ? C6 O6 1.172(16) . ? C7 O7 1.162(17) . ? C8 O8 1.180(17) . ? C9 O9 1.177(18) . ? C10 O10 1.20(2) . ? C11 O11 1.207(17) . ? C12 O12 1.202(17) . ? C13 O13 1.192(16) . ? C14 O14 1.237(18) . ? C15 O15 1.183(16) . ? C16 O16 1.171(16) . ? C17 O17 1.18(2) . ? C17' O17' 1.18(2) . ? C18 O18 1.176(16) . ? C19 O19 1.182(11) . ? C20 O20 1.186(11) . ? Ni17 C21 1.70(2) . ? Ni17 C19' 1.85(4) . ? Ni17 C20' 1.87(3) . ? C21 O21 1.179(11) . ? C19' O19' 1.183(11) . ? C20' O20' 1.189(11) . ? C22 C23 1.395(16) . ? C24 C25 1.394(17) . ? C26 O26 1.177(11) . ? C27 O27 1.187(10) . ? C28 O28 1.180(10) . ? Ni18 C29 1.63(4) . ? Ni18 C27' 2.31(6) . ? Ni18 C26' 2.15(10) . ? Ni18 C28' 2.24(4) . ? C26' O26' 1.181(11) . ? C27' O27' 1.182(11) . ? C28' O28' 1.176(11) . ? C29 O29 1.182(11) . ? Ni21 C38' 1.55(3) 3 ? Ni21 C32 1.88(2) . ? Ni21 C38 2.02(3) . ? Ni21 C41 2.102(12) . ? Ni21 C37 2.11(4) 3 ? Ni21 C42 2.126(13) . ? Ni21 Ni22 2.359(3) . ? Ni21 Ni28 2.536(3) . ? Ni21 Ni24 2.590(3) 3 ? Ni21 Ni27 2.778(3) . ? Ni22 C44' 1.69(5) . ? Ni22 C44 1.77(4) . ? Ni22 C32 1.85(2) . ? Ni22 C42 1.960(13) . ? Ni22 Ni25 2.573(3) . ? Ni22 Ni29 2.581(8) . ? Ni22 Ni24 2.612(3) . ? Ni22 Ni23 2.845(3) . ? Ni23 C43' 1.64(3) . ? Ni23 C43 1.81(2) . ? Ni23 C35 1.887(16) 3 ? Ni23 C41 1.980(13) 3 ? Ni23 Ni29 2.280(7) . ? Ni23 Ni26 2.343(3) 3 ? Ni23 Ni24 2.594(3) . ? Ni23 Ni28 2.617(3) 3 ? Ni24 C45' 1.73(4) . ? Ni24 C45 1.75(3) . ? Ni24 C42 2.044(14) . ? Ni24 C41 2.102(13) 3 ? Ni24 C37 2.21(3) . ? Ni24 Ni29 2.358(7) . ? Ni24 Ni21 2.590(3) 3 ? Ni24 Ni28 2.625(3) 3 ? Ni24 Ni26 2.645(3) . ? Ni24 Ni25 2.674(3) . ? Ni25 C33 1.624(19) . ? Ni25 C39 1.96(4) . ? Ni25 C34 2.03(2) . ? Ni25 C42 2.095(13) . ? Ni25 C39' 2.11(5) . ? Ni25 Ni27 2.393(3) . ? Ni25 Ni26 2.436(3) . ? Ni26 C39' 1.74(4) . ? Ni26 C35 1.849(17) . ? Ni26 C39 1.95(5) . ? Ni26 C37 2.08(4) . ? Ni26 C42 2.089(12) . ? Ni26 C41 2.124(13) . ? Ni26 Ni23 2.343(3) 3 ? Ni26 Ni27 2.746(3) . ? Ni27 C36 1.75(2) . ? Ni27 C34 1.77(2) . ? Ni27 C42 2.075(13) . ? Ni27 C41 2.089(13) . ? Ni27 Ni28 2.398(3) . ? Ni28 C31 1.661(18) . ? Ni28 C38 1.97(3) . ? Ni28 C41 2.024(14) . ? Ni28 C36 2.04(2) . ? Ni28 Ni23 2.617(3) 3 ? Ni28 Ni24 2.625(3) 3 ? C31 O31 1.190(19) . ? C32 O32 1.20(2) . ? C33 O33 1.24(2) . ? C34 O34 1.20(2) . ? C35 O35 1.183(17) . ? C35 Ni23 1.887(16) 3 ? C36 O36 1.21(2) . ? C37 O37 1.179(11) . ? C37 Ni21 2.11(4) 3 ? C38 O38 1.182(11) . ? C39 O39 1.185(11) . ? C38' O38' 1.184(11) . ? C38' Ni21 1.55(3) 3 ? C39' O39' 1.184(11) . ? C41 C42 1.370(18) . ? C41 Ni23 1.980(13) 3 ? C41 Ni24 2.102(13) 3 ? C43 O43 1.181(11) . ? C44 O44 1.188(11) . ? C45 O45 1.187(11) . ? Ni29 C46 1.55(3) . ? Ni29 C43' 2.02(4) . ? Ni29 C45' 2.15(5) . ? C43' O43' 1.179(11) . ? C44' O44' 1.184(11) . ? C45' O45' 1.185(11) . ? C46 O46 1.177(11) . ? N1 C107 1.469(8) . ? N1 C103 1.473(8) . ? N1 C101 1.472(8) . ? N1 C105 1.475(8) . ? C101 C102 1.533(9) . ? C101 H10A 0.9700 . ? C101 H10B 0.9700 . ? C102 H10C 0.9600 . ? C102 H10D 0.9600 . ? C102 H10E 0.9600 . ? C103 C104 1.539(9) . ? C103 H10F 0.9700 . ? C103 H10G 0.9700 . ? C104 H10H 0.9600 . ? C104 H10I 0.9600 . ? C104 H10J 0.9600 . ? C105 C106 1.535(9) . ? C105 H10K 0.9700 . ? C105 H10L 0.9700 . ? C106 H10M 0.9600 . ? C106 H10N 0.9600 . ? C106 H10O 0.9600 . ? C107 C108 1.529(9) . ? C107 H10P 0.9700 . ? C107 H10Q 0.9700 . ? C108 H10R 0.9600 . ? C108 H10S 0.9600 . ? C108 H10T 0.9600 . ? N2 C203 1.463(8) . ? N2 C207 1.471(8) . ? N2 C201 1.471(9) . ? N2 C205 1.477(9) . ? C201 C202 1.534(9) . ? C201 H20A 0.9700 . ? C201 H20B 0.9700 . ? C202 H20C 0.9600 . ? C202 H20D 0.9600 . ? C202 H20E 0.9600 . ? C203 C204 1.539(9) . ? C203 H20F 0.9700 . ? C203 H20G 0.9700 . ? C204 H20H 0.9600 . ? C204 H20I 0.9600 . ? C204 H20J 0.9600 . ? C205 C206 1.539(9) . ? C205 H20K 0.9700 . ? C205 H20L 0.9700 . ? C206 H20M 0.9600 . ? C206 H20N 0.9600 . ? C206 H20O 0.9600 . ? C207 C208 1.541(9) . ? C207 H20P 0.9700 . ? C207 H20Q 0.9700 . ? C208 H20R 0.9600 . ? C208 H20S 0.9600 . ? C208 H20T 0.9600 . ? N3 C3A5 1.458(14) . ? N3 C301 1.469(9) . ? N3 C307 1.471(9) . ? N3 C303 1.472(9) . ? N3 C3A7 1.474(14) . ? N3 C305 1.478(9) . ? N3 C3A3 1.479(14) . ? N3 C3A1 1.482(14) . ? C301 C302 1.536(9) . ? C301 H30A 0.9700 . ? C301 H30B 0.9700 . ? C302 H30C 0.9600 . ? C302 H30D 0.9600 . ? C302 H30E 0.9600 . ? C303 C304 1.531(9) . ? C303 H30F 0.9700 . ? C303 H30G 0.9700 . ? C304 H30H 0.9600 . ? C304 H30I 0.9600 . ? C304 H30J 0.9600 . ? C305 C306 1.535(9) . ? C305 H30K 0.9700 . ? C305 H30L 0.9700 . ? C306 H30M 0.9600 . ? C306 H30N 0.9600 . ? C306 H30O 0.9600 . ? C307 C308 1.536(9) . ? C307 H30P 0.9700 . ? C307 H30Q 0.9700 . ? C308 H30R 0.9600 . ? C308 H30S 0.9600 . ? C308 H30T 0.9600 . ? C3A1 C3A2 1.535(16) . ? C3A1 H3A1 0.9700 . ? C3A1 H3A2 0.9700 . ? C3A2 H3A3 0.9600 . ? C3A2 H3A4 0.9600 . ? C3A2 H3A5 0.9600 . ? C3A3 C3A4 1.541(16) . ? C3A3 H3A6 0.9700 . ? C3A3 H3A7 0.9700 . ? C3A4 H3A8 0.9600 . ? C3A4 H3A9 0.9600 . ? C3A4 H3AX 0.9600 . ? C3A5 C3A6 1.538(16) . ? C3A5 H3AY 0.9700 . ? C3A5 H3AZ 0.9700 . ? C3A6 H3AA 0.9600 . ? C3A6 H3AB 0.9600 . ? C3A6 H3AC 0.9600 . ? C3A7 C3A8 1.532(16) . ? C3A7 H3AD 0.9700 . ? C3A7 H3AE 0.9700 . ? C3A8 H3AF 0.9600 . ? C3A8 H3AG 0.9600 . ? C3A8 H3AH 0.9600 . ? N4 C407 1.467(9) . ? N4 C403 1.469(9) . ? N4 C405 1.472(9) . ? N4 C401 1.472(9) . ? C401 C402 1.523(9) . ? C401 H40A 0.9700 . ? C401 H40B 0.9700 . ? C402 H40C 0.9600 . ? C402 H40D 0.9600 . ? C402 H40E 0.9600 . ? C403 C404 1.521(9) . ? C403 H40F 0.9700 . ? C403 H40G 0.9700 . ? C404 H40H 0.9600 . ? C404 H40I 0.9600 . ? C404 H40J 0.9600 . ? C405 C406 1.531(9) . ? C405 H40K 0.9700 . ? C405 H40L 0.9700 . ? C406 H40M 0.9600 . ? C406 H40N 0.9600 . ? C406 H40O 0.9600 . ? C407 C408 1.531(9) . ? C407 H40P 0.9700 . ? C407 H40Q 0.9700 . ? C408 H40R 0.9600 . ? C408 H40S 0.9600 . ? C408 H40T 0.9600 . ? N5 C503 1.465(9) . ? N5 C505 1.466(9) . ? N5 C507 1.468(9) . ? N5 C501 1.469(9) . ? C501 C502 1.529(9) . ? C501 H50A 0.9700 . ? C501 H50B 0.9700 . ? C502 H50C 0.9600 . ? C502 H50D 0.9600 . ? C502 H50E 0.9600 . ? C503 C504 1.525(9) . ? C503 H50F 0.9700 . ? C503 H50G 0.9700 . ? C504 H50H 0.9600 . ? C504 H50I 0.9600 . ? C504 H50J 0.9600 . ? C505 C506 1.515(9) . ? C505 H50K 0.9700 . ? C505 H50L 0.9700 . ? C506 H50M 0.9600 . ? C506 H50N 0.9600 . ? C506 H50O 0.9600 . ? C507 C508 1.520(9) . ? C507 H50P 0.9700 . ? C507 H50Q 0.9700 . ? C508 H50R 0.9600 . ? C508 H50S 0.9600 . ? C508 H50T 0.9600 . ? N6 C6A7 1.443(14) . ? N6 C607 1.460(9) . ? N6 C605 1.472(9) . ? N6 C601 1.474(9) . ? N6 C6A5 1.476(14) . ? N6 C603 1.481(9) . ? N6 C6A1 1.486(14) . ? N6 C6A3 1.494(14) . ? C601 C602 1.534(9) . ? C601 H60A 0.9700 . ? C601 H60B 0.9700 . ? C602 H60C 0.9600 . ? C602 H60D 0.9600 . ? C602 H60E 0.9600 . ? C603 C604 1.530(9) . ? C603 H60F 0.9700 . ? C603 H60G 0.9700 . ? C604 H60H 0.9600 . ? C604 H60I 0.9600 . ? C604 H60J 0.9600 . ? C605 C606 1.526(9) . ? C605 H60K 0.9700 . ? C605 H60L 0.9700 . ? C606 H60M 0.9600 . ? C606 H60N 0.9600 . ? C606 H60O 0.9600 . ? C607 C608 1.529(9) . ? C607 H60P 0.9700 . ? C607 H60Q 0.9700 . ? C608 H60R 0.9600 . ? C608 H60S 0.9600 . ? C608 H60T 0.9600 . ? C6A1 C6A2 1.535(16) . ? C6A1 H6A1 0.9700 . ? C6A1 H6A2 0.9700 . ? C6A2 H6A3 0.9600 . ? C6A2 H6A4 0.9600 . ? C6A2 H6A5 0.9600 . ? C6A3 C6A4 1.525(16) . ? C6A3 H6A6 0.9700 . ? C6A3 H6A7 0.9700 . ? C6A4 H6A8 0.9600 . ? C6A4 H6A9 0.9600 . ? C6A4 H6AX 0.9600 . ? C6A5 C6A6 1.540(16) . ? C6A5 H6AY 0.9700 . ? C6A5 H6AZ 0.9700 . ? C6A6 H6AA 0.9600 . ? C6A6 H6AB 0.9600 . ? C6A6 H6AC 0.9600 . ? C6A7 C6A8 1.529(16) . ? C6A7 H6AD 0.9700 . ? C6A7 H6AE 0.9700 . ? C6A8 H6AF 0.9600 . ? C6A8 H6AG 0.9600 . ? C6A8 H6AH 0.9600 . ? C701 C702 1.518(9) . ? C701 H70A 0.9600 . ? C701 H70B 0.9600 . ? C701 H70C 0.9600 . ? C702 O704 1.203(10) . ? C702 C703 1.515(10) . ? C703 H70D 0.9600 . ? C703 H70E 0.9600 . ? C703 H70F 0.9600 . ? C801 C802 1.525(10) . ? C801 H80A 0.9600 . ? C801 H80B 0.9600 . ? C801 H80C 0.9600 . ? C802 O804 1.210(10) . ? C802 C803 1.526(10) . ? C803 H80D 0.9600 . ? C803 H80E 0.9600 . ? C803 H80F 0.9600 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C2 Ni1 C1 103.3(6) . . ? C2 Ni1 C13 100.2(7) . . ? C1 Ni1 C13 90.4(7) . . ? C2 Ni1 C23 141.1(5) . . ? C1 Ni1 C23 105.7(5) . . ? C13 Ni1 C23 104.9(6) . . ? C2 Ni1 C22 103.2(5) . . ? C1 Ni1 C22 132.8(6) . . ? C13 Ni1 C22 122.0(5) . . ? C23 Ni1 C22 38.0(4) . . ? C2 Ni1 Ni2 51.1(4) . . ? C1 Ni1 Ni2 138.1(5) . . ? C13 Ni1 Ni2 123.3(5) . . ? C23 Ni1 Ni2 90.1(3) . . ? C22 Ni1 Ni2 52.1(3) . . ? C2 Ni1 Ni5 146.0(4) . . ? C1 Ni1 Ni5 50.7(4) . . ? C13 Ni1 Ni5 101.3(5) . . ? C23 Ni1 Ni5 54.9(3) . . ? C22 Ni1 Ni5 87.2(3) . . ? Ni2 Ni1 Ni5 130.19(9) . . ? C2 Ni1 Ni12 145.6(4) . . ? C1 Ni1 Ni12 98.0(4) . . ? C13 Ni1 Ni12 52.5(5) . . ? C23 Ni1 Ni12 52.7(3) . . ? C22 Ni1 Ni12 80.6(3) . . ? Ni2 Ni1 Ni12 121.66(8) . . ? Ni5 Ni1 Ni12 67.47(7) . . ? C2 Ni1 Ni6 109.2(4) . . ? C1 Ni1 Ni6 86.7(5) . . ? C13 Ni1 Ni6 150.4(5) . . ? C23 Ni1 Ni6 48.4(3) . . ? C22 Ni1 Ni6 47.8(3) . . ? Ni2 Ni1 Ni6 75.27(7) . . ? Ni5 Ni1 Ni6 55.13(7) . . ? Ni12 Ni1 Ni6 98.71(7) . . ? C26 Ni2 C26' 10(3) . . ? C26 Ni2 C2 101.8(16) . . ? C26' Ni2 C2 106(4) . . ? C26 Ni2 C22 147.6(15) . . ? C26' Ni2 C22 141(3) . . ? C2 Ni2 C22 109.8(5) . . ? C26 Ni2 Ni1 152.1(16) . . ? C26' Ni2 Ni1 153(4) . . ? C2 Ni2 Ni1 50.7(4) . . ? C22 Ni2 Ni1 59.1(3) . . ? C26 Ni2 Ni18 55.5(15) . . ? C26' Ni2 Ni18 59(4) . . ? C2 Ni2 Ni18 134.8(5) . . ? C22 Ni2 Ni18 103.5(4) . . ? Ni1 Ni2 Ni18 145.15(18) . . ? C26 Ni2 Ni8 107.5(16) . . ? C26' Ni2 Ni8 108(4) . . ? C2 Ni2 Ni8 139.2(4) . . ? C22 Ni2 Ni8 50.6(3) . . ? Ni1 Ni2 Ni8 98.96(8) . . ? Ni18 Ni2 Ni8 53.78(18) . . ? C26 Ni2 Ni7 99.2(13) . . ? C26' Ni2 Ni7 91(3) . . ? C2 Ni2 Ni7 142.5(4) . . ? C22 Ni2 Ni7 50.3(3) . . ? Ni1 Ni2 Ni7 102.16(8) . . ? Ni18 Ni2 Ni7 82.6(2) . . ? Ni8 Ni2 Ni7 58.72(7) . . ? C26 Ni2 Ni3 95.7(12) . . ? C26' Ni2 Ni3 104(3) . . ? C2 Ni2 Ni3 93.9(4) . . ? C22 Ni2 Ni3 89.3(3) . . ? Ni1 Ni2 Ni3 91.52(7) . . ? Ni18 Ni2 Ni3 56.26(17) . . ? Ni8 Ni2 Ni3 55.95(6) . . ? Ni7 Ni2 Ni3 114.53(8) . . ? C27 Ni3 C27' 14(2) . . ? C27 Ni3 C3 103.7(10) . . ? C27' Ni3 C3 108(2) . . ? C27 Ni3 C25 145.5(9) . . ? C27' Ni3 C25 137.1(19) . . ? C3 Ni3 C25 110.1(6) . . ? C27 Ni3 Ni4 154.5(9) . . ? C27' Ni3 Ni4 154(2) . . ? C3 Ni3 Ni4 50.9(4) . . ? C25 Ni3 Ni4 59.4(4) . . ? C27 Ni3 Ni18 55.6(9) . . ? C27' Ni3 Ni18 62(2) . . ? C3 Ni3 Ni18 137.1(5) . . ? C25 Ni3 Ni18 100.9(4) . . ? Ni4 Ni3 Ni18 142.29(17) . . ? C27 Ni3 Ni8 105.8(9) . . ? C27' Ni3 Ni8 107(2) . . ? C3 Ni3 Ni8 141.0(4) . . ? C25 Ni3 Ni8 49.2(3) . . ? Ni4 Ni3 Ni8 97.99(8) . . ? Ni18 Ni3 Ni8 52.39(18) . . ? C27 Ni3 Ni9 97.8(8) . . ? C27' Ni3 Ni9 86.8(18) . . ? C3 Ni3 Ni9 139.5(5) . . ? C25 Ni3 Ni9 50.9(4) . . ? Ni4 Ni3 Ni9 102.18(9) . . ? Ni18 Ni3 Ni9 83.24(18) . . ? Ni8 Ni3 Ni9 59.51(7) . . ? C27 Ni3 Ni2 93.5(7) . . ? C27' Ni3 Ni2 105.8(18) . . ? C3 Ni3 Ni2 98.1(5) . . ? C25 Ni3 Ni2 88.8(3) . . ? Ni4 Ni3 Ni2 92.50(8) . . ? Ni18 Ni3 Ni2 52.78(15) . . ? Ni8 Ni3 Ni2 55.33(6) . . ? Ni9 Ni3 Ni2 114.51(8) . . ? C3 Ni4 C4 104.0(7) . . ? C3 Ni4 C13 99.9(7) . . ? C4 Ni4 C13 91.4(7) . . ? C3 Ni4 C24 140.5(6) . . ? C4 Ni4 C24 102.6(6) . . ? C13 Ni4 C24 108.1(6) . . ? C3 Ni4 C25 103.1(6) . . ? C4 Ni4 C25 130.2(7) . . ? C13 Ni4 C25 123.7(5) . . ? C24 Ni4 C25 37.8(5) . . ? C3 Ni4 Ni3 51.4(4) . . ? C4 Ni4 Ni3 138.7(6) . . ? C13 Ni4 Ni3 122.3(5) . . ? C24 Ni4 Ni3 89.6(4) . . ? C25 Ni4 Ni3 51.9(3) . . ? C3 Ni4 Ni11 146.4(5) . . ? C4 Ni4 Ni11 49.7(6) . . ? C13 Ni4 Ni11 101.1(5) . . ? C24 Ni4 Ni11 53.2(3) . . ? C25 Ni4 Ni11 86.6(3) . . ? Ni3 Ni4 Ni11 130.98(10) . . ? C3 Ni4 Ni12 146.5(5) . . ? C4 Ni4 Ni12 96.4(6) . . ? C13 Ni4 Ni12 52.8(5) . . ? C24 Ni4 Ni12 55.7(3) . . ? C25 Ni4 Ni12 82.6(3) . . ? Ni3 Ni4 Ni12 122.34(9) . . ? Ni11 Ni4 Ni12 65.92(7) . . ? C3 Ni4 Ni10 106.4(5) . . ? C4 Ni4 Ni10 83.6(6) . . ? C13 Ni4 Ni10 153.7(5) . . ? C24 Ni4 Ni10 48.8(3) . . ? C25 Ni4 Ni10 48.8(3) . . ? Ni3 Ni4 Ni10 75.26(8) . . ? Ni11 Ni4 Ni10 56.51(8) . . ? Ni12 Ni4 Ni10 101.99(8) . . ? C5 Ni5 C1 103.8(7) . . ? C5 Ni5 C23 146.2(6) . . ? C1 Ni5 C23 105.0(5) . . ? C5 Ni5 C6 98.4(6) . . ? C1 Ni5 C6 94.8(6) . . ? C23 Ni5 C6 96.6(5) . . ? C5 Ni5 Ni1 148.9(5) . . ? C1 Ni5 Ni1 50.2(4) . . ? C23 Ni5 Ni1 54.8(3) . . ? C6 Ni5 Ni1 100.3(4) . . ? C5 Ni5 Ni6 137.8(5) . . ? C1 Ni5 Ni6 97.1(5) . . ? C23 Ni5 Ni6 54.4(3) . . ? C6 Ni5 Ni6 43.0(4) . . ? Ni1 Ni5 Ni6 69.85(7) . . ? C5 Ni5 Ni14 99.0(5) . . ? C1 Ni5 Ni14 147.3(5) . . ? C23 Ni5 Ni14 47.7(3) . . ? C6 Ni5 Ni14 104.9(4) . . ? Ni1 Ni5 Ni14 99.93(8) . . ? Ni6 Ni5 Ni14 80.87(8) . . ? C5 Ni5 Ni12 113.7(5) . . ? C1 Ni5 Ni12 90.7(5) . . ? C23 Ni5 Ni12 48.9(3) . . ? C6 Ni5 Ni12 145.1(4) . . ? Ni1 Ni5 Ni12 58.34(6) . . ? Ni6 Ni5 Ni12 102.11(8) . . ? Ni14 Ni5 Ni12 58.42(6) . . ? C6 Ni6 C7 101.2(8) . . ? C6 Ni6 C22 151.4(7) . . ? C7 Ni6 C22 106.6(6) . . ? C6 Ni6 C23 116.8(7) . . ? C7 Ni6 C23 139.9(6) . . ? C22 Ni6 C23 39.1(5) . . ? C6 Ni6 Ni7 154.5(6) . . ? C7 Ni6 Ni7 53.4(5) . . ? C22 Ni6 Ni7 53.5(3) . . ? C23 Ni6 Ni7 88.3(3) . . ? C6 Ni6 Ni5 62.9(6) . . ? C7 Ni6 Ni5 164.0(6) . . ? C22 Ni6 Ni5 89.4(3) . . ? C23 Ni6 Ni5 55.0(3) . . ? Ni7 Ni6 Ni5 142.53(9) . . ? C6 Ni6 Ni1 103.3(6) . . ? C7 Ni6 Ni1 136.0(6) . . ? C22 Ni6 Ni1 50.9(3) . . ? C23 Ni6 Ni1 48.8(3) . . ? Ni7 Ni6 Ni1 96.64(8) . . ? Ni5 Ni6 Ni1 55.02(6) . . ? C6 Ni6 Ni13 135.2(6) . . ? C7 Ni6 Ni13 96.3(6) . . ? C22 Ni6 Ni13 48.3(3) . . ? C23 Ni6 Ni13 47.6(3) . . ? Ni7 Ni6 Ni13 58.72(7) . . ? Ni5 Ni6 Ni13 94.67(8) . . ? Ni1 Ni6 Ni13 91.45(7) . . ? C8 Ni7 C7 96.2(8) . . ? C8 Ni7 C22 157.7(6) . . ? C7 Ni7 C22 103.0(6) . . ? C8 Ni7 Ni6 143.7(6) . . ? C7 Ni7 Ni6 48.0(5) . . ? C22 Ni7 Ni6 55.2(3) . . ? C8 Ni7 Ni8 109.7(6) . . ? C7 Ni7 Ni8 153.8(5) . . ? C22 Ni7 Ni8 50.9(3) . . ? Ni6 Ni7 Ni8 105.89(8) . . ? C8 Ni7 Ni13 134.7(6) . . ? C7 Ni7 Ni13 100.3(6) . . ? C22 Ni7 Ni13 52.8(3) . . ? Ni6 Ni7 Ni13 68.62(7) . . ? Ni8 Ni7 Ni13 64.56(7) . . ? C8 Ni7 Ni2 114.2(6) . . ? C7 Ni7 Ni2 106.3(5) . . ? C22 Ni7 Ni2 49.3(3) . . ? Ni6 Ni7 Ni2 78.04(8) . . ? Ni8 Ni7 Ni2 59.70(7) . . ? Ni13 Ni7 Ni2 101.14(8) . . ? C28' Ni8 C28 23.3(16) . . ? C28' Ni8 C25 126.5(18) . . ? C28 Ni8 C25 134.8(9) . . ? C28' Ni8 C22 141.9(17) . . ? C28 Ni8 C22 131.5(9) . . ? C25 Ni8 C22 90.5(5) . . ? C28' Ni8 Ni18 67.8(17) . . ? C28 Ni8 Ni18 46.0(8) . . ? C25 Ni8 Ni18 112.2(4) . . ? C22 Ni8 Ni18 109.7(4) . . ? C28' Ni8 Ni7 90.5(17) . . ? C28 Ni8 Ni7 82.5(8) . . ? C25 Ni8 Ni7 142.0(4) . . ? C22 Ni8 Ni7 51.7(4) . . ? Ni18 Ni8 Ni7 87.94(19) . . ? C28' Ni8 Ni2 120.6(17) . . ? C28 Ni8 Ni2 97.8(8) . . ? C25 Ni8 Ni2 99.6(3) . . ? C22 Ni8 Ni2 50.3(3) . . ? Ni18 Ni8 Ni2 60.48(18) . . ? Ni7 Ni8 Ni2 61.58(7) . . ? C28' Ni8 Ni9 75.3(17) . . ? C28 Ni8 Ni9 85.5(8) . . ? C25 Ni8 Ni9 51.5(4) . . ? C22 Ni8 Ni9 142.0(4) . . ? Ni18 Ni8 Ni9 89.79(18) . . ? Ni7 Ni8 Ni9 165.39(9) . . ? Ni2 Ni8 Ni9 128.80(9) . . ? C28' Ni8 Ni3 111.7(16) . . ? C28 Ni8 Ni3 100.5(8) . . ? C25 Ni8 Ni3 49.8(3) . . ? C22 Ni8 Ni3 98.8(3) . . ? Ni18 Ni8 Ni3 63.2(2) . . ? Ni7 Ni8 Ni3 130.10(9) . . ? Ni2 Ni8 Ni3 68.72(7) . . ? Ni9 Ni8 Ni3 60.52(7) . . ? C28' Ni8 Ni13 110.0(17) . . ? C28 Ni8 Ni13 122.2(8) . . ? C25 Ni8 Ni13 96.0(4) . . ? C22 Ni8 Ni13 50.1(3) . . ? Ni18 Ni8 Ni13 146.5(2) . . ? Ni7 Ni8 Ni13 58.54(7) . . ? Ni2 Ni8 Ni13 98.39(7) . . ? Ni9 Ni8 Ni13 122.80(9) . . ? Ni3 Ni8 Ni13 137.02(9) . . ? C28' Ni8 Ni16 99.3(17) . . ? C28 Ni8 Ni16 121.9(8) . . ? C25 Ni8 Ni16 50.2(3) . . ? C22 Ni8 Ni16 98.8(4) . . ? Ni18 Ni8 Ni16 147.21(19) . . ? Ni7 Ni8 Ni16 123.26(9) . . ? Ni2 Ni8 Ni16 140.15(8) . . ? Ni9 Ni8 Ni16 57.45(7) . . ? Ni3 Ni8 Ni16 97.50(8) . . ? Ni13 Ni8 Ni16 65.67(7) . . ? C9 Ni9 C10 97.8(9) . . ? C9 Ni9 C25 158.3(7) . . ? C10 Ni9 C25 101.5(7) . . ? C9 Ni9 Ni10 145.1(6) . . ? C10 Ni9 Ni10 47.5(6) . . ? C25 Ni9 Ni10 55.5(3) . . ? C9 Ni9 C17' 91.0(15) . . ? C10 Ni9 C17' 104.2(18) . . ? C25 Ni9 C17' 93.9(14) . . ? Ni10 Ni9 C17' 94.5(15) . . ? C9 Ni9 Ni16 130.4(6) . . ? C10 Ni9 Ni16 104.2(7) . . ? C25 Ni9 Ni16 53.5(3) . . ? Ni10 Ni9 Ni16 67.96(8) . . ? C17' Ni9 Ni16 40.8(14) . . ? C9 Ni9 Ni8 110.4(6) . . ? C10 Ni9 Ni8 150.2(7) . . ? C25 Ni9 Ni8 49.2(3) . . ? Ni10 Ni9 Ni8 104.42(9) . . ? C17' Ni9 Ni8 85.3(16) . . ? Ni16 Ni9 Ni8 64.80(7) . . ? C9 Ni9 Ni3 117.9(6) . . ? C10 Ni9 Ni3 98.7(6) . . ? C25 Ni9 Ni3 49.2(3) . . ? Ni10 Ni9 Ni3 77.44(8) . . ? C17' Ni9 Ni3 140.1(14) . . ? Ni16 Ni9 Ni3 102.06(8) . . ? Ni8 Ni9 Ni3 59.97(7) . . ? C11 Ni10 C10 102.0(9) . . ? C11 Ni10 C24 116.8(7) . . ? C10 Ni10 C24 140.2(8) . . ? C11 Ni10 C25 152.8(7) . . ? C10 Ni10 C25 104.4(8) . . ? C24 Ni10 C25 39.1(5) . . ? C11 Ni10 Ni9 153.5(6) . . ? C10 Ni10 Ni9 52.3(7) . . ? C24 Ni10 Ni9 88.1(4) . . ? C25 Ni10 Ni9 53.7(4) . . ? C11 Ni10 Ni11 65.2(6) . . ? C10 Ni10 Ni11 166.5(7) . . ? C24 Ni10 Ni11 53.2(4) . . ? C25 Ni10 Ni11 87.9(4) . . ? Ni9 Ni10 Ni11 140.95(10) . . ? C11 Ni10 Ni4 105.3(6) . . ? C10 Ni10 Ni4 128.5(7) . . ? C24 Ni10 Ni4 50.4(3) . . ? C25 Ni10 Ni4 51.7(3) . . ? Ni9 Ni10 Ni4 97.46(8) . . ? Ni11 Ni10 Ni4 55.63(7) . . ? C11 Ni10 Ni16 131.4(5) . . ? C10 Ni10 Ni16 100.2(7) . . ? C24 Ni10 Ni16 47.6(3) . . ? C25 Ni10 Ni16 49.3(3) . . ? Ni9 Ni10 Ni16 58.83(8) . . ? Ni11 Ni10 Ni16 92.09(8) . . ? Ni4 Ni10 Ni16 93.32(8) . . ? C12 Ni11 C4 106.5(8) . . ? C12 Ni11 C24 146.4(6) . . ? C4 Ni11 C24 105.5(6) . . ? C12 Ni11 C11 96.0(7) . . ? C4 Ni11 C11 89.4(7) . . ? C24 Ni11 C11 94.2(5) . . ? C12 Ni11 Ni4 152.6(6) . . ? C4 Ni11 Ni4 49.9(6) . . ? C24 Ni11 Ni4 55.8(3) . . ? C11 Ni11 Ni4 97.2(4) . . ? C12 Ni11 Ni10 134.1(6) . . ? C4 Ni11 Ni10 91.8(6) . . ? C24 Ni11 Ni10 53.9(3) . . ? C11 Ni11 Ni10 41.3(4) . . ? Ni4 Ni11 Ni10 67.86(8) . . ? C12 Ni11 Ni15 99.1(5) . . ? C4 Ni11 Ni15 147.4(6) . . ? C24 Ni11 Ni15 47.3(3) . . ? C11 Ni11 Ni15 107.8(4) . . ? Ni4 Ni11 Ni15 99.45(8) . . ? Ni10 Ni11 Ni15 84.28(9) . . ? C12 Ni11 Ni12 116.1(6) . . ? C4 Ni11 Ni12 91.2(6) . . ? C24 Ni11 Ni12 53.2(3) . . ? C11 Ni11 Ni12 146.1(4) . . ? Ni4 Ni11 Ni12 58.88(7) . . ? Ni10 Ni11 Ni12 104.84(8) . . ? Ni15 Ni11 Ni12 59.08(6) . . ? C20 Ni12 C20' 15(2) . . ? C20 Ni12 C13 98(2) . . ? C20' Ni12 C13 86.7(9) . . ? C20 Ni12 C23 124(2) . . ? C20' Ni12 C23 136.3(10) . . ? C13 Ni12 C23 102.9(5) . . ? C20 Ni12 C24 137(3) . . ? C20' Ni12 C24 132.0(11) . . ? C13 Ni12 C24 102.4(6) . . ? C23 Ni12 C24 88.0(4) . . ? C20 Ni12 Ni17 44(2) . . ? C20' Ni12 Ni17 50.6(9) . . ? C13 Ni12 Ni17 134.2(4) . . ? C23 Ni12 Ni17 119.0(3) . . ? C24 Ni12 Ni17 97.0(3) . . ? C20 Ni12 Ni4 129(2) . . ? C20' Ni12 Ni4 114.3(9) . . ? C13 Ni12 Ni4 49.9(5) . . ? C23 Ni12 Ni4 103.7(3) . . ? C24 Ni12 Ni4 52.8(3) . . ? Ni17 Ni12 Ni4 127.13(12) . . ? C20 Ni12 Ni1 118(2) . . ? C20' Ni12 Ni1 117.5(10) . . ? C13 Ni12 Ni1 50.4(4) . . ? C23 Ni12 Ni1 52.9(3) . . ? C24 Ni12 Ni1 103.4(3) . . ? Ni17 Ni12 Ni1 157.28(12) . . ? Ni4 Ni12 Ni1 74.29(7) . . ? C20 Ni12 Ni14 89(2) . . ? C20' Ni12 Ni14 103.3(8) . . ? C13 Ni12 Ni14 144.5(4) . . ? C23 Ni12 Ni14 47.2(3) . . ? C24 Ni12 Ni14 95.8(3) . . ? Ni17 Ni12 Ni14 71.85(11) . . ? Ni4 Ni12 Ni14 141.45(9) . . ? Ni1 Ni12 Ni14 96.00(7) . . ? C20 Ni12 Ni15 100(2) . . ? C20' Ni12 Ni15 104.1(9) . . ? C13 Ni12 Ni15 145.4(5) . . ? C23 Ni12 Ni15 91.8(3) . . ? C24 Ni12 Ni15 46.3(3) . . ? Ni17 Ni12 Ni15 55.38(10) . . ? Ni4 Ni12 Ni15 96.33(8) . . ? Ni1 Ni12 Ni15 137.64(8) . . ? Ni14 Ni12 Ni15 65.58(7) . . ? C20 Ni12 Ni11 95(2) . . ? C20' Ni12 Ni11 85.1(10) . . ? C13 Ni12 Ni11 90.7(4) . . ? C23 Ni12 Ni11 136.2(3) . . ? C24 Ni12 Ni11 48.3(3) . . ? Ni17 Ni12 Ni11 72.19(11) . . ? Ni4 Ni12 Ni11 55.21(6) . . ? Ni1 Ni12 Ni11 129.47(8) . . ? Ni14 Ni12 Ni11 123.62(8) . . ? Ni15 Ni12 Ni11 58.39(7) . . ? C20 Ni12 Ni5 80(2) . . ? C20' Ni12 Ni5 89.2(10) . . ? C13 Ni12 Ni5 89.5(5) . . ? C23 Ni12 Ni5 49.1(3) . . ? C24 Ni12 Ni5 137.1(3) . . ? Ni17 Ni12 Ni5 103.65(11) . . ? Ni4 Ni12 Ni5 128.37(8) . . ? Ni1 Ni12 Ni5 54.19(6) . . ? Ni14 Ni12 Ni5 57.27(6) . . ? Ni15 Ni12 Ni5 122.85(8) . . ? Ni11 Ni12 Ni5 174.24(9) . . ? C14 Ni13 C15 98.9(8) . . ? C14 Ni13 C23 158.3(7) . . ? C15 Ni13 C23 101.1(6) . . ? C14 Ni13 C22 120.2(7) . . ? C15 Ni13 C22 139.8(6) . . ? C23 Ni13 C22 38.9(5) . . ? C14 Ni13 Ni14 149.1(6) . . ? C15 Ni13 Ni14 50.3(5) . . ? C23 Ni13 Ni14 51.1(3) . . ? C22 Ni13 Ni14 90.0(3) . . ? C14 Ni13 Ni7 74.8(6) . . ? C15 Ni13 Ni7 147.8(5) . . ? C23 Ni13 Ni7 83.8(3) . . ? C22 Ni13 Ni7 50.2(3) . . ? Ni14 Ni13 Ni7 128.62(9) . . ? C14 Ni13 Ni8 86.4(6) . . ? C15 Ni13 Ni8 155.3(5) . . ? C23 Ni13 Ni8 79.0(3) . . ? C22 Ni13 Ni8 47.0(3) . . ? Ni14 Ni13 Ni8 122.33(9) . . ? Ni7 Ni13 Ni8 56.90(7) . . ? C14 Ni13 Ni6 117.2(6) . . ? C15 Ni13 Ni6 107.9(5) . . ? C23 Ni13 Ni6 47.8(3) . . ? C22 Ni13 Ni6 47.4(3) . . ? Ni14 Ni13 Ni6 76.98(7) . . ? Ni7 Ni13 Ni6 52.66(7) . . ? Ni8 Ni13 Ni6 90.55(7) . . ? C14 Ni13 Ni16 92.3(6) . . ? C15 Ni13 Ni16 98.1(5) . . ? C23 Ni13 Ni16 93.3(3) . . ? C22 Ni13 Ni16 90.1(3) . . ? Ni14 Ni13 Ni16 94.50(9) . . ? Ni7 Ni13 Ni16 113.51(8) . . ? Ni8 Ni13 Ni16 57.40(6) . . ? Ni6 Ni13 Ni16 135.87(8) . . ? C18 Ni14 C15 98.6(7) . . ? C18 Ni14 C23 152.2(6) . . ? C15 Ni14 C23 107.2(6) . . ? C18 Ni14 Ni13 149.2(5) . . ? C15 Ni14 Ni13 50.8(5) . . ? C23 Ni14 Ni13 56.7(3) . . ? C18 Ni14 Ni5 100.0(5) . . ? C15 Ni14 Ni5 138.1(5) . . ? C23 Ni14 Ni5 53.4(3) . . ? Ni13 Ni14 Ni5 102.37(8) . . ? C18 Ni14 Ni12 112.3(5) . . ? C15 Ni14 Ni12 138.4(5) . . ? C23 Ni14 Ni12 52.5(4) . . ? Ni13 Ni14 Ni12 96.50(8) . . ? Ni5 Ni14 Ni12 64.31(7) . . ? C18 Ni14 Ni15 101.2(5) . . ? C15 Ni14 Ni15 90.6(5) . . ? C23 Ni14 Ni15 89.0(4) . . ? Ni13 Ni14 Ni15 84.75(8) . . ? Ni5 Ni14 Ni15 121.66(8) . . ? Ni12 Ni14 Ni15 57.35(6) . . ? C18 Ni14 Ni17 67.5(5) . . ? C15 Ni14 Ni17 127.2(5) . . ? C23 Ni14 Ni17 103.2(4) . . ? Ni13 Ni14 Ni17 130.73(11) . . ? Ni5 Ni14 Ni17 94.55(10) . . ? Ni12 Ni14 Ni17 50.80(8) . . ? Ni15 Ni14 Ni17 47.76(8) . . ? C19 Ni15 C19' 9(3) . . ? C19 Ni15 C16 91(3) . . ? C19' Ni15 C16 98.7(12) . . ? C19 Ni15 C24 159(3) . . ? C19' Ni15 C24 149.8(11) . . ? C16 Ni15 C24 107.1(6) . . ? C19 Ni15 Ni17 57(3) . . ? C19' Ni15 Ni17 51.3(12) . . ? C16 Ni15 Ni17 144.3(5) . . ? C24 Ni15 Ni17 107.6(4) . . ? C19 Ni15 Ni16 142(3) . . ? C19' Ni15 Ni16 148.6(12) . . ? C16 Ni15 Ni16 51.1(5) . . ? C24 Ni15 Ni16 56.3(4) . . ? Ni17 Ni15 Ni16 159.59(12) . . ? C19 Ni15 Ni11 107(3) . . ? C19' Ni15 Ni11 98.7(11) . . ? C16 Ni15 Ni11 135.2(5) . . ? C24 Ni15 Ni11 51.6(4) . . ? Ni17 Ni15 Ni11 75.19(12) . . ? Ni16 Ni15 Ni11 99.07(9) . . ? C19 Ni15 Ni12 114(3) . . ? C19' Ni15 Ni12 108.9(12) . . ? C16 Ni15 Ni12 144.6(5) . . ? C24 Ni15 Ni12 55.7(4) . . ? Ni17 Ni15 Ni12 57.62(10) . . ? Ni16 Ni15 Ni12 102.20(8) . . ? Ni11 Ni15 Ni12 62.53(7) . . ? C19 Ni15 Ni14 92(4) . . ? C19' Ni15 Ni14 94.8(15) . . ? C16 Ni15 Ni14 99.9(5) . . ? C24 Ni15 Ni14 95.8(4) . . ? Ni17 Ni15 Ni14 68.67(11) . . ? Ni16 Ni15 Ni14 98.71(9) . . ? Ni11 Ni15 Ni14 119.28(8) . . ? Ni12 Ni15 Ni14 57.07(6) . . ? C17 Ni16 C17' 21(3) . . ? C17 Ni16 C16 100.7(16) . . ? C17' Ni16 C16 100(2) . . ? C17 Ni16 C24 157.0(15) . . ? C17' Ni16 C24 149(2) . . ? C16 Ni16 C24 102.3(6) . . ? C17 Ni16 C25 118.2(15) . . ? C17' Ni16 C25 117(2) . . ? C16 Ni16 C25 141.0(6) . . ? C24 Ni16 C25 39.0(5) . . ? C17 Ni16 Ni15 151.5(15) . . ? C17' Ni16 Ni15 148(2) . . ? C16 Ni16 Ni15 51.1(5) . . ? C24 Ni16 Ni15 51.4(4) . . ? C25 Ni16 Ni15 89.9(4) . . ? C17 Ni16 Ni9 74.2(15) . . ? C17' Ni16 Ni9 67(2) . . ? C16 Ni16 Ni9 157.1(5) . . ? C24 Ni16 Ni9 84.3(4) . . ? C25 Ni16 Ni9 50.8(3) . . ? Ni15 Ni16 Ni9 133.07(10) . . ? C17 Ni16 Ni8 84.3(14) . . ? C17' Ni16 Ni8 96(2) . . ? C16 Ni16 Ni8 144.9(5) . . ? C24 Ni16 Ni8 77.4(3) . . ? C25 Ni16 Ni8 45.7(3) . . ? Ni15 Ni16 Ni8 115.78(9) . . ? Ni9 Ni16 Ni8 57.76(7) . . ? C17 Ni16 Ni10 119.1(15) . . ? C17' Ni16 Ni10 102(2) . . ? C16 Ni16 Ni10 115.7(5) . . ? C24 Ni16 Ni10 48.3(3) . . ? C25 Ni16 Ni10 48.4(3) . . ? Ni15 Ni16 Ni10 82.47(8) . . ? Ni9 Ni16 Ni10 53.21(8) . . ? Ni8 Ni16 Ni10 90.62(7) . . ? C17 Ni16 Ni13 94.3(14) . . ? C17' Ni16 Ni13 115(2) . . ? C16 Ni16 Ni13 88.0(5) . . ? C24 Ni16 Ni13 87.4(3) . . ? C25 Ni16 Ni13 86.2(3) . . ? Ni15 Ni16 Ni13 81.97(8) . . ? Ni9 Ni16 Ni13 114.41(9) . . ? Ni8 Ni16 Ni13 56.92(6) . . ? Ni10 Ni16 Ni13 131.74(8) . . ? O1 C1 Ni1 141.3(12) . . ? O1 C1 Ni5 139.6(12) . . ? Ni1 C1 Ni5 79.1(5) . . ? O2 C2 Ni1 142.5(12) . . ? O2 C2 Ni2 139.3(11) . . ? Ni1 C2 Ni2 78.2(5) . . ? O3 C3 Ni4 142.2(12) . . ? O3 C3 Ni3 140.0(12) . . ? Ni4 C3 Ni3 77.7(5) . . ? O4 C4 Ni11 141.5(15) . . ? O4 C4 Ni4 138.1(15) . . ? Ni11 C4 Ni4 80.4(7) . . ? O5 C5 Ni5 177.9(14) . . ? O6 C6 Ni6 162.4(16) . . ? O6 C6 Ni5 123.4(13) . . ? Ni6 C6 Ni5 74.0(6) . . ? O7 C7 Ni6 148.6(16) . . ? O7 C7 Ni7 132.0(15) . . ? Ni6 C7 Ni7 78.6(6) . . ? O8 C8 Ni7 177.0(16) . . ? O9 C9 Ni9 177.4(17) . . ? O10 C10 Ni10 147.4(19) . . ? O10 C10 Ni9 132.4(18) . . ? Ni10 C10 Ni9 80.2(9) . . ? O11 C11 Ni10 162.5(15) . . ? O11 C11 Ni11 122.9(13) . . ? Ni10 C11 Ni11 73.5(5) . . ? O12 C12 Ni11 176.0(17) . . ? O13 C13 Ni4 124.4(13) . . ? O13 C13 Ni1 123.6(12) . . ? Ni4 C13 Ni1 100.2(7) . . ? O13 C13 Ni12 139.6(13) . . ? Ni4 C13 Ni12 77.3(5) . . ? Ni1 C13 Ni12 77.1(5) . . ? O14 C14 Ni13 177.1(16) . . ? O15 C15 Ni14 140.9(15) . . ? O15 C15 Ni13 140.2(15) . . ? Ni14 C15 Ni13 78.9(6) . . ? O16 C16 Ni15 139.7(14) . . ? O16 C16 Ni16 142.5(14) . . ? Ni15 C16 Ni16 77.7(6) . . ? O17 C17 Ni16 174(4) . . ? O17' C17' Ni16 161(7) . . ? O17' C17' Ni9 124(5) . . ? Ni16 C17' Ni9 72.3(19) . . ? O18 C18 Ni14 172.1(14) . . ? O19 C19 Ni15 145(8) . . ? O20 C20 Ni12 160(6) . . ? C21 Ni17 C19' 96.6(13) . . ? C21 Ni17 C20' 99.7(12) . . ? C19' Ni17 C20' 158.4(15) . . ? C21 Ni17 Ni15 145.2(9) . . ? C19' Ni17 Ni15 49.0(10) . . ? C20' Ni17 Ni15 112.6(8) . . ? C21 Ni17 Ni12 147.2(9) . . ? C19' Ni17 Ni12 116.0(10) . . ? C20' Ni17 Ni12 47.8(7) . . ? Ni15 Ni17 Ni12 67.00(10) . . ? C21 Ni17 Ni14 131.1(9) . . ? C19' Ni17 Ni14 89.8(10) . . ? C20' Ni17 Ni14 90.1(9) . . ? Ni15 Ni17 Ni14 63.57(10) . . ? Ni12 Ni17 Ni14 57.35(9) . . ? O21 C21 Ni17 173(3) . . ? O19' C19' Ni15 156(4) . . ? O19' C19' Ni17 124(3) . . ? Ni15 C19' Ni17 79.7(9) . . ? O20' C20' Ni12 143(2) . . ? O20' C20' Ni17 135(2) . . ? Ni12 C20' Ni17 81.6(9) . . ? C23 C22 Ni2 136.8(9) . . ? C23 C22 Ni8 130.0(9) . . ? Ni2 C22 Ni8 79.1(4) . . ? C23 C22 Ni7 131.1(9) . . ? Ni2 C22 Ni7 80.4(5) . . ? Ni8 C22 Ni7 77.4(4) . . ? C23 C22 Ni6 70.8(7) . . ? Ni2 C22 Ni6 101.2(5) . . ? Ni8 C22 Ni6 148.2(7) . . ? Ni7 C22 Ni6 71.3(4) . . ? C23 C22 Ni13 69.5(7) . . ? Ni2 C22 Ni13 153.6(6) . . ? Ni8 C22 Ni13 82.9(4) . . ? Ni7 C22 Ni13 76.9(4) . . ? Ni6 C22 Ni13 84.2(4) . . ? C23 C22 Ni1 68.0(7) . . ? Ni2 C22 Ni1 68.8(4) . . ? Ni8 C22 Ni1 126.6(6) . . ? Ni7 C22 Ni1 133.5(6) . . ? Ni6 C22 Ni1 81.3(4) . . ? Ni13 C22 Ni1 137.5(6) . . ? C22 C23 Ni14 143.8(9) . . ? C22 C23 Ni13 71.6(7) . . ? Ni14 C23 Ni13 72.2(4) . . ? C22 C23 Ni6 70.1(7) . . ? Ni14 C23 Ni6 107.2(5) . . ? Ni13 C23 Ni6 84.7(4) . . ? C22 C23 Ni12 121.3(9) . . ? Ni14 C23 Ni12 80.3(5) . . ? Ni13 C23 Ni12 125.6(6) . . ? Ni6 C23 Ni12 149.1(6) . . ? C22 C23 Ni1 74.0(7) . . ? Ni14 C23 Ni1 142.3(6) . . ? Ni13 C23 Ni1 145.5(6) . . ? Ni6 C23 Ni1 82.9(4) . . ? Ni12 C23 Ni1 74.4(4) . . ? C22 C23 Ni5 129.1(9) . . ? Ni14 C23 Ni5 78.9(4) . . ? Ni13 C23 Ni5 134.1(6) . . ? Ni6 C23 Ni5 70.6(4) . . ? Ni12 C23 Ni5 82.0(4) . . ? Ni1 C23 Ni5 70.2(4) . . ? C25 C24 Ni15 143.6(9) . . ? C25 C24 Ni16 73.0(7) . . ? Ni15 C24 Ni16 72.3(4) . . ? C25 C24 Ni11 132.0(9) . . ? Ni15 C24 Ni11 81.0(5) . . ? Ni16 C24 Ni11 132.6(6) . . ? C25 C24 Ni10 70.9(7) . . ? Ni15 C24 Ni10 115.5(6) . . ? Ni16 C24 Ni10 84.1(5) . . ? Ni11 C24 Ni10 72.8(4) . . ? C25 C24 Ni4 73.1(7) . . ? Ni15 C24 Ni4 141.8(7) . . ? Ni16 C24 Ni4 145.8(7) . . ? Ni11 C24 Ni4 71.0(4) . . ? Ni10 C24 Ni4 80.9(4) . . ? C25 C24 Ni12 118.3(8) . . ? Ni15 C24 Ni12 78.0(4) . . ? Ni16 C24 Ni12 130.3(6) . . ? Ni11 C24 Ni12 78.5(4) . . ? Ni10 C24 Ni12 145.3(6) . . ? Ni4 C24 Ni12 71.5(4) . . ? C24 C25 Ni8 128.7(9) . . ? C24 C25 Ni3 137.8(9) . . ? Ni8 C25 Ni3 81.0(5) . . ? C24 C25 Ni9 129.1(9) . . ? Ni8 C25 Ni9 79.3(5) . . ? Ni3 C25 Ni9 79.9(5) . . ? C24 C25 Ni10 70.0(7) . . ? Ni8 C25 Ni10 149.4(7) . . ? Ni3 C25 Ni10 99.7(5) . . ? Ni9 C25 Ni10 70.8(4) . . ? C24 C25 Ni16 68.0(7) . . ? Ni8 C25 Ni16 84.1(4) . . ? Ni3 C25 Ni16 153.4(7) . . ? Ni9 C25 Ni16 75.8(4) . . ? Ni10 C25 Ni16 82.3(4) . . ? C24 C25 Ni4 69.1(7) . . ? Ni8 C25 Ni4 127.6(6) . . ? Ni3 C25 Ni4 68.7(4) . . ? Ni9 C25 Ni4 131.9(6) . . ? Ni10 C25 Ni4 79.5(4) . . ? Ni16 C25 Ni4 136.9(6) . . ? O26 C26 Ni2 167(4) . . ? O27 C27 Ni3 172(2) . . ? O28 C28 Ni8 178(2) . . ? C29 Ni18 C27' 100(2) . . ? C29 Ni18 C26' 104(3) . . ? C27' Ni18 C26' 116(3) . . ? C29 Ni18 C28' 89(2) . . ? C27' Ni18 C28' 110.0(18) . . ? C26' Ni18 C28' 128(3) . . ? C29 Ni18 Ni8 132(2) . . ? C27' Ni18 Ni8 99.6(11) . . ? C26' Ni18 Ni8 105.4(18) . . ? C28' Ni18 Ni8 42.8(10) . . ? C29 Ni18 Ni2 147(2) . . ? C27' Ni18 Ni2 104.1(14) . . ? C26' Ni18 Ni2 44.0(17) . . ? C28' Ni18 Ni2 103.5(12) . . ? Ni8 Ni18 Ni2 65.74(17) . . ? C29 Ni18 Ni3 139(2) . . ? C27' Ni18 Ni3 41.0(12) . . ? C26' Ni18 Ni3 105(2) . . ? C28' Ni18 Ni3 94.8(10) . . ? Ni8 Ni18 Ni3 64.43(17) . . ? Ni2 Ni18 Ni3 70.96(19) . . ? O26' C26' Ni2 163(8) . . ? O26' C26' Ni18 117(7) . . ? Ni2 C26' Ni18 77(3) . . ? O27' C27' Ni3 152(5) . . ? O27' C27' Ni18 122(4) . . ? Ni3 C27' Ni18 77.0(17) . . ? O28' C28' Ni8 155(4) . . ? O28' C28' Ni18 128(4) . . ? Ni8 C28' Ni18 69.4(13) . . ? O29 C29 Ni18 174(5) . . ? C38' Ni21 C32 92.9(17) 3 . ? C38' Ni21 C38 46.4(17) 3 . ? C32 Ni21 C38 107.4(12) . . ? C38' Ni21 C41 128.1(16) 3 . ? C32 Ni21 C41 138.8(7) . . ? C38 Ni21 C41 100.3(11) . . ? C38' Ni21 C37 43.4(17) 3 3 ? C32 Ni21 C37 106.4(12) . 3 ? C38 Ni21 C37 82.3(15) . 3 ? C41 Ni21 C37 107.0(10) . 3 ? C38' Ni21 C42 165.6(16) 3 . ? C32 Ni21 C42 101.4(7) . . ? C38 Ni21 C42 128.4(11) . . ? C41 Ni21 C42 37.8(5) . . ? C37 Ni21 C42 128.7(10) 3 . ? C38' Ni21 Ni22 142.6(16) 3 . ? C32 Ni21 Ni22 50.1(6) . . ? C38 Ni21 Ni22 139.3(11) . . ? C41 Ni21 Ni22 89.3(4) . . ? C37 Ni21 Ni22 132.6(11) 3 . ? C42 Ni21 Ni22 51.5(4) . . ? C38' Ni21 Ni28 85.8(16) 3 . ? C32 Ni21 Ni28 145.7(6) . . ? C38 Ni21 Ni28 49.6(10) . . ? C41 Ni21 Ni28 50.7(4) . . ? C37 Ni21 Ni28 96.0(11) 3 . ? C42 Ni21 Ni28 83.2(4) . . ? Ni22 Ni21 Ni28 126.68(11) . . ? C38' Ni21 Ni24 85.2(16) 3 3 ? C32 Ni21 Ni24 152.5(6) . 3 ? C38 Ni21 Ni24 91.0(11) . 3 ? C41 Ni21 Ni24 52.0(4) . 3 ? C37 Ni21 Ni24 55.0(10) 3 3 ? C42 Ni21 Ni24 81.4(4) . 3 ? Ni22 Ni21 Ni24 124.37(11) . 3 ? Ni28 Ni21 Ni24 61.59(8) . 3 ? C38' Ni21 Ni27 129.7(16) 3 . ? C32 Ni21 Ni27 105.2(6) . . ? C38 Ni21 Ni27 83.3(10) . . ? C41 Ni21 Ni27 48.3(4) . . ? C37 Ni21 Ni27 147.9(11) 3 . ? C42 Ni21 Ni27 47.8(3) . . ? Ni22 Ni21 Ni27 74.04(9) . . ? Ni28 Ni21 Ni27 53.40(7) . . ? Ni24 Ni21 Ni27 96.88(8) 3 . ? C44' Ni22 C44 13(4) . . ? C44' Ni22 C32 101(3) . . ? C44 Ni22 C32 99(2) . . ? C44' Ni22 C42 147(3) . . ? C44 Ni22 C42 152(2) . . ? C32 Ni22 C42 109.4(8) . . ? C44' Ni22 Ni21 151(3) . . ? C44 Ni22 Ni21 150(2) . . ? C32 Ni22 Ni21 51.5(6) . . ? C42 Ni22 Ni21 58.1(4) . . ? C44' Ni22 Ni25 94(3) . . ? C44 Ni22 Ni25 103(2) . . ? C32 Ni22 Ni25 141.6(6) . . ? C42 Ni22 Ni25 53.0(4) . . ? Ni21 Ni22 Ni25 103.75(10) . . ? C44' Ni22 Ni29 66(3) . . ? C44 Ni22 Ni29 57(2) . . ? C32 Ni22 Ni29 126.2(6) . . ? C42 Ni22 Ni29 104.7(4) . . ? Ni21 Ni22 Ni29 134.34(19) . . ? Ni25 Ni22 Ni29 92.16(19) . . ? C44' Ni22 Ni24 112(3) . . ? C44 Ni22 Ni24 108(2) . . ? C32 Ni22 Ni24 138.3(6) . . ? C42 Ni22 Ni24 50.7(4) . . ? Ni21 Ni22 Ni24 96.48(10) . . ? Ni25 Ni22 Ni24 62.08(8) . . ? Ni29 Ni22 Ni24 54.01(17) . . ? C44' Ni22 Ni23 106(3) . . ? C44 Ni22 Ni23 92.9(19) . . ? C32 Ni22 Ni23 91.2(6) . . ? C42 Ni22 Ni23 88.2(4) . . ? Ni21 Ni22 Ni23 86.01(10) . . ? Ni25 Ni22 Ni23 118.58(10) . . ? Ni29 Ni22 Ni23 49.40(17) . . ? Ni24 Ni22 Ni23 56.57(7) . . ? C43' Ni23 C43 13.7(19) . . ? C43' Ni23 C35 90.3(15) . 3 ? C43 Ni23 C35 103.7(11) . 3 ? C43' Ni23 C41 158.0(15) . 3 ? C43 Ni23 C41 144.9(11) . 3 ? C35 Ni23 C41 108.2(7) 3 3 ? C43' Ni23 Ni29 59.3(15) . . ? C43 Ni23 Ni29 49.3(12) . . ? C35 Ni23 Ni29 139.5(6) 3 . ? C41 Ni23 Ni29 108.3(4) 3 . ? C43' Ni23 Ni26 140.4(14) . 3 ? C43 Ni23 Ni26 153.1(10) . 3 ? C35 Ni23 Ni26 50.4(5) 3 3 ? C41 Ni23 Ni26 58.1(4) 3 3 ? Ni29 Ni23 Ni26 154.5(2) . 3 ? C43' Ni23 Ni24 116.5(15) . . ? C43 Ni23 Ni24 105.0(11) . . ? C35 Ni23 Ni24 145.3(5) 3 . ? C41 Ni23 Ni24 52.7(4) 3 . ? Ni29 Ni23 Ni24 57.44(19) . . ? Ni26 Ni23 Ni24 101.72(9) 3 . ? C43' Ni23 Ni28 108.6(16) . 3 ? C43 Ni23 Ni28 96.7(11) . 3 ? C35 Ni23 Ni28 134.0(6) 3 3 ? C41 Ni23 Ni28 49.9(4) 3 3 ? Ni29 Ni23 Ni28 84.0(2) . 3 ? Ni26 Ni23 Ni28 98.61(9) 3 3 ? Ni24 Ni23 Ni28 60.49(7) . 3 ? C43' Ni23 Ni22 94.4(18) . . ? C43 Ni23 Ni22 94.3(14) . . ? C35 Ni23 Ni22 101.8(5) 3 . ? C41 Ni23 Ni22 93.3(4) 3 . ? Ni29 Ni23 Ni22 59.3(2) . . ? Ni26 Ni23 Ni22 98.05(10) 3 . ? Ni24 Ni23 Ni22 57.17(7) . . ? Ni28 Ni23 Ni22 117.45(9) 3 . ? C45' Ni24 C45 8(3) . . ? C45' Ni24 C42 136(4) . . ? C45 Ni24 C42 134(3) . . ? C45' Ni24 C41 135(4) . 3 ? C45 Ni24 C41 134(3) . 3 ? C42 Ni24 C41 88.7(5) . 3 ? C45' Ni24 C37 79(2) . . ? C45 Ni24 C37 87.2(18) . . ? C42 Ni24 C37 100.7(10) . . ? C41 Ni24 C37 103.4(11) 3 . ? C45' Ni24 Ni29 61(2) . . ? C45 Ni24 Ni29 53.6(16) . . ? C42 Ni24 Ni29 110.2(4) . . ? C41 Ni24 Ni29 101.5(4) 3 . ? C37 Ni24 Ni29 140.4(10) . . ? C45' Ni24 Ni21 114(3) . 3 ? C45 Ni24 Ni21 120(2) . 3 ? C42 Ni24 Ni21 99.0(4) . 3 ? C41 Ni24 Ni21 52.0(3) 3 3 ? C37 Ni24 Ni21 51.4(10) . 3 ? Ni29 Ni24 Ni21 140.5(2) . 3 ? C45' Ni24 Ni23 109(2) . . ? C45 Ni24 Ni23 103.0(18) . . ? C42 Ni24 Ni23 93.7(3) . . ? C41 Ni24 Ni23 48.5(3) 3 . ? C37 Ni24 Ni23 148.3(11) . . ? Ni29 Ni24 Ni23 54.57(19) . . ? Ni21 Ni24 Ni23 98.69(9) 3 . ? C45' Ni24 Ni22 107(3) . . ? C45 Ni24 Ni22 101(2) . . ? C42 Ni24 Ni22 47.9(4) . . ? C41 Ni24 Ni22 97.4(4) 3 . ? C37 Ni24 Ni22 141.9(11) . . ? Ni29 Ni24 Ni22 62.3(2) . . ? Ni21 Ni24 Ni22 138.94(11) 3 . ? Ni23 Ni24 Ni22 66.26(8) . . ? C45' Ni24 Ni28 86(4) . 3 ? C45 Ni24 Ni28 87(3) . 3 ? C42 Ni24 Ni28 137.9(4) . 3 ? C41 Ni24 Ni28 49.2(4) 3 3 ? C37 Ni24 Ni28 91.1(11) . 3 ? Ni29 Ni24 Ni28 82.3(2) . 3 ? Ni21 Ni24 Ni28 58.21(8) 3 3 ? Ni23 Ni24 Ni28 60.19(8) . 3 ? Ni22 Ni24 Ni28 126.19(10) . 3 ? C45' Ni24 Ni26 112(3) . . ? C45 Ni24 Ni26 118(2) . . ? C42 Ni24 Ni26 51.0(3) . . ? C41 Ni24 Ni26 101.9(4) 3 . ? C37 Ni24 Ni26 49.8(10) . . ? Ni29 Ni24 Ni26 149.4(2) . . ? Ni21 Ni24 Ni26 70.19(8) 3 . ? Ni23 Ni24 Ni26 137.88(10) . . ? Ni22 Ni24 Ni26 95.08(9) . . ? Ni28 Ni24 Ni26 128.21(10) 3 . ? C45' Ni24 Ni25 86(4) . . ? C45 Ni24 Ni25 85(3) . . ? C42 Ni24 Ni25 50.6(4) . . ? C41 Ni24 Ni25 139.3(4) 3 . ? C37 Ni24 Ni25 85.9(11) . . ? Ni29 Ni24 Ni25 94.9(2) . . ? Ni21 Ni24 Ni25 124.50(10) 3 . ? Ni23 Ni24 Ni25 124.44(10) . . ? Ni22 Ni24 Ni25 58.26(8) . . ? Ni28 Ni24 Ni25 171.43(11) 3 . ? Ni26 Ni24 Ni25 54.53(8) . . ? C33 Ni25 C39 101.0(17) . . ? C33 Ni25 C34 99.2(9) . . ? C39 Ni25 C34 86.0(16) . . ? C33 Ni25 C42 148.4(8) . . ? C39 Ni25 C42 105.0(16) . . ? C34 Ni25 C42 100.2(7) . . ? C33 Ni25 C39' 102.3(15) . . ? C39 Ni25 C39' 16(2) . . ? C34 Ni25 C39' 101.6(16) . . ? C42 Ni25 C39' 97.9(13) . . ? C33 Ni25 Ni27 142.6(7) . . ? C39 Ni25 Ni27 91.6(16) . . ? C34 Ni25 Ni27 46.2(6) . . ? C42 Ni25 Ni27 54.6(4) . . ? C39' Ni25 Ni27 99.3(15) . . ? C33 Ni25 Ni26 143.8(7) . . ? C39 Ni25 Ni26 51.3(16) . . ? C34 Ni25 Ni26 101.0(6) . . ? C42 Ni25 Ni26 54.3(4) . . ? C39' Ni25 Ni26 44.2(13) . . ? Ni27 Ni25 Ni26 69.31(9) . . ? C33 Ni25 Ni22 102.8(7) . . ? C39 Ni25 Ni22 152.6(16) . . ? C34 Ni25 Ni22 103.1(6) . . ? C42 Ni25 Ni22 48.3(3) . . ? C39' Ni25 Ni22 141.1(13) . . ? Ni27 Ni25 Ni22 77.49(9) . . ? Ni26 Ni25 Ni22 101.41(10) . . ? C33 Ni25 Ni24 109.2(7) . . ? C39 Ni25 Ni24 99.7(15) . . ? C34 Ni25 Ni24 149.1(6) . . ? C42 Ni25 Ni24 48.9(4) . . ? C39' Ni25 Ni24 84.1(13) . . ? Ni27 Ni25 Ni24 103.04(10) . . ? Ni26 Ni25 Ni24 62.14(8) . . ? Ni22 Ni25 Ni24 59.67(8) . . ? C39' Ni26 C35 103(2) . . ? C39' Ni26 C39 17(2) . . ? C35 Ni26 C39 103.3(16) . . ? C39' Ni26 C37 74(2) . . ? C35 Ni26 C37 100.6(12) . . ? C39 Ni26 C37 90.5(18) . . ? C39' Ni26 C42 111.7(19) . . ? C35 Ni26 C42 141.8(7) . . ? C39 Ni26 C42 105.5(15) . . ? C37 Ni26 C42 103.6(10) . . ? C39' Ni26 C41 143.4(18) . . ? C35 Ni26 C41 103.9(6) . . ? C39 Ni26 C41 129.8(14) . . ? C37 Ni26 C41 124.3(10) . . ? C42 Ni26 C41 37.9(5) . . ? C39' Ni26 Ni23 150.0(19) . 3 ? C35 Ni26 Ni23 51.9(5) . 3 ? C39 Ni26 Ni23 139.3(16) . 3 ? C37 Ni26 Ni23 122.6(11) . 3 ? C42 Ni26 Ni23 90.1(4) . 3 ? C41 Ni26 Ni23 52.3(4) . 3 ? C39' Ni26 Ni25 57.9(18) . . ? C35 Ni26 Ni25 150.6(5) . . ? C39 Ni26 Ni25 51.5(14) . . ? C37 Ni26 Ni25 95.2(11) . . ? C42 Ni26 Ni25 54.5(4) . . ? C41 Ni26 Ni25 87.0(4) . . ? Ni23 Ni26 Ni25 134.68(11) 3 . ? C39' Ni26 Ni24 92.7(19) . . ? C35 Ni26 Ni24 145.1(5) . . ? C39 Ni26 Ni24 100.8(16) . . ? C37 Ni26 Ni24 54.2(10) . . ? C42 Ni26 Ni24 49.5(4) . . ? C41 Ni26 Ni24 78.6(4) . . ? Ni23 Ni26 Ni24 117.25(9) 3 . ? Ni25 Ni26 Ni24 63.34(8) . . ? C39' Ni26 Ni27 97.6(17) . . ? C35 Ni26 Ni27 113.2(6) . . ? C39 Ni26 Ni27 81.8(14) . . ? C37 Ni26 Ni27 146.2(11) . . ? C42 Ni26 Ni27 48.5(4) . . ? C41 Ni26 Ni27 48.8(4) . . ? Ni23 Ni26 Ni27 81.27(9) 3 . ? Ni25 Ni26 Ni27 54.59(8) . . ? Ni24 Ni26 Ni27 94.83(8) . . ? C36 Ni27 C34 105.4(9) . . ? C36 Ni27 C42 143.3(8) . . ? C34 Ni27 C42 110.7(8) . . ? C36 Ni27 C41 108.9(8) . . ? C34 Ni27 C41 143.8(8) . . ? C42 Ni27 C41 38.4(5) . . ? C36 Ni27 Ni25 161.2(7) . . ? C34 Ni27 Ni25 56.0(7) . . ? C42 Ni27 Ni25 55.4(4) . . ? C41 Ni27 Ni25 89.0(4) . . ? C36 Ni27 Ni28 56.3(7) . . ? C34 Ni27 Ni28 161.4(7) . . ? C42 Ni27 Ni28 87.9(4) . . ? C41 Ni27 Ni28 53.1(4) . . ? Ni25 Ni27 Ni28 141.99(11) . . ? C36 Ni27 Ni26 132.2(7) . . ? C34 Ni27 Ni26 97.5(7) . . ? C42 Ni27 Ni26 49.0(3) . . ? C41 Ni27 Ni26 49.9(4) . . ? Ni25 Ni27 Ni26 56.10(8) . . ? Ni28 Ni27 Ni26 93.84(9) . . ? C36 Ni27 Ni21 99.1(6) . . ? C34 Ni27 Ni21 135.5(7) . . ? C42 Ni27 Ni21 49.4(4) . . ? C41 Ni27 Ni21 48.7(3) . . ? Ni25 Ni27 Ni21 97.04(10) . . ? Ni28 Ni27 Ni21 58.13(8) . . ? Ni26 Ni27 Ni21 92.50(8) . . ? C31 Ni28 C38 91.9(12) . . ? C31 Ni28 C41 155.9(7) . . ? C38 Ni28 C41 105.0(11) . . ? C31 Ni28 C36 96.4(8) . . ? C38 Ni28 C36 89.9(13) . . ? C41 Ni28 C36 100.6(7) . . ? C31 Ni28 Ni27 141.0(6) . . ? C38 Ni28 Ni27 95.2(11) . . ? C41 Ni28 Ni27 55.6(4) . . ? C36 Ni28 Ni27 45.4(6) . . ? C31 Ni28 Ni21 139.6(6) . . ? C38 Ni28 Ni21 51.5(10) . . ? C41 Ni28 Ni21 53.5(3) . . ? C36 Ni28 Ni21 99.5(5) . . ? Ni27 Ni28 Ni21 68.47(8) . . ? C31 Ni28 Ni23 109.4(6) . 3 ? C38 Ni28 Ni23 148.2(11) . 3 ? C41 Ni28 Ni23 48.5(4) . 3 ? C36 Ni28 Ni23 110.1(6) . 3 ? Ni27 Ni28 Ni23 83.06(9) . 3 ? Ni21 Ni28 Ni23 99.47(9) . 3 ? C31 Ni28 Ni24 112.0(6) . 3 ? C38 Ni28 Ni24 91.2(11) . 3 ? C41 Ni28 Ni24 51.8(4) . 3 ? C36 Ni28 Ni24 151.6(6) . 3 ? Ni27 Ni28 Ni24 106.20(10) . 3 ? Ni21 Ni28 Ni24 60.21(8) . 3 ? Ni23 Ni28 Ni24 59.32(8) 3 3 ? O31 C31 Ni28 176.7(17) . . ? O32 C32 Ni22 140.7(17) . . ? O32 C32 Ni21 140.9(17) . . ? Ni22 C32 Ni21 78.4(8) . . ? O33 C33 Ni25 172.8(18) . . ? O34 C34 Ni27 150.7(18) . . ? O34 C34 Ni25 130.3(16) . . ? Ni27 C34 Ni25 77.8(8) . . ? O35 C35 Ni26 143.5(16) . . ? O35 C35 Ni23 138.8(16) . 3 ? Ni26 C35 Ni23 77.7(6) . 3 ? O36 C36 Ni27 152.5(18) . . ? O36 C36 Ni28 128.7(16) . . ? Ni27 C36 Ni28 78.2(8) . . ? O37 C37 Ni26 129(3) . . ? O37 C37 Ni21 127(3) . 3 ? Ni26 C37 Ni21 91.8(12) . 3 ? O37 C37 Ni24 140(3) . . ? Ni26 C37 Ni24 76.0(10) . . ? Ni21 C37 Ni24 73.6(10) 3 . ? O38 C38 Ni28 137(3) . . ? O38 C38 Ni21 144(3) . . ? Ni28 C38 Ni21 78.8(10) . . ? O39 C39 Ni25 147(5) . . ? O39 C39 Ni26 136(5) . . ? Ni25 C39 Ni26 77.2(13) . . ? O38' C38' Ni21 175(4) . 3 ? O39' C39' Ni26 154(5) . . ? O39' C39' Ni25 127(5) . . ? Ni26 C39' Ni25 78.0(16) . . ? C42 C41 Ni23 138.6(10) . 3 ? C42 C41 Ni28 132.0(10) . . ? Ni23 C41 Ni28 81.6(5) 3 . ? C42 C41 Ni27 70.2(8) . . ? Ni23 C41 Ni27 109.8(6) 3 . ? Ni28 C41 Ni27 71.3(4) . . ? C42 C41 Ni21 72.0(8) . . ? Ni23 C41 Ni21 148.9(8) 3 . ? Ni28 C41 Ni21 75.8(5) . . ? Ni27 C41 Ni21 83.0(5) . . ? C42 C41 Ni24 124.7(9) . 3 ? Ni23 C41 Ni24 78.8(5) 3 3 ? Ni28 C41 Ni24 79.0(5) . 3 ? Ni27 C41 Ni24 147.0(7) . 3 ? Ni21 C41 Ni24 76.0(4) . 3 ? C42 C41 Ni26 69.6(8) . . ? Ni23 C41 Ni26 69.5(4) 3 . ? Ni28 C41 Ni26 130.3(6) . . ? Ni27 C41 Ni26 81.4(5) . . ? Ni21 C41 Ni26 141.5(7) . . ? Ni24 C41 Ni26 130.1(7) 3 . ? C41 C42 Ni22 140.5(10) . . ? C41 C42 Ni24 125.4(10) . . ? Ni22 C42 Ni24 81.4(5) . . ? C41 C42 Ni27 71.3(8) . . ? Ni22 C42 Ni27 100.9(6) . . ? Ni24 C42 Ni27 149.1(7) . . ? C41 C42 Ni26 72.4(8) . . ? Ni22 C42 Ni26 146.6(8) . . ? Ni24 C42 Ni26 79.6(5) . . ? Ni27 C42 Ni26 82.5(4) . . ? C41 C42 Ni25 129.3(9) . . ? Ni22 C42 Ni25 78.7(5) . . ? Ni24 C42 Ni25 80.5(5) . . ? Ni27 C42 Ni25 70.0(4) . . ? Ni26 C42 Ni25 71.2(4) . . ? C41 C42 Ni21 70.2(8) . . ? Ni22 C42 Ni21 70.4(4) . . ? Ni24 C42 Ni21 125.8(6) . . ? Ni27 C42 Ni21 82.8(5) . . ? Ni26 C42 Ni21 142.5(7) . . ? Ni25 C42 Ni21 133.8(7) . . ? O43 C43 Ni23 167(4) . . ? O44 C44 Ni22 159(5) . . ? O45 C45 Ni24 173(5) . . ? C46 Ni29 C43' 99(2) . . ? C46 Ni29 C45' 99(2) . . ? C43' Ni29 C45' 143(3) . . ? C46 Ni29 Ni23 142(2) . . ? C43' Ni29 Ni23 44.4(10) . . ? C45' Ni29 Ni23 106.8(19) . . ? C46 Ni29 Ni24 144(2) . . ? C43' Ni29 Ni24 112.2(10) . . ? C45' Ni29 Ni24 44.8(13) . . ? Ni23 Ni29 Ni24 68.0(2) . . ? C46 Ni29 Ni22 133(2) . . ? C43' Ni29 Ni22 94.3(12) . . ? C45' Ni29 Ni22 96(2) . . ? Ni23 Ni29 Ni22 71.3(2) . . ? Ni24 Ni29 Ni22 63.66(18) . . ? O43' C43' Ni23 160(4) . . ? O43' C43' Ni29 123(3) . . ? Ni23 C43' Ni29 76.3(13) . . ? O44' C44' Ni22 159(7) . . ? O45' C45' Ni24 155(5) . . ? O45' C45' Ni29 131(5) . . ? Ni24 C45' Ni29 74.0(15) . . ? O46 C46 Ni29 176(5) . . ? C107 N1 C103 106.7(10) . . ? C107 N1 C101 111.1(11) . . ? C103 N1 C101 110.7(11) . . ? C107 N1 C105 112.4(11) . . ? C103 N1 C105 109.4(11) . . ? C101 N1 C105 106.7(10) . . ? N1 C101 C102 114.2(13) . . ? N1 C101 H10A 108.7 . . ? C102 C101 H10A 108.7 . . ? N1 C101 H10B 108.7 . . ? C102 C101 H10B 108.7 . . ? H10A C101 H10B 107.6 . . ? C101 C102 H10C 109.5 . . ? C101 C102 H10D 109.5 . . ? H10C C102 H10D 109.5 . . ? C101 C102 H10E 109.5 . . ? H10C C102 H10E 109.5 . . ? H10D C102 H10E 109.5 . . ? N1 C103 C104 112.5(12) . . ? N1 C103 H10F 109.1 . . ? C104 C103 H10F 109.1 . . ? N1 C103 H10G 109.1 . . ? C104 C103 H10G 109.1 . . ? H10F C103 H10G 107.8 . . ? C103 C104 H10H 109.5 . . ? C103 C104 H10I 109.5 . . ? H10H C104 H10I 109.5 . . ? C103 C104 H10J 109.5 . . ? H10H C104 H10J 109.5 . . ? H10I C104 H10J 109.5 . . ? N1 C105 C106 115.3(13) . . ? N1 C105 H10K 108.5 . . ? C106 C105 H10K 108.5 . . ? N1 C105 H10L 108.5 . . ? C106 C105 H10L 108.5 . . ? H10K C105 H10L 107.5 . . ? C105 C106 H10M 109.5 . . ? C105 C106 H10N 109.5 . . ? H10M C106 H10N 109.5 . . ? C105 C106 H10O 109.5 . . ? H10M C106 H10O 109.5 . . ? H10N C106 H10O 109.5 . . ? N1 C107 C108 116.5(12) . . ? N1 C107 H10P 108.2 . . ? C108 C107 H10P 108.2 . . ? N1 C107 H10Q 108.2 . . ? C108 C107 H10Q 108.2 . . ? H10P C107 H10Q 107.3 . . ? C107 C108 H10R 109.5 . . ? C107 C108 H10S 109.5 . . ? H10R C108 H10S 109.5 . . ? C107 C108 H10T 109.5 . . ? H10R C108 H10T 109.5 . . ? H10S C108 H10T 109.5 . . ? C203 N2 C207 109.3(11) . . ? C203 N2 C201 110.6(12) . . ? C207 N2 C201 112.0(13) . . ? C203 N2 C205 113.6(13) . . ? C207 N2 C205 109.5(13) . . ? C201 N2 C205 101.9(13) . . ? N2 C201 C202 114.0(13) . . ? N2 C201 H20A 108.8 . . ? C202 C201 H20A 108.8 . . ? N2 C201 H20B 108.8 . . ? C202 C201 H20B 108.8 . . ? H20A C201 H20B 107.6 . . ? C201 C202 H20C 109.5 . . ? C201 C202 H20D 109.5 . . ? H20C C202 H20D 109.5 . . ? C201 C202 H20E 109.5 . . ? H20C C202 H20E 109.5 . . ? H20D C202 H20E 109.5 . . ? N2 C203 C204 117.6(13) . . ? N2 C203 H20F 107.9 . . ? C204 C203 H20F 107.9 . . ? N2 C203 H20G 107.9 . . ? C204 C203 H20G 107.9 . . ? H20F C203 H20G 107.2 . . ? C203 C204 H20H 109.5 . . ? C203 C204 H20I 109.5 . . ? H20H C204 H20I 109.5 . . ? C203 C204 H20J 109.5 . . ? H20H C204 H20J 109.5 . . ? H20I C204 H20J 109.5 . . ? N2 C205 C206 112.7(13) . . ? N2 C205 H20K 109.1 . . ? C206 C205 H20K 109.1 . . ? N2 C205 H20L 109.1 . . ? C206 C205 H20L 109.1 . . ? H20K C205 H20L 107.8 . . ? C205 C206 H20M 109.5 . . ? C205 C206 H20N 109.5 . . ? H20M C206 H20N 109.5 . . ? C205 C206 H20O 109.5 . . ? H20M C206 H20O 109.5 . . ? H20N C206 H20O 109.5 . . ? N2 C207 C208 113.1(13) . . ? N2 C207 H20P 109.0 . . ? C208 C207 H20P 109.0 . . ? N2 C207 H20Q 109.0 . . ? C208 C207 H20Q 109.0 . . ? H20P C207 H20Q 107.8 . . ? C207 C208 H20R 109.5 . . ? C207 C208 H20S 109.5 . . ? H20R C208 H20S 109.5 . . ? C207 C208 H20T 109.5 . . ? H20R C208 H20T 109.5 . . ? H20S C208 H20T 109.5 . . ? C3A5 N3 C301 174.3(18) . . ? C3A5 N3 C307 73(2) . . ? C301 N3 C307 110.7(17) . . ? C3A5 N3 C303 70(2) . . ? C301 N3 C303 111.8(17) . . ? C307 N3 C303 109.0(16) . . ? C3A5 N3 C3A7 113.0(18) . . ? C301 N3 C3A7 63(2) . . ? C307 N3 C3A7 173(2) . . ? C303 N3 C3A7 77.2(19) . . ? C3A5 N3 C305 66.3(16) . . ? C301 N3 C305 108.2(15) . . ? C307 N3 C305 107.9(17) . . ? C303 N3 C305 109.3(17) . . ? C3A7 N3 C305 73(2) . . ? C3A5 N3 C3A3 109.1(17) . . ? C301 N3 C3A3 70(2) . . ? C307 N3 C3A3 66.1(18) . . ? C303 N3 C3A3 174.9(18) . . ? C3A7 N3 C3A3 107.6(16) . . ? C305 N3 C3A3 74(2) . . ? C3A5 N3 C3A1 111.0(15) . . ? C301 N3 C3A1 74.5(18) . . ? C307 N3 C3A1 71(2) . . ? C303 N3 C3A1 69.0(19) . . ? C3A7 N3 C3A1 108.7(17) . . ? C305 N3 C3A1 177.3(18) . . ? C3A3 N3 C3A1 107.2(17) . . ? N3 C301 C302 112.6(19) . . ? N3 C301 H30A 109.1 . . ? C302 C301 H30A 109.1 . . ? N3 C301 H30B 109.1 . . ? C302 C301 H30B 109.1 . . ? H30A C301 H30B 107.8 . . ? C301 C302 H30C 109.5 . . ? C301 C302 H30D 109.5 . . ? H30C C302 H30D 109.5 . . ? C301 C302 H30E 109.5 . . ? H30C C302 H30E 109.5 . . ? H30D C302 H30E 109.5 . . ? N3 C303 C304 117(2) . . ? N3 C303 H30F 108.1 . . ? C304 C303 H30F 108.1 . . ? N3 C303 H30G 108.1 . . ? C304 C303 H30G 108.1 . . ? H30F C303 H30G 107.3 . . ? C303 C304 H30H 109.5 . . ? C303 C304 H30I 109.5 . . ? H30H C304 H30I 109.5 . . ? C303 C304 H30J 109.5 . . ? H30H C304 H30J 109.5 . . ? H30I C304 H30J 109.5 . . ? N3 C305 C306 111.2(19) . . ? N3 C305 H30K 109.4 . . ? C306 C305 H30K 109.4 . . ? N3 C305 H30L 109.4 . . ? C306 C305 H30L 109.4 . . ? H30K C305 H30L 108.0 . . ? C305 C306 H30M 109.5 . . ? C305 C306 H30N 109.5 . . ? H30M C306 H30N 109.5 . . ? C305 C306 H30O 109.5 . . ? H30M C306 H30O 109.5 . . ? H30N C306 H30O 109.5 . . ? N3 C307 C308 112.4(19) . . ? N3 C307 H30P 109.1 . . ? C308 C307 H30P 109.1 . . ? N3 C307 H30Q 109.1 . . ? C308 C307 H30Q 109.1 . . ? H30P C307 H30Q 107.8 . . ? C307 C308 H30R 109.5 . . ? C307 C308 H30S 109.5 . . ? H30R C308 H30S 109.5 . . ? C307 C308 H30T 109.5 . . ? H30R C308 H30T 109.5 . . ? H30S C308 H30T 109.5 . . ? N3 C3A1 C3A2 112(2) . . ? N3 C3A1 H3A1 109.1 . . ? C3A2 C3A1 H3A1 109.1 . . ? N3 C3A1 H3A2 109.1 . . ? C3A2 C3A1 H3A2 109.1 . . ? H3A1 C3A1 H3A2 107.9 . . ? C3A1 C3A2 H3A3 109.5 . . ? C3A1 C3A2 H3A4 109.5 . . ? H3A3 C3A2 H3A4 109.5 . . ? C3A1 C3A2 H3A5 109.5 . . ? H3A3 C3A2 H3A5 109.5 . . ? H3A4 C3A2 H3A5 109.5 . . ? N3 C3A3 C3A4 116(2) . . ? N3 C3A3 H3A6 108.4 . . ? C3A4 C3A3 H3A6 108.4 . . ? N3 C3A3 H3A7 108.4 . . ? C3A4 C3A3 H3A7 108.4 . . ? H3A6 C3A3 H3A7 107.4 . . ? C3A3 C3A4 H3A8 109.5 . . ? C3A3 C3A4 H3A9 109.5 . . ? H3A8 C3A4 H3A9 109.5 . . ? C3A3 C3A4 H3AX 109.5 . . ? H3A8 C3A4 H3AX 109.5 . . ? H3A9 C3A4 H3AX 109.5 . . ? N3 C3A5 C3A6 115(2) . . ? N3 C3A5 H3AY 108.5 . . ? C3A6 C3A5 H3AY 108.5 . . ? N3 C3A5 H3AZ 108.5 . . ? C3A6 C3A5 H3AZ 108.5 . . ? H3AY C3A5 H3AZ 107.5 . . ? C3A5 C3A6 H3AA 109.5 . . ? C3A5 C3A6 H3AB 109.5 . . ? H3AA C3A6 H3AB 109.5 . . ? C3A5 C3A6 H3AC 109.5 . . ? H3AA C3A6 H3AC 109.5 . . ? H3AB C3A6 H3AC 109.5 . . ? N3 C3A7 C3A8 115(2) . . ? N3 C3A7 H3AD 108.6 . . ? C3A8 C3A7 H3AD 108.6 . . ? N3 C3A7 H3AE 108.6 . . ? C3A8 C3A7 H3AE 108.6 . . ? H3AD C3A7 H3AE 107.6 . . ? C3A7 C3A8 H3AF 109.5 . . ? C3A7 C3A8 H3AG 109.5 . . ? H3AF C3A8 H3AG 109.5 . . ? C3A7 C3A8 H3AH 109.5 . . ? H3AF C3A8 H3AH 109.5 . . ? H3AG C3A8 H3AH 109.5 . . ? C407 N4 C403 104.1(16) . . ? C407 N4 C405 112.8(17) . . ? C403 N4 C405 110.0(16) . . ? C407 N4 C401 111.0(15) . . ? C403 N4 C401 113.9(16) . . ? C405 N4 C401 105.3(9) . . ? N4 C401 C402 117.5(17) . . ? N4 C401 H40A 107.9 . . ? C402 C401 H40A 107.9 . . ? N4 C401 H40B 107.9 . . ? C402 C401 H40B 107.9 . . ? H40A C401 H40B 107.2 . . ? C401 C402 H40C 109.5 . . ? C401 C402 H40D 109.5 . . ? H40C C402 H40D 109.5 . . ? C401 C402 H40E 109.5 . . ? H40C C402 H40E 109.5 . . ? H40D C402 H40E 109.5 . . ? N4 C403 C404 115.1(19) . . ? N4 C403 H40F 108.5 . . ? C404 C403 H40F 108.5 . . ? N4 C403 H40G 108.5 . . ? C404 C403 H40G 108.5 . . ? H40F C403 H40G 107.5 . . ? C403 C404 H40H 109.5 . . ? C403 C404 H40I 109.5 . . ? H40H C404 H40I 109.5 . . ? C403 C404 H40J 109.5 . . ? H40H C404 H40J 109.5 . . ? H40I C404 H40J 109.5 . . ? N4 C405 C406 114.1(13) . . ? N4 C405 H40K 108.7 . . ? C406 C405 H40K 108.7 . . ? N4 C405 H40L 108.7 . . ? C406 C405 H40L 108.7 . . ? H40K C405 H40L 107.6 . . ? C405 C406 H40M 109.5 . . ? C405 C406 H40N 109.5 . . ? H40M C406 H40N 109.5 . . ? C405 C406 H40O 109.5 . . ? H40M C406 H40O 109.5 . . ? H40N C406 H40O 109.5 . . ? N4 C407 C408 114.4(16) . . ? N4 C407 H40P 108.7 . . ? C408 C407 H40P 108.7 . . ? N4 C407 H40Q 108.7 . . ? C408 C407 H40Q 108.7 . . ? H40P C407 H40Q 107.6 . . ? C407 C408 H40R 109.5 . . ? C407 C408 H40S 109.5 . . ? H40R C408 H40S 109.5 . . ? C407 C408 H40T 109.5 . . ? H40R C408 H40T 109.5 . . ? H40S C408 H40T 109.5 . . ? C503 N5 C505 109.2(15) . . ? C503 N5 C507 107.7(14) . . ? C505 N5 C507 113.2(14) . . ? C503 N5 C501 111.9(15) . . ? C505 N5 C501 107.3(14) . . ? C507 N5 C501 107.6(14) . . ? N5 C501 C502 114.3(17) . . ? N5 C501 H50A 108.7 . . ? C502 C501 H50A 108.7 . . ? N5 C501 H50B 108.7 . . ? C502 C501 H50B 108.7 . . ? H50A C501 H50B 107.6 . . ? C501 C502 H50C 109.5 . . ? C501 C502 H50D 109.5 . . ? H50C C502 H50D 109.5 . . ? C501 C502 H50E 109.5 . . ? H50C C502 H50E 109.5 . . ? H50D C502 H50E 109.5 . . ? N5 C503 C504 115.2(15) . . ? N5 C503 H50F 108.5 . . ? C504 C503 H50F 108.5 . . ? N5 C503 H50G 108.5 . . ? C504 C503 H50G 108.5 . . ? H50F C503 H50G 107.5 . . ? C503 C504 H50H 109.5 . . ? C503 C504 H50I 109.5 . . ? H50H C504 H50I 109.5 . . ? C503 C504 H50J 109.5 . . ? H50H C504 H50J 109.5 . . ? H50I C504 H50J 109.5 . . ? N5 C505 C506 113.8(16) . . ? N5 C505 H50K 108.8 . . ? C506 C505 H50K 108.8 . . ? N5 C505 H50L 108.8 . . ? C506 C505 H50L 108.8 . . ? H50K C505 H50L 107.7 . . ? C505 C506 H50M 109.5 . . ? C505 C506 H50N 109.5 . . ? H50M C506 H50N 109.5 . . ? C505 C506 H50O 109.5 . . ? H50M C506 H50O 109.5 . . ? H50N C506 H50O 109.5 . . ? N5 C507 C508 119.1(16) . . ? N5 C507 H50P 107.5 . . ? C508 C507 H50P 107.5 . . ? N5 C507 H50Q 107.5 . . ? C508 C507 H50Q 107.5 . . ? H50P C507 H50Q 107.0 . . ? C507 C508 H50R 109.5 . . ? C507 C508 H50S 109.5 . . ? H50R C508 H50S 109.5 . . ? C507 C508 H50T 109.5 . . ? H50R C508 H50T 109.5 . . ? H50S C508 H50T 109.5 . . ? C6A7 N6 C607 166(2) . . ? C6A7 N6 C605 54.3(19) . . ? C607 N6 C605 114.2(17) . . ? C6A7 N6 C601 77(2) . . ? C607 N6 C601 115.2(17) . . ? C605 N6 C601 105.7(14) . . ? C6A7 N6 C6A5 115.7(18) . . ? C607 N6 C6A5 53.6(19) . . ? C605 N6 C6A5 90.0(16) . . ? C601 N6 C6A5 164.0(16) . . ? C6A7 N6 C603 76.8(17) . . ? C607 N6 C603 103.4(14) . . ? C605 N6 C603 109.5(16) . . ? C601 N6 C603 108.6(16) . . ? C6A5 N6 C603 67.5(19) . . ? C6A7 N6 C6A1 115.0(17) . . ? C607 N6 C6A1 77.6(19) . . ? C605 N6 C6A1 165.5(17) . . ? C601 N6 C6A1 60.3(16) . . ? C6A5 N6 C6A1 104.2(15) . . ? C603 N6 C6A1 74.1(19) . . ? C6A7 N6 C6A3 106.6(16) . . ? C607 N6 C6A3 72.7(17) . . ? C605 N6 C6A3 71.0(18) . . ? C601 N6 C6A3 75(2) . . ? C6A5 N6 C6A3 108.3(17) . . ? C603 N6 C6A3 175.6(18) . . ? C6A1 N6 C6A3 106.5(16) . . ? N6 C601 C602 112.9(18) . . ? N6 C601 H60A 109.0 . . ? C602 C601 H60A 109.0 . . ? N6 C601 H60B 109.0 . . ? C602 C601 H60B 109.0 . . ? H60A C601 H60B 107.8 . . ? C601 C602 H60C 109.5 . . ? C601 C602 H60D 109.5 . . ? H60C C602 H60D 109.5 . . ? C601 C602 H60E 109.5 . . ? H60C C602 H60E 109.5 . . ? H60D C602 H60E 109.5 . . ? N6 C603 C604 114.4(19) . . ? N6 C603 H60F 108.7 . . ? C604 C603 H60F 108.7 . . ? N6 C603 H60G 108.7 . . ? C604 C603 H60G 108.7 . . ? H60F C603 H60G 107.6 . . ? C603 C604 H60H 109.5 . . ? C603 C604 H60I 109.5 . . ? H60H C604 H60I 109.5 . . ? C603 C604 H60J 109.5 . . ? H60H C604 H60J 109.5 . . ? H60I C604 H60J 109.5 . . ? N6 C605 C606 120(2) . . ? N6 C605 H60K 107.4 . . ? C606 C605 H60K 107.4 . . ? N6 C605 H60L 107.4 . . ? C606 C605 H60L 107.4 . . ? H60K C605 H60L 106.9 . . ? C605 C606 H60M 109.5 . . ? C605 C606 H60N 109.5 . . ? H60M C606 H60N 109.5 . . ? C605 C606 H60O 109.5 . . ? H60M C606 H60O 109.5 . . ? H60N C606 H60O 109.5 . . ? N6 C607 C608 113.1(18) . . ? N6 C607 H60P 109.0 . . ? C608 C607 H60P 109.0 . . ? N6 C607 H60Q 109.0 . . ? C608 C607 H60Q 109.0 . . ? H60P C607 H60Q 107.8 . . ? C607 C608 H60R 109.5 . . ? C607 C608 H60S 109.5 . . ? H60R C608 H60S 109.5 . . ? C607 C608 H60T 109.5 . . ? H60R C608 H60T 109.5 . . ? H60S C608 H60T 109.5 . . ? N6 C6A1 C6A2 113.5(19) . . ? N6 C6A1 H6A1 108.9 . . ? C6A2 C6A1 H6A1 108.9 . . ? N6 C6A1 H6A2 108.9 . . ? C6A2 C6A1 H6A2 108.9 . . ? H6A1 C6A1 H6A2 107.7 . . ? C6A1 C6A2 H6A3 109.5 . . ? C6A1 C6A2 H6A4 109.5 . . ? H6A3 C6A2 H6A4 109.5 . . ? C6A1 C6A2 H6A5 109.5 . . ? H6A3 C6A2 H6A5 109.5 . . ? H6A4 C6A2 H6A5 109.5 . . ? N6 C6A3 C6A4 116(2) . . ? N6 C6A3 H6A6 108.4 . . ? C6A4 C6A3 H6A6 108.4 . . ? N6 C6A3 H6A7 108.4 . . ? C6A4 C6A3 H6A7 108.4 . . ? H6A6 C6A3 H6A7 107.5 . . ? C6A3 C6A4 H6A8 109.5 . . ? C6A3 C6A4 H6A9 109.5 . . ? H6A8 C6A4 H6A9 109.5 . . ? C6A3 C6A4 H6AX 109.5 . . ? H6A8 C6A4 H6AX 109.5 . . ? H6A9 C6A4 H6AX 109.5 . . ? N6 C6A5 C6A6 111.0(19) . . ? N6 C6A5 H6AY 109.4 . . ? C6A6 C6A5 H6AY 109.4 . . ? N6 C6A5 H6AZ 109.4 . . ? C6A6 C6A5 H6AZ 109.4 . . ? H6AY C6A5 H6AZ 108.0 . . ? C6A5 C6A6 H6AA 109.5 . . ? C6A5 C6A6 H6AB 109.5 . . ? H6AA C6A6 H6AB 109.5 . . ? C6A5 C6A6 H6AC 109.5 . . ? H6AA C6A6 H6AC 109.5 . . ? H6AB C6A6 H6AC 109.5 . . ? N6 C6A7 C6A8 117(2) . . ? N6 C6A7 H6AD 108.1 . . ? C6A8 C6A7 H6AD 108.1 . . ? N6 C6A7 H6AE 108.1 . . ? C6A8 C6A7 H6AE 108.1 . . ? H6AD C6A7 H6AE 107.3 . . ? C6A7 C6A8 H6AF 109.5 . . ? C6A7 C6A8 H6AG 109.5 . . ? H6AF C6A8 H6AG 109.5 . . ? C6A7 C6A8 H6AH 109.5 . . ? H6AF C6A8 H6AH 109.5 . . ? H6AG C6A8 H6AH 109.5 . . ? C702 C701 H70A 109.5 . . ? C702 C701 H70B 109.5 . . ? H70A C701 H70B 109.5 . . ? C702 C701 H70C 109.5 . . ? H70A C701 H70C 109.5 . . ? H70B C701 H70C 109.5 . . ? O704 C702 C703 124(2) . . ? O704 C702 C701 120(2) . . ? C703 C702 C701 115(2) . . ? C702 C703 H70D 109.5 . . ? C702 C703 H70E 109.5 . . ? H70D C703 H70E 109.5 . . ? C702 C703 H70F 109.5 . . ? H70D C703 H70F 109.5 . . ? H70E C703 H70F 109.5 . . ? C802 C801 H80A 109.5 . . ? C802 C801 H80B 109.5 . . ? H80A C801 H80B 109.5 . . ? C802 C801 H80C 109.5 . . ? H80A C801 H80C 109.5 . . ? H80B C801 H80C 109.5 . . ? O804 C802 C801 109(3) . . ? O804 C802 C803 111(3) . . ? C801 C802 C803 110(3) . . ? C802 C803 H80D 109.5 . . ? C802 C803 H80E 109.5 . . ? H80D C803 H80E 109.5 . . ? C802 C803 H80F 109.5 . . ? H80D C803 H80F 109.5 . . ? H80E C803 H80F 109.5 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C2 Ni1 Ni2 C26 -12(2) . . . . ? C1 Ni1 Ni2 C26 51(3) . . . . ? C13 Ni1 Ni2 C26 -87(2) . . . . ? C23 Ni1 Ni2 C26 165(2) . . . . ? C22 Ni1 Ni2 C26 166(2) . . . . ? Ni5 Ni1 Ni2 C26 124(2) . . . . ? Ni12 Ni1 Ni2 C26 -150(2) . . . . ? Ni6 Ni1 Ni2 C26 119(2) . . . . ? C2 Ni1 Ni2 C26' -33(6) . . . . ? C1 Ni1 Ni2 C26' 30(6) . . . . ? C13 Ni1 Ni2 C26' -108(6) . . . . ? C23 Ni1 Ni2 C26' 144(6) . . . . ? C22 Ni1 Ni2 C26' 145(6) . . . . ? Ni5 Ni1 Ni2 C26' 103(6) . . . . ? Ni12 Ni1 Ni2 C26' -171(6) . . . . ? Ni6 Ni1 Ni2 C26' 98(6) . . . . ? C1 Ni1 Ni2 C2 62.9(9) . . . . ? C13 Ni1 Ni2 C2 -75.1(8) . . . . ? C23 Ni1 Ni2 C2 176.9(6) . . . . ? C22 Ni1 Ni2 C2 177.9(7) . . . . ? Ni5 Ni1 Ni2 C2 135.5(6) . . . . ? Ni12 Ni1 Ni2 C2 -138.4(6) . . . . ? Ni6 Ni1 Ni2 C2 130.4(5) . . . . ? C2 Ni1 Ni2 C22 -177.9(7) . . . . ? C1 Ni1 Ni2 C22 -115.0(8) . . . . ? C13 Ni1 Ni2 C22 107.0(7) . . . . ? C23 Ni1 Ni2 C22 -1.0(5) . . . . ? Ni5 Ni1 Ni2 C22 -42.4(4) . . . . ? Ni12 Ni1 Ni2 C22 43.7(4) . . . . ? Ni6 Ni1 Ni2 C22 -47.5(4) . . . . ? C2 Ni1 Ni2 Ni18 114.7(7) . . . . ? C1 Ni1 Ni2 Ni18 177.6(8) . . . . ? C13 Ni1 Ni2 Ni18 39.5(7) . . . . ? C23 Ni1 Ni2 Ni18 -68.4(5) . . . . ? C22 Ni1 Ni2 Ni18 -67.4(5) . . . . ? Ni5 Ni1 Ni2 Ni18 -109.8(4) . . . . ? Ni12 Ni1 Ni2 Ni18 -23.7(4) . . . . ? Ni6 Ni1 Ni2 Ni18 -115.0(4) . . . . ? C2 Ni1 Ni2 Ni8 149.5(6) . . . . ? C1 Ni1 Ni2 Ni8 -147.6(7) . . . . ? C13 Ni1 Ni2 Ni8 74.4(5) . . . . ? C23 Ni1 Ni2 Ni8 -33.5(3) . . . . ? C22 Ni1 Ni2 Ni8 -32.6(4) . . . . ? Ni5 Ni1 Ni2 Ni8 -74.93(12) . . . . ? Ni12 Ni1 Ni2 Ni8 11.14(12) . . . . ? Ni6 Ni1 Ni2 Ni8 -80.10(7) . . . . ? C2 Ni1 Ni2 Ni7 -150.7(5) . . . . ? C1 Ni1 Ni2 Ni7 -87.8(7) . . . . ? C13 Ni1 Ni2 Ni7 134.1(5) . . . . ? C23 Ni1 Ni2 Ni7 26.2(3) . . . . ? C22 Ni1 Ni2 Ni7 27.2(4) . . . . ? Ni5 Ni1 Ni2 Ni7 -15.19(14) . . . . ? Ni12 Ni1 Ni2 Ni7 70.89(11) . . . . ? Ni6 Ni1 Ni2 Ni7 -20.35(7) . . . . ? C2 Ni1 Ni2 Ni3 93.8(5) . . . . ? C1 Ni1 Ni2 Ni3 156.7(7) . . . . ? C13 Ni1 Ni2 Ni3 18.6(5) . . . . ? C23 Ni1 Ni2 Ni3 -89.3(3) . . . . ? C22 Ni1 Ni2 Ni3 -88.3(4) . . . . ? Ni5 Ni1 Ni2 Ni3 -130.68(10) . . . . ? Ni12 Ni1 Ni2 Ni3 -44.61(10) . . . . ? Ni6 Ni1 Ni2 Ni3 -135.85(7) . . . . ? C26 Ni2 Ni3 C27 -0.4(17) . . . . ? C26' Ni2 Ni3 C27 4(4) . . . . ? C2 Ni2 Ni3 C27 -102.7(9) . . . . ? C22 Ni2 Ni3 C27 147.5(9) . . . . ? Ni1 Ni2 Ni3 C27 -153.4(9) . . . . ? Ni18 Ni2 Ni3 C27 40.8(9) . . . . ? Ni8 Ni2 Ni3 C27 106.8(9) . . . . ? Ni7 Ni2 Ni3 C27 102.5(9) . . . . ? C26 Ni2 Ni3 C27' -7(2) . . . . ? C26' Ni2 Ni3 C27' -2(4) . . . . ? C2 Ni2 Ni3 C27' -109(2) . . . . ? C22 Ni2 Ni3 C27' 141(2) . . . . ? Ni1 Ni2 Ni3 C27' -160(2) . . . . ? Ni18 Ni2 Ni3 C27' 34(2) . . . . ? Ni8 Ni2 Ni3 C27' 100(2) . . . . ? Ni7 Ni2 Ni3 C27' 96(2) . . . . ? C26 Ni2 Ni3 C3 104.0(16) . . . . ? C26' Ni2 Ni3 C3 109(4) . . . . ? C2 Ni2 Ni3 C3 1.7(6) . . . . ? C22 Ni2 Ni3 C3 -108.1(6) . . . . ? Ni1 Ni2 Ni3 C3 -49.0(4) . . . . ? Ni18 Ni2 Ni3 C3 145.2(5) . . . . ? Ni8 Ni2 Ni3 C3 -148.8(4) . . . . ? Ni7 Ni2 Ni3 C3 -153.1(4) . . . . ? C26 Ni2 Ni3 C25 -145.9(15) . . . . ? C26' Ni2 Ni3 C25 -141(4) . . . . ? C2 Ni2 Ni3 C25 111.8(5) . . . . ? C22 Ni2 Ni3 C25 2.0(5) . . . . ? Ni1 Ni2 Ni3 C25 61.1(4) . . . . ? Ni18 Ni2 Ni3 C25 -104.7(4) . . . . ? Ni8 Ni2 Ni3 C25 -38.7(4) . . . . ? Ni7 Ni2 Ni3 C25 -43.0(4) . . . . ? C26 Ni2 Ni3 Ni4 154.8(15) . . . . ? C26' Ni2 Ni3 Ni4 160(4) . . . . ? C2 Ni2 Ni3 Ni4 52.5(4) . . . . ? C22 Ni2 Ni3 Ni4 -57.3(3) . . . . ? Ni1 Ni2 Ni3 Ni4 1.81(8) . . . . ? Ni18 Ni2 Ni3 Ni4 -164.0(2) . . . . ? Ni8 Ni2 Ni3 Ni4 -97.99(8) . . . . ? Ni7 Ni2 Ni3 Ni4 -102.30(9) . . . . ? C26 Ni2 Ni3 Ni18 -41.2(15) . . . . ? C26' Ni2 Ni3 Ni18 -36(4) . . . . ? C2 Ni2 Ni3 Ni18 -143.5(5) . . . . ? C22 Ni2 Ni3 Ni18 106.7(4) . . . . ? Ni1 Ni2 Ni3 Ni18 165.8(2) . . . . ? Ni8 Ni2 Ni3 Ni18 66.0(2) . . . . ? Ni7 Ni2 Ni3 Ni18 61.7(2) . . . . ? C26 Ni2 Ni3 Ni8 -107.2(15) . . . . ? C26' Ni2 Ni3 Ni8 -102(4) . . . . ? C2 Ni2 Ni3 Ni8 150.5(4) . . . . ? C22 Ni2 Ni3 Ni8 40.7(3) . . . . ? Ni1 Ni2 Ni3 Ni8 99.79(8) . . . . ? Ni18 Ni2 Ni3 Ni8 -66.0(2) . . . . ? Ni7 Ni2 Ni3 Ni8 -4.31(8) . . . . ? C26 Ni2 Ni3 Ni9 -100.6(15) . . . . ? C26' Ni2 Ni3 Ni9 -96(4) . . . . ? C2 Ni2 Ni3 Ni9 157.1(4) . . . . ? C22 Ni2 Ni3 Ni9 47.3(3) . . . . ? Ni1 Ni2 Ni3 Ni9 106.40(9) . . . . ? Ni18 Ni2 Ni3 Ni9 -59.4(2) . . . . ? Ni8 Ni2 Ni3 Ni9 6.61(8) . . . . ? Ni7 Ni2 Ni3 Ni9 2.29(12) . . . . ? C27 Ni3 Ni4 C3 5.2(18) . . . . ? C27' Ni3 Ni4 C3 37(4) . . . . ? C25 Ni3 Ni4 C3 174.5(7) . . . . ? Ni18 Ni3 Ni4 C3 -119.4(7) . . . . ? Ni8 Ni3 Ni4 C3 -153.7(6) . . . . ? Ni9 Ni3 Ni4 C3 145.8(6) . . . . ? Ni2 Ni3 Ni4 C3 -98.4(6) . . . . ? C27 Ni3 Ni4 C4 -58.8(19) . . . . ? C27' Ni3 Ni4 C4 -27(4) . . . . ? C3 Ni3 Ni4 C4 -64.0(10) . . . . ? C25 Ni3 Ni4 C4 110.5(9) . . . . ? Ni18 Ni3 Ni4 C4 176.6(9) . . . . ? Ni8 Ni3 Ni4 C4 142.3(9) . . . . ? Ni9 Ni3 Ni4 C4 81.9(9) . . . . ? Ni2 Ni3 Ni4 C4 -162.4(9) . . . . ? C27 Ni3 Ni4 C13 81.0(17) . . . . ? C27' Ni3 Ni4 C13 113(4) . . . . ? C3 Ni3 Ni4 C13 75.8(8) . . . . ? C25 Ni3 Ni4 C13 -109.7(7) . . . . ? Ni18 Ni3 Ni4 C13 -43.6(6) . . . . ? Ni8 Ni3 Ni4 C13 -78.0(6) . . . . ? Ni9 Ni3 Ni4 C13 -138.4(6) . . . . ? Ni2 Ni3 Ni4 C13 -22.6(6) . . . . ? C27 Ni3 Ni4 C24 -167.7(17) . . . . ? C27' Ni3 Ni4 C24 -135(4) . . . . ? C3 Ni3 Ni4 C24 -172.9(7) . . . . ? C25 Ni3 Ni4 C24 1.6(5) . . . . ? Ni18 Ni3 Ni4 C24 67.7(4) . . . . ? Ni8 Ni3 Ni4 C24 33.4(3) . . . . ? Ni9 Ni3 Ni4 C24 -27.0(3) . . . . ? Ni2 Ni3 Ni4 C24 88.7(3) . . . . ? C27 Ni3 Ni4 C25 -169.3(17) . . . . ? C27' Ni3 Ni4 C25 -137(4) . . . . ? C3 Ni3 Ni4 C25 -174.5(7) . . . . ? Ni18 Ni3 Ni4 C25 66.1(5) . . . . ? Ni8 Ni3 Ni4 C25 31.8(4) . . . . ? Ni9 Ni3 Ni4 C25 -28.6(4) . . . . ? Ni2 Ni3 Ni4 C25 87.1(4) . . . . ? C27 Ni3 Ni4 Ni11 -130.7(16) . . . . ? C27' Ni3 Ni4 Ni11 -98(4) . . . . ? C3 Ni3 Ni4 Ni11 -135.9(6) . . . . ? C25 Ni3 Ni4 Ni11 38.6(4) . . . . ? Ni18 Ni3 Ni4 Ni11 104.7(3) . . . . ? Ni8 Ni3 Ni4 Ni11 70.35(13) . . . . ? Ni9 Ni3 Ni4 Ni11 9.94(15) . . . . ? Ni2 Ni3 Ni4 Ni11 125.67(11) . . . . ? C27 Ni3 Ni4 Ni12 144.4(16) . . . . ? C27' Ni3 Ni4 Ni12 177(4) . . . . ? C3 Ni3 Ni4 Ni12 139.2(6) . . . . ? C25 Ni3 Ni4 Ni12 -46.3(4) . . . . ? Ni18 Ni3 Ni4 Ni12 19.8(3) . . . . ? Ni8 Ni3 Ni4 Ni12 -14.51(12) . . . . ? Ni9 Ni3 Ni4 Ni12 -74.92(11) . . . . ? Ni2 Ni3 Ni4 Ni12 40.81(11) . . . . ? C27 Ni3 Ni4 Ni10 -120.6(17) . . . . ? C27' Ni3 Ni4 Ni10 -88(4) . . . . ? C3 Ni3 Ni4 Ni10 -125.7(6) . . . . ? C25 Ni3 Ni4 Ni10 48.8(4) . . . . ? Ni18 Ni3 Ni4 Ni10 114.8(3) . . . . ? Ni8 Ni3 Ni4 Ni10 80.52(8) . . . . ? Ni9 Ni3 Ni4 Ni10 20.12(8) . . . . ? Ni2 Ni3 Ni4 Ni10 135.85(7) . . . . ? C2 Ni1 Ni5 C5 -85.6(12) . . . . ? C1 Ni1 Ni5 C5 -38.4(11) . . . . ? C13 Ni1 Ni5 C5 42.7(11) . . . . ? C23 Ni1 Ni5 C5 143.1(10) . . . . ? C22 Ni1 Ni5 C5 164.8(10) . . . . ? Ni2 Ni1 Ni5 C5 -163.1(9) . . . . ? Ni12 Ni1 Ni5 C5 83.8(10) . . . . ? Ni6 Ni1 Ni5 C5 -157.0(10) . . . . ? C2 Ni1 Ni5 C1 -47.1(10) . . . . ? C13 Ni1 Ni5 C1 81.2(8) . . . . ? C23 Ni1 Ni5 C1 -178.5(8) . . . . ? C22 Ni1 Ni5 C1 -156.8(7) . . . . ? Ni2 Ni1 Ni5 C1 -124.6(6) . . . . ? Ni12 Ni1 Ni5 C1 122.2(6) . . . . ? Ni6 Ni1 Ni5 C1 -118.5(6) . . . . ? C2 Ni1 Ni5 C23 131.4(9) . . . . ? C1 Ni1 Ni5 C23 178.5(8) . . . . ? C13 Ni1 Ni5 C23 -100.3(6) . . . . ? C22 Ni1 Ni5 C23 21.7(5) . . . . ? Ni2 Ni1 Ni5 C23 53.9(4) . . . . ? Ni12 Ni1 Ni5 C23 -59.3(4) . . . . ? Ni6 Ni1 Ni5 C23 60.0(4) . . . . ? C2 Ni1 Ni5 C6 40.5(9) . . . . ? C1 Ni1 Ni5 C6 87.6(7) . . . . ? C13 Ni1 Ni5 C6 168.8(6) . . . . ? C23 Ni1 Ni5 C6 -90.9(6) . . . . ? C22 Ni1 Ni5 C6 -69.2(5) . . . . ? Ni2 Ni1 Ni5 C6 -37.0(4) . . . . ? Ni12 Ni1 Ni5 C6 -150.2(4) . . . . ? Ni6 Ni1 Ni5 C6 -30.9(4) . . . . ? C2 Ni1 Ni5 Ni6 71.4(8) . . . . ? C1 Ni1 Ni5 Ni6 118.5(6) . . . . ? C13 Ni1 Ni5 Ni6 -160.3(4) . . . . ? C23 Ni1 Ni5 Ni6 -60.0(4) . . . . ? C22 Ni1 Ni5 Ni6 -38.3(3) . . . . ? Ni2 Ni1 Ni5 Ni6 -6.10(11) . . . . ? Ni12 Ni1 Ni5 Ni6 -119.26(8) . . . . ? C2 Ni1 Ni5 Ni14 147.8(8) . . . . ? C1 Ni1 Ni5 Ni14 -165.1(6) . . . . ? C13 Ni1 Ni5 Ni14 -84.0(4) . . . . ? C23 Ni1 Ni5 Ni14 16.4(4) . . . . ? C22 Ni1 Ni5 Ni14 38.1(3) . . . . ? Ni2 Ni1 Ni5 Ni14 70.27(13) . . . . ? Ni12 Ni1 Ni5 Ni14 -42.89(7) . . . . ? Ni6 Ni1 Ni5 Ni14 76.37(8) . . . . ? C2 Ni1 Ni5 Ni12 -169.3(8) . . . . ? C1 Ni1 Ni5 Ni12 -122.2(6) . . . . ? C13 Ni1 Ni5 Ni12 -41.1(4) . . . . ? C23 Ni1 Ni5 Ni12 59.3(4) . . . . ? C22 Ni1 Ni5 Ni12 81.0(3) . . . . ? Ni2 Ni1 Ni5 Ni12 113.16(12) . . . . ? Ni6 Ni1 Ni5 Ni12 119.26(8) . . . . ? C5 Ni5 Ni6 C6 30.3(10) . . . . ? C1 Ni5 Ni6 C6 -89.4(8) . . . . ? C23 Ni5 Ni6 C6 167.3(7) . . . . ? Ni1 Ni5 Ni6 C6 -132.2(6) . . . . ? Ni14 Ni5 Ni6 C6 123.6(6) . . . . ? Ni12 Ni5 Ni6 C6 178.4(6) . . . . ? C5 Ni5 Ni6 C7 24(2) . . . . ? C1 Ni5 Ni6 C7 -95(2) . . . . ? C23 Ni5 Ni6 C7 161(2) . . . . ? C6 Ni5 Ni6 C7 -6(2) . . . . ? Ni1 Ni5 Ni6 C7 -138(2) . . . . ? Ni14 Ni5 Ni6 C7 118(2) . . . . ? Ni12 Ni5 Ni6 C7 172(2) . . . . ? C5 Ni5 Ni6 C22 -157.1(8) . . . . ? C1 Ni5 Ni6 C22 83.3(6) . . . . ? C23 Ni5 Ni6 C22 -20.1(5) . . . . ? C6 Ni5 Ni6 C22 172.6(7) . . . . ? Ni1 Ni5 Ni6 C22 40.4(3) . . . . ? Ni14 Ni5 Ni6 C22 -63.8(3) . . . . ? Ni12 Ni5 Ni6 C22 -9.0(3) . . . . ? C5 Ni5 Ni6 C23 -137.0(8) . . . . ? C1 Ni5 Ni6 C23 103.4(6) . . . . ? C6 Ni5 Ni6 C23 -167.3(7) . . . . ? Ni1 Ni5 Ni6 C23 60.5(4) . . . . ? Ni14 Ni5 Ni6 C23 -43.6(4) . . . . ? Ni12 Ni5 Ni6 C23 11.1(4) . . . . ? C5 Ni5 Ni6 Ni7 -150.4(7) . . . . ? C1 Ni5 Ni6 Ni7 89.9(5) . . . . ? C23 Ni5 Ni6 Ni7 -13.5(4) . . . . ? C6 Ni5 Ni6 Ni7 179.3(6) . . . . ? Ni1 Ni5 Ni6 Ni7 47.07(16) . . . . ? Ni14 Ni5 Ni6 Ni7 -57.11(16) . . . . ? Ni12 Ni5 Ni6 Ni7 -2.35(18) . . . . ? C5 Ni5 Ni6 Ni1 162.5(7) . . . . ? C1 Ni5 Ni6 Ni1 42.9(5) . . . . ? C23 Ni5 Ni6 Ni1 -60.5(4) . . . . ? C6 Ni5 Ni6 Ni1 132.2(6) . . . . ? Ni14 Ni5 Ni6 Ni1 -104.18(7) . . . . ? Ni12 Ni5 Ni6 Ni1 -49.42(7) . . . . ? C5 Ni5 Ni6 Ni13 -109.0(7) . . . . ? C1 Ni5 Ni6 Ni13 131.4(5) . . . . ? C23 Ni5 Ni6 Ni13 28.0(4) . . . . ? C6 Ni5 Ni6 Ni13 -139.3(6) . . . . ? Ni1 Ni5 Ni6 Ni13 88.50(7) . . . . ? Ni14 Ni5 Ni6 Ni13 -15.68(7) . . . . ? Ni12 Ni5 Ni6 Ni13 39.08(8) . . . . ? C2 Ni1 Ni6 C6 -103.3(8) . . . . ? C1 Ni1 Ni6 C6 -0.3(8) . . . . ? C13 Ni1 Ni6 C6 84.6(11) . . . . ? C23 Ni1 Ni6 C6 114.1(8) . . . . ? C22 Ni1 Ni6 C6 166.1(8) . . . . ? Ni2 Ni1 Ni6 C6 -142.2(6) . . . . ? Ni5 Ni1 Ni6 C6 42.6(6) . . . . ? Ni12 Ni1 Ni6 C6 97.3(6) . . . . ? C2 Ni1 Ni6 C7 18.8(9) . . . . ? C1 Ni1 Ni6 C7 121.7(9) . . . . ? C13 Ni1 Ni6 C7 -153.4(12) . . . . ? C23 Ni1 Ni6 C7 -123.8(9) . . . . ? C22 Ni1 Ni6 C7 -71.9(9) . . . . ? Ni2 Ni1 Ni6 C7 -20.1(8) . . . . ? Ni5 Ni1 Ni6 C7 164.7(8) . . . . ? Ni12 Ni1 Ni6 C7 -140.7(8) . . . . ? C2 Ni1 Ni6 C22 90.7(6) . . . . ? C1 Ni1 Ni6 C22 -166.4(6) . . . . ? C13 Ni1 Ni6 C22 -81.5(10) . . . . ? C23 Ni1 Ni6 C22 -51.9(6) . . . . ? Ni2 Ni1 Ni6 C22 51.8(4) . . . . ? Ni5 Ni1 Ni6 C22 -123.4(4) . . . . ? Ni12 Ni1 Ni6 C22 -68.8(4) . . . . ? C2 Ni1 Ni6 C23 142.6(6) . . . . ? C1 Ni1 Ni6 C23 -114.5(6) . . . . ? C13 Ni1 Ni6 C23 -29.6(10) . . . . ? C22 Ni1 Ni6 C23 51.9(6) . . . . ? Ni2 Ni1 Ni6 C23 103.7(4) . . . . ? Ni5 Ni1 Ni6 C23 -71.5(4) . . . . ? Ni12 Ni1 Ni6 C23 -16.9(4) . . . . ? C2 Ni1 Ni6 Ni7 60.7(4) . . . . ? C1 Ni1 Ni6 Ni7 163.7(4) . . . . ? C13 Ni1 Ni6 Ni7 -111.4(9) . . . . ? C23 Ni1 Ni6 Ni7 -81.9(4) . . . . ? C22 Ni1 Ni6 Ni7 -30.0(4) . . . . ? Ni2 Ni1 Ni6 Ni7 21.83(8) . . . . ? Ni5 Ni1 Ni6 Ni7 -153.36(10) . . . . ? Ni12 Ni1 Ni6 Ni7 -98.75(8) . . . . ? C2 Ni1 Ni6 Ni5 -145.9(4) . . . . ? C1 Ni1 Ni6 Ni5 -43.0(4) . . . . ? C13 Ni1 Ni6 Ni5 41.9(9) . . . . ? C23 Ni1 Ni6 Ni5 71.5(4) . . . . ? C22 Ni1 Ni6 Ni5 123.4(4) . . . . ? Ni2 Ni1 Ni6 Ni5 175.19(9) . . . . ? Ni12 Ni1 Ni6 Ni5 54.61(7) . . . . ? C2 Ni1 Ni6 Ni13 119.4(4) . . . . ? C1 Ni1 Ni6 Ni13 -137.7(4) . . . . ? C13 Ni1 Ni6 Ni13 -52.7(9) . . . . ? C23 Ni1 Ni6 Ni13 -23.2(4) . . . . ? C22 Ni1 Ni6 Ni13 28.7(4) . . . . ? Ni2 Ni1 Ni6 Ni13 80.50(7) . . . . ? Ni5 Ni1 Ni6 Ni13 -94.69(8) . . . . ? Ni12 Ni1 Ni6 Ni13 -40.08(8) . . . . ? C6 Ni6 Ni7 C8 7.0(17) . . . . ? C7 Ni6 Ni7 C8 10.3(12) . . . . ? C22 Ni6 Ni7 C8 -163.2(11) . . . . ? C23 Ni6 Ni7 C8 177.5(10) . . . . ? Ni5 Ni6 Ni7 C8 -171.5(10) . . . . ? Ni1 Ni6 Ni7 C8 -134.3(10) . . . . ? Ni13 Ni6 Ni7 C8 138.0(10) . . . . ? C6 Ni6 Ni7 C7 -3.3(15) . . . . ? C22 Ni6 Ni7 C7 -173.5(9) . . . . ? C23 Ni6 Ni7 C7 167.2(8) . . . . ? Ni5 Ni6 Ni7 C7 178.2(8) . . . . ? Ni1 Ni6 Ni7 C7 -144.7(7) . . . . ? Ni13 Ni6 Ni7 C7 127.7(7) . . . . ? C6 Ni6 Ni7 C22 170.2(14) . . . . ? C7 Ni6 Ni7 C22 173.5(9) . . . . ? C23 Ni6 Ni7 C22 -19.3(5) . . . . ? Ni5 Ni6 Ni7 C22 -8.3(4) . . . . ? Ni1 Ni6 Ni7 C22 28.8(4) . . . . ? Ni13 Ni6 Ni7 C22 -58.8(4) . . . . ? C6 Ni6 Ni7 Ni8 175.3(13) . . . . ? C7 Ni6 Ni7 Ni8 178.6(8) . . . . ? C22 Ni6 Ni7 Ni8 5.0(4) . . . . ? C23 Ni6 Ni7 Ni8 -14.3(3) . . . . ? Ni5 Ni6 Ni7 Ni8 -3.26(19) . . . . ? Ni1 Ni6 Ni7 Ni8 33.89(10) . . . . ? Ni13 Ni6 Ni7 Ni8 -53.77(8) . . . . ? C6 Ni6 Ni7 Ni13 -131.0(13) . . . . ? C7 Ni6 Ni7 Ni13 -127.7(7) . . . . ? C22 Ni6 Ni7 Ni13 58.8(4) . . . . ? C23 Ni6 Ni7 Ni13 39.5(3) . . . . ? Ni5 Ni6 Ni7 Ni13 50.51(16) . . . . ? Ni1 Ni6 Ni7 Ni13 87.66(7) . . . . ? C6 Ni6 Ni7 Ni2 121.9(13) . . . . ? C7 Ni6 Ni7 Ni2 125.2(7) . . . . ? C22 Ni6 Ni7 Ni2 -48.3(4) . . . . ? C23 Ni6 Ni7 Ni2 -67.6(3) . . . . ? Ni5 Ni6 Ni7 Ni2 -56.65(16) . . . . ? Ni1 Ni6 Ni7 Ni2 -19.50(7) . . . . ? Ni13 Ni6 Ni7 Ni2 -107.16(8) . . . . ? C26 Ni2 Ni7 C8 5.4(16) . . . . ? C26' Ni2 Ni7 C8 11(3) . . . . ? C2 Ni2 Ni7 C8 129.0(9) . . . . ? C22 Ni2 Ni7 C8 -162.0(8) . . . . ? Ni1 Ni2 Ni7 C8 167.4(6) . . . . ? Ni18 Ni2 Ni7 C8 -47.7(6) . . . . ? Ni8 Ni2 Ni7 C8 -99.5(6) . . . . ? Ni3 Ni2 Ni7 C8 -95.3(6) . . . . ? C26 Ni2 Ni7 C7 -99.3(16) . . . . ? C26' Ni2 Ni7 C7 -94(3) . . . . ? C2 Ni2 Ni7 C7 24.3(9) . . . . ? C22 Ni2 Ni7 C7 93.3(7) . . . . ? Ni1 Ni2 Ni7 C7 62.7(6) . . . . ? Ni18 Ni2 Ni7 C7 -152.4(6) . . . . ? Ni8 Ni2 Ni7 C7 155.8(6) . . . . ? Ni3 Ni2 Ni7 C7 160.0(6) . . . . ? C26 Ni2 Ni7 C22 167.4(15) . . . . ? C26' Ni2 Ni7 C22 173(3) . . . . ? C2 Ni2 Ni7 C22 -69.0(8) . . . . ? Ni1 Ni2 Ni7 C22 -30.6(4) . . . . ? Ni18 Ni2 Ni7 C22 114.3(5) . . . . ? Ni8 Ni2 Ni7 C22 62.6(4) . . . . ? Ni3 Ni2 Ni7 C22 66.7(4) . . . . ? C26 Ni2 Ni7 Ni6 -138.5(14) . . . . ? C26' Ni2 Ni7 Ni6 -133(3) . . . . ? C2 Ni2 Ni7 Ni6 -15.0(7) . . . . ? C22 Ni2 Ni7 Ni6 54.0(4) . . . . ? Ni1 Ni2 Ni7 Ni6 23.43(9) . . . . ? Ni18 Ni2 Ni7 Ni6 168.38(17) . . . . ? Ni8 Ni2 Ni7 Ni6 116.60(8) . . . . ? Ni3 Ni2 Ni7 Ni6 120.79(8) . . . . ? C26 Ni2 Ni7 Ni8 104.9(14) . . . . ? C26' Ni2 Ni7 Ni8 110(3) . . . . ? C2 Ni2 Ni7 Ni8 -131.6(7) . . . . ? C22 Ni2 Ni7 Ni8 -62.6(4) . . . . ? Ni1 Ni2 Ni7 Ni8 -93.18(9) . . . . ? Ni18 Ni2 Ni7 Ni8 51.77(17) . . . . ? Ni3 Ni2 Ni7 Ni8 4.18(8) . . . . ? C26 Ni2 Ni7 Ni13 156.4(14) . . . . ? C26' Ni2 Ni7 Ni13 162(3) . . . . ? C2 Ni2 Ni7 Ni13 -80.0(7) . . . . ? C22 Ni2 Ni7 Ni13 -11.0(4) . . . . ? Ni1 Ni2 Ni7 Ni13 -41.64(10) . . . . ? Ni18 Ni2 Ni7 Ni13 103.31(17) . . . . ? Ni8 Ni2 Ni7 Ni13 51.54(8) . . . . ? Ni3 Ni2 Ni7 Ni13 55.72(10) . . . . ? C8 Ni7 Ni8 C28' -17.8(18) . . . . ? C7 Ni7 Ni8 C28' 172(2) . . . . ? C22 Ni7 Ni8 C28' 174.9(18) . . . . ? Ni6 Ni7 Ni8 C28' 169.6(17) . . . . ? Ni13 Ni7 Ni8 C28' 113.3(17) . . . . ? Ni2 Ni7 Ni8 C28' -125.0(17) . . . . ? C8 Ni7 Ni8 C28 4.1(10) . . . . ? C7 Ni7 Ni8 C28 -166.1(15) . . . . ? C22 Ni7 Ni8 C28 -163.2(9) . . . . ? Ni6 Ni7 Ni8 C28 -168.5(8) . . . . ? Ni13 Ni7 Ni8 C28 135.2(8) . . . . ? Ni2 Ni7 Ni8 C28 -103.1(8) . . . . ? C8 Ni7 Ni8 C25 174.6(8) . . . . ? C7 Ni7 Ni8 C25 4.4(14) . . . . ? C22 Ni7 Ni8 C25 7.3(7) . . . . ? Ni6 Ni7 Ni8 C25 2.0(6) . . . . ? Ni13 Ni7 Ni8 C25 -54.3(6) . . . . ? Ni2 Ni7 Ni8 C25 67.4(6) . . . . ? C8 Ni7 Ni8 C22 167.3(8) . . . . ? C7 Ni7 Ni8 C22 -2.9(13) . . . . ? Ni6 Ni7 Ni8 C22 -5.3(4) . . . . ? Ni13 Ni7 Ni8 C22 -61.6(4) . . . . ? Ni2 Ni7 Ni8 C22 60.1(4) . . . . ? C8 Ni7 Ni8 Ni18 50.0(6) . . . . ? C7 Ni7 Ni8 Ni18 -120.2(13) . . . . ? C22 Ni7 Ni8 Ni18 -117.3(5) . . . . ? Ni6 Ni7 Ni8 Ni18 -122.7(2) . . . . ? Ni13 Ni7 Ni8 Ni18 -178.9(2) . . . . ? Ni2 Ni7 Ni8 Ni18 -57.2(2) . . . . ? C8 Ni7 Ni8 Ni2 107.2(6) . . . . ? C7 Ni7 Ni8 Ni2 -63.0(13) . . . . ? C22 Ni7 Ni8 Ni2 -60.1(4) . . . . ? Ni6 Ni7 Ni8 Ni2 -65.43(9) . . . . ? Ni13 Ni7 Ni8 Ni2 -121.71(8) . . . . ? C8 Ni7 Ni8 Ni9 -31.3(8) . . . . ? C7 Ni7 Ni8 Ni9 158.5(13) . . . . ? C22 Ni7 Ni8 Ni9 161.4(6) . . . . ? Ni6 Ni7 Ni8 Ni9 156.1(4) . . . . ? Ni13 Ni7 Ni8 Ni9 99.8(4) . . . . ? Ni2 Ni7 Ni8 Ni9 -138.5(4) . . . . ? C8 Ni7 Ni8 Ni3 101.6(6) . . . . ? C7 Ni7 Ni8 Ni3 -68.6(13) . . . . ? C22 Ni7 Ni8 Ni3 -65.7(4) . . . . ? Ni6 Ni7 Ni8 Ni3 -71.03(13) . . . . ? Ni13 Ni7 Ni8 Ni3 -127.31(12) . . . . ? Ni2 Ni7 Ni8 Ni3 -5.60(10) . . . . ? C8 Ni7 Ni8 Ni13 -131.1(6) . . . . ? C7 Ni7 Ni8 Ni13 58.7(13) . . . . ? C22 Ni7 Ni8 Ni13 61.6(4) . . . . ? Ni6 Ni7 Ni8 Ni13 56.28(8) . . . . ? Ni2 Ni7 Ni8 Ni13 121.71(8) . . . . ? C8 Ni7 Ni8 Ni16 -119.3(6) . . . . ? C7 Ni7 Ni8 Ni16 70.5(13) . . . . ? C22 Ni7 Ni8 Ni16 73.5(4) . . . . ? Ni6 Ni7 Ni8 Ni16 68.12(12) . . . . ? Ni13 Ni7 Ni8 Ni16 11.84(9) . . . . ? Ni2 Ni7 Ni8 Ni16 133.55(10) . . . . ? C26 Ni2 Ni8 C28' -18(2) . . . . ? C26' Ni2 Ni8 C28' -8(3) . . . . ? C2 Ni2 Ni8 C28' -152(2) . . . . ? C22 Ni2 Ni8 C28' 134(2) . . . . ? Ni1 Ni2 Ni8 C28' 170.9(19) . . . . ? Ni18 Ni2 Ni8 C28' -32.9(19) . . . . ? Ni7 Ni2 Ni8 C28' 72.1(19) . . . . ? Ni3 Ni2 Ni8 C28' -103.3(19) . . . . ? C26 Ni2 Ni8 C28 -13.2(14) . . . . ? C26' Ni2 Ni8 C28 -3(3) . . . . ? C2 Ni2 Ni8 C28 -147.2(10) . . . . ? C22 Ni2 Ni8 C28 139.2(9) . . . . ? Ni1 Ni2 Ni8 C28 175.9(8) . . . . ? Ni18 Ni2 Ni8 C28 -28.0(8) . . . . ? Ni7 Ni2 Ni8 C28 77.1(8) . . . . ? Ni3 Ni2 Ni8 C28 -98.3(8) . . . . ? C26 Ni2 Ni8 C25 124.9(12) . . . . ? C26' Ni2 Ni8 C25 135(3) . . . . ? C2 Ni2 Ni8 C25 -9.0(7) . . . . ? C22 Ni2 Ni8 C25 -82.6(6) . . . . ? Ni1 Ni2 Ni8 C25 -45.9(4) . . . . ? Ni18 Ni2 Ni8 C25 110.2(4) . . . . ? Ni7 Ni2 Ni8 C25 -144.8(4) . . . . ? Ni3 Ni2 Ni8 C25 39.8(4) . . . . ? C26 Ni2 Ni8 C22 -152.5(12) . . . . ? C26' Ni2 Ni8 C22 -142(3) . . . . ? C2 Ni2 Ni8 C22 73.6(8) . . . . ? Ni1 Ni2 Ni8 C22 36.7(5) . . . . ? Ni18 Ni2 Ni8 C22 -167.2(5) . . . . ? Ni7 Ni2 Ni8 C22 -62.1(5) . . . . ? Ni3 Ni2 Ni8 C22 122.5(5) . . . . ? C26 Ni2 Ni8 Ni18 14.7(12) . . . . ? C26' Ni2 Ni8 Ni18 25(3) . . . . ? C2 Ni2 Ni8 Ni18 -119.2(7) . . . . ? C22 Ni2 Ni8 Ni18 167.2(5) . . . . ? Ni1 Ni2 Ni8 Ni18 -156.1(2) . . . . ? Ni7 Ni2 Ni8 Ni18 105.0(2) . . . . ? Ni3 Ni2 Ni8 Ni18 -70.4(2) . . . . ? C26 Ni2 Ni8 Ni7 -90.3(12) . . . . ? C26' Ni2 Ni8 Ni7 -80(3) . . . . ? C2 Ni2 Ni8 Ni7 135.8(6) . . . . ? C22 Ni2 Ni8 Ni7 62.1(5) . . . . ? Ni1 Ni2 Ni8 Ni7 98.85(9) . . . . ? Ni18 Ni2 Ni8 Ni7 -105.0(2) . . . . ? Ni3 Ni2 Ni8 Ni7 -175.41(8) . . . . ? C26 Ni2 Ni8 Ni9 77.3(12) . . . . ? C26' Ni2 Ni8 Ni9 87(3) . . . . ? C2 Ni2 Ni8 Ni9 -56.6(7) . . . . ? C22 Ni2 Ni8 Ni9 -130.3(5) . . . . ? Ni1 Ni2 Ni8 Ni9 -93.54(12) . . . . ? Ni18 Ni2 Ni8 Ni9 62.6(2) . . . . ? Ni7 Ni2 Ni8 Ni9 167.61(13) . . . . ? Ni3 Ni2 Ni8 Ni9 -7.80(10) . . . . ? C26 Ni2 Ni8 Ni3 85.1(12) . . . . ? C26' Ni2 Ni8 Ni3 95(3) . . . . ? C2 Ni2 Ni8 Ni3 -48.8(6) . . . . ? C22 Ni2 Ni8 Ni3 -122.5(5) . . . . ? Ni1 Ni2 Ni8 Ni3 -85.75(8) . . . . ? Ni18 Ni2 Ni8 Ni3 70.4(2) . . . . ? Ni7 Ni2 Ni8 Ni3 175.41(8) . . . . ? C26 Ni2 Ni8 Ni13 -137.5(12) . . . . ? C26' Ni2 Ni8 Ni13 -127(3) . . . . ? C2 Ni2 Ni8 Ni13 88.6(6) . . . . ? C22 Ni2 Ni8 Ni13 14.9(5) . . . . ? Ni1 Ni2 Ni8 Ni13 51.66(9) . . . . ? Ni18 Ni2 Ni8 Ni13 -152.2(2) . . . . ? Ni7 Ni2 Ni8 Ni13 -47.18(7) . . . . ? Ni3 Ni2 Ni8 Ni13 137.41(9) . . . . ? C26 Ni2 Ni8 Ni16 160.7(12) . . . . ? C26' Ni2 Ni8 Ni16 171(3) . . . . ? C2 Ni2 Ni8 Ni16 26.8(7) . . . . ? C22 Ni2 Ni8 Ni16 -46.8(5) . . . . ? Ni1 Ni2 Ni8 Ni16 -10.10(16) . . . . ? Ni18 Ni2 Ni8 Ni16 146.0(3) . . . . ? Ni7 Ni2 Ni8 Ni16 -108.95(14) . . . . ? Ni3 Ni2 Ni8 Ni16 75.64(13) . . . . ? C27 Ni3 Ni8 C28' 32(2) . . . . ? C27' Ni3 Ni8 C28' 18(3) . . . . ? C3 Ni3 Ni8 C28' 170(2) . . . . ? C25 Ni3 Ni8 C28' -120.1(19) . . . . ? Ni4 Ni3 Ni8 C28' -156.9(19) . . . . ? Ni18 Ni3 Ni8 C28' 48.9(19) . . . . ? Ni9 Ni3 Ni8 C28' -57.4(19) . . . . ? Ni2 Ni3 Ni8 C28' 115.6(19) . . . . ? C27 Ni3 Ni8 C28 11.1(11) . . . . ? C27' Ni3 Ni8 C28 -3(2) . . . . ? C3 Ni3 Ni8 C28 148.8(11) . . . . ? C25 Ni3 Ni8 C28 -141.4(9) . . . . ? Ni4 Ni3 Ni8 C28 -178.2(8) . . . . ? Ni18 Ni3 Ni8 C28 27.6(8) . . . . ? Ni9 Ni3 Ni8 C28 -78.7(8) . . . . ? Ni2 Ni3 Ni8 C28 94.3(8) . . . . ? C27 Ni3 Ni8 C25 152.5(9) . . . . ? C27' Ni3 Ni8 C25 138.2(19) . . . . ? C3 Ni3 Ni8 C25 -69.8(9) . . . . ? Ni4 Ni3 Ni8 C25 -36.8(5) . . . . ? Ni18 Ni3 Ni8 C25 169.0(5) . . . . ? Ni9 Ni3 Ni8 C25 62.7(5) . . . . ? Ni2 Ni3 Ni8 C25 -124.3(5) . . . . ? C27 Ni3 Ni8 C22 -124.3(8) . . . . ? C27' Ni3 Ni8 C22 -138.6(18) . . . . ? C3 Ni3 Ni8 C22 13.5(8) . . . . ? C25 Ni3 Ni8 C22 83.2(6) . . . . ? Ni4 Ni3 Ni8 C22 46.5(4) . . . . ? Ni18 Ni3 Ni8 C22 -107.7(4) . . . . ? Ni9 Ni3 Ni8 C22 145.9(4) . . . . ? Ni2 Ni3 Ni8 C22 -41.0(4) . . . . ? C27 Ni3 Ni8 Ni18 -16.5(8) . . . . ? C27' Ni3 Ni8 Ni18 -30.8(18) . . . . ? C3 Ni3 Ni8 Ni18 121.2(7) . . . . ? C25 Ni3 Ni8 Ni18 -169.0(5) . . . . ? Ni4 Ni3 Ni8 Ni18 154.2(2) . . . . ? Ni9 Ni3 Ni8 Ni18 -106.3(2) . . . . ? Ni2 Ni3 Ni8 Ni18 66.69(19) . . . . ? C27 Ni3 Ni8 Ni7 -77.9(7) . . . . ? C27' Ni3 Ni8 Ni7 -92.3(18) . . . . ? C3 Ni3 Ni8 Ni7 59.8(7) . . . . ? C25 Ni3 Ni8 Ni7 129.6(5) . . . . ? Ni4 Ni3 Ni8 Ni7 92.79(12) . . . . ? Ni18 Ni3 Ni8 Ni7 -61.4(2) . . . . ? Ni9 Ni3 Ni8 Ni7 -167.74(13) . . . . ? Ni2 Ni3 Ni8 Ni7 5.28(10) . . . . ? C27 Ni3 Ni8 Ni2 -83.2(7) . . . . ? C27' Ni3 Ni8 Ni2 -97.5(18) . . . . ? C3 Ni3 Ni8 Ni2 54.5(7) . . . . ? C25 Ni3 Ni8 Ni2 124.3(5) . . . . ? Ni4 Ni3 Ni8 Ni2 87.51(8) . . . . ? Ni18 Ni3 Ni8 Ni2 -66.69(19) . . . . ? Ni9 Ni3 Ni8 Ni2 -173.02(9) . . . . ? C27 Ni3 Ni8 Ni9 89.8(7) . . . . ? C27' Ni3 Ni8 Ni9 75.5(18) . . . . ? C3 Ni3 Ni8 Ni9 -132.5(7) . . . . ? C25 Ni3 Ni8 Ni9 -62.7(5) . . . . ? Ni4 Ni3 Ni8 Ni9 -99.47(9) . . . . ? Ni18 Ni3 Ni8 Ni9 106.3(2) . . . . ? Ni2 Ni3 Ni8 Ni9 173.02(9) . . . . ? C27 Ni3 Ni8 Ni13 -162.4(7) . . . . ? C27' Ni3 Ni8 Ni13 -176.7(18) . . . . ? C3 Ni3 Ni8 Ni13 -24.7(7) . . . . ? C25 Ni3 Ni8 Ni13 45.1(5) . . . . ? Ni4 Ni3 Ni8 Ni13 8.36(15) . . . . ? Ni18 Ni3 Ni8 Ni13 -145.8(2) . . . . ? Ni9 Ni3 Ni8 Ni13 107.83(14) . . . . ? Ni2 Ni3 Ni8 Ni13 -79.15(12) . . . . ? C27 Ni3 Ni8 Ni16 135.5(7) . . . . ? C27' Ni3 Ni8 Ni16 121.2(18) . . . . ? C3 Ni3 Ni8 Ni16 -86.7(7) . . . . ? C25 Ni3 Ni8 Ni16 -17.0(5) . . . . ? Ni4 Ni3 Ni8 Ni16 -53.73(9) . . . . ? Ni18 Ni3 Ni8 Ni16 152.1(2) . . . . ? Ni9 Ni3 Ni8 Ni16 45.74(8) . . . . ? Ni2 Ni3 Ni8 Ni16 -141.24(8) . . . . ? C28' Ni8 Ni9 C9 14.7(18) . . . . ? C28 Ni8 Ni9 C9 -6.5(10) . . . . ? C25 Ni8 Ni9 C9 -171.4(8) . . . . ? C22 Ni8 Ni9 C9 -175.3(8) . . . . ? Ni18 Ni8 Ni9 C9 -52.3(7) . . . . ? Ni7 Ni8 Ni9 C9 28.7(8) . . . . ? Ni2 Ni8 Ni9 C9 -102.9(6) . . . . ? Ni3 Ni8 Ni9 C9 -111.3(6) . . . . ? Ni13 Ni8 Ni9 C9 119.3(6) . . . . ? Ni16 Ni8 Ni9 C9 126.1(6) . . . . ? C28' Ni8 Ni9 C10 175(2) . . . . ? C28 Ni8 Ni9 C10 153.5(15) . . . . ? C25 Ni8 Ni9 C10 -11.4(14) . . . . ? C22 Ni8 Ni9 C10 -15.2(14) . . . . ? Ni18 Ni8 Ni9 C10 107.7(13) . . . . ? Ni7 Ni8 Ni9 C10 -171.3(13) . . . . ? Ni2 Ni8 Ni9 C10 57.1(13) . . . . ? Ni3 Ni8 Ni9 C10 48.8(13) . . . . ? Ni13 Ni8 Ni9 C10 -80.7(13) . . . . ? Ni16 Ni8 Ni9 C10 -73.8(13) . . . . ? C28' Ni8 Ni9 C25 -173.9(18) . . . . ? C28 Ni8 Ni9 C25 164.9(9) . . . . ? C22 Ni8 Ni9 C25 -3.8(7) . . . . ? Ni18 Ni8 Ni9 C25 119.1(5) . . . . ? Ni7 Ni8 Ni9 C25 -159.9(6) . . . . ? Ni2 Ni8 Ni9 C25 68.5(4) . . . . ? Ni3 Ni8 Ni9 C25 60.2(4) . . . . ? Ni13 Ni8 Ni9 C25 -69.3(4) . . . . ? Ni16 Ni8 Ni9 C25 -62.4(4) . . . . ? C28' Ni8 Ni9 Ni10 -168.1(17) . . . . ? C28 Ni8 Ni9 Ni10 170.7(8) . . . . ? C25 Ni8 Ni9 Ni10 5.7(4) . . . . ? C22 Ni8 Ni9 Ni10 1.9(6) . . . . ? Ni18 Ni8 Ni9 Ni10 124.8(2) . . . . ? Ni7 Ni8 Ni9 Ni10 -154.2(4) . . . . ? Ni2 Ni8 Ni9 Ni10 74.28(13) . . . . ? Ni3 Ni8 Ni9 Ni10 65.93(9) . . . . ? Ni13 Ni8 Ni9 Ni10 -63.53(12) . . . . ? Ni16 Ni8 Ni9 Ni10 -56.68(9) . . . . ? C28' Ni8 Ni9 C17' -75(2) . . . . ? C28 Ni8 Ni9 C17' -95.9(17) . . . . ? C25 Ni8 Ni9 C17' 99.2(15) . . . . ? C22 Ni8 Ni9 C17' 95.4(16) . . . . ? Ni18 Ni8 Ni9 C17' -141.7(15) . . . . ? Ni7 Ni8 Ni9 C17' -60.7(15) . . . . ? Ni2 Ni8 Ni9 C17' 167.7(14) . . . . ? Ni3 Ni8 Ni9 C17' 159.4(14) . . . . ? Ni13 Ni8 Ni9 C17' 29.9(14) . . . . ? Ni16 Ni8 Ni9 C17' 36.8(14) . . . . ? C28' Ni8 Ni9 Ni16 -111.4(17) . . . . ? C28 Ni8 Ni9 Ni16 -132.7(8) . . . . ? C25 Ni8 Ni9 Ni16 62.4(4) . . . . ? C22 Ni8 Ni9 Ni16 58.6(6) . . . . ? Ni18 Ni8 Ni9 Ni16 -178.5(2) . . . . ? Ni7 Ni8 Ni9 Ni16 -97.5(4) . . . . ? Ni2 Ni8 Ni9 Ni16 130.95(11) . . . . ? Ni3 Ni8 Ni9 Ni16 122.60(9) . . . . ? Ni13 Ni8 Ni9 Ni16 -6.86(10) . . . . ? C28' Ni8 Ni9 Ni3 126.0(17) . . . . ? C28 Ni8 Ni9 Ni3 104.7(8) . . . . ? C25 Ni8 Ni9 Ni3 -60.2(4) . . . . ? C22 Ni8 Ni9 Ni3 -64.0(6) . . . . ? Ni18 Ni8 Ni9 Ni3 58.9(2) . . . . ? Ni7 Ni8 Ni9 Ni3 139.9(4) . . . . ? Ni2 Ni8 Ni9 Ni3 8.35(11) . . . . ? Ni13 Ni8 Ni9 Ni3 -129.46(10) . . . . ? Ni16 Ni8 Ni9 Ni3 -122.60(9) . . . . ? C27 Ni3 Ni9 C9 -5.2(11) . . . . ? C27' Ni3 Ni9 C9 -14(2) . . . . ? C3 Ni3 Ni9 C9 -127.1(10) . . . . ? C25 Ni3 Ni9 C9 158.6(8) . . . . ? Ni4 Ni3 Ni9 C9 -169.3(7) . . . . ? Ni18 Ni3 Ni9 C9 48.6(7) . . . . ? Ni8 Ni3 Ni9 C9 98.6(7) . . . . ? Ni2 Ni3 Ni9 C9 92.2(7) . . . . ? C27 Ni3 Ni9 C10 98.4(11) . . . . ? C27' Ni3 Ni9 C10 90(2) . . . . ? C3 Ni3 Ni9 C10 -23.5(10) . . . . ? C25 Ni3 Ni9 C10 -97.8(8) . . . . ? Ni4 Ni3 Ni9 C10 -65.6(7) . . . . ? Ni18 Ni3 Ni9 C10 152.2(7) . . . . ? Ni8 Ni3 Ni9 C10 -157.8(7) . . . . ? Ni2 Ni3 Ni9 C10 -164.1(7) . . . . ? C27 Ni3 Ni9 C25 -163.9(9) . . . . ? C27' Ni3 Ni9 C25 -172(2) . . . . ? C3 Ni3 Ni9 C25 74.3(8) . . . . ? Ni4 Ni3 Ni9 C25 32.1(4) . . . . ? Ni18 Ni3 Ni9 C25 -110.0(5) . . . . ? Ni8 Ni3 Ni9 C25 -60.1(4) . . . . ? Ni2 Ni3 Ni9 C25 -66.4(4) . . . . ? C27 Ni3 Ni9 Ni10 141.1(8) . . . . ? C27' Ni3 Ni9 Ni10 133(2) . . . . ? C3 Ni3 Ni9 Ni10 19.3(7) . . . . ? C25 Ni3 Ni9 Ni10 -55.0(4) . . . . ? Ni4 Ni3 Ni9 Ni10 -22.88(9) . . . . ? Ni18 Ni3 Ni9 Ni10 -165.01(17) . . . . ? Ni8 Ni3 Ni9 Ni10 -115.05(9) . . . . ? Ni2 Ni3 Ni9 Ni10 -121.36(9) . . . . ? C27 Ni3 Ni9 C17' -137(3) . . . . ? C27' Ni3 Ni9 C17' -145(3) . . . . ? C3 Ni3 Ni9 C17' 101(3) . . . . ? C25 Ni3 Ni9 C17' 27(3) . . . . ? Ni4 Ni3 Ni9 C17' 59(2) . . . . ? Ni18 Ni3 Ni9 C17' -83(2) . . . . ? Ni8 Ni3 Ni9 C17' -33(2) . . . . ? Ni2 Ni3 Ni9 C17' -39(2) . . . . ? C27 Ni3 Ni9 Ni16 -155.0(8) . . . . ? C27' Ni3 Ni9 Ni16 -163(2) . . . . ? C3 Ni3 Ni9 Ni16 83.1(7) . . . . ? C25 Ni3 Ni9 Ni16 8.9(4) . . . . ? Ni4 Ni3 Ni9 Ni16 40.97(11) . . . . ? Ni18 Ni3 Ni9 Ni16 -101.17(18) . . . . ? Ni8 Ni3 Ni9 Ni16 -51.21(8) . . . . ? Ni2 Ni3 Ni9 Ni16 -57.51(11) . . . . ? C27 Ni3 Ni9 Ni8 -103.8(8) . . . . ? C27' Ni3 Ni9 Ni8 -112(2) . . . . ? C3 Ni3 Ni9 Ni8 134.3(7) . . . . ? C25 Ni3 Ni9 Ni8 60.1(4) . . . . ? Ni4 Ni3 Ni9 Ni8 92.18(9) . . . . ? Ni18 Ni3 Ni9 Ni8 -49.96(16) . . . . ? Ni2 Ni3 Ni9 Ni8 -6.30(8) . . . . ? C9 Ni9 Ni10 C11 -8.6(16) . . . . ? C10 Ni9 Ni10 C11 -15.4(14) . . . . ? C25 Ni9 Ni10 C11 -178.7(12) . . . . ? C17' Ni9 Ni10 C11 89.7(19) . . . . ? Ni16 Ni9 Ni10 C11 121.4(12) . . . . ? Ni8 Ni9 Ni10 C11 176.0(11) . . . . ? Ni3 Ni9 Ni10 C11 -129.9(11) . . . . ? C9 Ni9 Ni10 C10 6.8(13) . . . . ? C25 Ni9 Ni10 C10 -163.3(10) . . . . ? C17' Ni9 Ni10 C10 105.1(17) . . . . ? Ni16 Ni9 Ni10 C10 136.8(9) . . . . ? Ni8 Ni9 Ni10 C10 -168.6(9) . . . . ? Ni3 Ni9 Ni10 C10 -114.5(9) . . . . ? C9 Ni9 Ni10 C24 -169.7(11) . . . . ? C10 Ni9 Ni10 C24 -176.6(9) . . . . ? C25 Ni9 Ni10 C24 20.1(5) . . . . ? C17' Ni9 Ni10 C24 -71.5(16) . . . . ? Ni16 Ni9 Ni10 C24 -39.8(3) . . . . ? Ni8 Ni9 Ni10 C24 14.9(3) . . . . ? Ni3 Ni9 Ni10 C24 69.0(3) . . . . ? C9 Ni9 Ni10 C25 170.1(11) . . . . ? C10 Ni9 Ni10 C25 163.3(10) . . . . ? C17' Ni9 Ni10 C25 -91.6(16) . . . . ? Ni16 Ni9 Ni10 C25 -59.9(4) . . . . ? Ni8 Ni9 Ni10 C25 -5.3(4) . . . . ? Ni3 Ni9 Ni10 C25 48.8(4) . . . . ? C9 Ni9 Ni10 Ni11 -177.3(10) . . . . ? C10 Ni9 Ni10 Ni11 175.9(9) . . . . ? C25 Ni9 Ni10 Ni11 12.6(4) . . . . ? C17' Ni9 Ni10 Ni11 -79.0(15) . . . . ? Ni16 Ni9 Ni10 Ni11 -47.31(16) . . . . ? Ni8 Ni9 Ni10 Ni11 7.3(2) . . . . ? Ni3 Ni9 Ni10 Ni11 61.42(16) . . . . ? C9 Ni9 Ni10 Ni4 140.7(10) . . . . ? C10 Ni9 Ni10 Ni4 133.8(9) . . . . ? C25 Ni9 Ni10 Ni4 -29.4(4) . . . . ? C17' Ni9 Ni10 Ni4 -121.1(15) . . . . ? Ni16 Ni9 Ni10 Ni4 -89.37(8) . . . . ? Ni8 Ni9 Ni10 Ni4 -34.72(10) . . . . ? Ni3 Ni9 Ni10 Ni4 19.36(7) . . . . ? C9 Ni9 Ni10 Ni16 -130.0(10) . . . . ? C10 Ni9 Ni10 Ni16 -136.8(9) . . . . ? C25 Ni9 Ni10 Ni16 59.9(4) . . . . ? C17' Ni9 Ni10 Ni16 -31.7(15) . . . . ? Ni8 Ni9 Ni10 Ni16 54.65(8) . . . . ? Ni3 Ni9 Ni10 Ni16 108.73(8) . . . . ? C3 Ni4 Ni10 C11 103.4(7) . . . . ? C4 Ni4 Ni10 C11 0.6(8) . . . . ? C13 Ni4 Ni10 C11 -79.6(11) . . . . ? C24 Ni4 Ni10 C11 -112.4(7) . . . . ? C25 Ni4 Ni10 C11 -163.4(7) . . . . ? Ni3 Ni4 Ni10 C11 144.8(5) . . . . ? Ni11 Ni4 Ni10 C11 -44.4(5) . . . . ? Ni12 Ni4 Ni10 C11 -94.6(5) . . . . ? C3 Ni4 Ni10 C10 -16.1(10) . . . . ? C4 Ni4 Ni10 C10 -118.9(11) . . . . ? C13 Ni4 Ni10 C10 160.9(13) . . . . ? C24 Ni4 Ni10 C10 128.1(10) . . . . ? C25 Ni4 Ni10 C10 77.1(10) . . . . ? Ni3 Ni4 Ni10 C10 25.3(9) . . . . ? Ni11 Ni4 Ni10 C10 -164.0(9) . . . . ? Ni12 Ni4 Ni10 C10 145.9(9) . . . . ? C3 Ni4 Ni10 C24 -144.2(6) . . . . ? C4 Ni4 Ni10 C24 113.0(7) . . . . ? C13 Ni4 Ni10 C24 32.8(11) . . . . ? C25 Ni4 Ni10 C24 -51.0(6) . . . . ? Ni3 Ni4 Ni10 C24 -102.8(5) . . . . ? Ni11 Ni4 Ni10 C24 68.0(5) . . . . ? Ni12 Ni4 Ni10 C24 17.8(5) . . . . ? C3 Ni4 Ni10 C25 -93.2(6) . . . . ? C4 Ni4 Ni10 C25 164.0(7) . . . . ? C13 Ni4 Ni10 C25 83.8(11) . . . . ? C24 Ni4 Ni10 C25 51.0(6) . . . . ? Ni3 Ni4 Ni10 C25 -51.9(4) . . . . ? Ni11 Ni4 Ni10 C25 118.9(4) . . . . ? Ni12 Ni4 Ni10 C25 68.8(4) . . . . ? C3 Ni4 Ni10 Ni9 -62.9(5) . . . . ? C4 Ni4 Ni10 Ni9 -165.7(6) . . . . ? C13 Ni4 Ni10 Ni9 114.1(10) . . . . ? C24 Ni4 Ni10 Ni9 81.3(5) . . . . ? C25 Ni4 Ni10 Ni9 30.3(4) . . . . ? Ni3 Ni4 Ni10 Ni9 -21.55(8) . . . . ? Ni11 Ni4 Ni10 Ni9 149.25(10) . . . . ? Ni12 Ni4 Ni10 Ni9 99.09(9) . . . . ? C3 Ni4 Ni10 Ni11 147.8(5) . . . . ? C4 Ni4 Ni10 Ni11 45.0(6) . . . . ? C13 Ni4 Ni10 Ni11 -35.2(10) . . . . ? C24 Ni4 Ni10 Ni11 -68.0(5) . . . . ? C25 Ni4 Ni10 Ni11 -118.9(4) . . . . ? Ni3 Ni4 Ni10 Ni11 -170.80(9) . . . . ? Ni12 Ni4 Ni10 Ni11 -50.15(8) . . . . ? C3 Ni4 Ni10 Ni16 -121.9(5) . . . . ? C4 Ni4 Ni10 Ni16 135.3(6) . . . . ? C13 Ni4 Ni10 Ni16 55.1(10) . . . . ? C24 Ni4 Ni10 Ni16 22.3(5) . . . . ? C25 Ni4 Ni10 Ni16 -28.7(4) . . . . ? Ni3 Ni4 Ni10 Ni16 -80.53(8) . . . . ? Ni11 Ni4 Ni10 Ni16 90.26(9) . . . . ? Ni12 Ni4 Ni10 Ni16 40.11(9) . . . . ? C3 Ni4 Ni11 C12 80.6(15) . . . . ? C4 Ni4 Ni11 C12 35.3(14) . . . . ? C13 Ni4 Ni11 C12 -47.0(13) . . . . ? C24 Ni4 Ni11 C12 -151.4(13) . . . . ? C25 Ni4 Ni11 C12 -170.7(13) . . . . ? Ni3 Ni4 Ni11 C12 159.9(12) . . . . ? Ni12 Ni4 Ni11 C12 -87.3(12) . . . . ? Ni10 Ni4 Ni11 C12 148.1(13) . . . . ? C3 Ni4 Ni11 C4 45.3(11) . . . . ? C13 Ni4 Ni11 C4 -82.3(9) . . . . ? C24 Ni4 Ni11 C4 173.3(8) . . . . ? C25 Ni4 Ni11 C4 154.0(8) . . . . ? Ni3 Ni4 Ni11 C4 124.6(7) . . . . ? Ni12 Ni4 Ni11 C4 -122.6(7) . . . . ? Ni10 Ni4 Ni11 C4 112.8(7) . . . . ? C3 Ni4 Ni11 C24 -127.9(9) . . . . ? C4 Ni4 Ni11 C24 -173.3(8) . . . . ? C13 Ni4 Ni11 C24 104.4(6) . . . . ? C25 Ni4 Ni11 C24 -19.2(5) . . . . ? Ni3 Ni4 Ni11 C24 -48.7(4) . . . . ? Ni12 Ni4 Ni11 C24 64.1(4) . . . . ? Ni10 Ni4 Ni11 C24 -60.5(4) . . . . ? C3 Ni4 Ni11 C11 -37.7(9) . . . . ? C4 Ni4 Ni11 C11 -83.1(8) . . . . ? C13 Ni4 Ni11 C11 -165.4(6) . . . . ? C24 Ni4 Ni11 C11 90.2(6) . . . . ? C25 Ni4 Ni11 C11 71.0(5) . . . . ? Ni3 Ni4 Ni11 C11 41.5(4) . . . . ? Ni12 Ni4 Ni11 C11 154.3(4) . . . . ? Ni10 Ni4 Ni11 C11 29.7(4) . . . . ? C3 Ni4 Ni11 Ni10 -67.4(8) . . . . ? C4 Ni4 Ni11 Ni10 -112.8(7) . . . . ? C13 Ni4 Ni11 Ni10 164.9(5) . . . . ? C24 Ni4 Ni11 Ni10 60.5(4) . . . . ? C25 Ni4 Ni11 Ni10 41.3(3) . . . . ? Ni3 Ni4 Ni11 Ni10 11.83(12) . . . . ? Ni12 Ni4 Ni11 Ni10 124.65(8) . . . . ? C3 Ni4 Ni11 Ni15 -147.2(8) . . . . ? C4 Ni4 Ni11 Ni15 167.4(7) . . . . ? C13 Ni4 Ni11 Ni15 85.1(5) . . . . ? C24 Ni4 Ni11 Ni15 -19.3(4) . . . . ? C25 Ni4 Ni11 Ni15 -38.5(3) . . . . ? Ni3 Ni4 Ni11 Ni15 -67.98(14) . . . . ? Ni12 Ni4 Ni11 Ni15 44.84(8) . . . . ? Ni10 Ni4 Ni11 Ni15 -79.81(9) . . . . ? C3 Ni4 Ni11 Ni12 167.9(8) . . . . ? C4 Ni4 Ni11 Ni12 122.6(7) . . . . ? C13 Ni4 Ni11 Ni12 40.3(5) . . . . ? C24 Ni4 Ni11 Ni12 -64.1(4) . . . . ? C25 Ni4 Ni11 Ni12 -83.4(3) . . . . ? Ni3 Ni4 Ni11 Ni12 -112.83(12) . . . . ? Ni10 Ni4 Ni11 Ni12 -124.65(8) . . . . ? C11 Ni10 Ni11 C12 -28.2(10) . . . . ? C10 Ni10 Ni11 C12 -48(3) . . . . ? C24 Ni10 Ni11 C12 136.8(9) . . . . ? C25 Ni10 Ni11 C12 156.4(8) . . . . ? Ni9 Ni10 Ni11 C12 146.2(8) . . . . ? Ni4 Ni10 Ni11 C12 -160.2(8) . . . . ? Ni16 Ni10 Ni11 C12 107.2(8) . . . . ? C11 Ni10 Ni11 C4 87.0(8) . . . . ? C10 Ni10 Ni11 C4 67(3) . . . . ? C24 Ni10 Ni11 C4 -107.9(7) . . . . ? C25 Ni10 Ni11 C4 -88.4(6) . . . . ? Ni9 Ni10 Ni11 C4 -98.5(6) . . . . ? Ni4 Ni10 Ni11 C4 -44.9(6) . . . . ? Ni16 Ni10 Ni11 C4 -137.5(6) . . . . ? C11 Ni10 Ni11 C24 -165.1(7) . . . . ? C10 Ni10 Ni11 C24 175(3) . . . . ? C25 Ni10 Ni11 C24 19.6(5) . . . . ? Ni9 Ni10 Ni11 C24 9.4(4) . . . . ? Ni4 Ni10 Ni11 C24 63.0(4) . . . . ? Ni16 Ni10 Ni11 C24 -29.6(4) . . . . ? C10 Ni10 Ni11 C11 -20(3) . . . . ? C24 Ni10 Ni11 C11 165.1(7) . . . . ? C25 Ni10 Ni11 C11 -175.4(6) . . . . ? Ni9 Ni10 Ni11 C11 174.5(6) . . . . ? Ni4 Ni10 Ni11 C11 -131.9(6) . . . . ? Ni16 Ni10 Ni11 C11 135.5(6) . . . . ? C11 Ni10 Ni11 Ni4 131.9(6) . . . . ? C10 Ni10 Ni11 Ni4 112(3) . . . . ? C24 Ni10 Ni11 Ni4 -63.0(4) . . . . ? C25 Ni10 Ni11 Ni4 -43.4(3) . . . . ? Ni9 Ni10 Ni11 Ni4 -53.59(16) . . . . ? Ni16 Ni10 Ni11 Ni4 -92.59(8) . . . . ? C11 Ni10 Ni11 Ni15 -125.4(6) . . . . ? C10 Ni10 Ni11 Ni15 -145(3) . . . . ? C24 Ni10 Ni11 Ni15 39.6(4) . . . . ? C25 Ni10 Ni11 Ni15 59.2(3) . . . . ? Ni9 Ni10 Ni11 Ni15 49.06(17) . . . . ? Ni4 Ni10 Ni11 Ni15 102.65(8) . . . . ? Ni16 Ni10 Ni11 Ni15 10.06(7) . . . . ? C11 Ni10 Ni11 Ni12 178.7(6) . . . . ? C10 Ni10 Ni11 Ni12 159(3) . . . . ? C24 Ni10 Ni11 Ni12 -16.2(4) . . . . ? C25 Ni10 Ni11 Ni12 3.3(3) . . . . ? Ni9 Ni10 Ni11 Ni12 -6.83(19) . . . . ? Ni4 Ni10 Ni11 Ni12 46.76(7) . . . . ? Ni16 Ni10 Ni11 Ni12 -45.83(9) . . . . ? C3 Ni4 Ni12 C20 -104(3) . . . . ? C4 Ni4 Ni12 C20 24(3) . . . . ? C13 Ni4 Ni12 C20 -63(3) . . . . ? C24 Ni4 Ni12 C20 125(3) . . . . ? C25 Ni4 Ni12 C20 154(3) . . . . ? Ni3 Ni4 Ni12 C20 -171(3) . . . . ? Ni11 Ni4 Ni12 C20 64(3) . . . . ? Ni10 Ni4 Ni12 C20 109(3) . . . . ? C3 Ni4 Ni12 C20' -103.3(14) . . . . ? C4 Ni4 Ni12 C20' 24.4(12) . . . . ? C13 Ni4 Ni12 C20' -62.5(12) . . . . ? C24 Ni4 Ni12 C20' 125.4(12) . . . . ? C25 Ni4 Ni12 C20' 154.2(11) . . . . ? Ni3 Ni4 Ni12 C20' -170.8(11) . . . . ? Ni11 Ni4 Ni12 C20' 64.6(11) . . . . ? Ni10 Ni4 Ni12 C20' 109.2(11) . . . . ? C3 Ni4 Ni12 C13 -40.7(10) . . . . ? C4 Ni4 Ni12 C13 86.9(8) . . . . ? C24 Ni4 Ni12 C13 -172.1(7) . . . . ? C25 Ni4 Ni12 C13 -143.3(6) . . . . ? Ni3 Ni4 Ni12 C13 -108.3(6) . . . . ? Ni11 Ni4 Ni12 C13 127.2(5) . . . . ? Ni10 Ni4 Ni12 C13 171.7(5) . . . . ? C3 Ni4 Ni12 C23 54.7(9) . . . . ? C4 Ni4 Ni12 C23 -177.6(7) . . . . ? C13 Ni4 Ni12 C23 95.4(6) . . . . ? C24 Ni4 Ni12 C23 -76.7(5) . . . . ? C25 Ni4 Ni12 C23 -47.8(5) . . . . ? Ni3 Ni4 Ni12 C23 -12.8(3) . . . . ? Ni11 Ni4 Ni12 C23 -137.4(3) . . . . ? Ni10 Ni4 Ni12 C23 -92.9(3) . . . . ? C3 Ni4 Ni12 C24 131.4(9) . . . . ? C4 Ni4 Ni12 C24 -101.0(7) . . . . ? C13 Ni4 Ni12 C24 172.1(7) . . . . ? C25 Ni4 Ni12 C24 28.9(5) . . . . ? Ni3 Ni4 Ni12 C24 63.8(4) . . . . ? Ni11 Ni4 Ni12 C24 -60.7(4) . . . . ? Ni10 Ni4 Ni12 C24 -16.2(4) . . . . ? C3 Ni4 Ni12 Ni17 -161.2(8) . . . . ? C4 Ni4 Ni12 Ni17 -33.5(6) . . . . ? C13 Ni4 Ni12 Ni17 -120.4(6) . . . . ? C24 Ni4 Ni12 Ni17 67.4(4) . . . . ? C25 Ni4 Ni12 Ni17 96.3(3) . . . . ? Ni3 Ni4 Ni12 Ni17 131.28(14) . . . . ? Ni11 Ni4 Ni12 Ni17 6.72(14) . . . . ? Ni10 Ni4 Ni12 Ni17 51.26(15) . . . . ? C3 Ni4 Ni12 Ni1 10.3(8) . . . . ? C4 Ni4 Ni12 Ni1 137.9(6) . . . . ? C13 Ni4 Ni12 Ni1 51.0(5) . . . . ? C24 Ni4 Ni12 Ni1 -121.1(4) . . . . ? C25 Ni4 Ni12 Ni1 -92.3(3) . . . . ? Ni3 Ni4 Ni12 Ni1 -57.27(10) . . . . ? Ni11 Ni4 Ni12 Ni1 178.17(9) . . . . ? Ni10 Ni4 Ni12 Ni1 -137.30(8) . . . . ? C3 Ni4 Ni12 Ni14 90.0(8) . . . . ? C4 Ni4 Ni12 Ni14 -142.4(6) . . . . ? C13 Ni4 Ni12 Ni14 130.7(6) . . . . ? C24 Ni4 Ni12 Ni14 -41.4(4) . . . . ? C25 Ni4 Ni12 Ni14 -12.6(3) . . . . ? Ni3 Ni4 Ni12 Ni14 22.44(19) . . . . ? Ni11 Ni4 Ni12 Ni14 -102.12(14) . . . . ? Ni10 Ni4 Ni12 Ni14 -57.58(15) . . . . ? C3 Ni4 Ni12 Ni15 148.1(8) . . . . ? C4 Ni4 Ni12 Ni15 -84.3(6) . . . . ? C13 Ni4 Ni12 Ni15 -171.2(5) . . . . ? C24 Ni4 Ni12 Ni15 16.7(4) . . . . ? C25 Ni4 Ni12 Ni15 45.6(3) . . . . ? Ni3 Ni4 Ni12 Ni15 80.55(11) . . . . ? Ni11 Ni4 Ni12 Ni15 -44.01(8) . . . . ? Ni10 Ni4 Ni12 Ni15 0.53(9) . . . . ? C3 Ni4 Ni12 Ni11 -167.9(8) . . . . ? C4 Ni4 Ni12 Ni11 -40.3(6) . . . . ? C13 Ni4 Ni12 Ni11 -127.2(5) . . . . ? C24 Ni4 Ni12 Ni11 60.7(4) . . . . ? C25 Ni4 Ni12 Ni11 89.6(3) . . . . ? Ni3 Ni4 Ni12 Ni11 124.56(12) . . . . ? Ni10 Ni4 Ni12 Ni11 44.54(8) . . . . ? C3 Ni4 Ni12 Ni5 6.5(8) . . . . ? C4 Ni4 Ni12 Ni5 134.1(6) . . . . ? C13 Ni4 Ni12 Ni5 47.2(6) . . . . ? C24 Ni4 Ni12 Ni5 -124.9(4) . . . . ? C25 Ni4 Ni12 Ni5 -96.1(3) . . . . ? Ni3 Ni4 Ni12 Ni5 -61.07(14) . . . . ? Ni11 Ni4 Ni12 Ni5 174.37(11) . . . . ? Ni10 Ni4 Ni12 Ni5 -141.09(10) . . . . ? C2 Ni1 Ni12 C20 119(3) . . . . ? C1 Ni1 Ni12 C20 -9(2) . . . . ? C13 Ni1 Ni12 C20 76(2) . . . . ? C23 Ni1 Ni12 C20 -112(2) . . . . ? C22 Ni1 Ni12 C20 -141(2) . . . . ? Ni2 Ni1 Ni12 C20 -175(2) . . . . ? Ni5 Ni1 Ni12 C20 -50(2) . . . . ? Ni6 Ni1 Ni12 C20 -97(2) . . . . ? C2 Ni1 Ni12 C20' 102.8(13) . . . . ? C1 Ni1 Ni12 C20' -25.3(11) . . . . ? C13 Ni1 Ni12 C20' 59.0(12) . . . . ? C23 Ni1 Ni12 C20' -128.9(11) . . . . ? C22 Ni1 Ni12 C20' -157.5(11) . . . . ? Ni2 Ni1 Ni12 C20' 168.9(10) . . . . ? Ni5 Ni1 Ni12 C20' -66.7(10) . . . . ? Ni6 Ni1 Ni12 C20' -113.1(10) . . . . ? C2 Ni1 Ni12 C13 43.7(10) . . . . ? C1 Ni1 Ni12 C13 -84.3(8) . . . . ? C23 Ni1 Ni12 C13 172.0(7) . . . . ? C22 Ni1 Ni12 C13 143.4(7) . . . . ? Ni2 Ni1 Ni12 C13 109.8(6) . . . . ? Ni5 Ni1 Ni12 C13 -125.8(6) . . . . ? Ni6 Ni1 Ni12 C13 -172.2(6) . . . . ? C2 Ni1 Ni12 C23 -128.3(9) . . . . ? C1 Ni1 Ni12 C23 103.7(6) . . . . ? C13 Ni1 Ni12 C23 -172.0(7) . . . . ? C22 Ni1 Ni12 C23 -28.6(5) . . . . ? Ni2 Ni1 Ni12 C23 -62.2(4) . . . . ? Ni5 Ni1 Ni12 C23 62.2(4) . . . . ? Ni6 Ni1 Ni12 C23 15.8(4) . . . . ? C2 Ni1 Ni12 C24 -51.3(8) . . . . ? C1 Ni1 Ni12 C24 -179.4(6) . . . . ? C13 Ni1 Ni12 C24 -95.1(7) . . . . ? C23 Ni1 Ni12 C24 76.9(5) . . . . ? C22 Ni1 Ni12 C24 48.3(4) . . . . ? Ni2 Ni1 Ni12 C24 14.8(3) . . . . ? Ni5 Ni1 Ni12 C24 139.2(3) . . . . ? Ni6 Ni1 Ni12 C24 92.8(3) . . . . ? C2 Ni1 Ni12 Ni17 155.3(8) . . . . ? C1 Ni1 Ni12 Ni17 27.2(6) . . . . ? C13 Ni1 Ni12 Ni17 111.5(7) . . . . ? C23 Ni1 Ni12 Ni17 -76.4(5) . . . . ? C22 Ni1 Ni12 Ni17 -105.1(4) . . . . ? Ni2 Ni1 Ni12 Ni17 -138.6(3) . . . . ? Ni5 Ni1 Ni12 Ni17 -14.2(3) . . . . ? Ni6 Ni1 Ni12 Ni17 -60.6(3) . . . . ? C2 Ni1 Ni12 Ni4 -6.9(8) . . . . ? C1 Ni1 Ni12 Ni4 -134.9(5) . . . . ? C13 Ni1 Ni12 Ni4 -50.6(6) . . . . ? C23 Ni1 Ni12 Ni4 121.4(4) . . . . ? C22 Ni1 Ni12 Ni4 92.8(3) . . . . ? Ni2 Ni1 Ni12 Ni4 59.27(10) . . . . ? Ni5 Ni1 Ni12 Ni4 -176.33(8) . . . . ? Ni6 Ni1 Ni12 Ni4 137.28(7) . . . . ? C2 Ni1 Ni12 Ni14 -148.8(8) . . . . ? C1 Ni1 Ni12 Ni14 83.2(5) . . . . ? C13 Ni1 Ni12 Ni14 167.5(6) . . . . ? C23 Ni1 Ni12 Ni14 -20.5(4) . . . . ? C22 Ni1 Ni12 Ni14 -49.1(3) . . . . ? Ni2 Ni1 Ni12 Ni14 -82.67(10) . . . . ? Ni5 Ni1 Ni12 Ni14 41.74(7) . . . . ? Ni6 Ni1 Ni12 Ni14 -4.66(8) . . . . ? C2 Ni1 Ni12 Ni15 -88.9(8) . . . . ? C1 Ni1 Ni12 Ni15 143.0(5) . . . . ? C13 Ni1 Ni12 Ni15 -132.6(6) . . . . ? C23 Ni1 Ni12 Ni15 39.4(4) . . . . ? C22 Ni1 Ni12 Ni15 10.8(3) . . . . ? Ni2 Ni1 Ni12 Ni15 -22.77(17) . . . . ? Ni5 Ni1 Ni12 Ni15 101.63(13) . . . . ? Ni6 Ni1 Ni12 Ni15 55.23(13) . . . . ? C2 Ni1 Ni12 Ni11 -4.9(8) . . . . ? C1 Ni1 Ni12 Ni11 -133.0(5) . . . . ? C13 Ni1 Ni12 Ni11 -48.6(6) . . . . ? C23 Ni1 Ni12 Ni11 123.4(4) . . . . ? C22 Ni1 Ni12 Ni11 94.8(3) . . . . ? Ni2 Ni1 Ni12 Ni11 61.22(14) . . . . ? Ni5 Ni1 Ni12 Ni11 -174.38(11) . . . . ? Ni6 Ni1 Ni12 Ni11 139.23(10) . . . . ? C2 Ni1 Ni12 Ni5 169.5(8) . . . . ? C1 Ni1 Ni12 Ni5 41.4(5) . . . . ? C13 Ni1 Ni12 Ni5 125.8(6) . . . . ? C23 Ni1 Ni12 Ni5 -62.2(4) . . . . ? C22 Ni1 Ni12 Ni5 -90.8(3) . . . . ? Ni2 Ni1 Ni12 Ni5 -124.40(11) . . . . ? Ni6 Ni1 Ni12 Ni5 -46.40(7) . . . . ? C12 Ni11 Ni12 C20 14(2) . . . . ? C4 Ni11 Ni12 C20 -95(2) . . . . ? C24 Ni11 Ni12 C20 156(2) . . . . ? C11 Ni11 Ni12 C20 174(2) . . . . ? Ni4 Ni11 Ni12 C20 -135(2) . . . . ? Ni10 Ni11 Ni12 C20 173(2) . . . . ? Ni15 Ni11 Ni12 C20 99(2) . . . . ? C12 Ni11 Ni12 C20' 25.0(11) . . . . ? C4 Ni11 Ni12 C20' -84.1(10) . . . . ? C24 Ni11 Ni12 C20' 167.3(9) . . . . ? C11 Ni11 Ni12 C20' -174.7(11) . . . . ? Ni4 Ni11 Ni12 C20' -124.3(8) . . . . ? Ni10 Ni11 Ni12 C20' -176.3(8) . . . . ? Ni15 Ni11 Ni12 C20' 109.9(8) . . . . ? C12 Ni11 Ni12 C13 111.6(8) . . . . ? C4 Ni11 Ni12 C13 2.6(7) . . . . ? C24 Ni11 Ni12 C13 -106.0(6) . . . . ? C11 Ni11 Ni12 C13 -88.1(8) . . . . ? Ni4 Ni11 Ni12 C13 -37.6(4) . . . . ? Ni10 Ni11 Ni12 C13 -89.6(4) . . . . ? Ni15 Ni11 Ni12 C13 -163.4(4) . . . . ? C12 Ni11 Ni12 C23 -138.8(8) . . . . ? C4 Ni11 Ni12 C23 112.2(7) . . . . ? C24 Ni11 Ni12 C23 3.6(6) . . . . ? C11 Ni11 Ni12 C23 21.5(8) . . . . ? Ni4 Ni11 Ni12 C23 72.0(5) . . . . ? Ni10 Ni11 Ni12 C23 20.0(5) . . . . ? Ni15 Ni11 Ni12 C23 -53.8(5) . . . . ? C12 Ni11 Ni12 C24 -142.4(8) . . . . ? C4 Ni11 Ni12 C24 108.6(7) . . . . ? C11 Ni11 Ni12 C24 17.9(8) . . . . ? Ni4 Ni11 Ni12 C24 68.4(4) . . . . ? Ni10 Ni11 Ni12 C24 16.4(4) . . . . ? Ni15 Ni11 Ni12 C24 -57.4(4) . . . . ? C12 Ni11 Ni12 Ni17 -25.2(6) . . . . ? C4 Ni11 Ni12 Ni17 -134.2(6) . . . . ? C24 Ni11 Ni12 Ni17 117.2(4) . . . . ? C11 Ni11 Ni12 Ni17 135.1(7) . . . . ? Ni4 Ni11 Ni12 Ni17 -174.37(12) . . . . ? Ni10 Ni11 Ni12 Ni17 133.61(12) . . . . ? Ni15 Ni11 Ni12 Ni17 59.80(10) . . . . ? C12 Ni11 Ni12 Ni4 149.2(6) . . . . ? C4 Ni11 Ni12 Ni4 40.2(6) . . . . ? C24 Ni11 Ni12 Ni4 -68.4(4) . . . . ? C11 Ni11 Ni12 Ni4 -50.5(7) . . . . ? Ni10 Ni11 Ni12 Ni4 -52.02(8) . . . . ? Ni15 Ni11 Ni12 Ni4 -125.82(9) . . . . ? C12 Ni11 Ni12 Ni1 146.9(6) . . . . ? C4 Ni11 Ni12 Ni1 37.9(6) . . . . ? C24 Ni11 Ni12 Ni1 -70.7(4) . . . . ? C11 Ni11 Ni12 Ni1 -52.8(7) . . . . ? Ni4 Ni11 Ni12 Ni1 -2.28(11) . . . . ? Ni10 Ni11 Ni12 Ni1 -54.30(13) . . . . ? Ni15 Ni11 Ni12 Ni1 -128.11(11) . . . . ? C12 Ni11 Ni12 Ni14 -77.8(6) . . . . ? C4 Ni11 Ni12 Ni14 173.1(6) . . . . ? C24 Ni11 Ni12 Ni14 64.5(4) . . . . ? C11 Ni11 Ni12 Ni14 82.5(7) . . . . ? Ni4 Ni11 Ni12 Ni14 132.97(11) . . . . ? Ni10 Ni11 Ni12 Ni14 80.95(11) . . . . ? Ni15 Ni11 Ni12 Ni14 7.14(10) . . . . ? C12 Ni11 Ni12 Ni15 -85.0(6) . . . . ? C4 Ni11 Ni12 Ni15 166.0(6) . . . . ? C24 Ni11 Ni12 Ni15 57.4(4) . . . . ? C11 Ni11 Ni12 Ni15 75.3(7) . . . . ? Ni4 Ni11 Ni12 Ni15 125.82(9) . . . . ? Ni10 Ni11 Ni12 Ni15 73.80(9) . . . . ? C12 Ni11 Ni12 Ni5 19.2(11) . . . . ? C4 Ni11 Ni12 Ni5 -89.8(10) . . . . ? C24 Ni11 Ni12 Ni5 161.6(10) . . . . ? C11 Ni11 Ni12 Ni5 180(100) . . . . ? Ni4 Ni11 Ni12 Ni5 -130.0(9) . . . . ? Ni10 Ni11 Ni12 Ni5 178.0(8) . . . . ? Ni15 Ni11 Ni12 Ni5 104.2(9) . . . . ? C5 Ni5 Ni12 C20 -9(2) . . . . ? C1 Ni5 Ni12 C20 96(2) . . . . ? C23 Ni5 Ni12 C20 -154(2) . . . . ? C6 Ni5 Ni12 C20 -165(2) . . . . ? Ni1 Ni5 Ni12 C20 137(2) . . . . ? Ni6 Ni5 Ni12 C20 -166(2) . . . . ? Ni14 Ni5 Ni12 C20 -95(2) . . . . ? C5 Ni5 Ni12 C20' -20.5(10) . . . . ? C1 Ni5 Ni12 C20' 84.9(9) . . . . ? C23 Ni5 Ni12 C20' -165.7(9) . . . . ? C6 Ni5 Ni12 C20' -175.7(11) . . . . ? Ni1 Ni5 Ni12 C20' 125.4(8) . . . . ? Ni6 Ni5 Ni12 C20' -177.7(8) . . . . ? Ni14 Ni5 Ni12 C20' -106.5(8) . . . . ? C5 Ni5 Ni12 C13 -107.3(7) . . . . ? C1 Ni5 Ni12 C13 -1.9(6) . . . . ? C23 Ni5 Ni12 C13 107.6(6) . . . . ? C6 Ni5 Ni12 C13 97.5(9) . . . . ? Ni1 Ni5 Ni12 C13 38.7(4) . . . . ? Ni6 Ni5 Ni12 C13 95.6(4) . . . . ? Ni14 Ni5 Ni12 C13 166.8(4) . . . . ? C5 Ni5 Ni12 C23 145.2(7) . . . . ? C1 Ni5 Ni12 C23 -109.4(6) . . . . ? C6 Ni5 Ni12 C23 -10.1(9) . . . . ? Ni1 Ni5 Ni12 C23 -68.9(4) . . . . ? Ni6 Ni5 Ni12 C23 -12.0(4) . . . . ? Ni14 Ni5 Ni12 C23 59.2(4) . . . . ? C5 Ni5 Ni12 C24 144.9(7) . . . . ? C1 Ni5 Ni12 C24 -109.7(6) . . . . ? C23 Ni5 Ni12 C24 -0.2(6) . . . . ? C6 Ni5 Ni12 C24 -10.3(9) . . . . ? Ni1 Ni5 Ni12 C24 -69.1(5) . . . . ? Ni6 Ni5 Ni12 C24 -12.2(5) . . . . ? Ni14 Ni5 Ni12 C24 59.0(5) . . . . ? C5 Ni5 Ni12 Ni17 28.5(6) . . . . ? C1 Ni5 Ni12 Ni17 133.9(5) . . . . ? C23 Ni5 Ni12 Ni17 -116.7(4) . . . . ? C6 Ni5 Ni12 Ni17 -126.8(8) . . . . ? Ni1 Ni5 Ni12 Ni17 174.40(12) . . . . ? Ni6 Ni5 Ni12 Ni17 -128.70(11) . . . . ? Ni14 Ni5 Ni12 Ni17 -57.51(11) . . . . ? C5 Ni5 Ni12 Ni4 -141.4(6) . . . . ? C1 Ni5 Ni12 Ni4 -36.0(5) . . . . ? C23 Ni5 Ni12 Ni4 73.4(4) . . . . ? C6 Ni5 Ni12 Ni4 63.4(8) . . . . ? Ni1 Ni5 Ni12 Ni4 4.51(10) . . . . ? Ni6 Ni5 Ni12 Ni4 61.41(12) . . . . ? Ni14 Ni5 Ni12 Ni4 132.60(11) . . . . ? C5 Ni5 Ni12 Ni1 -145.9(6) . . . . ? C1 Ni5 Ni12 Ni1 -40.5(4) . . . . ? C23 Ni5 Ni12 Ni1 68.9(4) . . . . ? C6 Ni5 Ni12 Ni1 58.8(8) . . . . ? Ni6 Ni5 Ni12 Ni1 56.90(8) . . . . ? Ni14 Ni5 Ni12 Ni1 128.09(9) . . . . ? C5 Ni5 Ni12 Ni14 86.0(6) . . . . ? C1 Ni5 Ni12 Ni14 -168.6(4) . . . . ? C23 Ni5 Ni12 Ni14 -59.2(4) . . . . ? C6 Ni5 Ni12 Ni14 -69.2(8) . . . . ? Ni1 Ni5 Ni12 Ni14 -128.09(9) . . . . ? Ni6 Ni5 Ni12 Ni14 -71.20(8) . . . . ? C5 Ni5 Ni12 Ni15 85.8(6) . . . . ? C1 Ni5 Ni12 Ni15 -168.8(4) . . . . ? C23 Ni5 Ni12 Ni15 -59.3(4) . . . . ? C6 Ni5 Ni12 Ni15 -69.4(8) . . . . ? Ni1 Ni5 Ni12 Ni15 -128.22(10) . . . . ? Ni6 Ni5 Ni12 Ni15 -71.33(11) . . . . ? Ni14 Ni5 Ni12 Ni15 -0.13(9) . . . . ? C5 Ni5 Ni12 Ni11 -14.8(11) . . . . ? C1 Ni5 Ni12 Ni11 90.6(10) . . . . ? C23 Ni5 Ni12 Ni11 -160.0(10) . . . . ? C6 Ni5 Ni12 Ni11 -170.0(11) . . . . ? Ni1 Ni5 Ni12 Ni11 131.1(9) . . . . ? Ni6 Ni5 Ni12 Ni11 -172.0(8) . . . . ? Ni14 Ni5 Ni12 Ni11 -100.8(9) . . . . ? C8 Ni7 Ni13 C14 -2.7(10) . . . . ? C7 Ni7 Ni13 C14 106.8(8) . . . . ? C22 Ni7 Ni13 C14 -154.7(7) . . . . ? Ni6 Ni7 Ni13 C14 143.5(6) . . . . ? Ni8 Ni7 Ni13 C14 -95.8(6) . . . . ? Ni2 Ni7 Ni13 C14 -144.2(6) . . . . ? C8 Ni7 Ni13 C15 -85.2(13) . . . . ? C7 Ni7 Ni13 C15 24.3(11) . . . . ? C22 Ni7 Ni13 C15 122.8(11) . . . . ? Ni6 Ni7 Ni13 C15 61.0(10) . . . . ? Ni8 Ni7 Ni13 C15 -178.2(10) . . . . ? Ni2 Ni7 Ni13 C15 133.3(10) . . . . ? C8 Ni7 Ni13 C23 173.9(8) . . . . ? C7 Ni7 Ni13 C23 -76.6(6) . . . . ? C22 Ni7 Ni13 C23 21.9(5) . . . . ? Ni6 Ni7 Ni13 C23 -39.9(3) . . . . ? Ni8 Ni7 Ni13 C23 80.9(3) . . . . ? Ni2 Ni7 Ni13 C23 32.4(3) . . . . ? C8 Ni7 Ni13 C22 152.0(9) . . . . ? C7 Ni7 Ni13 C22 -98.5(7) . . . . ? Ni6 Ni7 Ni13 C22 -61.8(4) . . . . ? Ni8 Ni7 Ni13 C22 58.9(4) . . . . ? Ni2 Ni7 Ni13 C22 10.5(4) . . . . ? C8 Ni7 Ni13 Ni14 -159.7(8) . . . . ? C7 Ni7 Ni13 Ni14 -50.2(5) . . . . ? C22 Ni7 Ni13 Ni14 48.3(4) . . . . ? Ni6 Ni7 Ni13 Ni14 -13.55(12) . . . . ? Ni8 Ni7 Ni13 Ni14 107.24(13) . . . . ? Ni2 Ni7 Ni13 Ni14 58.76(14) . . . . ? C8 Ni7 Ni13 Ni8 93.1(8) . . . . ? C7 Ni7 Ni13 Ni8 -157.5(5) . . . . ? C22 Ni7 Ni13 Ni8 -58.9(4) . . . . ? Ni6 Ni7 Ni13 Ni8 -120.78(8) . . . . ? Ni2 Ni7 Ni13 Ni8 -48.47(7) . . . . ? C8 Ni7 Ni13 Ni6 -146.2(8) . . . . ? C7 Ni7 Ni13 Ni6 -36.7(5) . . . . ? C22 Ni7 Ni13 Ni6 61.8(4) . . . . ? Ni8 Ni7 Ni13 Ni6 120.78(8) . . . . ? Ni2 Ni7 Ni13 Ni6 72.31(8) . . . . ? C8 Ni7 Ni13 Ni16 83.1(8) . . . . ? C7 Ni7 Ni13 Ni16 -167.4(5) . . . . ? C22 Ni7 Ni13 Ni16 -68.9(4) . . . . ? Ni6 Ni7 Ni13 Ni16 -130.75(9) . . . . ? Ni8 Ni7 Ni13 Ni16 -9.96(8) . . . . ? Ni2 Ni7 Ni13 Ni16 -58.43(10) . . . . ? C28' Ni8 Ni13 C14 -4(2) . . . . ? C28 Ni8 Ni13 C14 18.6(11) . . . . ? C25 Ni8 Ni13 C14 -136.1(7) . . . . ? C22 Ni8 Ni13 C14 138.3(8) . . . . ? Ni18 Ni8 Ni13 C14 76.1(7) . . . . ? Ni7 Ni8 Ni13 C14 74.1(6) . . . . ? Ni2 Ni8 Ni13 C14 123.3(6) . . . . ? Ni9 Ni8 Ni13 C14 -88.7(6) . . . . ? Ni3 Ni8 Ni13 C14 -169.0(6) . . . . ? Ni16 Ni8 Ni13 C14 -95.0(6) . . . . ? C28' Ni8 Ni13 C15 100(2) . . . . ? C28 Ni8 Ni13 C15 122.2(16) . . . . ? C25 Ni8 Ni13 C15 -32.4(13) . . . . ? C22 Ni8 Ni13 C15 -118.1(14) . . . . ? Ni18 Ni8 Ni13 C15 179.7(13) . . . . ? Ni7 Ni8 Ni13 C15 177.8(13) . . . . ? Ni2 Ni8 Ni13 C15 -133.1(13) . . . . ? Ni9 Ni8 Ni13 C15 15.0(13) . . . . ? Ni3 Ni8 Ni13 C15 -65.4(13) . . . . ? Ni16 Ni8 Ni13 C15 8.6(13) . . . . ? C28' Ni8 Ni13 C23 -167.5(19) . . . . ? C28 Ni8 Ni13 C23 -145.3(10) . . . . ? C25 Ni8 Ni13 C23 60.1(5) . . . . ? C22 Ni8 Ni13 C23 -25.6(6) . . . . ? Ni18 Ni8 Ni13 C23 -87.8(5) . . . . ? Ni7 Ni8 Ni13 C23 -89.7(3) . . . . ? Ni2 Ni8 Ni13 C23 -40.6(3) . . . . ? Ni9 Ni8 Ni13 C23 107.5(4) . . . . ? Ni3 Ni8 Ni13 C23 27.1(4) . . . . ? Ni16 Ni8 Ni13 C23 101.1(3) . . . . ? C28' Ni8 Ni13 C22 -141.9(19) . . . . ? C28 Ni8 Ni13 C22 -119.7(10) . . . . ? C25 Ni8 Ni13 C22 85.7(6) . . . . ? Ni18 Ni8 Ni13 C22 -62.2(6) . . . . ? Ni7 Ni8 Ni13 C22 -64.1(5) . . . . ? Ni2 Ni8 Ni13 C22 -15.0(5) . . . . ? Ni9 Ni8 Ni13 C22 133.1(5) . . . . ? Ni3 Ni8 Ni13 C22 52.7(5) . . . . ? Ni16 Ni8 Ni13 C22 126.7(5) . . . . ? C28' Ni8 Ni13 Ni14 164.2(19) . . . . ? C28 Ni8 Ni13 Ni14 -173.6(9) . . . . ? C25 Ni8 Ni13 Ni14 31.8(4) . . . . ? C22 Ni8 Ni13 Ni14 -53.9(5) . . . . ? Ni18 Ni8 Ni13 Ni14 -116.1(4) . . . . ? Ni7 Ni8 Ni13 Ni14 -117.98(12) . . . . ? Ni2 Ni8 Ni13 Ni14 -68.84(12) . . . . ? Ni9 Ni8 Ni13 Ni14 79.22(13) . . . . ? Ni3 Ni8 Ni13 Ni14 -1.16(19) . . . . ? Ni16 Ni8 Ni13 Ni14 72.88(11) . . . . ? C28' Ni8 Ni13 Ni7 -77.8(19) . . . . ? C28 Ni8 Ni13 Ni7 -55.6(9) . . . . ? C25 Ni8 Ni13 Ni7 149.8(4) . . . . ? C22 Ni8 Ni13 Ni7 64.1(5) . . . . ? Ni18 Ni8 Ni13 Ni7 1.9(4) . . . . ? Ni2 Ni8 Ni13 Ni7 49.14(8) . . . . ? Ni9 Ni8 Ni13 Ni7 -162.81(11) . . . . ? Ni3 Ni8 Ni13 Ni7 116.82(14) . . . . ? Ni16 Ni8 Ni13 Ni7 -169.15(9) . . . . ? C28' Ni8 Ni13 Ni6 -120.9(19) . . . . ? C28 Ni8 Ni13 Ni6 -98.7(9) . . . . ? C25 Ni8 Ni13 Ni6 106.7(3) . . . . ? C22 Ni8 Ni13 Ni6 21.0(5) . . . . ? Ni18 Ni8 Ni13 Ni6 -41.2(4) . . . . ? Ni7 Ni8 Ni13 Ni6 -43.09(7) . . . . ? Ni2 Ni8 Ni13 Ni6 6.05(8) . . . . ? Ni9 Ni8 Ni13 Ni6 154.11(9) . . . . ? Ni3 Ni8 Ni13 Ni6 73.73(14) . . . . ? Ni16 Ni8 Ni13 Ni6 147.77(8) . . . . ? C28' Ni8 Ni13 Ni16 91.4(19) . . . . ? C28 Ni8 Ni13 Ni16 113.6(9) . . . . ? C25 Ni8 Ni13 Ni16 -41.1(3) . . . . ? C22 Ni8 Ni13 Ni16 -126.7(5) . . . . ? Ni18 Ni8 Ni13 Ni16 171.1(4) . . . . ? Ni7 Ni8 Ni13 Ni16 169.15(9) . . . . ? Ni2 Ni8 Ni13 Ni16 -141.72(8) . . . . ? Ni9 Ni8 Ni13 Ni16 6.34(9) . . . . ? Ni3 Ni8 Ni13 Ni16 -74.04(13) . . . . ? C6 Ni6 Ni13 C14 112.3(10) . . . . ? C7 Ni6 Ni13 C14 -0.5(9) . . . . ? C22 Ni6 Ni13 C14 -107.2(8) . . . . ? C23 Ni6 Ni13 C14 -160.8(8) . . . . ? Ni7 Ni6 Ni13 C14 -40.2(6) . . . . ? Ni5 Ni6 Ni13 C14 167.9(6) . . . . ? Ni1 Ni6 Ni13 C14 -137.1(6) . . . . ? C6 Ni6 Ni13 C15 1.9(10) . . . . ? C7 Ni6 Ni13 C15 -110.9(8) . . . . ? C22 Ni6 Ni13 C15 142.4(7) . . . . ? C23 Ni6 Ni13 C15 88.8(7) . . . . ? Ni7 Ni6 Ni13 C15 -150.6(6) . . . . ? Ni5 Ni6 Ni13 C15 57.5(6) . . . . ? Ni1 Ni6 Ni13 C15 112.5(6) . . . . ? C6 Ni6 Ni13 C23 -86.9(9) . . . . ? C7 Ni6 Ni13 C23 160.3(8) . . . . ? C22 Ni6 Ni13 C23 53.6(6) . . . . ? Ni7 Ni6 Ni13 C23 120.5(4) . . . . ? Ni5 Ni6 Ni13 C23 -31.4(4) . . . . ? Ni1 Ni6 Ni13 C23 23.7(4) . . . . ? C6 Ni6 Ni13 C22 -140.5(9) . . . . ? C7 Ni6 Ni13 C22 106.7(7) . . . . ? C23 Ni6 Ni13 C22 -53.6(6) . . . . ? Ni7 Ni6 Ni13 C22 66.9(5) . . . . ? Ni5 Ni6 Ni13 C22 -85.0(5) . . . . ? Ni1 Ni6 Ni13 C22 -30.0(4) . . . . ? C6 Ni6 Ni13 Ni14 -38.3(8) . . . . ? C7 Ni6 Ni13 Ni14 -151.1(6) . . . . ? C22 Ni6 Ni13 Ni14 102.2(5) . . . . ? C23 Ni6 Ni13 Ni14 48.6(4) . . . . ? Ni7 Ni6 Ni13 Ni14 169.17(9) . . . . ? Ni5 Ni6 Ni13 Ni14 17.27(8) . . . . ? Ni1 Ni6 Ni13 Ni14 72.29(7) . . . . ? C6 Ni6 Ni13 Ni7 152.6(8) . . . . ? C7 Ni6 Ni13 Ni7 39.8(6) . . . . ? C22 Ni6 Ni13 Ni7 -66.9(5) . . . . ? C23 Ni6 Ni13 Ni7 -120.5(4) . . . . ? Ni5 Ni6 Ni13 Ni7 -151.90(10) . . . . ? Ni1 Ni6 Ni13 Ni7 -96.89(8) . . . . ? C6 Ni6 Ni13 Ni8 -161.4(8) . . . . ? C7 Ni6 Ni13 Ni8 85.8(6) . . . . ? C22 Ni6 Ni13 Ni8 -20.9(4) . . . . ? C23 Ni6 Ni13 Ni8 -74.5(4) . . . . ? Ni7 Ni6 Ni13 Ni8 46.03(7) . . . . ? Ni5 Ni6 Ni13 Ni8 -105.87(8) . . . . ? Ni1 Ni6 Ni13 Ni8 -50.86(7) . . . . ? C6 Ni6 Ni13 Ni16 -121.2(8) . . . . ? C7 Ni6 Ni13 Ni16 126.0(6) . . . . ? C22 Ni6 Ni13 Ni16 19.3(5) . . . . ? C23 Ni6 Ni13 Ni16 -34.3(5) . . . . ? Ni7 Ni6 Ni13 Ni16 86.22(13) . . . . ? Ni5 Ni6 Ni13 Ni16 -65.68(13) . . . . ? Ni1 Ni6 Ni13 Ni16 -10.67(14) . . . . ? C14 Ni13 Ni14 C18 -2.9(16) . . . . ? C15 Ni13 Ni14 C18 -8.1(12) . . . . ? C23 Ni13 Ni14 C18 164.5(11) . . . . ? C22 Ni13 Ni14 C18 165.0(10) . . . . ? Ni7 Ni13 Ni14 C18 130.0(10) . . . . ? Ni8 Ni13 Ni14 C18 -158.8(10) . . . . ? Ni6 Ni13 Ni14 C18 118.9(10) . . . . ? Ni16 Ni13 Ni14 C18 -104.9(10) . . . . ? C14 Ni13 Ni14 C15 5.2(14) . . . . ? C23 Ni13 Ni14 C15 172.6(8) . . . . ? C22 Ni13 Ni14 C15 173.1(7) . . . . ? Ni7 Ni13 Ni14 C15 138.0(7) . . . . ? Ni8 Ni13 Ni14 C15 -150.7(7) . . . . ? Ni6 Ni13 Ni14 C15 127.0(7) . . . . ? Ni16 Ni13 Ni14 C15 -96.9(7) . . . . ? C14 Ni13 Ni14 C23 -167.4(13) . . . . ? C15 Ni13 Ni14 C23 -172.6(8) . . . . ? C22 Ni13 Ni14 C23 0.5(5) . . . . ? Ni7 Ni13 Ni14 C23 -34.5(4) . . . . ? Ni8 Ni13 Ni14 C23 36.7(4) . . . . ? Ni6 Ni13 Ni14 C23 -45.6(4) . . . . ? Ni16 Ni13 Ni14 C23 90.6(4) . . . . ? C14 Ni13 Ni14 Ni5 -138.4(12) . . . . ? C15 Ni13 Ni14 Ni5 -143.6(7) . . . . ? C23 Ni13 Ni14 Ni5 29.0(4) . . . . ? C22 Ni13 Ni14 Ni5 29.4(3) . . . . ? Ni7 Ni13 Ni14 Ni5 -5.56(15) . . . . ? Ni8 Ni13 Ni14 Ni5 65.68(12) . . . . ? Ni6 Ni13 Ni14 Ni5 -16.58(8) . . . . ? Ni16 Ni13 Ni14 Ni5 119.54(8) . . . . ? C14 Ni13 Ni14 Ni12 156.5(12) . . . . ? C15 Ni13 Ni14 Ni12 151.3(7) . . . . ? C23 Ni13 Ni14 Ni12 -36.1(4) . . . . ? C22 Ni13 Ni14 Ni12 -35.6(3) . . . . ? Ni7 Ni13 Ni14 Ni12 -70.62(13) . . . . ? Ni8 Ni13 Ni14 Ni12 0.62(12) . . . . ? Ni6 Ni13 Ni14 Ni12 -81.64(7) . . . . ? Ni16 Ni13 Ni14 Ni12 54.48(8) . . . . ? C14 Ni13 Ni14 Ni15 100.3(12) . . . . ? C15 Ni13 Ni14 Ni15 95.1(7) . . . . ? C23 Ni13 Ni14 Ni15 -92.3(4) . . . . ? C22 Ni13 Ni14 Ni15 -91.8(3) . . . . ? Ni7 Ni13 Ni14 Ni15 -126.86(12) . . . . ? Ni8 Ni13 Ni14 Ni15 -55.62(10) . . . . ? Ni6 Ni13 Ni14 Ni15 -137.88(7) . . . . ? Ni16 Ni13 Ni14 Ni15 -1.76(7) . . . . ? C14 Ni13 Ni14 Ni17 114.4(12) . . . . ? C15 Ni13 Ni14 Ni17 109.2(7) . . . . ? C23 Ni13 Ni14 Ni17 -78.2(4) . . . . ? C22 Ni13 Ni14 Ni17 -77.8(3) . . . . ? Ni7 Ni13 Ni14 Ni17 -112.78(15) . . . . ? Ni8 Ni13 Ni14 Ni17 -41.54(17) . . . . ? Ni6 Ni13 Ni14 Ni17 -123.80(13) . . . . ? Ni16 Ni13 Ni14 Ni17 12.32(14) . . . . ? C5 Ni5 Ni14 C18 -2.3(7) . . . . ? C1 Ni5 Ni14 C18 131.5(10) . . . . ? C23 Ni5 Ni14 C18 171.1(7) . . . . ? C6 Ni5 Ni14 C18 -103.5(7) . . . . ? Ni1 Ni5 Ni14 C18 152.9(5) . . . . ? Ni6 Ni5 Ni14 C18 -139.6(5) . . . . ? Ni12 Ni5 Ni14 C18 110.1(5) . . . . ? C5 Ni5 Ni14 C15 112.7(9) . . . . ? C1 Ni5 Ni14 C15 -113.5(12) . . . . ? C23 Ni5 Ni14 C15 -73.9(9) . . . . ? C6 Ni5 Ni14 C15 11.5(9) . . . . ? Ni1 Ni5 Ni14 C15 -92.0(8) . . . . ? Ni6 Ni5 Ni14 C15 -24.5(8) . . . . ? Ni12 Ni5 Ni14 C15 -134.9(8) . . . . ? C5 Ni5 Ni14 C23 -173.4(7) . . . . ? C1 Ni5 Ni14 C23 -39.6(10) . . . . ? C6 Ni5 Ni14 C23 85.4(6) . . . . ? Ni1 Ni5 Ni14 C23 -18.2(4) . . . . ? Ni6 Ni5 Ni14 C23 49.3(4) . . . . ? Ni12 Ni5 Ni14 C23 -61.0(4) . . . . ? C5 Ni5 Ni14 Ni13 156.3(5) . . . . ? C1 Ni5 Ni14 Ni13 -69.9(9) . . . . ? C23 Ni5 Ni14 Ni13 -30.3(4) . . . . ? C6 Ni5 Ni14 Ni13 55.1(4) . . . . ? Ni1 Ni5 Ni14 Ni13 -48.48(10) . . . . ? Ni6 Ni5 Ni14 Ni13 19.05(9) . . . . ? Ni12 Ni5 Ni14 Ni13 -91.33(9) . . . . ? C5 Ni5 Ni14 Ni12 -112.4(5) . . . . ? C1 Ni5 Ni14 Ni12 21.4(9) . . . . ? C23 Ni5 Ni14 Ni12 61.0(4) . . . . ? C6 Ni5 Ni14 Ni12 146.4(4) . . . . ? Ni1 Ni5 Ni14 Ni12 42.85(7) . . . . ? Ni6 Ni5 Ni14 Ni12 110.37(7) . . . . ? C5 Ni5 Ni14 Ni15 -112.3(5) . . . . ? C1 Ni5 Ni14 Ni15 21.5(9) . . . . ? C23 Ni5 Ni14 Ni15 61.1(4) . . . . ? C6 Ni5 Ni14 Ni15 146.5(4) . . . . ? Ni1 Ni5 Ni14 Ni15 42.97(12) . . . . ? Ni6 Ni5 Ni14 Ni15 110.49(10) . . . . ? Ni12 Ni5 Ni14 Ni15 0.12(8) . . . . ? C5 Ni5 Ni14 Ni17 -70.3(5) . . . . ? C1 Ni5 Ni14 Ni17 63.5(9) . . . . ? C23 Ni5 Ni14 Ni17 103.1(4) . . . . ? C6 Ni5 Ni14 Ni17 -171.5(4) . . . . ? Ni1 Ni5 Ni14 Ni17 84.96(10) . . . . ? Ni6 Ni5 Ni14 Ni17 152.48(9) . . . . ? Ni12 Ni5 Ni14 Ni17 42.11(8) . . . . ? C20 Ni12 Ni14 C18 -12(3) . . . . ? C20' Ni12 Ni14 C18 -10.4(12) . . . . ? C13 Ni12 Ni14 C18 -113.8(9) . . . . ? C23 Ni12 Ni14 C18 -152.9(7) . . . . ? C24 Ni12 Ni14 C18 125.3(6) . . . . ? Ni17 Ni12 Ni14 C18 29.8(5) . . . . ? Ni4 Ni12 Ni14 C18 157.2(5) . . . . ? Ni1 Ni12 Ni14 C18 -130.5(5) . . . . ? Ni15 Ni12 Ni14 C18 89.3(5) . . . . ? Ni11 Ni12 Ni14 C18 82.6(5) . . . . ? Ni5 Ni12 Ni14 C18 -90.6(5) . . . . ? C20 Ni12 Ni14 C15 -147(3) . . . . ? C20' Ni12 Ni14 C15 -145.1(13) . . . . ? C13 Ni12 Ni14 C15 111.4(11) . . . . ? C23 Ni12 Ni14 C15 72.4(9) . . . . ? C24 Ni12 Ni14 C15 -9.5(9) . . . . ? Ni17 Ni12 Ni14 C15 -105.0(8) . . . . ? Ni4 Ni12 Ni14 C15 22.5(8) . . . . ? Ni1 Ni12 Ni14 C15 94.7(8) . . . . ? Ni15 Ni12 Ni14 C15 -45.5(8) . . . . ? Ni11 Ni12 Ni14 C15 -52.2(8) . . . . ? Ni5 Ni12 Ni14 C15 134.6(8) . . . . ? C20 Ni12 Ni14 C23 141(3) . . . . ? C20' Ni12 Ni14 C23 142.5(11) . . . . ? C13 Ni12 Ni14 C23 39.1(9) . . . . ? C24 Ni12 Ni14 C23 -81.8(5) . . . . ? Ni17 Ni12 Ni14 C23 -177.3(4) . . . . ? Ni4 Ni12 Ni14 C23 -49.9(4) . . . . ? Ni1 Ni12 Ni14 C23 22.4(4) . . . . ? Ni15 Ni12 Ni14 C23 -117.8(4) . . . . ? Ni11 Ni12 Ni14 C23 -124.5(4) . . . . ? Ni5 Ni12 Ni14 C23 62.3(4) . . . . ? C20 Ni12 Ni14 Ni13 179(2) . . . . ? C20' Ni12 Ni14 Ni13 -179.2(10) . . . . ? C13 Ni12 Ni14 Ni13 77.4(8) . . . . ? C23 Ni12 Ni14 Ni13 38.3(4) . . . . ? C24 Ni12 Ni14 Ni13 -43.5(3) . . . . ? Ni17 Ni12 Ni14 Ni13 -138.98(12) . . . . ? Ni4 Ni12 Ni14 Ni13 -11.55(16) . . . . ? Ni1 Ni12 Ni14 Ni13 60.71(9) . . . . ? Ni15 Ni12 Ni14 Ni13 -79.49(8) . . . . ? Ni11 Ni12 Ni14 Ni13 -86.17(11) . . . . ? Ni5 Ni12 Ni14 Ni13 100.63(8) . . . . ? C20 Ni12 Ni14 Ni5 78(2) . . . . ? C20' Ni12 Ni14 Ni5 80.2(10) . . . . ? C13 Ni12 Ni14 Ni5 -23.2(8) . . . . ? C23 Ni12 Ni14 Ni5 -62.3(4) . . . . ? C24 Ni12 Ni14 Ni5 -144.1(3) . . . . ? Ni17 Ni12 Ni14 Ni5 120.39(11) . . . . ? Ni4 Ni12 Ni14 Ni5 -112.18(14) . . . . ? Ni1 Ni12 Ni14 Ni5 -39.92(7) . . . . ? Ni15 Ni12 Ni14 Ni5 179.88(8) . . . . ? Ni11 Ni12 Ni14 Ni5 173.20(10) . . . . ? C20 Ni12 Ni14 Ni15 -101(2) . . . . ? C20' Ni12 Ni14 Ni15 -99.7(10) . . . . ? C13 Ni12 Ni14 Ni15 156.9(8) . . . . ? C23 Ni12 Ni14 Ni15 117.8(4) . . . . ? C24 Ni12 Ni14 Ni15 36.0(3) . . . . ? Ni17 Ni12 Ni14 Ni15 -59.49(10) . . . . ? Ni4 Ni12 Ni14 Ni15 67.94(13) . . . . ? Ni1 Ni12 Ni14 Ni15 140.20(8) . . . . ? Ni11 Ni12 Ni14 Ni15 -6.68(9) . . . . ? Ni5 Ni12 Ni14 Ni15 -179.88(8) . . . . ? C20 Ni12 Ni14 Ni17 -42(2) . . . . ? C20' Ni12 Ni14 Ni17 -40.2(10) . . . . ? C13 Ni12 Ni14 Ni17 -143.6(8) . . . . ? C23 Ni12 Ni14 Ni17 177.3(4) . . . . ? C24 Ni12 Ni14 Ni17 95.5(3) . . . . ? Ni4 Ni12 Ni14 Ni17 127.43(17) . . . . ? Ni1 Ni12 Ni14 Ni17 -160.32(12) . . . . ? Ni15 Ni12 Ni14 Ni17 59.49(10) . . . . ? Ni11 Ni12 Ni14 Ni17 52.81(12) . . . . ? Ni5 Ni12 Ni14 Ni17 -120.39(11) . . . . ? C12 Ni11 Ni15 C19 6(4) . . . . ? C4 Ni11 Ni15 C19 -136(4) . . . . ? C24 Ni11 Ni15 C19 -176(4) . . . . ? C11 Ni11 Ni15 C19 105(4) . . . . ? Ni4 Ni11 Ni15 C19 -154(4) . . . . ? Ni10 Ni11 Ni15 C19 140(4) . . . . ? Ni12 Ni11 Ni15 C19 -109(4) . . . . ? C12 Ni11 Ni15 C19' 8.2(16) . . . . ? C4 Ni11 Ni15 C19' -133.6(18) . . . . ? C24 Ni11 Ni15 C19' -173.4(15) . . . . ? C11 Ni11 Ni15 C19' 107.6(15) . . . . ? Ni4 Ni11 Ni15 C19' -151.6(15) . . . . ? Ni10 Ni11 Ni15 C19' 142.0(15) . . . . ? Ni12 Ni11 Ni15 C19' -106.9(15) . . . . ? C12 Ni11 Ni15 C16 -103.7(9) . . . . ? C4 Ni11 Ni15 C16 114.6(13) . . . . ? C24 Ni11 Ni15 C16 74.7(8) . . . . ? C11 Ni11 Ni15 C16 -4.3(8) . . . . ? Ni4 Ni11 Ni15 C16 96.5(7) . . . . ? Ni10 Ni11 Ni15 C16 30.2(7) . . . . ? Ni12 Ni11 Ni15 C16 141.3(7) . . . . ? C12 Ni11 Ni15 C24 -178.4(8) . . . . ? C4 Ni11 Ni15 C24 39.8(11) . . . . ? C11 Ni11 Ni15 C24 -79.0(6) . . . . ? Ni4 Ni11 Ni15 C24 21.8(5) . . . . ? Ni10 Ni11 Ni15 C24 -44.5(5) . . . . ? Ni12 Ni11 Ni15 C24 66.6(5) . . . . ? C12 Ni11 Ni15 Ni17 54.2(6) . . . . ? C4 Ni11 Ni15 Ni17 -87.6(11) . . . . ? C24 Ni11 Ni15 Ni17 -127.4(5) . . . . ? C11 Ni11 Ni15 Ni17 153.6(4) . . . . ? Ni4 Ni11 Ni15 Ni17 -105.58(12) . . . . ? Ni10 Ni11 Ni15 Ni17 -171.96(11) . . . . ? Ni12 Ni11 Ni15 Ni17 -60.86(10) . . . . ? C12 Ni11 Ni15 Ni16 -145.8(6) . . . . ? C4 Ni11 Ni15 Ni16 72.4(11) . . . . ? C24 Ni11 Ni15 Ni16 32.5(5) . . . . ? C11 Ni11 Ni15 Ni16 -46.4(4) . . . . ? Ni4 Ni11 Ni15 Ni16 54.38(11) . . . . ? Ni10 Ni11 Ni15 Ni16 -12.00(9) . . . . ? Ni12 Ni11 Ni15 Ni16 99.10(9) . . . . ? C12 Ni11 Ni15 Ni12 115.1(6) . . . . ? C4 Ni11 Ni15 Ni12 -26.7(11) . . . . ? C24 Ni11 Ni15 Ni12 -66.6(5) . . . . ? C11 Ni11 Ni15 Ni12 -145.5(4) . . . . ? Ni4 Ni11 Ni15 Ni12 -44.72(8) . . . . ? Ni10 Ni11 Ni15 Ni12 -111.10(8) . . . . ? C12 Ni11 Ni15 Ni14 108.8(6) . . . . ? C4 Ni11 Ni15 Ni14 -33.0(11) . . . . ? C24 Ni11 Ni15 Ni14 -72.8(5) . . . . ? C11 Ni11 Ni15 Ni14 -151.8(4) . . . . ? Ni4 Ni11 Ni15 Ni14 -51.00(12) . . . . ? Ni10 Ni11 Ni15 Ni14 -117.38(10) . . . . ? Ni12 Ni11 Ni15 Ni14 -6.28(8) . . . . ? C20 Ni12 Ni15 C19 8(4) . . . . ? C20' Ni12 Ni15 C19 23(4) . . . . ? C13 Ni12 Ni15 C19 128(4) . . . . ? C23 Ni12 Ni15 C19 -116(4) . . . . ? C24 Ni12 Ni15 C19 158(4) . . . . ? Ni17 Ni12 Ni15 C19 8(3) . . . . ? Ni4 Ni12 Ni15 C19 140(3) . . . . ? Ni1 Ni12 Ni15 C19 -147(3) . . . . ? Ni14 Ni12 Ni15 C19 -76(3) . . . . ? Ni11 Ni12 Ni15 C19 98(3) . . . . ? Ni5 Ni12 Ni15 C19 -76(3) . . . . ? C20 Ni12 Ni15 C19' 1(3) . . . . ? C20' Ni12 Ni15 C19' 15.1(17) . . . . ? C13 Ni12 Ni15 C19' 120.3(16) . . . . ? C23 Ni12 Ni15 C19' -123.8(14) . . . . ? C24 Ni12 Ni15 C19' 150.7(15) . . . . ? Ni17 Ni12 Ni15 C19' 0.8(14) . . . . ? Ni4 Ni12 Ni15 C19' 132.2(14) . . . . ? Ni1 Ni12 Ni15 C19' -154.2(14) . . . . ? Ni14 Ni12 Ni15 C19' -83.3(14) . . . . ? Ni11 Ni12 Ni15 C19' 90.1(14) . . . . ? Ni5 Ni12 Ni15 C19' -83.2(14) . . . . ? C20 Ni12 Ni15 C16 140(2) . . . . ? C20' Ni12 Ni15 C16 154.5(13) . . . . ? C13 Ni12 Ni15 C16 -100.4(11) . . . . ? C23 Ni12 Ni15 C16 15.6(9) . . . . ? C24 Ni12 Ni15 C16 -70.0(9) . . . . ? Ni17 Ni12 Ni15 C16 140.2(8) . . . . ? Ni4 Ni12 Ni15 C16 -88.4(8) . . . . ? Ni1 Ni12 Ni15 C16 -14.9(9) . . . . ? Ni14 Ni12 Ni15 C16 56.0(8) . . . . ? Ni11 Ni12 Ni15 C16 -130.5(8) . . . . ? Ni5 Ni12 Ni15 C16 56.1(8) . . . . ? C20 Ni12 Ni15 C24 -150(2) . . . . ? C20' Ni12 Ni15 C24 -135.5(11) . . . . ? C13 Ni12 Ni15 C24 -30.4(9) . . . . ? C23 Ni12 Ni15 C24 85.5(5) . . . . ? Ni17 Ni12 Ni15 C24 -149.9(5) . . . . ? Ni4 Ni12 Ni15 C24 -18.5(4) . . . . ? Ni1 Ni12 Ni15 C24 55.1(4) . . . . ? Ni14 Ni12 Ni15 C24 126.0(4) . . . . ? Ni11 Ni12 Ni15 C24 -60.5(4) . . . . ? Ni5 Ni12 Ni15 C24 126.1(4) . . . . ? C20 Ni12 Ni15 Ni17 0(2) . . . . ? C20' Ni12 Ni15 Ni17 14.3(10) . . . . ? C13 Ni12 Ni15 Ni17 119.5(8) . . . . ? C23 Ni12 Ni15 Ni17 -124.6(3) . . . . ? C24 Ni12 Ni15 Ni17 149.9(5) . . . . ? Ni4 Ni12 Ni15 Ni17 131.41(14) . . . . ? Ni1 Ni12 Ni15 Ni17 -155.01(17) . . . . ? Ni14 Ni12 Ni15 Ni17 -84.13(13) . . . . ? Ni11 Ni12 Ni15 Ni17 89.34(13) . . . . ? Ni5 Ni12 Ni15 Ni17 -84.00(14) . . . . ? C20 Ni12 Ni15 Ni16 177(2) . . . . ? C20' Ni12 Ni15 Ni16 -169.0(10) . . . . ? C13 Ni12 Ni15 Ni16 -63.8(8) . . . . ? C23 Ni12 Ni15 Ni16 52.1(3) . . . . ? C24 Ni12 Ni15 Ni16 -33.5(4) . . . . ? Ni17 Ni12 Ni15 Ni16 176.68(15) . . . . ? Ni4 Ni12 Ni15 Ni16 -51.92(9) . . . . ? Ni1 Ni12 Ni15 Ni16 21.67(15) . . . . ? Ni14 Ni12 Ni15 Ni16 92.55(9) . . . . ? Ni11 Ni12 Ni15 Ni16 -93.98(9) . . . . ? Ni5 Ni12 Ni15 Ni16 92.67(10) . . . . ? C20 Ni12 Ni15 Ni11 -89(2) . . . . ? C20' Ni12 Ni15 Ni11 -75.0(10) . . . . ? C13 Ni12 Ni15 Ni11 30.1(7) . . . . ? C23 Ni12 Ni15 Ni11 146.1(3) . . . . ? C24 Ni12 Ni15 Ni11 60.5(4) . . . . ? Ni17 Ni12 Ni15 Ni11 -89.34(13) . . . . ? Ni4 Ni12 Ni15 Ni11 42.06(7) . . . . ? Ni1 Ni12 Ni15 Ni11 115.65(13) . . . . ? Ni14 Ni12 Ni15 Ni11 -173.47(9) . . . . ? Ni5 Ni12 Ni15 Ni11 -173.35(10) . . . . ? C20 Ni12 Ni15 Ni14 84(2) . . . . ? C20' Ni12 Ni15 Ni14 98.5(10) . . . . ? C13 Ni12 Ni15 Ni14 -156.4(7) . . . . ? C23 Ni12 Ni15 Ni14 -40.5(3) . . . . ? C24 Ni12 Ni15 Ni14 -126.0(4) . . . . ? Ni17 Ni12 Ni15 Ni14 84.13(13) . . . . ? Ni4 Ni12 Ni15 Ni14 -144.47(8) . . . . ? Ni1 Ni12 Ni15 Ni14 -70.88(12) . . . . ? Ni11 Ni12 Ni15 Ni14 173.47(9) . . . . ? Ni5 Ni12 Ni15 Ni14 0.12(8) . . . . ? C18 Ni14 Ni15 C19 9(3) . . . . ? C15 Ni14 Ni15 C19 -90(3) . . . . ? C23 Ni14 Ni15 C19 162(2) . . . . ? Ni13 Ni14 Ni15 C19 -141(2) . . . . ? Ni5 Ni14 Ni15 C19 118(2) . . . . ? Ni12 Ni14 Ni15 C19 118(2) . . . . ? Ni17 Ni14 Ni15 C19 54(2) . . . . ? C18 Ni14 Ni15 C19' 0.1(11) . . . . ? C15 Ni14 Ni15 C19' -98.8(12) . . . . ? C23 Ni14 Ni15 C19' 154.0(11) . . . . ? Ni13 Ni14 Ni15 C19' -149.3(10) . . . . ? Ni5 Ni14 Ni15 C19' 109.3(10) . . . . ? Ni12 Ni14 Ni15 C19' 109.5(10) . . . . ? Ni17 Ni14 Ni15 C19' 45.1(10) . . . . ? C18 Ni14 Ni15 C16 99.8(7) . . . . ? C15 Ni14 Ni15 C16 0.9(7) . . . . ? C23 Ni14 Ni15 C16 -106.2(6) . . . . ? Ni13 Ni14 Ni15 C16 -49.6(5) . . . . ? Ni5 Ni14 Ni15 C16 -150.9(5) . . . . ? Ni12 Ni14 Ni15 C16 -150.8(5) . . . . ? Ni17 Ni14 Ni15 C16 144.8(5) . . . . ? C18 Ni14 Ni15 C24 -151.6(6) . . . . ? C15 Ni14 Ni15 C24 109.5(6) . . . . ? C23 Ni14 Ni15 C24 2.3(5) . . . . ? Ni13 Ni14 Ni15 C24 59.0(4) . . . . ? Ni5 Ni14 Ni15 C24 -42.4(4) . . . . ? Ni12 Ni14 Ni15 C24 -42.2(4) . . . . ? Ni17 Ni14 Ni15 C24 -106.6(4) . . . . ? C18 Ni14 Ni15 Ni17 -45.0(5) . . . . ? C15 Ni14 Ni15 Ni17 -143.9(5) . . . . ? C23 Ni14 Ni15 Ni17 109.0(4) . . . . ? Ni13 Ni14 Ni15 Ni17 165.58(11) . . . . ? Ni5 Ni14 Ni15 Ni17 64.27(13) . . . . ? Ni12 Ni14 Ni15 Ni17 64.40(11) . . . . ? C18 Ni14 Ni15 Ni16 151.7(5) . . . . ? C15 Ni14 Ni15 Ni16 52.8(5) . . . . ? C23 Ni14 Ni15 Ni16 -54.4(4) . . . . ? Ni13 Ni14 Ni15 Ni16 2.24(8) . . . . ? Ni5 Ni14 Ni15 Ni16 -99.08(10) . . . . ? Ni12 Ni14 Ni15 Ni16 -98.95(8) . . . . ? Ni17 Ni14 Ni15 Ni16 -163.35(12) . . . . ? C18 Ni14 Ni15 Ni11 -102.8(5) . . . . ? C15 Ni14 Ni15 Ni11 158.4(5) . . . . ? C23 Ni14 Ni15 Ni11 51.2(4) . . . . ? Ni13 Ni14 Ni15 Ni11 107.83(10) . . . . ? Ni5 Ni14 Ni15 Ni11 6.52(14) . . . . ? Ni12 Ni14 Ni15 Ni11 6.64(9) . . . . ? Ni17 Ni14 Ni15 Ni11 -57.75(12) . . . . ? C18 Ni14 Ni15 Ni12 -109.4(5) . . . . ? C15 Ni14 Ni15 Ni12 151.7(5) . . . . ? C23 Ni14 Ni15 Ni12 44.6(4) . . . . ? Ni13 Ni14 Ni15 Ni12 101.18(8) . . . . ? Ni5 Ni14 Ni15 Ni12 -0.13(9) . . . . ? Ni17 Ni14 Ni15 Ni12 -64.40(11) . . . . ? C19 Ni15 Ni16 C17 19(6) . . . . ? C19' Ni15 Ni16 C17 29(4) . . . . ? C16 Ni15 Ni16 C17 10(3) . . . . ? C24 Ni15 Ni16 C17 -177(3) . . . . ? Ni17 Ni15 Ni16 C17 -136(3) . . . . ? Ni11 Ni15 Ni16 C17 152(3) . . . . ? Ni12 Ni15 Ni16 C17 -144(3) . . . . ? Ni14 Ni15 Ni16 C17 -86(3) . . . . ? C19 Ni15 Ni16 C17' -22(7) . . . . ? C19' Ni15 Ni16 C17' -13(5) . . . . ? C16 Ni15 Ni16 C17' -32(4) . . . . ? C24 Ni15 Ni16 C17' 142(4) . . . . ? Ni17 Ni15 Ni16 C17' -177(4) . . . . ? Ni11 Ni15 Ni16 C17' 111(4) . . . . ? Ni12 Ni15 Ni16 C17' 175(4) . . . . ? Ni14 Ni15 Ni16 C17' -127(4) . . . . ? C19 Ni15 Ni16 C16 9(6) . . . . ? C19' Ni15 Ni16 C16 19(3) . . . . ? C24 Ni15 Ni16 C16 173.1(7) . . . . ? Ni17 Ni15 Ni16 C16 -145.6(7) . . . . ? Ni11 Ni15 Ni16 C16 142.6(6) . . . . ? Ni12 Ni15 Ni16 C16 -153.7(6) . . . . ? Ni14 Ni15 Ni16 C16 -95.7(6) . . . . ? C19 Ni15 Ni16 C24 -164(6) . . . . ? C19' Ni15 Ni16 C24 -154(3) . . . . ? C16 Ni15 Ni16 C24 -173.1(7) . . . . ? Ni17 Ni15 Ni16 C24 41.3(6) . . . . ? Ni11 Ni15 Ni16 C24 -30.5(4) . . . . ? Ni12 Ni15 Ni16 C24 33.2(4) . . . . ? Ni14 Ni15 Ni16 C24 91.2(4) . . . . ? C19 Ni15 Ni16 C25 -171(6) . . . . ? C19' Ni15 Ni16 C25 -161(3) . . . . ? C16 Ni15 Ni16 C25 -179.9(7) . . . . ? C24 Ni15 Ni16 C25 -6.8(5) . . . . ? Ni17 Ni15 Ni16 C25 34.5(5) . . . . ? Ni11 Ni15 Ni16 C25 -37.3(3) . . . . ? Ni12 Ni15 Ni16 C25 26.4(3) . . . . ? Ni14 Ni15 Ni16 C25 84.4(3) . . . . ? C19 Ni15 Ni16 Ni9 -141(6) . . . . ? C19' Ni15 Ni16 Ni9 -131(3) . . . . ? C16 Ni15 Ni16 Ni9 -150.1(6) . . . . ? C24 Ni15 Ni16 Ni9 23.0(4) . . . . ? Ni17 Ni15 Ni16 Ni9 64.3(4) . . . . ? Ni11 Ni15 Ni16 Ni9 -7.43(16) . . . . ? Ni12 Ni15 Ni16 Ni9 56.25(15) . . . . ? Ni14 Ni15 Ni16 Ni9 114.27(13) . . . . ? C19 Ni15 Ni16 Ni8 150(6) . . . . ? C19' Ni15 Ni16 Ni8 160(3) . . . . ? C16 Ni15 Ni16 Ni8 141.0(6) . . . . ? C24 Ni15 Ni16 Ni8 -45.9(4) . . . . ? Ni17 Ni15 Ni16 Ni8 -4.6(4) . . . . ? Ni11 Ni15 Ni16 Ni8 -76.36(10) . . . . ? Ni12 Ni15 Ni16 Ni8 -12.68(11) . . . . ? Ni14 Ni15 Ni16 Ni8 45.34(10) . . . . ? C19 Ni15 Ni16 Ni10 -123(6) . . . . ? C19' Ni15 Ni16 Ni10 -113(3) . . . . ? C16 Ni15 Ni16 Ni10 -131.9(6) . . . . ? C24 Ni15 Ni16 Ni10 41.1(4) . . . . ? Ni17 Ni15 Ni16 Ni10 82.4(4) . . . . ? Ni11 Ni15 Ni16 Ni10 10.67(8) . . . . ? Ni12 Ni15 Ni16 Ni10 74.35(8) . . . . ? Ni14 Ni15 Ni16 Ni10 132.37(7) . . . . ? C19 Ni15 Ni16 Ni13 103(6) . . . . ? C19' Ni15 Ni16 Ni13 113(3) . . . . ? C16 Ni15 Ni16 Ni13 93.9(6) . . . . ? C24 Ni15 Ni16 Ni13 -93.0(4) . . . . ? Ni17 Ni15 Ni16 Ni13 -51.8(4) . . . . ? Ni11 Ni15 Ni16 Ni13 -123.50(7) . . . . ? Ni12 Ni15 Ni16 Ni13 -59.82(7) . . . . ? Ni14 Ni15 Ni16 Ni13 -1.80(7) . . . . ? C9 Ni9 Ni16 C17 -2.7(16) . . . . ? C10 Ni9 Ni16 C17 -116.1(16) . . . . ? C25 Ni9 Ni16 C17 149.9(15) . . . . ? Ni10 Ni9 Ni16 C17 -147.5(15) . . . . ? C17' Ni9 Ni16 C17 -21(3) . . . . ? Ni8 Ni9 Ni16 C17 93.3(15) . . . . ? Ni3 Ni9 Ni16 C17 141.5(15) . . . . ? C9 Ni9 Ni16 C17' 18(3) . . . . ? C10 Ni9 Ni16 C17' -95(3) . . . . ? C25 Ni9 Ni16 C17' 171(3) . . . . ? Ni10 Ni9 Ni16 C17' -127(3) . . . . ? Ni8 Ni9 Ni16 C17' 114(3) . . . . ? Ni3 Ni9 Ni16 C17' 162(3) . . . . ? C9 Ni9 Ni16 C16 77.1(15) . . . . ? C10 Ni9 Ni16 C16 -36.3(15) . . . . ? C25 Ni9 Ni16 C16 -130.3(14) . . . . ? Ni10 Ni9 Ni16 C16 -67.7(13) . . . . ? C17' Ni9 Ni16 C16 59(3) . . . . ? Ni8 Ni9 Ni16 C16 173.1(13) . . . . ? Ni3 Ni9 Ni16 C16 -138.6(13) . . . . ? C9 Ni9 Ni16 C24 -174.7(8) . . . . ? C10 Ni9 Ni16 C24 71.9(7) . . . . ? C25 Ni9 Ni16 C24 -22.1(5) . . . . ? Ni10 Ni9 Ni16 C24 40.5(3) . . . . ? C17' Ni9 Ni16 C24 167(3) . . . . ? Ni8 Ni9 Ni16 C24 -78.7(3) . . . . ? Ni3 Ni9 Ni16 C24 -30.4(3) . . . . ? C9 Ni9 Ni16 C25 -152.6(9) . . . . ? C10 Ni9 Ni16 C25 94.0(8) . . . . ? Ni10 Ni9 Ni16 C25 62.6(4) . . . . ? C17' Ni9 Ni16 C25 -171(3) . . . . ? Ni8 Ni9 Ni16 C25 -56.6(4) . . . . ? Ni3 Ni9 Ni16 C25 -8.3(4) . . . . ? C9 Ni9 Ni16 Ni15 167.4(8) . . . . ? C10 Ni9 Ni16 Ni15 54.0(7) . . . . ? C25 Ni9 Ni16 Ni15 -40.0(4) . . . . ? Ni10 Ni9 Ni16 Ni15 22.62(14) . . . . ? C17' Ni9 Ni16 Ni15 149(3) . . . . ? Ni8 Ni9 Ni16 Ni15 -96.56(14) . . . . ? Ni3 Ni9 Ni16 Ni15 -48.33(16) . . . . ? C9 Ni9 Ni16 Ni8 -96.0(8) . . . . ? C10 Ni9 Ni16 Ni8 150.6(7) . . . . ? C25 Ni9 Ni16 Ni8 56.6(4) . . . . ? Ni10 Ni9 Ni16 Ni8 119.18(9) . . . . ? C17' Ni9 Ni16 Ni8 -114(3) . . . . ? Ni3 Ni9 Ni16 Ni8 48.23(8) . . . . ? C9 Ni9 Ni16 Ni10 144.8(8) . . . . ? C10 Ni9 Ni16 Ni10 31.4(7) . . . . ? C25 Ni9 Ni16 Ni10 -62.6(4) . . . . ? C17' Ni9 Ni16 Ni10 127(3) . . . . ? Ni8 Ni9 Ni16 Ni10 -119.18(9) . . . . ? Ni3 Ni9 Ni16 Ni10 -70.95(9) . . . . ? C9 Ni9 Ni16 Ni13 -90.2(8) . . . . ? C10 Ni9 Ni16 Ni13 156.4(7) . . . . ? C25 Ni9 Ni16 Ni13 62.4(4) . . . . ? Ni10 Ni9 Ni16 Ni13 125.00(9) . . . . ? C17' Ni9 Ni16 Ni13 -108(3) . . . . ? Ni8 Ni9 Ni16 Ni13 5.82(8) . . . . ? Ni3 Ni9 Ni16 Ni13 54.04(11) . . . . ? C28' Ni8 Ni16 C17 -9(2) . . . . ? C28 Ni8 Ni16 C17 -15.2(17) . . . . ? C25 Ni8 Ni16 C17 -139.4(15) . . . . ? C22 Ni8 Ni16 C17 137.3(15) . . . . ? Ni18 Ni8 Ni16 C17 -72.0(15) . . . . ? Ni7 Ni8 Ni16 C17 87.8(15) . . . . ? Ni2 Ni8 Ni16 C17 171.9(15) . . . . ? Ni9 Ni8 Ni16 C17 -74.8(15) . . . . ? Ni3 Ni8 Ni16 C17 -122.5(15) . . . . ? Ni13 Ni8 Ni16 C17 98.8(15) . . . . ? C28' Ni8 Ni16 C17' 8(3) . . . . ? C28 Ni8 Ni16 C17' 2(3) . . . . ? C25 Ni8 Ni16 C17' -122(2) . . . . ? C22 Ni8 Ni16 C17' 154(2) . . . . ? Ni18 Ni8 Ni16 C17' -55(2) . . . . ? Ni7 Ni8 Ni16 C17' 105(2) . . . . ? Ni2 Ni8 Ni16 C17' -171(2) . . . . ? Ni9 Ni8 Ni16 C17' -58(2) . . . . ? Ni3 Ni8 Ni16 C17' -105(2) . . . . ? Ni13 Ni8 Ni16 C17' 116(2) . . . . ? C28' Ni8 Ni16 C16 -109.6(19) . . . . ? C28 Ni8 Ni16 C16 -115.7(13) . . . . ? C25 Ni8 Ni16 C16 120.1(10) . . . . ? C22 Ni8 Ni16 C16 36.8(10) . . . . ? Ni18 Ni8 Ni16 C16 -172.6(10) . . . . ? Ni7 Ni8 Ni16 C16 -12.8(9) . . . . ? Ni2 Ni8 Ni16 C16 71.4(9) . . . . ? Ni9 Ni8 Ni16 C16 -175.4(9) . . . . ? Ni3 Ni8 Ni16 C16 136.9(9) . . . . ? Ni13 Ni8 Ni16 C16 -1.7(9) . . . . ? C28' Ni8 Ni16 C24 157.0(17) . . . . ? C28 Ni8 Ni16 C24 150.9(10) . . . . ? C25 Ni8 Ni16 C24 26.6(6) . . . . ? C22 Ni8 Ni16 C24 -56.7(5) . . . . ? Ni18 Ni8 Ni16 C24 94.0(5) . . . . ? Ni7 Ni8 Ni16 C24 -106.2(4) . . . . ? Ni2 Ni8 Ni16 C24 -22.1(4) . . . . ? Ni9 Ni8 Ni16 C24 91.2(4) . . . . ? Ni3 Ni8 Ni16 C24 43.5(4) . . . . ? Ni13 Ni8 Ni16 C24 -95.1(4) . . . . ? C28' Ni8 Ni16 C25 130.4(17) . . . . ? C28 Ni8 Ni16 C25 124.2(10) . . . . ? C22 Ni8 Ni16 C25 -83.3(6) . . . . ? Ni18 Ni8 Ni16 C25 67.4(6) . . . . ? Ni7 Ni8 Ni16 C25 -132.8(5) . . . . ? Ni2 Ni8 Ni16 C25 -48.7(5) . . . . ? Ni9 Ni8 Ni16 C25 64.6(5) . . . . ? Ni3 Ni8 Ni16 C25 16.9(5) . . . . ? Ni13 Ni8 Ni16 C25 -121.7(5) . . . . ? C28' Ni8 Ni16 Ni15 -167.9(17) . . . . ? C28 Ni8 Ni16 Ni15 -174.0(9) . . . . ? C25 Ni8 Ni16 Ni15 61.7(5) . . . . ? C22 Ni8 Ni16 Ni15 -21.6(4) . . . . ? Ni18 Ni8 Ni16 Ni15 129.1(4) . . . . ? Ni7 Ni8 Ni16 Ni15 -71.10(13) . . . . ? Ni2 Ni8 Ni16 Ni15 13.02(18) . . . . ? Ni9 Ni8 Ni16 Ni15 126.30(11) . . . . ? Ni3 Ni8 Ni16 Ni15 78.60(11) . . . . ? Ni13 Ni8 Ni16 Ni15 -60.02(9) . . . . ? C28' Ni8 Ni16 Ni9 65.8(17) . . . . ? C28 Ni8 Ni16 Ni9 59.7(9) . . . . ? C25 Ni8 Ni16 Ni9 -64.6(5) . . . . ? C22 Ni8 Ni16 Ni9 -147.9(4) . . . . ? Ni18 Ni8 Ni16 Ni9 2.8(4) . . . . ? Ni7 Ni8 Ni16 Ni9 162.60(11) . . . . ? Ni2 Ni8 Ni16 Ni9 -113.28(14) . . . . ? Ni3 Ni8 Ni16 Ni9 -47.70(8) . . . . ? Ni13 Ni8 Ni16 Ni9 173.68(9) . . . . ? C28' Ni8 Ni16 Ni10 110.2(17) . . . . ? C28 Ni8 Ni16 Ni10 104.0(9) . . . . ? C25 Ni8 Ni16 Ni10 -20.2(5) . . . . ? C22 Ni8 Ni16 Ni10 -103.5(4) . . . . ? Ni18 Ni8 Ni16 Ni10 47.2(4) . . . . ? Ni7 Ni8 Ni16 Ni10 -153.03(9) . . . . ? Ni2 Ni8 Ni16 Ni10 -68.91(14) . . . . ? Ni9 Ni8 Ni16 Ni10 44.37(8) . . . . ? Ni3 Ni8 Ni16 Ni10 -3.34(8) . . . . ? Ni13 Ni8 Ni16 Ni10 -141.95(8) . . . . ? C28' Ni8 Ni16 Ni13 -107.9(17) . . . . ? C28 Ni8 Ni16 Ni13 -114.0(9) . . . . ? C25 Ni8 Ni16 Ni13 121.7(5) . . . . ? C22 Ni8 Ni16 Ni13 38.5(3) . . . . ? Ni18 Ni8 Ni16 Ni13 -170.9(4) . . . . ? Ni7 Ni8 Ni16 Ni13 -11.08(9) . . . . ? Ni2 Ni8 Ni16 Ni13 73.04(13) . . . . ? Ni9 Ni8 Ni16 Ni13 -173.68(9) . . . . ? Ni3 Ni8 Ni16 Ni13 138.62(8) . . . . ? C11 Ni10 Ni16 C17 -113.2(18) . . . . ? C10 Ni10 Ni16 C17 2.9(18) . . . . ? C24 Ni10 Ni16 C17 156.3(17) . . . . ? C25 Ni10 Ni16 C17 103.2(17) . . . . ? Ni9 Ni10 Ni16 C17 36.3(16) . . . . ? Ni11 Ni10 Ni16 C17 -171.3(16) . . . . ? Ni4 Ni10 Ni16 C17 133.0(16) . . . . ? C11 Ni10 Ni16 C17' -101(3) . . . . ? C10 Ni10 Ni16 C17' 15(3) . . . . ? C24 Ni10 Ni16 C17' 169(2) . . . . ? C25 Ni10 Ni16 C17' 116(2) . . . . ? Ni9 Ni10 Ni16 C17' 49(2) . . . . ? Ni11 Ni10 Ni16 C17' -159(2) . . . . ? Ni4 Ni10 Ni16 C17' 146(2) . . . . ? C11 Ni10 Ni16 C16 7.0(9) . . . . ? C10 Ni10 Ni16 C16 123.1(9) . . . . ? C24 Ni10 Ni16 C16 -83.5(7) . . . . ? C25 Ni10 Ni16 C16 -136.6(7) . . . . ? Ni9 Ni10 Ni16 C16 156.5(5) . . . . ? Ni11 Ni10 Ni16 C16 -51.1(5) . . . . ? Ni4 Ni10 Ni16 C16 -106.8(5) . . . . ? C11 Ni10 Ni16 C24 90.5(9) . . . . ? C10 Ni10 Ni16 C24 -153.4(8) . . . . ? C25 Ni10 Ni16 C24 -53.1(6) . . . . ? Ni9 Ni10 Ni16 C24 -120.0(5) . . . . ? Ni11 Ni10 Ni16 C24 32.4(5) . . . . ? Ni4 Ni10 Ni16 C24 -23.3(5) . . . . ? C11 Ni10 Ni16 C25 143.6(9) . . . . ? C10 Ni10 Ni16 C25 -100.3(8) . . . . ? C24 Ni10 Ni16 C25 53.1(6) . . . . ? Ni9 Ni10 Ni16 C25 -66.9(5) . . . . ? Ni11 Ni10 Ni16 C25 85.5(5) . . . . ? Ni4 Ni10 Ni16 C25 29.8(5) . . . . ? C11 Ni10 Ni16 Ni15 47.0(8) . . . . ? C10 Ni10 Ni16 Ni15 163.1(7) . . . . ? C24 Ni10 Ni16 Ni15 -43.5(5) . . . . ? C25 Ni10 Ni16 Ni15 -96.6(5) . . . . ? Ni9 Ni10 Ni16 Ni15 -163.54(10) . . . . ? Ni11 Ni10 Ni16 Ni15 -11.14(8) . . . . ? Ni4 Ni10 Ni16 Ni15 -66.82(8) . . . . ? C11 Ni10 Ni16 Ni9 -149.5(8) . . . . ? C10 Ni10 Ni16 Ni9 -33.4(7) . . . . ? C24 Ni10 Ni16 Ni9 120.0(5) . . . . ? C25 Ni10 Ni16 Ni9 66.9(5) . . . . ? Ni11 Ni10 Ni16 Ni9 152.39(10) . . . . ? Ni4 Ni10 Ni16 Ni9 96.71(9) . . . . ? C11 Ni10 Ni16 Ni8 162.9(8) . . . . ? C10 Ni10 Ni16 Ni8 -81.0(7) . . . . ? C24 Ni10 Ni16 Ni8 72.4(5) . . . . ? C25 Ni10 Ni16 Ni8 19.3(5) . . . . ? Ni9 Ni10 Ni16 Ni8 -47.60(7) . . . . ? Ni11 Ni10 Ni16 Ni8 104.79(8) . . . . ? Ni4 Ni10 Ni16 Ni8 49.11(8) . . . . ? C11 Ni10 Ni16 Ni13 119.1(8) . . . . ? C10 Ni10 Ni16 Ni13 -124.8(7) . . . . ? C24 Ni10 Ni16 Ni13 28.6(5) . . . . ? C25 Ni10 Ni16 Ni13 -24.5(5) . . . . ? Ni9 Ni10 Ni16 Ni13 -91.40(12) . . . . ? Ni11 Ni10 Ni16 Ni13 60.99(13) . . . . ? Ni4 Ni10 Ni16 Ni13 5.31(14) . . . . ? C14 Ni13 Ni16 C17 3.9(16) . . . . ? C15 Ni13 Ni16 C17 103.2(16) . . . . ? C23 Ni13 Ni16 C17 -155.1(15) . . . . ? C22 Ni13 Ni16 C17 -116.3(15) . . . . ? Ni14 Ni13 Ni16 C17 153.7(15) . . . . ? Ni7 Ni13 Ni16 C17 -70.5(15) . . . . ? Ni8 Ni13 Ni16 C17 -80.4(15) . . . . ? Ni6 Ni13 Ni16 C17 -130.4(15) . . . . ? C14 Ni13 Ni16 C17' 4(3) . . . . ? C15 Ni13 Ni16 C17' 103(3) . . . . ? C23 Ni13 Ni16 C17' -155(3) . . . . ? C22 Ni13 Ni16 C17' -117(3) . . . . ? Ni14 Ni13 Ni16 C17' 153(3) . . . . ? Ni7 Ni13 Ni16 C17' -71(3) . . . . ? Ni8 Ni13 Ni16 C17' -81(3) . . . . ? Ni6 Ni13 Ni16 C17' -131(3) . . . . ? C14 Ni13 Ni16 C16 -96.7(8) . . . . ? C15 Ni13 Ni16 C16 2.7(7) . . . . ? C23 Ni13 Ni16 C16 104.3(6) . . . . ? C22 Ni13 Ni16 C16 143.1(6) . . . . ? Ni14 Ni13 Ni16 C16 53.1(5) . . . . ? Ni7 Ni13 Ni16 C16 -171.1(5) . . . . ? Ni8 Ni13 Ni16 C16 179.0(5) . . . . ? Ni6 Ni13 Ni16 C16 129.0(5) . . . . ? C14 Ni13 Ni16 C24 160.9(7) . . . . ? C15 Ni13 Ni16 C24 -99.7(6) . . . . ? C23 Ni13 Ni16 C24 1.9(5) . . . . ? C22 Ni13 Ni16 C24 40.7(5) . . . . ? Ni14 Ni13 Ni16 C24 -49.3(4) . . . . ? Ni7 Ni13 Ni16 C24 86.5(4) . . . . ? Ni8 Ni13 Ni16 C24 76.6(4) . . . . ? Ni6 Ni13 Ni16 C24 26.6(4) . . . . ? C14 Ni13 Ni16 C25 121.9(7) . . . . ? C15 Ni13 Ni16 C25 -138.8(6) . . . . ? C23 Ni13 Ni16 C25 -37.1(5) . . . . ? C22 Ni13 Ni16 C25 1.7(5) . . . . ? Ni14 Ni13 Ni16 C25 -88.3(4) . . . . ? Ni7 Ni13 Ni16 C25 47.5(4) . . . . ? Ni8 Ni13 Ni16 C25 37.6(3) . . . . ? Ni6 Ni13 Ni16 C25 -12.4(4) . . . . ? C14 Ni13 Ni16 Ni15 -147.7(6) . . . . ? C15 Ni13 Ni16 Ni15 -48.4(5) . . . . ? C23 Ni13 Ni16 Ni15 53.3(3) . . . . ? C22 Ni13 Ni16 Ni15 92.1(3) . . . . ? Ni14 Ni13 Ni16 Ni15 2.12(8) . . . . ? Ni7 Ni13 Ni16 Ni15 137.93(9) . . . . ? Ni8 Ni13 Ni16 Ni15 128.03(8) . . . . ? Ni6 Ni13 Ni16 Ni15 78.03(13) . . . . ? C14 Ni13 Ni16 Ni9 78.4(6) . . . . ? C15 Ni13 Ni16 Ni9 177.8(5) . . . . ? C23 Ni13 Ni16 Ni9 -80.6(3) . . . . ? C22 Ni13 Ni16 Ni9 -41.8(3) . . . . ? Ni14 Ni13 Ni16 Ni9 -131.77(10) . . . . ? Ni7 Ni13 Ni16 Ni9 4.04(12) . . . . ? Ni8 Ni13 Ni16 Ni9 -5.87(8) . . . . ? Ni6 Ni13 Ni16 Ni9 -55.86(16) . . . . ? C14 Ni13 Ni16 Ni8 84.3(6) . . . . ? C15 Ni13 Ni16 Ni8 -176.4(5) . . . . ? C23 Ni13 Ni16 Ni8 -74.7(3) . . . . ? C22 Ni13 Ni16 Ni8 -35.9(3) . . . . ? Ni14 Ni13 Ni16 Ni8 -125.90(8) . . . . ? Ni7 Ni13 Ni16 Ni8 9.91(8) . . . . ? Ni6 Ni13 Ni16 Ni8 -49.99(12) . . . . ? C14 Ni13 Ni16 Ni10 140.0(6) . . . . ? C15 Ni13 Ni16 Ni10 -120.7(5) . . . . ? C23 Ni13 Ni16 Ni10 -19.0(4) . . . . ? C22 Ni13 Ni16 Ni10 19.8(4) . . . . ? Ni14 Ni13 Ni16 Ni10 -70.23(13) . . . . ? Ni7 Ni13 Ni16 Ni10 65.58(14) . . . . ? Ni8 Ni13 Ni16 Ni10 55.68(11) . . . . ? Ni6 Ni13 Ni16 Ni10 5.68(19) . . . . ? C2 Ni1 C1 O1 -23(2) . . . . ? C13 Ni1 C1 O1 77(2) . . . . ? C23 Ni1 C1 O1 -177(2) . . . . ? C22 Ni1 C1 O1 -146.1(19) . . . . ? Ni2 Ni1 C1 O1 -69(2) . . . . ? Ni5 Ni1 C1 O1 -179(2) . . . . ? Ni12 Ni1 C1 O1 129(2) . . . . ? Ni6 Ni1 C1 O1 -132(2) . . . . ? C2 Ni1 C1 Ni5 155.1(5) . . . . ? C13 Ni1 C1 Ni5 -104.3(6) . . . . ? C23 Ni1 C1 Ni5 1.3(6) . . . . ? C22 Ni1 C1 Ni5 32.5(9) . . . . ? Ni2 Ni1 C1 Ni5 109.7(5) . . . . ? Ni12 Ni1 C1 Ni5 -52.1(5) . . . . ? Ni6 Ni1 C1 Ni5 46.2(4) . . . . ? C5 Ni5 C1 O1 -21(2) . . . . ? C23 Ni5 C1 O1 177.4(19) . . . . ? C6 Ni5 C1 O1 79(2) . . . . ? Ni1 Ni5 C1 O1 179(2) . . . . ? Ni6 Ni5 C1 O1 122(2) . . . . ? Ni14 Ni5 C1 O1 -153.4(15) . . . . ? Ni12 Ni5 C1 O1 -135(2) . . . . ? C5 Ni5 C1 Ni1 160.7(6) . . . . ? C23 Ni5 C1 Ni1 -1.3(6) . . . . ? C6 Ni5 C1 Ni1 -99.4(6) . . . . ? Ni6 Ni5 C1 Ni1 -56.2(4) . . . . ? Ni14 Ni5 C1 Ni1 28.0(11) . . . . ? Ni12 Ni5 C1 Ni1 46.1(4) . . . . ? C1 Ni1 C2 O2 36(2) . . . . ? C13 Ni1 C2 O2 -57(2) . . . . ? C23 Ni1 C2 O2 173.4(15) . . . . ? C22 Ni1 C2 O2 176.6(18) . . . . ? Ni2 Ni1 C2 O2 178(2) . . . . ? Ni5 Ni1 C2 O2 72(2) . . . . ? Ni12 Ni1 C2 O2 -91(2) . . . . ? Ni6 Ni1 C2 O2 127.1(18) . . . . ? C1 Ni1 C2 Ni2 -142.3(6) . . . . ? C13 Ni1 C2 Ni2 124.8(6) . . . . ? C23 Ni1 C2 Ni2 -4.9(10) . . . . ? C22 Ni1 C2 Ni2 -1.7(5) . . . . ? Ni5 Ni1 C2 Ni2 -106.7(6) . . . . ? Ni12 Ni1 C2 Ni2 90.9(7) . . . . ? Ni6 Ni1 C2 Ni2 -51.3(4) . . . . ? C26 Ni2 C2 O2 -4(2) . . . . ? C26' Ni2 C2 O2 -13(3) . . . . ? C22 Ni2 C2 O2 -176.5(16) . . . . ? Ni1 Ni2 C2 O2 -178(2) . . . . ? Ni18 Ni2 C2 O2 49(2) . . . . ? Ni8 Ni2 C2 O2 131.5(15) . . . . ? Ni7 Ni2 C2 O2 -126.7(15) . . . . ? Ni3 Ni2 C2 O2 92.8(17) . . . . ? C26 Ni2 C2 Ni1 174.5(12) . . . . ? C26' Ni2 C2 Ni1 165(3) . . . . ? C22 Ni2 C2 Ni1 1.9(6) . . . . ? Ni18 Ni2 C2 Ni1 -133.0(4) . . . . ? Ni8 Ni2 C2 Ni1 -50.1(8) . . . . ? Ni7 Ni2 C2 Ni1 51.7(8) . . . . ? Ni3 Ni2 C2 Ni1 -88.8(4) . . . . ? C4 Ni4 C3 O3 -34(2) . . . . ? C13 Ni4 C3 O3 60(2) . . . . ? C24 Ni4 C3 O3 -165.4(16) . . . . ? C25 Ni4 C3 O3 -172.1(19) . . . . ? Ni3 Ni4 C3 O3 -177(2) . . . . ? Ni11 Ni4 C3 O3 -68(2) . . . . ? Ni12 Ni4 C3 O3 92(2) . . . . ? Ni10 Ni4 C3 O3 -121.7(19) . . . . ? C4 Ni4 C3 Ni3 142.3(7) . . . . ? C13 Ni4 C3 Ni3 -123.7(6) . . . . ? C24 Ni4 C3 Ni3 11.2(10) . . . . ? C25 Ni4 C3 Ni3 4.4(6) . . . . ? Ni11 Ni4 C3 Ni3 108.3(7) . . . . ? Ni12 Ni4 C3 Ni3 -91.9(8) . . . . ? Ni10 Ni4 C3 Ni3 54.9(5) . . . . ? C27 Ni3 C3 O3 -1(2) . . . . ? C27' Ni3 C3 O3 13(3) . . . . ? C25 Ni3 C3 O3 171.7(18) . . . . ? Ni4 Ni3 C3 O3 177(2) . . . . ? Ni18 Ni3 C3 O3 -55(2) . . . . ? Ni8 Ni3 C3 O3 -139.2(15) . . . . ? Ni9 Ni3 C3 O3 119.0(17) . . . . ? Ni2 Ni3 C3 O3 -96.6(19) . . . . ? C27 Ni3 C3 Ni4 -177.7(8) . . . . ? C27' Ni3 C3 Ni4 -164.0(19) . . . . ? C25 Ni3 C3 Ni4 -5.0(6) . . . . ? Ni18 Ni3 C3 Ni4 128.5(5) . . . . ? Ni8 Ni3 C3 Ni4 44.1(9) . . . . ? Ni9 Ni3 C3 Ni4 -57.7(8) . . . . ? Ni2 Ni3 C3 Ni4 86.6(4) . . . . ? C12 Ni11 C4 O4 19(3) . . . . ? C24 Ni11 C4 O4 -171(2) . . . . ? C11 Ni11 C4 O4 -77(2) . . . . ? Ni4 Ni11 C4 O4 -177(3) . . . . ? Ni10 Ni11 C4 O4 -118(2) . . . . ? Ni15 Ni11 C4 O4 159.4(17) . . . . ? Ni12 Ni11 C4 O4 137(2) . . . . ? C12 Ni11 C4 Ni4 -163.9(7) . . . . ? C24 Ni11 C4 Ni4 5.8(7) . . . . ? C11 Ni11 C4 Ni4 100.0(6) . . . . ? Ni10 Ni11 C4 Ni4 58.7(5) . . . . ? Ni15 Ni11 C4 Ni4 -23.5(13) . . . . ? Ni12 Ni11 C4 Ni4 -46.2(5) . . . . ? C3 Ni4 C4 O4 21(2) . . . . ? C13 Ni4 C4 O4 -79(2) . . . . ? C24 Ni4 C4 O4 172(2) . . . . ? C25 Ni4 C4 O4 142.4(19) . . . . ? Ni3 Ni4 C4 O4 68(2) . . . . ? Ni11 Ni4 C4 O4 177(3) . . . . ? Ni12 Ni4 C4 O4 -132(2) . . . . ? Ni10 Ni4 C4 O4 127(2) . . . . ? C3 Ni4 C4 Ni11 -156.1(6) . . . . ? C13 Ni4 C4 Ni11 103.4(7) . . . . ? C24 Ni4 C4 Ni11 -5.5(7) . . . . ? C25 Ni4 C4 Ni11 -34.9(10) . . . . ? Ni3 Ni4 C4 Ni11 -109.7(7) . . . . ? Ni12 Ni4 C4 Ni11 50.7(5) . . . . ? Ni10 Ni4 C4 Ni11 -50.7(4) . . . . ? C1 Ni5 C5 O5 -121(42) . . . . ? C23 Ni5 C5 O5 27(43) . . . . ? C6 Ni5 C5 O5 142(42) . . . . ? Ni1 Ni5 C5 O5 -91(42) . . . . ? Ni6 Ni5 C5 O5 122(42) . . . . ? Ni14 Ni5 C5 O5 36(42) . . . . ? Ni12 Ni5 C5 O5 -24(42) . . . . ? C7 Ni6 C6 O6 -10(5) . . . . ? C22 Ni6 C6 O6 156(4) . . . . ? C23 Ni6 C6 O6 -177(5) . . . . ? Ni7 Ni6 C6 O6 -7(6) . . . . ? Ni5 Ni6 C6 O6 172(5) . . . . ? Ni1 Ni6 C6 O6 133(5) . . . . ? Ni13 Ni6 C6 O6 -121(5) . . . . ? C7 Ni6 C6 Ni5 178.3(6) . . . . ? C22 Ni6 C6 Ni5 -15.6(15) . . . . ? C23 Ni6 C6 Ni5 11.7(7) . . . . ? Ni7 Ni6 C6 Ni5 -179.0(9) . . . . ? Ni1 Ni6 C6 Ni5 -38.6(4) . . . . ? Ni13 Ni6 C6 Ni5 67.4(7) . . . . ? C5 Ni5 C6 O6 23.0(16) . . . . ? C1 Ni5 C6 O6 -81.7(15) . . . . ? C23 Ni5 C6 O6 172.6(15) . . . . ? Ni1 Ni5 C6 O6 -132.1(14) . . . . ? Ni6 Ni5 C6 O6 -177.0(19) . . . . ? Ni14 Ni5 C6 O6 124.7(14) . . . . ? Ni12 Ni5 C6 O6 -179.8(10) . . . . ? C5 Ni5 C6 Ni6 -160.0(6) . . . . ? C1 Ni5 C6 Ni6 95.3(6) . . . . ? C23 Ni5 C6 Ni6 -10.4(6) . . . . ? Ni1 Ni5 C6 Ni6 45.0(5) . . . . ? Ni14 Ni5 C6 Ni6 -58.3(5) . . . . ? Ni12 Ni5 C6 Ni6 -2.8(11) . . . . ? C6 Ni6 C7 O7 -13(3) . . . . ? C22 Ni6 C7 O7 174(3) . . . . ? C23 Ni6 C7 O7 149(3) . . . . ? Ni7 Ni6 C7 O7 169(4) . . . . ? Ni5 Ni6 C7 O7 -7(5) . . . . ? Ni1 Ni6 C7 O7 -135(3) . . . . ? Ni13 Ni6 C7 O7 126(3) . . . . ? C6 Ni6 C7 Ni7 178.6(7) . . . . ? C22 Ni6 C7 Ni7 5.4(7) . . . . ? C23 Ni6 C7 Ni7 -20.2(13) . . . . ? Ni5 Ni6 C7 Ni7 -176.0(17) . . . . ? Ni1 Ni6 C7 Ni7 55.8(9) . . . . ? Ni13 Ni6 C7 Ni7 -42.9(5) . . . . ? C8 Ni7 C7 O7 14(2) . . . . ? C22 Ni7 C7 O7 -178(2) . . . . ? Ni6 Ni7 C7 O7 -172(3) . . . . ? Ni8 Ni7 C7 O7 -175.4(12) . . . . ? Ni13 Ni7 C7 O7 -124(2) . . . . ? Ni2 Ni7 C7 O7 131.3(19) . . . . ? C8 Ni7 C7 Ni6 -173.9(7) . . . . ? C22 Ni7 C7 Ni6 -5.5(7) . . . . ? Ni8 Ni7 C7 Ni6 -3.1(16) . . . . ? Ni13 Ni7 C7 Ni6 48.5(6) . . . . ? Ni2 Ni7 C7 Ni6 -56.4(6) . . . . ? C7 Ni7 C8 O8 64(30) . . . . ? C22 Ni7 C8 O8 -85(30) . . . . ? Ni6 Ni7 C8 O8 57(30) . . . . ? Ni8 Ni7 C8 O8 -111(30) . . . . ? Ni13 Ni7 C8 O8 175(100) . . . . ? Ni2 Ni7 C8 O8 -47(30) . . . . ? C10 Ni9 C9 O9 -63(38) . . . . ? C25 Ni9 C9 O9 89(38) . . . . ? Ni10 Ni9 C9 O9 -68(38) . . . . ? C17' Ni9 C9 O9 -168(38) . . . . ? Ni16 Ni9 C9 O9 -179(100) . . . . ? Ni8 Ni9 C9 O9 107(38) . . . . ? Ni3 Ni9 C9 O9 41(38) . . . . ? C11 Ni10 C10 O10 -6(4) . . . . ? C24 Ni10 C10 O10 -173(3) . . . . ? C25 Ni10 C10 O10 167(3) . . . . ? Ni9 Ni10 C10 O10 -179(4) . . . . ? Ni11 Ni10 C10 O10 12(6) . . . . ? Ni4 Ni10 C10 O10 115(3) . . . . ? Ni16 Ni10 C10 O10 -142(3) . . . . ? C11 Ni10 C10 Ni9 173.0(7) . . . . ? C24 Ni10 C10 Ni9 5.4(15) . . . . ? C25 Ni10 C10 Ni9 -13.9(8) . . . . ? Ni11 Ni10 C10 Ni9 -169(2) . . . . ? Ni4 Ni10 C10 Ni9 -66.1(9) . . . . ? Ni16 Ni10 C10 Ni9 36.5(6) . . . . ? C9 Ni9 C10 O10 3(2) . . . . ? C25 Ni9 C10 O10 -167(2) . . . . ? Ni10 Ni9 C10 O10 179(3) . . . . ? C17' Ni9 C10 O10 96(3) . . . . ? Ni16 Ni9 C10 O10 138(2) . . . . ? Ni8 Ni9 C10 O10 -158.1(15) . . . . ? Ni3 Ni9 C10 O10 -117(2) . . . . ? C9 Ni9 C10 Ni10 -176.1(8) . . . . ? C25 Ni9 C10 Ni10 14.0(8) . . . . ? C17' Ni9 C10 Ni10 -83.0(15) . . . . ? Ni16 Ni9 C10 Ni10 -40.9(7) . . . . ? Ni8 Ni9 C10 Ni10 22.8(17) . . . . ? Ni3 Ni9 C10 Ni10 64.0(6) . . . . ? C10 Ni10 C11 O11 15(5) . . . . ? C24 Ni10 C11 O11 -173(4) . . . . ? C25 Ni10 C11 O11 -150(4) . . . . ? Ni9 Ni10 C11 O11 28(5) . . . . ? Ni11 Ni10 C11 O11 -160(5) . . . . ? Ni4 Ni10 C11 O11 -120(5) . . . . ? Ni16 Ni10 C11 O11 131(4) . . . . ? C10 Ni10 C11 Ni11 175.4(7) . . . . ? C24 Ni10 C11 Ni11 -13.4(6) . . . . ? C25 Ni10 C11 Ni11 10.1(14) . . . . ? Ni9 Ni10 C11 Ni11 -172.2(8) . . . . ? Ni4 Ni10 C11 Ni11 39.5(4) . . . . ? Ni16 Ni10 C11 Ni11 -69.2(6) . . . . ? C12 Ni11 C11 O11 -27.0(14) . . . . ? C4 Ni11 C11 O11 79.5(14) . . . . ? C24 Ni11 C11 O11 -175.0(13) . . . . ? Ni4 Ni11 C11 O11 128.9(13) . . . . ? Ni10 Ni11 C11 O11 172.9(17) . . . . ? Ni15 Ni11 C11 O11 -128.7(12) . . . . ? Ni12 Ni11 C11 O11 170.7(9) . . . . ? C12 Ni11 C11 Ni10 160.0(7) . . . . ? C4 Ni11 C11 Ni10 -93.4(7) . . . . ? C24 Ni11 C11 Ni10 12.1(6) . . . . ? Ni4 Ni11 C11 Ni10 -44.0(5) . . . . ? Ni15 Ni11 C11 Ni10 58.4(5) . . . . ? Ni12 Ni11 C11 Ni10 -2.3(10) . . . . ? C4 Ni11 C12 O12 -104(23) . . . . ? C24 Ni11 C12 O12 94(23) . . . . ? C11 Ni11 C12 O12 -13(23) . . . . ? Ni4 Ni11 C12 O12 -131(22) . . . . ? Ni10 Ni11 C12 O12 6(23) . . . . ? Ni15 Ni11 C12 O12 97(23) . . . . ? Ni12 Ni11 C12 O12 157(23) . . . . ? C3 Ni4 C13 O13 -59.1(15) . . . . ? C4 Ni4 C13 O13 45.4(16) . . . . ? C24 Ni4 C13 O13 149.2(14) . . . . ? C25 Ni4 C13 O13 -172.2(12) . . . . ? Ni3 Ni4 C13 O13 -109.3(14) . . . . ? Ni11 Ni4 C13 O13 94.5(15) . . . . ? Ni12 Ni4 C13 O13 142.3(17) . . . . ? Ni10 Ni4 C13 O13 123.8(13) . . . . ? C3 Ni4 C13 Ni1 84.4(7) . . . . ? C4 Ni4 C13 Ni1 -171.1(8) . . . . ? C24 Ni4 C13 Ni1 -67.3(7) . . . . ? C25 Ni4 C13 Ni1 -28.7(10) . . . . ? Ni3 Ni4 C13 Ni1 34.2(8) . . . . ? Ni11 Ni4 C13 Ni1 -122.0(5) . . . . ? Ni12 Ni4 C13 Ni1 -74.2(6) . . . . ? Ni10 Ni4 C13 Ni1 -92.7(10) . . . . ? C3 Ni4 C13 Ni12 158.6(5) . . . . ? C4 Ni4 C13 Ni12 -96.9(6) . . . . ? C24 Ni4 C13 Ni12 6.9(6) . . . . ? C25 Ni4 C13 Ni12 45.4(7) . . . . ? Ni3 Ni4 C13 Ni12 108.3(4) . . . . ? Ni11 Ni4 C13 Ni12 -47.8(4) . . . . ? Ni10 Ni4 C13 Ni12 -18.5(12) . . . . ? C2 Ni1 C13 O13 61.7(16) . . . . ? C1 Ni1 C13 O13 -42.0(16) . . . . ? C23 Ni1 C13 O13 -148.3(15) . . . . ? C22 Ni1 C13 O13 174.4(13) . . . . ? Ni2 Ni1 C13 O13 111.5(15) . . . . ? Ni5 Ni1 C13 O13 -91.9(16) . . . . ? Ni12 Ni1 C13 O13 -141.7(18) . . . . ? Ni6 Ni1 C13 O13 -125.9(13) . . . . ? C2 Ni1 C13 Ni4 -82.3(7) . . . . ? C1 Ni1 C13 Ni4 174.1(7) . . . . ? C23 Ni1 C13 Ni4 67.8(7) . . . . ? C22 Ni1 C13 Ni4 30.4(10) . . . . ? Ni2 Ni1 C13 Ni4 -32.4(8) . . . . ? Ni5 Ni1 C13 Ni4 124.2(5) . . . . ? Ni12 Ni1 C13 Ni4 74.3(5) . . . . ? Ni6 Ni1 C13 Ni4 90.2(11) . . . . ? C2 Ni1 C13 Ni12 -156.6(5) . . . . ? C1 Ni1 C13 Ni12 99.8(6) . . . . ? C23 Ni1 C13 Ni12 -6.6(6) . . . . ? C22 Ni1 C13 Ni12 -43.9(7) . . . . ? Ni2 Ni1 C13 Ni12 -106.7(4) . . . . ? Ni5 Ni1 C13 Ni12 49.8(4) . . . . ? Ni6 Ni1 C13 Ni12 15.8(12) . . . . ? C20 Ni12 C13 O13 7(3) . . . . ? C20' Ni12 C13 O13 -3(2) . . . . ? C23 Ni12 C13 O13 133.8(19) . . . . ? C24 Ni12 C13 O13 -135.4(19) . . . . ? Ni17 Ni12 C13 O13 -23(2) . . . . ? Ni4 Ni12 C13 O13 -129(2) . . . . ? Ni1 Ni12 C13 O13 127(2) . . . . ? Ni14 Ni12 C13 O13 105.5(18) . . . . ? Ni15 Ni12 C13 O13 -113.4(19) . . . . ? Ni11 Ni12 C13 O13 -88.1(19) . . . . ? Ni5 Ni12 C13 O13 86.1(19) . . . . ? C20 Ni12 C13 Ni4 136(3) . . . . ? C20' Ni12 C13 Ni4 125.9(11) . . . . ? C23 Ni12 C13 Ni4 -97.2(5) . . . . ? C24 Ni12 C13 Ni4 -6.4(5) . . . . ? Ni17 Ni12 C13 Ni4 106.4(5) . . . . ? Ni1 Ni12 C13 Ni4 -103.7(6) . . . . ? Ni14 Ni12 C13 Ni4 -125.5(5) . . . . ? Ni15 Ni12 C13 Ni4 15.5(10) . . . . ? Ni11 Ni12 C13 Ni4 40.9(4) . . . . ? Ni5 Ni12 C13 Ni4 -144.9(4) . . . . ? C20 Ni12 C13 Ni1 -121(3) . . . . ? C20' Ni12 C13 Ni1 -130.4(11) . . . . ? C23 Ni12 C13 Ni1 6.5(6) . . . . ? C24 Ni12 C13 Ni1 97.3(5) . . . . ? Ni17 Ni12 C13 Ni1 -149.9(3) . . . . ? Ni4 Ni12 C13 Ni1 103.7(6) . . . . ? Ni14 Ni12 C13 Ni1 -21.8(10) . . . . ? Ni15 Ni12 C13 Ni1 119.3(6) . . . . ? Ni11 Ni12 C13 Ni1 144.6(4) . . . . ? Ni5 Ni12 C13 Ni1 -41.2(4) . . . . ? C15 Ni13 C14 O14 14(35) . . . . ? C23 Ni13 C14 O14 -142(34) . . . . ? C22 Ni13 C14 O14 -156(35) . . . . ? Ni14 Ni13 C14 O14 10(36) . . . . ? Ni7 Ni13 C14 O14 -133(35) . . . . ? Ni8 Ni13 C14 O14 170(35) . . . . ? Ni6 Ni13 C14 O14 -101(35) . . . . ? Ni16 Ni13 C14 O14 113(35) . . . . ? C18 Ni14 C15 O15 -6(2) . . . . ? C23 Ni14 C15 O15 -175(2) . . . . ? Ni13 Ni14 C15 O15 179(3) . . . . ? Ni5 Ni14 C15 O15 -121(2) . . . . ? Ni12 Ni14 C15 O15 132.7(18) . . . . ? Ni15 Ni14 C15 O15 96(2) . . . . ? Ni17 Ni14 C15 O15 63(2) . . . . ? C18 Ni14 C15 Ni13 175.8(6) . . . . ? C23 Ni14 C15 Ni13 6.5(7) . . . . ? Ni5 Ni14 C15 Ni13 60.3(8) . . . . ? Ni12 Ni14 C15 Ni13 -45.8(9) . . . . ? Ni15 Ni14 C15 Ni13 -82.7(4) . . . . ? Ni17 Ni14 C15 Ni13 -116.0(5) . . . . ? C14 Ni13 C15 O15 4(2) . . . . ? C23 Ni13 C15 O15 176(2) . . . . ? C22 Ni13 C15 O15 170.7(16) . . . . ? Ni14 Ni13 C15 O15 -179(2) . . . . ? Ni7 Ni13 C15 O15 80(2) . . . . ? Ni8 Ni13 C15 O15 -97(2) . . . . ? Ni6 Ni13 C15 O15 127(2) . . . . ? Ni16 Ni13 C15 O15 -89(2) . . . . ? C14 Ni13 C15 Ni14 -177.3(7) . . . . ? C23 Ni13 C15 Ni14 -5.9(6) . . . . ? C22 Ni13 C15 Ni14 -10.8(11) . . . . ? Ni7 Ni13 C15 Ni14 -101.7(9) . . . . ? Ni8 Ni13 C15 Ni14 81.8(13) . . . . ? Ni6 Ni13 C15 Ni14 -54.8(5) . . . . ? Ni16 Ni13 C15 Ni14 89.1(4) . . . . ? C19 Ni15 C16 O16 7(4) . . . . ? C19' Ni15 C16 O16 11(3) . . . . ? C24 Ni15 C16 O16 174.8(18) . . . . ? Ni17 Ni15 C16 O16 -19(3) . . . . ? Ni16 Ni15 C16 O16 -179(2) . . . . ? Ni11 Ni15 C16 O16 122.5(17) . . . . ? Ni12 Ni15 C16 O16 -130.8(16) . . . . ? Ni14 Ni15 C16 O16 -85.9(19) . . . . ? C19 Ni15 C16 Ni16 -174(4) . . . . ? C19' Ni15 C16 Ni16 -170.2(15) . . . . ? C24 Ni15 C16 Ni16 -6.0(6) . . . . ? Ni17 Ni15 C16 Ni16 160.3(4) . . . . ? Ni11 Ni15 C16 Ni16 -58.3(8) . . . . ? Ni12 Ni15 C16 Ni16 48.3(10) . . . . ? Ni14 Ni15 C16 Ni16 93.3(4) . . . . ? C17 Ni16 C16 O16 4(3) . . . . ? C17' Ni16 C16 O16 -17(3) . . . . ? C24 Ni16 C16 O16 -175(2) . . . . ? C25 Ni16 C16 O16 179.3(16) . . . . ? Ni15 Ni16 C16 O16 179(2) . . . . ? Ni9 Ni16 C16 O16 -71(3) . . . . ? Ni8 Ni16 C16 O16 99(2) . . . . ? Ni10 Ni16 C16 O16 -126(2) . . . . ? Ni13 Ni16 C16 O16 98(2) . . . . ? C17 Ni16 C16 Ni15 -175.3(15) . . . . ? C17' Ni16 C16 Ni15 164(2) . . . . ? C24 Ni16 C16 Ni15 5.5(6) . . . . ? C25 Ni16 C16 Ni15 0.2(11) . . . . ? Ni9 Ni16 C16 Ni15 110.2(12) . . . . ? Ni8 Ni16 C16 Ni15 -79.9(9) . . . . ? Ni10 Ni16 C16 Ni15 54.9(5) . . . . ? Ni13 Ni16 C16 Ni15 -81.3(4) . . . . ? C17' Ni16 C17 O17 55(33) . . . . ? C16 Ni16 C17 O17 -36(37) . . . . ? C24 Ni16 C17 O17 142(34) . . . . ? C25 Ni16 C17 O17 147(36) . . . . ? Ni15 Ni16 C17 O17 -43(38) . . . . ? Ni9 Ni16 C17 O17 121(37) . . . . ? Ni8 Ni16 C17 O17 179(100) . . . . ? Ni10 Ni16 C17 O17 92(37) . . . . ? Ni13 Ni16 C17 O17 -124(37) . . . . ? C17 Ni16 C17' O17' -102(23) . . . . ? C16 Ni16 C17' O17' -9(19) . . . . ? C24 Ni16 C17' O17' 126(17) . . . . ? C25 Ni16 C17' O17' 159(18) . . . . ? Ni15 Ni16 C17' O17' 15(22) . . . . ? Ni9 Ni16 C17' O17' 151(20) . . . . ? Ni8 Ni16 C17' O17' -158(19) . . . . ? Ni10 Ni16 C17' O17' 110(19) . . . . ? Ni13 Ni16 C17' O17' -102(19) . . . . ? C17 Ni16 C17' Ni9 107(10) . . . . ? C16 Ni16 C17' Ni9 -160.2(8) . . . . ? C24 Ni16 C17' Ni9 -25(5) . . . . ? C25 Ni16 C17' Ni9 8(2) . . . . ? Ni15 Ni16 C17' Ni9 -136(3) . . . . ? Ni8 Ni16 C17' Ni9 51.0(12) . . . . ? Ni10 Ni16 C17' Ni9 -41.0(14) . . . . ? Ni13 Ni16 C17' Ni9 107.2(13) . . . . ? C9 Ni9 C17' O17' 25(6) . . . . ? C10 Ni9 C17' O17' -74(6) . . . . ? C25 Ni9 C17' O17' -177(6) . . . . ? Ni10 Ni9 C17' O17' -121(6) . . . . ? Ni16 Ni9 C17' O17' -169(8) . . . . ? Ni8 Ni9 C17' O17' 135(6) . . . . ? Ni3 Ni9 C17' O17' 163(4) . . . . ? C9 Ni9 C17' Ni16 -166(2) . . . . ? C10 Ni9 C17' Ni16 95(2) . . . . ? C25 Ni9 C17' Ni16 -8(2) . . . . ? Ni10 Ni9 C17' Ni16 48(2) . . . . ? Ni8 Ni9 C17' Ni16 -56.0(19) . . . . ? Ni3 Ni9 C17' Ni16 -28(4) . . . . ? C15 Ni14 C18 O18 -69(10) . . . . ? C23 Ni14 C18 O18 89(10) . . . . ? Ni13 Ni14 C18 O18 -62(10) . . . . ? Ni5 Ni14 C18 O18 74(10) . . . . ? Ni12 Ni14 C18 O18 140(10) . . . . ? Ni15 Ni14 C18 O18 -161(10) . . . . ? Ni17 Ni14 C18 O18 164(10) . . . . ? C16 Ni15 C19 O19 13(15) . . . . ? C24 Ni15 C19 O19 -135(9) . . . . ? Ni17 Ni15 C19 O19 175(17) . . . . ? Ni16 Ni15 C19 O19 5(19) . . . . ? Ni11 Ni15 C19 O19 -126(14) . . . . ? Ni12 Ni15 C19 O19 167(13) . . . . ? Ni14 Ni15 C19 O19 112(14) . . . . ? C20' Ni12 C20 O20 -119(27) . . . . ? C13 Ni12 C20 O20 -160(18) . . . . ? C23 Ni12 C20 O20 89(19) . . . . ? C24 Ni12 C20 O20 -43(20) . . . . ? Ni17 Ni12 C20 O20 -10(16) . . . . ? Ni4 Ni12 C20 O20 -117(17) . . . . ? Ni1 Ni12 C20 O20 151(17) . . . . ? Ni14 Ni12 C20 O20 55(18) . . . . ? Ni15 Ni12 C20 O20 -10(19) . . . . ? Ni11 Ni12 C20 O20 -69(18) . . . . ? Ni5 Ni12 C20 O20 112(18) . . . . ? C19 Ni15 Ni17 C21 17(4) . . . . ? C19' Ni15 Ni17 C21 10(2) . . . . ? C16 Ni15 Ni17 C21 48.1(19) . . . . ? C24 Ni15 Ni17 C21 -145.7(17) . . . . ? Ni16 Ni15 Ni17 C21 179.2(16) . . . . ? Ni11 Ni15 Ni17 C21 -104.9(17) . . . . ? Ni12 Ni15 Ni17 C21 -171.5(17) . . . . ? Ni14 Ni15 Ni17 C21 124.9(17) . . . . ? C19 Ni15 Ni17 C19' 8(5) . . . . ? C16 Ni15 Ni17 C19' 38.6(19) . . . . ? C24 Ni15 Ni17 C19' -155.2(18) . . . . ? Ni16 Ni15 Ni17 C19' 169.7(17) . . . . ? Ni11 Ni15 Ni17 C19' -114.4(17) . . . . ? Ni12 Ni15 Ni17 C19' 179.0(17) . . . . ? Ni14 Ni15 Ni17 C19' 115.4(17) . . . . ? C19 Ni15 Ni17 C20' 175(4) . . . . ? C19' Ni15 Ni17 C20' 167(2) . . . . ? C16 Ni15 Ni17 C20' -154.9(13) . . . . ? C24 Ni15 Ni17 C20' 11.4(11) . . . . ? Ni16 Ni15 Ni17 C20' -23.8(11) . . . . ? Ni11 Ni15 Ni17 C20' 52.2(10) . . . . ? Ni12 Ni15 Ni17 C20' -14.4(10) . . . . ? Ni14 Ni15 Ni17 C20' -78.1(10) . . . . ? C19 Ni15 Ni17 Ni12 -171(4) . . . . ? C19' Ni15 Ni17 Ni12 -179.0(17) . . . . ? C16 Ni15 Ni17 Ni12 -140.5(8) . . . . ? C24 Ni15 Ni17 Ni12 25.8(4) . . . . ? Ni16 Ni15 Ni17 Ni12 -9.4(4) . . . . ? Ni11 Ni15 Ni17 Ni12 66.59(8) . . . . ? Ni14 Ni15 Ni17 Ni12 -63.68(8) . . . . ? C19 Ni15 Ni17 Ni14 -107(4) . . . . ? C19' Ni15 Ni17 Ni14 -115.4(17) . . . . ? C16 Ni15 Ni17 Ni14 -76.8(8) . . . . ? C24 Ni15 Ni17 Ni14 89.5(4) . . . . ? Ni16 Ni15 Ni17 Ni14 54.3(4) . . . . ? Ni11 Ni15 Ni17 Ni14 130.27(8) . . . . ? Ni12 Ni15 Ni17 Ni14 63.68(8) . . . . ? C20 Ni12 Ni17 C21 -9(4) . . . . ? C20' Ni12 Ni17 C21 9(2) . . . . ? C13 Ni12 Ni17 C21 34.7(19) . . . . ? C23 Ni12 Ni17 C21 -118.8(18) . . . . ? C24 Ni12 Ni17 C21 149.6(18) . . . . ? Ni4 Ni12 Ni17 C21 101.8(17) . . . . ? Ni1 Ni12 Ni17 C21 -56.5(18) . . . . ? Ni14 Ni12 Ni17 C21 -116.6(17) . . . . ? Ni15 Ni12 Ni17 C21 171.0(18) . . . . ? Ni11 Ni12 Ni17 C21 107.6(17) . . . . ? Ni5 Ni12 Ni17 C21 -68.3(17) . . . . ? C20 Ni12 Ni17 C19' 179(4) . . . . ? C20' Ni12 Ni17 C19' -162.7(19) . . . . ? C13 Ni12 Ni17 C19' -137.1(16) . . . . ? C23 Ni12 Ni17 C19' 69.3(15) . . . . ? C24 Ni12 Ni17 C19' -22.2(15) . . . . ? Ni4 Ni12 Ni17 C19' -70.0(15) . . . . ? Ni1 Ni12 Ni17 C19' 131.7(15) . . . . ? Ni14 Ni12 Ni17 C19' 71.6(15) . . . . ? Ni15 Ni12 Ni17 C19' -0.8(14) . . . . ? Ni11 Ni12 Ni17 C19' -64.2(15) . . . . ? Ni5 Ni12 Ni17 C19' 119.9(15) . . . . ? C20 Ni12 Ni17 C20' -18(4) . . . . ? C13 Ni12 Ni17 C20' 25.6(14) . . . . ? C23 Ni12 Ni17 C20' -127.9(13) . . . . ? C24 Ni12 Ni17 C20' 140.5(13) . . . . ? Ni4 Ni12 Ni17 C20' 92.7(13) . . . . ? Ni1 Ni12 Ni17 C20' -65.6(13) . . . . ? Ni14 Ni12 Ni17 C20' -125.7(13) . . . . ? Ni15 Ni12 Ni17 C20' 161.9(13) . . . . ? Ni11 Ni12 Ni17 C20' 98.5(13) . . . . ? Ni5 Ni12 Ni17 C20' -77.4(13) . . . . ? C20 Ni12 Ni17 Ni15 180(3) . . . . ? C20' Ni12 Ni17 Ni15 -161.9(13) . . . . ? C13 Ni12 Ni17 Ni15 -136.3(7) . . . . ? C23 Ni12 Ni17 Ni15 70.1(4) . . . . ? C24 Ni12 Ni17 Ni15 -21.4(3) . . . . ? Ni4 Ni12 Ni17 Ni15 -69.23(14) . . . . ? Ni1 Ni12 Ni17 Ni15 132.5(3) . . . . ? Ni14 Ni12 Ni17 Ni15 72.40(9) . . . . ? Ni11 Ni12 Ni17 Ni15 -63.43(9) . . . . ? Ni5 Ni12 Ni17 Ni15 120.71(10) . . . . ? C20 Ni12 Ni17 Ni14 108(3) . . . . ? C20' Ni12 Ni17 Ni14 125.7(13) . . . . ? C13 Ni12 Ni17 Ni14 151.3(7) . . . . ? C23 Ni12 Ni17 Ni14 -2.3(4) . . . . ? C24 Ni12 Ni17 Ni14 -93.8(3) . . . . ? Ni4 Ni12 Ni17 Ni14 -141.63(12) . . . . ? Ni1 Ni12 Ni17 Ni14 60.1(3) . . . . ? Ni15 Ni12 Ni17 Ni14 -72.40(9) . . . . ? Ni11 Ni12 Ni17 Ni14 -135.84(9) . . . . ? Ni5 Ni12 Ni17 Ni14 48.31(8) . . . . ? C18 Ni14 Ni17 C21 -10.2(13) . . . . ? C15 Ni14 Ni17 C21 -93.8(14) . . . . ? C23 Ni14 Ni17 C21 142.1(13) . . . . ? Ni13 Ni14 Ni17 C21 -160.7(12) . . . . ? Ni5 Ni14 Ni17 C21 88.7(12) . . . . ? Ni12 Ni14 Ni17 C21 140.0(12) . . . . ? Ni15 Ni14 Ni17 C21 -141.6(12) . . . . ? C18 Ni14 Ni17 C19' 88.4(14) . . . . ? C15 Ni14 Ni17 C19' 4.8(14) . . . . ? C23 Ni14 Ni17 C19' -119.3(13) . . . . ? Ni13 Ni14 Ni17 C19' -62.1(13) . . . . ? Ni5 Ni14 Ni17 C19' -172.7(13) . . . . ? Ni12 Ni14 Ni17 C19' -121.5(13) . . . . ? Ni15 Ni14 Ni17 C19' -43.0(13) . . . . ? C18 Ni14 Ni17 C20' -113.2(10) . . . . ? C15 Ni14 Ni17 C20' 163.2(10) . . . . ? C23 Ni14 Ni17 C20' 39.1(9) . . . . ? Ni13 Ni14 Ni17 C20' 96.3(8) . . . . ? Ni5 Ni14 Ni17 C20' -14.3(8) . . . . ? Ni12 Ni14 Ni17 C20' 37.0(8) . . . . ? Ni15 Ni14 Ni17 C20' 115.4(8) . . . . ? C18 Ni14 Ni17 Ni15 131.4(5) . . . . ? C15 Ni14 Ni17 Ni15 47.8(7) . . . . ? C23 Ni14 Ni17 Ni15 -76.3(4) . . . . ? Ni13 Ni14 Ni17 Ni15 -19.10(15) . . . . ? Ni5 Ni14 Ni17 Ni15 -129.72(10) . . . . ? Ni12 Ni14 Ni17 Ni15 -78.48(10) . . . . ? C18 Ni14 Ni17 Ni12 -150.2(5) . . . . ? C15 Ni14 Ni17 Ni12 126.2(6) . . . . ? C23 Ni14 Ni17 Ni12 2.2(4) . . . . ? Ni13 Ni14 Ni17 Ni12 59.38(14) . . . . ? Ni5 Ni14 Ni17 Ni12 -51.24(9) . . . . ? Ni15 Ni14 Ni17 Ni12 78.48(10) . . . . ? C19' Ni17 C21 O21 -174(23) . . . . ? C20' Ni17 C21 O21 20(23) . . . . ? Ni15 Ni17 C21 O21 179(100) . . . . ? Ni12 Ni17 C21 O21 14(24) . . . . ? Ni14 Ni17 C21 O21 -78(23) . . . . ? C19 Ni15 C19' O19' 63(28) . . . . ? C16 Ni15 C19' O19' 35(8) . . . . ? C24 Ni15 C19' O19' -114(7) . . . . ? Ni17 Ni15 C19' O19' -167(9) . . . . ? Ni16 Ni15 C19' O19' 20(10) . . . . ? Ni11 Ni15 C19' O19' -104(8) . . . . ? Ni12 Ni15 C19' O19' -168(7) . . . . ? Ni14 Ni15 C19' O19' 136(8) . . . . ? C19 Ni15 C19' Ni17 -131(34) . . . . ? C16 Ni15 C19' Ni17 -158.4(10) . . . . ? C24 Ni15 C19' Ni17 53(4) . . . . ? Ni16 Ni15 C19' Ni17 -173.1(12) . . . . ? Ni11 Ni15 C19' Ni17 63.0(12) . . . . ? Ni12 Ni15 C19' Ni17 -0.9(15) . . . . ? Ni14 Ni15 C19' Ni17 -57.6(11) . . . . ? C21 Ni17 C19' O19' -1(4) . . . . ? C20' Ni17 C19' O19' 138(3) . . . . ? Ni15 Ni17 C19' O19' 173(5) . . . . ? Ni12 Ni17 C19' O19' 174(3) . . . . ? Ni14 Ni17 C19' O19' -133(4) . . . . ? C21 Ni17 C19' Ni15 -174.6(13) . . . . ? C20' Ni17 C19' Ni15 -36(4) . . . . ? Ni12 Ni17 C19' Ni15 1.0(18) . . . . ? Ni14 Ni17 C19' Ni15 54.0(11) . . . . ? C20 Ni12 C20' O20' -122(15) . . . . ? C13 Ni12 C20' O20' 16(4) . . . . ? C23 Ni12 C20' O20' -89(4) . . . . ? C24 Ni12 C20' O20' 120(4) . . . . ? Ni17 Ni12 C20' O20' 178(5) . . . . ? Ni4 Ni12 C20' O20' 59(5) . . . . ? Ni1 Ni12 C20' O20' -25(5) . . . . ? Ni14 Ni12 C20' O20' -129(4) . . . . ? Ni15 Ni12 C20' O20' 163(4) . . . . ? Ni11 Ni12 C20' O20' 107(4) . . . . ? Ni5 Ni12 C20' O20' -73(4) . . . . ? C20 Ni12 C20' Ni17 59(12) . . . . ? C13 Ni12 C20' Ni17 -161.9(10) . . . . ? C23 Ni12 C20' Ni17 92.8(14) . . . . ? C24 Ni12 C20' Ni17 -58.2(14) . . . . ? Ni4 Ni12 C20' Ni17 -119.1(6) . . . . ? Ni1 Ni12 C20' Ni17 156.6(4) . . . . ? Ni14 Ni12 C20' Ni17 52.5(10) . . . . ? Ni15 Ni12 C20' Ni17 -15.3(10) . . . . ? Ni11 Ni12 C20' Ni17 -70.9(8) . . . . ? Ni5 Ni12 C20' Ni17 108.5(8) . . . . ? C21 Ni17 C20' O20' 6(4) . . . . ? C19' Ni17 C20' O20' -132(4) . . . . ? Ni15 Ni17 C20' O20' -161(3) . . . . ? Ni12 Ni17 C20' O20' -179(4) . . . . ? Ni14 Ni17 C20' O20' 138(3) . . . . ? C21 Ni17 C20' Ni12 -175.0(12) . . . . ? C19' Ni17 C20' Ni12 47(4) . . . . ? Ni15 Ni17 C20' Ni12 18.0(13) . . . . ? Ni14 Ni17 C20' Ni12 -43.1(9) . . . . ? C26 Ni2 C22 C23 -166(3) . . . . ? C26' Ni2 C22 C23 -154(5) . . . . ? C2 Ni2 C22 C23 0.4(15) . . . . ? Ni1 Ni2 C22 C23 2.1(11) . . . . ? Ni18 Ni2 C22 C23 149.3(12) . . . . ? Ni8 Ni2 C22 C23 138.7(15) . . . . ? Ni7 Ni2 C22 C23 -142.4(15) . . . . ? Ni3 Ni2 C22 C23 94.3(13) . . . . ? C26 Ni2 C22 Ni8 55(3) . . . . ? C26' Ni2 C22 Ni8 68(5) . . . . ? C2 Ni2 C22 Ni8 -138.2(5) . . . . ? Ni1 Ni2 C22 Ni8 -136.5(5) . . . . ? Ni18 Ni2 C22 Ni8 10.6(4) . . . . ? Ni7 Ni2 C22 Ni8 78.9(4) . . . . ? Ni3 Ni2 C22 Ni8 -44.4(3) . . . . ? C26 Ni2 C22 Ni7 -24(3) . . . . ? C26' Ni2 C22 Ni7 -11(5) . . . . ? C2 Ni2 C22 Ni7 142.8(5) . . . . ? Ni1 Ni2 C22 Ni7 144.5(5) . . . . ? Ni18 Ni2 C22 Ni7 -68.3(4) . . . . ? Ni8 Ni2 C22 Ni7 -78.9(4) . . . . ? Ni3 Ni2 C22 Ni7 -123.3(3) . . . . ? C26 Ni2 C22 Ni6 -92(2) . . . . ? C26' Ni2 C22 Ni6 -80(5) . . . . ? C2 Ni2 C22 Ni6 74.2(6) . . . . ? Ni1 Ni2 C22 Ni6 75.9(4) . . . . ? Ni18 Ni2 C22 Ni6 -136.9(4) . . . . ? Ni8 Ni2 C22 Ni6 -147.6(7) . . . . ? Ni7 Ni2 C22 Ni6 -68.6(4) . . . . ? Ni3 Ni2 C22 Ni6 168.1(4) . . . . ? C26 Ni2 C22 Ni13 7(3) . . . . ? C26' Ni2 C22 Ni13 20(5) . . . . ? C2 Ni2 C22 Ni13 173.8(14) . . . . ? Ni1 Ni2 C22 Ni13 175.6(16) . . . . ? Ni18 Ni2 C22 Ni13 -37.3(15) . . . . ? Ni8 Ni2 C22 Ni13 -47.9(12) . . . . ? Ni7 Ni2 C22 Ni13 31.0(12) . . . . ? Ni3 Ni2 C22 Ni13 -92.3(14) . . . . ? C26 Ni2 C22 Ni1 -168(2) . . . . ? C26' Ni2 C22 Ni1 -156(5) . . . . ? C2 Ni2 C22 Ni1 -1.7(6) . . . . ? Ni18 Ni2 C22 Ni1 147.1(2) . . . . ? Ni8 Ni2 C22 Ni1 136.5(5) . . . . ? Ni7 Ni2 C22 Ni1 -144.5(5) . . . . ? Ni3 Ni2 C22 Ni1 92.2(2) . . . . ? C28' Ni8 C22 C23 126(3) . . . . ? C28 Ni8 C22 C23 156.3(14) . . . . ? C25 Ni8 C22 C23 -41.7(12) . . . . ? Ni18 Ni8 C22 C23 -155.7(10) . . . . ? Ni7 Ni8 C22 C23 133.8(13) . . . . ? Ni2 Ni8 C22 C23 -143.8(13) . . . . ? Ni9 Ni8 C22 C23 -38.8(14) . . . . ? Ni3 Ni8 C22 C23 -91.1(11) . . . . ? Ni13 Ni8 C22 C23 55.6(10) . . . . ? Ni16 Ni8 C22 C23 8.0(12) . . . . ? C28' Ni8 C22 Ni2 -91(3) . . . . ? C28 Ni8 C22 Ni2 -59.9(12) . . . . ? C25 Ni8 C22 Ni2 102.1(5) . . . . ? Ni18 Ni8 C22 Ni2 -11.9(5) . . . . ? Ni7 Ni8 C22 Ni2 -82.4(4) . . . . ? Ni9 Ni8 C22 Ni2 105.0(5) . . . . ? Ni3 Ni8 C22 Ni2 52.7(3) . . . . ? Ni13 Ni8 C22 Ni2 -160.6(6) . . . . ? Ni16 Ni8 C22 Ni2 151.8(3) . . . . ? C28' Ni8 C22 Ni7 -8(3) . . . . ? C28 Ni8 C22 Ni7 22.6(12) . . . . ? C25 Ni8 C22 Ni7 -175.5(4) . . . . ? Ni18 Ni8 C22 Ni7 70.6(4) . . . . ? Ni2 Ni8 C22 Ni7 82.4(4) . . . . ? Ni9 Ni8 C22 Ni7 -172.5(2) . . . . ? Ni3 Ni8 C22 Ni7 135.1(2) . . . . ? Ni13 Ni8 C22 Ni7 -78.1(4) . . . . ? Ni16 Ni8 C22 Ni7 -125.8(3) . . . . ? C28' Ni8 C22 Ni6 3(3) . . . . ? C28 Ni8 C22 Ni6 33.9(18) . . . . ? C25 Ni8 C22 Ni6 -164.2(12) . . . . ? Ni18 Ni8 C22 Ni6 81.9(12) . . . . ? Ni7 Ni8 C22 Ni6 11.3(9) . . . . ? Ni2 Ni8 C22 Ni6 93.7(12) . . . . ? Ni9 Ni8 C22 Ni6 -161.2(8) . . . . ? Ni3 Ni8 C22 Ni6 146.4(11) . . . . ? Ni13 Ni8 C22 Ni6 -66.8(11) . . . . ? Ni16 Ni8 C22 Ni6 -114.5(12) . . . . ? C28' Ni8 C22 Ni13 70(3) . . . . ? C28 Ni8 C22 Ni13 100.7(11) . . . . ? C25 Ni8 C22 Ni13 -97.4(4) . . . . ? Ni18 Ni8 C22 Ni13 148.7(3) . . . . ? Ni7 Ni8 C22 Ni13 78.1(4) . . . . ? Ni2 Ni8 C22 Ni13 160.6(6) . . . . ? Ni9 Ni8 C22 Ni13 -94.4(5) . . . . ? Ni3 Ni8 C22 Ni13 -146.7(3) . . . . ? Ni16 Ni8 C22 Ni13 -47.7(3) . . . . ? C28' Ni8 C22 Ni1 -144(3) . . . . ? C28 Ni8 C22 Ni1 -112.9(12) . . . . ? C25 Ni8 C22 Ni1 49.1(8) . . . . ? Ni18 Ni8 C22 Ni1 -64.8(8) . . . . ? Ni7 Ni8 C22 Ni1 -135.4(9) . . . . ? Ni2 Ni8 C22 Ni1 -53.0(5) . . . . ? Ni9 Ni8 C22 Ni1 52.1(10) . . . . ? Ni3 Ni8 C22 Ni1 -0.3(7) . . . . ? Ni13 Ni8 C22 Ni1 146.4(9) . . . . ? Ni16 Ni8 C22 Ni1 98.8(7) . . . . ? C8 Ni7 C22 C23 -165.8(17) . . . . ? C7 Ni7 C22 C23 45.9(13) . . . . ? Ni6 Ni7 C22 C23 41.0(10) . . . . ? Ni8 Ni7 C22 C23 -132.8(13) . . . . ? Ni13 Ni7 C22 C23 -47.3(10) . . . . ? Ni2 Ni7 C22 C23 146.3(13) . . . . ? C8 Ni7 C22 Ni2 47.8(18) . . . . ? C7 Ni7 C22 Ni2 -100.4(6) . . . . ? Ni6 Ni7 C22 Ni2 -105.4(4) . . . . ? Ni8 Ni7 C22 Ni2 80.9(4) . . . . ? Ni13 Ni7 C22 Ni2 166.4(5) . . . . ? C8 Ni7 C22 Ni8 -33.1(19) . . . . ? C7 Ni7 C22 Ni8 178.7(6) . . . . ? Ni6 Ni7 C22 Ni8 173.7(5) . . . . ? Ni13 Ni7 C22 Ni8 85.5(4) . . . . ? Ni2 Ni7 C22 Ni8 -80.9(4) . . . . ? C8 Ni7 C22 Ni6 153.2(17) . . . . ? C7 Ni7 C22 Ni6 4.9(7) . . . . ? Ni8 Ni7 C22 Ni6 -173.7(5) . . . . ? Ni13 Ni7 C22 Ni6 -88.3(3) . . . . ? Ni2 Ni7 C22 Ni6 105.4(4) . . . . ? C8 Ni7 C22 Ni13 -118.6(17) . . . . ? C7 Ni7 C22 Ni13 93.2(6) . . . . ? Ni6 Ni7 C22 Ni13 88.3(3) . . . . ? Ni8 Ni7 C22 Ni13 -85.5(4) . . . . ? Ni2 Ni7 C22 Ni13 -166.4(5) . . . . ? C8 Ni7 C22 Ni1 96.0(19) . . . . ? C7 Ni7 C22 Ni1 -52.3(10) . . . . ? Ni6 Ni7 C22 Ni1 -57.2(6) . . . . ? Ni8 Ni7 C22 Ni1 129.0(9) . . . . ? Ni13 Ni7 C22 Ni1 -145.5(9) . . . . ? Ni2 Ni7 C22 Ni1 48.2(6) . . . . ? C6 Ni6 C22 C23 40.4(16) . . . . ? C7 Ni6 C22 C23 -153.9(9) . . . . ? Ni7 Ni6 C22 C23 -148.4(8) . . . . ? Ni5 Ni6 C22 C23 26.5(6) . . . . ? Ni1 Ni6 C22 C23 69.7(6) . . . . ? Ni13 Ni6 C22 C23 -70.3(7) . . . . ? C6 Ni6 C22 Ni2 -95.5(14) . . . . ? C7 Ni6 C22 Ni2 70.3(8) . . . . ? C23 Ni6 C22 Ni2 -135.8(9) . . . . ? Ni7 Ni6 C22 Ni2 75.7(4) . . . . ? Ni5 Ni6 C22 Ni2 -109.3(4) . . . . ? Ni1 Ni6 C22 Ni2 -66.2(4) . . . . ? Ni13 Ni6 C22 Ni2 153.8(7) . . . . ? C6 Ni6 C22 Ni8 177.1(13) . . . . ? C7 Ni6 C22 Ni8 -17.1(14) . . . . ? C23 Ni6 C22 Ni8 136.8(16) . . . . ? Ni7 Ni6 C22 Ni8 -11.6(9) . . . . ? Ni5 Ni6 C22 Ni8 163.3(12) . . . . ? Ni1 Ni6 C22 Ni8 -153.5(14) . . . . ? Ni13 Ni6 C22 Ni8 66.5(11) . . . . ? C6 Ni6 C22 Ni7 -171.2(13) . . . . ? C7 Ni6 C22 Ni7 -5.4(7) . . . . ? C23 Ni6 C22 Ni7 148.4(8) . . . . ? Ni5 Ni6 C22 Ni7 175.0(3) . . . . ? Ni1 Ni6 C22 Ni7 -141.9(5) . . . . ? Ni13 Ni6 C22 Ni7 78.1(3) . . . . ? C6 Ni6 C22 Ni13 110.7(13) . . . . ? C7 Ni6 C22 Ni13 -83.6(7) . . . . ? C23 Ni6 C22 Ni13 70.3(7) . . . . ? Ni7 Ni6 C22 Ni13 -78.1(3) . . . . ? Ni5 Ni6 C22 Ni13 96.8(3) . . . . ? Ni1 Ni6 C22 Ni13 140.0(5) . . . . ? C6 Ni6 C22 Ni1 -29.3(15) . . . . ? C7 Ni6 C22 Ni1 136.5(7) . . . . ? C23 Ni6 C22 Ni1 -69.7(6) . . . . ? Ni7 Ni6 C22 Ni1 141.9(5) . . . . ? Ni5 Ni6 C22 Ni1 -43.2(3) . . . . ? Ni13 Ni6 C22 Ni1 -140.0(5) . . . . ? C14 Ni13 C22 C23 172.2(9) . . . . ? C15 Ni13 C22 C23 7.7(12) . . . . ? Ni14 Ni13 C22 C23 -0.6(7) . . . . ? Ni7 Ni13 C22 C23 143.8(8) . . . . ? Ni8 Ni13 C22 C23 -137.5(9) . . . . ? Ni6 Ni13 C22 C23 71.6(7) . . . . ? Ni16 Ni13 C22 C23 -95.1(7) . . . . ? C14 Ni13 C22 Ni2 -3.0(17) . . . . ? C15 Ni13 C22 Ni2 -167.5(13) . . . . ? C23 Ni13 C22 Ni2 -175.2(19) . . . . ? Ni14 Ni13 C22 Ni2 -175.8(14) . . . . ? Ni7 Ni13 C22 Ni2 -31.5(12) . . . . ? Ni8 Ni13 C22 Ni2 47.3(12) . . . . ? Ni6 Ni13 C22 Ni2 -103.6(15) . . . . ? Ni16 Ni13 C22 Ni2 89.7(14) . . . . ? C14 Ni13 C22 Ni8 -50.2(9) . . . . ? C15 Ni13 C22 Ni8 145.2(8) . . . . ? C23 Ni13 C22 Ni8 137.5(9) . . . . ? Ni14 Ni13 C22 Ni8 137.0(3) . . . . ? Ni7 Ni13 C22 Ni8 -78.7(4) . . . . ? Ni6 Ni13 C22 Ni8 -150.8(6) . . . . ? Ni16 Ni13 C22 Ni8 42.5(3) . . . . ? C14 Ni13 C22 Ni7 28.5(8) . . . . ? C15 Ni13 C22 Ni7 -136.0(9) . . . . ? C23 Ni13 C22 Ni7 -143.8(8) . . . . ? Ni14 Ni13 C22 Ni7 -144.3(3) . . . . ? Ni8 Ni13 C22 Ni7 78.7(4) . . . . ? Ni6 Ni13 C22 Ni7 -72.1(4) . . . . ? Ni16 Ni13 C22 Ni7 121.2(3) . . . . ? C14 Ni13 C22 Ni6 100.6(8) . . . . ? C15 Ni13 C22 Ni6 -63.9(10) . . . . ? C23 Ni13 C22 Ni6 -71.6(7) . . . . ? Ni14 Ni13 C22 Ni6 -72.2(3) . . . . ? Ni7 Ni13 C22 Ni6 72.1(4) . . . . ? Ni8 Ni13 C22 Ni6 150.8(6) . . . . ? Ni16 Ni13 C22 Ni6 -166.7(3) . . . . ? C14 Ni13 C22 Ni1 170.9(10) . . . . ? C15 Ni13 C22 Ni1 6.4(15) . . . . ? C23 Ni13 C22 Ni1 -1.3(7) . . . . ? Ni14 Ni13 C22 Ni1 -1.9(8) . . . . ? Ni7 Ni13 C22 Ni1 142.4(10) . . . . ? Ni8 Ni13 C22 Ni1 -138.9(11) . . . . ? Ni6 Ni13 C22 Ni1 70.3(8) . . . . ? Ni16 Ni13 C22 Ni1 -96.4(8) . . . . ? C2 Ni1 C22 C23 -176.7(8) . . . . ? C1 Ni1 C22 C23 -54.0(10) . . . . ? C13 Ni1 C22 C23 72.1(9) . . . . ? Ni2 Ni1 C22 C23 -178.4(8) . . . . ? Ni5 Ni1 C22 C23 -29.4(7) . . . . ? Ni12 Ni1 C22 C23 38.2(6) . . . . ? Ni6 Ni1 C22 C23 -72.7(7) . . . . ? C2 Ni1 C22 Ni2 1.7(5) . . . . ? C1 Ni1 C22 Ni2 124.4(7) . . . . ? C13 Ni1 C22 Ni2 -109.5(7) . . . . ? C23 Ni1 C22 Ni2 178.4(8) . . . . ? Ni5 Ni1 C22 Ni2 149.0(3) . . . . ? Ni12 Ni1 C22 Ni2 -143.4(3) . . . . ? Ni6 Ni1 C22 Ni2 105.7(4) . . . . ? C2 Ni1 C22 Ni8 59.0(8) . . . . ? C1 Ni1 C22 Ni8 -178.3(7) . . . . ? C13 Ni1 C22 Ni8 -52.2(10) . . . . ? C23 Ni1 C22 Ni8 -124.3(11) . . . . ? Ni2 Ni1 C22 Ni8 57.3(6) . . . . ? Ni5 Ni1 C22 Ni8 -153.7(7) . . . . ? Ni12 Ni1 C22 Ni8 -86.1(7) . . . . ? Ni6 Ni1 C22 Ni8 163.0(10) . . . . ? C2 Ni1 C22 Ni7 -50.3(9) . . . . ? C1 Ni1 C22 Ni7 72.4(11) . . . . ? C13 Ni1 C22 Ni7 -161.5(8) . . . . ? C23 Ni1 C22 Ni7 126.4(12) . . . . ? Ni2 Ni1 C22 Ni7 -52.0(6) . . . . ? Ni5 Ni1 C22 Ni7 97.0(7) . . . . ? Ni12 Ni1 C22 Ni7 164.6(8) . . . . ? Ni6 Ni1 C22 Ni7 53.7(6) . . . . ? C2 Ni1 C22 Ni6 -104.0(5) . . . . ? C1 Ni1 C22 Ni6 18.7(8) . . . . ? C13 Ni1 C22 Ni6 144.8(6) . . . . ? C23 Ni1 C22 Ni6 72.7(7) . . . . ? Ni2 Ni1 C22 Ni6 -105.7(4) . . . . ? Ni5 Ni1 C22 Ni6 43.3(3) . . . . ? Ni12 Ni1 C22 Ni6 110.9(3) . . . . ? C2 Ni1 C22 Ni13 -175.4(9) . . . . ? C1 Ni1 C22 Ni13 -52.7(12) . . . . ? C13 Ni1 C22 Ni13 73.4(11) . . . . ? C23 Ni1 C22 Ni13 1.3(7) . . . . ? Ni2 Ni1 C22 Ni13 -177.1(11) . . . . ? Ni5 Ni1 C22 Ni13 -28.1(8) . . . . ? Ni12 Ni1 C22 Ni13 39.5(8) . . . . ? Ni6 Ni1 C22 Ni13 -71.4(8) . . . . ? Ni2 C22 C23 Ni14 178.1(8) . . . . ? Ni8 C22 C23 Ni14 -60(2) . . . . ? Ni7 C22 C23 Ni14 51(2) . . . . ? Ni6 C22 C23 Ni14 92.1(15) . . . . ? Ni13 C22 C23 Ni14 1.2(14) . . . . ? Ni1 C22 C23 Ni14 -179.8(15) . . . . ? Ni2 C22 C23 Ni13 176.9(12) . . . . ? Ni8 C22 C23 Ni13 -60.9(9) . . . . ? Ni7 C22 C23 Ni13 49.8(9) . . . . ? Ni6 C22 C23 Ni13 90.9(4) . . . . ? Ni1 C22 C23 Ni13 179.0(5) . . . . ? Ni2 C22 C23 Ni6 85.9(12) . . . . ? Ni8 C22 C23 Ni6 -151.9(10) . . . . ? Ni7 C22 C23 Ni6 -41.1(9) . . . . ? Ni13 C22 C23 Ni6 -90.9(4) . . . . ? Ni1 C22 C23 Ni6 88.1(3) . . . . ? Ni2 C22 C23 Ni12 -62.0(16) . . . . ? Ni8 C22 C23 Ni12 60.1(14) . . . . ? Ni7 C22 C23 Ni12 170.9(6) . . . . ? Ni6 C22 C23 Ni12 -148.0(8) . . . . ? Ni13 C22 C23 Ni12 121.1(8) . . . . ? Ni1 C22 C23 Ni12 -59.9(7) . . . . ? Ni2 C22 C23 Ni1 -2.2(11) . . . . ? Ni8 C22 C23 Ni1 120.0(10) . . . . ? Ni7 C22 C23 Ni1 -129.2(10) . . . . ? Ni6 C22 C23 Ni1 -88.1(3) . . . . ? Ni13 C22 C23 Ni1 -179.0(5) . . . . ? Ni2 C22 C23 Ni5 44.5(18) . . . . ? Ni8 C22 C23 Ni5 166.6(6) . . . . ? Ni7 C22 C23 Ni5 -82.6(14) . . . . ? Ni6 C22 C23 Ni5 -41.5(9) . . . . ? Ni13 C22 C23 Ni5 -132.4(10) . . . . ? Ni1 C22 C23 Ni5 46.6(9) . . . . ? C18 Ni14 C23 C22 -164.1(15) . . . . ? C15 Ni14 C23 C22 -7.2(17) . . . . ? Ni13 Ni14 C23 C22 -1.2(14) . . . . ? Ni5 Ni14 C23 C22 -145.0(17) . . . . ? Ni12 Ni14 C23 C22 131.3(17) . . . . ? Ni15 Ni14 C23 C22 83.2(15) . . . . ? Ni17 Ni14 C23 C22 129.2(15) . . . . ? C18 Ni14 C23 Ni13 -163.0(12) . . . . ? C15 Ni14 C23 Ni13 -6.0(6) . . . . ? Ni5 Ni14 C23 Ni13 -143.9(5) . . . . ? Ni12 Ni14 C23 Ni13 132.5(5) . . . . ? Ni15 Ni14 C23 Ni13 84.3(2) . . . . ? Ni17 Ni14 C23 Ni13 130.3(2) . . . . ? C18 Ni14 C23 Ni6 -84.6(13) . . . . ? C15 Ni14 C23 Ni6 72.4(7) . . . . ? Ni13 Ni14 C23 Ni6 78.4(5) . . . . ? Ni5 Ni14 C23 Ni6 -65.5(4) . . . . ? Ni12 Ni14 C23 Ni6 -149.1(7) . . . . ? Ni15 Ni14 C23 Ni6 162.7(4) . . . . ? Ni17 Ni14 C23 Ni6 -151.3(4) . . . . ? C18 Ni14 C23 Ni12 64.6(13) . . . . ? C15 Ni14 C23 Ni12 -138.5(6) . . . . ? Ni13 Ni14 C23 Ni12 -132.5(5) . . . . ? Ni5 Ni14 C23 Ni12 83.7(4) . . . . ? Ni15 Ni14 C23 Ni12 -48.1(3) . . . . ? Ni17 Ni14 C23 Ni12 -2.1(3) . . . . ? C18 Ni14 C23 Ni1 16.2(19) . . . . ? C15 Ni14 C23 Ni1 173.2(10) . . . . ? Ni13 Ni14 C23 Ni1 179.2(12) . . . . ? Ni5 Ni14 C23 Ni1 35.3(8) . . . . ? Ni12 Ni14 C23 Ni1 -48.3(8) . . . . ? Ni15 Ni14 C23 Ni1 -96.5(10) . . . . ? Ni17 Ni14 C23 Ni1 -50.5(10) . . . . ? C18 Ni14 C23 Ni5 -19.1(14) . . . . ? C15 Ni14 C23 Ni5 137.9(6) . . . . ? Ni13 Ni14 C23 Ni5 143.9(5) . . . . ? Ni12 Ni14 C23 Ni5 -83.7(4) . . . . ? Ni15 Ni14 C23 Ni5 -131.8(3) . . . . ? Ni17 Ni14 C23 Ni5 -85.8(3) . . . . ? C14 Ni13 C23 C22 -18(2) . . . . ? C15 Ni13 C23 C22 -174.9(8) . . . . ? Ni14 Ni13 C23 C22 179.3(8) . . . . ? Ni7 Ni13 C23 C22 -27.2(6) . . . . ? Ni8 Ni13 C23 C22 30.2(6) . . . . ? Ni6 Ni13 C23 C22 -70.7(7) . . . . ? Ni16 Ni13 C23 C22 86.1(7) . . . . ? C14 Ni13 C23 Ni14 162.3(18) . . . . ? C15 Ni13 C23 Ni14 5.8(6) . . . . ? C22 Ni13 C23 Ni14 -179.3(8) . . . . ? Ni7 Ni13 C23 Ni14 153.5(3) . . . . ? Ni8 Ni13 C23 Ni14 -149.0(3) . . . . ? Ni6 Ni13 C23 Ni14 110.0(5) . . . . ? Ni16 Ni13 C23 Ni14 -93.2(3) . . . . ? C14 Ni13 C23 Ni6 52.3(19) . . . . ? C15 Ni13 C23 Ni6 -104.2(6) . . . . ? C22 Ni13 C23 Ni6 70.7(7) . . . . ? Ni14 Ni13 C23 Ni6 -110.0(5) . . . . ? Ni7 Ni13 C23 Ni6 43.5(3) . . . . ? Ni8 Ni13 C23 Ni6 101.0(3) . . . . ? Ni16 Ni13 C23 Ni6 156.8(3) . . . . ? C14 Ni13 C23 Ni12 -134.2(18) . . . . ? C15 Ni13 C23 Ni12 69.2(8) . . . . ? C22 Ni13 C23 Ni12 -115.8(10) . . . . ? Ni14 Ni13 C23 Ni12 63.4(6) . . . . ? Ni7 Ni13 C23 Ni12 -143.0(7) . . . . ? Ni8 Ni13 C23 Ni12 -85.6(6) . . . . ? Ni6 Ni13 C23 Ni12 173.4(9) . . . . ? Ni16 Ni13 C23 Ni12 -29.7(7) . . . . ? C14 Ni13 C23 Ni1 -17(2) . . . . ? C15 Ni13 C23 Ni1 -173.3(11) . . . . ? C22 Ni13 C23 Ni1 1.6(8) . . . . ? Ni14 Ni13 C23 Ni1 -179.1(13) . . . . ? Ni7 Ni13 C23 Ni1 -25.6(10) . . . . ? Ni8 Ni13 C23 Ni1 31.8(10) . . . . ? Ni6 Ni13 C23 Ni1 -69.1(10) . . . . ? Ni16 Ni13 C23 Ni1 87.7(10) . . . . ? C14 Ni13 C23 Ni5 108.6(19) . . . . ? C15 Ni13 C23 Ni5 -47.9(10) . . . . ? C22 Ni13 C23 Ni5 127.0(12) . . . . ? Ni14 Ni13 C23 Ni5 -53.7(7) . . . . ? Ni7 Ni13 C23 Ni5 99.8(8) . . . . ? Ni8 Ni13 C23 Ni5 157.2(9) . . . . ? Ni6 Ni13 C23 Ni5 56.3(7) . . . . ? Ni16 Ni13 C23 Ni5 -146.9(8) . . . . ? C6 Ni6 C23 C22 -159.7(8) . . . . ? C7 Ni6 C23 C22 41.0(13) . . . . ? Ni7 Ni6 C23 C22 24.9(6) . . . . ? Ni5 Ni6 C23 C22 -147.0(8) . . . . ? Ni1 Ni6 C23 C22 -75.5(7) . . . . ? Ni13 Ni6 C23 C22 72.3(7) . . . . ? C6 Ni6 C23 Ni14 58.5(8) . . . . ? C7 Ni6 C23 Ni14 -100.9(11) . . . . ? C22 Ni6 C23 Ni14 -141.8(10) . . . . ? Ni7 Ni6 C23 Ni14 -116.9(5) . . . . ? Ni5 Ni6 C23 Ni14 71.2(5) . . . . ? Ni1 Ni6 C23 Ni14 142.7(7) . . . . ? Ni13 Ni6 C23 Ni14 -69.5(4) . . . . ? C6 Ni6 C23 Ni13 128.0(7) . . . . ? C7 Ni6 C23 Ni13 -31.4(12) . . . . ? C22 Ni6 C23 Ni13 -72.3(7) . . . . ? Ni7 Ni6 C23 Ni13 -47.4(3) . . . . ? Ni5 Ni6 C23 Ni13 140.7(5) . . . . ? Ni1 Ni6 C23 Ni13 -147.8(6) . . . . ? C6 Ni6 C23 Ni12 -41.6(14) . . . . ? C7 Ni6 C23 Ni12 159.1(12) . . . . ? C22 Ni6 C23 Ni12 118.1(15) . . . . ? Ni7 Ni6 C23 Ni12 143.0(12) . . . . ? Ni5 Ni6 C23 Ni12 -28.9(10) . . . . ? Ni1 Ni6 C23 Ni12 42.7(10) . . . . ? Ni13 Ni6 C23 Ni12 -169.6(15) . . . . ? C6 Ni6 C23 Ni1 -84.2(7) . . . . ? C7 Ni6 C23 Ni1 116.4(10) . . . . ? C22 Ni6 C23 Ni1 75.5(7) . . . . ? Ni7 Ni6 C23 Ni1 100.4(3) . . . . ? Ni5 Ni6 C23 Ni1 -71.5(3) . . . . ? Ni13 Ni6 C23 Ni1 147.8(6) . . . . ? C6 Ni6 C23 Ni5 -12.7(7) . . . . ? C7 Ni6 C23 Ni5 -172.1(10) . . . . ? C22 Ni6 C23 Ni5 147.0(8) . . . . ? Ni7 Ni6 C23 Ni5 171.9(2) . . . . ? Ni1 Ni6 C23 Ni5 71.5(3) . . . . ? Ni13 Ni6 C23 Ni5 -140.7(5) . . . . ? C20 Ni12 C23 C22 162(3) . . . . ? C20' Ni12 C23 C22 152.3(15) . . . . ? C13 Ni12 C23 C22 53.3(11) . . . . ? C24 Ni12 C23 C22 -48.9(10) . . . . ? Ni17 Ni12 C23 C22 -145.8(8) . . . . ? Ni4 Ni12 C23 C22 1.9(10) . . . . ? Ni1 Ni12 C23 C22 59.6(9) . . . . ? Ni14 Ni12 C23 C22 -148.7(12) . . . . ? Ni15 Ni12 C23 C22 -95.0(9) . . . . ? Ni11 Ni12 C23 C22 -51.6(11) . . . . ? Ni5 Ni12 C23 C22 131.3(11) . . . . ? C20 Ni12 C23 Ni14 -49(3) . . . . ? C20' Ni12 C23 Ni14 -59.0(14) . . . . ? C13 Ni12 C23 Ni14 -158.0(5) . . . . ? C24 Ni12 C23 Ni14 99.8(4) . . . . ? Ni17 Ni12 C23 Ni14 2.9(5) . . . . ? Ni4 Ni12 C23 Ni14 150.6(2) . . . . ? Ni1 Ni12 C23 Ni14 -151.7(5) . . . . ? Ni15 Ni12 C23 Ni14 53.7(3) . . . . ? Ni11 Ni12 C23 Ni14 97.1(4) . . . . ? Ni5 Ni12 C23 Ni14 -80.0(4) . . . . ? C20 Ni12 C23 Ni13 -109(3) . . . . ? C20' Ni12 C23 Ni13 -118.8(14) . . . . ? C13 Ni12 C23 Ni13 142.3(7) . . . . ? C24 Ni12 C23 Ni13 40.0(7) . . . . ? Ni17 Ni12 C23 Ni13 -56.9(7) . . . . ? Ni4 Ni12 C23 Ni13 90.8(6) . . . . ? Ni1 Ni12 C23 Ni13 148.6(8) . . . . ? Ni14 Ni12 C23 Ni13 -59.8(6) . . . . ? Ni15 Ni12 C23 Ni13 -6.1(6) . . . . ? Ni11 Ni12 C23 Ni13 37.3(9) . . . . ? Ni5 Ni12 C23 Ni13 -139.8(9) . . . . ? C20 Ni12 C23 Ni6 58(3) . . . . ? C20' Ni12 C23 Ni6 48.4(19) . . . . ? C13 Ni12 C23 Ni6 -50.6(13) . . . . ? C24 Ni12 C23 Ni6 -152.8(12) . . . . ? Ni17 Ni12 C23 Ni6 110.3(11) . . . . ? Ni4 Ni12 C23 Ni6 -102.0(12) . . . . ? Ni1 Ni12 C23 Ni6 -44.3(10) . . . . ? Ni14 Ni12 C23 Ni6 107.4(13) . . . . ? Ni15 Ni12 C23 Ni6 161.1(12) . . . . ? Ni11 Ni12 C23 Ni6 -155.5(9) . . . . ? Ni5 Ni12 C23 Ni6 27.4(9) . . . . ? C20 Ni12 C23 Ni1 102(3) . . . . ? C20' Ni12 C23 Ni1 92.6(13) . . . . ? C13 Ni12 C23 Ni1 -6.3(6) . . . . ? C24 Ni12 C23 Ni1 -108.5(4) . . . . ? Ni17 Ni12 C23 Ni1 154.58(18) . . . . ? Ni4 Ni12 C23 Ni1 -57.7(3) . . . . ? Ni14 Ni12 C23 Ni1 151.7(5) . . . . ? Ni15 Ni12 C23 Ni1 -154.7(2) . . . . ? Ni11 Ni12 C23 Ni1 -111.2(3) . . . . ? Ni5 Ni12 C23 Ni1 71.6(3) . . . . ? C20 Ni12 C23 Ni5 31(3) . . . . ? C20' Ni12 C23 Ni5 21.0(14) . . . . ? C13 Ni12 C23 Ni5 -77.9(6) . . . . ? C24 Ni12 C23 Ni5 179.8(4) . . . . ? Ni17 Ni12 C23 Ni5 83.0(4) . . . . ? Ni4 Ni12 C23 Ni5 -129.3(2) . . . . ? Ni1 Ni12 C23 Ni5 -71.6(3) . . . . ? Ni14 Ni12 C23 Ni5 80.0(4) . . . . ? Ni15 Ni12 C23 Ni5 133.7(3) . . . . ? Ni11 Ni12 C23 Ni5 177.15(14) . . . . ? C2 Ni1 C23 C22 5.1(12) . . . . ? C1 Ni1 C23 C22 141.9(8) . . . . ? C13 Ni1 C23 C22 -123.4(8) . . . . ? Ni2 Ni1 C23 C22 1.3(7) . . . . ? Ni5 Ni1 C23 C22 143.2(8) . . . . ? Ni12 Ni1 C23 C22 -129.9(8) . . . . ? Ni6 Ni1 C23 C22 71.2(7) . . . . ? C2 Ni1 C23 Ni14 -175.2(9) . . . . ? C1 Ni1 C23 Ni14 -38.3(12) . . . . ? C13 Ni1 C23 Ni14 56.4(12) . . . . ? C22 Ni1 C23 Ni14 179.8(15) . . . . ? Ni2 Ni1 C23 Ni14 -179.0(10) . . . . ? Ni5 Ni1 C23 Ni14 -37.1(8) . . . . ? Ni12 Ni1 C23 Ni14 49.9(9) . . . . ? Ni6 Ni1 C23 Ni14 -109.0(11) . . . . ? C2 Ni1 C23 Ni13 3.5(16) . . . . ? C1 Ni1 C23 Ni13 140.3(11) . . . . ? C13 Ni1 C23 Ni13 -125.0(11) . . . . ? C22 Ni1 C23 Ni13 -1.6(8) . . . . ? Ni2 Ni1 C23 Ni13 -0.4(11) . . . . ? Ni5 Ni1 C23 Ni13 141.5(12) . . . . ? Ni12 Ni1 C23 Ni13 -131.5(12) . . . . ? Ni6 Ni1 C23 Ni13 69.6(10) . . . . ? C2 Ni1 C23 Ni6 -66.2(9) . . . . ? C1 Ni1 C23 Ni6 70.7(6) . . . . ? C13 Ni1 C23 Ni6 165.4(5) . . . . ? C22 Ni1 C23 Ni6 -71.2(7) . . . . ? Ni2 Ni1 C23 Ni6 -70.0(3) . . . . ? Ni5 Ni1 C23 Ni6 71.9(3) . . . . ? Ni12 Ni1 C23 Ni6 158.8(5) . . . . ? C2 Ni1 C23 Ni12 135.0(7) . . . . ? C1 Ni1 C23 Ni12 -88.1(6) . . . . ? C13 Ni1 C23 Ni12 6.6(6) . . . . ? C22 Ni1 C23 Ni12 129.9(8) . . . . ? Ni2 Ni1 C23 Ni12 131.2(3) . . . . ? Ni5 Ni1 C23 Ni12 -86.9(3) . . . . ? Ni6 Ni1 C23 Ni12 -158.8(5) . . . . ? C2 Ni1 C23 Ni5 -138.1(7) . . . . ? C1 Ni1 C23 Ni5 -1.2(6) . . . . ? C13 Ni1 C23 Ni5 93.5(6) . . . . ? C22 Ni1 C23 Ni5 -143.2(8) . . . . ? Ni2 Ni1 C23 Ni5 -141.9(2) . . . . ? Ni12 Ni1 C23 Ni5 86.9(3) . . . . ? Ni6 Ni1 C23 Ni5 -71.9(3) . . . . ? C5 Ni5 C23 C22 165.9(12) . . . . ? C1 Ni5 C23 C22 -46.7(12) . . . . ? C6 Ni5 C23 C22 50.0(12) . . . . ? Ni1 Ni5 C23 C22 -47.9(10) . . . . ? Ni6 Ni5 C23 C22 41.3(10) . . . . ? Ni14 Ni5 C23 C22 154.2(13) . . . . ? Ni12 Ni5 C23 C22 -124.2(12) . . . . ? C5 Ni5 C23 Ni14 11.7(12) . . . . ? C1 Ni5 C23 Ni14 159.1(6) . . . . ? C6 Ni5 C23 Ni14 -104.1(5) . . . . ? Ni1 Ni5 C23 Ni14 157.9(5) . . . . ? Ni6 Ni5 C23 Ni14 -112.9(4) . . . . ? Ni12 Ni5 C23 Ni14 81.6(4) . . . . ? C5 Ni5 C23 Ni13 63.2(14) . . . . ? C1 Ni5 C23 Ni13 -149.4(9) . . . . ? C6 Ni5 C23 Ni13 -52.7(9) . . . . ? Ni1 Ni5 C23 Ni13 -150.6(10) . . . . ? Ni6 Ni5 C23 Ni13 -61.4(7) . . . . ? Ni14 Ni5 C23 Ni13 51.5(6) . . . . ? Ni12 Ni5 C23 Ni13 133.1(10) . . . . ? C5 Ni5 C23 Ni6 124.6(10) . . . . ? C1 Ni5 C23 Ni6 -88.0(6) . . . . ? C6 Ni5 C23 Ni6 8.7(5) . . . . ? Ni1 Ni5 C23 Ni6 -89.2(3) . . . . ? Ni14 Ni5 C23 Ni6 112.9(4) . . . . ? Ni12 Ni5 C23 Ni6 -165.5(5) . . . . ? C5 Ni5 C23 Ni12 -69.9(11) . . . . ? C1 Ni5 C23 Ni12 77.5(6) . . . . ? C6 Ni5 C23 Ni12 174.2(5) . . . . ? Ni1 Ni5 C23 Ni12 76.3(3) . . . . ? Ni6 Ni5 C23 Ni12 165.5(5) . . . . ? Ni14 Ni5 C23 Ni12 -81.6(4) . . . . ? C5 Ni5 C23 Ni1 -146.2(10) . . . . ? C1 Ni5 C23 Ni1 1.2(6) . . . . ? C6 Ni5 C23 Ni1 98.0(5) . . . . ? Ni6 Ni5 C23 Ni1 89.2(3) . . . . ? Ni14 Ni5 C23 Ni1 -157.9(5) . . . . ? Ni12 Ni5 C23 Ni1 -76.3(3) . . . . ? C19 Ni15 C24 C25 170(10) . . . . ? C19' Ni15 C24 C25 171(3) . . . . ? C16 Ni15 C24 C25 23.3(17) . . . . ? Ni17 Ni15 C24 C25 -148.3(15) . . . . ? Ni16 Ni15 C24 C25 17.7(14) . . . . ? Ni11 Ni15 C24 C25 158.0(18) . . . . ? Ni12 Ni15 C24 C25 -121.9(17) . . . . ? Ni14 Ni15 C24 C25 -78.9(15) . . . . ? C19 Ni15 C24 Ni16 152(10) . . . . ? C19' Ni15 C24 Ni16 153(3) . . . . ? C16 Ni15 C24 Ni16 5.6(6) . . . . ? Ni17 Ni15 C24 Ni16 -166.03(19) . . . . ? Ni11 Ni15 C24 Ni16 140.3(5) . . . . ? Ni12 Ni15 C24 Ni16 -139.6(4) . . . . ? Ni14 Ni15 C24 Ni16 -96.6(2) . . . . ? C19 Ni15 C24 Ni11 12(10) . . . . ? C19' Ni15 C24 Ni11 13(3) . . . . ? C16 Ni15 C24 Ni11 -134.7(5) . . . . ? Ni17 Ni15 C24 Ni11 53.7(4) . . . . ? Ni16 Ni15 C24 Ni11 -140.3(5) . . . . ? Ni12 Ni15 C24 Ni11 80.1(4) . . . . ? Ni14 Ni15 C24 Ni11 123.1(3) . . . . ? C19 Ni15 C24 Ni10 78(10) . . . . ? C19' Ni15 C24 Ni10 79(3) . . . . ? C16 Ni15 C24 Ni10 -68.6(8) . . . . ? Ni17 Ni15 C24 Ni10 119.7(5) . . . . ? Ni16 Ni15 C24 Ni10 -74.3(5) . . . . ? Ni11 Ni15 C24 Ni10 66.1(5) . . . . ? Ni12 Ni15 C24 Ni10 146.1(8) . . . . ? Ni14 Ni15 C24 Ni10 -170.8(5) . . . . ? C19 Ni15 C24 Ni4 -31(10) . . . . ? C19' Ni15 C24 Ni4 -30(3) . . . . ? C16 Ni15 C24 Ni4 -177.4(10) . . . . ? Ni17 Ni15 C24 Ni4 10.9(11) . . . . ? Ni16 Ni15 C24 Ni4 177.0(12) . . . . ? Ni11 Ni15 C24 Ni4 -42.7(8) . . . . ? Ni12 Ni15 C24 Ni4 37.3(8) . . . . ? Ni14 Ni15 C24 Ni4 80.4(10) . . . . ? C19 Ni15 C24 Ni12 -69(10) . . . . ? C19' Ni15 C24 Ni12 -67(3) . . . . ? C16 Ni15 C24 Ni12 145.3(5) . . . . ? Ni17 Ni15 C24 Ni12 -26.4(4) . . . . ? Ni16 Ni15 C24 Ni12 139.6(4) . . . . ? Ni11 Ni15 C24 Ni12 -80.1(4) . . . . ? Ni14 Ni15 C24 Ni12 43.0(3) . . . . ? C17 Ni16 C24 C25 7(4) . . . . ? C17' Ni16 C24 C25 50(5) . . . . ? C16 Ni16 C24 C25 -174.6(8) . . . . ? Ni15 Ni16 C24 C25 -169.1(8) . . . . ? Ni9 Ni16 C24 C25 27.6(6) . . . . ? Ni8 Ni16 C24 C25 -30.6(6) . . . . ? Ni10 Ni16 C24 C25 71.7(7) . . . . ? Ni13 Ni16 C24 C25 -87.3(6) . . . . ? C17 Ni16 C24 Ni15 177(4) . . . . ? C17' Ni16 C24 Ni15 -140(5) . . . . ? C16 Ni16 C24 Ni15 -5.5(6) . . . . ? C25 Ni16 C24 Ni15 169.1(8) . . . . ? Ni9 Ni16 C24 Ni15 -163.3(3) . . . . ? Ni8 Ni16 C24 Ni15 138.5(3) . . . . ? Ni10 Ni16 C24 Ni15 -119.1(5) . . . . ? Ni13 Ni16 C24 Ni15 81.8(3) . . . . ? C17 Ni16 C24 Ni11 -125(4) . . . . ? C17' Ni16 C24 Ni11 -81(5) . . . . ? C16 Ni16 C24 Ni11 53.5(10) . . . . ? C25 Ni16 C24 Ni11 -131.9(12) . . . . ? Ni15 Ni16 C24 Ni11 59.0(7) . . . . ? Ni9 Ni16 C24 Ni11 -104.3(8) . . . . ? Ni8 Ni16 C24 Ni11 -162.5(9) . . . . ? Ni10 Ni16 C24 Ni11 -60.2(7) . . . . ? Ni13 Ni16 C24 Ni11 140.8(8) . . . . ? C17 Ni16 C24 Ni10 -64(4) . . . . ? C17' Ni16 C24 Ni10 -21(5) . . . . ? C16 Ni16 C24 Ni10 113.6(6) . . . . ? C25 Ni16 C24 Ni10 -71.7(7) . . . . ? Ni15 Ni16 C24 Ni10 119.1(5) . . . . ? Ni9 Ni16 C24 Ni10 -44.2(3) . . . . ? Ni8 Ni16 C24 Ni10 -102.4(3) . . . . ? Ni13 Ni16 C24 Ni10 -159.0(3) . . . . ? C17 Ni16 C24 Ni4 0(4) . . . . ? C17' Ni16 C24 Ni4 43(5) . . . . ? C16 Ni16 C24 Ni4 177.8(11) . . . . ? C25 Ni16 C24 Ni4 -7.5(8) . . . . ? Ni15 Ni16 C24 Ni4 -176.7(13) . . . . ? Ni9 Ni16 C24 Ni4 20.0(10) . . . . ? Ni8 Ni16 C24 Ni4 -38.2(10) . . . . ? Ni10 Ni16 C24 Ni4 64.2(10) . . . . ? Ni13 Ni16 C24 Ni4 -94.8(10) . . . . ? C17 Ni16 C24 Ni12 120(4) . . . . ? C17' Ni16 C24 Ni12 163(5) . . . . ? C16 Ni16 C24 Ni12 -61.7(9) . . . . ? C25 Ni16 C24 Ni12 113.0(11) . . . . ? Ni15 Ni16 C24 Ni12 -56.2(6) . . . . ? Ni9 Ni16 C24 Ni12 140.5(7) . . . . ? Ni8 Ni16 C24 Ni12 82.3(7) . . . . ? Ni10 Ni16 C24 Ni12 -175.3(10) . . . . ? Ni13 Ni16 C24 Ni12 25.7(7) . . . . ? C12 Ni11 C24 C25 -159.7(14) . . . . ? C4 Ni11 C24 C25 38.3(14) . . . . ? C11 Ni11 C24 C25 -52.2(12) . . . . ? Ni4 Ni11 C24 C25 43.7(10) . . . . ? Ni10 Ni11 C24 C25 -42.4(10) . . . . ? Ni15 Ni11 C24 C25 -162.6(14) . . . . ? Ni12 Ni11 C24 C25 117.9(13) . . . . ? C12 Ni11 C24 Ni15 2.9(14) . . . . ? C4 Ni11 C24 Ni15 -159.0(6) . . . . ? C11 Ni11 C24 Ni15 110.4(5) . . . . ? Ni4 Ni11 C24 Ni15 -153.7(5) . . . . ? Ni10 Ni11 C24 Ni15 120.3(5) . . . . ? Ni12 Ni11 C24 Ni15 -79.5(4) . . . . ? C12 Ni11 C24 Ni16 -52.8(16) . . . . ? C4 Ni11 C24 Ni16 145.3(9) . . . . ? C11 Ni11 C24 Ni16 54.7(9) . . . . ? Ni4 Ni11 C24 Ni16 150.6(10) . . . . ? Ni10 Ni11 C24 Ni16 64.6(7) . . . . ? Ni15 Ni11 C24 Ni16 -55.7(7) . . . . ? Ni12 Ni11 C24 Ni16 -135.2(10) . . . . ? C12 Ni11 C24 Ni10 -117.4(12) . . . . ? C4 Ni11 C24 Ni10 80.7(6) . . . . ? C11 Ni11 C24 Ni10 -9.8(5) . . . . ? Ni4 Ni11 C24 Ni10 86.1(3) . . . . ? Ni15 Ni11 C24 Ni10 -120.3(5) . . . . ? Ni12 Ni11 C24 Ni10 160.3(5) . . . . ? C12 Ni11 C24 Ni4 156.6(12) . . . . ? C4 Ni11 C24 Ni4 -5.3(7) . . . . ? C11 Ni11 C24 Ni4 -95.9(4) . . . . ? Ni10 Ni11 C24 Ni4 -86.1(3) . . . . ? Ni15 Ni11 C24 Ni4 153.7(5) . . . . ? Ni12 Ni11 C24 Ni4 74.2(3) . . . . ? C12 Ni11 C24 Ni12 82.4(13) . . . . ? C4 Ni11 C24 Ni12 -79.6(7) . . . . ? C11 Ni11 C24 Ni12 -170.1(4) . . . . ? Ni4 Ni11 C24 Ni12 -74.2(3) . . . . ? Ni10 Ni11 C24 Ni12 -160.3(5) . . . . ? Ni15 Ni11 C24 Ni12 79.5(4) . . . . ? C11 Ni10 C24 C25 163.2(8) . . . . ? C10 Ni10 C24 C25 -30.4(14) . . . . ? Ni9 Ni10 C24 C25 -26.1(6) . . . . ? Ni11 Ni10 C24 C25 148.0(8) . . . . ? Ni4 Ni10 C24 C25 75.2(7) . . . . ? Ni16 Ni10 C24 C25 -74.0(7) . . . . ? C11 Ni10 C24 Ni15 -55.7(9) . . . . ? C10 Ni10 C24 Ni15 110.8(12) . . . . ? C25 Ni10 C24 Ni15 141.2(11) . . . . ? Ni9 Ni10 C24 Ni15 115.0(6) . . . . ? Ni11 Ni10 C24 Ni15 -70.9(6) . . . . ? Ni4 Ni10 C24 Ni15 -143.6(8) . . . . ? Ni16 Ni10 C24 Ni15 67.2(5) . . . . ? C11 Ni10 C24 Ni16 -122.9(6) . . . . ? C10 Ni10 C24 Ni16 43.6(13) . . . . ? C25 Ni10 C24 Ni16 74.0(7) . . . . ? Ni9 Ni10 C24 Ni16 47.9(3) . . . . ? Ni11 Ni10 C24 Ni16 -138.1(5) . . . . ? Ni4 Ni10 C24 Ni16 149.2(6) . . . . ? C11 Ni10 C24 Ni11 15.2(7) . . . . ? C10 Ni10 C24 Ni11 -178.3(11) . . . . ? C25 Ni10 C24 Ni11 -148.0(8) . . . . ? Ni9 Ni10 C24 Ni11 -174.1(3) . . . . ? Ni4 Ni10 C24 Ni11 -72.8(3) . . . . ? Ni16 Ni10 C24 Ni11 138.1(5) . . . . ? C11 Ni10 C24 Ni4 88.0(7) . . . . ? C10 Ni10 C24 Ni4 -105.5(12) . . . . ? C25 Ni10 C24 Ni4 -75.2(7) . . . . ? Ni9 Ni10 C24 Ni4 -101.3(3) . . . . ? Ni11 Ni10 C24 Ni4 72.8(3) . . . . ? Ni16 Ni10 C24 Ni4 -149.2(6) . . . . ? C11 Ni10 C24 Ni12 50.8(13) . . . . ? C10 Ni10 C24 Ni12 -142.7(13) . . . . ? C25 Ni10 C24 Ni12 -112.4(13) . . . . ? Ni9 Ni10 C24 Ni12 -138.5(11) . . . . ? Ni11 Ni10 C24 Ni12 35.6(9) . . . . ? Ni4 Ni10 C24 Ni12 -37.2(8) . . . . ? Ni16 Ni10 C24 Ni12 173.7(14) . . . . ? C3 Ni4 C24 C25 -10.8(12) . . . . ? C4 Ni4 C24 C25 -142.3(8) . . . . ? C13 Ni4 C24 C25 122.0(8) . . . . ? Ni3 Ni4 C24 C25 -2.1(6) . . . . ? Ni11 Ni4 C24 C25 -147.5(8) . . . . ? Ni12 Ni4 C24 C25 128.6(8) . . . . ? Ni10 Ni4 C24 C25 -72.6(7) . . . . ? C3 Ni4 C24 Ni15 -178.1(9) . . . . ? C4 Ni4 C24 Ni15 50.4(12) . . . . ? C13 Ni4 C24 Ni15 -45.3(11) . . . . ? C25 Ni4 C24 Ni15 -167.3(15) . . . . ? Ni3 Ni4 C24 Ni15 -169.4(10) . . . . ? Ni11 Ni4 C24 Ni15 45.1(8) . . . . ? Ni12 Ni4 C24 Ni15 -38.7(8) . . . . ? Ni10 Ni4 C24 Ni15 120.0(11) . . . . ? C3 Ni4 C24 Ni16 -3.3(16) . . . . ? C4 Ni4 C24 Ni16 -134.7(11) . . . . ? C13 Ni4 C24 Ni16 129.5(11) . . . . ? C25 Ni4 C24 Ni16 7.5(8) . . . . ? Ni3 Ni4 C24 Ni16 5.5(10) . . . . ? Ni11 Ni4 C24 Ni16 -140.0(12) . . . . ? Ni12 Ni4 C24 Ni16 136.1(12) . . . . ? Ni10 Ni4 C24 Ni16 -65.1(10) . . . . ? C3 Ni4 C24 Ni11 136.7(8) . . . . ? C4 Ni4 C24 Ni11 5.3(7) . . . . ? C13 Ni4 C24 Ni11 -90.5(5) . . . . ? C25 Ni4 C24 Ni11 147.5(8) . . . . ? Ni3 Ni4 C24 Ni11 145.5(3) . . . . ? Ni12 Ni4 C24 Ni11 -83.9(3) . . . . ? Ni10 Ni4 C24 Ni11 74.9(3) . . . . ? C3 Ni4 C24 Ni10 61.8(9) . . . . ? C4 Ni4 C24 Ni10 -69.6(7) . . . . ? C13 Ni4 C24 Ni10 -165.4(5) . . . . ? C25 Ni4 C24 Ni10 72.6(7) . . . . ? Ni3 Ni4 C24 Ni10 70.6(3) . . . . ? Ni11 Ni4 C24 Ni10 -74.9(3) . . . . ? Ni12 Ni4 C24 Ni10 -158.8(5) . . . . ? C3 Ni4 C24 Ni12 -139.4(8) . . . . ? C4 Ni4 C24 Ni12 89.1(6) . . . . ? C13 Ni4 C24 Ni12 -6.6(6) . . . . ? C25 Ni4 C24 Ni12 -128.6(8) . . . . ? Ni3 Ni4 C24 Ni12 -130.7(2) . . . . ? Ni11 Ni4 C24 Ni12 83.9(3) . . . . ? Ni10 Ni4 C24 Ni12 158.8(5) . . . . ? C20 Ni12 C24 C25 -168(3) . . . . ? C20' Ni12 C24 C25 -148.8(13) . . . . ? C13 Ni12 C24 C25 -52.0(10) . . . . ? C23 Ni12 C24 C25 50.8(10) . . . . ? Ni17 Ni12 C24 C25 169.7(9) . . . . ? Ni4 Ni12 C24 C25 -58.1(8) . . . . ? Ni1 Ni12 C24 C25 -0.2(10) . . . . ? Ni14 Ni12 C24 C25 97.4(9) . . . . ? Ni15 Ni12 C24 C25 145.1(11) . . . . ? Ni11 Ni12 C24 C25 -131.7(11) . . . . ? Ni5 Ni12 C24 C25 51.0(11) . . . . ? C20 Ni12 C24 Ni15 47(3) . . . . ? C20' Ni12 C24 Ni15 66.0(12) . . . . ? C13 Ni12 C24 Ni15 162.9(5) . . . . ? C23 Ni12 C24 Ni15 -94.4(4) . . . . ? Ni17 Ni12 C24 Ni15 24.6(4) . . . . ? Ni4 Ni12 C24 Ni15 156.7(5) . . . . ? Ni1 Ni12 C24 Ni15 -145.4(3) . . . . ? Ni14 Ni12 C24 Ni15 -47.8(3) . . . . ? Ni11 Ni12 C24 Ni15 83.1(4) . . . . ? Ni5 Ni12 C24 Ni15 -94.2(5) . . . . ? C20 Ni12 C24 Ni16 101(3) . . . . ? C20' Ni12 C24 Ni16 120.0(13) . . . . ? C13 Ni12 C24 Ni16 -143.1(8) . . . . ? C23 Ni12 C24 Ni16 -40.4(8) . . . . ? Ni17 Ni12 C24 Ni16 78.6(7) . . . . ? Ni4 Ni12 C24 Ni16 -149.3(9) . . . . ? Ni1 Ni12 C24 Ni16 -91.4(7) . . . . ? Ni14 Ni12 C24 Ni16 6.2(8) . . . . ? Ni15 Ni12 C24 Ni16 54.0(6) . . . . ? Ni11 Ni12 C24 Ni16 137.1(9) . . . . ? Ni5 Ni12 C24 Ni16 -40.2(10) . . . . ? C20 Ni12 C24 Ni11 -36(3) . . . . ? C20' Ni12 C24 Ni11 -17.1(12) . . . . ? C13 Ni12 C24 Ni11 79.7(5) . . . . ? C23 Ni12 C24 Ni11 -177.5(4) . . . . ? Ni17 Ni12 C24 Ni11 -58.6(3) . . . . ? Ni4 Ni12 C24 Ni11 73.6(3) . . . . ? Ni1 Ni12 C24 Ni11 131.5(2) . . . . ? Ni14 Ni12 C24 Ni11 -130.9(3) . . . . ? Ni15 Ni12 C24 Ni11 -83.1(4) . . . . ? Ni5 Ni12 C24 Ni11 -177.33(14) . . . . ? C20 Ni12 C24 Ni10 -71(3) . . . . ? C20' Ni12 C24 Ni10 -51.7(17) . . . . ? C13 Ni12 C24 Ni10 45.2(12) . . . . ? C23 Ni12 C24 Ni10 147.9(11) . . . . ? Ni17 Ni12 C24 Ni10 -93.1(11) . . . . ? Ni4 Ni12 C24 Ni10 39.0(9) . . . . ? Ni1 Ni12 C24 Ni10 96.9(11) . . . . ? Ni14 Ni12 C24 Ni10 -165.5(10) . . . . ? Ni15 Ni12 C24 Ni10 -117.7(12) . . . . ? Ni11 Ni12 C24 Ni10 -34.6(9) . . . . ? Ni5 Ni12 C24 Ni10 148.1(8) . . . . ? C20 Ni12 C24 Ni4 -110(3) . . . . ? C20' Ni12 C24 Ni4 -90.7(12) . . . . ? C13 Ni12 C24 Ni4 6.2(5) . . . . ? C23 Ni12 C24 Ni4 108.9(4) . . . . ? Ni17 Ni12 C24 Ni4 -132.1(2) . . . . ? Ni1 Ni12 C24 Ni4 57.9(3) . . . . ? Ni14 Ni12 C24 Ni4 155.5(2) . . . . ? Ni15 Ni12 C24 Ni4 -156.7(5) . . . . ? Ni11 Ni12 C24 Ni4 -73.6(3) . . . . ? Ni5 Ni12 C24 Ni4 109.1(4) . . . . ? Ni15 C24 C25 Ni8 45(2) . . . . ? Ni16 C24 C25 Ni8 62.3(9) . . . . ? Ni11 C24 C25 Ni8 -165.1(7) . . . . ? Ni10 C24 C25 Ni8 151.9(10) . . . . ? Ni4 C24 C25 Ni8 -122.1(10) . . . . ? Ni12 C24 C25 Ni8 -64.8(13) . . . . ? Ni15 C24 C25 Ni3 170.4(8) . . . . ? Ni16 C24 C25 Ni3 -171.9(12) . . . . ? Ni11 C24 C25 Ni3 -39.4(19) . . . . ? Ni10 C24 C25 Ni3 -82.3(12) . . . . ? Ni4 C24 C25 Ni3 3.6(11) . . . . ? Ni12 C24 C25 Ni3 61.0(15) . . . . ? Ni15 C24 C25 Ni9 -65.6(19) . . . . ? Ni16 C24 C25 Ni9 -48.0(9) . . . . ? Ni11 C24 C25 Ni9 84.6(14) . . . . ? Ni10 C24 C25 Ni9 41.6(9) . . . . ? Ni4 C24 C25 Ni9 127.6(10) . . . . ? Ni12 C24 C25 Ni9 -175.1(6) . . . . ? Ni15 C24 C25 Ni10 -107.2(15) . . . . ? Ni16 C24 C25 Ni10 -89.6(3) . . . . ? Ni11 C24 C25 Ni10 43.0(10) . . . . ? Ni4 C24 C25 Ni10 86.0(3) . . . . ? Ni12 C24 C25 Ni10 143.3(8) . . . . ? Ni15 C24 C25 Ni16 -17.6(13) . . . . ? Ni11 C24 C25 Ni16 132.5(11) . . . . ? Ni10 C24 C25 Ni16 89.6(3) . . . . ? Ni4 C24 C25 Ni16 175.6(5) . . . . ? Ni12 C24 C25 Ni16 -127.1(8) . . . . ? Ni15 C24 C25 Ni4 166.8(15) . . . . ? Ni16 C24 C25 Ni4 -175.6(5) . . . . ? Ni11 C24 C25 Ni4 -43.0(9) . . . . ? Ni10 C24 C25 Ni4 -86.0(3) . . . . ? Ni12 C24 C25 Ni4 57.3(6) . . . . ? C28' Ni8 C25 C24 -125(2) . . . . ? C28 Ni8 C25 C24 -153.7(14) . . . . ? C22 Ni8 C25 C24 45.4(12) . . . . ? Ni18 Ni8 C25 C24 157.0(10) . . . . ? Ni7 Ni8 C25 C24 39.7(14) . . . . ? Ni2 Ni8 C25 C24 95.1(11) . . . . ? Ni9 Ni8 C25 C24 -132.2(13) . . . . ? Ni3 Ni8 C25 C24 146.5(13) . . . . ? Ni13 Ni8 C25 C24 -4.5(11) . . . . ? Ni16 Ni8 C25 C24 -55.6(10) . . . . ? C28' Ni8 C25 Ni3 89(2) . . . . ? C28 Ni8 C25 Ni3 59.8(12) . . . . ? C22 Ni8 C25 Ni3 -101.1(4) . . . . ? Ni18 Ni8 C25 Ni3 10.6(5) . . . . ? Ni7 Ni8 C25 Ni3 -106.8(5) . . . . ? Ni2 Ni8 C25 Ni3 -51.4(3) . . . . ? Ni9 Ni8 C25 Ni3 81.3(4) . . . . ? Ni13 Ni8 C25 Ni3 -150.9(3) . . . . ? Ni16 Ni8 C25 Ni3 157.9(6) . . . . ? C28' Ni8 C25 Ni9 7(2) . . . . ? C28 Ni8 C25 Ni9 -21.5(12) . . . . ? C22 Ni8 C25 Ni9 177.6(4) . . . . ? Ni18 Ni8 C25 Ni9 -70.7(4) . . . . ? Ni7 Ni8 C25 Ni9 171.9(2) . . . . ? Ni2 Ni8 C25 Ni9 -132.6(2) . . . . ? Ni3 Ni8 C25 Ni9 -81.3(4) . . . . ? Ni13 Ni8 C25 Ni9 127.8(3) . . . . ? Ni16 Ni8 C25 Ni9 76.6(4) . . . . ? C28' Ni8 C25 Ni10 -5(3) . . . . ? C28 Ni8 C25 Ni10 -34.0(19) . . . . ? C22 Ni8 C25 Ni10 165.1(13) . . . . ? Ni18 Ni8 C25 Ni10 -83.3(13) . . . . ? Ni7 Ni8 C25 Ni10 159.3(8) . . . . ? Ni2 Ni8 C25 Ni10 -145.2(12) . . . . ? Ni9 Ni8 C25 Ni10 -12.6(10) . . . . ? Ni3 Ni8 C25 Ni10 -93.9(13) . . . . ? Ni13 Ni8 C25 Ni10 115.2(12) . . . . ? Ni16 Ni8 C25 Ni10 64.0(11) . . . . ? C28' Ni8 C25 Ni16 -69(2) . . . . ? C28 Ni8 C25 Ni16 -98.0(12) . . . . ? C22 Ni8 C25 Ni16 101.1(5) . . . . ? Ni18 Ni8 C25 Ni16 -147.3(3) . . . . ? Ni7 Ni8 C25 Ni16 95.3(5) . . . . ? Ni2 Ni8 C25 Ni16 150.8(3) . . . . ? Ni9 Ni8 C25 Ni16 -76.6(4) . . . . ? Ni3 Ni8 C25 Ni16 -157.9(6) . . . . ? Ni13 Ni8 C25 Ni16 51.2(3) . . . . ? C28' Ni8 C25 Ni4 143(2) . . . . ? C28 Ni8 C25 Ni4 114.0(13) . . . . ? C22 Ni8 C25 Ni4 -46.9(8) . . . . ? Ni18 Ni8 C25 Ni4 64.7(8) . . . . ? Ni7 Ni8 C25 Ni4 -52.7(10) . . . . ? Ni2 Ni8 C25 Ni4 2.8(7) . . . . ? Ni9 Ni8 C25 Ni4 135.4(9) . . . . ? Ni3 Ni8 C25 Ni4 54.1(6) . . . . ? Ni13 Ni8 C25 Ni4 -96.8(7) . . . . ? Ni16 Ni8 C25 Ni4 -148.0(9) . . . . ? C27 Ni3 C25 C24 168.3(16) . . . . ? C27' Ni3 C25 C24 151(3) . . . . ? C3 Ni3 C25 C24 0.9(15) . . . . ? Ni4 Ni3 C25 C24 -3.7(11) . . . . ? Ni18 Ni3 C25 C24 -148.9(13) . . . . ? Ni8 Ni3 C25 C24 -140.1(15) . . . . ? Ni9 Ni3 C25 C24 139.2(15) . . . . ? Ni2 Ni3 C25 C24 -97.3(13) . . . . ? C27 Ni3 C25 Ni8 -51.6(15) . . . . ? C27' Ni3 C25 Ni8 -69(3) . . . . ? C3 Ni3 C25 Ni8 141.0(5) . . . . ? Ni4 Ni3 C25 Ni8 136.5(5) . . . . ? Ni18 Ni3 C25 Ni8 -8.8(4) . . . . ? Ni9 Ni3 C25 Ni8 -80.7(4) . . . . ? Ni2 Ni3 C25 Ni8 42.8(3) . . . . ? C27 Ni3 C25 Ni9 29.1(15) . . . . ? C27' Ni3 C25 Ni9 11(3) . . . . ? C3 Ni3 C25 Ni9 -138.3(5) . . . . ? Ni4 Ni3 C25 Ni9 -142.9(4) . . . . ? Ni18 Ni3 C25 Ni9 71.9(3) . . . . ? Ni8 Ni3 C25 Ni9 80.7(4) . . . . ? Ni2 Ni3 C25 Ni9 123.5(3) . . . . ? C27 Ni3 C25 Ni10 97.3(14) . . . . ? C27' Ni3 C25 Ni10 80(3) . . . . ? C3 Ni3 C25 Ni10 -70.0(7) . . . . ? Ni4 Ni3 C25 Ni10 -74.6(4) . . . . ? Ni18 Ni3 C25 Ni10 140.1(4) . . . . ? Ni8 Ni3 C25 Ni10 149.0(7) . . . . ? Ni9 Ni3 C25 Ni10 68.3(4) . . . . ? Ni2 Ni3 C25 Ni10 -168.2(4) . . . . ? C27 Ni3 C25 Ni16 5(2) . . . . ? C27' Ni3 C25 Ni16 -12(3) . . . . ? C3 Ni3 C25 Ni16 -162.2(13) . . . . ? Ni4 Ni3 C25 Ni16 -166.8(15) . . . . ? Ni18 Ni3 C25 Ni16 47.9(14) . . . . ? Ni8 Ni3 C25 Ni16 56.8(12) . . . . ? Ni9 Ni3 C25 Ni16 -23.9(11) . . . . ? Ni2 Ni3 C25 Ni16 99.6(14) . . . . ? C27 Ni3 C25 Ni4 171.9(13) . . . . ? C27' Ni3 C25 Ni4 154(3) . . . . ? C3 Ni3 C25 Ni4 4.5(6) . . . . ? Ni18 Ni3 C25 Ni4 -145.3(2) . . . . ? Ni8 Ni3 C25 Ni4 -136.5(5) . . . . ? Ni9 Ni3 C25 Ni4 142.9(4) . . . . ? Ni2 Ni3 C25 Ni4 -93.6(2) . . . . ? C9 Ni9 C25 C24 154.0(18) . . . . ? C10 Ni9 C25 C24 -53.9(13) . . . . ? Ni10 Ni9 C25 C24 -41.4(10) . . . . ? C17' Ni9 C25 C24 51(2) . . . . ? Ni16 Ni9 C25 C24 45.3(10) . . . . ? Ni8 Ni9 C25 C24 131.8(13) . . . . ? Ni3 Ni9 C25 C24 -145.5(13) . . . . ? C9 Ni9 C25 Ni8 22.2(19) . . . . ? C10 Ni9 C25 Ni8 174.2(7) . . . . ? Ni10 Ni9 C25 Ni8 -173.2(5) . . . . ? C17' Ni9 C25 Ni8 -80.4(17) . . . . ? Ni16 Ni9 C25 Ni8 -86.6(4) . . . . ? Ni3 Ni9 C25 Ni8 82.6(4) . . . . ? C9 Ni9 C25 Ni3 -60.5(19) . . . . ? C10 Ni9 C25 Ni3 91.6(7) . . . . ? Ni10 Ni9 C25 Ni3 104.1(4) . . . . ? C17' Ni9 C25 Ni3 -163.1(17) . . . . ? Ni16 Ni9 C25 Ni3 -169.2(5) . . . . ? Ni8 Ni9 C25 Ni3 -82.6(4) . . . . ? C9 Ni9 C25 Ni10 -164.6(17) . . . . ? C10 Ni9 C25 Ni10 -12.5(7) . . . . ? C17' Ni9 C25 Ni10 92.8(17) . . . . ? Ni16 Ni9 C25 Ni10 86.7(3) . . . . ? Ni8 Ni9 C25 Ni10 173.2(5) . . . . ? Ni3 Ni9 C25 Ni10 -104.1(4) . . . . ? C9 Ni9 C25 Ni16 108.7(18) . . . . ? C10 Ni9 C25 Ni16 -99.2(7) . . . . ? Ni10 Ni9 C25 Ni16 -86.7(3) . . . . ? C17' Ni9 C25 Ni16 6.1(17) . . . . ? Ni8 Ni9 C25 Ni16 86.6(4) . . . . ? Ni3 Ni9 C25 Ni16 169.2(5) . . . . ? C9 Ni9 C25 Ni4 -109.6(18) . . . . ? C10 Ni9 C25 Ni4 42.5(10) . . . . ? Ni10 Ni9 C25 Ni4 55.0(6) . . . . ? C17' Ni9 C25 Ni4 147.8(18) . . . . ? Ni16 Ni9 C25 Ni4 141.7(9) . . . . ? Ni8 Ni9 C25 Ni4 -131.7(9) . . . . ? Ni3 Ni9 C25 Ni4 -49.1(6) . . . . ? C11 Ni10 C25 C24 -34.3(16) . . . . ? C10 Ni10 C25 C24 160.5(9) . . . . ? Ni9 Ni10 C25 C24 146.9(8) . . . . ? Ni11 Ni10 C25 C24 -25.2(6) . . . . ? Ni4 Ni10 C25 C24 -71.5(7) . . . . ? Ni16 Ni10 C25 C24 69.4(7) . . . . ? C11 Ni10 C25 Ni8 -168.2(13) . . . . ? C10 Ni10 C25 Ni8 26.7(15) . . . . ? C24 Ni10 C25 Ni8 -133.8(16) . . . . ? Ni9 Ni10 C25 Ni8 13.1(10) . . . . ? Ni11 Ni10 C25 Ni8 -159.0(12) . . . . ? Ni4 Ni10 C25 Ni8 154.7(15) . . . . ? Ni16 Ni10 C25 Ni8 -64.4(11) . . . . ? C11 Ni10 C25 Ni3 103.1(13) . . . . ? C10 Ni10 C25 Ni3 -62.0(9) . . . . ? C24 Ni10 C25 Ni3 137.5(9) . . . . ? Ni9 Ni10 C25 Ni3 -75.6(4) . . . . ? Ni11 Ni10 C25 Ni3 112.3(4) . . . . ? Ni4 Ni10 C25 Ni3 66.0(4) . . . . ? Ni16 Ni10 C25 Ni3 -153.2(7) . . . . ? C11 Ni10 C25 Ni9 178.7(12) . . . . ? C10 Ni10 C25 Ni9 13.6(8) . . . . ? C24 Ni10 C25 Ni9 -146.9(8) . . . . ? Ni11 Ni10 C25 Ni9 -172.1(3) . . . . ? Ni4 Ni10 C25 Ni9 141.6(5) . . . . ? Ni16 Ni10 C25 Ni9 -77.6(3) . . . . ? C11 Ni10 C25 Ni16 -103.7(13) . . . . ? C10 Ni10 C25 Ni16 91.1(8) . . . . ? C24 Ni10 C25 Ni16 -69.4(7) . . . . ? Ni9 Ni10 C25 Ni16 77.6(3) . . . . ? Ni11 Ni10 C25 Ni16 -94.5(3) . . . . ? Ni4 Ni10 C25 Ni16 -140.8(5) . . . . ? C11 Ni10 C25 Ni4 37.1(14) . . . . ? C10 Ni10 C25 Ni4 -128.0(7) . . . . ? C24 Ni10 C25 Ni4 71.5(7) . . . . ? Ni9 Ni10 C25 Ni4 -141.6(5) . . . . ? Ni11 Ni10 C25 Ni4 46.3(3) . . . . ? Ni16 Ni10 C25 Ni4 140.8(5) . . . . ? C17 Ni16 C25 C24 -176.7(17) . . . . ? C17' Ni16 C25 C24 -153(3) . . . . ? C16 Ni16 C25 C24 8.3(12) . . . . ? Ni15 Ni16 C25 C24 8.5(7) . . . . ? Ni9 Ni16 C25 C24 -143.5(8) . . . . ? Ni8 Ni16 C25 C24 136.0(8) . . . . ? Ni10 Ni16 C25 C24 -71.5(7) . . . . ? Ni13 Ni16 C25 C24 90.4(7) . . . . ? C17 Ni16 C25 Ni8 47.3(17) . . . . ? C17' Ni16 C25 Ni8 71(3) . . . . ? C16 Ni16 C25 Ni8 -127.7(8) . . . . ? C24 Ni16 C25 Ni8 -136.0(8) . . . . ? Ni15 Ni16 C25 Ni8 -127.5(3) . . . . ? Ni9 Ni16 C25 Ni8 80.5(4) . . . . ? Ni10 Ni16 C25 Ni8 152.5(6) . . . . ? Ni13 Ni16 C25 Ni8 -45.6(3) . . . . ? C17 Ni16 C25 Ni3 -9(2) . . . . ? C17' Ni16 C25 Ni3 15(3) . . . . ? C16 Ni16 C25 Ni3 176.2(12) . . . . ? C24 Ni16 C25 Ni3 167.9(18) . . . . ? Ni15 Ni16 C25 Ni3 176.3(14) . . . . ? Ni9 Ni16 C25 Ni3 24.3(11) . . . . ? Ni8 Ni16 C25 Ni3 -56.1(12) . . . . ? Ni10 Ni16 C25 Ni3 96.3(14) . . . . ? Ni13 Ni16 C25 Ni3 -101.7(14) . . . . ? C17 Ni16 C25 Ni9 -33.2(16) . . . . ? C17' Ni16 C25 Ni9 -10(3) . . . . ? C16 Ni16 C25 Ni9 151.9(8) . . . . ? C24 Ni16 C25 Ni9 143.5(8) . . . . ? Ni15 Ni16 C25 Ni9 152.0(3) . . . . ? Ni8 Ni16 C25 Ni9 -80.5(4) . . . . ? Ni10 Ni16 C25 Ni9 72.0(3) . . . . ? Ni13 Ni16 C25 Ni9 -126.0(3) . . . . ? C17 Ni16 C25 Ni10 -105.2(16) . . . . ? C17' Ni16 C25 Ni10 -82(3) . . . . ? C16 Ni16 C25 Ni10 79.9(9) . . . . ? C24 Ni16 C25 Ni10 71.5(7) . . . . ? Ni15 Ni16 C25 Ni10 80.0(3) . . . . ? Ni9 Ni16 C25 Ni10 -72.0(3) . . . . ? Ni8 Ni16 C25 Ni10 -152.5(6) . . . . ? Ni13 Ni16 C25 Ni10 161.9(3) . . . . ? C17 Ni16 C25 Ni4 -170.7(17) . . . . ? C17' Ni16 C25 Ni4 -147(3) . . . . ? C16 Ni16 C25 Ni4 14.4(14) . . . . ? C24 Ni16 C25 Ni4 6.1(6) . . . . ? Ni15 Ni16 C25 Ni4 14.5(8) . . . . ? Ni9 Ni16 C25 Ni4 -137.5(10) . . . . ? Ni8 Ni16 C25 Ni4 142.1(10) . . . . ? Ni10 Ni16 C25 Ni4 -65.5(7) . . . . ? Ni13 Ni16 C25 Ni4 96.5(8) . . . . ? C3 Ni4 C25 C24 173.0(8) . . . . ? C4 Ni4 C25 C24 51.4(11) . . . . ? C13 Ni4 C25 C24 -75.5(9) . . . . ? Ni3 Ni4 C25 C24 177.4(8) . . . . ? Ni11 Ni4 C25 C24 25.5(6) . . . . ? Ni12 Ni4 C25 C24 -40.6(6) . . . . ? Ni10 Ni4 C25 C24 72.5(7) . . . . ? C3 Ni4 C25 Ni8 -63.6(9) . . . . ? C4 Ni4 C25 Ni8 174.9(8) . . . . ? C13 Ni4 C25 Ni8 47.9(10) . . . . ? C24 Ni4 C25 Ni8 123.4(11) . . . . ? Ni3 Ni4 C25 Ni8 -59.2(6) . . . . ? Ni11 Ni4 C25 Ni8 148.9(7) . . . . ? Ni12 Ni4 C25 Ni8 82.8(7) . . . . ? Ni10 Ni4 C25 Ni8 -164.1(10) . . . . ? C3 Ni4 C25 Ni3 -4.4(6) . . . . ? C4 Ni4 C25 Ni3 -126.0(8) . . . . ? C13 Ni4 C25 Ni3 107.1(6) . . . . ? C24 Ni4 C25 Ni3 -177.4(8) . . . . ? Ni11 Ni4 C25 Ni3 -151.9(3) . . . . ? Ni12 Ni4 C25 Ni3 142.0(3) . . . . ? Ni10 Ni4 C25 Ni3 -104.9(4) . . . . ? C3 Ni4 C25 Ni9 48.5(9) . . . . ? C4 Ni4 C25 Ni9 -73.0(11) . . . . ? C13 Ni4 C25 Ni9 160.1(8) . . . . ? C24 Ni4 C25 Ni9 -124.4(11) . . . . ? Ni3 Ni4 C25 Ni9 53.0(6) . . . . ? Ni11 Ni4 C25 Ni9 -98.9(7) . . . . ? Ni12 Ni4 C25 Ni9 -165.0(8) . . . . ? Ni10 Ni4 C25 Ni9 -51.9(6) . . . . ? C3 Ni4 C25 Ni10 100.5(5) . . . . ? C4 Ni4 C25 Ni10 -21.1(9) . . . . ? C13 Ni4 C25 Ni10 -148.0(6) . . . . ? C24 Ni4 C25 Ni10 -72.5(7) . . . . ? Ni3 Ni4 C25 Ni10 104.9(4) . . . . ? Ni11 Ni4 C25 Ni10 -47.0(3) . . . . ? Ni12 Ni4 C25 Ni10 -113.1(3) . . . . ? C3 Ni4 C25 Ni16 167.0(9) . . . . ? C4 Ni4 C25 Ni16 45.4(12) . . . . ? C13 Ni4 C25 Ni16 -81.5(10) . . . . ? C24 Ni4 C25 Ni16 -6.0(6) . . . . ? Ni3 Ni4 C25 Ni16 171.4(10) . . . . ? Ni11 Ni4 C25 Ni16 19.5(8) . . . . ? Ni12 Ni4 C25 Ni16 -46.6(8) . . . . ? Ni10 Ni4 C25 Ni16 66.5(7) . . . . ? C26' Ni2 C26 O26 68(27) . . . . ? C2 Ni2 C26 O26 -46(14) . . . . ? C22 Ni2 C26 O26 121(14) . . . . ? Ni1 Ni2 C26 O26 -37(15) . . . . ? Ni18 Ni2 C26 O26 177(15) . . . . ? Ni8 Ni2 C26 O26 163(14) . . . . ? Ni7 Ni2 C26 O26 103(14) . . . . ? Ni3 Ni2 C26 O26 -141(14) . . . . ? C27' Ni3 C27 O27 16(11) . . . . ? C3 Ni3 C27 O27 123(16) . . . . ? C25 Ni3 C27 O27 -44(17) . . . . ? Ni4 Ni3 C27 O27 119(16) . . . . ? Ni18 Ni3 C27 O27 -98(16) . . . . ? Ni8 Ni3 C27 O27 -82(16) . . . . ? Ni9 Ni3 C27 O27 -22(16) . . . . ? Ni2 Ni3 C27 O27 -137(16) . . . . ? C28' Ni8 C28 O28 -95(83) . . . . ? C25 Ni8 C28 O28 -16(83) . . . . ? C22 Ni8 C28 O28 138(82) . . . . ? Ni18 Ni8 C28 O28 61(82) . . . . ? Ni7 Ni8 C28 O28 156(82) . . . . ? Ni2 Ni8 C28 O28 96(82) . . . . ? Ni9 Ni8 C28 O28 -33(82) . . . . ? Ni3 Ni8 C28 O28 26(82) . . . . ? Ni13 Ni8 C28 O28 -159(82) . . . . ? Ni16 Ni8 C28 O28 -80(82) . . . . ? C28' Ni8 Ni18 C29 3(3) . . . . ? C28 Ni8 Ni18 C29 -6(3) . . . . ? C25 Ni8 Ni18 C29 125(3) . . . . ? C22 Ni8 Ni18 C29 -136(3) . . . . ? Ni7 Ni8 Ni18 C29 -88(3) . . . . ? Ni2 Ni8 Ni18 C29 -146(3) . . . . ? Ni9 Ni8 Ni18 C29 78(3) . . . . ? Ni3 Ni8 Ni18 C29 134(3) . . . . ? Ni13 Ni8 Ni18 C29 -90(3) . . . . ? Ni16 Ni8 Ni18 C29 75(3) . . . . ? C28' Ni8 Ni18 C27' -109(2) . . . . ? C28 Ni8 Ni18 C27' -119.0(19) . . . . ? C25 Ni8 Ni18 C27' 12.6(15) . . . . ? C22 Ni8 Ni18 C27' 111.7(15) . . . . ? Ni7 Ni8 Ni18 C27' 159.4(15) . . . . ? Ni2 Ni8 Ni18 C27' 101.2(15) . . . . ? Ni9 Ni8 Ni18 C27' -35.0(15) . . . . ? Ni3 Ni8 Ni18 C27' 21.6(15) . . . . ? Ni13 Ni8 Ni18 C27' 157.8(15) . . . . ? Ni16 Ni8 Ni18 C27' -37.4(15) . . . . ? C28' Ni8 Ni18 C26' 130(3) . . . . ? C28 Ni8 Ni18 C26' 120(3) . . . . ? C25 Ni8 Ni18 C26' -108(2) . . . . ? C22 Ni8 Ni18 C26' -9(2) . . . . ? Ni7 Ni8 Ni18 C26' 39(2) . . . . ? Ni2 Ni8 Ni18 C26' -20(2) . . . . ? Ni9 Ni8 Ni18 C26' -156(2) . . . . ? Ni3 Ni8 Ni18 C26' -99(2) . . . . ? Ni13 Ni8 Ni18 C26' 37(2) . . . . ? Ni16 Ni8 Ni18 C26' -158(2) . . . . ? C28 Ni8 Ni18 C28' -10(2) . . . . ? C25 Ni8 Ni18 C28' 121.8(19) . . . . ? C22 Ni8 Ni18 C28' -139.2(19) . . . . ? Ni7 Ni8 Ni18 C28' -91.4(18) . . . . ? Ni2 Ni8 Ni18 C28' -149.6(18) . . . . ? Ni9 Ni8 Ni18 C28' 74.2(18) . . . . ? Ni3 Ni8 Ni18 C28' 130.8(18) . . . . ? Ni13 Ni8 Ni18 C28' -93.0(19) . . . . ? Ni16 Ni8 Ni18 C28' 71.8(19) . . . . ? C28' Ni8 Ni18 Ni2 149.6(18) . . . . ? C28 Ni8 Ni18 Ni2 139.8(12) . . . . ? C25 Ni8 Ni18 Ni2 -88.6(4) . . . . ? C22 Ni8 Ni18 Ni2 10.5(4) . . . . ? Ni7 Ni8 Ni18 Ni2 58.20(13) . . . . ? Ni9 Ni8 Ni18 Ni2 -136.23(14) . . . . ? Ni3 Ni8 Ni18 Ni2 -79.57(15) . . . . ? Ni13 Ni8 Ni18 Ni2 56.6(4) . . . . ? Ni16 Ni8 Ni18 Ni2 -138.6(3) . . . . ? C28' Ni8 Ni18 Ni3 -130.8(18) . . . . ? C28 Ni8 Ni18 Ni3 -140.7(11) . . . . ? C25 Ni8 Ni18 Ni3 -9.0(4) . . . . ? C22 Ni8 Ni18 Ni3 90.0(4) . . . . ? Ni7 Ni8 Ni18 Ni3 137.77(12) . . . . ? Ni2 Ni8 Ni18 Ni3 79.57(15) . . . . ? Ni9 Ni8 Ni18 Ni3 -56.66(11) . . . . ? Ni13 Ni8 Ni18 Ni3 136.1(3) . . . . ? Ni16 Ni8 Ni18 Ni3 -59.0(4) . . . . ? C26 Ni2 Ni18 C29 -32(4) . . . . ? C26' Ni2 Ni18 C29 -21(5) . . . . ? C2 Ni2 Ni18 C29 -102(4) . . . . ? C22 Ni2 Ni18 C29 121(4) . . . . ? Ni1 Ni2 Ni18 C29 176(4) . . . . ? Ni8 Ni2 Ni18 C29 131(4) . . . . ? Ni7 Ni2 Ni18 C29 75(4) . . . . ? Ni3 Ni2 Ni18 C29 -159(4) . . . . ? C26 Ni2 Ni18 C27' 102.8(18) . . . . ? C26' Ni2 Ni18 C27' 113(4) . . . . ? C2 Ni2 Ni18 C27' 32.2(13) . . . . ? C22 Ni2 Ni18 C27' -104.5(12) . . . . ? Ni1 Ni2 Ni18 C27' -49.9(12) . . . . ? Ni8 Ni2 Ni18 C27' -94.3(12) . . . . ? Ni7 Ni2 Ni18 C27' -150.6(12) . . . . ? Ni3 Ni2 Ni18 C27' -24.5(11) . . . . ? C26 Ni2 Ni18 C26' -11(4) . . . . ? C2 Ni2 Ni18 C26' -81(3) . . . . ? C22 Ni2 Ni18 C26' 142(3) . . . . ? Ni1 Ni2 Ni18 C26' -163(3) . . . . ? Ni8 Ni2 Ni18 C26' 152(3) . . . . ? Ni7 Ni2 Ni18 C26' 96(3) . . . . ? Ni3 Ni2 Ni18 C26' -138(3) . . . . ? C26 Ni2 Ni18 C28' -142.2(18) . . . . ? C26' Ni2 Ni18 C28' -131(4) . . . . ? C2 Ni2 Ni18 C28' 147.3(13) . . . . ? C22 Ni2 Ni18 C28' 10.5(12) . . . . ? Ni1 Ni2 Ni18 C28' 65.1(12) . . . . ? Ni8 Ni2 Ni18 C28' 20.7(11) . . . . ? Ni7 Ni2 Ni18 C28' -35.6(12) . . . . ? Ni3 Ni2 Ni18 C28' 90.5(12) . . . . ? C26 Ni2 Ni18 Ni8 -162.9(14) . . . . ? C26' Ni2 Ni18 Ni8 -152(3) . . . . ? C2 Ni2 Ni18 Ni8 126.5(6) . . . . ? C22 Ni2 Ni18 Ni8 -10.2(4) . . . . ? Ni1 Ni2 Ni18 Ni8 44.4(4) . . . . ? Ni7 Ni2 Ni18 Ni8 -56.32(14) . . . . ? Ni3 Ni2 Ni18 Ni8 69.80(14) . . . . ? C26 Ni2 Ni18 Ni3 127.3(14) . . . . ? C26' Ni2 Ni18 Ni3 138(3) . . . . ? C2 Ni2 Ni18 Ni3 56.7(6) . . . . ? C22 Ni2 Ni18 Ni3 -80.0(4) . . . . ? Ni1 Ni2 Ni18 Ni3 -25.4(4) . . . . ? Ni8 Ni2 Ni18 Ni3 -69.80(14) . . . . ? Ni7 Ni2 Ni18 Ni3 -126.12(15) . . . . ? C27 Ni3 Ni18 C29 35(3) . . . . ? C27' Ni3 Ni18 C29 20(4) . . . . ? C3 Ni3 Ni18 C29 106(3) . . . . ? C25 Ni3 Ni18 C29 -117(3) . . . . ? Ni4 Ni3 Ni18 C29 -171(3) . . . . ? Ni8 Ni3 Ni18 C29 -126(3) . . . . ? Ni9 Ni3 Ni18 C29 -69(3) . . . . ? Ni2 Ni3 Ni18 C29 163(3) . . . . ? C27 Ni3 Ni18 C27' 14(3) . . . . ? C3 Ni3 Ni18 C27' 86(2) . . . . ? C25 Ni3 Ni18 C27' -138(2) . . . . ? Ni4 Ni3 Ni18 C27' 169(2) . . . . ? Ni8 Ni3 Ni18 C27' -146(2) . . . . ? Ni9 Ni3 Ni18 C27' -90(2) . . . . ? Ni2 Ni3 Ni18 C27' 142(2) . . . . ? C27 Ni3 Ni18 C26' -99(2) . . . . ? C27' Ni3 Ni18 C26' -113(3) . . . . ? C3 Ni3 Ni18 C26' -27(2) . . . . ? C25 Ni3 Ni18 C26' 109(2) . . . . ? Ni4 Ni3 Ni18 C26' 55(2) . . . . ? Ni8 Ni3 Ni18 C26' 100(2) . . . . ? Ni9 Ni3 Ni18 C26' 157(2) . . . . ? Ni2 Ni3 Ni18 C26' 29(2) . . . . ? C27 Ni3 Ni18 C28' 129.5(16) . . . . ? C27' Ni3 Ni18 C28' 115(2) . . . . ? C3 Ni3 Ni18 C28' -158.8(14) . . . . ? C25 Ni3 Ni18 C28' -22.7(13) . . . . ? Ni4 Ni3 Ni18 C28' -75.9(13) . . . . ? Ni8 Ni3 Ni18 C28' -31.1(13) . . . . ? Ni9 Ni3 Ni18 C28' 25.3(13) . . . . ? Ni2 Ni3 Ni18 C28' -102.6(13) . . . . ? C27 Ni3 Ni18 Ni8 160.6(9) . . . . ? C27' Ni3 Ni18 Ni8 146(2) . . . . ? C3 Ni3 Ni18 Ni8 -127.7(7) . . . . ? C25 Ni3 Ni18 Ni8 8.4(4) . . . . ? Ni4 Ni3 Ni18 Ni8 -44.8(3) . . . . ? Ni9 Ni3 Ni18 Ni8 56.38(13) . . . . ? Ni2 Ni3 Ni18 Ni8 -71.54(15) . . . . ? C27 Ni3 Ni18 Ni2 -127.8(9) . . . . ? C27' Ni3 Ni18 Ni2 -142(2) . . . . ? C3 Ni3 Ni18 Ni2 -56.2(7) . . . . ? C25 Ni3 Ni18 Ni2 80.0(4) . . . . ? Ni4 Ni3 Ni18 Ni2 26.7(4) . . . . ? Ni8 Ni3 Ni18 Ni2 71.54(15) . . . . ? Ni9 Ni3 Ni18 Ni2 127.92(16) . . . . ? C2 Ni2 C26' O26' -78(30) . . . . ? C22 Ni2 C26' O26' 76(32) . . . . ? Ni1 Ni2 C26' O26' -53(32) . . . . ? Ni18 Ni2 C26' O26' 148(31) . . . . ? Ni8 Ni2 C26' O26' 125(29) . . . . ? Ni7 Ni2 C26' O26' 68(30) . . . . ? Ni3 Ni2 C26' O26' -177(29) . . . . ? C26 Ni2 C26' Ni18 65(29) . . . . ? C2 Ni2 C26' Ni18 133.3(16) . . . . ? C22 Ni2 C26' Ni18 -72(4) . . . . ? Ni1 Ni2 C26' Ni18 159(4) . . . . ? Ni8 Ni2 C26' Ni18 -23(2) . . . . ? Ni7 Ni2 C26' Ni18 -80.7(17) . . . . ? Ni3 Ni2 C26' Ni18 35(2) . . . . ? C29 Ni18 C26' O26' -2(7) . . . . ? C27' Ni18 C26' O26' 107(6) . . . . ? C28' Ni18 C26' O26' -103(6) . . . . ? Ni8 Ni18 C26' O26' -144(6) . . . . ? Ni2 Ni18 C26' O26' -170(8) . . . . ? Ni3 Ni18 C26' O26' 149(6) . . . . ? C29 Ni18 C26' Ni2 168(3) . . . . ? C27' Ni18 C26' Ni2 -83(3) . . . . ? C28' Ni18 C26' Ni2 68(4) . . . . ? Ni8 Ni18 C26' Ni2 26(3) . . . . ? Ni3 Ni18 C26' Ni2 -41(3) . . . . ? C27 Ni3 C27' O27' 79(13) . . . . ? C3 Ni3 C27' O27' 3(10) . . . . ? C25 Ni3 C27' O27' -147(8) . . . . ? Ni4 Ni3 C27' O27' -27(13) . . . . ? Ni18 Ni3 C27' O27' 137(10) . . . . ? Ni8 Ni3 C27' O27' 165(9) . . . . ? Ni9 Ni3 C27' O27' -138(10) . . . . ? Ni2 Ni3 C27' O27' 107(10) . . . . ? C27 Ni3 C27' Ni18 -59(11) . . . . ? C3 Ni3 C27' Ni18 -134.6(9) . . . . ? C25 Ni3 C27' Ni18 75(2) . . . . ? Ni4 Ni3 C27' Ni18 -164(3) . . . . ? Ni8 Ni3 C27' Ni18 27.4(14) . . . . ? Ni9 Ni3 C27' Ni18 84.1(10) . . . . ? Ni2 Ni3 C27' Ni18 -30.5(15) . . . . ? C29 Ni18 C27' O27' 36(5) . . . . ? C26' Ni18 C27' O27' -76(5) . . . . ? C28' Ni18 C27' O27' 129(5) . . . . ? Ni8 Ni18 C27' O27' 172(5) . . . . ? Ni2 Ni18 C27' O27' -121(5) . . . . ? Ni3 Ni18 C27' O27' -158(6) . . . . ? C29 Ni18 C27' Ni3 -167(2) . . . . ? C26' Ni18 C27' Ni3 82(2) . . . . ? C28' Ni18 C27' Ni3 -74(2) . . . . ? Ni8 Ni18 C27' Ni3 -30.5(18) . . . . ? Ni2 Ni18 C27' Ni3 36.7(18) . . . . ? C28 Ni8 C28' O28' -119(13) . . . . ? C25 Ni8 C28' O28' 121(10) . . . . ? C22 Ni8 C28' O28' -43(12) . . . . ? Ni18 Ni8 C28' O28' -137(11) . . . . ? Ni7 Ni8 C28' O28' -49(11) . . . . ? Ni2 Ni8 C28' O28' -106(10) . . . . ? Ni9 Ni8 C28' O28' 127(11) . . . . ? Ni3 Ni8 C28' O28' 177(10) . . . . ? Ni13 Ni8 C28' O28' 7(11) . . . . ? Ni16 Ni8 C28' O28' 75(11) . . . . ? C28 Ni8 C28' Ni18 18(4) . . . . ? C25 Ni8 C28' Ni18 -101.9(14) . . . . ? C22 Ni8 C28' Ni18 94(2) . . . . ? Ni7 Ni8 C28' Ni18 87.6(7) . . . . ? Ni2 Ni8 C28' Ni18 30.7(16) . . . . ? Ni9 Ni8 C28' Ni18 -95.9(9) . . . . ? Ni3 Ni8 C28' Ni18 -46.6(13) . . . . ? Ni13 Ni8 C28' Ni18 144.0(5) . . . . ? Ni16 Ni8 C28' Ni18 -148.6(5) . . . . ? C29 Ni18 C28' O28' -19(5) . . . . ? C27' Ni18 C28' O28' -119(5) . . . . ? C26' Ni18 C28' O28' 89(5) . . . . ? Ni8 Ni18 C28' O28' 158(6) . . . . ? Ni2 Ni18 C28' O28' 130(5) . . . . ? Ni3 Ni18 C28' O28' -158(5) . . . . ? C29 Ni18 C28' Ni8 -177(2) . . . . ? C27' Ni18 C28' Ni8 82(2) . . . . ? C26' Ni18 C28' Ni8 -70(3) . . . . ? Ni2 Ni18 C28' Ni8 -28.3(16) . . . . ? Ni3 Ni18 C28' Ni8 43.2(14) . . . . ? C27' Ni18 C29 O29 -33(49) . . . . ? C26' Ni18 C29 O29 87(49) . . . . ? C28' Ni18 C29 O29 -144(49) . . . . ? Ni8 Ni18 C29 O29 -146(48) . . . . ? Ni2 Ni18 C29 O29 102(49) . . . . ? Ni3 Ni18 C29 O29 -47(50) . . . . ? C38' Ni21 Ni22 C44' 30(6) 3 . . . ? C32 Ni21 Ni22 C44' 21(6) . . . . ? C38 Ni21 Ni22 C44' -47(6) . . . . ? C41 Ni21 Ni22 C44' -152(6) . . . . ? C37 Ni21 Ni22 C44' 95(6) 3 . . . ? C42 Ni21 Ni22 C44' -154(6) . . . . ? Ni28 Ni21 Ni22 C44' -115(6) . . . . ? Ni24 Ni21 Ni22 C44' 167(6) 3 . . . ? Ni27 Ni21 Ni22 C44' -106(6) . . . . ? C38' Ni21 Ni22 C44 4(5) 3 . . . ? C32 Ni21 Ni22 C44 -6(4) . . . . ? C38 Ni21 Ni22 C44 -74(4) . . . . ? C41 Ni21 Ni22 C44 -179(4) . . . . ? C37 Ni21 Ni22 C44 69(4) 3 . . . ? C42 Ni21 Ni22 C44 179(4) . . . . ? Ni28 Ni21 Ni22 C44 -142(4) . . . . ? Ni24 Ni21 Ni22 C44 140(4) 3 . . . ? Ni27 Ni21 Ni22 C44 -132(4) . . . . ? C38' Ni21 Ni22 C32 10(3) 3 . . . ? C38 Ni21 Ni22 C32 -67.9(18) . . . . ? C41 Ni21 Ni22 C32 -173.0(9) . . . . ? C37 Ni21 Ni22 C32 74.4(15) 3 . . . ? C42 Ni21 Ni22 C32 -174.8(9) . . . . ? Ni28 Ni21 Ni22 C32 -136.0(8) . . . . ? Ni24 Ni21 Ni22 C32 146.0(8) 3 . . . ? Ni27 Ni21 Ni22 C32 -126.5(8) . . . . ? C38' Ni21 Ni22 C42 -176(3) 3 . . . ? C32 Ni21 Ni22 C42 174.8(9) . . . . ? C38 Ni21 Ni22 C42 107.0(16) . . . . ? C41 Ni21 Ni22 C42 1.9(6) . . . . ? C37 Ni21 Ni22 C42 -110.8(13) 3 . . . ? Ni28 Ni21 Ni22 C42 38.8(5) . . . . ? Ni24 Ni21 Ni22 C42 -39.1(5) 3 . . . ? Ni27 Ni21 Ni22 C42 48.3(4) . . . . ? C38' Ni21 Ni22 Ni25 156(3) 3 . . . ? C32 Ni21 Ni22 Ni25 146.8(8) . . . . ? C38 Ni21 Ni22 Ni25 78.9(16) . . . . ? C41 Ni21 Ni22 Ni25 -26.2(4) . . . . ? C37 Ni21 Ni22 Ni25 -138.8(13) 3 . . . ? C42 Ni21 Ni22 Ni25 -28.1(4) . . . . ? Ni28 Ni21 Ni22 Ni25 10.73(17) . . . . ? Ni24 Ni21 Ni22 Ni25 -67.18(14) 3 . . . ? Ni27 Ni21 Ni22 Ni25 20.26(9) . . . . ? C38' Ni21 Ni22 Ni29 -97(3) 3 . . . ? C32 Ni21 Ni22 Ni29 -106.2(8) . . . . ? C38 Ni21 Ni22 Ni29 -174.0(16) . . . . ? C41 Ni21 Ni22 Ni29 80.9(4) . . . . ? C37 Ni21 Ni22 Ni29 -31.8(13) 3 . . . ? C42 Ni21 Ni22 Ni29 79.0(5) . . . . ? Ni28 Ni21 Ni22 Ni29 117.8(3) . . . . ? Ni24 Ni21 Ni22 Ni29 39.9(3) 3 . . . ? Ni27 Ni21 Ni22 Ni29 127.3(3) . . . . ? C38' Ni21 Ni22 Ni24 -141(3) 3 . . . ? C32 Ni21 Ni22 Ni24 -150.5(8) . . . . ? C38 Ni21 Ni22 Ni24 141.7(16) . . . . ? C41 Ni21 Ni22 Ni24 36.6(4) . . . . ? C37 Ni21 Ni22 Ni24 -76.0(13) 3 . . . ? C42 Ni21 Ni22 Ni24 34.7(4) . . . . ? Ni28 Ni21 Ni22 Ni24 73.51(14) . . . . ? Ni24 Ni21 Ni22 Ni24 -4.40(16) 3 . . . ? Ni27 Ni21 Ni22 Ni24 83.04(9) . . . . ? C38' Ni21 Ni22 Ni23 -85(3) 3 . . . ? C32 Ni21 Ni22 Ni23 -94.8(8) . . . . ? C38 Ni21 Ni22 Ni23 -162.6(16) . . . . ? C41 Ni21 Ni22 Ni23 92.3(4) . . . . ? C37 Ni21 Ni22 Ni23 -20.4(13) 3 . . . ? C42 Ni21 Ni22 Ni23 90.4(5) . . . . ? Ni28 Ni21 Ni22 Ni23 129.19(13) . . . . ? Ni24 Ni21 Ni22 Ni23 51.28(13) 3 . . . ? Ni27 Ni21 Ni22 Ni23 138.72(8) . . . . ? C44' Ni22 Ni23 C43' -12(3) . . . . ? C44 Ni22 Ni23 C43' -10(2) . . . . ? C32 Ni22 Ni23 C43' 89.4(15) . . . . ? C42 Ni22 Ni23 C43' -161.2(14) . . . . ? Ni21 Ni22 Ni23 C43' 140.7(14) . . . . ? Ni25 Ni22 Ni23 C43' -115.8(14) . . . . ? Ni29 Ni22 Ni23 C43' -50.1(14) . . . . ? Ni24 Ni22 Ni23 C43' -118.9(14) . . . . ? C44' Ni22 Ni23 C43 2(3) . . . . ? C44 Ni22 Ni23 C43 4(2) . . . . ? C32 Ni22 Ni23 C43 103.1(12) . . . . ? C42 Ni22 Ni23 C43 -147.5(11) . . . . ? Ni21 Ni22 Ni23 C43 154.4(10) . . . . ? Ni25 Ni22 Ni23 C43 -102.1(10) . . . . ? Ni29 Ni22 Ni23 C43 -36.3(10) . . . . ? Ni24 Ni22 Ni23 C43 -105.1(10) . . . . ? C44' Ni22 Ni23 C35 -103(3) . . . 3 ? C44 Ni22 Ni23 C35 -101(2) . . . 3 ? C32 Ni22 Ni23 C35 -1.8(9) . . . 3 ? C42 Ni22 Ni23 C35 107.6(7) . . . 3 ? Ni21 Ni22 Ni23 C35 49.5(6) . . . 3 ? Ni25 Ni22 Ni23 C35 153.0(6) . . . 3 ? Ni29 Ni22 Ni23 C35 -141.3(6) . . . 3 ? Ni24 Ni22 Ni23 C35 149.9(6) . . . 3 ? C44' Ni22 Ni23 C41 147(3) . . . 3 ? C44 Ni22 Ni23 C41 150(2) . . . 3 ? C32 Ni22 Ni23 C41 -111.2(7) . . . 3 ? C42 Ni22 Ni23 C41 -1.8(6) . . . 3 ? Ni21 Ni22 Ni23 C41 -59.9(4) . . . 3 ? Ni25 Ni22 Ni23 C41 43.6(4) . . . 3 ? Ni29 Ni22 Ni23 C41 109.3(5) . . . 3 ? Ni24 Ni22 Ni23 C41 40.5(4) . . . 3 ? C44' Ni22 Ni23 Ni29 38(3) . . . . ? C44 Ni22 Ni23 Ni29 41(2) . . . . ? C32 Ni22 Ni23 Ni29 139.5(7) . . . . ? C42 Ni22 Ni23 Ni29 -111.1(5) . . . . ? Ni21 Ni22 Ni23 Ni29 -169.3(2) . . . . ? Ni25 Ni22 Ni23 Ni29 -65.8(2) . . . . ? Ni24 Ni22 Ni23 Ni29 -68.8(2) . . . . ? C44' Ni22 Ni23 Ni26 -154(3) . . . 3 ? C44 Ni22 Ni23 Ni26 -152(2) . . . 3 ? C32 Ni22 Ni23 Ni26 -52.9(6) . . . 3 ? C42 Ni22 Ni23 Ni26 56.5(4) . . . 3 ? Ni21 Ni22 Ni23 Ni26 -1.67(10) . . . 3 ? Ni25 Ni22 Ni23 Ni26 101.83(12) . . . 3 ? Ni29 Ni22 Ni23 Ni26 167.6(2) . . . 3 ? Ni24 Ni22 Ni23 Ni26 98.80(10) . . . 3 ? C44' Ni22 Ni23 Ni24 107(3) . . . . ? C44 Ni22 Ni23 Ni24 109(2) . . . . ? C32 Ni22 Ni23 Ni24 -151.7(6) . . . . ? C42 Ni22 Ni23 Ni24 -42.3(4) . . . . ? Ni21 Ni22 Ni23 Ni24 -100.46(9) . . . . ? Ni25 Ni22 Ni23 Ni24 3.03(10) . . . . ? Ni29 Ni22 Ni23 Ni24 68.8(2) . . . . ? C44' Ni22 Ni23 Ni28 102(3) . . . 3 ? C44 Ni22 Ni23 Ni28 104(2) . . . 3 ? C32 Ni22 Ni23 Ni28 -157.0(6) . . . 3 ? C42 Ni22 Ni23 Ni28 -47.6(4) . . . 3 ? Ni21 Ni22 Ni23 Ni28 -105.77(11) . . . 3 ? Ni25 Ni22 Ni23 Ni28 -2.28(16) . . . 3 ? Ni29 Ni22 Ni23 Ni28 63.5(2) . . . 3 ? Ni24 Ni22 Ni23 Ni28 -5.31(10) . . . 3 ? C43' Ni23 Ni24 C45' -24(4) . . . . ? C43 Ni23 Ni24 C45' -16(4) . . . . ? C35 Ni23 Ni24 C45' -161(4) 3 . . . ? C41 Ni23 Ni24 C45' 133(4) 3 . . . ? Ni29 Ni23 Ni24 C45' -29(4) . . . . ? Ni26 Ni23 Ni24 C45' 167(4) 3 . . . ? Ni28 Ni23 Ni24 C45' 73(4) 3 . . . ? Ni22 Ni23 Ni24 C45' -101(4) . . . . ? C43' Ni23 Ni24 C45 -19(3) . . . . ? C43 Ni23 Ni24 C45 -11(3) . . . . ? C35 Ni23 Ni24 C45 -156(3) 3 . . . ? C41 Ni23 Ni24 C45 138(3) 3 . . . ? Ni29 Ni23 Ni24 C45 -24(3) . . . . ? Ni26 Ni23 Ni24 C45 172(3) 3 . . . ? Ni28 Ni23 Ni24 C45 78(3) 3 . . . ? Ni22 Ni23 Ni24 C45 -96(3) . . . . ? C43' Ni23 Ni24 C42 118(2) . . . . ? C43 Ni23 Ni24 C42 125.7(14) . . . . ? C35 Ni23 Ni24 C42 -19.3(11) 3 . . . ? C41 Ni23 Ni24 C42 -85.0(6) 3 . . . ? Ni29 Ni23 Ni24 C42 112.3(5) . . . . ? Ni26 Ni23 Ni24 C42 -51.8(4) 3 . . . ? Ni28 Ni23 Ni24 C42 -145.1(4) 3 . . . ? Ni22 Ni23 Ni24 C42 40.3(4) . . . . ? C43' Ni23 Ni24 C41 -157(2) . . . 3 ? C43 Ni23 Ni24 C41 -149.3(14) . . . 3 ? C35 Ni23 Ni24 C41 65.7(11) 3 . . 3 ? Ni29 Ni23 Ni24 C41 -162.7(6) . . . 3 ? Ni26 Ni23 Ni24 C41 33.2(5) 3 . . 3 ? Ni28 Ni23 Ni24 C41 -60.1(5) 3 . . 3 ? Ni22 Ni23 Ni24 C41 125.3(5) . . . 3 ? C43' Ni23 Ni24 C37 -125(3) . . . . ? C43 Ni23 Ni24 C37 -117(2) . . . . ? C35 Ni23 Ni24 C37 98(2) 3 . . . ? C41 Ni23 Ni24 C37 32.3(19) 3 . . . ? Ni29 Ni23 Ni24 C37 -130.4(18) . . . . ? Ni26 Ni23 Ni24 C37 65.5(18) 3 . . . ? Ni28 Ni23 Ni24 C37 -27.8(18) 3 . . . ? Ni22 Ni23 Ni24 C37 157.6(18) . . . . ? C43' Ni23 Ni24 Ni29 5(2) . . . . ? C43 Ni23 Ni24 Ni29 13.4(14) . . . . ? C35 Ni23 Ni24 Ni29 -131.6(10) 3 . . . ? C41 Ni23 Ni24 Ni29 162.7(6) 3 . . . ? Ni26 Ni23 Ni24 Ni29 -164.0(3) 3 . . . ? Ni28 Ni23 Ni24 Ni29 102.6(3) 3 . . . ? Ni22 Ni23 Ni24 Ni29 -72.0(3) . . . . ? C43' Ni23 Ni24 Ni21 -143(2) . . . 3 ? C43 Ni23 Ni24 Ni21 -134.7(13) . . . 3 ? C35 Ni23 Ni24 Ni21 80.4(10) 3 . . 3 ? C41 Ni23 Ni24 Ni21 14.7(5) 3 . . 3 ? Ni29 Ni23 Ni24 Ni21 -148.0(3) . . . 3 ? Ni26 Ni23 Ni24 Ni21 47.92(11) 3 . . 3 ? Ni28 Ni23 Ni24 Ni21 -45.42(9) 3 . . 3 ? Ni22 Ni23 Ni24 Ni21 140.00(11) . . . 3 ? C43' Ni23 Ni24 Ni22 77(2) . . . . ? C43 Ni23 Ni24 Ni22 85.3(13) . . . . ? C35 Ni23 Ni24 Ni22 -59.6(10) 3 . . . ? C41 Ni23 Ni24 Ni22 -125.3(5) 3 . . . ? Ni29 Ni23 Ni24 Ni22 72.0(3) . . . . ? Ni26 Ni23 Ni24 Ni22 -92.08(11) 3 . . . ? Ni28 Ni23 Ni24 Ni22 174.59(10) 3 . . . ? C43' Ni23 Ni24 Ni28 -97(2) . . . 3 ? C43 Ni23 Ni24 Ni28 -89.2(13) . . . 3 ? C35 Ni23 Ni24 Ni28 125.8(10) 3 . . 3 ? C41 Ni23 Ni24 Ni28 60.1(5) 3 . . 3 ? Ni29 Ni23 Ni24 Ni28 -102.6(3) . . . 3 ? Ni26 Ni23 Ni24 Ni28 93.34(10) 3 . . 3 ? Ni22 Ni23 Ni24 Ni28 -174.59(10) . . . 3 ? C43' Ni23 Ni24 Ni26 147(2) . . . . ? C43 Ni23 Ni24 Ni26 155.3(13) . . . . ? C35 Ni23 Ni24 Ni26 10.4(10) 3 . . . ? C41 Ni23 Ni24 Ni26 -55.3(5) 3 . . . ? Ni29 Ni23 Ni24 Ni26 142.0(3) . . . . ? Ni26 Ni23 Ni24 Ni26 -22.1(2) 3 . . . ? Ni28 Ni23 Ni24 Ni26 -115.42(15) 3 . . . ? Ni22 Ni23 Ni24 Ni26 70.00(15) . . . . ? C43' Ni23 Ni24 Ni25 74(2) . . . . ? C43 Ni23 Ni24 Ni25 82.2(13) . . . . ? C35 Ni23 Ni24 Ni25 -62.7(10) 3 . . . ? C41 Ni23 Ni24 Ni25 -128.4(5) 3 . . . ? Ni29 Ni23 Ni24 Ni25 68.9(3) . . . . ? Ni26 Ni23 Ni24 Ni25 -95.18(13) 3 . . . ? Ni28 Ni23 Ni24 Ni25 171.48(13) 3 . . . ? Ni22 Ni23 Ni24 Ni25 -3.11(11) . . . . ? C44' Ni22 Ni24 C45' 9(4) . . . . ? C44 Ni22 Ni24 C45' 22(4) . . . . ? C32 Ni22 Ni24 C45' 149(3) . . . . ? C42 Ni22 Ni24 C45' -137(3) . . . . ? Ni21 Ni22 Ni24 C45' -175(3) . . . . ? Ni25 Ni22 Ni24 C45' -73(3) . . . . ? Ni29 Ni22 Ni24 C45' 43(3) . . . . ? Ni23 Ni22 Ni24 C45' 104(3) . . . . ? C44' Ni22 Ni24 C45 5(4) . . . . ? C44 Ni22 Ni24 C45 18(3) . . . . ? C32 Ni22 Ni24 C45 145(3) . . . . ? C42 Ni22 Ni24 C45 -141(2) . . . . ? Ni21 Ni22 Ni24 C45 -180(2) . . . . ? Ni25 Ni22 Ni24 C45 -77(2) . . . . ? Ni29 Ni22 Ni24 C45 38(2) . . . . ? Ni23 Ni22 Ni24 C45 99(2) . . . . ? C44' Ni22 Ni24 C42 146(3) . . . . ? C44 Ni22 Ni24 C42 159(2) . . . . ? C32 Ni22 Ni24 C42 -74.1(11) . . . . ? Ni21 Ni22 Ni24 C42 -38.7(5) . . . . ? Ni25 Ni22 Ni24 C42 63.5(5) . . . . ? Ni29 Ni22 Ni24 C42 179.4(5) . . . . ? Ni23 Ni22 Ni24 C42 -119.5(5) . . . . ? C44' Ni22 Ni24 C41 -132(3) . . . 3 ? C44 Ni22 Ni24 C41 -120(2) . . . 3 ? C32 Ni22 Ni24 C41 7.4(10) . . . 3 ? C42 Ni22 Ni24 C41 81.5(6) . . . 3 ? Ni21 Ni22 Ni24 C41 42.8(4) . . . 3 ? Ni25 Ni22 Ni24 C41 145.0(4) . . . 3 ? Ni29 Ni22 Ni24 C41 -99.1(4) . . . 3 ? Ni23 Ni22 Ni24 C41 -38.0(4) . . . 3 ? C44' Ni22 Ni24 C37 104(3) . . . . ? C44 Ni22 Ni24 C37 117(3) . . . . ? C32 Ni22 Ni24 C37 -115.7(18) . . . . ? C42 Ni22 Ni24 C37 -41.5(16) . . . . ? Ni21 Ni22 Ni24 C37 -80.2(15) . . . . ? Ni25 Ni22 Ni24 C37 21.9(15) . . . . ? Ni29 Ni22 Ni24 C37 137.9(16) . . . . ? Ni23 Ni22 Ni24 C37 -161.1(15) . . . . ? C44' Ni22 Ni24 Ni29 -33(3) . . . . ? C44 Ni22 Ni24 Ni29 -21(2) . . . . ? C32 Ni22 Ni24 Ni29 106.4(10) . . . . ? C42 Ni22 Ni24 Ni29 -179.4(5) . . . . ? Ni21 Ni22 Ni24 Ni29 141.9(2) . . . . ? Ni25 Ni22 Ni24 Ni29 -116.0(2) . . . . ? Ni23 Ni22 Ni24 Ni29 61.0(2) . . . . ? C44' Ni22 Ni24 Ni21 -170(3) . . . 3 ? C44 Ni22 Ni24 Ni21 -157(2) . . . 3 ? C32 Ni22 Ni24 Ni21 -29.9(10) . . . 3 ? C42 Ni22 Ni24 Ni21 44.2(5) . . . 3 ? Ni21 Ni22 Ni24 Ni21 5.5(2) . . . 3 ? Ni25 Ni22 Ni24 Ni21 107.69(16) . . . 3 ? Ni29 Ni22 Ni24 Ni21 -136.3(3) . . . 3 ? Ni23 Ni22 Ni24 Ni21 -75.32(15) . . . 3 ? C44' Ni22 Ni24 Ni23 -94(3) . . . . ? C44 Ni22 Ni24 Ni23 -82(2) . . . . ? C32 Ni22 Ni24 Ni23 45.4(9) . . . . ? C42 Ni22 Ni24 Ni23 119.5(5) . . . . ? Ni21 Ni22 Ni24 Ni23 80.86(10) . . . . ? Ni25 Ni22 Ni24 Ni23 -176.99(10) . . . . ? Ni29 Ni22 Ni24 Ni23 -61.0(2) . . . . ? C44' Ni22 Ni24 Ni28 -89(3) . . . 3 ? C44 Ni22 Ni24 Ni28 -76(2) . . . 3 ? C32 Ni22 Ni24 Ni28 51.2(10) . . . 3 ? C42 Ni22 Ni24 Ni28 125.4(5) . . . 3 ? Ni21 Ni22 Ni24 Ni28 86.68(13) . . . 3 ? Ni25 Ni22 Ni24 Ni28 -171.17(13) . . . 3 ? Ni29 Ni22 Ni24 Ni28 -55.2(2) . . . 3 ? Ni23 Ni22 Ni24 Ni28 5.82(11) . . . 3 ? C44' Ni22 Ni24 Ni26 125(3) . . . . ? C44 Ni22 Ni24 Ni26 138(2) . . . . ? C32 Ni22 Ni24 Ni26 -95.4(9) . . . . ? C42 Ni22 Ni24 Ni26 -21.2(5) . . . . ? Ni21 Ni22 Ni24 Ni26 -59.89(10) . . . . ? Ni25 Ni22 Ni24 Ni26 42.26(9) . . . . ? Ni29 Ni22 Ni24 Ni26 158.2(2) . . . . ? Ni23 Ni22 Ni24 Ni26 -140.75(10) . . . . ? C44' Ni22 Ni24 Ni25 83(3) . . . . ? C44 Ni22 Ni24 Ni25 95(2) . . . . ? C32 Ni22 Ni24 Ni25 -137.6(10) . . . . ? C42 Ni22 Ni24 Ni25 -63.5(5) . . . . ? Ni21 Ni22 Ni24 Ni25 -102.15(10) . . . . ? Ni29 Ni22 Ni24 Ni25 116.0(2) . . . . ? Ni23 Ni22 Ni24 Ni25 176.99(10) . . . . ? C44' Ni22 Ni25 C33 -8(3) . . . . ? C44 Ni22 Ni25 C33 2(2) . . . . ? C32 Ni22 Ni25 C33 -121.2(12) . . . . ? C42 Ni22 Ni25 C33 165.1(9) . . . . ? Ni21 Ni22 Ni25 C33 -164.9(7) . . . . ? Ni29 Ni22 Ni25 C33 58.3(7) . . . . ? Ni24 Ni22 Ni25 C33 105.0(7) . . . . ? Ni23 Ni22 Ni25 C33 102.1(7) . . . . ? C44' Ni22 Ni25 C39 -158(4) . . . . ? C44 Ni22 Ni25 C39 -148(4) . . . . ? C32 Ni22 Ni25 C39 89(4) . . . . ? C42 Ni22 Ni25 C39 15(3) . . . . ? Ni21 Ni22 Ni25 C39 45(3) . . . . ? Ni29 Ni22 Ni25 C39 -92(3) . . . . ? Ni24 Ni22 Ni25 C39 -45(3) . . . . ? Ni23 Ni22 Ni25 C39 -48(3) . . . . ? C44' Ni22 Ni25 C34 95(3) . . . . ? C44 Ni22 Ni25 C34 104(2) . . . . ? C32 Ni22 Ni25 C34 -18.4(12) . . . . ? C42 Ni22 Ni25 C34 -92.1(8) . . . . ? Ni21 Ni22 Ni25 C34 -62.1(6) . . . . ? Ni29 Ni22 Ni25 C34 161.1(6) . . . . ? Ni24 Ni22 Ni25 C34 -152.2(6) . . . . ? Ni23 Ni22 Ni25 C34 -155.0(6) . . . . ? C44' Ni22 Ni25 C42 -173(3) . . . . ? C44 Ni22 Ni25 C42 -164(2) . . . . ? C32 Ni22 Ni25 C42 73.7(11) . . . . ? Ni21 Ni22 Ni25 C42 30.0(5) . . . . ? Ni29 Ni22 Ni25 C42 -106.8(5) . . . . ? Ni24 Ni22 Ni25 C42 -60.1(5) . . . . ? Ni23 Ni22 Ni25 C42 -63.0(5) . . . . ? C44' Ni22 Ni25 C39' -137(4) . . . . ? C44 Ni22 Ni25 C39' -127(3) . . . . ? C32 Ni22 Ni25 C39' 110(3) . . . . ? C42 Ni22 Ni25 C39' 36(2) . . . . ? Ni21 Ni22 Ni25 C39' 66(2) . . . . ? Ni29 Ni22 Ni25 C39' -71(2) . . . . ? Ni24 Ni22 Ni25 C39' -24(2) . . . . ? Ni23 Ni22 Ni25 C39' -27(2) . . . . ? C44' Ni22 Ni25 Ni27 133(3) . . . . ? C44 Ni22 Ni25 Ni27 143(2) . . . . ? C32 Ni22 Ni25 Ni27 20.3(10) . . . . ? C42 Ni22 Ni25 Ni27 -53.3(5) . . . . ? Ni21 Ni22 Ni25 Ni27 -23.33(11) . . . . ? Ni29 Ni22 Ni25 Ni27 -160.15(18) . . . . ? Ni24 Ni22 Ni25 Ni27 -113.43(9) . . . . ? Ni23 Ni22 Ni25 Ni27 -116.29(12) . . . . ? C44' Ni22 Ni25 Ni26 -161(3) . . . . ? C44 Ni22 Ni25 Ni26 -151(2) . . . . ? C32 Ni22 Ni25 Ni26 85.9(10) . . . . ? C42 Ni22 Ni25 Ni26 12.2(5) . . . . ? Ni21 Ni22 Ni25 Ni26 42.22(13) . . . . ? Ni29 Ni22 Ni25 Ni26 -94.61(19) . . . . ? Ni24 Ni22 Ni25 Ni26 -47.89(10) . . . . ? Ni23 Ni22 Ni25 Ni26 -50.75(14) . . . . ? C44' Ni22 Ni25 Ni24 -113(3) . . . . ? C44 Ni22 Ni25 Ni24 -103(2) . . . . ? C32 Ni22 Ni25 Ni24 133.8(10) . . . . ? C42 Ni22 Ni25 Ni24 60.1(5) . . . . ? Ni21 Ni22 Ni25 Ni24 90.11(10) . . . . ? Ni29 Ni22 Ni25 Ni24 -46.72(17) . . . . ? Ni23 Ni22 Ni25 Ni24 -2.86(10) . . . . ? C45' Ni24 Ni25 C33 20(2) . . . . ? C45 Ni24 Ni25 C33 11.9(18) . . . . ? C42 Ni24 Ni25 C33 -153.1(9) . . . . ? C41 Ni24 Ni25 C33 -154.8(9) 3 . . . ? C37 Ni24 Ni25 C33 99.4(12) . . . . ? Ni29 Ni24 Ni25 C33 -40.9(8) . . . . ? Ni21 Ni24 Ni25 C33 135.5(8) 3 . . . ? Ni23 Ni24 Ni25 C33 -90.6(8) . . . . ? Ni22 Ni24 Ni25 C33 -93.9(8) . . . . ? Ni28 Ni24 Ni25 C33 29.8(11) 3 . . . ? Ni26 Ni24 Ni25 C33 141.4(8) . . . . ? C45' Ni24 Ni25 C39 -86(3) . . . . ? C45 Ni24 Ni25 C39 -93(2) . . . . ? C42 Ni24 Ni25 C39 101.5(17) . . . . ? C41 Ni24 Ni25 C39 99.9(17) 3 . . . ? C37 Ni24 Ni25 C39 -5.9(19) . . . . ? Ni29 Ni24 Ni25 C39 -146.2(16) . . . . ? Ni21 Ni24 Ni25 C39 30.2(16) 3 . . . ? Ni23 Ni24 Ni25 C39 164.1(16) . . . . ? Ni22 Ni24 Ni25 C39 160.8(16) . . . . ? Ni28 Ni24 Ni25 C39 -75.5(18) 3 . . . ? Ni26 Ni24 Ni25 C39 36.1(16) . . . . ? C45' Ni24 Ni25 C34 176(2) . . . . ? C45 Ni24 Ni25 C34 168.1(19) . . . . ? C42 Ni24 Ni25 C34 3.1(12) . . . . ? C41 Ni24 Ni25 C34 1.4(13) 3 . . . ? C37 Ni24 Ni25 C34 -104.4(15) . . . . ? Ni29 Ni24 Ni25 C34 115.3(11) . . . . ? Ni21 Ni24 Ni25 C34 -68.3(11) 3 . . . ? Ni23 Ni24 Ni25 C34 65.6(11) . . . . ? Ni22 Ni24 Ni25 C34 62.3(11) . . . . ? Ni28 Ni24 Ni25 C34 -174.0(12) 3 . . . ? Ni26 Ni24 Ni25 C34 -62.4(11) . . . . ? C45' Ni24 Ni25 C42 173(2) . . . . ? C45 Ni24 Ni25 C42 165.1(17) . . . . ? C41 Ni24 Ni25 C42 -1.7(7) 3 . . . ? C37 Ni24 Ni25 C42 -107.4(10) . . . . ? Ni29 Ni24 Ni25 C42 112.3(5) . . . . ? Ni21 Ni24 Ni25 C42 -71.4(5) 3 . . . ? Ni23 Ni24 Ni25 C42 62.6(5) . . . . ? Ni22 Ni24 Ni25 C42 59.2(5) . . . . ? Ni28 Ni24 Ni25 C42 -177.1(9) 3 . . . ? Ni26 Ni24 Ni25 C42 -65.4(5) . . . . ? C45' Ni24 Ni25 C39' -81(2) . . . . ? C45 Ni24 Ni25 C39' -89(2) . . . . ? C42 Ni24 Ni25 C39' 105.9(15) . . . . ? C41 Ni24 Ni25 C39' 104.2(15) 3 . . . ? C37 Ni24 Ni25 C39' -1.5(17) . . . . ? Ni29 Ni24 Ni25 C39' -141.9(14) . . . . ? Ni21 Ni24 Ni25 C39' 34.5(14) 3 . . . ? Ni23 Ni24 Ni25 C39' 168.4(14) . . . . ? Ni22 Ni24 Ni25 C39' 165.1(14) . . . . ? Ni28 Ni24 Ni25 C39' -71.2(16) 3 . . . ? Ni26 Ni24 Ni25 C39' 40.4(14) . . . . ? C45' Ni24 Ni25 Ni27 -179(2) . . . . ? C45 Ni24 Ni25 Ni27 172.7(16) . . . . ? C42 Ni24 Ni25 Ni27 7.6(5) . . . . ? C41 Ni24 Ni25 Ni27 6.0(6) 3 . . . ? C37 Ni24 Ni25 Ni27 -99.8(9) . . . . ? Ni29 Ni24 Ni25 Ni27 119.9(2) . . . . ? Ni21 Ni24 Ni25 Ni27 -63.74(15) 3 . . . ? Ni23 Ni24 Ni25 Ni27 70.19(14) . . . . ? Ni22 Ni24 Ni25 Ni27 66.85(10) . . . . ? Ni28 Ni24 Ni25 Ni27 -169.4(7) 3 . . . ? Ni26 Ni24 Ni25 Ni27 -57.81(10) . . . . ? C45' Ni24 Ni25 Ni26 -122(2) . . . . ? C45 Ni24 Ni25 Ni26 -129.5(16) . . . . ? C42 Ni24 Ni25 Ni26 65.4(5) . . . . ? C41 Ni24 Ni25 Ni26 63.8(5) 3 . . . ? C37 Ni24 Ni25 Ni26 -42.0(9) . . . . ? Ni29 Ni24 Ni25 Ni26 177.7(2) . . . . ? Ni21 Ni24 Ni25 Ni26 -5.93(12) 3 . . . ? Ni23 Ni24 Ni25 Ni26 128.00(13) . . . . ? Ni22 Ni24 Ni25 Ni26 124.66(11) . . . . ? Ni28 Ni24 Ni25 Ni26 -111.6(7) 3 . . . ? C45' Ni24 Ni25 Ni22 114(2) . . . . ? C45 Ni24 Ni25 Ni22 105.8(16) . . . . ? C42 Ni24 Ni25 Ni22 -59.2(5) . . . . ? C41 Ni24 Ni25 Ni22 -60.9(5) 3 . . . ? C37 Ni24 Ni25 Ni22 -166.6(9) . . . . ? Ni29 Ni24 Ni25 Ni22 53.1(2) . . . . ? Ni21 Ni24 Ni25 Ni22 -130.59(13) 3 . . . ? Ni23 Ni24 Ni25 Ni22 3.34(12) . . . . ? Ni28 Ni24 Ni25 Ni22 123.7(7) 3 . . . ? Ni26 Ni24 Ni25 Ni22 -124.66(11) . . . . ? C33 Ni25 Ni26 C39' 27(2) . . . . ? C39 Ni25 Ni26 C39' -20(3) . . . . ? C34 Ni25 Ni26 C39' -95(2) . . . . ? C42 Ni25 Ni26 C39' 170(2) . . . . ? Ni27 Ni25 Ni26 C39' -130(2) . . . . ? Ni22 Ni25 Ni26 C39' 159(2) . . . . ? Ni24 Ni25 Ni26 C39' 112(2) . . . . ? C33 Ni25 Ni26 C35 83.0(16) . . . . ? C39 Ni25 Ni26 C35 36(2) . . . . ? C34 Ni25 Ni26 C35 -39.8(13) . . . . ? C42 Ni25 Ni26 C35 -134.5(12) . . . . ? C39' Ni25 Ni26 C35 56(2) . . . . ? Ni27 Ni25 Ni26 C35 -74.0(11) . . . . ? Ni22 Ni25 Ni26 C35 -145.8(11) . . . . ? Ni24 Ni25 Ni26 C35 167.8(11) . . . . ? C33 Ni25 Ni26 C39 47(2) . . . . ? C34 Ni25 Ni26 C39 -76(2) . . . . ? C42 Ni25 Ni26 C39 -170(2) . . . . ? C39' Ni25 Ni26 C39 20(3) . . . . ? Ni27 Ni25 Ni26 C39 -110(2) . . . . ? Ni22 Ni25 Ni26 C39 178(2) . . . . ? Ni24 Ni25 Ni26 C39 132(2) . . . . ? C33 Ni25 Ni26 C37 -39.4(15) . . . . ? C39 Ni25 Ni26 C37 -86(2) . . . . ? C34 Ni25 Ni26 C37 -162.2(11) . . . . ? C42 Ni25 Ni26 C37 103.0(10) . . . . ? C39' Ni25 Ni26 C37 -67(2) . . . . ? Ni27 Ni25 Ni26 C37 163.6(9) . . . . ? Ni22 Ni25 Ni26 C37 91.8(9) . . . . ? Ni24 Ni25 Ni26 C37 45.4(9) . . . . ? C33 Ni25 Ni26 C42 -142.4(13) . . . . ? C39 Ni25 Ni26 C42 170(2) . . . . ? C34 Ni25 Ni26 C42 94.8(7) . . . . ? C39' Ni25 Ni26 C42 -170(2) . . . . ? Ni27 Ni25 Ni26 C42 60.6(5) . . . . ? Ni22 Ni25 Ni26 C42 -11.2(5) . . . . ? Ni24 Ni25 Ni26 C42 -57.6(5) . . . . ? C33 Ni25 Ni26 C41 -163.6(12) . . . . ? C39 Ni25 Ni26 C41 149(2) . . . . ? C34 Ni25 Ni26 C41 73.6(7) . . . . ? C42 Ni25 Ni26 C41 -21.2(6) . . . . ? C39' Ni25 Ni26 C41 169(2) . . . . ? Ni27 Ni25 Ni26 C41 39.4(3) . . . . ? Ni22 Ni25 Ni26 C41 -32.4(4) . . . . ? Ni24 Ni25 Ni26 C41 -78.8(3) . . . . ? C33 Ni25 Ni26 Ni23 172.3(12) . . . 3 ? C39 Ni25 Ni26 Ni23 125(2) . . . 3 ? C34 Ni25 Ni26 Ni23 49.5(6) . . . 3 ? C42 Ni25 Ni26 Ni23 -45.3(5) . . . 3 ? C39' Ni25 Ni26 Ni23 145(2) . . . 3 ? Ni27 Ni25 Ni26 Ni23 15.26(15) . . . 3 ? Ni22 Ni25 Ni26 Ni23 -56.54(18) . . . 3 ? Ni24 Ni25 Ni26 Ni23 -102.94(15) . . . 3 ? C33 Ni25 Ni26 Ni24 -84.8(12) . . . . ? C39 Ni25 Ni26 Ni24 -132(2) . . . . ? C34 Ni25 Ni26 Ni24 152.4(6) . . . . ? C42 Ni25 Ni26 Ni24 57.6(5) . . . . ? C39' Ni25 Ni26 Ni24 -112(2) . . . . ? Ni27 Ni25 Ni26 Ni24 118.20(9) . . . . ? Ni22 Ni25 Ni26 Ni24 46.41(9) . . . . ? C33 Ni25 Ni26 Ni27 157.0(12) . . . . ? C39 Ni25 Ni26 Ni27 110(2) . . . . ? C34 Ni25 Ni26 Ni27 34.2(6) . . . . ? C42 Ni25 Ni26 Ni27 -60.6(5) . . . . ? C39' Ni25 Ni26 Ni27 130(2) . . . . ? Ni22 Ni25 Ni26 Ni27 -71.79(10) . . . . ? Ni24 Ni25 Ni26 Ni27 -118.20(9) . . . . ? C45' Ni24 Ni26 C39' 15(4) . . . . ? C45 Ni24 Ni26 C39' 9(3) . . . . ? C42 Ni24 Ni26 C39' -116.5(18) . . . . ? C41 Ni24 Ni26 C39' 165.0(18) 3 . . . ? C37 Ni24 Ni26 C39' 67(2) . . . . ? Ni29 Ni24 Ni26 C39' -56.2(18) . . . . ? Ni21 Ni24 Ni26 C39' 123.1(18) 3 . . . ? Ni23 Ni24 Ni26 C39' -156.0(18) . . . . ? Ni22 Ni24 Ni26 C39' -96.3(18) . . . . ? Ni28 Ni24 Ni26 C39' 118.1(18) 3 . . . ? Ni25 Ni24 Ni26 C39' -51.7(18) . . . . ? C45' Ni24 Ni26 C35 -103(4) . . . . ? C45 Ni24 Ni26 C35 -109(3) . . . . ? C42 Ni24 Ni26 C35 125.6(11) . . . . ? C41 Ni24 Ni26 C35 47.1(10) 3 . . . ? C37 Ni24 Ni26 C35 -50.5(16) . . . . ? Ni29 Ni24 Ni26 C35 -174.1(10) . . . . ? Ni21 Ni24 Ni26 C35 5.2(9) 3 . . . ? Ni23 Ni24 Ni26 C35 86.1(9) . . . . ? Ni22 Ni24 Ni26 C35 145.8(9) . . . . ? Ni28 Ni24 Ni26 C35 0.3(10) 3 . . . ? Ni25 Ni24 Ni26 C35 -169.6(9) . . . . ? C45' Ni24 Ni26 C39 30(4) . . . . ? C45 Ni24 Ni26 C39 24(3) . . . . ? C42 Ni24 Ni26 C39 -101.2(15) . . . . ? C41 Ni24 Ni26 C39 -179.7(15) 3 . . . ? C37 Ni24 Ni26 C39 82.7(19) . . . . ? Ni29 Ni24 Ni26 C39 -40.9(15) . . . . ? Ni21 Ni24 Ni26 C39 138.4(14) 3 . . . ? Ni23 Ni24 Ni26 C39 -140.7(14) . . . . ? Ni22 Ni24 Ni26 C39 -81.0(14) . . . . ? Ni28 Ni24 Ni26 C39 133.5(14) 3 . . . ? Ni25 Ni24 Ni26 C39 -36.4(14) . . . . ? C45' Ni24 Ni26 C37 -52(4) . . . . ? C45 Ni24 Ni26 C37 -59(3) . . . . ? C42 Ni24 Ni26 C37 176.1(14) . . . . ? C41 Ni24 Ni26 C37 97.6(14) 3 . . . ? Ni29 Ni24 Ni26 C37 -123.6(14) . . . . ? Ni21 Ni24 Ni26 C37 55.7(13) 3 . . . ? Ni23 Ni24 Ni26 C37 136.6(13) . . . . ? Ni22 Ni24 Ni26 C37 -163.7(13) . . . . ? Ni28 Ni24 Ni26 C37 50.7(13) 3 . . . ? Ni25 Ni24 Ni26 C37 -119.1(13) . . . . ? C45' Ni24 Ni26 C42 132(4) . . . . ? C45 Ni24 Ni26 C42 125(3) . . . . ? C41 Ni24 Ni26 C42 -78.5(6) 3 . . . ? C37 Ni24 Ni26 C42 -176.1(14) . . . . ? Ni29 Ni24 Ni26 C42 60.4(6) . . . . ? Ni21 Ni24 Ni26 C42 -120.4(5) 3 . . . ? Ni23 Ni24 Ni26 C42 -39.5(5) . . . . ? Ni22 Ni24 Ni26 C42 20.2(5) . . . . ? Ni28 Ni24 Ni26 C42 -125.3(5) 3 . . . ? Ni25 Ni24 Ni26 C42 64.8(5) . . . . ? C45' Ni24 Ni26 C41 159(4) . . . . ? C45 Ni24 Ni26 C41 153(3) . . . . ? C42 Ni24 Ni26 C41 27.5(6) . . . . ? C41 Ni24 Ni26 C41 -51.0(7) 3 . . . ? C37 Ni24 Ni26 C41 -148.5(14) . . . . ? Ni29 Ni24 Ni26 C41 87.9(6) . . . . ? Ni21 Ni24 Ni26 C41 -92.8(4) 3 . . . ? Ni23 Ni24 Ni26 C41 -12.0(4) . . . . ? Ni22 Ni24 Ni26 C41 47.7(4) . . . . ? Ni28 Ni24 Ni26 C41 -97.8(4) 3 . . . ? Ni25 Ni24 Ni26 C41 92.4(4) . . . . ? C45' Ni24 Ni26 Ni23 -165(4) . . . 3 ? C45 Ni24 Ni26 Ni23 -171(3) . . . 3 ? C42 Ni24 Ni26 Ni23 64.0(5) . . . 3 ? C41 Ni24 Ni26 Ni23 -14.5(4) 3 . . 3 ? C37 Ni24 Ni26 Ni23 -112.1(13) . . . 3 ? Ni29 Ni24 Ni26 Ni23 124.3(4) . . . 3 ? Ni21 Ni24 Ni26 Ni23 -56.40(11) 3 . . 3 ? Ni23 Ni24 Ni26 Ni23 24.5(2) . . . 3 ? Ni22 Ni24 Ni26 Ni23 84.18(12) . . . 3 ? Ni28 Ni24 Ni26 Ni23 -61.36(16) 3 . . 3 ? Ni25 Ni24 Ni26 Ni23 128.79(13) . . . 3 ? C45' Ni24 Ni26 Ni25 67(4) . . . . ? C45 Ni24 Ni26 Ni25 61(3) . . . . ? C42 Ni24 Ni26 Ni25 -64.8(5) . . . . ? C41 Ni24 Ni26 Ni25 -143.3(4) 3 . . . ? C37 Ni24 Ni26 Ni25 119.1(13) . . . . ? Ni29 Ni24 Ni26 Ni25 -4.5(4) . . . . ? Ni21 Ni24 Ni26 Ni25 174.81(11) 3 . . . ? Ni23 Ni24 Ni26 Ni25 -104.33(16) . . . . ? Ni22 Ni24 Ni26 Ni25 -44.61(9) . . . . ? Ni28 Ni24 Ni26 Ni25 169.85(14) 3 . . . ? C45' Ni24 Ni26 Ni27 113(4) . . . . ? C45 Ni24 Ni26 Ni27 107(3) . . . . ? C42 Ni24 Ni26 Ni27 -18.7(5) . . . . ? C41 Ni24 Ni26 Ni27 -97.2(4) 3 . . . ? C37 Ni24 Ni26 Ni27 165.2(13) . . . . ? Ni29 Ni24 Ni26 Ni27 41.6(4) . . . . ? Ni21 Ni24 Ni26 Ni27 -139.07(9) 3 . . . ? Ni23 Ni24 Ni26 Ni27 -58.20(16) . . . . ? Ni22 Ni24 Ni26 Ni27 1.52(10) . . . . ? Ni28 Ni24 Ni26 Ni27 -144.02(12) 3 . . . ? Ni25 Ni24 Ni26 Ni27 46.13(8) . . . . ? C33 Ni25 Ni27 C36 -35(2) . . . . ? C39 Ni25 Ni27 C36 75(3) . . . . ? C34 Ni25 Ni27 C36 -8(2) . . . . ? C42 Ni25 Ni27 C36 -177(2) . . . . ? C39' Ni25 Ni27 C36 90(2) . . . . ? Ni26 Ni25 Ni27 C36 123(2) . . . . ? Ni22 Ni25 Ni27 C36 -130(2) . . . . ? Ni24 Ni25 Ni27 C36 176(2) . . . . ? C33 Ni25 Ni27 C34 -27.5(14) . . . . ? C39 Ni25 Ni27 C34 82.9(17) . . . . ? C42 Ni25 Ni27 C34 -169.7(9) . . . . ? C39' Ni25 Ni27 C34 97.2(15) . . . . ? Ni26 Ni25 Ni27 C34 130.1(8) . . . . ? Ni22 Ni25 Ni27 C34 -122.4(8) . . . . ? Ni24 Ni25 Ni27 C34 -176.8(8) . . . . ? C33 Ni25 Ni27 C42 142.2(12) . . . . ? C39 Ni25 Ni27 C42 -107.4(16) . . . . ? C34 Ni25 Ni27 C42 169.7(9) . . . . ? C39' Ni25 Ni27 C42 -93.1(14) . . . . ? Ni26 Ni25 Ni27 C42 -60.2(4) . . . . ? Ni22 Ni25 Ni27 C42 47.3(4) . . . . ? Ni24 Ni25 Ni27 C42 -7.1(4) . . . . ? C33 Ni25 Ni27 C41 162.2(12) . . . . ? C39 Ni25 Ni27 C41 -87.3(16) . . . . ? C34 Ni25 Ni27 C41 -170.3(8) . . . . ? C42 Ni25 Ni27 C41 20.0(5) . . . . ? C39' Ni25 Ni27 C41 -73.1(14) . . . . ? Ni26 Ni25 Ni27 C41 -40.1(3) . . . . ? Ni22 Ni25 Ni27 C41 67.3(3) . . . . ? Ni24 Ni25 Ni27 C41 13.0(3) . . . . ? C33 Ni25 Ni27 Ni28 159.1(12) . . . . ? C39 Ni25 Ni27 Ni28 -90.4(15) . . . . ? C34 Ni25 Ni27 Ni28 -173.3(8) . . . . ? C42 Ni25 Ni27 Ni28 17.0(5) . . . . ? C39' Ni25 Ni27 Ni28 -76.2(13) . . . . ? Ni26 Ni25 Ni27 Ni28 -43.19(18) . . . . ? Ni22 Ni25 Ni27 Ni28 64.29(18) . . . . ? Ni24 Ni25 Ni27 Ni28 9.9(2) . . . . ? C33 Ni25 Ni27 Ni26 -157.7(12) . . . . ? C39 Ni25 Ni27 Ni26 -47.2(15) . . . . ? C34 Ni25 Ni27 Ni26 -130.1(8) . . . . ? C42 Ni25 Ni27 Ni26 60.2(4) . . . . ? C39' Ni25 Ni27 Ni26 -33.0(13) . . . . ? Ni22 Ni25 Ni27 Ni26 107.49(9) . . . . ? Ni24 Ni25 Ni27 Ni26 53.11(8) . . . . ? C33 Ni25 Ni27 Ni21 114.1(12) . . . . ? C39 Ni25 Ni27 Ni21 -135.5(15) . . . . ? C34 Ni25 Ni27 Ni21 141.6(8) . . . . ? C42 Ni25 Ni27 Ni21 -28.1(4) . . . . ? C39' Ni25 Ni27 Ni21 -121.2(13) . . . . ? Ni26 Ni25 Ni27 Ni21 -88.27(9) . . . . ? Ni22 Ni25 Ni27 Ni21 19.21(9) . . . . ? Ni24 Ni25 Ni27 Ni21 -35.17(11) . . . . ? C39' Ni26 Ni27 C36 -117(2) . . . . ? C35 Ni26 Ni27 C36 -9.5(11) . . . . ? C39 Ni26 Ni27 C36 -110.5(18) . . . . ? C37 Ni26 Ni27 C36 171(2) . . . . ? C42 Ni26 Ni27 C36 130.3(10) . . . . ? C41 Ni26 Ni27 C36 78.9(10) . . . . ? Ni23 Ni26 Ni27 C36 32.4(9) 3 . . . ? Ni25 Ni26 Ni27 C36 -158.5(9) . . . . ? Ni24 Ni26 Ni27 C36 149.2(9) . . . . ? C39' Ni26 Ni27 C34 1(2) . . . . ? C35 Ni26 Ni27 C34 109.4(9) . . . . ? C39 Ni26 Ni27 C34 8.3(17) . . . . ? C37 Ni26 Ni27 C34 -70.1(19) . . . . ? C42 Ni26 Ni27 C34 -110.9(8) . . . . ? C41 Ni26 Ni27 C34 -162.3(8) . . . . ? Ni23 Ni26 Ni27 C34 151.2(7) 3 . . . ? Ni25 Ni26 Ni27 C34 -39.7(7) . . . . ? Ni24 Ni26 Ni27 C34 -91.9(7) . . . . ? C39' Ni26 Ni27 C42 112(2) . . . . ? C35 Ni26 Ni27 C42 -139.7(8) . . . . ? C39 Ni26 Ni27 C42 119.2(17) . . . . ? C37 Ni26 Ni27 C42 40.8(18) . . . . ? C41 Ni26 Ni27 C42 -51.3(6) . . . . ? Ni23 Ni26 Ni27 C42 -97.9(5) 3 . . . ? Ni25 Ni26 Ni27 C42 71.2(5) . . . . ? Ni24 Ni26 Ni27 C42 19.0(5) . . . . ? C39' Ni26 Ni27 C41 164(2) . . . . ? C35 Ni26 Ni27 C41 -88.4(7) . . . . ? C39 Ni26 Ni27 C41 170.6(17) . . . . ? C37 Ni26 Ni27 C41 92.1(18) . . . . ? C42 Ni26 Ni27 C41 51.3(6) . . . . ? Ni23 Ni26 Ni27 C41 -46.6(5) 3 . . . ? Ni25 Ni26 Ni27 C41 122.5(5) . . . . ? Ni24 Ni26 Ni27 C41 70.3(5) . . . . ? C39' Ni26 Ni27 Ni25 41.2(19) . . . . ? C35 Ni26 Ni27 Ni25 149.1(6) . . . . ? C39 Ni26 Ni27 Ni25 48.0(16) . . . . ? C37 Ni26 Ni27 Ni25 -30.4(18) . . . . ? C42 Ni26 Ni27 Ni25 -71.2(5) . . . . ? C41 Ni26 Ni27 Ni25 -122.5(5) . . . . ? Ni23 Ni26 Ni27 Ni25 -169.09(11) 3 . . . ? Ni24 Ni26 Ni27 Ni25 -52.22(9) . . . . ? C39' Ni26 Ni27 Ni28 -163.8(19) . . . . ? C35 Ni26 Ni27 Ni28 -55.9(6) . . . . ? C39 Ni26 Ni27 Ni28 -157.0(16) . . . . ? C37 Ni26 Ni27 Ni28 124.6(18) . . . . ? C42 Ni26 Ni27 Ni28 83.8(5) . . . . ? C41 Ni26 Ni27 Ni28 32.5(5) . . . . ? Ni23 Ni26 Ni27 Ni28 -14.08(9) 3 . . . ? Ni25 Ni26 Ni27 Ni28 155.01(11) . . . . ? Ni24 Ni26 Ni27 Ni28 102.79(9) . . . . ? C39' Ni26 Ni27 Ni21 138.0(19) . . . . ? C35 Ni26 Ni27 Ni21 -114.1(6) . . . . ? C39 Ni26 Ni27 Ni21 144.8(16) . . . . ? C37 Ni26 Ni27 Ni21 66.4(18) . . . . ? C42 Ni26 Ni27 Ni21 25.6(5) . . . . ? C41 Ni26 Ni27 Ni21 -25.7(5) . . . . ? Ni23 Ni26 Ni27 Ni21 -72.28(9) 3 . . . ? Ni25 Ni26 Ni27 Ni21 96.80(10) . . . . ? Ni24 Ni26 Ni27 Ni21 44.58(9) . . . . ? C38' Ni21 Ni27 C36 2(2) 3 . . . ? C32 Ni21 Ni27 C36 109.3(9) . . . . ? C38 Ni21 Ni27 C36 3.1(12) . . . . ? C41 Ni21 Ni27 C36 -107.3(8) . . . . ? C37 Ni21 Ni27 C36 -60.7(19) 3 . . . ? C42 Ni21 Ni27 C36 -158.9(8) . . . . ? Ni22 Ni21 Ni27 C36 149.0(7) . . . . ? Ni28 Ni21 Ni27 C36 -40.5(7) . . . . ? Ni24 Ni21 Ni27 C36 -87.2(7) 3 . . . ? C38' Ni21 Ni27 C34 -121(2) 3 . . . ? C32 Ni21 Ni27 C34 -13.8(12) . . . . ? C38 Ni21 Ni27 C34 -120.1(14) . . . . ? C41 Ni21 Ni27 C34 129.6(11) . . . . ? C37 Ni21 Ni27 C34 176(2) 3 . . . ? C42 Ni21 Ni27 C34 78.0(11) . . . . ? Ni22 Ni21 Ni27 C34 25.9(10) . . . . ? Ni28 Ni21 Ni27 C34 -163.6(10) . . . . ? Ni24 Ni21 Ni27 C34 149.7(10) 3 . . . ? C38' Ni21 Ni27 C42 161(2) 3 . . . ? C32 Ni21 Ni27 C42 -91.8(8) . . . . ? C38 Ni21 Ni27 C42 162.0(12) . . . . ? C41 Ni21 Ni27 C42 51.6(7) . . . . ? C37 Ni21 Ni27 C42 98.2(18) 3 . . . ? Ni22 Ni21 Ni27 C42 -52.1(5) . . . . ? Ni28 Ni21 Ni27 C42 118.4(5) . . . . ? Ni24 Ni21 Ni27 C42 71.7(5) 3 . . . ? C38' Ni21 Ni27 C41 110(2) 3 . . . ? C32 Ni21 Ni27 C41 -143.4(8) . . . . ? C38 Ni21 Ni27 C41 110.3(12) . . . . ? C37 Ni21 Ni27 C41 46.6(18) 3 . . . ? C42 Ni21 Ni27 C41 -51.6(7) . . . . ? Ni22 Ni21 Ni27 C41 -103.7(5) . . . . ? Ni28 Ni21 Ni27 C41 66.7(5) . . . . ? Ni24 Ni21 Ni27 C41 20.1(5) 3 . . . ? C38' Ni21 Ni27 Ni25 -168(2) 3 . . . ? C32 Ni21 Ni27 Ni25 -61.1(7) . . . . ? C38 Ni21 Ni27 Ni25 -167.3(11) . . . . ? C41 Ni21 Ni27 Ni25 82.4(5) . . . . ? C37 Ni21 Ni27 Ni25 128.9(18) 3 . . . ? C42 Ni21 Ni27 Ni25 30.7(5) . . . . ? Ni22 Ni21 Ni27 Ni25 -21.38(10) . . . . ? Ni28 Ni21 Ni27 Ni25 149.11(11) . . . . ? Ni24 Ni21 Ni27 Ni25 102.47(11) 3 . . . ? C38' Ni21 Ni27 Ni28 43(2) 3 . . . ? C32 Ni21 Ni27 Ni28 149.8(7) . . . . ? C38 Ni21 Ni27 Ni28 43.6(11) . . . . ? C41 Ni21 Ni27 Ni28 -66.7(5) . . . . ? C37 Ni21 Ni27 Ni28 -20.2(18) 3 . . . ? C42 Ni21 Ni27 Ni28 -118.4(5) . . . . ? Ni22 Ni21 Ni27 Ni28 -170.48(11) . . . . ? Ni24 Ni21 Ni27 Ni28 -46.64(9) 3 . . . ? C38' Ni21 Ni27 Ni26 136(2) 3 . . . ? C32 Ni21 Ni27 Ni26 -117.2(7) . . . . ? C38 Ni21 Ni27 Ni26 136.6(11) . . . . ? C41 Ni21 Ni27 Ni26 26.2(5) . . . . ? C37 Ni21 Ni27 Ni26 72.8(18) 3 . . . ? C42 Ni21 Ni27 Ni26 -25.4(5) . . . . ? Ni22 Ni21 Ni27 Ni26 -77.51(9) . . . . ? Ni28 Ni21 Ni27 Ni26 92.97(9) . . . . ? Ni24 Ni21 Ni27 Ni26 46.33(10) 3 . . . ? C36 Ni27 Ni28 C31 -14.9(12) . . . . ? C34 Ni27 Ni28 C31 -3(2) . . . . ? C42 Ni27 Ni28 C31 173.6(11) . . . . ? C41 Ni27 Ni28 C31 155.8(11) . . . . ? Ni25 Ni27 Ni28 C31 159.6(10) . . . . ? Ni26 Ni27 Ni28 C31 124.9(10) . . . . ? Ni21 Ni27 Ni28 C31 -144.5(10) . . . . ? C36 Ni27 Ni28 C38 84.7(13) . . . . ? C34 Ni27 Ni28 C38 97(2) . . . . ? C42 Ni27 Ni28 C38 -86.9(11) . . . . ? C41 Ni27 Ni28 C38 -104.6(12) . . . . ? Ni25 Ni27 Ni28 C38 -100.8(11) . . . . ? Ni26 Ni27 Ni28 C38 -135.5(11) . . . . ? Ni21 Ni27 Ni28 C38 -44.9(11) . . . . ? C36 Ni27 Ni28 C41 -170.7(9) . . . . ? C34 Ni27 Ni28 C41 -159(2) . . . . ? C42 Ni27 Ni28 C41 17.7(5) . . . . ? Ni25 Ni27 Ni28 C41 3.8(4) . . . . ? Ni26 Ni27 Ni28 C41 -30.9(4) . . . . ? Ni21 Ni27 Ni28 C41 59.7(4) . . . . ? C34 Ni27 Ni28 C36 12(2) . . . . ? C42 Ni27 Ni28 C36 -171.5(8) . . . . ? C41 Ni27 Ni28 C36 170.7(9) . . . . ? Ni25 Ni27 Ni28 C36 174.6(8) . . . . ? Ni26 Ni27 Ni28 C36 139.9(8) . . . . ? Ni21 Ni27 Ni28 C36 -129.6(7) . . . . ? C36 Ni27 Ni28 Ni21 129.6(7) . . . . ? C34 Ni27 Ni28 Ni21 142(2) . . . . ? C42 Ni27 Ni28 Ni21 -41.9(4) . . . . ? C41 Ni27 Ni28 Ni21 -59.7(4) . . . . ? Ni25 Ni27 Ni28 Ni21 -55.85(18) . . . . ? Ni26 Ni27 Ni28 Ni21 -90.55(9) . . . . ? C36 Ni27 Ni28 Ni23 -127.3(7) . . . 3 ? C34 Ni27 Ni28 Ni23 -115(2) . . . 3 ? C42 Ni27 Ni28 Ni23 61.1(4) . . . 3 ? C41 Ni27 Ni28 Ni23 43.4(4) . . . 3 ? Ni25 Ni27 Ni28 Ni23 47.23(19) . . . 3 ? Ni26 Ni27 Ni28 Ni23 12.52(8) . . . 3 ? Ni21 Ni27 Ni28 Ni23 103.08(9) . . . 3 ? C36 Ni27 Ni28 Ni24 177.5(8) . . . 3 ? C34 Ni27 Ni28 Ni24 -170(2) . . . 3 ? C42 Ni27 Ni28 Ni24 5.9(4) . . . 3 ? C41 Ni27 Ni28 Ni24 -11.8(4) . . . 3 ? Ni25 Ni27 Ni28 Ni24 -8.0(2) . . . 3 ? Ni26 Ni27 Ni28 Ni24 -42.68(10) . . . 3 ? Ni21 Ni27 Ni28 Ni24 47.87(9) . . . 3 ? C38' Ni21 Ni28 C31 -2.8(19) 3 . . . ? C32 Ni21 Ni28 C31 86.2(15) . . . . ? C38 Ni21 Ni28 C31 29.6(17) . . . . ? C41 Ni21 Ni28 C31 -152.0(11) . . . . ? C37 Ni21 Ni28 C31 -45.0(13) 3 . . . ? C42 Ni21 Ni28 C31 -173.4(10) . . . . ? Ni22 Ni21 Ni28 C31 157.1(9) . . . . ? Ni24 Ni21 Ni28 C31 -89.5(9) 3 . . . ? Ni27 Ni21 Ni28 C31 145.6(10) . . . . ? C38' Ni21 Ni28 C38 -32(2) 3 . . . ? C32 Ni21 Ni28 C38 56.7(18) . . . . ? C41 Ni21 Ni28 C38 178.4(15) . . . . ? C37 Ni21 Ni28 C38 -74.6(17) 3 . . . ? C42 Ni21 Ni28 C38 157.1(15) . . . . ? Ni22 Ni21 Ni28 C38 127.5(14) . . . . ? Ni24 Ni21 Ni28 C38 -119.1(14) 3 . . . ? Ni27 Ni21 Ni28 C38 116.0(14) . . . . ? C38' Ni21 Ni28 C41 149.2(17) 3 . . . ? C32 Ni21 Ni28 C41 -121.8(12) . . . . ? C38 Ni21 Ni28 C41 -178.4(15) . . . . ? C37 Ni21 Ni28 C41 107.0(10) 3 . . . ? C42 Ni21 Ni28 C41 -21.4(6) . . . . ? Ni22 Ni21 Ni28 C41 -50.9(5) . . . . ? Ni24 Ni21 Ni28 C41 62.5(5) 3 . . . ? Ni27 Ni21 Ni28 C41 -62.4(5) . . . . ? C38' Ni21 Ni28 C36 -114.6(17) 3 . . . ? C32 Ni21 Ni28 C36 -25.6(12) . . . . ? C38 Ni21 Ni28 C36 -82.2(15) . . . . ? C41 Ni21 Ni28 C36 96.2(7) . . . . ? C37 Ni21 Ni28 C36 -156.8(11) 3 . . . ? C42 Ni21 Ni28 C36 74.8(7) . . . . ? Ni22 Ni21 Ni28 C36 45.3(6) . . . . ? Ni24 Ni21 Ni28 C36 158.7(6) 3 . . . ? Ni27 Ni21 Ni28 C36 33.8(6) . . . . ? C38' Ni21 Ni28 Ni27 -148.4(16) 3 . . . ? C32 Ni21 Ni28 Ni27 -59.4(11) . . . . ? C38 Ni21 Ni28 Ni27 -116.0(14) . . . . ? C41 Ni21 Ni28 Ni27 62.4(5) . . . . ? C37 Ni21 Ni28 Ni27 169.4(9) 3 . . . ? C42 Ni21 Ni28 Ni27 41.0(4) . . . . ? Ni22 Ni21 Ni28 Ni27 11.43(13) . . . . ? Ni24 Ni21 Ni28 Ni27 124.85(10) 3 . . . ? C38' Ni21 Ni28 Ni23 133.0(16) 3 . . 3 ? C32 Ni21 Ni28 Ni23 -138.0(11) . . . 3 ? C38 Ni21 Ni28 Ni23 165.3(14) . . . 3 ? C41 Ni21 Ni28 Ni23 -16.2(5) . . . 3 ? C37 Ni21 Ni28 Ni23 90.8(9) 3 . . 3 ? C42 Ni21 Ni28 Ni23 -37.6(4) . . . 3 ? Ni22 Ni21 Ni28 Ni23 -67.17(15) . . . 3 ? Ni24 Ni21 Ni28 Ni23 46.24(9) 3 . . 3 ? Ni27 Ni21 Ni28 Ni23 -78.60(9) . . . 3 ? C38' Ni21 Ni28 Ni24 86.8(16) 3 . . 3 ? C32 Ni21 Ni28 Ni24 175.8(11) . . . 3 ? C38 Ni21 Ni28 Ni24 119.1(14) . . . 3 ? C41 Ni21 Ni28 Ni24 -62.5(5) . . . 3 ? C37 Ni21 Ni28 Ni24 44.5(9) 3 . . 3 ? C42 Ni21 Ni28 Ni24 -83.8(4) . . . 3 ? Ni22 Ni21 Ni28 Ni24 -113.41(14) . . . 3 ? Ni27 Ni21 Ni28 Ni24 -124.85(10) . . . 3 ? C38 Ni28 C31 O31 132(30) . . . . ? C41 Ni28 C31 O31 -3(31) . . . . ? C36 Ni28 C31 O31 -138(30) . . . . ? Ni27 Ni28 C31 O31 -127(29) . . . . ? Ni21 Ni28 C31 O31 110(30) . . . . ? Ni23 Ni28 C31 O31 -24(30) 3 . . . ? Ni24 Ni28 C31 O31 40(30) 3 . . . ? C44' Ni22 C32 O32 11(4) . . . . ? C44 Ni22 C32 O32 -2(3) . . . . ? C42 Ni22 C32 O32 176(2) . . . . ? Ni25 Ni22 C32 O32 122(2) . . . . ? Ni29 Ni22 C32 O32 -58(3) . . . . ? Ni24 Ni22 C32 O32 -132(2) . . . . ? Ni23 Ni22 C32 O32 -95(3) . . . . ? C44' Ni22 C32 Ni21 -170(3) . . . . ? C44 Ni22 C32 Ni21 177(2) . . . . ? C42 Ni22 C32 Ni21 -4.7(8) . . . . ? Ni25 Ni22 C32 Ni21 -59.0(11) . . . . ? Ni29 Ni22 C32 Ni21 121.6(5) . . . . ? Ni24 Ni22 C32 Ni21 47.4(11) . . . . ? Ni23 Ni22 C32 Ni21 83.9(5) . . . . ? C38' Ni21 C32 O32 5(3) 3 . . . ? C38 Ni21 C32 O32 -40(3) . . . . ? C41 Ni21 C32 O32 -170(2) . . . . ? C37 Ni21 C32 O32 47(3) 3 . . . ? C42 Ni21 C32 O32 -177(2) . . . . ? Ni28 Ni21 C32 O32 -82(3) . . . . ? Ni24 Ni21 C32 O32 90(3) 3 . . . ? Ni27 Ni21 C32 O32 -128(2) . . . . ? C38' Ni21 C32 Ni22 -174.2(17) 3 . . . ? C38 Ni21 C32 Ni22 140.8(12) . . . . ? C41 Ni21 C32 Ni22 10.7(13) . . . . ? C37 Ni21 C32 Ni22 -132.3(11) 3 . . . ? C42 Ni21 C32 Ni22 4.1(7) . . . . ? Ni28 Ni21 C32 Ni22 98.9(10) . . . . ? Ni24 Ni21 C32 Ni22 -89.2(13) 3 . . . ? Ni27 Ni21 C32 Ni22 53.2(6) . . . . ? C39 Ni25 C33 O33 -145(14) . . . . ? C34 Ni25 C33 O33 -57(14) . . . . ? C42 Ni25 C33 O33 70(15) . . . . ? C39' Ni25 C33 O33 -161(14) . . . . ? Ni27 Ni25 C33 O33 -37(15) . . . . ? Ni26 Ni25 C33 O33 180(100) . . . . ? Ni22 Ni25 C33 O33 49(14) . . . . ? Ni24 Ni25 C33 O33 111(14) . . . . ? C36 Ni27 C34 O34 12(4) . . . . ? C42 Ni27 C34 O34 -175(3) . . . . ? C41 Ni27 C34 O34 -149(3) . . . . ? Ni25 Ni27 C34 O34 -165(4) . . . . ? Ni28 Ni27 C34 O34 2(5) . . . . ? Ni26 Ni27 C34 O34 -126(3) . . . . ? Ni21 Ni27 C34 O34 133(3) . . . . ? C36 Ni27 C34 Ni25 177.5(7) . . . . ? C42 Ni27 C34 Ni25 -9.1(8) . . . . ? C41 Ni27 C34 Ni25 16.6(14) . . . . ? Ni28 Ni27 C34 Ni25 167.0(15) . . . . ? Ni26 Ni27 C34 Ni25 39.8(5) . . . . ? Ni21 Ni27 C34 Ni25 -61.6(10) . . . . ? C33 Ni25 C34 O34 -26(2) . . . . ? C39 Ni25 C34 O34 75(3) . . . . ? C42 Ni25 C34 O34 179.2(19) . . . . ? C39' Ni25 C34 O34 79(2) . . . . ? Ni27 Ni25 C34 O34 171(2) . . . . ? Ni26 Ni25 C34 O34 123.9(19) . . . . ? Ni22 Ni25 C34 O34 -131.4(19) . . . . ? Ni24 Ni25 C34 O34 176.9(12) . . . . ? C33 Ni25 C34 Ni27 163.5(8) . . . . ? C39 Ni25 C34 Ni27 -96.0(17) . . . . ? C42 Ni25 C34 Ni27 8.5(7) . . . . ? C39' Ni25 C34 Ni27 -91.9(14) . . . . ? Ni26 Ni25 C34 Ni27 -46.8(6) . . . . ? Ni22 Ni25 C34 Ni27 57.9(6) . . . . ? Ni24 Ni25 C34 Ni27 6.2(15) . . . . ? C39' Ni26 C35 O35 -18(3) . . . . ? C39 Ni26 C35 O35 -36(3) . . . . ? C37 Ni26 C35 O35 57(3) . . . . ? C42 Ni26 C35 O35 -174.1(19) . . . . ? C41 Ni26 C35 O35 -173(2) . . . . ? Ni23 Ni26 C35 O35 -179(3) 3 . . . ? Ni25 Ni26 C35 O35 -64(3) . . . . ? Ni24 Ni26 C35 O35 97(2) . . . . ? Ni27 Ni26 C35 O35 -122(2) . . . . ? C39' Ni26 C35 Ni23 161.3(18) . . . 3 ? C39 Ni26 C35 Ni23 143.6(16) . . . 3 ? C37 Ni26 C35 Ni23 -123.4(11) . . . 3 ? C42 Ni26 C35 Ni23 5.3(13) . . . 3 ? C41 Ni26 C35 Ni23 6.2(7) . . . 3 ? Ni25 Ni26 C35 Ni23 115.4(9) . . . 3 ? Ni24 Ni26 C35 Ni23 -83.8(9) . . . 3 ? Ni27 Ni26 C35 Ni23 56.9(6) . . . 3 ? C34 Ni27 C36 O36 15(4) . . . . ? C42 Ni27 C36 O36 -154(3) . . . . ? C41 Ni27 C36 O36 -177(3) . . . . ? Ni25 Ni27 C36 O36 22(5) . . . . ? Ni28 Ni27 C36 O36 -169(4) . . . . ? Ni26 Ni27 C36 O36 131(3) . . . . ? Ni21 Ni27 C36 O36 -127(4) . . . . ? C34 Ni27 C36 Ni28 -176.0(7) . . . . ? C42 Ni27 C36 Ni28 14.3(14) . . . . ? C41 Ni27 C36 Ni28 -7.8(7) . . . . ? Ni25 Ni27 C36 Ni28 -169.5(15) . . . . ? Ni26 Ni27 C36 Ni28 -60.3(9) . . . . ? Ni21 Ni27 C36 Ni28 41.5(5) . . . . ? C31 Ni28 C36 O36 -16(2) . . . . ? C38 Ni28 C36 O36 76(2) . . . . ? C41 Ni28 C36 O36 -178.9(18) . . . . ? Ni27 Ni28 C36 O36 173(2) . . . . ? Ni21 Ni28 C36 O36 126.8(18) . . . . ? Ni23 Ni28 C36 O36 -129.4(17) 3 . . . ? Ni24 Ni28 C36 O36 168.3(11) 3 . . . ? C31 Ni28 C36 Ni27 170.6(8) . . . . ? C38 Ni28 C36 Ni27 -97.5(11) . . . . ? C41 Ni28 C36 Ni27 7.8(7) . . . . ? Ni21 Ni28 C36 Ni27 -46.6(6) . . . . ? Ni23 Ni28 C36 Ni27 57.2(6) 3 . . . ? Ni24 Ni28 C36 Ni27 -5.1(15) 3 . . . ? C39' Ni26 C37 O37 39(4) . . . . ? C35 Ni26 C37 O37 -62(4) . . . . ? C39 Ni26 C37 O37 42(4) . . . . ? C42 Ni26 C37 O37 148(4) . . . . ? C41 Ni26 C37 O37 -177(3) . . . . ? Ni23 Ni26 C37 O37 -113(4) 3 . . . ? Ni25 Ni26 C37 O37 93(4) . . . . ? Ni24 Ni26 C37 O37 145(5) . . . . ? Ni27 Ni26 C37 O37 117(3) . . . . ? C39' Ni26 C37 Ni21 -179(2) . . . 3 ? C35 Ni26 C37 Ni21 80.7(12) . . . 3 ? C39 Ni26 C37 Ni21 -175.6(18) . . . 3 ? C42 Ni26 C37 Ni21 -69.5(13) . . . 3 ? C41 Ni26 C37 Ni21 -34.3(18) . . . 3 ? Ni23 Ni26 C37 Ni21 29.5(16) 3 . . 3 ? Ni25 Ni26 C37 Ni21 -124.2(10) . . . 3 ? Ni24 Ni26 C37 Ni21 -72.6(10) . . . 3 ? Ni27 Ni26 C37 Ni21 -99.7(18) . . . 3 ? C39' Ni26 C37 Ni24 -106(2) . . . . ? C35 Ni26 C37 Ni24 153.3(8) . . . . ? C39 Ni26 C37 Ni24 -103.0(17) . . . . ? C42 Ni26 C37 Ni24 3.1(11) . . . . ? C41 Ni26 C37 Ni24 38.3(16) . . . . ? Ni23 Ni26 C37 Ni24 102.1(10) 3 . . . ? Ni25 Ni26 C37 Ni24 -51.6(8) . . . . ? Ni27 Ni26 C37 Ni24 -27(2) . . . . ? C45' Ni24 C37 O37 -3(6) . . . . ? C45 Ni24 C37 O37 -4(6) . . . . ? C42 Ni24 C37 O37 -138(5) . . . . ? C41 Ni24 C37 O37 131(5) 3 . . . ? Ni29 Ni24 C37 O37 3(6) . . . . ? Ni21 Ni24 C37 O37 129(6) 3 . . . ? Ni23 Ni24 C37 O37 106(5) . . . . ? Ni22 Ni24 C37 O37 -108(5) . . . . ? Ni28 Ni24 C37 O37 82(5) 3 . . . ? Ni26 Ni24 C37 O37 -135(6) . . . . ? Ni25 Ni24 C37 O37 -90(5) . . . . ? C45' Ni24 C37 Ni26 132(4) . . . . ? C45 Ni24 C37 Ni26 131(3) . . . . ? C42 Ni24 C37 Ni26 -3.1(11) . . . . ? C41 Ni24 C37 Ni26 -94.4(10) 3 . . . ? Ni29 Ni24 C37 Ni26 138.2(9) . . . . ? Ni21 Ni24 C37 Ni26 -96.1(11) 3 . . . ? Ni23 Ni24 C37 Ni26 -118.6(14) . . . . ? Ni22 Ni24 C37 Ni26 27(2) . . . . ? Ni28 Ni24 C37 Ni26 -142.5(8) 3 . . . ? Ni25 Ni24 C37 Ni26 45.5(8) . . . . ? C45' Ni24 C37 Ni21 -132(4) . . . 3 ? C45 Ni24 C37 Ni21 -133(3) . . . 3 ? C42 Ni24 C37 Ni21 93.0(9) . . . 3 ? C41 Ni24 C37 Ni21 1.8(11) 3 . . 3 ? Ni29 Ni24 C37 Ni21 -125.7(11) . . . 3 ? Ni23 Ni24 C37 Ni21 -23(2) . . . 3 ? Ni22 Ni24 C37 Ni21 123.1(11) . . . 3 ? Ni28 Ni24 C37 Ni21 -46.4(8) 3 . . 3 ? Ni26 Ni24 C37 Ni21 96.1(11) . . . 3 ? Ni25 Ni24 C37 Ni21 141.7(8) . . . 3 ? C31 Ni28 C38 O38 12(5) . . . . ? C41 Ni28 C38 O38 175(4) . . . . ? C36 Ni28 C38 O38 -84(5) . . . . ? Ni27 Ni28 C38 O38 -130(4) . . . . ? Ni21 Ni28 C38 O38 173(5) . . . . ? Ni23 Ni28 C38 O38 145(3) 3 . . . ? Ni24 Ni28 C38 O38 124(5) 3 . . . ? C31 Ni28 C38 Ni21 -161.3(11) . . . . ? C41 Ni28 C38 Ni21 1.3(13) . . . . ? C36 Ni28 C38 Ni21 102.2(11) . . . . ? Ni27 Ni28 C38 Ni21 57.1(10) . . . . ? Ni23 Ni28 C38 Ni21 -28(3) 3 . . . ? Ni24 Ni28 C38 Ni21 -49.3(9) 3 . . . ? C38' Ni21 C38 O38 -40(5) 3 . . . ? C32 Ni21 C38 O38 37(6) . . . . ? C41 Ni21 C38 O38 -174(5) . . . . ? C37 Ni21 C38 O38 -68(5) 3 . . . ? C42 Ni21 C38 O38 158(5) . . . . ? Ni22 Ni21 C38 O38 85(6) . . . . ? Ni28 Ni21 C38 O38 -172(6) . . . . ? Ni24 Ni21 C38 O38 -122(5) 3 . . . ? Ni27 Ni21 C38 O38 141(5) . . . . ? C38' Ni21 C38 Ni28 133(3) 3 . . . ? C32 Ni21 C38 Ni28 -150.4(9) . . . . ? C41 Ni21 C38 Ni28 -1.2(12) . . . . ? C37 Ni21 C38 Ni28 104.7(14) 3 . . . ? C42 Ni21 C38 Ni28 -29.6(18) . . . . ? Ni22 Ni21 C38 Ni28 -102.3(13) . . . . ? Ni24 Ni21 C38 Ni28 50.2(9) 3 . . . ? Ni27 Ni21 C38 Ni28 -46.6(8) . . . . ? C33 Ni25 C39 O39 23(9) . . . . ? C34 Ni25 C39 O39 -76(8) . . . . ? C42 Ni25 C39 O39 -176(8) . . . . ? C39' Ni25 C39 O39 119(14) . . . . ? Ni27 Ni25 C39 O39 -122(8) . . . . ? Ni26 Ni25 C39 O39 176(10) . . . . ? Ni22 Ni25 C39 O39 173(6) . . . . ? Ni24 Ni25 C39 O39 135(8) . . . . ? C33 Ni25 C39 Ni26 -153.8(12) . . . . ? C34 Ni25 C39 Ni26 107.5(14) . . . . ? C42 Ni25 C39 Ni26 8.0(17) . . . . ? C39' Ni25 C39 Ni26 -58(9) . . . . ? Ni27 Ni25 C39 Ni26 61.6(13) . . . . ? Ni22 Ni25 C39 Ni26 -4(4) . . . . ? Ni24 Ni25 C39 Ni26 -41.9(15) . . . . ? C39' Ni26 C39 O39 -72(9) . . . . ? C35 Ni26 C39 O39 20(7) . . . . ? C37 Ni26 C39 O39 -81(6) . . . . ? C42 Ni26 C39 O39 175(6) . . . . ? C41 Ni26 C39 O39 141(5) . . . . ? Ni23 Ni26 C39 O39 66(7) 3 . . . ? Ni25 Ni26 C39 O39 -177(7) . . . . ? Ni24 Ni26 C39 O39 -135(6) . . . . ? Ni27 Ni26 C39 O39 132(6) . . . . ? C39' Ni26 C39 Ni25 106(11) . . . . ? C35 Ni26 C39 Ni25 -162.8(11) . . . . ? C37 Ni26 C39 Ni25 96.2(16) . . . . ? C42 Ni26 C39 Ni25 -8.0(17) . . . . ? C41 Ni26 C39 Ni25 -42(3) . . . . ? Ni23 Ni26 C39 Ni25 -116.9(16) 3 . . . ? Ni24 Ni26 C39 Ni25 42.6(15) . . . . ? Ni27 Ni26 C39 Ni25 -50.7(11) . . . . ? C35 Ni26 C39' O39' 32(12) . . . . ? C39 Ni26 C39' O39' 125(18) . . . . ? C37 Ni26 C39' O39' -65(11) . . . . ? C42 Ni26 C39' O39' -164(11) . . . . ? C41 Ni26 C39' O39' 169(9) . . . . ? Ni23 Ni26 C39' O39' 63(13) 3 . . . ? Ni25 Ni26 C39' O39' -172(13) . . . . ? Ni24 Ni26 C39' O39' -116(12) . . . . ? Ni27 Ni26 C39' O39' 148(11) . . . . ? C35 Ni26 C39' Ni25 -155.4(10) . . . . ? C39 Ni26 C39' Ni25 -63(10) . . . . ? C37 Ni26 C39' Ni25 107.3(18) . . . . ? C42 Ni26 C39' Ni25 8.9(19) . . . . ? C41 Ni26 C39' Ni25 -19(4) . . . . ? Ni23 Ni26 C39' Ni25 -125(3) 3 . . . ? Ni24 Ni26 C39' Ni25 55.9(12) . . . . ? Ni27 Ni26 C39' Ni25 -39.3(13) . . . . ? C33 Ni25 C39' O39' 12(6) . . . . ? C39 Ni25 C39' O39' -75(9) . . . . ? C34 Ni25 C39' O39' -90(5) . . . . ? C42 Ni25 C39' O39' 168(5) . . . . ? Ni27 Ni25 C39' O39' -137(5) . . . . ? Ni26 Ni25 C39' O39' 176(7) . . . . ? Ni22 Ni25 C39' O39' 141(4) . . . . ? Ni24 Ni25 C39' O39' 121(5) . . . . ? C33 Ni25 C39' Ni26 -163.8(14) . . . . ? C39 Ni25 C39' Ni26 109(10) . . . . ? C34 Ni25 C39' Ni26 93.9(16) . . . . ? C42 Ni25 C39' Ni26 -8.3(18) . . . . ? Ni27 Ni25 C39' Ni26 46.9(17) . . . . ? Ni22 Ni25 C39' Ni26 -35(3) . . . . ? Ni24 Ni25 C39' Ni26 -55.4(14) . . . . ? C31 Ni28 C41 C42 -179.1(17) . . . . ? C38 Ni28 C41 C42 47.8(17) . . . . ? C36 Ni28 C41 C42 -45.0(13) . . . . ? Ni27 Ni28 C41 C42 -38.3(11) . . . . ? Ni21 Ni28 C41 C42 49.0(11) . . . . ? Ni23 Ni28 C41 C42 -152.6(15) 3 . . . ? Ni24 Ni28 C41 C42 127.2(14) 3 . . . ? C31 Ni28 C41 Ni23 -26.5(18) . . . 3 ? C38 Ni28 C41 Ni23 -159.7(12) . . . 3 ? C36 Ni28 C41 Ni23 107.6(6) . . . 3 ? Ni27 Ni28 C41 Ni23 114.3(5) . . . 3 ? Ni21 Ni28 C41 Ni23 -158.4(6) . . . 3 ? Ni24 Ni28 C41 Ni23 -80.2(4) 3 . . 3 ? C31 Ni28 C41 Ni27 -140.8(16) . . . . ? C38 Ni28 C41 Ni27 86.1(12) . . . . ? C36 Ni28 C41 Ni27 -6.7(6) . . . . ? Ni21 Ni28 C41 Ni27 87.3(4) . . . . ? Ni23 Ni28 C41 Ni27 -114.3(5) 3 . . . ? Ni24 Ni28 C41 Ni27 165.6(5) 3 . . . ? C31 Ni28 C41 Ni21 131.8(16) . . . . ? C38 Ni28 C41 Ni21 -1.3(12) . . . . ? C36 Ni28 C41 Ni21 -94.0(6) . . . . ? Ni27 Ni28 C41 Ni21 -87.3(4) . . . . ? Ni23 Ni28 C41 Ni21 158.4(6) 3 . . . ? Ni24 Ni28 C41 Ni21 78.2(3) 3 . . . ? C31 Ni28 C41 Ni24 53.6(18) . . . 3 ? C38 Ni28 C41 Ni24 -79.5(12) . . . 3 ? C36 Ni28 C41 Ni24 -172.2(6) . . . 3 ? Ni27 Ni28 C41 Ni24 -165.6(5) . . . 3 ? Ni21 Ni28 C41 Ni24 -78.2(3) . . . 3 ? Ni23 Ni28 C41 Ni24 80.2(4) 3 . . 3 ? C31 Ni28 C41 Ni26 -80.5(19) . . . . ? C38 Ni28 C41 Ni26 146.4(14) . . . . ? C36 Ni28 C41 Ni26 53.6(10) . . . . ? Ni27 Ni28 C41 Ni26 60.3(7) . . . . ? Ni21 Ni28 C41 Ni26 147.7(11) . . . . ? Ni23 Ni28 C41 Ni26 -53.9(7) 3 . . . ? Ni24 Ni28 C41 Ni26 -134.1(10) 3 . . . ? C36 Ni27 C41 C42 158.8(9) . . . . ? C34 Ni27 C41 C42 -40.6(15) . . . . ? Ni25 Ni27 C41 C42 -27.0(7) . . . . ? Ni28 Ni27 C41 C42 150.7(9) . . . . ? Ni26 Ni27 C41 C42 -71.4(7) . . . . ? Ni21 Ni27 C41 C42 73.4(7) . . . . ? C36 Ni27 C41 Ni23 -65.3(9) . . . 3 ? C34 Ni27 C41 Ni23 95.2(13) . . . 3 ? C42 Ni27 C41 Ni23 135.9(11) . . . 3 ? Ni25 Ni27 C41 Ni23 108.9(6) . . . 3 ? Ni28 Ni27 C41 Ni23 -73.4(6) . . . 3 ? Ni26 Ni27 C41 Ni23 64.5(5) . . . 3 ? Ni21 Ni27 C41 Ni23 -150.8(9) . . . 3 ? C36 Ni27 C41 Ni28 8.1(7) . . . . ? C34 Ni27 C41 Ni28 168.7(11) . . . . ? C42 Ni27 C41 Ni28 -150.7(9) . . . . ? Ni25 Ni27 C41 Ni28 -177.7(3) . . . . ? Ni26 Ni27 C41 Ni28 137.9(5) . . . . ? Ni21 Ni27 C41 Ni28 -77.3(4) . . . . ? C36 Ni27 C41 Ni21 85.5(8) . . . . ? C34 Ni27 C41 Ni21 -114.0(12) . . . . ? C42 Ni27 C41 Ni21 -73.4(7) . . . . ? Ni25 Ni27 C41 Ni21 -100.3(4) . . . . ? Ni28 Ni27 C41 Ni21 77.3(4) . . . . ? Ni26 Ni27 C41 Ni21 -144.7(6) . . . . ? C36 Ni27 C41 Ni24 34.9(14) . . . 3 ? C34 Ni27 C41 Ni24 -164.6(13) . . . 3 ? C42 Ni27 C41 Ni24 -123.9(15) . . . 3 ? Ni25 Ni27 C41 Ni24 -150.9(12) . . . 3 ? Ni28 Ni27 C41 Ni24 26.8(10) . . . 3 ? Ni26 Ni27 C41 Ni24 164.7(15) . . . 3 ? Ni21 Ni27 C41 Ni24 -50.6(10) . . . 3 ? C36 Ni27 C41 Ni26 -129.8(7) . . . . ? C34 Ni27 C41 Ni26 30.7(13) . . . . ? C42 Ni27 C41 Ni26 71.4(7) . . . . ? Ni25 Ni27 C41 Ni26 44.4(3) . . . . ? Ni28 Ni27 C41 Ni26 -137.9(5) . . . . ? Ni21 Ni27 C41 Ni26 144.7(6) . . . . ? C38' Ni21 C41 C42 176(2) 3 . . . ? C32 Ni21 C41 C42 -10.6(14) . . . . ? C38 Ni21 C41 C42 -142.6(13) . . . . ? C37 Ni21 C41 C42 132.4(13) 3 . . . ? Ni22 Ni21 C41 C42 -2.4(7) . . . . ? Ni28 Ni21 C41 C42 -143.8(9) . . . . ? Ni24 Ni21 C41 C42 134.2(9) 3 . . . ? Ni27 Ni21 C41 C42 -71.4(8) . . . . ? C38' Ni21 C41 Ni23 4(3) 3 . . 3 ? C32 Ni21 C41 Ni23 178.1(13) . . . 3 ? C38 Ni21 C41 Ni23 46.0(17) . . . 3 ? C37 Ni21 C41 Ni23 -39.0(18) 3 . . 3 ? C42 Ni21 C41 Ni23 -171.3(18) . . . 3 ? Ni22 Ni21 C41 Ni23 -173.7(13) . . . 3 ? Ni28 Ni21 C41 Ni23 44.8(11) . . . 3 ? Ni24 Ni21 C41 Ni23 -37.1(11) 3 . . 3 ? Ni27 Ni21 C41 Ni23 117.2(15) . . . 3 ? C38' Ni21 C41 Ni28 -40(2) 3 . . . ? C32 Ni21 C41 Ni28 133.3(10) . . . . ? C38 Ni21 C41 Ni28 1.2(12) . . . . ? C37 Ni21 C41 Ni28 -83.8(11) 3 . . . ? C42 Ni21 C41 Ni28 143.8(9) . . . . ? Ni22 Ni21 C41 Ni28 141.5(3) . . . . ? Ni24 Ni21 C41 Ni28 -81.9(4) 3 . . . ? Ni27 Ni21 C41 Ni28 72.4(4) . . . . ? C38' Ni21 C41 Ni27 -113(2) 3 . . . ? C32 Ni21 C41 Ni27 60.9(11) . . . . ? C38 Ni21 C41 Ni27 -71.2(12) . . . . ? C37 Ni21 C41 Ni27 -156.2(11) 3 . . . ? C42 Ni21 C41 Ni27 71.4(8) . . . . ? Ni22 Ni21 C41 Ni27 69.1(3) . . . . ? Ni28 Ni21 C41 Ni27 -72.4(4) . . . . ? Ni24 Ni21 C41 Ni27 -154.3(6) 3 . . . ? C38' Ni21 C41 Ni24 41(2) 3 . . 3 ? C32 Ni21 C41 Ni24 -144.8(10) . . . 3 ? C38 Ni21 C41 Ni24 83.1(12) . . . 3 ? C37 Ni21 C41 Ni24 -1.9(11) 3 . . 3 ? C42 Ni21 C41 Ni24 -134.2(9) . . . 3 ? Ni22 Ni21 C41 Ni24 -136.6(3) . . . 3 ? Ni28 Ni21 C41 Ni24 81.9(4) . . . 3 ? Ni27 Ni21 C41 Ni24 154.3(6) . . . 3 ? C38' Ni21 C41 Ni26 -179(2) 3 . . . ? C32 Ni21 C41 Ni26 -5.8(17) . . . . ? C38 Ni21 C41 Ni26 -137.8(15) . . . . ? C37 Ni21 C41 Ni26 137.2(14) 3 . . . ? C42 Ni21 C41 Ni26 4.8(8) . . . . ? Ni22 Ni21 C41 Ni26 2.4(10) . . . . ? Ni28 Ni21 C41 Ni26 -139.0(12) . . . . ? Ni24 Ni21 C41 Ni26 139.0(12) 3 . . . ? Ni27 Ni21 C41 Ni26 -66.6(9) . . . . ? C39' Ni26 C41 C42 44(3) . . . . ? C35 Ni26 C41 C42 -179.1(9) . . . . ? C39 Ni26 C41 C42 60(2) . . . . ? C37 Ni26 C41 C42 -65.7(16) . . . . ? Ni23 Ni26 C41 C42 -173.0(9) 3 . . . ? Ni25 Ni26 C41 C42 28.6(7) . . . . ? Ni24 Ni26 C41 C42 -34.8(7) . . . . ? Ni27 Ni26 C41 C42 72.0(8) . . . . ? C39' Ni26 C41 Ni23 -143(3) . . . 3 ? C35 Ni26 C41 Ni23 -6.1(7) . . . 3 ? C39 Ni26 C41 Ni23 -127(2) . . . 3 ? C37 Ni26 C41 Ni23 107.3(14) . . . 3 ? C42 Ni26 C41 Ni23 173.0(9) . . . 3 ? Ni25 Ni26 C41 Ni23 -158.4(3) . . . 3 ? Ni24 Ni26 C41 Ni23 138.2(3) . . . 3 ? Ni27 Ni26 C41 Ni23 -115.0(5) . . . 3 ? C39' Ni26 C41 Ni28 -84(3) . . . . ? C35 Ni26 C41 Ni28 52.5(10) . . . . ? C39 Ni26 C41 Ni28 -69(2) . . . . ? C37 Ni26 C41 Ni28 165.9(15) . . . . ? C42 Ni26 C41 Ni28 -128.4(13) . . . . ? Ni23 Ni26 C41 Ni28 58.6(7) 3 . . . ? Ni25 Ni26 C41 Ni28 -99.8(8) . . . . ? Ni24 Ni26 C41 Ni28 -163.2(9) . . . . ? Ni27 Ni26 C41 Ni28 -56.4(7) . . . . ? C39' Ni26 C41 Ni27 -28(3) . . . . ? C35 Ni26 C41 Ni27 108.8(6) . . . . ? C39 Ni26 C41 Ni27 -12(2) . . . . ? C37 Ni26 C41 Ni27 -137.7(14) . . . . ? C42 Ni26 C41 Ni27 -72.0(8) . . . . ? Ni23 Ni26 C41 Ni27 115.0(5) 3 . . . ? Ni25 Ni26 C41 Ni27 -43.5(3) . . . . ? Ni24 Ni26 C41 Ni27 -106.9(4) . . . . ? C39' Ni26 C41 Ni21 39(3) . . . . ? C35 Ni26 C41 Ni21 176.0(11) . . . . ? C39 Ni26 C41 Ni21 55(2) . . . . ? C37 Ni26 C41 Ni21 -70.5(18) . . . . ? C42 Ni26 C41 Ni21 -4.9(8) . . . . ? Ni23 Ni26 C41 Ni21 -177.9(13) 3 . . . ? Ni25 Ni26 C41 Ni21 23.7(10) . . . . ? Ni24 Ni26 C41 Ni21 -39.7(10) . . . . ? Ni27 Ni26 C41 Ni21 67.2(10) . . . . ? C39' Ni26 C41 Ni24 163(3) . . . 3 ? C35 Ni26 C41 Ni24 -60.3(10) . . . 3 ? C39 Ni26 C41 Ni24 179(2) . . . 3 ? C37 Ni26 C41 Ni24 53.1(17) . . . 3 ? C42 Ni26 C41 Ni24 118.8(12) . . . 3 ? Ni23 Ni26 C41 Ni24 -54.2(7) 3 . . 3 ? Ni25 Ni26 C41 Ni24 147.4(8) . . . 3 ? Ni24 Ni26 C41 Ni24 84.0(8) . . . 3 ? Ni27 Ni26 C41 Ni24 -169.2(11) . . . 3 ? Ni23 C41 C42 Ni22 177.7(8) 3 . . . ? Ni28 C41 C42 Ni22 -46(2) . . . . ? Ni27 C41 C42 Ni22 -84.5(14) . . . . ? Ni21 C41 C42 Ni22 4.5(14) . . . . ? Ni24 C41 C42 Ni22 62(2) 3 . . . ? Ni26 C41 C42 Ni22 -172.3(15) . . . . ? Ni23 C41 C42 Ni24 52.8(19) 3 . . . ? Ni28 C41 C42 Ni24 -170.8(6) . . . . ? Ni27 C41 C42 Ni24 150.6(10) . . . . ? Ni21 C41 C42 Ni24 -120.4(9) . . . . ? Ni24 C41 C42 Ni24 -62.7(15) 3 . . . ? Ni26 C41 C42 Ni24 62.8(9) . . . . ? Ni23 C41 C42 Ni27 -97.8(13) 3 . . . ? Ni28 C41 C42 Ni27 38.6(10) . . . . ? Ni21 C41 C42 Ni27 88.9(4) . . . . ? Ni24 C41 C42 Ni27 146.7(10) 3 . . . ? Ni26 C41 C42 Ni27 -87.9(3) . . . . ? Ni23 C41 C42 Ni26 -9.9(13) 3 . . . ? Ni28 C41 C42 Ni26 126.5(11) . . . . ? Ni27 C41 C42 Ni26 87.9(3) . . . . ? Ni21 C41 C42 Ni26 176.8(5) . . . . ? Ni24 C41 C42 Ni26 -125.4(10) 3 . . . ? Ni23 C41 C42 Ni25 -56(2) 3 . . . ? Ni28 C41 C42 Ni25 80.6(16) . . . . ? Ni27 C41 C42 Ni25 42.0(10) . . . . ? Ni21 C41 C42 Ni25 130.9(11) . . . . ? Ni24 C41 C42 Ni25 -171.3(7) 3 . . . ? Ni26 C41 C42 Ni25 -45.9(10) . . . . ? Ni23 C41 C42 Ni21 173.2(14) 3 . . . ? Ni28 C41 C42 Ni21 -50.3(10) . . . . ? Ni27 C41 C42 Ni21 -88.9(4) . . . . ? Ni24 C41 C42 Ni21 57.8(9) 3 . . . ? Ni26 C41 C42 Ni21 -176.8(5) . . . . ? C44' Ni22 C42 C41 153(5) . . . . ? C44 Ni22 C42 C41 176(4) . . . . ? C32 Ni22 C42 C41 -0.2(18) . . . . ? Ni21 Ni22 C42 C41 -4.5(14) . . . . ? Ni25 Ni22 C42 C41 140.6(18) . . . . ? Ni29 Ni22 C42 C41 -137.9(15) . . . . ? Ni24 Ni22 C42 C41 -137.4(18) . . . . ? Ni23 Ni22 C42 C41 -90.9(16) . . . . ? C44' Ni22 C42 Ni24 -70(5) . . . . ? C44 Ni22 C42 Ni24 -46(4) . . . . ? C32 Ni22 C42 Ni24 137.3(7) . . . . ? Ni21 Ni22 C42 Ni24 133.0(5) . . . . ? Ni25 Ni22 C42 Ni24 -81.9(4) . . . . ? Ni29 Ni22 C42 Ni24 -0.5(4) . . . . ? Ni23 Ni22 C42 Ni24 46.6(3) . . . . ? C44' Ni22 C42 Ni27 79(5) . . . . ? C44 Ni22 C42 Ni27 102(4) . . . . ? C32 Ni22 C42 Ni27 -74.0(8) . . . . ? Ni21 Ni22 C42 Ni27 -78.2(5) . . . . ? Ni25 Ni22 C42 Ni27 66.9(4) . . . . ? Ni29 Ni22 C42 Ni27 148.3(4) . . . . ? Ni24 Ni22 C42 Ni27 148.8(7) . . . . ? Ni23 Ni22 C42 Ni27 -164.6(5) . . . . ? C44' Ni22 C42 Ni26 -14(5) . . . . ? C44 Ni22 C42 Ni26 10(5) . . . . ? C32 Ni22 C42 Ni26 -166.9(13) . . . . ? Ni21 Ni22 C42 Ni26 -171.1(15) . . . . ? Ni25 Ni22 C42 Ni26 -26.0(10) . . . . ? Ni29 Ni22 C42 Ni26 55.4(13) . . . . ? Ni24 Ni22 C42 Ni26 55.9(11) . . . . ? Ni23 Ni22 C42 Ni26 102.5(12) . . . . ? C44' Ni22 C42 Ni25 12(5) . . . . ? C44 Ni22 C42 Ni25 36(4) . . . . ? C32 Ni22 C42 Ni25 -140.8(7) . . . . ? Ni21 Ni22 C42 Ni25 -145.1(5) . . . . ? Ni29 Ni22 C42 Ni25 81.4(4) . . . . ? Ni24 Ni22 C42 Ni25 81.9(4) . . . . ? Ni23 Ni22 C42 Ni25 128.5(3) . . . . ? C44' Ni22 C42 Ni21 157(5) . . . . ? C44 Ni22 C42 Ni21 -179(4) . . . . ? C32 Ni22 C42 Ni21 4.3(7) . . . . ? Ni25 Ni22 C42 Ni21 145.1(5) . . . . ? Ni29 Ni22 C42 Ni21 -133.5(3) . . . . ? Ni24 Ni22 C42 Ni21 -133.0(5) . . . . ? Ni23 Ni22 C42 Ni21 -86.4(3) . . . . ? C45' Ni24 C42 C41 -142(3) . . . . ? C45 Ni24 C42 C41 -153(2) . . . . ? C41 Ni24 C42 C41 46.9(12) 3 . . . ? C37 Ni24 C42 C41 -56.5(15) . . . . ? Ni29 Ni24 C42 C41 148.7(10) . . . . ? Ni21 Ni24 C42 C41 -4.2(11) 3 . . . ? Ni23 Ni24 C42 C41 95.2(11) . . . . ? Ni22 Ni24 C42 C41 148.1(13) . . . . ? Ni28 Ni24 C42 C41 47.4(13) 3 . . . ? Ni26 Ni24 C42 C41 -59.5(10) . . . . ? Ni25 Ni24 C42 C41 -132.0(12) . . . . ? C45' Ni24 C42 Ni22 70(3) . . . . ? C45 Ni24 C42 Ni22 59(2) . . . . ? C41 Ni24 C42 Ni22 -101.2(5) 3 . . . ? C37 Ni24 C42 Ni22 155.4(11) . . . . ? Ni29 Ni24 C42 Ni22 0.5(5) . . . . ? Ni21 Ni24 C42 Ni22 -152.4(3) 3 . . . ? Ni23 Ni24 C42 Ni22 -52.9(4) . . . . ? Ni28 Ni24 C42 Ni22 -100.8(5) 3 . . . ? Ni26 Ni24 C42 Ni22 152.4(6) . . . . ? Ni25 Ni24 C42 Ni22 79.9(4) . . . . ? C45' Ni24 C42 Ni27 -27(3) . . . . ? C45 Ni24 C42 Ni27 -38(3) . . . . ? C41 Ni24 C42 Ni27 162.0(14) 3 . . . ? C37 Ni24 C42 Ni27 58.6(17) . . . . ? Ni29 Ni24 C42 Ni27 -96.3(13) . . . . ? Ni21 Ni24 C42 Ni27 110.8(13) 3 . . . ? Ni23 Ni24 C42 Ni27 -149.7(13) . . . . ? Ni22 Ni24 C42 Ni27 -96.8(15) . . . . ? Ni28 Ni24 C42 Ni27 162.4(10) 3 . . . ? Ni26 Ni24 C42 Ni27 55.6(12) . . . . ? Ni25 Ni24 C42 Ni27 -16.9(11) . . . . ? C45' Ni24 C42 Ni26 -83(3) . . . . ? C45 Ni24 C42 Ni26 -93(2) . . . . ? C41 Ni24 C42 Ni26 106.4(5) 3 . . . ? C37 Ni24 C42 Ni26 3.1(11) . . . . ? Ni29 Ni24 C42 Ni26 -151.8(3) . . . . ? Ni21 Ni24 C42 Ni26 55.3(4) 3 . . . ? Ni23 Ni24 C42 Ni26 154.7(3) . . . . ? Ni22 Ni24 C42 Ni26 -152.4(6) . . . . ? Ni28 Ni24 C42 Ni26 106.9(4) 3 . . . ? Ni25 Ni24 C42 Ni26 -72.5(3) . . . . ? C45' Ni24 C42 Ni25 -10(3) . . . . ? C45 Ni24 C42 Ni25 -21(2) . . . . ? C41 Ni24 C42 Ni25 178.9(5) 3 . . . ? C37 Ni24 C42 Ni25 75.5(11) . . . . ? Ni29 Ni24 C42 Ni25 -79.3(4) . . . . ? Ni21 Ni24 C42 Ni25 127.8(3) 3 . . . ? Ni23 Ni24 C42 Ni25 -132.8(3) . . . . ? Ni22 Ni24 C42 Ni25 -79.9(4) . . . . ? Ni28 Ni24 C42 Ni25 179.35(19) 3 . . . ? Ni26 Ni24 C42 Ni25 72.5(3) . . . . ? C45' Ni24 C42 Ni21 128(3) . . . . ? C45 Ni24 C42 Ni21 117(2) . . . . ? C41 Ni24 C42 Ni21 -43.0(8) 3 . . . ? C37 Ni24 C42 Ni21 -146.4(12) . . . . ? Ni29 Ni24 C42 Ni21 58.7(8) . . . . ? Ni21 Ni24 C42 Ni21 -94.2(7) 3 . . . ? Ni23 Ni24 C42 Ni21 5.2(8) . . . . ? Ni22 Ni24 C42 Ni21 58.2(6) . . . . ? Ni28 Ni24 C42 Ni21 -42.6(11) 3 . . . ? Ni26 Ni24 C42 Ni21 -149.5(10) . . . . ? Ni25 Ni24 C42 Ni21 138.0(10) . . . . ? C36 Ni27 C42 C41 -34.9(15) . . . . ? C34 Ni27 C42 C41 155.7(9) . . . . ? Ni25 Ni27 C42 C41 146.6(9) . . . . ? Ni28 Ni27 C42 C41 -23.1(7) . . . . ? Ni26 Ni27 C42 C41 73.9(7) . . . . ? Ni21 Ni27 C42 C41 -71.4(7) . . . . ? C36 Ni27 C42 Ni22 104.9(12) . . . . ? C34 Ni27 C42 Ni22 -64.5(9) . . . . ? C41 Ni27 C42 Ni22 139.8(10) . . . . ? Ni25 Ni27 C42 Ni22 -73.6(5) . . . . ? Ni28 Ni27 C42 Ni22 116.8(5) . . . . ? Ni26 Ni27 C42 Ni22 -146.3(8) . . . . ? Ni21 Ni27 C42 Ni22 68.4(4) . . . . ? C36 Ni27 C42 Ni24 -163.7(14) . . . . ? C34 Ni27 C42 Ni24 26.9(16) . . . . ? C41 Ni27 C42 Ni24 -128.8(17) . . . . ? Ni25 Ni27 C42 Ni24 17.8(11) . . . . ? Ni28 Ni27 C42 Ni24 -151.9(14) . . . . ? Ni26 Ni27 C42 Ni24 -54.9(12) . . . . ? Ni21 Ni27 C42 Ni24 159.8(16) . . . . ? C36 Ni27 C42 Ni26 -108.8(12) . . . . ? C34 Ni27 C42 Ni26 81.8(8) . . . . ? C41 Ni27 C42 Ni26 -73.9(7) . . . . ? Ni25 Ni27 C42 Ni26 72.7(3) . . . . ? Ni28 Ni27 C42 Ni26 -97.0(3) . . . . ? Ni21 Ni27 C42 Ni26 -145.3(6) . . . . ? C36 Ni27 C42 Ni25 178.5(11) . . . . ? C34 Ni27 C42 Ni25 9.1(8) . . . . ? C41 Ni27 C42 Ni25 -146.6(9) . . . . ? Ni28 Ni27 C42 Ni25 -169.6(3) . . . . ? Ni26 Ni27 C42 Ni25 -72.7(3) . . . . ? Ni21 Ni27 C42 Ni25 142.0(5) . . . . ? C36 Ni27 C42 Ni21 36.5(13) . . . . ? C34 Ni27 C42 Ni21 -132.9(7) . . . . ? C41 Ni27 C42 Ni21 71.4(7) . . . . ? Ni25 Ni27 C42 Ni21 -142.0(5) . . . . ? Ni28 Ni27 C42 Ni21 48.4(3) . . . . ? Ni26 Ni27 C42 Ni21 145.3(6) . . . . ? C39' Ni26 C42 C41 -153(2) . . . . ? C35 Ni26 C42 C41 1.4(14) . . . . ? C39 Ni26 C42 C41 -136.4(18) . . . . ? C37 Ni26 C42 C41 129.2(13) . . . . ? Ni23 Ni26 C42 C41 5.5(7) 3 . . . ? Ni25 Ni26 C42 C41 -144.1(9) . . . . ? Ni24 Ni26 C42 C41 132.5(9) . . . . ? Ni27 Ni26 C42 C41 -72.7(8) . . . . ? C39' Ni26 C42 Ni22 18(2) . . . . ? C35 Ni26 C42 Ni22 172.5(12) . . . . ? C39 Ni26 C42 Ni22 35(2) . . . . ? C37 Ni26 C42 Ni22 -59.6(17) . . . . ? C41 Ni26 C42 Ni22 171.1(18) . . . . ? Ni23 Ni26 C42 Ni22 176.7(12) 3 . . . ? Ni25 Ni26 C42 Ni22 27.0(10) . . . . ? Ni24 Ni26 C42 Ni22 -56.3(11) . . . . ? Ni27 Ni26 C42 Ni22 98.4(13) . . . . ? C39' Ni26 C42 Ni24 74.1(19) . . . . ? C35 Ni26 C42 Ni24 -131.2(10) . . . . ? C39 Ni26 C42 Ni24 91.1(17) . . . . ? C37 Ni26 C42 Ni24 -3.3(12) . . . . ? C41 Ni26 C42 Ni24 -132.5(9) . . . . ? Ni23 Ni26 C42 Ni24 -127.0(3) 3 . . . ? Ni25 Ni26 C42 Ni24 83.4(4) . . . . ? Ni27 Ni26 C42 Ni24 154.8(6) . . . . ? C39' Ni26 C42 Ni27 -80.6(19) . . . . ? C35 Ni26 C42 Ni27 74.1(11) . . . . ? C39 Ni26 C42 Ni27 -63.7(17) . . . . ? C37 Ni26 C42 Ni27 -158.0(11) . . . . ? C41 Ni26 C42 Ni27 72.7(8) . . . . ? Ni23 Ni26 C42 Ni27 78.3(4) 3 . . . ? Ni25 Ni26 C42 Ni27 -71.4(4) . . . . ? Ni24 Ni26 C42 Ni27 -154.8(6) . . . . ? C39' Ni26 C42 Ni25 -9.3(19) . . . . ? C35 Ni26 C42 Ni25 145.5(9) . . . . ? C39 Ni26 C42 Ni25 7.7(17) . . . . ? C37 Ni26 C42 Ni25 -86.7(12) . . . . ? C41 Ni26 C42 Ni25 144.1(9) . . . . ? Ni23 Ni26 C42 Ni25 149.6(3) 3 . . . ? Ni24 Ni26 C42 Ni25 -83.4(4) . . . . ? Ni27 Ni26 C42 Ni25 71.4(4) . . . . ? C39' Ni26 C42 Ni21 -148(2) . . . . ? C35 Ni26 C42 Ni21 6.3(18) . . . . ? C39 Ni26 C42 Ni21 -131.5(19) . . . . ? C37 Ni26 C42 Ni21 134.2(15) . . . . ? C41 Ni26 C42 Ni21 4.9(8) . . . . ? Ni23 Ni26 C42 Ni21 10.5(11) 3 . . . ? Ni25 Ni26 C42 Ni21 -139.2(13) . . . . ? Ni24 Ni26 C42 Ni21 137.4(13) . . . . ? Ni27 Ni26 C42 Ni21 -67.8(10) . . . . ? C33 Ni25 C42 C41 -177.1(16) . . . . ? C39 Ni25 C42 C41 39(2) . . . . ? C34 Ni25 C42 C41 -50.0(14) . . . . ? C39' Ni25 C42 C41 53(2) . . . . ? Ni27 Ni25 C42 C41 -42.4(11) . . . . ? Ni26 Ni25 C42 C41 46.3(11) . . . . ? Ni22 Ni25 C42 C41 -148.5(15) . . . . ? Ni24 Ni25 C42 C41 128.4(15) . . . . ? C33 Ni25 C42 Ni22 -28.6(16) . . . . ? C39 Ni25 C42 Ni22 -172.9(16) . . . . ? C34 Ni25 C42 Ni22 98.6(7) . . . . ? C39' Ni25 C42 Ni22 -158.1(15) . . . . ? Ni27 Ni25 C42 Ni22 106.1(5) . . . . ? Ni26 Ni25 C42 Ni22 -165.2(6) . . . . ? Ni24 Ni25 C42 Ni22 -83.0(4) . . . . ? C33 Ni25 C42 Ni24 54.5(16) . . . . ? C39 Ni25 C42 Ni24 -89.8(17) . . . . ? C34 Ni25 C42 Ni24 -178.4(6) . . . . ? C39' Ni25 C42 Ni24 -75.0(15) . . . . ? Ni27 Ni25 C42 Ni24 -170.9(6) . . . . ? Ni26 Ni25 C42 Ni24 -82.1(4) . . . . ? Ni22 Ni25 C42 Ni24 83.0(4) . . . . ? C33 Ni25 C42 Ni27 -134.7(14) . . . . ? C39 Ni25 C42 Ni27 81.0(17) . . . . ? C34 Ni25 C42 Ni27 -7.5(6) . . . . ? C39' Ni25 C42 Ni27 95.8(15) . . . . ? Ni26 Ni25 C42 Ni27 88.7(4) . . . . ? Ni22 Ni25 C42 Ni27 -106.1(5) . . . . ? Ni24 Ni25 C42 Ni27 170.9(6) . . . . ? C33 Ni25 C42 Ni26 136.6(14) . . . . ? C39 Ni25 C42 Ni26 -7.7(17) . . . . ? C34 Ni25 C42 Ni26 -96.3(6) . . . . ? C39' Ni25 C42 Ni26 7.1(15) . . . . ? Ni27 Ni25 C42 Ni26 -88.7(4) . . . . ? Ni22 Ni25 C42 Ni26 165.2(6) . . . . ? Ni24 Ni25 C42 Ni26 82.1(4) . . . . ? C33 Ni25 C42 Ni21 -76.9(18) . . . . ? C39 Ni25 C42 Ni21 138.9(18) . . . . ? C34 Ni25 C42 Ni21 50.3(10) . . . . ? C39' Ni25 C42 Ni21 153.7(17) . . . . ? Ni27 Ni25 C42 Ni21 57.8(7) . . . . ? Ni26 Ni25 C42 Ni21 146.5(10) . . . . ? Ni22 Ni25 C42 Ni21 -48.3(7) . . . . ? Ni24 Ni25 C42 Ni21 -131.3(10) . . . . ? C38' Ni21 C42 C41 -14(7) 3 . . . ? C32 Ni21 C42 C41 172.9(9) . . . . ? C38 Ni21 C42 C41 49.6(16) . . . . ? C37 Ni21 C42 C41 -64.9(17) 3 . . . ? Ni22 Ni21 C42 C41 177.0(9) . . . . ? Ni28 Ni21 C42 C41 27.4(7) . . . . ? Ni24 Ni21 C42 C41 -34.8(7) 3 . . . ? Ni27 Ni21 C42 C41 72.7(7) . . . . ? C38' Ni21 C42 Ni22 169(7) 3 . . . ? C32 Ni21 C42 Ni22 -4.0(7) . . . . ? C38 Ni21 C42 Ni22 -127.4(14) . . . . ? C41 Ni21 C42 Ni22 -177.0(9) . . . . ? C37 Ni21 C42 Ni22 118.1(14) 3 . . . ? Ni28 Ni21 C42 Ni22 -149.6(3) . . . . ? Ni24 Ni21 C42 Ni22 148.2(3) 3 . . . ? Ni27 Ni21 C42 Ni22 -104.3(5) . . . . ? C38' Ni21 C42 Ni24 106(7) 3 . . . ? C32 Ni21 C42 Ni24 -67.1(10) . . . . ? C38 Ni21 C42 Ni24 169.6(15) . . . . ? C41 Ni21 C42 Ni24 119.9(12) . . . . ? C37 Ni21 C42 Ni24 55.0(17) 3 . . . ? Ni22 Ni21 C42 Ni24 -63.1(7) . . . . ? Ni28 Ni21 C42 Ni24 147.3(8) . . . . ? Ni24 Ni21 C42 Ni24 85.1(7) 3 . . . ? Ni27 Ni21 C42 Ni24 -167.4(11) . . . . ? C38' Ni21 C42 Ni27 -86(7) 3 . . . ? C32 Ni21 C42 Ni27 100.2(7) . . . . ? C38 Ni21 C42 Ni27 -23.1(15) . . . . ? C41 Ni21 C42 Ni27 -72.7(7) . . . . ? C37 Ni21 C42 Ni27 -137.7(14) 3 . . . ? Ni22 Ni21 C42 Ni27 104.3(5) . . . . ? Ni28 Ni21 C42 Ni27 -45.3(3) . . . . ? Ni24 Ni21 C42 Ni27 -107.5(4) 3 . . . ? C38' Ni21 C42 Ni26 -19(7) 3 . . . ? C32 Ni21 C42 Ni26 167.9(12) . . . . ? C38 Ni21 C42 Ni26 44.6(19) . . . . ? C41 Ni21 C42 Ni26 -5.0(8) . . . . ? C37 Ni21 C42 Ni26 -69.9(18) 3 . . . ? Ni22 Ni21 C42 Ni26 172.0(13) . . . . ? Ni28 Ni21 C42 Ni26 22.4(10) . . . . ? Ni24 Ni21 C42 Ni26 -39.8(10) 3 . . . ? Ni27 Ni21 C42 Ni26 67.7(10) . . . . ? C38' Ni21 C42 Ni25 -140(7) 3 . . . ? C32 Ni21 C42 Ni25 46.9(11) . . . . ? C38 Ni21 C42 Ni25 -76.4(17) . . . . ? C41 Ni21 C42 Ni25 -126.0(13) . . . . ? C37 Ni21 C42 Ni25 169.1(15) 3 . . . ? Ni22 Ni21 C42 Ni25 51.0(7) . . . . ? Ni28 Ni21 C42 Ni25 -98.6(8) . . . . ? Ni24 Ni21 C42 Ni25 -160.8(9) 3 . . . ? Ni27 Ni21 C42 Ni25 -53.3(7) . . . . ? C43' Ni23 C43 O43 -104(20) . . . . ? C35 Ni23 C43 O43 -92(13) 3 . . . ? C41 Ni23 C43 O43 63(14) 3 . . . ? Ni29 Ni23 C43 O43 122(13) . . . . ? Ni26 Ni23 C43 O43 -78(13) 3 . . . ? Ni24 Ni23 C43 O43 108(13) . . . . ? Ni28 Ni23 C43 O43 46(13) 3 . . . ? Ni22 Ni23 C43 O43 165(13) . . . . ? C44' Ni22 C44 O44 43(16) . . . . ? C32 Ni22 C44 O44 142(15) . . . . ? C42 Ni22 C44 O44 -35(18) . . . . ? Ni21 Ni22 C44 O44 146(13) . . . . ? Ni25 Ni22 C44 O44 -6(16) . . . . ? Ni29 Ni22 C44 O44 -91(16) . . . . ? Ni24 Ni22 C44 O44 -71(16) . . . . ? Ni23 Ni22 C44 O44 -127(15) . . . . ? C45' Ni24 C45 O45 131(95) . . . . ? C42 Ni24 C45 O45 -121(53) . . . . ? C41 Ni24 C45 O45 31(55) 3 . . . ? C37 Ni24 C45 O45 137(53) . . . . ? Ni29 Ni24 C45 O45 -37(51) . . . . ? Ni21 Ni24 C45 O45 96(52) 3 . . . ? Ni23 Ni24 C45 O45 -12(54) . . . . ? Ni22 Ni24 C45 O45 -80(53) . . . . ? Ni28 Ni24 C45 O45 46(53) 3 . . . ? Ni26 Ni24 C45 O45 178(100) . . . . ? Ni25 Ni24 C45 O45 -137(53) . . . . ? C43' Ni23 Ni29 C46 -20(4) . . . . ? C43 Ni23 Ni29 C46 -9(4) . . . . ? C35 Ni23 Ni29 C46 -67(3) 3 . . . ? C41 Ni23 Ni29 C46 140(3) 3 . . . ? Ni26 Ni23 Ni29 C46 -167(3) 3 . . . ? Ni24 Ni23 Ni29 C46 154(3) . . . . ? Ni28 Ni23 Ni29 C46 95(3) 3 . . . ? Ni22 Ni23 Ni29 C46 -138(3) . . . . ? C43 Ni23 Ni29 C43' 12(3) . . . . ? C35 Ni23 Ni29 C43' -47(2) 3 . . . ? C41 Ni23 Ni29 C43' 160(2) 3 . . . ? Ni26 Ni23 Ni29 C43' -147(2) 3 . . . ? Ni24 Ni23 Ni29 C43' 174(2) . . . . ? Ni28 Ni23 Ni29 C43' 116(2) 3 . . . ? Ni22 Ni23 Ni29 C43' -117(2) . . . . ? C43' Ni23 Ni29 C45' -152(3) . . . . ? C43 Ni23 Ni29 C45' -140(3) . . . . ? C35 Ni23 Ni29 C45' 162(3) 3 . . . ? C41 Ni23 Ni29 C45' 8(3) 3 . . . ? Ni26 Ni23 Ni29 C45' 62(3) 3 . . . ? Ni24 Ni23 Ni29 C45' 23(3) . . . . ? Ni28 Ni23 Ni29 C45' -36(3) 3 . . . ? Ni22 Ni23 Ni29 C45' 91(3) . . . . ? C43' Ni23 Ni29 Ni24 -174(2) . . . . ? C43 Ni23 Ni29 Ni24 -162.8(16) . . . . ? C35 Ni23 Ni29 Ni24 139.1(8) 3 . . . ? C41 Ni23 Ni29 Ni24 -14.4(5) 3 . . . ? Ni26 Ni23 Ni29 Ni24 38.8(6) 3 . . . ? Ni28 Ni23 Ni29 Ni24 -58.64(14) 3 . . . ? Ni22 Ni23 Ni29 Ni24 68.37(14) . . . . ? C43' Ni23 Ni29 Ni22 117(2) . . . . ? C43 Ni23 Ni29 Ni22 128.8(16) . . . . ? C35 Ni23 Ni29 Ni22 70.7(9) 3 . . . ? C41 Ni23 Ni29 Ni22 -82.8(4) 3 . . . ? Ni26 Ni23 Ni29 Ni22 -29.6(6) 3 . . . ? Ni24 Ni23 Ni29 Ni22 -68.37(14) . . . . ? Ni28 Ni23 Ni29 Ni22 -127.01(14) 3 . . . ? C45' Ni24 Ni29 C46 -5(6) . . . . ? C45 Ni24 Ni29 C46 -3(5) . . . . ? C42 Ni24 Ni29 C46 127(4) . . . . ? C41 Ni24 Ni29 C46 -140(4) 3 . . . ? C37 Ni24 Ni29 C46 -12(4) . . . . ? Ni21 Ni24 Ni29 C46 -98(4) 3 . . . ? Ni23 Ni24 Ni29 C46 -153(4) . . . . ? Ni22 Ni24 Ni29 C46 128(4) . . . . ? Ni28 Ni24 Ni29 C46 -94(4) 3 . . . ? Ni26 Ni24 Ni29 C46 81(4) . . . . ? Ni25 Ni24 Ni29 C46 78(4) . . . . ? C45' Ni24 Ni29 C43' 144(5) . . . . ? C45 Ni24 Ni29 C43' 146(4) . . . . ? C42 Ni24 Ni29 C43' -84.0(16) . . . . ? C41 Ni24 Ni29 C43' 8.9(16) 3 . . . ? C37 Ni24 Ni29 C43' 137(2) . . . . ? Ni21 Ni24 Ni29 C43' 51.0(16) 3 . . . ? Ni23 Ni24 Ni29 C43' -4.2(15) . . . . ? Ni22 Ni24 Ni29 C43' -83.6(15) . . . . ? Ni28 Ni24 Ni29 C43' 54.5(15) 3 . . . ? Ni26 Ni24 Ni29 C43' -130.0(15) . . . . ? Ni25 Ni24 Ni29 C43' -133.7(15) . . . . ? C45 Ni24 Ni29 C45' 2(8) . . . . ? C42 Ni24 Ni29 C45' 132(4) . . . . ? C41 Ni24 Ni29 C45' -135(4) 3 . . . ? C37 Ni24 Ni29 C45' -7(5) . . . . ? Ni21 Ni24 Ni29 C45' -93(4) 3 . . . ? Ni23 Ni24 Ni29 C45' -148(4) . . . . ? Ni22 Ni24 Ni29 C45' 132(4) . . . . ? Ni28 Ni24 Ni29 C45' -90(4) 3 . . . ? Ni26 Ni24 Ni29 C45' 86(4) . . . . ? Ni25 Ni24 Ni29 C45' 82(4) . . . . ? C45' Ni24 Ni29 Ni23 148(4) . . . . ? C45 Ni24 Ni29 Ni23 150(3) . . . . ? C42 Ni24 Ni29 Ni23 -79.8(4) . . . . ? C41 Ni24 Ni29 Ni23 13.1(4) 3 . . . ? C37 Ni24 Ni29 Ni23 141.1(17) . . . . ? Ni21 Ni24 Ni29 Ni23 55.2(4) 3 . . . ? Ni22 Ni24 Ni29 Ni23 -79.35(18) . . . . ? Ni28 Ni24 Ni29 Ni23 58.68(15) 3 . . . ? Ni26 Ni24 Ni29 Ni23 -125.8(3) . . . . ? Ni25 Ni24 Ni29 Ni23 -129.47(16) . . . . ? C45' Ni24 Ni29 Ni22 -132(4) . . . . ? C45 Ni24 Ni29 Ni22 -131(3) . . . . ? C42 Ni24 Ni29 Ni22 -0.5(4) . . . . ? C41 Ni24 Ni29 Ni22 92.5(4) 3 . . . ? C37 Ni24 Ni29 Ni22 -139.5(17) . . . . ? Ni21 Ni24 Ni29 Ni22 134.6(3) 3 . . . ? Ni23 Ni24 Ni29 Ni22 79.35(18) . . . . ? Ni28 Ni24 Ni29 Ni22 138.03(14) 3 . . . ? Ni26 Ni24 Ni29 Ni22 -46.5(4) . . . . ? Ni25 Ni24 Ni29 Ni22 -50.12(13) . . . . ? C44' Ni22 Ni29 C46 6(4) . . . . ? C44 Ni22 Ni29 C46 16(4) . . . . ? C32 Ni22 Ni29 C46 92(3) . . . . ? C42 Ni22 Ni29 C46 -140(3) . . . . ? Ni21 Ni22 Ni29 C46 160(3) . . . . ? Ni25 Ni22 Ni29 C46 -88(3) . . . . ? Ni24 Ni22 Ni29 C46 -141(3) . . . . ? Ni23 Ni22 Ni29 C46 145(3) . . . . ? C44' Ni22 Ni29 C43' -101(3) . . . . ? C44 Ni22 Ni29 C43' -91(3) . . . . ? C32 Ni22 Ni29 C43' -15.0(15) . . . . ? C42 Ni22 Ni29 C43' 113.2(13) . . . . ? Ni21 Ni22 Ni29 C43' 53.7(13) . . . . ? Ni25 Ni22 Ni29 C43' 165.4(12) . . . . ? Ni24 Ni22 Ni29 C43' 112.7(12) . . . . ? Ni23 Ni22 Ni29 C43' 38.6(12) . . . . ? C44' Ni22 Ni29 C45' 115(4) . . . . ? C44 Ni22 Ni29 C45' 125(3) . . . . ? C32 Ni22 Ni29 C45' -159(3) . . . . ? C42 Ni22 Ni29 C45' -31(2) . . . . ? Ni21 Ni22 Ni29 C45' -91(2) . . . . ? Ni25 Ni22 Ni29 C45' 21(2) . . . . ? Ni24 Ni22 Ni29 C45' -32(2) . . . . ? Ni23 Ni22 Ni29 C45' -106(2) . . . . ? C44' Ni22 Ni29 Ni23 -140(3) . . . . ? C44 Ni22 Ni29 Ni23 -129(2) . . . . ? C32 Ni22 Ni29 Ni23 -53.6(8) . . . . ? C42 Ni22 Ni29 Ni23 74.5(4) . . . . ? Ni21 Ni22 Ni29 Ni23 15.1(3) . . . . ? Ni25 Ni22 Ni29 Ni23 126.73(16) . . . . ? Ni24 Ni22 Ni29 Ni23 74.08(17) . . . . ? C44' Ni22 Ni29 Ni24 146(3) . . . . ? C44 Ni22 Ni29 Ni24 157(2) . . . . ? C32 Ni22 Ni29 Ni24 -127.7(8) . . . . ? C42 Ni22 Ni29 Ni24 0.5(4) . . . . ? Ni21 Ni22 Ni29 Ni24 -59.0(3) . . . . ? Ni25 Ni22 Ni29 Ni24 52.65(14) . . . . ? Ni23 Ni22 Ni29 Ni24 -74.08(17) . . . . ? C43 Ni23 C43' O43' 146(24) . . . . ? C35 Ni23 C43' O43' -22(13) 3 . . . ? C41 Ni23 C43' O43' 126(11) 3 . . . ? Ni29 Ni23 C43' O43' -174(14) . . . . ? Ni26 Ni23 C43' O43' -16(15) 3 . . . ? Ni28 Ni23 C43' O43' 115(13) 3 . . . ? Ni22 Ni23 C43' O43' -124(13) . . . . ? C43 Ni23 C43' Ni29 -40(12) . . . . ? C35 Ni23 C43' Ni29 151.9(12) 3 . . . ? C41 Ni23 C43' Ni29 -60(5) 3 . . . ? Ni26 Ni23 C43' Ni29 158.3(13) 3 . . . ? Ni24 Ni23 C43' Ni29 -5.2(19) . . . . ? Ni28 Ni23 C43' Ni29 -70.8(14) 3 . . . ? Ni22 Ni23 C43' Ni29 50.1(11) . . . . ? C46 Ni29 C43' O43' -15(5) . . . . ? C45' Ni29 C43' O43' -134(4) . . . . ? Ni23 Ni29 C43' O43' 178(6) . . . . ? Ni24 Ni29 C43' O43' -177(4) . . . . ? Ni22 Ni29 C43' O43' 120(4) . . . . ? C46 Ni29 C43' Ni23 167(2) . . . . ? C45' Ni29 C43' Ni23 49(4) . . . . ? Ni24 Ni29 C43' Ni23 6(2) . . . . ? Ni22 Ni29 C43' Ni23 -57.7(15) . . . . ? C44 Ni22 C44' O44' 99(29) . . . . ? C32 Ni22 C44' O44' 15(20) . . . . ? C42 Ni22 C44' O44' -139(17) . . . . ? Ni25 Ni22 C44' O44' -129(19) . . . . ? Ni29 Ni22 C44' O44' 141(20) . . . . ? Ni24 Ni22 C44' O44' 170(18) . . . . ? Ni23 Ni22 C44' O44' 110(19) . . . . ? C42 Ni24 C45' O45' 85(22) . . . . ? C41 Ni24 C45' O45' -107(21) 3 . . . ? C37 Ni24 C45' O45' -9(21) . . . . ? Ni29 Ni24 C45' O45' 176(24) . . . . ? Ni21 Ni24 C45' O45' -48(23) 3 . . . ? Ni23 Ni24 C45' O45' -157(21) . . . . ? Ni22 Ni24 C45' O45' 132(21) . . . . ? Ni28 Ni24 C45' O45' -101(22) 3 . . . ? Ni26 Ni24 C45' O45' 29(23) . . . . ? Ni25 Ni24 C45' O45' 78(22) . . . . ? C42 Ni24 C45' Ni29 -90(3) . . . . ? C41 Ni24 C45' Ni29 77(4) 3 . . . ? C37 Ni24 C45' Ni29 175(3) . . . . ? Ni21 Ni24 C45' Ni29 136.1(11) 3 . . . ? Ni23 Ni24 C45' Ni29 27(3) . . . . ? Ni22 Ni24 C45' Ni29 -43(3) . . . . ? Ni28 Ni24 C45' Ni29 83(2) 3 . . . ? Ni26 Ni24 C45' Ni29 -146.6(9) . . . . ? Ni25 Ni24 C45' Ni29 -98(2) . . . . ? C46 Ni29 C45' O45' 0(11) . . . . ? C43' Ni29 C45' O45' 119(9) . . . . ? Ni23 Ni29 C45' O45' 152(10) . . . . ? Ni24 Ni29 C45' O45' -178(13) . . . . ? Ni22 Ni29 C45' O45' -136(10) . . . . ? C46 Ni29 C45' Ni24 177(3) . . . . ? C43' Ni29 C45' Ni24 -64(5) . . . . ? Ni23 Ni29 C45' Ni24 -31(4) . . . . ? Ni22 Ni29 C45' Ni24 42(3) . . . . ? C43' Ni29 C46 O46 85(89) . . . . ? C45' Ni29 C46 O46 -128(88) . . . . ? Ni23 Ni29 C46 O46 99(88) . . . . ? Ni24 Ni29 C46 O46 -125(87) . . . . ? Ni22 Ni29 C46 O46 -20(90) . . . . ? C107 N1 C101 C102 -58.7(19) . . . . ? C103 N1 C101 C102 59.6(19) . . . . ? C105 N1 C101 C102 178.5(17) . . . . ? C107 N1 C103 C104 176.9(15) . . . . ? C101 N1 C103 C104 56.0(18) . . . . ? C105 N1 C103 C104 -61.3(18) . . . . ? C107 N1 C105 C106 58.2(19) . . . . ? C103 N1 C105 C106 -60.0(19) . . . . ? C101 N1 C105 C106 -179.8(16) . . . . ? C103 N1 C107 C108 175.4(16) . . . . ? C101 N1 C107 C108 -63.9(19) . . . . ? C105 N1 C107 C108 55.6(19) . . . . ? C203 N2 C201 C202 64(2) . . . . ? C207 N2 C201 C202 -58(2) . . . . ? C205 N2 C201 C202 -175(2) . . . . ? C207 N2 C203 C204 178.0(19) . . . . ? C201 N2 C203 C204 54(2) . . . . ? C205 N2 C203 C204 -59(2) . . . . ? C203 N2 C205 C206 -52(3) . . . . ? C207 N2 C205 C206 70(3) . . . . ? C201 N2 C205 C206 -171(2) . . . . ? C203 N2 C207 C208 173.6(18) . . . . ? C201 N2 C207 C208 -64(2) . . . . ? C205 N2 C207 C208 49(2) . . . . ? C3A5 N3 C301 C302 148(21) . . . . ? C307 N3 C301 C302 -80(4) . . . . ? C303 N3 C301 C302 42(4) . . . . ? C3A7 N3 C301 C302 103(4) . . . . ? C305 N3 C301 C302 162(4) . . . . ? C3A3 N3 C301 C302 -133(4) . . . . ? C3A1 N3 C301 C302 -18(4) . . . . ? C3A5 N3 C303 C304 -103(4) . . . . ? C301 N3 C303 C304 72(4) . . . . ? C307 N3 C303 C304 -166(4) . . . . ? C3A7 N3 C303 C304 18(4) . . . . ? C305 N3 C303 C304 -48(4) . . . . ? C3A3 N3 C303 C304 177(100) . . . . ? C3A1 N3 C303 C304 134(4) . . . . ? C3A5 N3 C305 C306 -8(4) . . . . ? C301 N3 C305 C306 174(4) . . . . ? C307 N3 C305 C306 54(4) . . . . ? C303 N3 C305 C306 -64(4) . . . . ? C3A7 N3 C305 C306 -134(4) . . . . ? C3A3 N3 C305 C306 112(4) . . . . ? C3A1 N3 C305 C306 -13(49) . . . . ? C3A5 N3 C307 C308 139(4) . . . . ? C301 N3 C307 C308 -36(4) . . . . ? C303 N3 C307 C308 -159(4) . . . . ? C3A7 N3 C307 C308 -11(19) . . . . ? C305 N3 C307 C308 82(4) . . . . ? C3A3 N3 C307 C308 19(4) . . . . ? C3A1 N3 C307 C308 -101(4) . . . . ? C3A5 N3 C3A1 C3A2 161(4) . . . . ? C301 N3 C3A1 C3A2 -20(4) . . . . ? C307 N3 C3A1 C3A2 99(4) . . . . ? C303 N3 C3A1 C3A2 -141(4) . . . . ? C3A7 N3 C3A1 C3A2 -74(4) . . . . ? C305 N3 C3A1 C3A2 167(46) . . . . ? C3A3 N3 C3A1 C3A2 42(4) . . . . ? C3A5 N3 C3A3 C3A4 -47(4) . . . . ? C301 N3 C3A3 C3A4 139(4) . . . . ? C307 N3 C3A3 C3A4 13(4) . . . . ? C303 N3 C3A3 C3A4 31(26) . . . . ? C3A7 N3 C3A3 C3A4 -170(4) . . . . ? C305 N3 C3A3 C3A4 -105(4) . . . . ? C3A1 N3 C3A3 C3A4 73(4) . . . . ? C301 N3 C3A5 C3A6 0(24) . . . . ? C307 N3 C3A5 C3A6 -133(4) . . . . ? C303 N3 C3A5 C3A6 109(4) . . . . ? C3A7 N3 C3A5 C3A6 43(4) . . . . ? C305 N3 C3A5 C3A6 -14(4) . . . . ? C3A3 N3 C3A5 C3A6 -76(4) . . . . ? C3A1 N3 C3A5 C3A6 166(4) . . . . ? C3A5 N3 C3A7 C3A8 73(4) . . . . ? C301 N3 C3A7 C3A8 -112(4) . . . . ? C307 N3 C3A7 C3A8 -138(17) . . . . ? C303 N3 C3A7 C3A8 11(4) . . . . ? C305 N3 C3A7 C3A8 127(4) . . . . ? C3A3 N3 C3A7 C3A8 -167(4) . . . . ? C3A1 N3 C3A7 C3A8 -51(4) . . . . ? C407 N4 C401 C402 -60(3) . . . . ? C403 N4 C401 C402 57(3) . . . . ? C405 N4 C401 C402 177(3) . . . . ? C407 N4 C403 C404 -174(3) . . . . ? C405 N4 C403 C404 -53(4) . . . . ? C401 N4 C403 C404 65(4) . . . . ? C407 N4 C405 C406 -45(3) . . . . ? C403 N4 C405 C406 -160(2) . . . . ? C401 N4 C405 C406 77(2) . . . . ? C403 N4 C407 C408 60(4) . . . . ? C405 N4 C407 C408 -59(4) . . . . ? C401 N4 C407 C408 -177(3) . . . . ? C503 N5 C501 C502 58(3) . . . . ? C505 N5 C501 C502 178(2) . . . . ? C507 N5 C501 C502 -60(3) . . . . ? C505 N5 C503 C504 -70(3) . . . . ? C507 N5 C503 C504 167(3) . . . . ? C501 N5 C503 C504 49(3) . . . . ? C503 N5 C505 C506 177(2) . . . . ? C507 N5 C505 C506 -63(3) . . . . ? C501 N5 C505 C506 55(3) . . . . ? C503 N5 C507 C508 71(3) . . . . ? C505 N5 C507 C508 -49(3) . . . . ? C501 N5 C507 C508 -168(2) . . . . ? C6A7 N6 C601 C602 140(4) . . . . ? C607 N6 C601 C602 -46(4) . . . . ? C605 N6 C601 C602 -173(4) . . . . ? C6A5 N6 C601 C602 -4(9) . . . . ? C603 N6 C601 C602 69(4) . . . . ? C6A1 N6 C601 C602 11(3) . . . . ? C6A3 N6 C601 C602 -108(4) . . . . ? C6A7 N6 C603 C604 -11(4) . . . . ? C607 N6 C603 C604 -177(4) . . . . ? C605 N6 C603 C604 -55(4) . . . . ? C601 N6 C603 C604 60(4) . . . . ? C6A5 N6 C603 C604 -136(4) . . . . ? C6A1 N6 C603 C604 110(4) . . . . ? C6A3 N6 C603 C604 -151(23) . . . . ? C6A7 N6 C605 C606 -102(4) . . . . ? C607 N6 C605 C606 69(4) . . . . ? C601 N6 C605 C606 -163(4) . . . . ? C6A5 N6 C605 C606 20(4) . . . . ? C603 N6 C605 C606 -46(4) . . . . ? C6A1 N6 C605 C606 -148(7) . . . . ? C6A3 N6 C605 C606 129(4) . . . . ? C6A7 N6 C607 C608 81(8) . . . . ? C605 N6 C607 C608 51(4) . . . . ? C601 N6 C607 C608 -71(4) . . . . ? C6A5 N6 C607 C608 122(4) . . . . ? C603 N6 C607 C608 170(3) . . . . ? C6A1 N6 C607 C608 -120(4) . . . . ? C6A3 N6 C607 C608 -8(3) . . . . ? C6A7 N6 C6A1 C6A2 -52(4) . . . . ? C607 N6 C6A1 C6A2 133(4) . . . . ? C605 N6 C6A1 C6A2 -12(10) . . . . ? C601 N6 C6A1 C6A2 4(4) . . . . ? C6A5 N6 C6A1 C6A2 180(4) . . . . ? C603 N6 C6A1 C6A2 -119(4) . . . . ? C6A3 N6 C6A1 C6A2 66(4) . . . . ? C6A7 N6 C6A3 C6A4 177(3) . . . . ? C607 N6 C6A3 C6A4 -18(3) . . . . ? C605 N6 C6A3 C6A4 -142(4) . . . . ? C601 N6 C6A3 C6A4 105(4) . . . . ? C6A5 N6 C6A3 C6A4 -58(4) . . . . ? C603 N6 C6A3 C6A4 -44(26) . . . . ? C6A1 N6 C6A3 C6A4 53(4) . . . . ? C6A7 N6 C6A5 C6A6 49(4) . . . . ? C607 N6 C6A5 C6A6 -121(4) . . . . ? C605 N6 C6A5 C6A6 -1(4) . . . . ? C601 N6 C6A5 C6A6 -171(7) . . . . ? C603 N6 C6A5 C6A6 110(4) . . . . ? C6A1 N6 C6A5 C6A6 176(3) . . . . ? C6A3 N6 C6A5 C6A6 -71(4) . . . . ? C607 N6 C6A7 C6A8 118(7) . . . . ? C605 N6 C6A7 C6A8 152(5) . . . . ? C601 N6 C6A7 C6A8 -87(4) . . . . ? C6A5 N6 C6A7 C6A8 83(4) . . . . ? C603 N6 C6A7 C6A8 26(4) . . . . ? C6A1 N6 C6A7 C6A8 -39(4) . . . . ? C6A3 N6 C6A7 C6A8 -157(4) . . . . ? _diffrn_measured_fraction_theta_max 0.999 _diffrn_reflns_theta_full 25.03 _diffrn_measured_fraction_theta_full 0.999 _refine_diff_density_max 1.909 _refine_diff_density_min -1.325 _refine_diff_density_rms 0.156 # Attachment '- ni25P2N.CIF' data_p2n _database_code_depnum_ccdc_archive 'CCDC 846298' #TrackingRef '- ni25P2N.CIF' _audit_creation_method SHELXL-97 _chemical_name_systematic ; ? ; _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'C81 H98 N4 Ni25 O35' _chemical_formula_weight 3155.38 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ni Ni 0.3393 1.1124 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _symmetry_cell_setting monoclinic _symmetry_space_group_name_H-M P2/n loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y, -z+1/2' '-x, -y, -z' 'x-1/2, -y, z-1/2' _cell_length_a 17.2678(8) _cell_length_b 14.1381(6) _cell_length_c 22.0522(10) _cell_angle_alpha 90.00 _cell_angle_beta 91.4890(10) _cell_angle_gamma 90.00 _cell_volume 5381.9(4) _cell_formula_units_Z 2 _cell_measurement_temperature 293(2) _cell_measurement_reflns_used 9924 _cell_measurement_theta_min 2.343 _cell_measurement_theta_max 24.3095 _exptl_crystal_description prism _exptl_crystal_colour dark-brown _exptl_crystal_size_max 0.19 _exptl_crystal_size_mid 0.15 _exptl_crystal_size_min 0.12 _exptl_crystal_density_meas ? _exptl_crystal_density_diffrn 1.947 _exptl_crystal_density_method 'not measured' _exptl_crystal_F_000 3184 _exptl_absorpt_coefficient_mu 4.328 _exptl_absorpt_correction_type empirical _exptl_absorpt_correction_T_min 0.4935 _exptl_absorpt_correction_T_max 0.6247 _exptl_absorpt_process_details ? _exptl_special_details ; ? ; _diffrn_ambient_temperature 293(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_radiation_source 'fine-focus sealed tube' _diffrn_radiation_monochromator graphite _diffrn_measurement_device_type 'CCD area detector' _diffrn_measurement_method 'phi and omega scans' _diffrn_detector_area_resol_mean ? _diffrn_standards_number ? _diffrn_standards_interval_count ? _diffrn_standards_interval_time ? _diffrn_standards_decay_% ? _diffrn_reflns_number 55055 _diffrn_reflns_av_R_equivalents 0.0680 _diffrn_reflns_av_sigmaI/netI 0.0539 _diffrn_reflns_limit_h_min -21 _diffrn_reflns_limit_h_max 21 _diffrn_reflns_limit_k_min -17 _diffrn_reflns_limit_k_max 17 _diffrn_reflns_limit_l_min -27 _diffrn_reflns_limit_l_max 27 _diffrn_reflns_theta_min 1.44 _diffrn_reflns_theta_max 26.00 _reflns_number_total 10574 _reflns_number_gt 6456 _reflns_threshold_expression >2sigma(I) _computing_data_collection ? _computing_cell_refinement ? _computing_data_reduction ? _computing_structure_solution 'SHELXS-97 (Sheldrick, 1990)' _computing_structure_refinement 'SHELXL-97 (Sheldrick, 1997)' _computing_molecular_graphics ? _computing_publication_material ? _refine_special_details ; Refinement of F^2^ against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F^2^, conventional R-factors R are based on F, with F set to zero for negative F^2^. The threshold expression of F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F^2^ are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger. ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'calc w=1/[\s^2^(Fo^2^)+(0.0421P)^2^+9.5882P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef ? _refine_ls_number_reflns 10574 _refine_ls_number_parameters 624 _refine_ls_number_restraints 114 _refine_ls_R_factor_all 0.0893 _refine_ls_R_factor_gt 0.0417 _refine_ls_wR_factor_ref 0.1089 _refine_ls_wR_factor_gt 0.0873 _refine_ls_goodness_of_fit_ref 1.000 _refine_ls_restrained_S_all 1.040 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_symmetry_multiplicity _atom_site_calc_flag _atom_site_refinement_flags _atom_site_disorder_assembly _atom_site_disorder_group Ni1 Ni 0.7500 0.28050(7) 0.7500 0.0327(2) Uani 1 2 d S . . Ni2 Ni 0.83645(5) 0.28914(5) 0.64851(3) 0.0387(2) Uani 1 1 d . . . Ni3 Ni 0.61887(4) 0.27183(5) 0.67842(3) 0.03808(19) Uani 1 1 d . . . Ni4 Ni 0.73577(4) 0.14185(6) 0.66312(4) 0.0391(2) Uani 1 1 d . . . Ni5 Ni 0.71974(4) 0.41522(6) 0.66489(3) 0.03651(19) Uani 1 1 d . . . Ni6 Ni 0.94797(4) 0.38137(6) 0.72234(4) 0.0414(2) Uani 1 1 d . . . Ni7 Ni 0.94775(5) 0.18452(6) 0.72328(4) 0.0434(2) Uani 1 1 d . . . Ni8 Ni 0.82821(5) 0.52675(6) 0.73737(4) 0.0404(2) Uani 1 1 d . . . Ni9 Ni 0.57679(5) 0.44388(6) 0.67681(4) 0.0441(2) Uani 1 1 d . . . Ni10 Ni 0.82999(5) 0.03364(6) 0.73971(4) 0.0446(2) Uani 1 1 d . . . Ni11 Ni 0.85442(5) 0.46520(6) 0.63660(4) 0.0443(2) Uani 1 1 d . . . Ni12 Ni 0.87663(5) 0.11922(6) 0.63605(4) 0.0465(2) Uani 1 1 d . . . Ni13 Ni 0.59572(5) 0.09563(6) 0.67308(4) 0.0472(2) Uani 1 1 d . . . C1 C 0.6557(3) 0.3861(4) 0.7319(3) 0.0328(13) Uani 1 1 d . . . C2 C 0.8267(3) 0.3868(4) 0.7073(3) 0.0333(13) Uani 1 1 d . . . C3 C 0.6573(3) 0.1740(4) 0.7302(3) 0.0379(14) Uani 1 1 d . . . C4 C 0.8282(3) 0.1749(4) 0.7080(3) 0.0354(14) Uani 1 1 d . . . C5 C 0.5220(4) 0.0840(5) 0.6202(4) 0.068(2) Uani 1 1 d . . . C6 C 0.5687(4) 0.2944(5) 0.6092(3) 0.0567(19) Uani 1 1 d . . . C7 C 0.5499(4) 0.5182(5) 0.6161(3) 0.0543(18) Uani 1 1 d . . . C8 C 0.7213(4) 0.4572(6) 0.5905(3) 0.060(2) Uani 1 1 d . . . C9 C 0.8293(4) 0.6222(5) 0.7879(3) 0.0591(19) Uani 1 1 d . . . C10 C 0.8490(4) 0.5914(5) 0.6644(3) 0.0496(17) Uani 1 1 d . . . C11 C 1.0124(4) 0.3704(5) 0.6632(3) 0.0555(19) Uani 1 1 d . . . C12 C 1.0368(5) 0.2021(6) 0.7613(4) 0.068(2) Uani 1 1 d . . . C13 C 0.9838(4) 0.1354(5) 0.6491(3) 0.0541(18) Uani 1 1 d . . . C14 C 0.8047(5) -0.0622(6) 0.6922(4) 0.067(2) Uani 1 1 d . . . C15 C 0.6989(5) 0.0884(6) 0.5971(4) 0.071(2) Uani 1 1 d . . . C16 C 0.8726(4) 0.0449(5) 0.5746(3) 0.060(2) Uani 1 1 d . . . C17 C 0.8562(6) 0.2649(6) 0.5734(4) 0.086(3) Uani 1 1 d . . . C18 C 0.8921(4) 0.4811(5) 0.5656(3) 0.064(2) Uani 1 1 d . . . C19 C 0.4837(4) 0.4342(5) 0.7182(3) 0.0567(19) Uani 1 1 d . . . C20 C 0.8914(4) -0.0301(5) 0.7990(3) 0.0532(18) Uani 1 1 d . . . O5 O 0.4715(4) 0.0760(5) 0.5850(3) 0.116(2) Uani 1 1 d U . . O6 O 0.5384(4) 0.2983(4) 0.5623(3) 0.091(2) Uani 1 1 d . . . O7 O 0.5309(4) 0.5678(5) 0.5783(3) 0.100(2) Uani 1 1 d . . . O8 O 0.7103(4) 0.4815(5) 0.5410(3) 0.0971(19) Uani 1 1 d U . . O9 O 0.8308(4) 0.6868(4) 0.8190(3) 0.096(2) Uani 1 1 d . . . O10 O 0.8552(3) 0.6674(4) 0.6454(2) 0.0747(16) Uani 1 1 d . . . O11 O 1.0560(3) 0.3650(5) 0.6250(3) 0.0896(19) Uani 1 1 d . . . O12 O 1.0969(3) 0.2100(5) 0.7832(3) 0.102(2) Uani 1 1 d . . . O13 O 1.0420(3) 0.1215(4) 0.6248(3) 0.0813(17) Uani 1 1 d . . . O14 O 0.7911(4) -0.1245(4) 0.6610(3) 0.100(2) Uani 1 1 d . . . O15 O 0.6878(4) 0.0532(5) 0.5501(3) 0.108(2) Uani 1 1 d U . . O16 O 0.8708(4) -0.0048(5) 0.5338(3) 0.102(2) Uani 1 1 d U . . O17 O 0.8669(5) 0.2655(5) 0.5220(3) 0.118(2) Uani 1 1 d U . . O18 O 0.9145(4) 0.4945(5) 0.5178(3) 0.106(2) Uani 1 1 d U . . O19 O 0.4181(3) 0.4516(4) 0.7111(3) 0.0847(17) Uani 1 1 d U . . O20 O 0.9125(3) -0.1058(4) 0.8125(2) 0.0776(16) Uani 1 1 d . . . N1 N 0.0716(3) 0.7922(4) 0.6808(3) 0.0624(16) Uani 1 1 d D . . C101 C 0.0179(6) 0.7565(7) 0.7273(4) 0.101(3) Uani 1 1 d DU . . H10A H -0.0226 0.7201 0.7069 0.122 Uiso 1 1 calc R . . H10B H -0.0065 0.8103 0.7462 0.122 Uiso 1 1 calc R . . C102 C 0.0549(7) 0.6955(8) 0.7766(5) 0.130(4) Uani 1 1 d DU . . H10C H 0.0162 0.6770 0.8048 0.196 Uiso 1 1 calc R . . H10D H 0.0949 0.7308 0.7975 0.196 Uiso 1 1 calc R . . H10E H 0.0769 0.6401 0.7587 0.196 Uiso 1 1 calc R . . C103 C 0.1339(4) 0.8522(6) 0.7085(4) 0.083(2) Uani 1 1 d DU . . H10F H 0.1674 0.8728 0.6764 0.099 Uiso 1 1 calc R . . H10G H 0.1648 0.8130 0.7359 0.099 Uiso 1 1 calc R . . C104 C 0.1083(6) 0.9391(6) 0.7432(4) 0.097(3) Uani 1 1 d DU . . H10H H 0.1530 0.9722 0.7589 0.146 Uiso 1 1 calc R . . H10I H 0.0765 0.9201 0.7761 0.146 Uiso 1 1 calc R . . H10J H 0.0791 0.9801 0.7164 0.146 Uiso 1 1 calc R . . C105 C 0.0212(5) 0.8477(7) 0.6379(4) 0.097(3) Uani 1 1 d DU . . H10K H -0.0029 0.8984 0.6603 0.116 Uiso 1 1 calc R . . H10L H -0.0199 0.8067 0.6226 0.116 Uiso 1 1 calc R . . C106 C 0.0615(6) 0.8906(7) 0.5840(4) 0.116(3) Uani 1 1 d DU . . H10M H 0.0244 0.9243 0.5591 0.175 Uiso 1 1 calc R . . H10N H 0.0846 0.8412 0.5607 0.175 Uiso 1 1 calc R . . H10O H 0.1011 0.9335 0.5983 0.175 Uiso 1 1 calc R . . C107 C 0.1109(5) 0.7127(5) 0.6487(4) 0.084(2) Uani 1 1 d DU . . H10P H 0.1440 0.6795 0.6778 0.101 Uiso 1 1 calc R . . H10Q H 0.1440 0.7396 0.6182 0.101 Uiso 1 1 calc R . . C108 C 0.0573(5) 0.6414(6) 0.6180(4) 0.096(3) Uani 1 1 d DU . . H10R H 0.0874 0.5938 0.5986 0.144 Uiso 1 1 calc R . . H10S H 0.0249 0.6730 0.5883 0.144 Uiso 1 1 calc R . . H10T H 0.0254 0.6124 0.6479 0.144 Uiso 1 1 calc R . . N2 N 0.2766(3) 0.2349(4) 0.5330(2) 0.0543(15) Uani 1 1 d D . . C201 C 0.2015(4) 0.2843(6) 0.5395(4) 0.080(2) Uani 1 1 d DU . . H20A H 0.2083 0.3498 0.5278 0.096 Uiso 1 1 calc R . . H20B H 0.1889 0.2839 0.5821 0.096 Uiso 1 1 calc R . . C202 C 0.1325(4) 0.2452(6) 0.5037(4) 0.082(2) Uani 1 1 d DU . . H20C H 0.0875 0.2826 0.5116 0.123 Uiso 1 1 calc R . . H20D H 0.1234 0.1809 0.5157 0.123 Uiso 1 1 calc R . . H20E H 0.1429 0.2472 0.4612 0.123 Uiso 1 1 calc R . . C203 C 0.3355(4) 0.2785(5) 0.5762(3) 0.071(2) Uani 1 1 d DU . . H20F H 0.3821 0.2402 0.5759 0.085 Uiso 1 1 calc R . . H20G H 0.3154 0.2756 0.6168 0.085 Uiso 1 1 calc R . . C204 C 0.3580(5) 0.3806(5) 0.5631(4) 0.082(2) Uani 1 1 d DU . . H20H H 0.3952 0.4017 0.5933 0.123 Uiso 1 1 calc R . . H20I H 0.3127 0.4200 0.5643 0.123 Uiso 1 1 calc R . . H20J H 0.3801 0.3844 0.5237 0.123 Uiso 1 1 calc R . . C205 C 0.2708(5) 0.1325(5) 0.5489(4) 0.088(3) Uani 1 1 d DU . . H20K H 0.3214 0.1040 0.5442 0.105 Uiso 1 1 calc R . . H20L H 0.2356 0.1027 0.5197 0.105 Uiso 1 1 calc R . . C206 C 0.2435(6) 0.1092(7) 0.6121(4) 0.111(3) Uani 1 1 d DU . . H20M H 0.2409 0.0418 0.6169 0.167 Uiso 1 1 calc R . . H20N H 0.1931 0.1360 0.6175 0.167 Uiso 1 1 calc R . . H20O H 0.2793 0.1351 0.6417 0.167 Uiso 1 1 calc R . . C207 C 0.3017(5) 0.2412(7) 0.4689(3) 0.085(3) Uani 1 1 d DU . . H20P H 0.3006 0.3071 0.4568 0.103 Uiso 1 1 calc R . . H20Q H 0.2640 0.2080 0.4434 0.103 Uiso 1 1 calc R . . C208 C 0.3816(5) 0.2016(7) 0.4561(4) 0.094(3) Uani 1 1 d DU . . H20R H 0.3925 0.2103 0.4140 0.141 Uiso 1 1 calc R . . H20S H 0.3829 0.1354 0.4657 0.141 Uiso 1 1 calc R . . H20T H 0.4199 0.2342 0.4806 0.141 Uiso 1 1 calc R . . O300 O 0.7086(6) 0.1698(7) 0.3788(5) 0.173(4) Uiso 1 1 d D . . C301 C 0.6803(9) 0.3029(10) 0.4391(7) 0.207(6) Uiso 1 1 d DU . . H30A H 0.7296 0.3257 0.4262 0.310 Uiso 1 1 calc R . . H30B H 0.6797 0.3016 0.4826 0.310 Uiso 1 1 calc R . . H30C H 0.6400 0.3441 0.4239 0.310 Uiso 1 1 calc R . . C302 C 0.6672(8) 0.2060(9) 0.4151(6) 0.155(5) Uiso 1 1 d DU . . C303 C 0.5926(7) 0.1582(9) 0.4300(6) 0.152(4) Uiso 1 1 d DU . . H30D H 0.5894 0.0984 0.4096 0.227 Uiso 1 1 calc R . . H30E H 0.5499 0.1974 0.4170 0.227 Uiso 1 1 calc R . . H30F H 0.5908 0.1484 0.4730 0.227 Uiso 1 1 calc R . . O400 O 0.2500 0.5961(11) 0.7500 0.209(7) Uiso 1 2 d SD . . C401 C 0.2292(8) 0.4604(9) 0.6943(5) 0.157(5) Uiso 1 1 d DU . . H40A H 0.2177 0.5050 0.6625 0.235 Uiso 1 1 calc R . . H40B H 0.1844 0.4218 0.7008 0.235 Uiso 1 1 calc R . . H40C H 0.2716 0.4210 0.6828 0.235 Uiso 1 1 calc R . . C402 C 0.2500 0.5110(12) 0.7500 0.132(5) Uiso 1 2 d SDU . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Ni1 0.0298(6) 0.0297(6) 0.0387(6) 0.000 0.0016(5) 0.000 Ni2 0.0452(5) 0.0332(4) 0.0379(4) -0.0029(4) 0.0059(4) 0.0014(4) Ni3 0.0385(4) 0.0346(4) 0.0409(4) 0.0013(4) -0.0033(3) -0.0013(4) Ni4 0.0350(4) 0.0399(5) 0.0426(5) -0.0044(4) 0.0016(4) -0.0010(4) Ni5 0.0329(4) 0.0390(5) 0.0378(4) 0.0041(4) 0.0029(3) 0.0003(3) Ni6 0.0327(4) 0.0453(5) 0.0465(5) -0.0058(4) 0.0062(4) 0.0008(4) Ni7 0.0341(4) 0.0443(5) 0.0518(5) -0.0031(4) 0.0021(4) -0.0005(4) Ni8 0.0444(5) 0.0324(4) 0.0446(5) -0.0027(4) 0.0033(4) -0.0001(4) Ni9 0.0342(4) 0.0486(5) 0.0496(5) 0.0125(4) 0.0010(4) 0.0054(4) Ni10 0.0474(5) 0.0319(5) 0.0545(5) -0.0031(4) 0.0023(4) -0.0008(4) Ni11 0.0513(5) 0.0386(5) 0.0436(5) 0.0012(4) 0.0134(4) -0.0059(4) Ni12 0.0426(5) 0.0448(5) 0.0524(5) -0.0138(4) 0.0078(4) 0.0027(4) Ni13 0.0448(5) 0.0380(5) 0.0582(6) -0.0025(4) -0.0090(4) -0.0074(4) C1 0.027(3) 0.033(3) 0.039(3) 0.001(3) -0.001(3) 0.002(3) C2 0.031(3) 0.030(3) 0.039(3) -0.004(3) 0.005(3) -0.003(3) C3 0.032(3) 0.032(3) 0.050(4) 0.003(3) 0.005(3) -0.005(3) C4 0.032(3) 0.025(3) 0.049(4) -0.003(3) 0.004(3) 0.000(3) C5 0.059(5) 0.057(5) 0.086(6) -0.009(4) -0.024(4) -0.009(4) C6 0.060(5) 0.046(4) 0.063(5) 0.001(4) -0.012(4) -0.009(4) C7 0.056(5) 0.051(4) 0.055(4) 0.007(4) -0.007(4) 0.005(4) C8 0.053(5) 0.079(6) 0.050(4) 0.020(4) 0.007(4) 0.009(4) C9 0.065(5) 0.044(4) 0.068(5) -0.005(4) 0.002(4) -0.005(4) C10 0.055(4) 0.037(4) 0.057(4) 0.000(3) 0.006(3) -0.003(3) C11 0.043(4) 0.059(5) 0.065(5) -0.011(4) 0.011(4) -0.001(3) C12 0.056(5) 0.075(6) 0.074(6) -0.002(4) 0.000(4) 0.000(4) C13 0.046(4) 0.057(5) 0.060(5) -0.007(4) 0.016(4) -0.001(3) C14 0.070(5) 0.046(5) 0.084(6) -0.005(4) 0.006(4) 0.000(4) C15 0.065(5) 0.080(6) 0.068(5) -0.029(5) -0.012(4) 0.002(4) C16 0.065(5) 0.053(5) 0.063(5) -0.027(4) 0.015(4) -0.006(4) C17 0.158(9) 0.061(5) 0.041(4) -0.005(4) 0.030(5) 0.007(6) C18 0.070(5) 0.066(5) 0.057(5) 0.001(4) 0.026(4) -0.008(4) C19 0.032(4) 0.072(5) 0.066(5) 0.007(4) 0.001(3) 0.004(4) C20 0.058(4) 0.041(4) 0.061(5) -0.002(4) 0.008(4) 0.014(4) O5 0.107(4) 0.111(4) 0.128(4) -0.008(3) -0.042(4) -0.004(3) O6 0.113(5) 0.086(4) 0.070(4) 0.000(3) -0.049(4) 0.004(4) O7 0.114(5) 0.100(5) 0.086(4) 0.052(4) -0.015(4) 0.017(4) O8 0.092(4) 0.126(4) 0.073(3) 0.030(3) -0.002(3) 0.003(3) O9 0.122(5) 0.056(4) 0.108(5) -0.043(4) -0.006(4) -0.003(4) O10 0.104(4) 0.044(3) 0.078(4) 0.006(3) 0.022(3) -0.003(3) O11 0.067(4) 0.119(5) 0.085(4) -0.010(4) 0.036(3) -0.001(4) O12 0.050(4) 0.135(6) 0.119(5) -0.005(4) -0.028(4) -0.007(4) O13 0.053(3) 0.103(5) 0.089(4) -0.023(3) 0.025(3) 0.000(3) O14 0.140(6) 0.054(4) 0.107(5) -0.031(4) 0.000(4) -0.015(4) O15 0.095(4) 0.135(4) 0.093(4) -0.042(3) -0.007(3) 0.002(3) O16 0.109(4) 0.099(4) 0.097(4) -0.043(3) 0.012(3) -0.003(3) O17 0.169(5) 0.098(4) 0.087(4) -0.001(3) 0.030(4) 0.009(4) O18 0.117(4) 0.114(4) 0.089(4) 0.007(3) 0.036(3) -0.013(3) O19 0.052(3) 0.116(4) 0.086(3) 0.021(3) 0.005(3) 0.011(3) O20 0.100(4) 0.046(3) 0.087(4) 0.004(3) -0.002(3) 0.017(3) N1 0.052(4) 0.061(4) 0.075(4) -0.006(3) 0.012(3) -0.003(3) C101 0.117(8) 0.098(7) 0.090(6) -0.023(5) 0.033(6) -0.033(6) C102 0.164(9) 0.119(8) 0.110(8) 0.005(6) 0.032(7) -0.037(7) C103 0.080(6) 0.072(5) 0.096(6) -0.012(5) 0.007(5) -0.015(5) C104 0.109(7) 0.077(6) 0.106(6) -0.021(5) -0.003(5) -0.008(5) C105 0.101(7) 0.099(7) 0.091(6) -0.010(5) 0.000(5) 0.038(6) C106 0.151(8) 0.106(7) 0.092(7) 0.004(6) 0.009(6) 0.040(6) C107 0.083(6) 0.065(5) 0.106(6) -0.021(5) 0.016(5) 0.008(4) C108 0.100(6) 0.076(6) 0.113(7) -0.032(5) 0.018(5) 0.003(5) N2 0.059(4) 0.060(4) 0.044(3) -0.005(3) -0.006(3) 0.008(3) C201 0.076(5) 0.095(6) 0.069(5) -0.006(5) -0.005(4) 0.020(5) C202 0.068(5) 0.098(6) 0.080(5) -0.006(5) -0.008(4) 0.010(5) C203 0.072(5) 0.078(5) 0.061(5) 0.001(4) -0.011(4) -0.002(4) C204 0.091(6) 0.078(5) 0.078(5) -0.003(5) -0.010(4) -0.006(5) C205 0.069(5) 0.083(6) 0.110(7) 0.013(5) -0.006(5) -0.004(5) C206 0.098(6) 0.105(7) 0.131(7) 0.031(6) -0.002(6) -0.025(6) C207 0.092(6) 0.114(7) 0.051(5) -0.012(4) -0.005(4) 0.018(5) C208 0.094(6) 0.125(7) 0.064(5) -0.014(5) 0.012(5) 0.013(6) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Ni1 C2 2.228(6) . ? Ni1 C2 2.228(6) 2_656 ? Ni1 C4 2.230(6) 2_656 ? Ni1 C4 2.230(6) . ? Ni1 C3 2.233(6) . ? Ni1 C3 2.233(6) 2_656 ? Ni1 C1 2.237(5) 2_656 ? Ni1 C1 2.237(5) . ? Ni1 Ni5 2.7153(10) 2_656 ? Ni1 Ni5 2.7153(10) . ? Ni1 Ni2 2.7251(8) 2_656 ? Ni1 Ni2 2.7251(8) . ? Ni2 C17 1.734(8) . ? Ni2 C2 1.905(6) . ? Ni2 C4 2.088(6) . ? Ni2 Ni12 2.5175(11) . ? Ni2 Ni11 2.5229(11) . ? Ni2 Ni5 2.7216(11) . ? Ni2 Ni4 2.7371(11) . ? Ni2 Ni6 2.8101(11) . ? Ni2 Ni7 2.9044(11) . ? Ni3 C6 1.765(8) . ? Ni3 C3 1.902(6) . ? Ni3 C1 2.091(6) . ? Ni3 Ni13 2.5253(11) . ? Ni3 Ni9 2.5387(11) . ? Ni3 Ni5 2.6944(11) . ? Ni3 Ni4 2.7570(11) . ? Ni3 Ni7 2.7705(11) 2_656 ? Ni3 Ni6 2.9412(11) 2_656 ? Ni4 C15 1.746(8) . ? Ni4 C4 1.914(6) . ? Ni4 C3 2.082(6) . ? Ni4 Ni13 2.5203(11) . ? Ni4 Ni12 2.5397(11) . ? Ni4 Ni10 2.7745(11) . ? Ni4 Ni10 2.8893(11) 2_656 ? Ni5 C8 1.744(7) . ? Ni5 C1 1.914(6) . ? Ni5 C2 2.088(6) . ? Ni5 Ni9 2.5220(11) . ? Ni5 Ni11 2.5244(11) . ? Ni5 Ni8 2.8126(11) 2_656 ? Ni5 Ni8 2.8973(11) . ? Ni6 C11 1.744(7) . ? Ni6 C19 1.895(7) 2_656 ? Ni6 C1 2.079(5) 2_656 ? Ni6 C2 2.113(6) . ? Ni6 Ni9 2.4411(11) 2_656 ? Ni6 Ni11 2.7258(12) . ? Ni6 Ni7 2.7831(12) . ? Ni6 Ni8 2.9405(11) . ? Ni6 Ni3 2.9412(11) 2_656 ? Ni7 C12 1.750(8) . ? Ni7 C13 1.897(7) . ? Ni7 C4 2.088(6) . ? Ni7 C3 2.112(6) 2_656 ? Ni7 Ni12 2.4368(12) . ? Ni7 Ni13 2.7306(12) 2_656 ? Ni7 Ni3 2.7705(11) 2_656 ? Ni7 Ni10 2.9758(12) . ? Ni8 C9 1.751(8) . ? Ni8 C10 1.893(7) . ? Ni8 C2 2.087(6) . ? Ni8 C1 2.116(6) 2_656 ? Ni8 Ni11 2.4397(11) . ? Ni8 Ni9 2.7357(11) 2_656 ? Ni8 Ni8 2.7722(16) 2_656 ? Ni8 Ni5 2.8126(11) 2_656 ? Ni9 C7 1.755(7) . ? Ni9 C19 1.874(7) . ? Ni9 C1 1.979(5) . ? Ni9 Ni6 2.4411(11) 2_656 ? Ni9 Ni8 2.7357(12) 2_656 ? Ni10 C14 1.762(8) . ? Ni10 C20 1.891(7) . ? Ni10 C3 2.102(6) 2_656 ? Ni10 C4 2.116(6) . ? Ni10 Ni13 2.4462(12) 2_656 ? Ni10 Ni12 2.7266(12) . ? Ni10 Ni10 2.8111(16) 2_656 ? Ni10 Ni4 2.8893(11) 2_656 ? Ni11 C18 1.726(7) . ? Ni11 C10 1.889(7) . ? Ni11 C2 1.982(6) . ? Ni11 C8 2.491(7) . ? Ni12 C16 1.715(7) . ? Ni12 C13 1.879(7) . ? Ni12 C4 1.977(6) . ? Ni12 C17 2.500(8) . ? Ni13 C5 1.712(8) . ? Ni13 C20 1.893(7) 2_656 ? Ni13 C3 1.969(6) . ? Ni13 Ni10 2.4462(12) 2_656 ? Ni13 C15 2.480(8) . ? Ni13 Ni7 2.7306(12) 2_656 ? C1 C2 1.366(8) 2_656 ? C1 Ni6 2.079(5) 2_656 ? C1 Ni8 2.116(6) 2_656 ? C2 C1 1.366(8) 2_656 ? C3 C4 1.379(8) 2_656 ? C3 Ni10 2.102(6) 2_656 ? C3 Ni7 2.112(6) 2_656 ? C4 C3 1.379(8) 2_656 ? C5 O5 1.157(8) . ? C6 O6 1.148(8) . ? C7 O7 1.132(7) . ? C8 O8 1.156(8) . ? C9 O9 1.141(8) . ? C10 O10 1.160(7) . ? C11 O11 1.146(8) . ? C12 O12 1.139(8) . ? C13 O13 1.168(7) . ? C14 O14 1.138(8) . ? C15 O15 1.160(8) . ? C16 O16 1.141(7) . ? C17 O17 1.153(9) . ? C18 O18 1.147(8) . ? C19 O19 1.165(7) . ? C19 Ni6 1.895(7) 2_656 ? C20 O20 1.167(8) . ? C20 Ni13 1.893(7) 2_656 ? N1 C101 1.487(7) . ? N1 C103 1.489(7) . ? N1 C105 1.493(7) . ? N1 C107 1.500(7) . ? C101 C102 1.516(8) . ? C101 H10A 0.9700 . ? C101 H10B 0.9700 . ? C102 H10C 0.9600 . ? C102 H10D 0.9600 . ? C102 H10E 0.9600 . ? C103 C104 1.520(8) . ? C103 H10F 0.9700 . ? C103 H10G 0.9700 . ? C104 H10H 0.9600 . ? C104 H10I 0.9600 . ? C104 H10J 0.9600 . ? C105 C106 1.519(8) . ? C105 H10K 0.9700 . ? C105 H10L 0.9700 . ? C106 H10M 0.9600 . ? C106 H10N 0.9600 . ? C106 H10O 0.9600 . ? C107 C108 1.516(8) . ? C107 H10P 0.9700 . ? C107 H10Q 0.9700 . ? C108 H10R 0.9600 . ? C108 H10S 0.9600 . ? C108 H10T 0.9600 . ? N2 C201 1.484(7) . ? N2 C207 1.492(7) . ? N2 C205 1.494(7) . ? N2 C203 1.506(7) . ? C201 C202 1.516(8) . ? C201 H20A 0.9700 . ? C201 H20B 0.9700 . ? C202 H20C 0.9600 . ? C202 H20D 0.9600 . ? C202 H20E 0.9600 . ? C203 C204 1.523(7) . ? C203 H20F 0.9700 . ? C203 H20G 0.9700 . ? C204 H20H 0.9600 . ? C204 H20I 0.9600 . ? C204 H20J 0.9600 . ? C205 C206 1.518(8) . ? C205 H20K 0.9700 . ? C205 H20L 0.9700 . ? C206 H20M 0.9600 . ? C206 H20N 0.9600 . ? C206 H20O 0.9600 . ? C207 C208 1.522(8) . ? C207 H20P 0.9700 . ? C207 H20Q 0.9700 . ? C208 H20R 0.9600 . ? C208 H20S 0.9600 . ? C208 H20T 0.9600 . ? O300 C302 1.201(9) . ? C301 C302 1.484(9) . ? C301 H30A 0.9600 . ? C301 H30B 0.9600 . ? C301 H30C 0.9600 . ? C302 C303 1.498(9) . ? C303 H30D 0.9600 . ? C303 H30E 0.9600 . ? C303 H30F 0.9600 . ? O400 C402 1.203(9) . ? C401 C402 1.460(8) . ? C401 H40A 0.9600 . ? C401 H40B 0.9600 . ? C401 H40C 0.9600 . ? C402 C401 1.460(8) 2_556 ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C2 Ni1 C2 95.2(3) . 2_656 ? C2 Ni1 C4 179.2(2) . 2_656 ? C2 Ni1 C4 84.4(2) 2_656 2_656 ? C2 Ni1 C4 84.4(2) . . ? C2 Ni1 C4 179.2(2) 2_656 . ? C4 Ni1 C4 96.0(3) 2_656 . ? C2 Ni1 C3 143.5(2) . . ? C2 Ni1 C3 96.1(2) 2_656 . ? C4 Ni1 C3 36.0(2) 2_656 . ? C4 Ni1 C3 84.6(2) . . ? C2 Ni1 C3 96.1(2) . 2_656 ? C2 Ni1 C3 143.5(2) 2_656 2_656 ? C4 Ni1 C3 84.6(2) 2_656 2_656 ? C4 Ni1 C3 36.0(2) . 2_656 ? C3 Ni1 C3 95.2(3) . 2_656 ? C2 Ni1 C1 35.6(2) . 2_656 ? C2 Ni1 C1 85.0(2) 2_656 2_656 ? C4 Ni1 C1 144.9(2) 2_656 2_656 ? C4 Ni1 C1 94.3(2) . 2_656 ? C3 Ni1 C1 178.8(2) . 2_656 ? C3 Ni1 C1 84.3(2) 2_656 2_656 ? C2 Ni1 C1 85.0(2) . . ? C2 Ni1 C1 35.62(19) 2_656 . ? C4 Ni1 C1 94.3(2) 2_656 . ? C4 Ni1 C1 144.9(2) . . ? C3 Ni1 C1 84.3(2) . . ? C3 Ni1 C1 178.8(2) 2_656 . ? C1 Ni1 C1 96.2(3) 2_656 . ? C2 Ni1 Ni5 73.32(15) . 2_656 ? C2 Ni1 Ni5 48.75(15) 2_656 2_656 ? C4 Ni1 Ni5 106.87(15) 2_656 2_656 ? C4 Ni1 Ni5 130.45(15) . 2_656 ? C3 Ni1 Ni5 137.09(15) . 2_656 ? C3 Ni1 Ni5 102.36(16) 2_656 2_656 ? C1 Ni1 Ni5 44.16(15) 2_656 2_656 ? C1 Ni1 Ni5 77.34(15) . 2_656 ? C2 Ni1 Ni5 48.75(15) . . ? C2 Ni1 Ni5 73.32(15) 2_656 . ? C4 Ni1 Ni5 130.45(15) 2_656 . ? C4 Ni1 Ni5 106.87(15) . . ? C3 Ni1 Ni5 102.36(16) . . ? C3 Ni1 Ni5 137.09(16) 2_656 . ? C1 Ni1 Ni5 77.34(15) 2_656 . ? C1 Ni1 Ni5 44.16(15) . . ? Ni5 Ni1 Ni5 90.91(5) 2_656 . ? C2 Ni1 Ni2 131.38(15) . 2_656 ? C2 Ni1 Ni2 43.81(14) 2_656 2_656 ? C4 Ni1 Ni2 48.58(15) 2_656 2_656 ? C4 Ni1 Ni2 136.18(16) . 2_656 ? C3 Ni1 Ni2 77.61(16) . 2_656 ? C3 Ni1 Ni2 105.97(16) 2_656 2_656 ? C1 Ni1 Ni2 103.61(15) 2_656 2_656 ? C1 Ni1 Ni2 72.83(15) . 2_656 ? Ni5 Ni1 Ni2 60.03(2) 2_656 2_656 ? Ni5 Ni1 Ni2 115.89(3) . 2_656 ? C2 Ni1 Ni2 43.81(14) . . ? C2 Ni1 Ni2 131.38(15) 2_656 . ? C4 Ni1 Ni2 136.18(16) 2_656 . ? C4 Ni1 Ni2 48.58(15) . . ? C3 Ni1 Ni2 105.97(16) . . ? C3 Ni1 Ni2 77.61(16) 2_656 . ? C1 Ni1 Ni2 72.83(15) 2_656 . ? C1 Ni1 Ni2 103.61(15) . . ? Ni5 Ni1 Ni2 115.89(3) 2_656 . ? Ni5 Ni1 Ni2 60.03(2) . . ? Ni2 Ni1 Ni2 174.86(5) 2_656 . ? C17 Ni2 C2 144.8(3) . . ? C17 Ni2 C4 117.8(3) . . ? C2 Ni2 C4 97.1(2) . . ? C17 Ni2 Ni12 69.2(3) . . ? C2 Ni2 Ni12 142.70(18) . . ? C4 Ni2 Ni12 49.77(16) . . ? C17 Ni2 Ni11 93.9(3) . . ? C2 Ni2 Ni11 50.87(17) . . ? C4 Ni2 Ni11 147.04(16) . . ? Ni12 Ni2 Ni11 153.52(4) . . ? C17 Ni2 Ni5 114.9(3) . . ? C2 Ni2 Ni5 49.91(17) . . ? C4 Ni2 Ni5 111.11(16) . . ? Ni12 Ni2 Ni5 147.84(4) . . ? Ni11 Ni2 Ni5 57.39(3) . . ? C17 Ni2 Ni1 154.3(3) . . ? C2 Ni2 Ni1 54.08(17) . . ? C4 Ni2 Ni1 53.23(16) . . ? Ni12 Ni2 Ni1 101.85(4) . . ? Ni11 Ni2 Ni1 101.61(4) . . ? Ni5 Ni2 Ni1 59.80(3) . . ? C17 Ni2 Ni4 95.9(3) . . ? C2 Ni2 Ni4 113.81(17) . . ? C4 Ni2 Ni4 44.24(16) . . ? Ni12 Ni2 Ni4 57.63(3) . . ? Ni11 Ni2 Ni4 147.47(4) . . ? Ni5 Ni2 Ni4 90.45(3) . . ? Ni1 Ni2 Ni4 60.40(3) . . ? C17 Ni2 Ni6 119.7(4) . . ? C2 Ni2 Ni6 48.73(17) . . ? C4 Ni2 Ni6 92.97(16) . . ? Ni12 Ni2 Ni6 108.63(4) . . ? Ni11 Ni2 Ni6 61.20(3) . . ? Ni5 Ni2 Ni6 96.77(3) . . ? Ni1 Ni2 Ni6 85.80(3) . . ? Ni4 Ni2 Ni6 135.45(4) . . ? C17 Ni2 Ni7 107.3(3) . . ? C2 Ni2 Ni7 92.95(18) . . ? C4 Ni2 Ni7 45.93(15) . . ? Ni12 Ni2 Ni7 52.83(3) . . ? Ni11 Ni2 Ni7 118.69(4) . . ? Ni5 Ni2 Ni7 137.69(4) . . ? Ni1 Ni2 Ni7 83.08(3) . . ? Ni4 Ni2 Ni7 87.63(3) . . ? Ni6 Ni2 Ni7 58.26(3) . . ? C6 Ni3 C3 143.8(3) . . ? C6 Ni3 C1 118.9(3) . . ? C3 Ni3 C1 97.3(2) . . ? C6 Ni3 Ni13 93.7(2) . . ? C3 Ni3 Ni13 50.44(18) . . ? C1 Ni3 Ni13 146.56(16) . . ? C6 Ni3 Ni9 71.4(2) . . ? C3 Ni3 Ni9 143.17(19) . . ? C1 Ni3 Ni9 49.46(15) . . ? Ni13 Ni3 Ni9 154.11(4) . . ? C6 Ni3 Ni5 94.1(2) . . ? C3 Ni3 Ni5 113.41(17) . . ? C1 Ni3 Ni5 44.98(15) . . ? Ni13 Ni3 Ni5 147.04(4) . . ? Ni9 Ni3 Ni5 57.53(3) . . ? C6 Ni3 Ni1 150.9(2) . . ? C3 Ni3 Ni1 54.14(17) . . ? C1 Ni3 Ni1 53.34(15) . . ? Ni13 Ni3 Ni1 101.50(4) . . ? Ni9 Ni3 Ni1 101.42(4) . . ? Ni5 Ni3 Ni1 60.08(3) . . ? C6 Ni3 Ni4 111.1(2) . . ? C3 Ni3 Ni4 48.99(18) . . ? C1 Ni3 Ni4 111.80(15) . . ? Ni13 Ni3 Ni4 56.79(3) . . ? Ni9 Ni3 Ni4 147.90(4) . . ? Ni5 Ni3 Ni4 90.60(3) . . ? Ni1 Ni3 Ni4 60.11(3) . . ? C6 Ni3 Ni7 123.6(2) . 2_656 ? C3 Ni3 Ni7 49.59(17) . 2_656 ? C1 Ni3 Ni7 91.68(16) . 2_656 ? Ni13 Ni3 Ni7 61.87(3) . 2_656 ? Ni9 Ni3 Ni7 108.26(4) . 2_656 ? Ni5 Ni3 Ni7 134.80(4) . 2_656 ? Ni1 Ni3 Ni7 85.56(3) . 2_656 ? Ni4 Ni3 Ni7 96.84(3) . 2_656 ? C6 Ni3 Ni6 110.8(2) . 2_656 ? C3 Ni3 Ni6 94.22(19) . 2_656 ? C1 Ni3 Ni6 44.97(15) . 2_656 ? Ni13 Ni3 Ni6 119.30(4) . 2_656 ? Ni9 Ni3 Ni6 52.28(3) . 2_656 ? Ni5 Ni3 Ni6 87.34(3) . 2_656 ? Ni1 Ni3 Ni6 83.21(3) . 2_656 ? Ni4 Ni3 Ni6 138.14(4) . 2_656 ? Ni7 Ni3 Ni6 58.23(3) 2_656 2_656 ? C15 Ni4 C4 144.9(3) . . ? C15 Ni4 C3 117.2(3) . . ? C4 Ni4 C3 97.4(2) . . ? C15 Ni4 Ni13 68.3(3) . . ? C4 Ni4 Ni13 143.84(18) . . ? C3 Ni4 Ni13 49.54(16) . . ? C15 Ni4 Ni12 94.6(3) . . ? C4 Ni4 Ni12 50.33(17) . . ? C3 Ni4 Ni12 147.07(17) . . ? Ni13 Ni4 Ni12 156.19(4) . . ? C15 Ni4 Ni2 116.8(3) . . ? C4 Ni4 Ni2 49.56(18) . . ? C3 Ni4 Ni2 110.16(16) . . ? Ni13 Ni4 Ni2 145.23(4) . . ? Ni12 Ni4 Ni2 56.84(3) . . ? C15 Ni4 Ni1 156.1(3) . . ? C4 Ni4 Ni1 53.61(17) . . ? C3 Ni4 Ni1 52.91(16) . . ? Ni13 Ni4 Ni1 101.12(3) . . ? Ni12 Ni4 Ni1 100.66(3) . . ? Ni2 Ni4 Ni1 59.58(2) . . ? C15 Ni4 Ni3 98.0(3) . . ? C4 Ni4 Ni3 112.15(17) . . ? C3 Ni4 Ni3 43.58(17) . . ? Ni13 Ni4 Ni3 56.97(3) . . ? Ni12 Ni4 Ni3 145.23(4) . . ? Ni2 Ni4 Ni3 88.66(3) . . ? Ni1 Ni4 Ni3 59.44(2) . . ? C15 Ni4 Ni10 117.7(3) . . ? C4 Ni4 Ni10 49.61(17) . . ? C3 Ni4 Ni10 94.00(17) . . ? Ni13 Ni4 Ni10 110.66(4) . . ? Ni12 Ni4 Ni10 61.55(3) . . ? Ni2 Ni4 Ni10 97.30(3) . . ? Ni1 Ni4 Ni10 85.90(3) . . ? Ni3 Ni4 Ni10 135.45(4) . . ? C15 Ni4 Ni10 104.3(3) . 2_656 ? C4 Ni4 Ni10 94.84(18) . 2_656 ? C3 Ni4 Ni10 46.60(16) . 2_656 ? Ni13 Ni4 Ni10 53.24(3) . 2_656 ? Ni12 Ni4 Ni10 120.32(4) . 2_656 ? Ni2 Ni4 Ni10 138.87(4) . 2_656 ? Ni1 Ni4 Ni10 83.70(3) . 2_656 ? Ni3 Ni4 Ni10 87.65(3) . 2_656 ? Ni10 Ni4 Ni10 59.47(3) . 2_656 ? C8 Ni5 C1 145.4(3) . . ? C8 Ni5 C2 116.8(3) . . ? C1 Ni5 C2 97.7(2) . . ? C8 Ni5 Ni9 94.7(2) . . ? C1 Ni5 Ni9 50.75(16) . . ? C2 Ni5 Ni9 147.26(16) . . ? C8 Ni5 Ni11 68.6(2) . . ? C1 Ni5 Ni11 143.65(17) . . ? C2 Ni5 Ni11 49.80(16) . . ? Ni9 Ni5 Ni11 153.04(4) . . ? C8 Ni5 Ni3 112.7(3) . . ? C1 Ni5 Ni3 50.56(17) . . ? C2 Ni5 Ni3 111.87(16) . . ? Ni9 Ni5 Ni3 58.13(3) . . ? Ni11 Ni5 Ni3 147.18(4) . . ? C8 Ni5 Ni1 151.7(3) . . ? C1 Ni5 Ni1 54.54(16) . . ? C2 Ni5 Ni1 53.35(16) . . ? Ni9 Ni5 Ni1 102.24(3) . . ? Ni11 Ni5 Ni1 101.84(3) . . ? Ni3 Ni5 Ni1 60.59(3) . . ? C8 Ni5 Ni2 93.9(2) . . ? C1 Ni5 Ni2 113.98(17) . . ? C2 Ni5 Ni2 44.26(15) . . ? Ni9 Ni5 Ni2 148.13(4) . . ? Ni11 Ni5 Ni2 57.34(3) . . ? Ni3 Ni5 Ni2 90.28(3) . . ? Ni1 Ni5 Ni2 60.16(2) . . ? C8 Ni5 Ni8 122.8(3) . 2_656 ? C1 Ni5 Ni8 48.76(17) . 2_656 ? C2 Ni5 Ni8 92.24(16) . 2_656 ? Ni9 Ni5 Ni8 61.42(3) . 2_656 ? Ni11 Ni5 Ni8 108.90(4) . 2_656 ? Ni3 Ni5 Ni8 97.64(3) . 2_656 ? Ni1 Ni5 Ni8 85.34(3) . 2_656 ? Ni2 Ni5 Ni8 134.64(4) . 2_656 ? C8 Ni5 Ni8 107.9(3) . . ? C1 Ni5 Ni8 93.95(17) . . ? C2 Ni5 Ni8 46.03(15) . . ? Ni9 Ni5 Ni8 118.40(4) . . ? Ni11 Ni5 Ni8 52.94(3) . . ? Ni3 Ni5 Ni8 139.37(4) . . ? Ni1 Ni5 Ni8 83.71(3) . . ? Ni2 Ni5 Ni8 87.67(3) . . ? Ni8 Ni5 Ni8 58.07(3) 2_656 . ? C11 Ni6 C19 98.9(3) . 2_656 ? C11 Ni6 C1 160.1(3) . 2_656 ? C19 Ni6 C1 100.4(3) 2_656 2_656 ? C11 Ni6 C2 122.3(3) . . ? C19 Ni6 C2 133.7(3) 2_656 . ? C1 Ni6 C2 38.0(2) 2_656 . ? C11 Ni6 Ni9 147.6(2) . 2_656 ? C19 Ni6 Ni9 49.2(2) 2_656 2_656 ? C1 Ni6 Ni9 51.16(15) 2_656 2_656 ? C2 Ni6 Ni9 86.18(16) . 2_656 ? C11 Ni6 Ni11 84.1(2) . . ? C19 Ni6 Ni11 131.0(2) 2_656 . ? C1 Ni6 Ni11 79.63(16) 2_656 . ? C2 Ni6 Ni11 46.24(16) . . ? Ni9 Ni6 Ni11 111.09(4) 2_656 . ? C11 Ni6 Ni7 85.3(2) . . ? C19 Ni6 Ni7 113.0(2) 2_656 . ? C1 Ni6 Ni7 91.58(16) 2_656 . ? C2 Ni6 Ni7 92.06(15) . . ? Ni9 Ni6 Ni7 110.79(4) 2_656 . ? Ni11 Ni6 Ni7 116.04(4) . . ? C11 Ni6 Ni2 88.0(2) . . ? C19 Ni6 Ni2 171.5(2) 2_656 . ? C1 Ni6 Ni2 73.15(15) 2_656 . ? C2 Ni6 Ni2 42.66(15) . . ? Ni9 Ni6 Ni2 124.21(4) 2_656 . ? Ni11 Ni6 Ni2 54.20(3) . . ? Ni7 Ni6 Ni2 62.57(3) . . ? C11 Ni6 Ni8 127.6(2) . . ? C19 Ni6 Ni8 94.2(2) 2_656 . ? C1 Ni6 Ni8 46.01(16) 2_656 . ? C2 Ni6 Ni8 45.19(15) . . ? Ni9 Ni6 Ni8 60.26(3) 2_656 . ? Ni11 Ni6 Ni8 50.83(3) . . ? Ni7 Ni6 Ni8 134.19(4) . . ? Ni2 Ni6 Ni8 85.20(3) . . ? C11 Ni6 Ni3 141.3(2) . 2_656 ? C19 Ni6 Ni3 86.7(2) 2_656 2_656 ? C1 Ni6 Ni3 45.30(16) 2_656 2_656 ? C2 Ni6 Ni3 74.30(16) . 2_656 ? Ni9 Ni6 Ni3 55.35(3) 2_656 2_656 ? Ni11 Ni6 Ni3 120.54(3) . 2_656 ? Ni7 Ni6 Ni3 57.81(3) . 2_656 ? Ni2 Ni6 Ni3 84.87(3) . 2_656 ? Ni8 Ni6 Ni3 89.63(3) . 2_656 ? C12 Ni7 C13 99.3(3) . . ? C12 Ni7 C4 159.9(3) . . ? C13 Ni7 C4 100.5(3) . . ? C12 Ni7 C3 122.1(3) . 2_656 ? C13 Ni7 C3 134.2(3) . 2_656 ? C4 Ni7 C3 38.3(2) . 2_656 ? C12 Ni7 Ni12 148.3(3) . . ? C13 Ni7 Ni12 49.5(2) . . ? C4 Ni7 Ni12 51.10(16) . . ? C3 Ni7 Ni12 86.27(17) 2_656 . ? C12 Ni7 Ni13 85.5(3) . 2_656 ? C13 Ni7 Ni13 131.1(2) . 2_656 ? C4 Ni7 Ni13 79.22(17) . 2_656 ? C3 Ni7 Ni13 45.80(16) 2_656 2_656 ? Ni12 Ni7 Ni13 110.03(4) . 2_656 ? C12 Ni7 Ni3 86.5(3) . 2_656 ? C13 Ni7 Ni3 171.9(2) . 2_656 ? C4 Ni7 Ni3 74.10(16) . 2_656 ? C3 Ni7 Ni3 43.30(17) 2_656 2_656 ? Ni12 Ni7 Ni3 125.13(4) . 2_656 ? Ni13 Ni7 Ni3 54.65(3) 2_656 2_656 ? C12 Ni7 Ni6 81.9(3) . . ? C13 Ni7 Ni6 111.0(2) . . ? C4 Ni7 Ni6 93.74(16) . . ? C3 Ni7 Ni6 94.33(16) 2_656 . ? Ni12 Ni7 Ni6 111.95(4) . . ? Ni13 Ni7 Ni6 117.83(4) 2_656 . ? Ni3 Ni7 Ni6 63.96(3) 2_656 . ? C12 Ni7 Ni2 139.5(3) . . ? C13 Ni7 Ni2 85.6(2) . . ? C4 Ni7 Ni2 45.93(16) . . ? C3 Ni7 Ni2 75.38(17) 2_656 . ? Ni12 Ni7 Ni2 55.41(3) . . ? Ni13 Ni7 Ni2 121.15(4) 2_656 . ? Ni3 Ni7 Ni2 86.28(3) 2_656 . ? Ni6 Ni7 Ni2 59.17(3) . . ? C12 Ni7 Ni10 129.7(3) . . ? C13 Ni7 Ni10 94.8(2) . . ? C4 Ni7 Ni10 45.33(16) . . ? C3 Ni7 Ni10 44.93(16) 2_656 . ? Ni12 Ni7 Ni10 59.51(3) . . ? Ni13 Ni7 Ni10 50.54(3) 2_656 . ? Ni3 Ni7 Ni10 85.70(3) 2_656 . ? Ni6 Ni7 Ni10 135.95(4) . . ? Ni2 Ni7 Ni10 89.43(3) . . ? C9 Ni8 C10 99.8(3) . . ? C9 Ni8 C2 159.0(3) . . ? C10 Ni8 C2 100.9(3) . . ? C9 Ni8 C1 121.4(3) . 2_656 ? C10 Ni8 C1 134.4(3) . 2_656 ? C2 Ni8 C1 37.9(2) . 2_656 ? C9 Ni8 Ni11 148.9(2) . . ? C10 Ni8 Ni11 49.8(2) . . ? C2 Ni8 Ni11 51.21(16) . . ? C1 Ni8 Ni11 86.01(16) 2_656 . ? C9 Ni8 Ni9 83.9(2) . 2_656 ? C10 Ni8 Ni9 132.1(2) . 2_656 ? C2 Ni8 Ni9 79.39(16) . 2_656 ? C1 Ni8 Ni9 45.98(15) 2_656 2_656 ? Ni11 Ni8 Ni9 110.81(4) . 2_656 ? C9 Ni8 Ni8 82.3(2) . 2_656 ? C10 Ni8 Ni8 112.2(2) . 2_656 ? C2 Ni8 Ni8 93.42(15) . 2_656 ? C1 Ni8 Ni8 93.21(15) 2_656 2_656 ? Ni11 Ni8 Ni8 112.82(5) . 2_656 ? Ni9 Ni8 Ni8 115.52(4) 2_656 2_656 ? C9 Ni8 Ni5 86.7(2) . 2_656 ? C10 Ni8 Ni5 171.2(2) . 2_656 ? C2 Ni8 Ni5 73.16(16) . 2_656 ? C1 Ni8 Ni5 42.85(15) 2_656 2_656 ? Ni11 Ni8 Ni5 124.28(4) . 2_656 ? Ni9 Ni8 Ni5 54.05(3) 2_656 2_656 ? Ni8 Ni8 Ni5 62.50(3) 2_656 2_656 ? C9 Ni8 Ni5 140.1(2) . . ? C10 Ni8 Ni5 85.9(2) . . ? C2 Ni8 Ni5 46.06(16) . . ? C1 Ni8 Ni5 75.09(15) 2_656 . ? Ni11 Ni8 Ni5 55.66(3) . . ? Ni9 Ni8 Ni5 121.06(4) 2_656 . ? Ni8 Ni8 Ni5 59.44(3) 2_656 . ? Ni5 Ni8 Ni5 85.34(3) 2_656 . ? C9 Ni8 Ni6 128.0(2) . . ? C10 Ni8 Ni6 95.3(2) . . ? C2 Ni8 Ni6 45.92(15) . . ? C1 Ni8 Ni6 44.98(15) 2_656 . ? Ni11 Ni8 Ni6 60.03(3) . . ? Ni9 Ni8 Ni6 50.79(3) 2_656 . ? Ni8 Ni8 Ni6 135.59(2) 2_656 . ? Ni5 Ni8 Ni6 85.20(3) 2_656 . ? Ni5 Ni8 Ni6 90.22(3) . . ? C7 Ni9 C19 101.7(3) . . ? C7 Ni9 C1 151.6(3) . . ? C19 Ni9 C1 104.9(3) . . ? C7 Ni9 Ni6 149.6(2) . 2_656 ? C19 Ni9 Ni6 50.0(2) . 2_656 ? C1 Ni9 Ni6 54.91(16) . 2_656 ? C7 Ni9 Ni5 104.9(2) . . ? C19 Ni9 Ni5 153.3(2) . . ? C1 Ni9 Ni5 48.49(16) . . ? Ni6 Ni9 Ni5 103.41(4) 2_656 . ? C7 Ni9 Ni3 130.9(2) . . ? C19 Ni9 Ni3 99.9(2) . . ? C1 Ni9 Ni3 53.40(17) . . ? Ni6 Ni9 Ni3 72.37(3) 2_656 . ? Ni5 Ni9 Ni3 64.34(3) . . ? C7 Ni9 Ni8 114.4(2) . 2_656 ? C19 Ni9 Ni8 101.6(2) . 2_656 ? C1 Ni9 Ni8 50.25(17) . 2_656 ? Ni6 Ni9 Ni8 68.95(3) 2_656 2_656 ? Ni5 Ni9 Ni8 64.53(3) . 2_656 ? Ni3 Ni9 Ni8 103.56(4) . 2_656 ? C14 Ni10 C20 99.8(3) . . ? C14 Ni10 C3 159.5(3) . 2_656 ? C20 Ni10 C3 100.4(3) . 2_656 ? C14 Ni10 C4 121.9(3) . . ? C20 Ni10 C4 133.0(3) . . ? C3 Ni10 C4 38.2(2) 2_656 . ? C14 Ni10 Ni13 149.4(3) . 2_656 ? C20 Ni10 Ni13 49.8(2) . 2_656 ? C3 Ni10 Ni13 50.61(17) 2_656 2_656 ? C4 Ni10 Ni13 85.67(16) . 2_656 ? C14 Ni10 Ni12 85.2(3) . . ? C20 Ni10 Ni12 128.2(2) . . ? C3 Ni10 Ni12 79.33(17) 2_656 . ? C4 Ni10 Ni12 46.07(16) . . ? Ni13 Ni10 Ni12 109.87(4) 2_656 . ? C14 Ni10 Ni4 86.0(3) . . ? C20 Ni10 Ni4 173.4(2) . . ? C3 Ni10 Ni4 74.11(17) 2_656 . ? C4 Ni10 Ni4 43.53(16) . . ? Ni13 Ni10 Ni4 124.63(4) 2_656 . ? Ni12 Ni10 Ni4 54.98(3) . . ? C14 Ni10 Ni10 82.3(3) . 2_656 ? C20 Ni10 Ni10 115.1(2) . 2_656 ? C3 Ni10 Ni10 92.53(15) 2_656 2_656 ? C4 Ni10 Ni10 92.71(15) . 2_656 ? Ni13 Ni10 Ni10 111.75(5) 2_656 2_656 ? Ni12 Ni10 Ni10 116.63(4) . 2_656 ? Ni4 Ni10 Ni10 62.30(3) . 2_656 ? C14 Ni10 Ni4 138.8(3) . 2_656 ? C20 Ni10 Ni4 87.9(2) . 2_656 ? C3 Ni10 Ni4 46.05(16) 2_656 2_656 ? C4 Ni10 Ni4 75.08(16) . 2_656 ? Ni13 Ni10 Ni4 55.63(3) 2_656 2_656 ? Ni12 Ni10 Ni4 121.14(4) . 2_656 ? Ni4 Ni10 Ni4 85.64(4) . 2_656 ? Ni10 Ni10 Ni4 58.23(3) 2_656 2_656 ? C14 Ni10 Ni7 129.7(3) . . ? C20 Ni10 Ni7 93.1(2) . . ? C3 Ni10 Ni7 45.22(16) 2_656 . ? C4 Ni10 Ni7 44.55(15) . . ? Ni13 Ni10 Ni7 59.53(3) 2_656 . ? Ni12 Ni10 Ni7 50.37(3) . . ? Ni4 Ni10 Ni7 85.55(3) . . ? Ni10 Ni10 Ni7 134.20(2) 2_656 . ? Ni4 Ni10 Ni7 89.64(3) 2_656 . ? C18 Ni11 C10 101.2(3) . . ? C18 Ni11 C2 153.0(3) . . ? C10 Ni11 C2 104.9(3) . . ? C18 Ni11 Ni8 149.7(3) . . ? C10 Ni11 Ni8 49.9(2) . . ? C2 Ni11 Ni8 55.15(16) . . ? C18 Ni11 C8 90.1(3) . . ? C10 Ni11 C8 97.0(3) . . ? C2 Ni11 C8 93.2(2) . . ? Ni8 Ni11 C8 101.34(17) . . ? C18 Ni11 Ni2 105.9(3) . . ? C10 Ni11 Ni2 152.9(2) . . ? C2 Ni11 Ni2 48.20(16) . . ? Ni8 Ni11 Ni2 103.35(4) . . ? C8 Ni11 Ni2 83.27(18) . . ? C18 Ni11 Ni5 129.2(3) . . ? C10 Ni11 Ni5 97.5(2) . . ? C2 Ni11 Ni5 53.57(16) . . ? Ni8 Ni11 Ni5 71.39(3) . . ? C8 Ni11 Ni5 40.70(16) . . ? Ni2 Ni11 Ni5 65.26(3) . . ? C18 Ni11 Ni6 117.1(3) . . ? C10 Ni11 Ni6 102.6(2) . . ? C2 Ni11 Ni6 50.35(16) . . ? Ni8 Ni11 Ni6 69.14(3) . . ? C8 Ni11 Ni6 141.90(17) . . ? Ni2 Ni11 Ni6 64.60(3) . . ? Ni5 Ni11 Ni6 103.89(4) . . ? C16 Ni12 C13 102.4(3) . . ? C16 Ni12 C4 150.4(3) . . ? C13 Ni12 C4 105.3(3) . . ? C16 Ni12 Ni7 149.9(3) . . ? C13 Ni12 Ni7 50.1(2) . . ? C4 Ni12 Ni7 55.28(17) . . ? C16 Ni12 C17 93.8(3) . . ? C13 Ni12 C17 96.2(3) . . ? C4 Ni12 C17 93.4(2) . . ? Ni7 Ni12 C17 100.7(2) . . ? C16 Ni12 Ni2 131.7(3) . . ? C13 Ni12 Ni2 98.1(2) . . ? C4 Ni12 Ni2 53.74(17) . . ? Ni7 Ni12 Ni2 71.76(3) . . ? C17 Ni12 Ni2 40.43(17) . . ? C16 Ni12 Ni4 104.1(2) . . ? C13 Ni12 Ni4 153.4(2) . . ? C4 Ni12 Ni4 48.18(17) . . ? Ni7 Ni12 Ni4 103.46(4) . . ? C17 Ni12 Ni4 84.5(2) . . ? Ni2 Ni12 Ni4 65.53(3) . . ? C16 Ni12 Ni10 112.6(3) . . ? C13 Ni12 Ni10 103.7(2) . . ? C4 Ni12 Ni10 50.46(17) . . ? Ni7 Ni12 Ni10 70.13(3) . . ? C17 Ni12 Ni10 142.0(2) . . ? Ni2 Ni12 Ni10 104.10(4) . . ? Ni4 Ni12 Ni10 63.47(3) . . ? C5 Ni13 C20 102.1(3) . 2_656 ? C5 Ni13 C3 150.4(3) . . ? C20 Ni13 C3 105.3(3) 2_656 . ? C5 Ni13 Ni10 150.1(3) . 2_656 ? C20 Ni13 Ni10 49.7(2) 2_656 2_656 ? C3 Ni13 Ni10 55.59(18) . 2_656 ? C5 Ni13 C15 94.0(3) . . ? C20 Ni13 C15 95.8(3) 2_656 . ? C3 Ni13 C15 94.0(2) . . ? Ni10 Ni13 C15 98.34(19) 2_656 . ? C5 Ni13 Ni4 131.6(3) . . ? C20 Ni13 Ni4 99.6(2) 2_656 . ? C3 Ni13 Ni4 53.58(17) . . ? Ni10 Ni13 Ni4 71.13(3) 2_656 . ? C15 Ni13 Ni4 40.87(17) . . ? C5 Ni13 Ni3 103.9(3) . . ? C20 Ni13 Ni3 153.4(2) 2_656 . ? C3 Ni13 Ni3 48.15(18) . . ? Ni10 Ni13 Ni3 103.74(4) 2_656 . ? C15 Ni13 Ni3 87.5(2) . . ? Ni4 Ni13 Ni3 66.24(3) . . ? C5 Ni13 Ni7 113.5(3) . 2_656 ? C20 Ni13 Ni7 101.1(2) 2_656 2_656 ? C3 Ni13 Ni7 50.28(17) . 2_656 ? Ni10 Ni13 Ni7 69.93(3) 2_656 2_656 ? C15 Ni13 Ni7 143.39(18) . 2_656 ? Ni4 Ni13 Ni7 103.82(4) . 2_656 ? Ni3 Ni13 Ni7 63.48(3) . 2_656 ? C2 C1 Ni5 129.7(4) 2_656 . ? C2 C1 Ni9 137.0(4) 2_656 . ? Ni5 C1 Ni9 80.8(2) . . ? C2 C1 Ni6 72.3(3) 2_656 2_656 ? Ni5 C1 Ni6 154.7(3) . 2_656 ? Ni9 C1 Ni6 73.92(18) . 2_656 ? C2 C1 Ni3 128.0(4) 2_656 . ? Ni5 C1 Ni3 84.5(2) . . ? Ni9 C1 Ni3 77.1(2) . . ? Ni6 C1 Ni3 89.7(2) 2_656 . ? C2 C1 Ni8 69.9(3) 2_656 2_656 ? Ni5 C1 Ni8 88.4(2) . 2_656 ? Ni9 C1 Ni8 83.8(2) . 2_656 ? Ni6 C1 Ni8 89.0(2) 2_656 2_656 ? Ni3 C1 Ni8 160.4(3) . 2_656 ? C2 C1 Ni1 71.8(3) 2_656 . ? Ni5 C1 Ni1 81.3(2) . . ? Ni9 C1 Ni1 150.6(3) . . ? Ni6 C1 Ni1 121.6(3) 2_656 . ? Ni3 C1 Ni1 78.10(19) . . ? Ni8 C1 Ni1 118.8(2) 2_656 . ? C1 C2 Ni2 129.9(4) 2_656 . ? C1 C2 Ni11 136.3(4) 2_656 . ? Ni2 C2 Ni11 80.9(2) . . ? C1 C2 Ni8 72.2(3) 2_656 . ? Ni2 C2 Ni8 154.6(3) . . ? Ni11 C2 Ni8 73.64(19) . . ? C1 C2 Ni5 127.8(4) 2_656 . ? Ni2 C2 Ni5 85.8(2) . . ? Ni11 C2 Ni5 76.6(2) . . ? Ni8 C2 Ni5 87.9(2) . . ? C1 C2 Ni6 69.6(3) 2_656 . ? Ni2 C2 Ni6 88.6(2) . . ? Ni11 C2 Ni6 83.4(2) . . ? Ni8 C2 Ni6 88.9(2) . . ? Ni5 C2 Ni6 159.9(3) . . ? C1 C2 Ni1 72.6(3) 2_656 . ? Ni2 C2 Ni1 82.1(2) . . ? Ni11 C2 Ni1 150.2(3) . . ? Ni8 C2 Ni1 120.5(3) . . ? Ni5 C2 Ni1 77.90(18) . . ? Ni6 C2 Ni1 120.5(3) . . ? C4 C3 Ni3 129.6(5) 2_656 . ? C4 C3 Ni13 136.0(4) 2_656 . ? Ni3 C3 Ni13 81.4(2) . . ? C4 C3 Ni4 126.8(4) 2_656 . ? Ni3 C3 Ni4 87.4(2) . . ? Ni13 C3 Ni4 76.9(2) . . ? C4 C3 Ni10 71.5(3) 2_656 2_656 ? Ni3 C3 Ni10 155.2(3) . 2_656 ? Ni13 C3 Ni10 73.8(2) . 2_656 ? Ni4 C3 Ni10 87.3(2) . 2_656 ? C4 C3 Ni7 69.9(3) 2_656 2_656 ? Ni3 C3 Ni7 87.1(2) . 2_656 ? Ni13 C3 Ni7 83.9(2) . 2_656 ? Ni4 C3 Ni7 160.6(3) . 2_656 ? Ni10 C3 Ni7 89.8(2) 2_656 2_656 ? C4 C3 Ni1 71.9(3) 2_656 . ? Ni3 C3 Ni1 82.2(2) . . ? Ni13 C3 Ni1 151.3(3) . . ? Ni4 C3 Ni1 79.02(19) . . ? Ni10 C3 Ni1 120.4(3) 2_656 . ? Ni7 C3 Ni1 118.6(3) 2_656 . ? C3 C4 Ni4 129.5(4) 2_656 . ? C3 C4 Ni12 136.0(4) 2_656 . ? Ni4 C4 Ni12 81.5(2) . . ? C3 C4 Ni7 71.8(3) 2_656 . ? Ni4 C4 Ni7 155.1(3) . . ? Ni12 C4 Ni7 73.62(19) . . ? C3 C4 Ni2 127.9(4) 2_656 . ? Ni4 C4 Ni2 86.2(2) . . ? Ni12 C4 Ni2 76.5(2) . . ? Ni7 C4 Ni2 88.1(2) . . ? C3 C4 Ni10 70.3(3) 2_656 . ? Ni4 C4 Ni10 86.9(2) . . ? Ni12 C4 Ni10 83.5(2) . . ? Ni7 C4 Ni10 90.1(2) . . ? Ni2 C4 Ni10 159.5(3) . . ? C3 C4 Ni1 72.1(3) 2_656 . ? Ni4 C4 Ni1 82.7(2) . . ? Ni12 C4 Ni1 150.9(3) . . ? Ni7 C4 Ni1 119.8(3) . . ? Ni2 C4 Ni1 78.19(19) . . ? Ni10 C4 Ni1 119.9(3) . . ? O5 C5 Ni13 179.2(9) . . ? O6 C6 Ni3 171.8(7) . . ? O7 C7 Ni9 177.5(7) . . ? O8 C8 Ni5 169.4(7) . . ? O8 C8 Ni11 120.0(6) . . ? Ni5 C8 Ni11 70.7(2) . . ? O9 C9 Ni8 177.2(7) . . ? O10 C10 Ni11 138.8(6) . . ? O10 C10 Ni8 140.9(6) . . ? Ni11 C10 Ni8 80.3(3) . . ? O11 C11 Ni6 178.1(7) . . ? O12 C12 Ni7 175.4(8) . . ? O13 C13 Ni12 140.0(6) . . ? O13 C13 Ni7 139.6(6) . . ? Ni12 C13 Ni7 80.4(3) . . ? O14 C14 Ni10 177.5(8) . . ? O15 C15 Ni4 168.0(8) . . ? O15 C15 Ni13 121.0(6) . . ? Ni4 C15 Ni13 70.8(3) . . ? O16 C16 Ni12 179.2(8) . . ? O17 C17 Ni2 167.9(8) . . ? O17 C17 Ni12 121.7(7) . . ? Ni2 C17 Ni12 70.3(3) . . ? O18 C18 Ni11 177.0(8) . . ? O19 C19 Ni9 139.7(6) . . ? O19 C19 Ni6 139.5(6) . 2_656 ? Ni9 C19 Ni6 80.7(3) . 2_656 ? O20 C20 Ni10 141.3(6) . . ? O20 C20 Ni13 138.2(6) . 2_656 ? Ni10 C20 Ni13 80.6(3) . 2_656 ? C101 N1 C103 111.6(6) . . ? C101 N1 C105 104.6(6) . . ? C103 N1 C105 111.4(7) . . ? C101 N1 C107 111.7(6) . . ? C103 N1 C107 106.8(5) . . ? C105 N1 C107 111.0(6) . . ? N1 C101 C102 115.4(8) . . ? N1 C101 H10A 108.4 . . ? C102 C101 H10A 108.4 . . ? N1 C101 H10B 108.4 . . ? C102 C101 H10B 108.4 . . ? H10A C101 H10B 107.5 . . ? C101 C102 H10C 109.5 . . ? C101 C102 H10D 109.5 . . ? H10C C102 H10D 109.5 . . ? C101 C102 H10E 109.5 . . ? H10C C102 H10E 109.5 . . ? H10D C102 H10E 109.5 . . ? N1 C103 C104 116.7(7) . . ? N1 C103 H10F 108.1 . . ? C104 C103 H10F 108.1 . . ? N1 C103 H10G 108.1 . . ? C104 C103 H10G 108.1 . . ? H10F C103 H10G 107.3 . . ? C103 C104 H10H 109.5 . . ? C103 C104 H10I 109.5 . . ? H10H C104 H10I 109.5 . . ? C103 C104 H10J 109.5 . . ? H10H C104 H10J 109.5 . . ? H10I C104 H10J 109.5 . . ? N1 C105 C106 115.7(7) . . ? N1 C105 H10K 108.3 . . ? C106 C105 H10K 108.3 . . ? N1 C105 H10L 108.3 . . ? C106 C105 H10L 108.3 . . ? H10K C105 H10L 107.4 . . ? C105 C106 H10M 109.5 . . ? C105 C106 H10N 109.5 . . ? H10M C106 H10N 109.5 . . ? C105 C106 H10O 109.5 . . ? H10M C106 H10O 109.5 . . ? H10N C106 H10O 109.5 . . ? N1 C107 C108 115.4(7) . . ? N1 C107 H10P 108.4 . . ? C108 C107 H10P 108.4 . . ? N1 C107 H10Q 108.4 . . ? C108 C107 H10Q 108.4 . . ? H10P C107 H10Q 107.5 . . ? C107 C108 H10R 109.5 . . ? C107 C108 H10S 109.5 . . ? H10R C108 H10S 109.5 . . ? C107 C108 H10T 109.5 . . ? H10R C108 H10T 109.5 . . ? H10S C108 H10T 109.5 . . ? C201 N2 C207 109.9(5) . . ? C201 N2 C205 111.6(6) . . ? C207 N2 C205 107.6(6) . . ? C201 N2 C203 108.9(5) . . ? C207 N2 C203 111.5(6) . . ? C205 N2 C203 107.3(5) . . ? N2 C201 C202 117.1(6) . . ? N2 C201 H20A 108.0 . . ? C202 C201 H20A 108.0 . . ? N2 C201 H20B 108.0 . . ? C202 C201 H20B 108.0 . . ? H20A C201 H20B 107.3 . . ? C201 C202 H20C 109.5 . . ? C201 C202 H20D 109.5 . . ? H20C C202 H20D 109.5 . . ? C201 C202 H20E 109.5 . . ? H20C C202 H20E 109.5 . . ? H20D C202 H20E 109.5 . . ? N2 C203 C204 116.1(6) . . ? N2 C203 H20F 108.3 . . ? C204 C203 H20F 108.3 . . ? N2 C203 H20G 108.3 . . ? C204 C203 H20G 108.3 . . ? H20F C203 H20G 107.4 . . ? C203 C204 H20H 109.5 . . ? C203 C204 H20I 109.5 . . ? H20H C204 H20I 109.5 . . ? C203 C204 H20J 109.5 . . ? H20H C204 H20J 109.5 . . ? H20I C204 H20J 109.5 . . ? N2 C205 C206 116.7(7) . . ? N2 C205 H20K 108.1 . . ? C206 C205 H20K 108.1 . . ? N2 C205 H20L 108.1 . . ? C206 C205 H20L 108.1 . . ? H20K C205 H20L 107.3 . . ? C205 C206 H20M 109.5 . . ? C205 C206 H20N 109.5 . . ? H20M C206 H20N 109.5 . . ? C205 C206 H20O 109.5 . . ? H20M C206 H20O 109.5 . . ? H20N C206 H20O 109.5 . . ? N2 C207 C208 116.1(6) . . ? N2 C207 H20P 108.3 . . ? C208 C207 H20P 108.3 . . ? N2 C207 H20Q 108.3 . . ? C208 C207 H20Q 108.3 . . ? H20P C207 H20Q 107.4 . . ? C207 C208 H20R 109.5 . . ? C207 C208 H20S 109.5 . . ? H20R C208 H20S 109.5 . . ? C207 C208 H20T 109.5 . . ? H20R C208 H20T 109.5 . . ? H20S C208 H20T 109.5 . . ? C302 C301 H30A 109.5 . . ? C302 C301 H30B 109.5 . . ? H30A C301 H30B 109.5 . . ? C302 C301 H30C 109.5 . . ? H30A C301 H30C 109.5 . . ? H30B C301 H30C 109.5 . . ? O300 C302 C301 122.9(13) . . ? O300 C302 C303 119.0(13) . . ? C301 C302 C303 117.5(12) . . ? C302 C303 H30D 109.5 . . ? C302 C303 H30E 109.5 . . ? H30D C303 H30E 109.5 . . ? C302 C303 H30F 109.5 . . ? H30D C303 H30F 109.5 . . ? H30E C303 H30F 109.5 . . ? C402 C401 H40A 109.5 . . ? C402 C401 H40B 109.5 . . ? H40A C401 H40B 109.5 . . ? C402 C401 H40C 109.5 . . ? H40A C401 H40C 109.5 . . ? H40B C401 H40C 109.5 . . ? O400 C402 C401 119.4(8) . . ? O400 C402 C401 119.4(8) . 2_556 ? C401 C402 C401 121.2(16) . 2_556 ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C2 Ni1 Ni2 C17 -145.2(7) . . . . ? C2 Ni1 Ni2 C17 -103.3(7) 2_656 . . . ? C4 Ni1 Ni2 C17 33.7(7) 2_656 . . . ? C4 Ni1 Ni2 C17 77.7(7) . . . . ? C3 Ni1 Ni2 C17 10.2(7) . . . . ? C3 Ni1 Ni2 C17 102.1(7) 2_656 . . . ? C1 Ni1 Ni2 C17 -170.1(7) 2_656 . . . ? C1 Ni1 Ni2 C17 -77.7(7) . . . . ? Ni5 Ni1 Ni2 C17 -160.0(7) 2_656 . . . ? Ni5 Ni1 Ni2 C17 -85.1(7) . . . . ? Ni2 Ni1 Ni2 C17 -123.4(7) 2_656 . . . ? C2 Ni1 Ni2 C2 41.8(4) 2_656 . . . ? C4 Ni1 Ni2 C2 178.8(3) 2_656 . . . ? C4 Ni1 Ni2 C2 -137.1(3) . . . . ? C3 Ni1 Ni2 C2 155.4(3) . . . . ? C3 Ni1 Ni2 C2 -112.7(3) 2_656 . . . ? C1 Ni1 Ni2 C2 -24.9(3) 2_656 . . . ? C1 Ni1 Ni2 C2 67.5(3) . . . . ? Ni5 Ni1 Ni2 C2 -14.9(2) 2_656 . . . ? Ni5 Ni1 Ni2 C2 60.1(2) . . . . ? Ni2 Ni1 Ni2 C2 21.8(2) 2_656 . . . ? C2 Ni1 Ni2 C4 137.1(3) . . . . ? C2 Ni1 Ni2 C4 178.9(3) 2_656 . . . ? C4 Ni1 Ni2 C4 -44.0(4) 2_656 . . . ? C3 Ni1 Ni2 C4 -67.5(3) . . . . ? C3 Ni1 Ni2 C4 24.4(2) 2_656 . . . ? C1 Ni1 Ni2 C4 112.2(2) 2_656 . . . ? C1 Ni1 Ni2 C4 -155.4(2) . . . . ? Ni5 Ni1 Ni2 C4 122.3(2) 2_656 . . . ? Ni5 Ni1 Ni2 C4 -162.8(2) . . . . ? Ni2 Ni1 Ni2 C4 158.9(2) 2_656 . . . ? C2 Ni1 Ni2 Ni12 148.4(2) . . . . ? C2 Ni1 Ni2 Ni12 -169.8(2) 2_656 . . . ? C4 Ni1 Ni2 Ni12 -32.7(2) 2_656 . . . ? C4 Ni1 Ni2 Ni12 11.3(2) . . . . ? C3 Ni1 Ni2 Ni12 -56.22(16) . . . . ? C3 Ni1 Ni2 Ni12 35.67(16) 2_656 . . . ? C1 Ni1 Ni2 Ni12 123.47(15) 2_656 . . . ? C1 Ni1 Ni2 Ni12 -144.11(15) . . . . ? Ni5 Ni1 Ni2 Ni12 133.54(4) 2_656 . . . ? Ni5 Ni1 Ni2 Ni12 -151.49(4) . . . . ? Ni2 Ni1 Ni2 Ni12 170.20(3) 2_656 . . . ? C2 Ni1 Ni2 Ni11 -19.2(2) . . . . ? C2 Ni1 Ni2 Ni11 22.6(2) 2_656 . . . ? C4 Ni1 Ni2 Ni11 159.6(2) 2_656 . . . ? C4 Ni1 Ni2 Ni11 -156.3(2) . . . . ? C3 Ni1 Ni2 Ni11 136.17(16) . . . . ? C3 Ni1 Ni2 Ni11 -131.94(16) 2_656 . . . ? C1 Ni1 Ni2 Ni11 -44.14(15) 2_656 . . . ? C1 Ni1 Ni2 Ni11 48.28(15) . . . . ? Ni5 Ni1 Ni2 Ni11 -34.08(5) 2_656 . . . ? Ni5 Ni1 Ni2 Ni11 40.89(3) . . . . ? Ni2 Ni1 Ni2 Ni11 2.58(3) 2_656 . . . ? C2 Ni1 Ni2 Ni5 -60.1(2) . . . . ? C2 Ni1 Ni2 Ni5 -18.3(2) 2_656 . . . ? C4 Ni1 Ni2 Ni5 118.7(2) 2_656 . . . ? C4 Ni1 Ni2 Ni5 162.8(2) . . . . ? C3 Ni1 Ni2 Ni5 95.28(16) . . . . ? C3 Ni1 Ni2 Ni5 -172.83(16) 2_656 . . . ? C1 Ni1 Ni2 Ni5 -85.03(15) 2_656 . . . ? C1 Ni1 Ni2 Ni5 7.39(15) . . . . ? Ni5 Ni1 Ni2 Ni5 -74.97(5) 2_656 . . . ? Ni2 Ni1 Ni2 Ni5 -38.31(2) 2_656 . . . ? C2 Ni1 Ni2 Ni4 -170.0(2) . . . . ? C2 Ni1 Ni2 Ni4 -128.2(2) 2_656 . . . ? C4 Ni1 Ni2 Ni4 8.8(2) 2_656 . . . ? C4 Ni1 Ni2 Ni4 52.8(2) . . . . ? C3 Ni1 Ni2 Ni4 -14.67(16) . . . . ? C3 Ni1 Ni2 Ni4 77.22(16) 2_656 . . . ? C1 Ni1 Ni2 Ni4 165.02(15) 2_656 . . . ? C1 Ni1 Ni2 Ni4 -102.56(15) . . . . ? Ni5 Ni1 Ni2 Ni4 175.09(4) 2_656 . . . ? Ni5 Ni1 Ni2 Ni4 -109.94(3) . . . . ? Ni2 Ni1 Ni2 Ni4 -148.25(2) 2_656 . . . ? C2 Ni1 Ni2 Ni6 40.2(2) . . . . ? C2 Ni1 Ni2 Ni6 82.1(2) 2_656 . . . ? C4 Ni1 Ni2 Ni6 -140.9(2) 2_656 . . . ? C4 Ni1 Ni2 Ni6 -96.9(2) . . . . ? C3 Ni1 Ni2 Ni6 -164.38(16) . . . . ? C3 Ni1 Ni2 Ni6 -72.49(16) 2_656 . . . ? C1 Ni1 Ni2 Ni6 15.31(15) 2_656 . . . ? C1 Ni1 Ni2 Ni6 107.73(15) . . . . ? Ni5 Ni1 Ni2 Ni6 25.37(4) 2_656 . . . ? Ni5 Ni1 Ni2 Ni6 100.34(3) . . . . ? Ni2 Ni1 Ni2 Ni6 62.03(2) 2_656 . . . ? C2 Ni1 Ni2 Ni7 98.7(2) . . . . ? C2 Ni1 Ni2 Ni7 140.6(2) 2_656 . . . ? C4 Ni1 Ni2 Ni7 -82.4(2) 2_656 . . . ? C4 Ni1 Ni2 Ni7 -38.4(2) . . . . ? C3 Ni1 Ni2 Ni7 -105.88(16) . . . . ? C3 Ni1 Ni2 Ni7 -13.99(16) 2_656 . . . ? C1 Ni1 Ni2 Ni7 73.81(15) 2_656 . . . ? C1 Ni1 Ni2 Ni7 166.23(15) . . . . ? Ni5 Ni1 Ni2 Ni7 83.88(3) 2_656 . . . ? Ni5 Ni1 Ni2 Ni7 158.85(4) . . . . ? Ni2 Ni1 Ni2 Ni7 120.54(2) 2_656 . . . ? C2 Ni1 Ni3 C6 16.7(5) . . . . ? C2 Ni1 Ni3 C6 108.5(5) 2_656 . . . ? C4 Ni1 Ni3 C6 -163.6(5) 2_656 . . . ? C4 Ni1 Ni3 C6 -71.3(5) . . . . ? C3 Ni1 Ni3 C6 -138.4(5) . . . . ? C3 Ni1 Ni3 C6 -97.2(5) 2_656 . . . ? C1 Ni1 Ni3 C6 39.8(5) 2_656 . . . ? C1 Ni1 Ni3 C6 84.4(5) . . . . ? Ni5 Ni1 Ni3 C6 97.4(5) 2_656 . . . ? Ni5 Ni1 Ni3 C6 30.5(5) . . . . ? Ni2 Ni1 Ni3 C6 150.5(5) 2_656 . . . ? Ni2 Ni1 Ni3 C6 -24.3(5) . . . . ? C2 Ni1 Ni3 C3 155.1(3) . . . . ? C2 Ni1 Ni3 C3 -113.1(3) 2_656 . . . ? C4 Ni1 Ni3 C3 -25.2(3) 2_656 . . . ? C4 Ni1 Ni3 C3 67.1(3) . . . . ? C3 Ni1 Ni3 C3 41.2(4) 2_656 . . . ? C1 Ni1 Ni3 C3 178.2(3) 2_656 . . . ? C1 Ni1 Ni3 C3 -137.2(3) . . . . ? Ni5 Ni1 Ni3 C3 -124.2(2) 2_656 . . . ? Ni5 Ni1 Ni3 C3 168.9(2) . . . . ? Ni2 Ni1 Ni3 C3 -71.1(2) 2_656 . . . ? Ni2 Ni1 Ni3 C3 114.1(2) . . . . ? C2 Ni1 Ni3 C1 -67.7(2) . . . . ? C2 Ni1 Ni3 C1 24.0(2) 2_656 . . . ? C4 Ni1 Ni3 C1 112.0(2) 2_656 . . . ? C4 Ni1 Ni3 C1 -155.8(2) . . . . ? C3 Ni1 Ni3 C1 137.2(3) . . . . ? C3 Ni1 Ni3 C1 178.3(3) 2_656 . . . ? C1 Ni1 Ni3 C1 -44.6(4) 2_656 . . . ? Ni5 Ni1 Ni3 C1 13.0(2) 2_656 . . . ? Ni5 Ni1 Ni3 C1 -53.91(19) . . . . ? Ni2 Ni1 Ni3 C1 66.08(19) 2_656 . . . ? Ni2 Ni1 Ni3 C1 -108.8(2) . . . . ? C2 Ni1 Ni3 Ni13 136.74(15) . . . . ? C2 Ni1 Ni3 Ni13 -131.50(15) 2_656 . . . ? C4 Ni1 Ni3 Ni13 -43.53(16) 2_656 . . . ? C4 Ni1 Ni3 Ni13 48.71(16) . . . . ? C3 Ni1 Ni3 Ni13 -18.4(2) . . . . ? C3 Ni1 Ni3 Ni13 22.8(2) 2_656 . . . ? C1 Ni1 Ni3 Ni13 159.8(2) 2_656 . . . ? C1 Ni1 Ni3 Ni13 -155.5(2) . . . . ? Ni5 Ni1 Ni3 Ni13 -142.54(4) 2_656 . . . ? Ni5 Ni1 Ni3 Ni13 150.56(4) . . . . ? Ni2 Ni1 Ni3 Ni13 -89.45(4) 2_656 . . . ? Ni2 Ni1 Ni3 Ni13 95.69(4) . . . . ? C2 Ni1 Ni3 Ni9 -55.40(15) . . . . ? C2 Ni1 Ni3 Ni9 36.36(15) 2_656 . . . ? C4 Ni1 Ni3 Ni9 124.33(16) 2_656 . . . ? C4 Ni1 Ni3 Ni9 -143.43(16) . . . . ? C3 Ni1 Ni3 Ni9 149.5(2) . . . . ? C3 Ni1 Ni3 Ni9 -169.3(2) 2_656 . . . ? C1 Ni1 Ni3 Ni9 -32.3(2) 2_656 . . . ? C1 Ni1 Ni3 Ni9 12.34(19) . . . . ? Ni5 Ni1 Ni3 Ni9 25.32(5) 2_656 . . . ? Ni5 Ni1 Ni3 Ni9 -41.57(3) . . . . ? Ni2 Ni1 Ni3 Ni9 78.42(4) 2_656 . . . ? Ni2 Ni1 Ni3 Ni9 -96.45(4) . . . . ? C2 Ni1 Ni3 Ni5 -13.82(15) . . . . ? C2 Ni1 Ni3 Ni5 77.94(15) 2_656 . . . ? C4 Ni1 Ni3 Ni5 165.91(16) 2_656 . . . ? C4 Ni1 Ni3 Ni5 -101.85(15) . . . . ? C3 Ni1 Ni3 Ni5 -168.9(2) . . . . ? C3 Ni1 Ni3 Ni5 -127.7(2) 2_656 . . . ? C1 Ni1 Ni3 Ni5 9.3(2) 2_656 . . . ? C1 Ni1 Ni3 Ni5 53.91(19) . . . . ? Ni5 Ni1 Ni3 Ni5 66.90(5) 2_656 . . . ? Ni2 Ni1 Ni3 Ni5 119.99(4) 2_656 . . . ? Ni2 Ni1 Ni3 Ni5 -54.87(3) . . . . ? C2 Ni1 Ni3 Ni4 96.34(15) . . . . ? C2 Ni1 Ni3 Ni4 -171.90(15) 2_656 . . . ? C4 Ni1 Ni3 Ni4 -83.93(16) 2_656 . . . ? C4 Ni1 Ni3 Ni4 8.31(16) . . . . ? C3 Ni1 Ni3 Ni4 -58.8(2) . . . . ? C3 Ni1 Ni3 Ni4 -17.6(2) 2_656 . . . ? C1 Ni1 Ni3 Ni4 119.4(2) 2_656 . . . ? C1 Ni1 Ni3 Ni4 164.08(19) . . . . ? Ni5 Ni1 Ni3 Ni4 177.06(4) 2_656 . . . ? Ni5 Ni1 Ni3 Ni4 110.16(3) . . . . ? Ni2 Ni1 Ni3 Ni4 -129.84(4) 2_656 . . . ? Ni2 Ni1 Ni3 Ni4 55.29(3) . . . . ? C2 Ni1 Ni3 Ni7 -163.15(15) . . . 2_656 ? C2 Ni1 Ni3 Ni7 -71.39(15) 2_656 . . 2_656 ? C4 Ni1 Ni3 Ni7 16.58(16) 2_656 . . 2_656 ? C4 Ni1 Ni3 Ni7 108.82(16) . . . 2_656 ? C3 Ni1 Ni3 Ni7 41.7(2) . . . 2_656 ? C3 Ni1 Ni3 Ni7 82.9(2) 2_656 . . 2_656 ? C1 Ni1 Ni3 Ni7 -140.1(2) 2_656 . . 2_656 ? C1 Ni1 Ni3 Ni7 -95.42(19) . . . 2_656 ? Ni5 Ni1 Ni3 Ni7 -82.43(4) 2_656 . . 2_656 ? Ni5 Ni1 Ni3 Ni7 -149.33(4) . . . 2_656 ? Ni2 Ni1 Ni3 Ni7 -29.33(4) 2_656 . . 2_656 ? Ni2 Ni1 Ni3 Ni7 155.80(4) . . . 2_656 ? C2 Ni1 Ni3 Ni6 -104.66(15) . . . 2_656 ? C2 Ni1 Ni3 Ni6 -12.90(15) 2_656 . . 2_656 ? C4 Ni1 Ni3 Ni6 75.07(16) 2_656 . . 2_656 ? C4 Ni1 Ni3 Ni6 167.31(16) . . . 2_656 ? C3 Ni1 Ni3 Ni6 100.2(2) . . . 2_656 ? C3 Ni1 Ni3 Ni6 141.4(2) 2_656 . . 2_656 ? C1 Ni1 Ni3 Ni6 -81.6(2) 2_656 . . 2_656 ? C1 Ni1 Ni3 Ni6 -36.92(19) . . . 2_656 ? Ni5 Ni1 Ni3 Ni6 -23.94(4) 2_656 . . 2_656 ? Ni5 Ni1 Ni3 Ni6 -90.83(3) . . . 2_656 ? Ni2 Ni1 Ni3 Ni6 29.16(3) 2_656 . . 2_656 ? Ni2 Ni1 Ni3 Ni6 -145.71(3) . . . 2_656 ? C17 Ni2 Ni4 C15 -16.4(4) . . . . ? C2 Ni2 Ni4 C15 144.3(4) . . . . ? C4 Ni2 Ni4 C15 -140.7(4) . . . . ? Ni12 Ni2 Ni4 C15 -77.2(3) . . . . ? Ni11 Ni2 Ni4 C15 90.5(3) . . . . ? Ni5 Ni2 Ni4 C15 98.7(3) . . . . ? Ni1 Ni2 Ni4 C15 153.1(3) . . . . ? Ni6 Ni2 Ni4 C15 -161.1(3) . . . . ? Ni7 Ni2 Ni4 C15 -123.5(3) . . . . ? C17 Ni2 Ni4 C4 124.4(4) . . . . ? C2 Ni2 Ni4 C4 -75.0(3) . . . . ? Ni12 Ni2 Ni4 C4 63.6(2) . . . . ? Ni11 Ni2 Ni4 C4 -128.8(2) . . . . ? Ni5 Ni2 Ni4 C4 -120.5(2) . . . . ? Ni1 Ni2 Ni4 C4 -66.2(2) . . . . ? Ni6 Ni2 Ni4 C4 -20.4(2) . . . . ? Ni7 Ni2 Ni4 C4 17.2(2) . . . . ? C17 Ni2 Ni4 C3 -153.3(4) . . . . ? C2 Ni2 Ni4 C3 7.3(3) . . . . ? C4 Ni2 Ni4 C3 82.3(3) . . . . ? Ni12 Ni2 Ni4 C3 145.91(18) . . . . ? Ni11 Ni2 Ni4 C3 -46.4(2) . . . . ? Ni5 Ni2 Ni4 C3 -38.20(18) . . . . ? Ni1 Ni2 Ni4 C3 16.14(18) . . . . ? Ni6 Ni2 Ni4 C3 61.94(19) . . . . ? Ni7 Ni2 Ni4 C3 99.52(18) . . . . ? C17 Ni2 Ni4 Ni13 -106.4(3) . . . . ? C2 Ni2 Ni4 Ni13 54.2(2) . . . . ? C4 Ni2 Ni4 Ni13 129.2(2) . . . . ? Ni12 Ni2 Ni4 Ni13 -167.19(8) . . . . ? Ni11 Ni2 Ni4 Ni13 0.45(12) . . . . ? Ni5 Ni2 Ni4 Ni13 8.70(8) . . . . ? Ni1 Ni2 Ni4 Ni13 63.04(7) . . . . ? Ni6 Ni2 Ni4 Ni13 108.83(8) . . . . ? Ni7 Ni2 Ni4 Ni13 146.42(7) . . . . ? C17 Ni2 Ni4 Ni12 60.8(3) . . . . ? C2 Ni2 Ni4 Ni12 -138.57(19) . . . . ? C4 Ni2 Ni4 Ni12 -63.6(2) . . . . ? Ni11 Ni2 Ni4 Ni12 167.64(8) . . . . ? Ni5 Ni2 Ni4 Ni12 175.89(4) . . . . ? Ni1 Ni2 Ni4 Ni12 -129.77(4) . . . . ? Ni6 Ni2 Ni4 Ni12 -83.98(5) . . . . ? Ni7 Ni2 Ni4 Ni12 -46.39(3) . . . . ? C17 Ni2 Ni4 Ni1 -169.4(3) . . . . ? C2 Ni2 Ni4 Ni1 -8.80(19) . . . . ? C4 Ni2 Ni4 Ni1 66.2(2) . . . . ? Ni12 Ni2 Ni4 Ni1 129.77(4) . . . . ? Ni11 Ni2 Ni4 Ni1 -62.59(7) . . . . ? Ni5 Ni2 Ni4 Ni1 -54.34(3) . . . . ? Ni6 Ni2 Ni4 Ni1 45.79(5) . . . . ? Ni7 Ni2 Ni4 Ni1 83.38(3) . . . . ? C17 Ni2 Ni4 Ni3 -114.6(3) . . . . ? C2 Ni2 Ni4 Ni3 46.03(19) . . . . ? C4 Ni2 Ni4 Ni3 121.0(2) . . . . ? Ni12 Ni2 Ni4 Ni3 -175.40(4) . . . . ? Ni11 Ni2 Ni4 Ni3 -7.76(8) . . . . ? Ni5 Ni2 Ni4 Ni3 0.49(3) . . . . ? Ni1 Ni2 Ni4 Ni3 54.83(3) . . . . ? Ni6 Ni2 Ni4 Ni3 100.63(5) . . . . ? Ni7 Ni2 Ni4 Ni3 138.21(3) . . . . ? C17 Ni2 Ni4 Ni10 109.7(3) . . . . ? C2 Ni2 Ni4 Ni10 -89.67(19) . . . . ? C4 Ni2 Ni4 Ni10 -14.7(2) . . . . ? Ni12 Ni2 Ni4 Ni10 48.91(3) . . . . ? Ni11 Ni2 Ni4 Ni10 -143.45(7) . . . . ? Ni5 Ni2 Ni4 Ni10 -135.21(3) . . . . ? Ni1 Ni2 Ni4 Ni10 -80.86(3) . . . . ? Ni6 Ni2 Ni4 Ni10 -35.07(6) . . . . ? Ni7 Ni2 Ni4 Ni10 2.52(3) . . . . ? C17 Ni2 Ni4 Ni10 160.5(3) . . . 2_656 ? C2 Ni2 Ni4 Ni10 -38.9(2) . . . 2_656 ? C4 Ni2 Ni4 Ni10 36.1(2) . . . 2_656 ? Ni12 Ni2 Ni4 Ni10 99.72(6) . . . 2_656 ? Ni11 Ni2 Ni4 Ni10 -92.64(9) . . . 2_656 ? Ni5 Ni2 Ni4 Ni10 -84.40(6) . . . 2_656 ? Ni1 Ni2 Ni4 Ni10 -30.05(5) . . . 2_656 ? Ni6 Ni2 Ni4 Ni10 15.74(9) . . . 2_656 ? Ni7 Ni2 Ni4 Ni10 53.33(6) . . . 2_656 ? C2 Ni1 Ni4 C15 -80.9(7) . . . . ? C2 Ni1 Ni4 C15 32.1(7) 2_656 . . . ? C4 Ni1 Ni4 C15 98.3(7) 2_656 . . . ? C4 Ni1 Ni4 C15 -147.8(7) . . . . ? C3 Ni1 Ni4 C15 73.0(7) . . . . ? C3 Ni1 Ni4 C15 -173.2(7) 2_656 . . . ? C1 Ni1 Ni4 C15 -106.9(7) 2_656 . . . ? C1 Ni1 Ni4 C15 8.0(7) . . . . ? Ni5 Ni1 Ni4 C15 -135.7(8) 2_656 . . . ? Ni5 Ni1 Ni4 C15 -33.4(7) . . . . ? Ni2 Ni1 Ni4 C15 88.8(7) 2_656 . . . ? Ni2 Ni1 Ni4 C15 -87.9(7) . . . . ? C2 Ni1 Ni4 C4 67.0(3) . . . . ? C2 Ni1 Ni4 C4 179.9(3) 2_656 . . . ? C4 Ni1 Ni4 C4 -113.9(3) 2_656 . . . ? C3 Ni1 Ni4 C4 -139.2(3) . . . . ? C3 Ni1 Ni4 C4 -25.4(3) 2_656 . . . ? C1 Ni1 Ni4 C4 40.9(3) 2_656 . . . ? C1 Ni1 Ni4 C4 155.8(3) . . . . ? Ni5 Ni1 Ni4 C4 12.1(4) 2_656 . . . ? Ni5 Ni1 Ni4 C4 114.4(2) . . . . ? Ni2 Ni1 Ni4 C4 -123.4(2) 2_656 . . . ? Ni2 Ni1 Ni4 C4 59.9(2) . . . . ? C2 Ni1 Ni4 C3 -153.8(3) . . . . ? C2 Ni1 Ni4 C3 -40.9(3) 2_656 . . . ? C4 Ni1 Ni4 C3 25.3(3) 2_656 . . . ? C4 Ni1 Ni4 C3 139.2(3) . . . . ? C3 Ni1 Ni4 C3 113.8(3) 2_656 . . . ? C1 Ni1 Ni4 C3 -179.9(3) 2_656 . . . ? C1 Ni1 Ni4 C3 -65.0(3) . . . . ? Ni5 Ni1 Ni4 C3 151.3(4) 2_656 . . . ? Ni5 Ni1 Ni4 C3 -106.4(2) . . . . ? Ni2 Ni1 Ni4 C3 15.8(2) 2_656 . . . ? Ni2 Ni1 Ni4 C3 -160.9(2) . . . . ? C2 Ni1 Ni4 Ni13 -141.73(15) . . . . ? C2 Ni1 Ni4 Ni13 -28.8(2) 2_656 . . . ? C4 Ni1 Ni4 Ni13 37.46(15) 2_656 . . . ? C4 Ni1 Ni4 Ni13 151.3(2) . . . . ? C3 Ni1 Ni4 Ni13 12.1(2) . . . . ? C3 Ni1 Ni4 Ni13 125.88(16) 2_656 . . . ? C1 Ni1 Ni4 Ni13 -167.80(19) 2_656 . . . ? C1 Ni1 Ni4 Ni13 -52.88(15) . . . . ? Ni5 Ni1 Ni4 Ni13 163.4(4) 2_656 . . . ? Ni5 Ni1 Ni4 Ni13 -94.27(3) . . . . ? Ni2 Ni1 Ni4 Ni13 27.93(5) 2_656 . . . ? Ni2 Ni1 Ni4 Ni13 -148.80(4) . . . . ? C2 Ni1 Ni4 Ni12 47.97(15) . . . . ? C2 Ni1 Ni4 Ni12 160.9(2) 2_656 . . . ? C4 Ni1 Ni4 Ni12 -132.85(15) 2_656 . . . ? C4 Ni1 Ni4 Ni12 -19.0(2) . . . . ? C3 Ni1 Ni4 Ni12 -158.2(2) . . . . ? C3 Ni1 Ni4 Ni12 -44.42(16) 2_656 . . . ? C1 Ni1 Ni4 Ni12 21.9(2) 2_656 . . . ? C1 Ni1 Ni4 Ni12 136.82(15) . . . . ? Ni5 Ni1 Ni4 Ni12 -6.9(4) 2_656 . . . ? Ni5 Ni1 Ni4 Ni12 95.43(3) . . . . ? Ni2 Ni1 Ni4 Ni12 -142.37(4) 2_656 . . . ? Ni2 Ni1 Ni4 Ni12 40.90(3) . . . . ? C2 Ni1 Ni4 Ni2 7.06(15) . . . . ? C2 Ni1 Ni4 Ni2 120.0(2) 2_656 . . . ? C4 Ni1 Ni4 Ni2 -173.75(15) 2_656 . . . ? C4 Ni1 Ni4 Ni2 -59.9(2) . . . . ? C3 Ni1 Ni4 Ni2 160.9(2) . . . . ? C3 Ni1 Ni4 Ni2 -85.32(16) 2_656 . . . ? C1 Ni1 Ni4 Ni2 -19.00(19) 2_656 . . . ? C1 Ni1 Ni4 Ni2 95.92(15) . . . . ? Ni5 Ni1 Ni4 Ni2 -47.8(4) 2_656 . . . ? Ni5 Ni1 Ni4 Ni2 54.53(3) . . . . ? Ni2 Ni1 Ni4 Ni2 176.73(4) 2_656 . . . ? C2 Ni1 Ni4 Ni3 -101.30(15) . . . . ? C2 Ni1 Ni4 Ni3 11.7(2) 2_656 . . . ? C4 Ni1 Ni4 Ni3 77.88(15) 2_656 . . . ? C4 Ni1 Ni4 Ni3 -168.3(2) . . . . ? C3 Ni1 Ni4 Ni3 52.5(2) . . . . ? C3 Ni1 Ni4 Ni3 166.31(16) 2_656 . . . ? C1 Ni1 Ni4 Ni3 -127.37(19) 2_656 . . . ? C1 Ni1 Ni4 Ni3 -12.45(15) . . . . ? Ni5 Ni1 Ni4 Ni3 -156.2(4) 2_656 . . . ? Ni5 Ni1 Ni4 Ni3 -53.84(3) . . . . ? Ni2 Ni1 Ni4 Ni3 68.36(4) 2_656 . . . ? Ni2 Ni1 Ni4 Ni3 -108.37(3) . . . . ? C2 Ni1 Ni4 Ni10 108.00(15) . . . . ? C2 Ni1 Ni4 Ni10 -139.0(2) 2_656 . . . ? C4 Ni1 Ni4 Ni10 -72.81(15) 2_656 . . . ? C4 Ni1 Ni4 Ni10 41.0(2) . . . . ? C3 Ni1 Ni4 Ni10 -98.2(2) . . . . ? C3 Ni1 Ni4 Ni10 15.61(16) 2_656 . . . ? C1 Ni1 Ni4 Ni10 81.94(19) 2_656 . . . ? C1 Ni1 Ni4 Ni10 -163.15(15) . . . . ? Ni5 Ni1 Ni4 Ni10 53.2(4) 2_656 . . . ? Ni5 Ni1 Ni4 Ni10 155.46(3) . . . . ? Ni2 Ni1 Ni4 Ni10 -82.33(4) 2_656 . . . ? Ni2 Ni1 Ni4 Ni10 100.94(3) . . . . ? C2 Ni1 Ni4 Ni10 167.71(15) . . . 2_656 ? C2 Ni1 Ni4 Ni10 -79.3(2) 2_656 . . 2_656 ? C4 Ni1 Ni4 Ni10 -13.10(15) 2_656 . . 2_656 ? C4 Ni1 Ni4 Ni10 100.8(2) . . . 2_656 ? C3 Ni1 Ni4 Ni10 -38.5(2) . . . 2_656 ? C3 Ni1 Ni4 Ni10 75.32(16) 2_656 . . 2_656 ? C1 Ni1 Ni4 Ni10 141.64(19) 2_656 . . 2_656 ? C1 Ni1 Ni4 Ni10 -103.44(15) . . . 2_656 ? Ni5 Ni1 Ni4 Ni10 112.9(4) 2_656 . . 2_656 ? Ni5 Ni1 Ni4 Ni10 -144.83(3) . . . 2_656 ? Ni2 Ni1 Ni4 Ni10 -22.63(4) 2_656 . . 2_656 ? Ni2 Ni1 Ni4 Ni10 160.64(3) . . . 2_656 ? C6 Ni3 Ni4 C15 -22.7(4) . . . . ? C3 Ni3 Ni4 C15 121.5(4) . . . . ? C1 Ni3 Ni4 C15 -158.1(3) . . . . ? Ni13 Ni3 Ni4 C15 57.6(3) . . . . ? Ni9 Ni3 Ni4 C15 -110.9(3) . . . . ? Ni5 Ni3 Ni4 C15 -117.3(3) . . . . ? Ni1 Ni3 Ni4 C15 -171.8(3) . . . . ? Ni7 Ni3 Ni4 C15 107.3(3) 2_656 . . . ? Ni6 Ni3 Ni4 C15 156.0(3) 2_656 . . . ? C6 Ni3 Ni4 C4 138.9(3) . . . . ? C3 Ni3 Ni4 C4 -76.9(3) . . . . ? C1 Ni3 Ni4 C4 3.5(3) . . . . ? Ni13 Ni3 Ni4 C4 -140.8(2) . . . . ? Ni9 Ni3 Ni4 C4 50.7(2) . . . . ? Ni5 Ni3 Ni4 C4 44.3(2) . . . . ? Ni1 Ni3 Ni4 C4 -10.19(19) . . . . ? Ni7 Ni3 Ni4 C4 -91.1(2) 2_656 . . . ? Ni6 Ni3 Ni4 C4 -42.4(2) 2_656 . . . ? C6 Ni3 Ni4 C3 -144.2(3) . . . . ? C1 Ni3 Ni4 C3 80.4(3) . . . . ? Ni13 Ni3 Ni4 C3 -63.9(2) . . . . ? Ni9 Ni3 Ni4 C3 127.6(2) . . . . ? Ni5 Ni3 Ni4 C3 121.2(2) . . . . ? Ni1 Ni3 Ni4 C3 66.7(2) . . . . ? Ni7 Ni3 Ni4 C3 -14.2(2) 2_656 . . . ? Ni6 Ni3 Ni4 C3 34.5(2) 2_656 . . . ? C6 Ni3 Ni4 Ni13 -80.2(2) . . . . ? C3 Ni3 Ni4 Ni13 63.9(2) . . . . ? C1 Ni3 Ni4 Ni13 144.33(17) . . . . ? Ni9 Ni3 Ni4 Ni13 -168.51(8) . . . . ? Ni5 Ni3 Ni4 Ni13 -174.92(4) . . . . ? Ni1 Ni3 Ni4 Ni13 130.62(4) . . . . ? Ni7 Ni3 Ni4 Ni13 49.76(3) 2_656 . . . ? Ni6 Ni3 Ni4 Ni13 98.40(6) 2_656 . . . ? C6 Ni3 Ni4 Ni12 87.4(3) . . . . ? C3 Ni3 Ni4 Ni12 -128.4(2) . . . . ? C1 Ni3 Ni4 Ni12 -48.00(18) . . . . ? Ni13 Ni3 Ni4 Ni12 167.66(8) . . . . ? Ni9 Ni3 Ni4 Ni12 -0.84(12) . . . . ? Ni5 Ni3 Ni4 Ni12 -7.26(8) . . . . ? Ni1 Ni3 Ni4 Ni12 -61.72(7) . . . . ? Ni7 Ni3 Ni4 Ni12 -142.58(7) 2_656 . . . ? Ni6 Ni3 Ni4 Ni12 -93.94(8) 2_656 . . . ? C6 Ni3 Ni4 Ni2 94.2(2) . . . . ? C3 Ni3 Ni4 Ni2 -121.7(2) . . . . ? C1 Ni3 Ni4 Ni2 -41.24(17) . . . . ? Ni13 Ni3 Ni4 Ni2 174.43(4) . . . . ? Ni9 Ni3 Ni4 Ni2 5.92(8) . . . . ? Ni5 Ni3 Ni4 Ni2 -0.50(3) . . . . ? Ni1 Ni3 Ni4 Ni2 -54.95(3) . . . . ? Ni7 Ni3 Ni4 Ni2 -135.81(3) 2_656 . . . ? Ni6 Ni3 Ni4 Ni2 -87.17(6) 2_656 . . . ? C6 Ni3 Ni4 Ni1 149.1(2) . . . . ? C3 Ni3 Ni4 Ni1 -66.7(2) . . . . ? C1 Ni3 Ni4 Ni1 13.71(17) . . . . ? Ni13 Ni3 Ni4 Ni1 -130.62(4) . . . . ? Ni9 Ni3 Ni4 Ni1 60.87(7) . . . . ? Ni5 Ni3 Ni4 Ni1 54.46(3) . . . . ? Ni7 Ni3 Ni4 Ni1 -80.86(3) 2_656 . . . ? Ni6 Ni3 Ni4 Ni1 -32.22(5) 2_656 . . . ? C6 Ni3 Ni4 Ni10 -166.8(2) . . . . ? C3 Ni3 Ni4 Ni10 -22.6(2) . . . . ? C1 Ni3 Ni4 Ni10 57.81(18) . . . . ? Ni13 Ni3 Ni4 Ni10 -86.52(6) . . . . ? Ni9 Ni3 Ni4 Ni10 104.97(8) . . . . ? Ni5 Ni3 Ni4 Ni10 98.55(5) . . . . ? Ni1 Ni3 Ni4 Ni10 44.10(5) . . . . ? Ni7 Ni3 Ni4 Ni10 -36.76(6) 2_656 . . . ? Ni6 Ni3 Ni4 Ni10 11.88(9) 2_656 . . . ? C6 Ni3 Ni4 Ni10 -126.8(2) . . . 2_656 ? C3 Ni3 Ni4 Ni10 17.4(2) . . . 2_656 ? C1 Ni3 Ni4 Ni10 97.79(17) . . . 2_656 ? Ni13 Ni3 Ni4 Ni10 -46.55(3) . . . 2_656 ? Ni9 Ni3 Ni4 Ni10 144.95(7) . . . 2_656 ? Ni5 Ni3 Ni4 Ni10 138.53(3) . . . 2_656 ? Ni1 Ni3 Ni4 Ni10 84.08(3) . . . 2_656 ? Ni7 Ni3 Ni4 Ni10 3.21(3) 2_656 . . 2_656 ? Ni6 Ni3 Ni4 Ni10 51.85(6) 2_656 . . 2_656 ? C6 Ni3 Ni5 C8 -16.3(4) . . . . ? C3 Ni3 Ni5 C8 139.6(3) . . . . ? C1 Ni3 Ni5 C8 -144.1(3) . . . . ? Ni13 Ni3 Ni5 C8 87.0(3) . . . . ? Ni9 Ni3 Ni5 C8 -81.1(3) . . . . ? Ni1 Ni3 Ni5 C8 149.3(3) . . . . ? Ni4 Ni3 Ni5 C8 94.9(3) . . . . ? Ni7 Ni3 Ni5 C8 -164.9(3) 2_656 . . . ? Ni6 Ni3 Ni5 C8 -127.0(3) 2_656 . . . ? C6 Ni3 Ni5 C1 127.8(3) . . . . ? C3 Ni3 Ni5 C1 -76.3(3) . . . . ? Ni13 Ni3 Ni5 C1 -128.8(2) . . . . ? Ni9 Ni3 Ni5 C1 63.1(2) . . . . ? Ni1 Ni3 Ni5 C1 -66.5(2) . . . . ? Ni4 Ni3 Ni5 C1 -121.0(2) . . . . ? Ni7 Ni3 Ni5 C1 -20.7(2) 2_656 . . . ? Ni6 Ni3 Ni5 C1 17.2(2) 2_656 . . . ? C6 Ni3 Ni5 C2 -150.3(3) . . . . ? C3 Ni3 Ni5 C2 5.5(3) . . . . ? C1 Ni3 Ni5 C2 81.8(3) . . . . ? Ni13 Ni3 Ni5 C2 -47.00(19) . . . . ? Ni9 Ni3 Ni5 C2 144.86(17) . . . . ? Ni1 Ni3 Ni5 C2 15.30(17) . . . . ? Ni4 Ni3 Ni5 C2 -39.18(17) . . . . ? Ni7 Ni3 Ni5 C2 61.09(18) 2_656 . . . ? Ni6 Ni3 Ni5 C2 98.99(17) 2_656 . . . ? C6 Ni3 Ni5 Ni9 64.8(2) . . . . ? C3 Ni3 Ni5 Ni9 -139.3(2) . . . . ? C1 Ni3 Ni5 Ni9 -63.1(2) . . . . ? Ni13 Ni3 Ni5 Ni9 168.14(8) . . . . ? Ni1 Ni3 Ni5 Ni9 -129.56(4) . . . . ? Ni4 Ni3 Ni5 Ni9 175.97(4) . . . . ? Ni7 Ni3 Ni5 Ni9 -83.77(5) 2_656 . . . ? Ni6 Ni3 Ni5 Ni9 -45.86(3) 2_656 . . . ? C6 Ni3 Ni5 Ni11 -101.7(3) . . . . ? C3 Ni3 Ni5 Ni11 54.2(2) . . . . ? C1 Ni3 Ni5 Ni11 130.4(2) . . . . ? Ni13 Ni3 Ni5 Ni11 1.64(12) . . . . ? Ni9 Ni3 Ni5 Ni11 -166.50(8) . . . . ? Ni1 Ni3 Ni5 Ni11 63.94(7) . . . . ? Ni4 Ni3 Ni5 Ni11 9.46(8) . . . . ? Ni7 Ni3 Ni5 Ni11 109.73(8) 2_656 . . . ? Ni6 Ni3 Ni5 Ni11 147.63(7) 2_656 . . . ? C6 Ni3 Ni5 Ni1 -165.6(2) . . . . ? C3 Ni3 Ni5 Ni1 -9.8(2) . . . . ? C1 Ni3 Ni5 Ni1 66.5(2) . . . . ? Ni13 Ni3 Ni5 Ni1 -62.30(7) . . . . ? Ni9 Ni3 Ni5 Ni1 129.56(4) . . . . ? Ni4 Ni3 Ni5 Ni1 -54.48(3) . . . . ? Ni7 Ni3 Ni5 Ni1 45.79(5) 2_656 . . . ? Ni6 Ni3 Ni5 Ni1 83.69(3) 2_656 . . . ? C6 Ni3 Ni5 Ni2 -110.7(2) . . . . ? C3 Ni3 Ni5 Ni2 45.2(2) . . . . ? C1 Ni3 Ni5 Ni2 121.5(2) . . . . ? Ni13 Ni3 Ni5 Ni2 -7.32(8) . . . . ? Ni9 Ni3 Ni5 Ni2 -175.47(4) . . . . ? Ni1 Ni3 Ni5 Ni2 54.97(3) . . . . ? Ni4 Ni3 Ni5 Ni2 0.50(3) . . . . ? Ni7 Ni3 Ni5 Ni2 100.77(5) 2_656 . . . ? Ni6 Ni3 Ni5 Ni2 138.67(3) 2_656 . . . ? C6 Ni3 Ni5 Ni8 114.1(2) . . . 2_656 ? C3 Ni3 Ni5 Ni8 -90.0(2) . . . 2_656 ? C1 Ni3 Ni5 Ni8 -13.7(2) . . . 2_656 ? Ni13 Ni3 Ni5 Ni8 -142.53(7) . . . 2_656 ? Ni9 Ni3 Ni5 Ni8 49.33(3) . . . 2_656 ? Ni1 Ni3 Ni5 Ni8 -80.23(3) . . . 2_656 ? Ni4 Ni3 Ni5 Ni8 -134.71(3) . . . 2_656 ? Ni7 Ni3 Ni5 Ni8 -34.44(6) 2_656 . . 2_656 ? Ni6 Ni3 Ni5 Ni8 3.47(3) 2_656 . . 2_656 ? C6 Ni3 Ni5 Ni8 162.6(2) . . . . ? C3 Ni3 Ni5 Ni8 -41.5(2) . . . . ? C1 Ni3 Ni5 Ni8 34.7(2) . . . . ? Ni13 Ni3 Ni5 Ni8 -94.07(9) . . . . ? Ni9 Ni3 Ni5 Ni8 97.78(6) . . . . ? Ni1 Ni3 Ni5 Ni8 -31.78(5) . . . . ? Ni4 Ni3 Ni5 Ni8 -86.25(6) . . . . ? Ni7 Ni3 Ni5 Ni8 14.02(9) 2_656 . . . ? Ni6 Ni3 Ni5 Ni8 51.92(6) 2_656 . . . ? C2 Ni1 Ni5 C8 78.7(6) . . . . ? C2 Ni1 Ni5 C8 -168.5(5) 2_656 . . . ? C4 Ni1 Ni5 C8 -101.3(6) 2_656 . . . ? C4 Ni1 Ni5 C8 12.3(5) . . . . ? C3 Ni1 Ni5 C8 -75.7(5) . . . . ? C3 Ni1 Ni5 C8 36.1(6) 2_656 . . . ? C1 Ni1 Ni5 C8 103.0(5) 2_656 . . . ? C1 Ni1 Ni5 C8 -143.9(6) . . . . ? Ni5 Ni1 Ni5 C8 145.4(5) 2_656 . . . ? Ni2 Ni1 Ni5 C8 -157.8(5) 2_656 . . . ? Ni2 Ni1 Ni5 C8 25.7(5) . . . . ? C2 Ni1 Ni5 C1 -137.4(3) . . . . ? C2 Ni1 Ni5 C1 -24.6(3) 2_656 . . . ? C4 Ni1 Ni5 C1 42.6(3) 2_656 . . . ? C4 Ni1 Ni5 C1 156.3(3) . . . . ? C3 Ni1 Ni5 C1 68.2(3) . . . . ? C3 Ni1 Ni5 C1 180.0(3) 2_656 . . . ? C1 Ni1 Ni5 C1 -113.0(3) 2_656 . . . ? Ni5 Ni1 Ni5 C1 -70.7(2) 2_656 . . . ? Ni2 Ni1 Ni5 C1 -13.9(2) 2_656 . . . ? Ni2 Ni1 Ni5 C1 169.7(2) . . . . ? C2 Ni1 Ni5 C2 112.8(3) 2_656 . . . ? C4 Ni1 Ni5 C2 179.9(3) 2_656 . . . ? C4 Ni1 Ni5 C2 -66.4(2) . . . . ? C3 Ni1 Ni5 C2 -154.4(2) . . . . ? C3 Ni1 Ni5 C2 -42.7(3) 2_656 . . . ? C1 Ni1 Ni5 C2 24.3(2) 2_656 . . . ? C1 Ni1 Ni5 C2 137.4(3) . . . . ? Ni5 Ni1 Ni5 C2 66.69(19) 2_656 . . . ? Ni2 Ni1 Ni5 C2 123.49(19) 2_656 . . . ? Ni2 Ni1 Ni5 C2 -52.97(19) . . . . ? C2 Ni1 Ni5 Ni9 -155.70(19) . . . . ? C2 Ni1 Ni5 Ni9 -42.90(15) 2_656 . . . ? C4 Ni1 Ni5 Ni9 24.2(2) 2_656 . . . ? C4 Ni1 Ni5 Ni9 137.92(15) . . . . ? C3 Ni1 Ni5 Ni9 49.86(16) . . . . ? C3 Ni1 Ni5 Ni9 161.6(2) 2_656 . . . ? C1 Ni1 Ni5 Ni9 -131.37(15) 2_656 . . . ? C1 Ni1 Ni5 Ni9 -18.3(2) . . . . ? Ni5 Ni1 Ni5 Ni9 -89.01(3) 2_656 . . . ? Ni2 Ni1 Ni5 Ni9 -32.21(5) 2_656 . . . ? Ni2 Ni1 Ni5 Ni9 151.33(4) . . . . ? C2 Ni1 Ni5 Ni11 12.07(19) . . . . ? C2 Ni1 Ni5 Ni11 124.88(15) 2_656 . . . ? C4 Ni1 Ni5 Ni11 -168.0(2) 2_656 . . . ? C4 Ni1 Ni5 Ni11 -54.31(15) . . . . ? C3 Ni1 Ni5 Ni11 -142.37(16) . . . . ? C3 Ni1 Ni5 Ni11 -30.6(2) 2_656 . . . ? C1 Ni1 Ni5 Ni11 36.40(15) 2_656 . . . ? C1 Ni1 Ni5 Ni11 149.4(2) . . . . ? Ni5 Ni1 Ni5 Ni11 78.76(3) 2_656 . . . ? Ni2 Ni1 Ni5 Ni11 135.56(4) 2_656 . . . ? Ni2 Ni1 Ni5 Ni11 -40.90(3) . . . . ? C2 Ni1 Ni5 Ni3 162.23(19) . . . . ? C2 Ni1 Ni5 Ni3 -84.96(15) 2_656 . . . ? C4 Ni1 Ni5 Ni3 -17.8(2) 2_656 . . . ? C4 Ni1 Ni5 Ni3 95.85(15) . . . . ? C3 Ni1 Ni5 Ni3 7.80(16) . . . . ? C3 Ni1 Ni5 Ni3 119.6(2) 2_656 . . . ? C1 Ni1 Ni5 Ni3 -173.44(15) 2_656 . . . ? C1 Ni1 Ni5 Ni3 -60.4(2) . . . . ? Ni5 Ni1 Ni5 Ni3 -131.08(3) 2_656 . . . ? Ni2 Ni1 Ni5 Ni3 -74.28(3) 2_656 . . . ? Ni2 Ni1 Ni5 Ni3 109.26(3) . . . . ? C2 Ni1 Ni5 Ni2 52.97(19) . . . . ? C2 Ni1 Ni5 Ni2 165.78(15) 2_656 . . . ? C4 Ni1 Ni5 Ni2 -127.1(2) 2_656 . . . ? C4 Ni1 Ni5 Ni2 -13.41(15) . . . . ? C3 Ni1 Ni5 Ni2 -101.46(16) . . . . ? C3 Ni1 Ni5 Ni2 10.3(2) 2_656 . . . ? C1 Ni1 Ni5 Ni2 77.30(15) 2_656 . . . ? C1 Ni1 Ni5 Ni2 -169.7(2) . . . . ? Ni5 Ni1 Ni5 Ni2 119.66(3) 2_656 . . . ? Ni2 Ni1 Ni5 Ni2 176.46(4) 2_656 . . . ? C2 Ni1 Ni5 Ni8 -96.29(19) . . . 2_656 ? C2 Ni1 Ni5 Ni8 16.52(15) 2_656 . . 2_656 ? C4 Ni1 Ni5 Ni8 83.7(2) 2_656 . . 2_656 ? C4 Ni1 Ni5 Ni8 -162.67(15) . . . 2_656 ? C3 Ni1 Ni5 Ni8 109.28(16) . . . 2_656 ? C3 Ni1 Ni5 Ni8 -139.0(2) 2_656 . . 2_656 ? C1 Ni1 Ni5 Ni8 -71.96(15) 2_656 . . 2_656 ? C1 Ni1 Ni5 Ni8 41.1(2) . . . 2_656 ? Ni5 Ni1 Ni5 Ni8 -29.600(18) 2_656 . . 2_656 ? Ni2 Ni1 Ni5 Ni8 27.20(4) 2_656 . . 2_656 ? Ni2 Ni1 Ni5 Ni8 -149.26(3) . . . 2_656 ? C2 Ni1 Ni5 Ni8 -37.95(19) . . . . ? C2 Ni1 Ni5 Ni8 74.86(15) 2_656 . . . ? C4 Ni1 Ni5 Ni8 142.0(2) 2_656 . . . ? C4 Ni1 Ni5 Ni8 -104.33(15) . . . . ? C3 Ni1 Ni5 Ni8 167.62(16) . . . . ? C3 Ni1 Ni5 Ni8 -80.6(2) 2_656 . . . ? C1 Ni1 Ni5 Ni8 -13.62(15) 2_656 . . . ? C1 Ni1 Ni5 Ni8 99.4(2) . . . . ? Ni5 Ni1 Ni5 Ni8 28.739(17) 2_656 . . . ? Ni2 Ni1 Ni5 Ni8 85.54(4) 2_656 . . . ? Ni2 Ni1 Ni5 Ni8 -90.92(3) . . . . ? C17 Ni2 Ni5 C8 -16.5(4) . . . . ? C2 Ni2 Ni5 C8 125.3(3) . . . . ? C4 Ni2 Ni5 C8 -153.4(3) . . . . ? Ni12 Ni2 Ni5 C8 -106.7(3) . . . . ? Ni11 Ni2 Ni5 C8 61.5(3) . . . . ? Ni1 Ni2 Ni5 C8 -168.1(3) . . . . ? Ni4 Ni2 Ni5 C8 -113.3(3) . . . . ? Ni6 Ni2 Ni5 C8 110.8(3) . . . . ? Ni7 Ni2 Ni5 C8 159.7(3) . . . . ? C17 Ni2 Ni5 C1 142.4(4) . . . . ? C2 Ni2 Ni5 C1 -75.8(3) . . . . ? C4 Ni2 Ni5 C1 5.5(3) . . . . ? Ni12 Ni2 Ni5 C1 52.2(2) . . . . ? Ni11 Ni2 Ni5 C1 -139.63(19) . . . . ? Ni1 Ni2 Ni5 C1 -9.20(19) . . . . ? Ni4 Ni2 Ni5 C1 45.62(19) . . . . ? Ni6 Ni2 Ni5 C1 -90.31(19) . . . . ? Ni7 Ni2 Ni5 C1 -41.4(2) . . . . ? C17 Ni2 Ni5 C2 -141.8(4) . . . . ? C4 Ni2 Ni5 C2 81.3(3) . . . . ? Ni12 Ni2 Ni5 C2 127.9(2) . . . . ? Ni11 Ni2 Ni5 C2 -63.8(2) . . . . ? Ni1 Ni2 Ni5 C2 66.6(2) . . . . ? Ni4 Ni2 Ni5 C2 121.4(2) . . . . ? Ni6 Ni2 Ni5 C2 -14.5(2) . . . . ? Ni7 Ni2 Ni5 C2 34.4(2) . . . . ? C17 Ni2 Ni5 Ni9 89.0(4) . . . . ? C2 Ni2 Ni5 Ni9 -129.2(2) . . . . ? C4 Ni2 Ni5 Ni9 -47.90(19) . . . . ? Ni12 Ni2 Ni5 Ni9 -1.27(13) . . . . ? Ni11 Ni2 Ni5 Ni9 166.94(8) . . . . ? Ni1 Ni2 Ni5 Ni9 -62.63(7) . . . . ? Ni4 Ni2 Ni5 Ni9 -7.80(8) . . . . ? Ni6 Ni2 Ni5 Ni9 -143.74(7) . . . . ? Ni7 Ni2 Ni5 Ni9 -94.78(9) . . . . ? C17 Ni2 Ni5 Ni11 -78.0(4) . . . . ? C2 Ni2 Ni5 Ni11 63.8(2) . . . . ? C4 Ni2 Ni5 Ni11 145.15(18) . . . . ? Ni12 Ni2 Ni5 Ni11 -168.21(8) . . . . ? Ni1 Ni2 Ni5 Ni11 130.43(4) . . . . ? Ni4 Ni2 Ni5 Ni11 -174.74(4) . . . . ? Ni6 Ni2 Ni5 Ni11 49.32(3) . . . . ? Ni7 Ni2 Ni5 Ni11 98.28(6) . . . . ? C17 Ni2 Ni5 Ni3 96.3(3) . . . . ? C2 Ni2 Ni5 Ni3 -121.9(2) . . . . ? C4 Ni2 Ni5 Ni3 -40.60(17) . . . . ? Ni12 Ni2 Ni5 Ni3 6.03(8) . . . . ? Ni11 Ni2 Ni5 Ni3 174.24(4) . . . . ? Ni1 Ni2 Ni5 Ni3 -55.32(3) . . . . ? Ni4 Ni2 Ni5 Ni3 -0.50(3) . . . . ? Ni6 Ni2 Ni5 Ni3 -136.44(3) . . . . ? Ni7 Ni2 Ni5 Ni3 -87.48(6) . . . . ? C17 Ni2 Ni5 Ni1 151.6(4) . . . . ? C2 Ni2 Ni5 Ni1 -66.6(2) . . . . ? C4 Ni2 Ni5 Ni1 14.72(17) . . . . ? Ni12 Ni2 Ni5 Ni1 61.36(7) . . . . ? Ni11 Ni2 Ni5 Ni1 -130.43(4) . . . . ? Ni4 Ni2 Ni5 Ni1 54.82(3) . . . . ? Ni6 Ni2 Ni5 Ni1 -81.11(3) . . . . ? Ni7 Ni2 Ni5 Ni1 -32.15(5) . . . . ? C17 Ni2 Ni5 Ni8 -162.7(3) . . . 2_656 ? C2 Ni2 Ni5 Ni8 -20.9(2) . . . 2_656 ? C4 Ni2 Ni5 Ni8 60.45(18) . . . 2_656 ? Ni12 Ni2 Ni5 Ni8 107.08(8) . . . 2_656 ? Ni11 Ni2 Ni5 Ni8 -84.71(5) . . . 2_656 ? Ni1 Ni2 Ni5 Ni8 45.73(5) . . . 2_656 ? Ni4 Ni2 Ni5 Ni8 100.55(5) . . . 2_656 ? Ni6 Ni2 Ni5 Ni8 -35.39(6) . . . 2_656 ? Ni7 Ni2 Ni5 Ni8 13.57(9) . . . 2_656 ? C17 Ni2 Ni5 Ni8 -124.3(3) . . . . ? C2 Ni2 Ni5 Ni8 17.5(2) . . . . ? C4 Ni2 Ni5 Ni8 98.80(17) . . . . ? Ni12 Ni2 Ni5 Ni8 145.44(7) . . . . ? Ni11 Ni2 Ni5 Ni8 -46.35(3) . . . . ? Ni1 Ni2 Ni5 Ni8 84.08(3) . . . . ? Ni4 Ni2 Ni5 Ni8 138.90(3) . . . . ? Ni6 Ni2 Ni5 Ni8 2.97(3) . . . . ? Ni7 Ni2 Ni5 Ni8 51.93(6) . . . . ? C17 Ni2 Ni6 C11 -7.2(4) . . . . ? C2 Ni2 Ni6 C11 -145.8(3) . . . . ? C4 Ni2 Ni6 C11 117.4(3) . . . . ? Ni12 Ni2 Ni6 C11 69.0(2) . . . . ? Ni11 Ni2 Ni6 C11 -84.2(2) . . . . ? Ni5 Ni2 Ni6 C11 -131.0(2) . . . . ? Ni1 Ni2 Ni6 C11 170.1(2) . . . . ? Ni4 Ni2 Ni6 C11 131.5(2) . . . . ? Ni7 Ni2 Ni6 C11 85.7(2) . . . . ? C17 Ni2 Ni6 C19 -152.8(15) . . . 2_656 ? C2 Ni2 Ni6 C19 68.6(15) . . . 2_656 ? C4 Ni2 Ni6 C19 -28.2(15) . . . 2_656 ? Ni12 Ni2 Ni6 C19 -76.5(15) . . . 2_656 ? Ni11 Ni2 Ni6 C19 130.2(15) . . . 2_656 ? Ni5 Ni2 Ni6 C19 83.4(15) . . . 2_656 ? Ni1 Ni2 Ni6 C19 24.5(15) . . . 2_656 ? Ni4 Ni2 Ni6 C19 -14.1(15) . . . 2_656 ? Ni7 Ni2 Ni6 C19 -59.9(15) . . . 2_656 ? C17 Ni2 Ni6 C1 166.2(4) . . . 2_656 ? C2 Ni2 Ni6 C1 27.6(3) . . . 2_656 ? C4 Ni2 Ni6 C1 -69.3(2) . . . 2_656 ? Ni12 Ni2 Ni6 C1 -117.57(17) . . . 2_656 ? Ni11 Ni2 Ni6 C1 89.22(17) . . . 2_656 ? Ni5 Ni2 Ni6 C1 42.42(17) . . . 2_656 ? Ni1 Ni2 Ni6 C1 -16.48(17) . . . 2_656 ? Ni4 Ni2 Ni6 C1 -55.16(17) . . . 2_656 ? Ni7 Ni2 Ni6 C1 -100.93(17) . . . 2_656 ? C17 Ni2 Ni6 C2 138.6(4) . . . . ? C4 Ni2 Ni6 C2 -96.9(3) . . . . ? Ni12 Ni2 Ni6 C2 -145.2(2) . . . . ? Ni11 Ni2 Ni6 C2 61.6(2) . . . . ? Ni5 Ni2 Ni6 C2 14.8(2) . . . . ? Ni1 Ni2 Ni6 C2 -44.1(2) . . . . ? Ni4 Ni2 Ni6 C2 -82.8(2) . . . . ? Ni7 Ni2 Ni6 C2 -128.6(2) . . . . ? C17 Ni2 Ni6 Ni9 169.6(3) . . . 2_656 ? C2 Ni2 Ni6 Ni9 31.0(2) . . . 2_656 ? C4 Ni2 Ni6 Ni9 -65.83(16) . . . 2_656 ? Ni12 Ni2 Ni6 Ni9 -114.15(5) . . . 2_656 ? Ni11 Ni2 Ni6 Ni9 92.65(5) . . . 2_656 ? Ni5 Ni2 Ni6 Ni9 45.84(5) . . . 2_656 ? Ni1 Ni2 Ni6 Ni9 -13.06(5) . . . 2_656 ? Ni4 Ni2 Ni6 Ni9 -51.74(7) . . . 2_656 ? Ni7 Ni2 Ni6 Ni9 -97.51(5) . . . 2_656 ? C17 Ni2 Ni6 Ni11 77.0(3) . . . . ? C2 Ni2 Ni6 Ni11 -61.6(2) . . . . ? C4 Ni2 Ni6 Ni11 -158.48(16) . . . . ? Ni12 Ni2 Ni6 Ni11 153.20(4) . . . . ? Ni5 Ni2 Ni6 Ni11 -46.80(3) . . . . ? Ni1 Ni2 Ni6 Ni11 -105.70(4) . . . . ? Ni4 Ni2 Ni6 Ni11 -144.38(6) . . . . ? Ni7 Ni2 Ni6 Ni11 169.85(4) . . . . ? C17 Ni2 Ni6 Ni7 -92.9(3) . . . . ? C2 Ni2 Ni6 Ni7 128.6(2) . . . . ? C4 Ni2 Ni6 Ni7 31.67(16) . . . . ? Ni12 Ni2 Ni6 Ni7 -16.64(4) . . . . ? Ni11 Ni2 Ni6 Ni7 -169.85(4) . . . . ? Ni5 Ni2 Ni6 Ni7 143.35(4) . . . . ? Ni1 Ni2 Ni6 Ni7 84.45(3) . . . . ? Ni4 Ni2 Ni6 Ni7 45.77(5) . . . . ? C17 Ni2 Ni6 Ni8 120.9(3) . . . . ? C2 Ni2 Ni6 Ni8 -17.7(2) . . . . ? C4 Ni2 Ni6 Ni8 -114.61(16) . . . . ? Ni12 Ni2 Ni6 Ni8 -162.92(4) . . . . ? Ni11 Ni2 Ni6 Ni8 43.87(3) . . . . ? Ni5 Ni2 Ni6 Ni8 -2.93(3) . . . . ? Ni1 Ni2 Ni6 Ni8 -61.83(3) . . . . ? Ni4 Ni2 Ni6 Ni8 -100.51(5) . . . . ? Ni7 Ni2 Ni6 Ni8 -146.28(4) . . . . ? C17 Ni2 Ni6 Ni3 -149.1(3) . . . 2_656 ? C2 Ni2 Ni6 Ni3 72.3(2) . . . 2_656 ? C4 Ni2 Ni6 Ni3 -24.55(16) . . . 2_656 ? Ni12 Ni2 Ni6 Ni3 -72.87(4) . . . 2_656 ? Ni11 Ni2 Ni6 Ni3 133.93(3) . . . 2_656 ? Ni5 Ni2 Ni6 Ni3 87.13(3) . . . 2_656 ? Ni1 Ni2 Ni6 Ni3 28.23(3) . . . 2_656 ? Ni4 Ni2 Ni6 Ni3 -10.45(6) . . . 2_656 ? Ni7 Ni2 Ni6 Ni3 -56.22(3) . . . 2_656 ? C11 Ni6 Ni7 C12 77.8(4) . . . . ? C19 Ni6 Ni7 C12 -20.0(3) 2_656 . . . ? C1 Ni6 Ni7 C12 -121.9(3) 2_656 . . . ? C2 Ni6 Ni7 C12 -160.0(3) . . . . ? Ni9 Ni6 Ni7 C12 -73.3(3) 2_656 . . . ? Ni11 Ni6 Ni7 C12 158.8(3) . . . . ? Ni2 Ni6 Ni7 C12 168.0(3) . . . . ? Ni8 Ni6 Ni7 C12 -141.5(3) . . . . ? Ni3 Ni6 Ni7 C12 -90.0(3) 2_656 . . . ? C11 Ni6 Ni7 C13 -19.2(3) . . . . ? C19 Ni6 Ni7 C13 -116.9(3) 2_656 . . . ? C1 Ni6 Ni7 C13 141.1(3) 2_656 . . . ? C2 Ni6 Ni7 C13 103.1(3) . . . . ? Ni9 Ni6 Ni7 C13 -170.2(2) 2_656 . . . ? Ni11 Ni6 Ni7 C13 61.9(2) . . . . ? Ni2 Ni6 Ni7 C13 71.0(2) . . . . ? Ni8 Ni6 Ni7 C13 121.5(2) . . . . ? Ni3 Ni6 Ni7 C13 173.0(2) 2_656 . . . ? C11 Ni6 Ni7 C4 -121.9(3) . . . . ? C19 Ni6 Ni7 C4 140.3(3) 2_656 . . . ? C1 Ni6 Ni7 C4 38.4(2) 2_656 . . . ? C2 Ni6 Ni7 C4 0.3(2) . . . . ? Ni9 Ni6 Ni7 C4 87.02(17) 2_656 . . . ? Ni11 Ni6 Ni7 C4 -40.86(17) . . . . ? Ni2 Ni6 Ni7 C4 -31.70(17) . . . . ? Ni8 Ni6 Ni7 C4 18.79(18) . . . . ? Ni3 Ni6 Ni7 C4 70.28(17) 2_656 . . . ? C11 Ni6 Ni7 C3 -160.4(3) . . . 2_656 ? C19 Ni6 Ni7 C3 101.9(3) 2_656 . . 2_656 ? C1 Ni6 Ni7 C3 -0.1(2) 2_656 . . 2_656 ? C2 Ni6 Ni7 C3 -38.1(2) . . . 2_656 ? Ni9 Ni6 Ni7 C3 48.60(17) 2_656 . . 2_656 ? Ni11 Ni6 Ni7 C3 -79.28(17) . . . 2_656 ? Ni2 Ni6 Ni7 C3 -70.12(17) . . . 2_656 ? Ni8 Ni6 Ni7 C3 -19.63(18) . . . 2_656 ? Ni3 Ni6 Ni7 C3 31.86(17) 2_656 . . 2_656 ? C11 Ni6 Ni7 Ni12 -72.7(2) . . . . ? C19 Ni6 Ni7 Ni12 -170.4(2) 2_656 . . . ? C1 Ni6 Ni7 Ni12 87.66(16) 2_656 . . . ? C2 Ni6 Ni7 Ni12 49.62(16) . . . . ? Ni9 Ni6 Ni7 Ni12 136.32(4) 2_656 . . . ? Ni11 Ni6 Ni7 Ni12 8.44(5) . . . . ? Ni2 Ni6 Ni7 Ni12 17.59(4) . . . . ? Ni8 Ni6 Ni7 Ni12 68.08(6) . . . . ? Ni3 Ni6 Ni7 Ni12 119.58(4) 2_656 . . . ? C11 Ni6 Ni7 Ni13 158.3(2) . . . 2_656 ? C19 Ni6 Ni7 Ni13 60.5(2) 2_656 . . 2_656 ? C1 Ni6 Ni7 Ni13 -41.42(16) 2_656 . . 2_656 ? C2 Ni6 Ni7 Ni13 -79.46(16) . . . 2_656 ? Ni9 Ni6 Ni7 Ni13 7.24(5) 2_656 . . 2_656 ? Ni11 Ni6 Ni7 Ni13 -120.64(4) . . . 2_656 ? Ni2 Ni6 Ni7 Ni13 -111.48(4) . . . 2_656 ? Ni8 Ni6 Ni7 Ni13 -60.99(6) . . . 2_656 ? Ni3 Ni6 Ni7 Ni13 -9.50(4) 2_656 . . 2_656 ? C11 Ni6 Ni7 Ni3 167.8(2) . . . 2_656 ? C19 Ni6 Ni7 Ni3 70.0(2) 2_656 . . 2_656 ? C1 Ni6 Ni7 Ni3 -31.92(15) 2_656 . . 2_656 ? C2 Ni6 Ni7 Ni3 -69.96(16) . . . 2_656 ? Ni9 Ni6 Ni7 Ni3 16.74(4) 2_656 . . 2_656 ? Ni11 Ni6 Ni7 Ni3 -111.14(4) . . . 2_656 ? Ni2 Ni6 Ni7 Ni3 -101.98(3) . . . 2_656 ? Ni8 Ni6 Ni7 Ni3 -51.49(5) . . . 2_656 ? C11 Ni6 Ni7 Ni2 -90.2(2) . . . . ? C19 Ni6 Ni7 Ni2 172.0(2) 2_656 . . . ? C1 Ni6 Ni7 Ni2 70.06(16) 2_656 . . . ? C2 Ni6 Ni7 Ni2 32.02(16) . . . . ? Ni9 Ni6 Ni7 Ni2 118.72(4) 2_656 . . . ? Ni11 Ni6 Ni7 Ni2 -9.16(3) . . . . ? Ni8 Ni6 Ni7 Ni2 50.49(5) . . . . ? Ni3 Ni6 Ni7 Ni2 101.98(3) 2_656 . . . ? C11 Ni6 Ni7 Ni10 -140.9(2) . . . . ? C19 Ni6 Ni7 Ni10 121.4(2) 2_656 . . . ? C1 Ni6 Ni7 Ni10 19.39(16) 2_656 . . . ? C2 Ni6 Ni7 Ni10 -18.65(17) . . . . ? Ni9 Ni6 Ni7 Ni10 68.05(6) 2_656 . . . ? Ni11 Ni6 Ni7 Ni10 -59.83(7) . . . . ? Ni2 Ni6 Ni7 Ni10 -50.67(5) . . . . ? Ni8 Ni6 Ni7 Ni10 -0.18(9) . . . . ? Ni3 Ni6 Ni7 Ni10 51.31(5) 2_656 . . . ? C17 Ni2 Ni7 C12 96.3(5) . . . . ? C2 Ni2 Ni7 C12 -54.5(4) . . . . ? C4 Ni2 Ni7 C12 -151.6(5) . . . . ? Ni12 Ni2 Ni7 C12 141.6(4) . . . . ? Ni11 Ni2 Ni7 C12 -8.3(4) . . . . ? Ni5 Ni2 Ni7 C12 -80.2(4) . . . . ? Ni1 Ni2 Ni7 C12 -107.8(4) . . . . ? Ni4 Ni2 Ni7 C12 -168.3(4) . . . . ? Ni6 Ni2 Ni7 C12 -18.5(4) . . . . ? C17 Ni2 Ni7 C13 -3.0(4) . . . . ? C2 Ni2 Ni7 C13 -153.8(3) . . . . ? C4 Ni2 Ni7 C13 109.2(3) . . . . ? Ni12 Ni2 Ni7 C13 42.4(2) . . . . ? Ni11 Ni2 Ni7 C13 -107.6(2) . . . . ? Ni5 Ni2 Ni7 C13 -179.4(2) . . . . ? Ni1 Ni2 Ni7 C13 152.9(2) . . . . ? Ni4 Ni2 Ni7 C13 92.5(2) . . . . ? Ni6 Ni2 Ni7 C13 -117.7(2) . . . . ? C17 Ni2 Ni7 C4 -112.2(4) . . . . ? C2 Ni2 Ni7 C4 97.1(3) . . . . ? Ni12 Ni2 Ni7 C4 -66.8(2) . . . . ? Ni11 Ni2 Ni7 C4 143.3(2) . . . . ? Ni5 Ni2 Ni7 C4 71.4(2) . . . . ? Ni1 Ni2 Ni7 C4 43.8(2) . . . . ? Ni4 Ni2 Ni7 C4 -16.7(2) . . . . ? Ni6 Ni2 Ni7 C4 133.1(2) . . . . ? C17 Ni2 Ni7 C3 -141.0(4) . . . 2_656 ? C2 Ni2 Ni7 C3 68.2(2) . . . 2_656 ? C4 Ni2 Ni7 C3 -28.9(3) . . . 2_656 ? Ni12 Ni2 Ni7 C3 -95.64(17) . . . 2_656 ? Ni11 Ni2 Ni7 C3 114.41(17) . . . 2_656 ? Ni5 Ni2 Ni7 C3 42.55(18) . . . 2_656 ? Ni1 Ni2 Ni7 C3 14.94(17) . . . 2_656 ? Ni4 Ni2 Ni7 C3 -45.52(17) . . . 2_656 ? Ni6 Ni2 Ni7 C3 104.27(17) . . . 2_656 ? C17 Ni2 Ni7 Ni12 -45.4(3) . . . . ? C2 Ni2 Ni7 Ni12 163.85(17) . . . . ? C4 Ni2 Ni7 Ni12 66.8(2) . . . . ? Ni11 Ni2 Ni7 Ni12 -149.94(5) . . . . ? Ni5 Ni2 Ni7 Ni12 138.19(6) . . . . ? Ni1 Ni2 Ni7 Ni12 110.58(4) . . . . ? Ni4 Ni2 Ni7 Ni12 50.12(3) . . . . ? Ni6 Ni2 Ni7 Ni12 -160.09(4) . . . . ? C17 Ni2 Ni7 Ni13 -139.3(3) . . . 2_656 ? C2 Ni2 Ni7 Ni13 69.88(17) . . . 2_656 ? C4 Ni2 Ni7 Ni13 -27.2(2) . . . 2_656 ? Ni12 Ni2 Ni7 Ni13 -93.97(5) . . . 2_656 ? Ni11 Ni2 Ni7 Ni13 116.08(5) . . . 2_656 ? Ni5 Ni2 Ni7 Ni13 44.21(7) . . . 2_656 ? Ni1 Ni2 Ni7 Ni13 16.61(5) . . . 2_656 ? Ni4 Ni2 Ni7 Ni13 -43.85(5) . . . 2_656 ? Ni6 Ni2 Ni7 Ni13 105.94(5) . . . 2_656 ? C17 Ni2 Ni7 Ni3 176.4(3) . . . 2_656 ? C2 Ni2 Ni7 Ni3 25.67(17) . . . 2_656 ? C4 Ni2 Ni7 Ni3 -71.4(2) . . . 2_656 ? Ni12 Ni2 Ni7 Ni3 -138.18(4) . . . 2_656 ? Ni11 Ni2 Ni7 Ni3 71.87(4) . . . 2_656 ? Ni5 Ni2 Ni7 Ni3 0.01(6) . . . 2_656 ? Ni1 Ni2 Ni7 Ni3 -27.60(3) . . . 2_656 ? Ni4 Ni2 Ni7 Ni3 -88.06(3) . . . 2_656 ? Ni6 Ni2 Ni7 Ni3 61.73(3) . . . 2_656 ? C17 Ni2 Ni7 Ni6 114.7(3) . . . . ? C2 Ni2 Ni7 Ni6 -36.06(17) . . . . ? C4 Ni2 Ni7 Ni6 -133.1(2) . . . . ? Ni12 Ni2 Ni7 Ni6 160.09(4) . . . . ? Ni11 Ni2 Ni7 Ni6 10.14(4) . . . . ? Ni5 Ni2 Ni7 Ni6 -61.72(5) . . . . ? Ni1 Ni2 Ni7 Ni6 -89.33(3) . . . . ? Ni4 Ni2 Ni7 Ni6 -149.79(4) . . . . ? C17 Ni2 Ni7 Ni10 -97.8(3) . . . . ? C2 Ni2 Ni7 Ni10 111.41(17) . . . . ? C4 Ni2 Ni7 Ni10 14.3(2) . . . . ? Ni12 Ni2 Ni7 Ni10 -52.45(3) . . . . ? Ni11 Ni2 Ni7 Ni10 157.61(4) . . . . ? Ni5 Ni2 Ni7 Ni10 85.74(6) . . . . ? Ni1 Ni2 Ni7 Ni10 58.14(3) . . . . ? Ni4 Ni2 Ni7 Ni10 -2.33(3) . . . . ? Ni6 Ni2 Ni7 Ni10 147.46(4) . . . . ? C8 Ni5 Ni8 C9 99.4(5) . . . . ? C1 Ni5 Ni8 C9 -53.3(4) . . . . ? C2 Ni5 Ni8 C9 -150.2(4) . . . . ? Ni9 Ni5 Ni8 C9 -6.4(4) . . . . ? Ni11 Ni5 Ni8 C9 143.1(4) . . . . ? Ni3 Ni5 Ni8 C9 -79.5(4) . . . . ? Ni1 Ni5 Ni8 C9 -107.0(4) . . . . ? Ni2 Ni5 Ni8 C9 -167.2(4) . . . . ? Ni8 Ni5 Ni8 C9 -18.5(4) 2_656 . . . ? C8 Ni5 Ni8 C10 -0.9(3) . . . . ? C1 Ni5 Ni8 C10 -153.7(3) . . . . ? C2 Ni5 Ni8 C10 109.4(3) . . . . ? Ni9 Ni5 Ni8 C10 -106.8(2) . . . . ? Ni11 Ni5 Ni8 C10 42.7(2) . . . . ? Ni3 Ni5 Ni8 C10 -179.8(2) . . . . ? Ni1 Ni5 Ni8 C10 152.7(2) . . . . ? Ni2 Ni5 Ni8 C10 92.5(2) . . . . ? Ni8 Ni5 Ni8 C10 -118.9(2) 2_656 . . . ? C8 Ni5 Ni8 C2 -110.3(3) . . . . ? C1 Ni5 Ni8 C2 96.9(3) . . . . ? Ni9 Ni5 Ni8 C2 143.8(2) . . . . ? Ni11 Ni5 Ni8 C2 -66.7(2) . . . . ? Ni3 Ni5 Ni8 C2 70.8(2) . . . . ? Ni1 Ni5 Ni8 C2 43.3(2) . . . . ? Ni2 Ni5 Ni8 C2 -17.0(2) . . . . ? Ni8 Ni5 Ni8 C2 131.7(2) 2_656 . . . ? C8 Ni5 Ni8 C1 -139.0(3) . . . 2_656 ? C1 Ni5 Ni8 C1 68.2(2) . . . 2_656 ? C2 Ni5 Ni8 C1 -28.7(3) . . . 2_656 ? Ni9 Ni5 Ni8 C1 115.09(16) . . . 2_656 ? Ni11 Ni5 Ni8 C1 -95.43(16) . . . 2_656 ? Ni3 Ni5 Ni8 C1 42.04(17) . . . 2_656 ? Ni1 Ni5 Ni8 C1 14.56(16) . . . 2_656 ? Ni2 Ni5 Ni8 C1 -45.67(16) . . . 2_656 ? Ni8 Ni5 Ni8 C1 102.98(16) 2_656 . . 2_656 ? C8 Ni5 Ni8 Ni11 -43.6(3) . . . . ? C1 Ni5 Ni8 Ni11 163.65(17) . . . . ? C2 Ni5 Ni8 Ni11 66.7(2) . . . . ? Ni9 Ni5 Ni8 Ni11 -149.48(5) . . . . ? Ni3 Ni5 Ni8 Ni11 137.48(6) . . . . ? Ni1 Ni5 Ni8 Ni11 109.99(3) . . . . ? Ni2 Ni5 Ni8 Ni11 49.76(3) . . . . ? Ni8 Ni5 Ni8 Ni11 -161.59(4) 2_656 . . . ? C8 Ni5 Ni8 Ni9 -138.8(3) . . . 2_656 ? C1 Ni5 Ni8 Ni9 68.44(17) . . . 2_656 ? C2 Ni5 Ni8 Ni9 -28.5(2) . . . 2_656 ? Ni9 Ni5 Ni8 Ni9 115.32(4) . . . 2_656 ? Ni11 Ni5 Ni8 Ni9 -95.21(5) . . . 2_656 ? Ni3 Ni5 Ni8 Ni9 42.27(7) . . . 2_656 ? Ni1 Ni5 Ni8 Ni9 14.79(4) . . . 2_656 ? Ni2 Ni5 Ni8 Ni9 -45.45(4) . . . 2_656 ? Ni8 Ni5 Ni8 Ni9 103.20(5) 2_656 . . 2_656 ? C8 Ni5 Ni8 Ni8 118.0(3) . . . 2_656 ? C1 Ni5 Ni8 Ni8 -34.76(17) . . . 2_656 ? C2 Ni5 Ni8 Ni8 -131.7(2) . . . 2_656 ? Ni9 Ni5 Ni8 Ni8 12.11(4) . . . 2_656 ? Ni11 Ni5 Ni8 Ni8 161.59(4) . . . 2_656 ? Ni3 Ni5 Ni8 Ni8 -60.93(5) . . . 2_656 ? Ni1 Ni5 Ni8 Ni8 -88.42(3) . . . 2_656 ? Ni2 Ni5 Ni8 Ni8 -148.65(3) . . . 2_656 ? C8 Ni5 Ni8 Ni5 178.6(3) . . . 2_656 ? C1 Ni5 Ni8 Ni5 25.90(17) . . . 2_656 ? C2 Ni5 Ni8 Ni5 -71.0(2) . . . 2_656 ? Ni9 Ni5 Ni8 Ni5 72.78(5) . . . 2_656 ? Ni11 Ni5 Ni8 Ni5 -137.75(4) . . . 2_656 ? Ni3 Ni5 Ni8 Ni5 -0.27(6) . . . 2_656 ? Ni1 Ni5 Ni8 Ni5 -27.75(2) . . . 2_656 ? Ni2 Ni5 Ni8 Ni5 -87.99(3) . . . 2_656 ? Ni8 Ni5 Ni8 Ni5 60.66(3) 2_656 . . 2_656 ? C8 Ni5 Ni8 Ni6 -96.2(3) . . . . ? C1 Ni5 Ni8 Ni6 111.07(17) . . . . ? C2 Ni5 Ni8 Ni6 14.1(2) . . . . ? Ni9 Ni5 Ni8 Ni6 157.95(4) . . . . ? Ni11 Ni5 Ni8 Ni6 -52.58(3) . . . . ? Ni3 Ni5 Ni8 Ni6 84.90(6) . . . . ? Ni1 Ni5 Ni8 Ni6 57.42(3) . . . . ? Ni2 Ni5 Ni8 Ni6 -2.82(3) . . . . ? Ni8 Ni5 Ni8 Ni6 145.83(4) 2_656 . . . ? C11 Ni6 Ni8 C9 -106.1(4) . . . . ? C19 Ni6 Ni8 C9 -1.4(4) 2_656 . . . ? C1 Ni6 Ni8 C9 98.9(4) 2_656 . . . ? C2 Ni6 Ni8 C9 153.2(4) . . . . ? Ni9 Ni6 Ni8 C9 35.8(3) 2_656 . . . ? Ni11 Ni6 Ni8 C9 -143.5(3) . . . . ? Ni7 Ni6 Ni8 C9 126.7(3) . . . . ? Ni2 Ni6 Ni8 C9 170.1(3) . . . . ? Ni3 Ni6 Ni8 C9 85.2(3) 2_656 . . . ? C11 Ni6 Ni8 C10 0.7(4) . . . . ? C19 Ni6 Ni8 C10 105.3(3) 2_656 . . . ? C1 Ni6 Ni8 C10 -154.3(3) 2_656 . . . ? C2 Ni6 Ni8 C10 -100.1(3) . . . . ? Ni9 Ni6 Ni8 C10 142.6(2) 2_656 . . . ? Ni11 Ni6 Ni8 C10 -36.7(2) . . . . ? Ni7 Ni6 Ni8 C10 -126.6(2) . . . . ? Ni2 Ni6 Ni8 C10 -83.1(2) . . . . ? Ni3 Ni6 Ni8 C10 -168.0(2) 2_656 . . . ? C11 Ni6 Ni8 C2 100.7(4) . . . . ? C19 Ni6 Ni8 C2 -154.6(3) 2_656 . . . ? C1 Ni6 Ni8 C2 -54.2(3) 2_656 . . . ? Ni9 Ni6 Ni8 C2 -117.3(2) 2_656 . . . ? Ni11 Ni6 Ni8 C2 63.4(2) . . . . ? Ni7 Ni6 Ni8 C2 -26.5(2) . . . . ? Ni2 Ni6 Ni8 C2 16.9(2) . . . . ? Ni3 Ni6 Ni8 C2 -68.0(2) 2_656 . . . ? C11 Ni6 Ni8 C1 154.9(4) . . . 2_656 ? C19 Ni6 Ni8 C1 -100.4(3) 2_656 . . 2_656 ? C2 Ni6 Ni8 C1 54.2(3) . . . 2_656 ? Ni9 Ni6 Ni8 C1 -63.1(2) 2_656 . . 2_656 ? Ni11 Ni6 Ni8 C1 117.6(2) . . . 2_656 ? Ni7 Ni6 Ni8 C1 27.7(2) . . . 2_656 ? Ni2 Ni6 Ni8 C1 71.1(2) . . . 2_656 ? Ni3 Ni6 Ni8 C1 -13.7(2) 2_656 . . 2_656 ? C11 Ni6 Ni8 Ni11 37.3(3) . . . . ? C19 Ni6 Ni8 Ni11 142.0(2) 2_656 . . . ? C1 Ni6 Ni8 Ni11 -117.6(2) 2_656 . . . ? C2 Ni6 Ni8 Ni11 -63.4(2) . . . . ? Ni9 Ni6 Ni8 Ni11 179.28(4) 2_656 . . . ? Ni7 Ni6 Ni8 Ni11 -89.87(5) . . . . ? Ni2 Ni6 Ni8 Ni11 -46.47(3) . . . . ? Ni3 Ni6 Ni8 Ni11 -131.35(4) 2_656 . . . ? C11 Ni6 Ni8 Ni9 -142.0(3) . . . 2_656 ? C19 Ni6 Ni8 Ni9 -37.3(2) 2_656 . . 2_656 ? C1 Ni6 Ni8 Ni9 63.1(2) 2_656 . . 2_656 ? C2 Ni6 Ni8 Ni9 117.3(2) . . . 2_656 ? Ni11 Ni6 Ni8 Ni9 -179.28(4) . . . 2_656 ? Ni7 Ni6 Ni8 Ni9 90.85(6) . . . 2_656 ? Ni2 Ni6 Ni8 Ni9 134.25(4) . . . 2_656 ? Ni3 Ni6 Ni8 Ni9 49.37(3) 2_656 . . 2_656 ? C11 Ni6 Ni8 Ni8 130.2(3) . . . 2_656 ? C19 Ni6 Ni8 Ni8 -125.1(2) 2_656 . . 2_656 ? C1 Ni6 Ni8 Ni8 -24.7(2) 2_656 . . 2_656 ? C2 Ni6 Ni8 Ni8 29.5(2) . . . 2_656 ? Ni9 Ni6 Ni8 Ni8 -87.80(7) 2_656 . . 2_656 ? Ni11 Ni6 Ni8 Ni8 92.92(7) . . . 2_656 ? Ni7 Ni6 Ni8 Ni8 3.04(10) . . . 2_656 ? Ni2 Ni6 Ni8 Ni8 46.45(7) . . . 2_656 ? Ni3 Ni6 Ni8 Ni8 -38.43(7) 2_656 . . 2_656 ? C11 Ni6 Ni8 Ni5 171.8(3) . . . 2_656 ? C19 Ni6 Ni8 Ni5 -83.5(2) 2_656 . . 2_656 ? C1 Ni6 Ni8 Ni5 16.9(2) 2_656 . . 2_656 ? C2 Ni6 Ni8 Ni5 71.1(2) . . . 2_656 ? Ni9 Ni6 Ni8 Ni5 -46.22(3) 2_656 . . 2_656 ? Ni11 Ni6 Ni8 Ni5 134.50(4) . . . 2_656 ? Ni7 Ni6 Ni8 Ni5 44.63(5) . . . 2_656 ? Ni2 Ni6 Ni8 Ni5 88.03(3) . . . 2_656 ? Ni3 Ni6 Ni8 Ni5 3.15(3) 2_656 . . 2_656 ? C11 Ni6 Ni8 Ni5 86.5(3) . . . . ? C19 Ni6 Ni8 Ni5 -168.8(2) 2_656 . . . ? C1 Ni6 Ni8 Ni5 -68.4(2) 2_656 . . . ? C2 Ni6 Ni8 Ni5 -14.2(2) . . . . ? Ni9 Ni6 Ni8 Ni5 -131.52(4) 2_656 . . . ? Ni11 Ni6 Ni8 Ni5 49.20(3) . . . . ? Ni7 Ni6 Ni8 Ni5 -40.67(6) . . . . ? Ni2 Ni6 Ni8 Ni5 2.73(3) . . . . ? Ni3 Ni6 Ni8 Ni5 -82.15(3) 2_656 . . . ? C8 Ni5 Ni9 C7 -14.7(4) . . . . ? C1 Ni5 Ni9 C7 168.7(3) . . . . ? C2 Ni5 Ni9 C7 150.4(4) . . . . ? Ni11 Ni5 Ni9 C7 35.2(3) . . . . ? Ni3 Ni5 Ni9 C7 -128.6(2) . . . . ? Ni1 Ni5 Ni9 C7 -172.0(2) . . . . ? Ni2 Ni5 Ni9 C7 -120.0(2) . . . . ? Ni8 Ni5 Ni9 C7 110.3(2) 2_656 . . . ? Ni8 Ni5 Ni9 C7 98.6(2) . . . . ? C8 Ni5 Ni9 C19 171.8(6) . . . . ? C1 Ni5 Ni9 C19 -4.8(6) . . . . ? C2 Ni5 Ni9 C19 -23.1(6) . . . . ? Ni11 Ni5 Ni9 C19 -138.2(5) . . . . ? Ni3 Ni5 Ni9 C19 58.0(5) . . . . ? Ni1 Ni5 Ni9 C19 14.5(5) . . . . ? Ni2 Ni5 Ni9 C19 66.6(5) . . . . ? Ni8 Ni5 Ni9 C19 -63.2(5) 2_656 . . . ? Ni8 Ni5 Ni9 C19 -74.9(5) . . . . ? C8 Ni5 Ni9 C1 176.6(3) . . . . ? C2 Ni5 Ni9 C1 -18.3(4) . . . . ? Ni11 Ni5 Ni9 C1 -133.5(2) . . . . ? Ni3 Ni5 Ni9 C1 62.7(2) . . . . ? Ni1 Ni5 Ni9 C1 19.3(2) . . . . ? Ni2 Ni5 Ni9 C1 71.3(2) . . . . ? Ni8 Ni5 Ni9 C1 -58.4(2) 2_656 . . . ? Ni8 Ni5 Ni9 C1 -70.1(2) . . . . ? C8 Ni5 Ni9 Ni6 176.5(3) . . . 2_656 ? C1 Ni5 Ni9 Ni6 -0.1(2) . . . 2_656 ? C2 Ni5 Ni9 Ni6 -18.4(3) . . . 2_656 ? Ni11 Ni5 Ni9 Ni6 -133.58(9) . . . 2_656 ? Ni3 Ni5 Ni9 Ni6 62.62(4) . . . 2_656 ? Ni1 Ni5 Ni9 Ni6 19.21(5) . . . 2_656 ? Ni2 Ni5 Ni9 Ni6 71.23(8) . . . 2_656 ? Ni8 Ni5 Ni9 Ni6 -58.50(4) 2_656 . . 2_656 ? Ni8 Ni5 Ni9 Ni6 -70.20(5) . . . 2_656 ? C8 Ni5 Ni9 Ni3 113.9(3) . . . . ? C1 Ni5 Ni9 Ni3 -62.7(2) . . . . ? C2 Ni5 Ni9 Ni3 -81.0(3) . . . . ? Ni11 Ni5 Ni9 Ni3 163.80(10) . . . . ? Ni1 Ni5 Ni9 Ni3 -43.41(3) . . . . ? Ni2 Ni5 Ni9 Ni3 8.61(7) . . . . ? Ni8 Ni5 Ni9 Ni3 -121.12(3) 2_656 . . . ? Ni8 Ni5 Ni9 Ni3 -132.82(4) . . . . ? C8 Ni5 Ni9 Ni8 -125.0(3) . . . 2_656 ? C1 Ni5 Ni9 Ni8 58.4(2) . . . 2_656 ? C2 Ni5 Ni9 Ni8 40.1(3) . . . 2_656 ? Ni11 Ni5 Ni9 Ni8 -75.08(9) . . . 2_656 ? Ni3 Ni5 Ni9 Ni8 121.12(3) . . . 2_656 ? Ni1 Ni5 Ni9 Ni8 77.71(3) . . . 2_656 ? Ni2 Ni5 Ni9 Ni8 129.73(8) . . . 2_656 ? Ni8 Ni5 Ni9 Ni8 -11.70(4) . . . 2_656 ? C6 Ni3 Ni9 C7 -20.0(4) . . . . ? C3 Ni3 Ni9 C7 174.1(4) . . . . ? C1 Ni3 Ni9 C7 143.8(4) . . . . ? Ni13 Ni3 Ni9 C7 -77.4(3) . . . . ? Ni5 Ni3 Ni9 C7 87.8(3) . . . . ? Ni1 Ni3 Ni9 C7 130.7(3) . . . . ? Ni4 Ni3 Ni9 C7 80.1(3) . . . . ? Ni7 Ni3 Ni9 C7 -140.2(3) 2_656 . . . ? Ni6 Ni3 Ni9 C7 -157.2(3) 2_656 . . . ? C6 Ni3 Ni9 C19 95.0(3) . . . . ? C3 Ni3 Ni9 C19 -70.9(4) . . . . ? C1 Ni3 Ni9 C19 -101.2(3) . . . . ? Ni13 Ni3 Ni9 C19 37.6(2) . . . . ? Ni5 Ni3 Ni9 C19 -157.3(2) . . . . ? Ni1 Ni3 Ni9 C19 -114.3(2) . . . . ? Ni4 Ni3 Ni9 C19 -164.9(2) . . . . ? Ni7 Ni3 Ni9 C19 -25.2(2) 2_656 . . . ? Ni6 Ni3 Ni9 C19 -42.3(2) 2_656 . . . ? C6 Ni3 Ni9 C1 -163.8(3) . . . . ? C3 Ni3 Ni9 C1 30.3(4) . . . . ? Ni13 Ni3 Ni9 C1 138.8(2) . . . . ? Ni5 Ni3 Ni9 C1 -56.0(2) . . . . ? Ni1 Ni3 Ni9 C1 -13.0(2) . . . . ? Ni4 Ni3 Ni9 C1 -63.6(2) . . . . ? Ni7 Ni3 Ni9 C1 76.0(2) 2_656 . . . ? Ni6 Ni3 Ni9 C1 59.0(2) 2_656 . . . ? C6 Ni3 Ni9 Ni6 137.2(3) . . . 2_656 ? C3 Ni3 Ni9 Ni6 -28.7(3) . . . 2_656 ? C1 Ni3 Ni9 Ni6 -59.0(2) . . . 2_656 ? Ni13 Ni3 Ni9 Ni6 79.84(10) . . . 2_656 ? Ni5 Ni3 Ni9 Ni6 -115.00(4) . . . 2_656 ? Ni1 Ni3 Ni9 Ni6 -72.02(3) . . . 2_656 ? Ni4 Ni3 Ni9 Ni6 -122.61(7) . . . 2_656 ? Ni7 Ni3 Ni9 Ni6 17.04(4) 2_656 . . 2_656 ? C6 Ni3 Ni9 Ni5 -107.8(3) . . . . ? C3 Ni3 Ni9 Ni5 86.3(3) . . . . ? C1 Ni3 Ni9 Ni5 56.0(2) . . . . ? Ni13 Ni3 Ni9 Ni5 -165.17(10) . . . . ? Ni1 Ni3 Ni9 Ni5 42.98(3) . . . . ? Ni4 Ni3 Ni9 Ni5 -7.61(7) . . . . ? Ni7 Ni3 Ni9 Ni5 132.04(4) 2_656 . . . ? Ni6 Ni3 Ni9 Ni5 115.00(4) 2_656 . . . ? C6 Ni3 Ni9 Ni8 -160.4(3) . . . 2_656 ? C3 Ni3 Ni9 Ni8 33.7(3) . . . 2_656 ? C1 Ni3 Ni9 Ni8 3.4(2) . . . 2_656 ? Ni13 Ni3 Ni9 Ni8 142.17(9) . . . 2_656 ? Ni5 Ni3 Ni9 Ni8 -52.66(3) . . . 2_656 ? Ni1 Ni3 Ni9 Ni8 -9.68(4) . . . 2_656 ? Ni4 Ni3 Ni9 Ni8 -60.27(8) . . . 2_656 ? Ni7 Ni3 Ni9 Ni8 79.38(4) 2_656 . . 2_656 ? Ni6 Ni3 Ni9 Ni8 62.34(3) 2_656 . . 2_656 ? C15 Ni4 Ni10 C14 -7.4(4) . . . . ? C4 Ni4 Ni10 C14 -147.5(3) . . . . ? C3 Ni4 Ni10 C14 116.2(3) . . . . ? Ni13 Ni4 Ni10 C14 68.2(3) . . . . ? Ni12 Ni4 Ni10 C14 -87.0(3) . . . . ? Ni2 Ni4 Ni10 C14 -132.8(3) . . . . ? Ni1 Ni4 Ni10 C14 168.6(3) . . . . ? Ni3 Ni4 Ni10 C14 131.6(3) . . . . ? Ni10 Ni4 Ni10 C14 83.5(3) 2_656 . . . ? C15 Ni4 Ni10 C20 -159(2) . . . . ? C4 Ni4 Ni10 C20 61(2) . . . . ? C3 Ni4 Ni10 C20 -36(2) . . . . ? Ni13 Ni4 Ni10 C20 -84(2) . . . . ? Ni12 Ni4 Ni10 C20 121(2) . . . . ? Ni2 Ni4 Ni10 C20 75(2) . . . . ? Ni1 Ni4 Ni10 C20 17(2) . . . . ? Ni3 Ni4 Ni10 C20 -20(2) . . . . ? Ni10 Ni4 Ni10 C20 -68(2) 2_656 . . . ? C15 Ni4 Ni10 C3 167.5(4) . . . 2_656 ? C4 Ni4 Ni10 C3 27.5(3) . . . 2_656 ? C3 Ni4 Ni10 C3 -68.8(2) . . . 2_656 ? Ni13 Ni4 Ni10 C3 -116.85(17) . . . 2_656 ? Ni12 Ni4 Ni10 C3 87.96(17) . . . 2_656 ? Ni2 Ni4 Ni10 C3 42.11(17) . . . 2_656 ? Ni1 Ni4 Ni10 C3 -16.50(17) . . . 2_656 ? Ni3 Ni4 Ni10 C3 -53.43(17) . . . 2_656 ? Ni10 Ni4 Ni10 C3 -101.61(17) 2_656 . . 2_656 ? C15 Ni4 Ni10 C4 140.1(4) . . . . ? C3 Ni4 Ni10 C4 -96.3(3) . . . . ? Ni13 Ni4 Ni10 C4 -144.3(2) . . . . ? Ni12 Ni4 Ni10 C4 60.5(2) . . . . ? Ni2 Ni4 Ni10 C4 14.7(2) . . . . ? Ni1 Ni4 Ni10 C4 -44.0(2) . . . . ? Ni3 Ni4 Ni10 C4 -80.9(2) . . . . ? Ni10 Ni4 Ni10 C4 -129.1(2) 2_656 . . . ? C15 Ni4 Ni10 Ni13 170.7(3) . . . 2_656 ? C4 Ni4 Ni10 Ni13 30.7(2) . . . 2_656 ? C3 Ni4 Ni10 Ni13 -65.62(17) . . . 2_656 ? Ni13 Ni4 Ni10 Ni13 -113.64(4) . . . 2_656 ? Ni12 Ni4 Ni10 Ni13 91.17(5) . . . 2_656 ? Ni2 Ni4 Ni10 Ni13 45.32(5) . . . 2_656 ? Ni1 Ni4 Ni10 Ni13 -13.29(5) . . . 2_656 ? Ni3 Ni4 Ni10 Ni13 -50.22(8) . . . 2_656 ? Ni10 Ni4 Ni10 Ni13 -98.40(6) 2_656 . . 2_656 ? C15 Ni4 Ni10 Ni12 79.6(3) . . . . ? C4 Ni4 Ni10 Ni12 -60.5(2) . . . . ? C3 Ni4 Ni10 Ni12 -156.79(16) . . . . ? Ni13 Ni4 Ni10 Ni12 155.19(5) . . . . ? Ni2 Ni4 Ni10 Ni12 -45.85(3) . . . . ? Ni1 Ni4 Ni10 Ni12 -104.46(3) . . . . ? Ni3 Ni4 Ni10 Ni12 -141.39(6) . . . . ? Ni10 Ni4 Ni10 Ni12 170.43(4) 2_656 . . . ? C15 Ni4 Ni10 Ni10 -90.9(3) . . . 2_656 ? C4 Ni4 Ni10 Ni10 129.1(2) . . . 2_656 ? C3 Ni4 Ni10 Ni10 32.78(16) . . . 2_656 ? Ni13 Ni4 Ni10 Ni10 -15.24(3) . . . 2_656 ? Ni12 Ni4 Ni10 Ni10 -170.43(4) . . . 2_656 ? Ni2 Ni4 Ni10 Ni10 143.71(4) . . . 2_656 ? Ni1 Ni4 Ni10 Ni10 85.10(3) . . . 2_656 ? Ni3 Ni4 Ni10 Ni10 48.18(5) . . . 2_656 ? C15 Ni4 Ni10 Ni4 -147.1(3) . . . 2_656 ? C4 Ni4 Ni10 Ni4 72.9(2) . . . 2_656 ? C3 Ni4 Ni10 Ni4 -23.42(16) . . . 2_656 ? Ni13 Ni4 Ni10 Ni4 -71.43(5) . . . 2_656 ? Ni12 Ni4 Ni10 Ni4 133.37(3) . . . 2_656 ? Ni2 Ni4 Ni10 Ni4 87.52(3) . . . 2_656 ? Ni1 Ni4 Ni10 Ni4 28.91(2) . . . 2_656 ? Ni3 Ni4 Ni10 Ni4 -8.02(6) . . . 2_656 ? Ni10 Ni4 Ni10 Ni4 -56.19(3) 2_656 . . 2_656 ? C15 Ni4 Ni10 Ni7 123.0(3) . . . . ? C4 Ni4 Ni10 Ni7 -17.1(2) . . . . ? C3 Ni4 Ni10 Ni7 -113.40(16) . . . . ? Ni13 Ni4 Ni10 Ni7 -161.42(4) . . . . ? Ni12 Ni4 Ni10 Ni7 43.39(3) . . . . ? Ni2 Ni4 Ni10 Ni7 -2.46(3) . . . . ? Ni1 Ni4 Ni10 Ni7 -61.07(3) . . . . ? Ni3 Ni4 Ni10 Ni7 -98.00(5) . . . . ? Ni10 Ni4 Ni10 Ni7 -146.17(3) 2_656 . . . ? C12 Ni7 Ni10 C14 -108.5(5) . . . . ? C13 Ni7 Ni10 C14 -2.2(4) . . . . ? C4 Ni7 Ni10 C14 97.8(4) . . . . ? C3 Ni7 Ni10 C14 153.0(4) 2_656 . . . ? Ni12 Ni7 Ni10 C14 34.1(3) . . . . ? Ni13 Ni7 Ni10 C14 -144.0(3) 2_656 . . . ? Ni3 Ni7 Ni10 C14 169.6(3) 2_656 . . . ? Ni6 Ni7 Ni10 C14 124.9(3) . . . . ? Ni2 Ni7 Ni10 C14 83.3(3) . . . . ? C12 Ni7 Ni10 C20 -3.1(4) . . . . ? C13 Ni7 Ni10 C20 103.2(3) . . . . ? C4 Ni7 Ni10 C20 -156.8(3) . . . . ? C3 Ni7 Ni10 C20 -101.6(3) 2_656 . . . ? Ni12 Ni7 Ni10 C20 139.5(2) . . . . ? Ni13 Ni7 Ni10 C20 -38.6(2) 2_656 . . . ? Ni3 Ni7 Ni10 C20 -85.0(2) 2_656 . . . ? Ni6 Ni7 Ni10 C20 -129.6(2) . . . . ? Ni2 Ni7 Ni10 C20 -171.3(2) . . . . ? C12 Ni7 Ni10 C3 98.5(4) . . . 2_656 ? C13 Ni7 Ni10 C3 -155.2(3) . . . 2_656 ? C4 Ni7 Ni10 C3 -55.2(3) . . . 2_656 ? Ni12 Ni7 Ni10 C3 -118.9(2) . . . 2_656 ? Ni13 Ni7 Ni10 C3 63.0(2) 2_656 . . 2_656 ? Ni3 Ni7 Ni10 C3 16.6(2) 2_656 . . 2_656 ? Ni6 Ni7 Ni10 C3 -28.0(2) . . . 2_656 ? Ni2 Ni7 Ni10 C3 -69.7(2) . . . 2_656 ? C12 Ni7 Ni10 C4 153.7(4) . . . . ? C13 Ni7 Ni10 C4 -100.0(3) . . . . ? C3 Ni7 Ni10 C4 55.2(3) 2_656 . . . ? Ni12 Ni7 Ni10 C4 -63.7(2) . . . . ? Ni13 Ni7 Ni10 C4 118.2(2) 2_656 . . . ? Ni3 Ni7 Ni10 C4 71.8(2) 2_656 . . . ? Ni6 Ni7 Ni10 C4 27.1(2) . . . . ? Ni2 Ni7 Ni10 C4 -14.5(2) . . . . ? C12 Ni7 Ni10 Ni13 35.4(3) . . . 2_656 ? C13 Ni7 Ni10 Ni13 141.7(2) . . . 2_656 ? C4 Ni7 Ni10 Ni13 -118.2(2) . . . 2_656 ? C3 Ni7 Ni10 Ni13 -63.0(2) 2_656 . . 2_656 ? Ni12 Ni7 Ni10 Ni13 178.06(4) . . . 2_656 ? Ni3 Ni7 Ni10 Ni13 -46.39(3) 2_656 . . 2_656 ? Ni6 Ni7 Ni10 Ni13 -91.08(6) . . . 2_656 ? Ni2 Ni7 Ni10 Ni13 -132.71(4) . . . 2_656 ? C12 Ni7 Ni10 Ni12 -142.6(3) . . . . ? C13 Ni7 Ni10 Ni12 -36.3(2) . . . . ? C4 Ni7 Ni10 Ni12 63.7(2) . . . . ? C3 Ni7 Ni10 Ni12 118.9(2) 2_656 . . . ? Ni13 Ni7 Ni10 Ni12 -178.06(4) 2_656 . . . ? Ni3 Ni7 Ni10 Ni12 135.55(4) 2_656 . . . ? Ni6 Ni7 Ni10 Ni12 90.86(6) . . . . ? Ni2 Ni7 Ni10 Ni12 49.24(3) . . . . ? C12 Ni7 Ni10 Ni4 170.5(3) . . . . ? C13 Ni7 Ni10 Ni4 -83.3(2) . . . . ? C4 Ni7 Ni10 Ni4 16.8(2) . . . . ? C3 Ni7 Ni10 Ni4 72.0(2) 2_656 . . . ? Ni12 Ni7 Ni10 Ni4 -46.93(3) . . . . ? Ni13 Ni7 Ni10 Ni4 135.01(4) 2_656 . . . ? Ni3 Ni7 Ni10 Ni4 88.62(3) 2_656 . . . ? Ni6 Ni7 Ni10 Ni4 43.93(6) . . . . ? Ni2 Ni7 Ni10 Ni4 2.30(3) . . . . ? C12 Ni7 Ni10 Ni10 127.0(3) . . . 2_656 ? C13 Ni7 Ni10 Ni10 -126.7(2) . . . 2_656 ? C4 Ni7 Ni10 Ni10 -26.6(2) . . . 2_656 ? C3 Ni7 Ni10 Ni10 28.5(2) 2_656 . . 2_656 ? Ni12 Ni7 Ni10 Ni10 -90.36(7) . . . 2_656 ? Ni13 Ni7 Ni10 Ni10 91.58(7) 2_656 . . 2_656 ? Ni3 Ni7 Ni10 Ni10 45.19(7) 2_656 . . 2_656 ? Ni6 Ni7 Ni10 Ni10 0.50(10) . . . 2_656 ? Ni2 Ni7 Ni10 Ni10 -41.13(7) . . . 2_656 ? C12 Ni7 Ni10 Ni4 84.8(3) . . . 2_656 ? C13 Ni7 Ni10 Ni4 -168.9(2) . . . 2_656 ? C4 Ni7 Ni10 Ni4 -68.9(2) . . . 2_656 ? C3 Ni7 Ni10 Ni4 -13.7(2) 2_656 . . 2_656 ? Ni12 Ni7 Ni10 Ni4 -132.59(4) . . . 2_656 ? Ni13 Ni7 Ni10 Ni4 49.36(3) 2_656 . . 2_656 ? Ni3 Ni7 Ni10 Ni4 2.96(3) 2_656 . . 2_656 ? Ni6 Ni7 Ni10 Ni4 -41.73(6) . . . 2_656 ? Ni2 Ni7 Ni10 Ni4 -83.35(3) . . . 2_656 ? C9 Ni8 Ni11 C18 6.4(7) . . . . ? C10 Ni8 Ni11 C18 20.5(6) . . . . ? C2 Ni8 Ni11 C18 -163.8(6) . . . . ? C1 Ni8 Ni11 C18 -147.2(6) 2_656 . . . ? Ni9 Ni8 Ni11 C18 -107.7(5) 2_656 . . . ? Ni8 Ni8 Ni11 C18 121.0(5) 2_656 . . . ? Ni5 Ni8 Ni11 C18 -167.7(5) 2_656 . . . ? Ni5 Ni8 Ni11 C18 138.1(5) . . . . ? Ni6 Ni8 Ni11 C18 -108.3(5) . . . . ? C9 Ni8 Ni11 C10 -14.1(6) . . . . ? C2 Ni8 Ni11 C10 175.7(3) . . . . ? C1 Ni8 Ni11 C10 -167.7(3) 2_656 . . . ? Ni9 Ni8 Ni11 C10 -128.2(3) 2_656 . . . ? Ni8 Ni8 Ni11 C10 100.5(3) 2_656 . . . ? Ni5 Ni8 Ni11 C10 171.8(3) 2_656 . . . ? Ni5 Ni8 Ni11 C10 117.6(3) . . . . ? Ni6 Ni8 Ni11 C10 -128.8(3) . . . . ? C9 Ni8 Ni11 C2 170.2(5) . . . . ? C10 Ni8 Ni11 C2 -175.7(3) . . . . ? C1 Ni8 Ni11 C2 16.6(2) 2_656 . . . ? Ni9 Ni8 Ni11 C2 56.1(2) 2_656 . . . ? Ni8 Ni8 Ni11 C2 -75.2(2) 2_656 . . . ? Ni5 Ni8 Ni11 C2 -3.9(2) 2_656 . . . ? Ni5 Ni8 Ni11 C2 -58.1(2) . . . . ? Ni6 Ni8 Ni11 C2 55.5(2) . . . . ? C9 Ni8 Ni11 C8 -103.8(5) . . . . ? C10 Ni8 Ni11 C8 -89.7(3) . . . . ? C2 Ni8 Ni11 C8 86.0(3) . . . . ? C1 Ni8 Ni11 C8 102.6(2) 2_656 . . . ? Ni9 Ni8 Ni11 C8 142.08(18) 2_656 . . . ? Ni8 Ni8 Ni11 C8 10.79(18) 2_656 . . . ? Ni5 Ni8 Ni11 C8 82.15(19) 2_656 . . . ? Ni5 Ni8 Ni11 C8 27.95(18) . . . . ? Ni6 Ni8 Ni11 C8 141.48(18) . . . . ? C9 Ni8 Ni11 Ni2 170.5(5) . . . . ? C10 Ni8 Ni11 Ni2 -175.4(3) . . . . ? C2 Ni8 Ni11 Ni2 0.3(2) . . . . ? C1 Ni8 Ni11 Ni2 16.91(15) 2_656 . . . ? Ni9 Ni8 Ni11 Ni2 56.39(5) 2_656 . . . ? Ni8 Ni8 Ni11 Ni2 -74.90(4) 2_656 . . . ? Ni5 Ni8 Ni11 Ni2 -3.54(6) 2_656 . . . ? Ni5 Ni8 Ni11 Ni2 -57.74(3) . . . . ? Ni6 Ni8 Ni11 Ni2 55.80(4) . . . . ? C9 Ni8 Ni11 Ni5 -131.7(5) . . . . ? C10 Ni8 Ni11 Ni5 -117.6(3) . . . . ? C2 Ni8 Ni11 Ni5 58.1(2) . . . . ? C1 Ni8 Ni11 Ni5 74.65(15) 2_656 . . . ? Ni9 Ni8 Ni11 Ni5 114.14(4) 2_656 . . . ? Ni8 Ni8 Ni11 Ni5 -17.16(3) 2_656 . . . ? Ni5 Ni8 Ni11 Ni5 54.21(5) 2_656 . . . ? Ni6 Ni8 Ni11 Ni5 113.54(4) . . . . ? C9 Ni8 Ni11 Ni6 114.7(5) . . . . ? C10 Ni8 Ni11 Ni6 128.8(3) . . . . ? C2 Ni8 Ni11 Ni6 -55.5(2) . . . . ? C1 Ni8 Ni11 Ni6 -38.89(15) 2_656 . . . ? Ni9 Ni8 Ni11 Ni6 0.60(4) 2_656 . . . ? Ni8 Ni8 Ni11 Ni6 -130.70(3) 2_656 . . . ? Ni5 Ni8 Ni11 Ni6 -59.33(4) 2_656 . . . ? Ni5 Ni8 Ni11 Ni6 -113.54(4) . . . . ? C17 Ni2 Ni11 C18 -9.1(5) . . . . ? C2 Ni2 Ni11 C18 171.4(4) . . . . ? C4 Ni2 Ni11 C18 155.2(4) . . . . ? Ni12 Ni2 Ni11 C18 39.6(3) . . . . ? Ni5 Ni2 Ni11 C18 -126.3(3) . . . . ? Ni1 Ni2 Ni11 C18 -168.5(3) . . . . ? Ni4 Ni2 Ni11 C18 -116.5(3) . . . . ? Ni6 Ni2 Ni11 C18 112.9(3) . . . . ? Ni7 Ni2 Ni11 C18 103.1(3) . . . . ? C17 Ni2 Ni11 C10 171.4(6) . . . . ? C2 Ni2 Ni11 C10 -8.1(5) . . . . ? C4 Ni2 Ni11 C10 -24.3(6) . . . . ? Ni12 Ni2 Ni11 C10 -140.0(5) . . . . ? Ni5 Ni2 Ni11 C10 54.2(5) . . . . ? Ni1 Ni2 Ni11 C10 12.0(5) . . . . ? Ni4 Ni2 Ni11 C10 64.0(5) . . . . ? Ni6 Ni2 Ni11 C10 -66.6(5) . . . . ? Ni7 Ni2 Ni11 C10 -76.4(5) . . . . ? C17 Ni2 Ni11 C2 179.5(4) . . . . ? C4 Ni2 Ni11 C2 -16.1(4) . . . . ? Ni12 Ni2 Ni11 C2 -131.8(2) . . . . ? Ni5 Ni2 Ni11 C2 62.3(2) . . . . ? Ni1 Ni2 Ni11 C2 20.1(2) . . . . ? Ni4 Ni2 Ni11 C2 72.1(2) . . . . ? Ni6 Ni2 Ni11 C2 -58.5(2) . . . . ? Ni7 Ni2 Ni11 C2 -68.3(2) . . . . ? C17 Ni2 Ni11 Ni8 179.2(4) . . . . ? C2 Ni2 Ni11 Ni8 -0.3(2) . . . . ? C4 Ni2 Ni11 Ni8 -16.5(3) . . . . ? Ni12 Ni2 Ni11 Ni8 -132.18(9) . . . . ? Ni5 Ni2 Ni11 Ni8 61.94(4) . . . . ? Ni1 Ni2 Ni11 Ni8 19.75(4) . . . . ? Ni4 Ni2 Ni11 Ni8 71.74(8) . . . . ? Ni6 Ni2 Ni11 Ni8 -58.82(4) . . . . ? Ni7 Ni2 Ni11 Ni8 -68.66(5) . . . . ? C17 Ni2 Ni11 C8 79.1(4) . . . . ? C2 Ni2 Ni11 C8 -100.5(3) . . . . ? C4 Ni2 Ni11 C8 -116.6(3) . . . . ? Ni12 Ni2 Ni11 C8 127.72(19) . . . . ? Ni5 Ni2 Ni11 C8 -38.17(17) . . . . ? Ni1 Ni2 Ni11 C8 -80.36(17) . . . . ? Ni4 Ni2 Ni11 C8 -28.36(18) . . . . ? Ni6 Ni2 Ni11 C8 -158.92(17) . . . . ? Ni7 Ni2 Ni11 C8 -168.76(17) . . . . ? C17 Ni2 Ni11 Ni5 117.2(4) . . . . ? C2 Ni2 Ni11 Ni5 -62.3(2) . . . . ? C4 Ni2 Ni11 Ni5 -78.4(3) . . . . ? Ni12 Ni2 Ni11 Ni5 165.89(10) . . . . ? Ni1 Ni2 Ni11 Ni5 -42.19(3) . . . . ? Ni4 Ni2 Ni11 Ni5 9.81(7) . . . . ? Ni6 Ni2 Ni11 Ni5 -120.75(3) . . . . ? Ni7 Ni2 Ni11 Ni5 -130.60(4) . . . . ? C17 Ni2 Ni11 Ni6 -122.0(4) . . . . ? C2 Ni2 Ni11 Ni6 58.5(2) . . . . ? C4 Ni2 Ni11 Ni6 42.3(3) . . . . ? Ni12 Ni2 Ni11 Ni6 -73.36(10) . . . . ? Ni5 Ni2 Ni11 Ni6 120.75(3) . . . . ? Ni1 Ni2 Ni11 Ni6 78.56(3) . . . . ? Ni4 Ni2 Ni11 Ni6 130.56(8) . . . . ? Ni7 Ni2 Ni11 Ni6 -9.84(4) . . . . ? C8 Ni5 Ni11 C18 -19.0(4) . . . . ? C1 Ni5 Ni11 C18 177.5(4) . . . . ? C2 Ni5 Ni11 C18 145.8(4) . . . . ? Ni9 Ni5 Ni11 C18 -74.0(4) . . . . ? Ni3 Ni5 Ni11 C18 80.1(3) . . . . ? Ni1 Ni5 Ni11 C18 133.2(3) . . . . ? Ni2 Ni5 Ni11 C18 90.7(3) . . . . ? Ni8 Ni5 Ni11 C18 -137.8(3) 2_656 . . . ? Ni8 Ni5 Ni11 C18 -154.2(3) . . . . ? C8 Ni5 Ni11 C10 92.1(4) . . . . ? C1 Ni5 Ni11 C10 -71.4(4) . . . . ? C2 Ni5 Ni11 C10 -103.1(3) . . . . ? Ni9 Ni5 Ni11 C10 37.1(2) . . . . ? Ni3 Ni5 Ni11 C10 -168.8(2) . . . . ? Ni1 Ni5 Ni11 C10 -115.7(2) . . . . ? Ni2 Ni5 Ni11 C10 -158.2(2) . . . . ? Ni8 Ni5 Ni11 C10 -26.7(2) 2_656 . . . ? Ni8 Ni5 Ni11 C10 -43.1(2) . . . . ? C8 Ni5 Ni11 C2 -164.9(3) . . . . ? C1 Ni5 Ni11 C2 31.7(4) . . . . ? Ni9 Ni5 Ni11 C2 140.1(2) . . . . ? Ni3 Ni5 Ni11 C2 -65.8(2) . . . . ? Ni1 Ni5 Ni11 C2 -12.7(2) . . . . ? Ni2 Ni5 Ni11 C2 -55.1(2) . . . . ? Ni8 Ni5 Ni11 C2 76.4(2) 2_656 . . . ? Ni8 Ni5 Ni11 C2 59.9(2) . . . . ? C8 Ni5 Ni11 Ni8 135.2(3) . . . . ? C1 Ni5 Ni11 Ni8 -28.3(3) . . . . ? C2 Ni5 Ni11 Ni8 -59.9(2) . . . . ? Ni9 Ni5 Ni11 Ni8 80.21(10) . . . . ? Ni3 Ni5 Ni11 Ni8 -125.71(7) . . . . ? Ni1 Ni5 Ni11 Ni8 -72.62(4) . . . . ? Ni2 Ni5 Ni11 Ni8 -115.05(4) . . . . ? Ni8 Ni5 Ni11 Ni8 16.46(4) 2_656 . . . ? C1 Ni5 Ni11 C8 -163.5(4) . . . . ? C2 Ni5 Ni11 C8 164.9(3) . . . . ? Ni9 Ni5 Ni11 C8 -55.0(3) . . . . ? Ni3 Ni5 Ni11 C8 99.1(3) . . . . ? Ni1 Ni5 Ni11 C8 152.2(3) . . . . ? Ni2 Ni5 Ni11 C8 109.8(3) . . . . ? Ni8 Ni5 Ni11 C8 -118.7(3) 2_656 . . . ? Ni8 Ni5 Ni11 C8 -135.2(3) . . . . ? C8 Ni5 Ni11 Ni2 -109.8(3) . . . . ? C1 Ni5 Ni11 Ni2 86.8(3) . . . . ? C2 Ni5 Ni11 Ni2 55.1(2) . . . . ? Ni9 Ni5 Ni11 Ni2 -164.74(10) . . . . ? Ni3 Ni5 Ni11 Ni2 -10.66(7) . . . . ? Ni1 Ni5 Ni11 Ni2 42.42(3) . . . . ? Ni8 Ni5 Ni11 Ni2 131.51(4) 2_656 . . . ? Ni8 Ni5 Ni11 Ni2 115.05(4) . . . . ? C8 Ni5 Ni11 Ni6 -162.9(3) . . . . ? C1 Ni5 Ni11 Ni6 33.7(3) . . . . ? C2 Ni5 Ni11 Ni6 2.0(2) . . . . ? Ni9 Ni5 Ni11 Ni6 142.15(9) . . . . ? Ni3 Ni5 Ni11 Ni6 -63.77(8) . . . . ? Ni1 Ni5 Ni11 Ni6 -10.68(4) . . . . ? Ni2 Ni5 Ni11 Ni6 -53.10(3) . . . . ? Ni8 Ni5 Ni11 Ni6 78.40(4) 2_656 . . . ? Ni8 Ni5 Ni11 Ni6 61.95(3) . . . . ? C11 Ni6 Ni11 C18 -3.7(4) . . . . ? C19 Ni6 Ni11 C18 93.0(4) 2_656 . . . ? C1 Ni6 Ni11 C18 -172.2(3) 2_656 . . . ? C2 Ni6 Ni11 C18 -151.2(4) . . . . ? Ni9 Ni6 Ni11 C18 146.7(3) 2_656 . . . ? Ni7 Ni6 Ni11 C18 -85.5(3) . . . . ? Ni2 Ni6 Ni11 C18 -95.6(3) . . . . ? Ni8 Ni6 Ni11 C18 147.4(3) . . . . ? Ni3 Ni6 Ni11 C18 -152.0(3) 2_656 . . . ? C11 Ni6 Ni11 C10 -113.5(3) . . . . ? C19 Ni6 Ni11 C10 -16.7(3) 2_656 . . . ? C1 Ni6 Ni11 C10 78.0(3) 2_656 . . . ? C2 Ni6 Ni11 C10 99.1(3) . . . . ? Ni9 Ni6 Ni11 C10 37.0(2) 2_656 . . . ? Ni7 Ni6 Ni11 C10 164.7(2) . . . . ? Ni2 Ni6 Ni11 C10 154.7(2) . . . . ? Ni8 Ni6 Ni11 C10 37.6(2) . . . . ? Ni3 Ni6 Ni11 C10 98.3(2) 2_656 . . . ? C11 Ni6 Ni11 C2 147.4(3) . . . . ? C19 Ni6 Ni11 C2 -115.8(3) 2_656 . . . ? C1 Ni6 Ni11 C2 -21.0(3) 2_656 . . . ? Ni9 Ni6 Ni11 C2 -62.1(2) 2_656 . . . ? Ni7 Ni6 Ni11 C2 65.6(2) . . . . ? Ni2 Ni6 Ni11 C2 55.6(2) . . . . ? Ni8 Ni6 Ni11 C2 -61.4(2) . . . . ? Ni3 Ni6 Ni11 C2 -0.8(2) 2_656 . . . ? C11 Ni6 Ni11 Ni8 -151.1(2) . . . . ? C19 Ni6 Ni11 Ni8 -54.4(3) 2_656 . . . ? C1 Ni6 Ni11 Ni8 40.40(16) 2_656 . . . ? C2 Ni6 Ni11 Ni8 61.4(2) . . . . ? Ni9 Ni6 Ni11 Ni8 -0.67(4) 2_656 . . . ? Ni7 Ni6 Ni11 Ni8 127.06(4) . . . . ? Ni2 Ni6 Ni11 Ni8 117.03(4) . . . . ? Ni3 Ni6 Ni11 Ni8 60.64(4) 2_656 . . . ? C11 Ni6 Ni11 C8 127.2(4) . . . . ? C19 Ni6 Ni11 C8 -136.0(4) 2_656 . . . ? C1 Ni6 Ni11 C8 -41.3(3) 2_656 . . . ? C2 Ni6 Ni11 C8 -20.2(4) . . . . ? Ni9 Ni6 Ni11 C8 -82.3(3) 2_656 . . . ? Ni7 Ni6 Ni11 C8 45.4(3) . . . . ? Ni2 Ni6 Ni11 C8 35.4(3) . . . . ? Ni8 Ni6 Ni11 C8 -81.7(3) . . . . ? Ni3 Ni6 Ni11 C8 -21.0(3) 2_656 . . . ? C11 Ni6 Ni11 Ni2 91.8(2) . . . . ? C19 Ni6 Ni11 Ni2 -171.4(3) 2_656 . . . ? C1 Ni6 Ni11 Ni2 -76.63(16) 2_656 . . . ? C2 Ni6 Ni11 Ni2 -55.6(2) . . . . ? Ni9 Ni6 Ni11 Ni2 -117.70(4) 2_656 . . . ? Ni7 Ni6 Ni11 Ni2 10.03(4) . . . . ? Ni8 Ni6 Ni11 Ni2 -117.03(4) . . . . ? Ni3 Ni6 Ni11 Ni2 -56.39(4) 2_656 . . . ? C11 Ni6 Ni11 Ni5 145.4(2) . . . . ? C19 Ni6 Ni11 Ni5 -117.9(3) 2_656 . . . ? C1 Ni6 Ni11 Ni5 -23.11(16) 2_656 . . . ? C2 Ni6 Ni11 Ni5 -2.1(2) . . . . ? Ni9 Ni6 Ni11 Ni5 -64.18(5) 2_656 . . . ? Ni7 Ni6 Ni11 Ni5 63.55(5) . . . . ? Ni2 Ni6 Ni11 Ni5 53.52(3) . . . . ? Ni8 Ni6 Ni11 Ni5 -63.51(4) . . . . ? Ni3 Ni6 Ni11 Ni5 -2.87(5) 2_656 . . . ? C12 Ni7 Ni12 C16 16.1(7) . . . . ? C13 Ni7 Ni12 C16 28.1(6) . . . . ? C4 Ni7 Ni12 C16 -156.0(6) . . . . ? C3 Ni7 Ni12 C16 -139.3(5) 2_656 . . . ? Ni13 Ni7 Ni12 C16 -99.4(5) 2_656 . . . ? Ni3 Ni7 Ni12 C16 -159.6(5) 2_656 . . . ? Ni6 Ni7 Ni12 C16 127.6(5) . . . . ? Ni2 Ni7 Ni12 C16 145.9(5) . . . . ? Ni10 Ni7 Ni12 C16 -101.0(5) . . . . ? C12 Ni7 Ni12 C13 -11.9(6) . . . . ? C4 Ni7 Ni12 C13 175.9(4) . . . . ? C3 Ni7 Ni12 C13 -167.3(3) 2_656 . . . ? Ni13 Ni7 Ni12 C13 -127.5(3) 2_656 . . . ? Ni3 Ni7 Ni12 C13 172.3(3) 2_656 . . . ? Ni6 Ni7 Ni12 C13 99.5(3) . . . . ? Ni2 Ni7 Ni12 C13 117.9(3) . . . . ? Ni10 Ni7 Ni12 C13 -129.1(3) . . . . ? C12 Ni7 Ni12 C4 172.2(6) . . . . ? C13 Ni7 Ni12 C4 -175.9(4) . . . . ? C3 Ni7 Ni12 C4 16.7(3) 2_656 . . . ? Ni13 Ni7 Ni12 C4 56.6(2) 2_656 . . . ? Ni3 Ni7 Ni12 C4 -3.6(2) 2_656 . . . ? Ni6 Ni7 Ni12 C4 -76.4(2) . . . . ? Ni2 Ni7 Ni12 C4 -58.0(2) . . . . ? Ni10 Ni7 Ni12 C4 55.0(2) . . . . ? C12 Ni7 Ni12 C17 -101.1(6) . . . . ? C13 Ni7 Ni12 C17 -89.2(4) . . . . ? C4 Ni7 Ni12 C17 86.7(3) . . . . ? C3 Ni7 Ni12 C17 103.4(3) 2_656 . . . ? Ni13 Ni7 Ni12 C17 143.3(2) 2_656 . . . ? Ni3 Ni7 Ni12 C17 83.1(2) 2_656 . . . ? Ni6 Ni7 Ni12 C17 10.3(2) . . . . ? Ni2 Ni7 Ni12 C17 28.7(2) . . . . ? Ni10 Ni7 Ni12 C17 141.7(2) . . . . ? C12 Ni7 Ni12 Ni2 -129.8(5) . . . . ? C13 Ni7 Ni12 Ni2 -117.9(3) . . . . ? C4 Ni7 Ni12 Ni2 58.0(2) . . . . ? C3 Ni7 Ni12 Ni2 74.79(16) 2_656 . . . ? Ni13 Ni7 Ni12 Ni2 114.67(4) 2_656 . . . ? Ni3 Ni7 Ni12 Ni2 54.45(5) 2_656 . . . ? Ni6 Ni7 Ni12 Ni2 -18.38(4) . . . . ? Ni10 Ni7 Ni12 Ni2 113.08(3) . . . . ? C12 Ni7 Ni12 Ni4 172.0(5) . . . . ? C13 Ni7 Ni12 Ni4 -176.0(3) . . . . ? C4 Ni7 Ni12 Ni4 -0.1(2) . . . . ? C3 Ni7 Ni12 Ni4 16.61(17) 2_656 . . . ? Ni13 Ni7 Ni12 Ni4 56.50(5) 2_656 . . . ? Ni3 Ni7 Ni12 Ni4 -3.73(6) 2_656 . . . ? Ni6 Ni7 Ni12 Ni4 -76.55(5) . . . . ? Ni2 Ni7 Ni12 Ni4 -58.17(3) . . . . ? Ni10 Ni7 Ni12 Ni4 54.90(4) . . . . ? C12 Ni7 Ni12 Ni10 117.1(5) . . . . ? C13 Ni7 Ni12 Ni10 129.1(3) . . . . ? C4 Ni7 Ni12 Ni10 -55.0(2) . . . . ? C3 Ni7 Ni12 Ni10 -38.29(16) 2_656 . . . ? Ni13 Ni7 Ni12 Ni10 1.60(4) 2_656 . . . ? Ni3 Ni7 Ni12 Ni10 -58.63(5) 2_656 . . . ? Ni6 Ni7 Ni12 Ni10 -131.45(4) . . . . ? Ni2 Ni7 Ni12 Ni10 -113.08(3) . . . . ? C17 Ni2 Ni12 C16 -24.5(5) . . . . ? C2 Ni2 Ni12 C16 174.8(4) . . . . ? C4 Ni2 Ni12 C16 142.2(4) . . . . ? Ni11 Ni2 Ni12 C16 -77.8(3) . . . . ? Ni5 Ni2 Ni12 C16 79.5(3) . . . . ? Ni1 Ni2 Ni12 C16 130.4(3) . . . . ? Ni4 Ni2 Ni12 C16 87.3(3) . . . . ? Ni6 Ni2 Ni12 C16 -140.1(3) . . . . ? Ni7 Ni2 Ni12 C16 -157.9(3) . . . . ? C17 Ni2 Ni12 C13 90.1(4) . . . . ? C2 Ni2 Ni12 C13 -70.6(4) . . . . ? C4 Ni2 Ni12 C13 -103.1(3) . . . . ? Ni11 Ni2 Ni12 C13 36.9(2) . . . . ? Ni5 Ni2 Ni12 C13 -165.8(2) . . . . ? Ni1 Ni2 Ni12 C13 -115.0(2) . . . . ? Ni4 Ni2 Ni12 C13 -158.1(2) . . . . ? Ni6 Ni2 Ni12 C13 -25.5(2) . . . . ? Ni7 Ni2 Ni12 C13 -43.3(2) . . . . ? C17 Ni2 Ni12 C4 -166.7(4) . . . . ? C2 Ni2 Ni12 C4 32.6(3) . . . . ? Ni11 Ni2 Ni12 C4 140.0(2) . . . . ? Ni5 Ni2 Ni12 C4 -62.7(2) . . . . ? Ni1 Ni2 Ni12 C4 -11.9(2) . . . . ? Ni4 Ni2 Ni12 C4 -54.9(2) . . . . ? Ni6 Ni2 Ni12 C4 77.7(2) . . . . ? Ni7 Ni2 Ni12 C4 59.9(2) . . . . ? C17 Ni2 Ni12 Ni7 133.4(4) . . . . ? C2 Ni2 Ni12 Ni7 -27.3(3) . . . . ? C4 Ni2 Ni12 Ni7 -59.9(2) . . . . ? Ni11 Ni2 Ni12 Ni7 80.17(10) . . . . ? Ni5 Ni2 Ni12 Ni7 -122.53(7) . . . . ? Ni1 Ni2 Ni12 Ni7 -71.72(3) . . . . ? Ni4 Ni2 Ni12 Ni7 -114.79(4) . . . . ? Ni6 Ni2 Ni12 Ni7 17.80(4) . . . . ? C2 Ni2 Ni12 C17 -160.7(5) . . . . ? C4 Ni2 Ni12 C17 166.7(4) . . . . ? Ni11 Ni2 Ni12 C17 -53.2(4) . . . . ? Ni5 Ni2 Ni12 C17 104.1(4) . . . . ? Ni1 Ni2 Ni12 C17 154.9(4) . . . . ? Ni4 Ni2 Ni12 C17 111.8(4) . . . . ? Ni6 Ni2 Ni12 C17 -115.6(4) . . . . ? Ni7 Ni2 Ni12 C17 -133.4(4) . . . . ? C17 Ni2 Ni12 Ni4 -111.8(4) . . . . ? C2 Ni2 Ni12 Ni4 87.5(3) . . . . ? C4 Ni2 Ni12 Ni4 54.9(2) . . . . ? Ni11 Ni2 Ni12 Ni4 -165.04(10) . . . . ? Ni5 Ni2 Ni12 Ni4 -7.74(8) . . . . ? Ni1 Ni2 Ni12 Ni4 43.07(3) . . . . ? Ni6 Ni2 Ni12 Ni4 132.59(4) . . . . ? Ni7 Ni2 Ni12 Ni4 114.79(4) . . . . ? C17 Ni2 Ni12 Ni10 -163.5(4) . . . . ? C2 Ni2 Ni12 Ni10 35.9(3) . . . . ? C4 Ni2 Ni12 Ni10 3.3(2) . . . . ? Ni11 Ni2 Ni12 Ni10 143.31(9) . . . . ? Ni5 Ni2 Ni12 Ni10 -59.40(8) . . . . ? Ni1 Ni2 Ni12 Ni10 -8.59(4) . . . . ? Ni4 Ni2 Ni12 Ni10 -51.65(3) . . . . ? Ni6 Ni2 Ni12 Ni10 80.93(4) . . . . ? Ni7 Ni2 Ni12 Ni10 63.14(4) . . . . ? C15 Ni4 Ni12 C16 -10.6(4) . . . . ? C4 Ni4 Ni12 C16 168.0(4) . . . . ? C3 Ni4 Ni12 C16 154.8(4) . . . . ? Ni13 Ni4 Ni12 C16 32.0(3) . . . . ? Ni2 Ni4 Ni12 C16 -129.7(3) . . . . ? Ni1 Ni4 Ni12 C16 -172.2(3) . . . . ? Ni3 Ni4 Ni12 C16 -121.7(3) . . . . ? Ni10 Ni4 Ni12 C16 108.5(3) . . . . ? Ni10 Ni4 Ni12 C16 98.9(3) 2_656 . . . ? C15 Ni4 Ni12 C13 174.8(6) . . . . ? C4 Ni4 Ni12 C13 -6.6(5) . . . . ? C3 Ni4 Ni12 C13 -19.8(6) . . . . ? Ni13 Ni4 Ni12 C13 -142.6(5) . . . . ? Ni2 Ni4 Ni12 C13 55.7(5) . . . . ? Ni1 Ni4 Ni12 C13 13.2(5) . . . . ? Ni3 Ni4 Ni12 C13 63.7(5) . . . . ? Ni10 Ni4 Ni12 C13 -66.1(5) . . . . ? Ni10 Ni4 Ni12 C13 -75.7(5) 2_656 . . . ? C15 Ni4 Ni12 C4 -178.5(4) . . . . ? C3 Ni4 Ni12 C4 -13.1(4) . . . . ? Ni13 Ni4 Ni12 C4 -135.9(2) . . . . ? Ni2 Ni4 Ni12 C4 62.3(2) . . . . ? Ni1 Ni4 Ni12 C4 19.9(2) . . . . ? Ni3 Ni4 Ni12 C4 70.4(2) . . . . ? Ni10 Ni4 Ni12 C4 -59.5(2) . . . . ? Ni10 Ni4 Ni12 C4 -69.0(2) 2_656 . . . ? C15 Ni4 Ni12 Ni7 -178.4(3) . . . . ? C4 Ni4 Ni12 Ni7 0.1(2) . . . . ? C3 Ni4 Ni12 Ni7 -13.0(3) . . . . ? Ni13 Ni4 Ni12 Ni7 -135.80(10) . . . . ? Ni2 Ni4 Ni12 Ni7 62.45(4) . . . . ? Ni1 Ni4 Ni12 Ni7 20.03(5) . . . . ? Ni3 Ni4 Ni12 Ni7 70.53(8) . . . . ? Ni10 Ni4 Ni12 Ni7 -59.32(4) . . . . ? Ni10 Ni4 Ni12 Ni7 -68.87(5) 2_656 . . . ? C15 Ni4 Ni12 C17 81.9(4) . . . . ? C4 Ni4 Ni12 C17 -99.5(3) . . . . ? C3 Ni4 Ni12 C17 -112.7(4) . . . . ? Ni13 Ni4 Ni12 C17 124.5(2) . . . . ? Ni2 Ni4 Ni12 C17 -37.22(19) . . . . ? Ni1 Ni4 Ni12 C17 -79.6(2) . . . . ? Ni3 Ni4 Ni12 C17 -29.1(2) . . . . ? Ni10 Ni4 Ni12 C17 -159.0(2) . . . . ? Ni10 Ni4 Ni12 C17 -168.5(2) 2_656 . . . ? C15 Ni4 Ni12 Ni2 119.1(3) . . . . ? C4 Ni4 Ni12 Ni2 -62.3(2) . . . . ? C3 Ni4 Ni12 Ni2 -75.4(3) . . . . ? Ni13 Ni4 Ni12 Ni2 161.75(11) . . . . ? Ni1 Ni4 Ni12 Ni2 -42.41(3) . . . . ? Ni3 Ni4 Ni12 Ni2 8.09(7) . . . . ? Ni10 Ni4 Ni12 Ni2 -121.77(4) . . . . ? Ni10 Ni4 Ni12 Ni2 -131.31(4) 2_656 . . . ? C15 Ni4 Ni12 Ni10 -119.1(3) . . . . ? C4 Ni4 Ni12 Ni10 59.5(2) . . . . ? C3 Ni4 Ni12 Ni10 46.3(3) . . . . ? Ni13 Ni4 Ni12 Ni10 -76.48(11) . . . . ? Ni2 Ni4 Ni12 Ni10 121.77(4) . . . . ? Ni1 Ni4 Ni12 Ni10 79.35(3) . . . . ? Ni3 Ni4 Ni12 Ni10 129.85(7) . . . . ? Ni10 Ni4 Ni12 Ni10 -9.55(4) 2_656 . . . ? C14 Ni10 Ni12 C16 -6.6(4) . . . . ? C20 Ni10 Ni12 C16 92.2(4) . . . . ? C3 Ni10 Ni12 C16 -173.0(3) 2_656 . . . ? C4 Ni10 Ni12 C16 -151.3(4) . . . . ? Ni13 Ni10 Ni12 C16 146.0(3) 2_656 . . . ? Ni4 Ni10 Ni12 C16 -95.0(3) . . . . ? Ni10 Ni10 Ni12 C16 -85.5(3) 2_656 . . . ? Ni4 Ni10 Ni12 C16 -152.9(3) 2_656 . . . ? Ni7 Ni10 Ni12 C16 147.8(3) . . . . ? C14 Ni10 Ni12 C13 -116.5(3) . . . . ? C20 Ni10 Ni12 C13 -17.8(3) . . . . ? C3 Ni10 Ni12 C13 77.1(3) 2_656 . . . ? C4 Ni10 Ni12 C13 98.7(3) . . . . ? Ni13 Ni10 Ni12 C13 36.1(2) 2_656 . . . ? Ni4 Ni10 Ni12 C13 155.1(2) . . . . ? Ni10 Ni10 Ni12 C13 164.5(2) 2_656 . . . ? Ni4 Ni10 Ni12 C13 97.2(2) 2_656 . . . ? Ni7 Ni10 Ni12 C13 37.9(2) . . . . ? C14 Ni10 Ni12 C4 144.8(3) . . . . ? C20 Ni10 Ni12 C4 -116.5(3) . . . . ? C3 Ni10 Ni12 C4 -21.6(3) 2_656 . . . ? Ni13 Ni10 Ni12 C4 -62.6(2) 2_656 . . . ? Ni4 Ni10 Ni12 C4 56.3(2) . . . . ? Ni10 Ni10 Ni12 C4 65.8(2) 2_656 . . . ? Ni4 Ni10 Ni12 C4 -1.5(2) 2_656 . . . ? Ni7 Ni10 Ni12 C4 -60.9(2) . . . . ? C14 Ni10 Ni12 Ni7 -154.4(3) . . . . ? C20 Ni10 Ni12 Ni7 -55.7(3) . . . . ? C3 Ni10 Ni12 Ni7 39.22(16) 2_656 . . . ? C4 Ni10 Ni12 Ni7 60.9(2) . . . . ? Ni13 Ni10 Ni12 Ni7 -1.78(4) 2_656 . . . ? Ni4 Ni10 Ni12 Ni7 117.21(4) . . . . ? Ni10 Ni10 Ni12 Ni7 126.68(3) 2_656 . . . ? Ni4 Ni10 Ni12 Ni7 59.34(4) 2_656 . . . ? C14 Ni10 Ni12 C17 123.9(5) . . . . ? C20 Ni10 Ni12 C17 -137.4(5) . . . . ? C3 Ni10 Ni12 C17 -42.5(4) 2_656 . . . ? C4 Ni10 Ni12 C17 -20.9(4) . . . . ? Ni13 Ni10 Ni12 C17 -83.5(4) 2_656 . . . ? Ni4 Ni10 Ni12 C17 35.5(4) . . . . ? Ni10 Ni10 Ni12 C17 44.9(4) 2_656 . . . ? Ni4 Ni10 Ni12 C17 -22.4(4) 2_656 . . . ? Ni7 Ni10 Ni12 C17 -81.7(4) . . . . ? C14 Ni10 Ni12 Ni2 141.4(3) . . . . ? C20 Ni10 Ni12 Ni2 -119.9(3) . . . . ? C3 Ni10 Ni12 Ni2 -25.06(16) 2_656 . . . ? C4 Ni10 Ni12 Ni2 -3.4(2) . . . . ? Ni13 Ni10 Ni12 Ni2 -66.06(5) 2_656 . . . ? Ni4 Ni10 Ni12 Ni2 52.93(4) . . . . ? Ni10 Ni10 Ni12 Ni2 62.40(4) 2_656 . . . ? Ni4 Ni10 Ni12 Ni2 -4.94(5) 2_656 . . . ? Ni7 Ni10 Ni12 Ni2 -64.28(4) . . . . ? C14 Ni10 Ni12 Ni4 88.4(3) . . . . ? C20 Ni10 Ni12 Ni4 -172.9(3) . . . . ? C3 Ni10 Ni12 Ni4 -77.99(16) 2_656 . . . ? C4 Ni10 Ni12 Ni4 -56.3(2) . . . . ? Ni13 Ni10 Ni12 Ni4 -118.99(4) 2_656 . . . ? Ni10 Ni10 Ni12 Ni4 9.47(3) 2_656 . . . ? Ni4 Ni10 Ni12 Ni4 -57.87(4) 2_656 . . . ? Ni7 Ni10 Ni12 Ni4 -117.21(4) . . . . ? C15 Ni4 Ni13 C5 -28.1(5) . . . . ? C4 Ni4 Ni13 C5 170.5(5) . . . . ? C3 Ni4 Ni13 C5 142.2(4) . . . . ? Ni12 Ni4 Ni13 C5 -74.7(4) . . . . ? Ni2 Ni4 Ni13 C5 78.0(4) . . . . ? Ni1 Ni4 Ni13 C5 129.5(4) . . . . ? Ni3 Ni4 Ni13 C5 87.8(4) . . . . ? Ni10 Ni4 Ni13 C5 -140.7(4) . . . . ? Ni10 Ni4 Ni13 C5 -157.1(4) 2_656 . . . ? C15 Ni4 Ni13 C20 87.7(4) . . . 2_656 ? C4 Ni4 Ni13 C20 -73.7(4) . . . 2_656 ? C3 Ni4 Ni13 C20 -101.9(3) . . . 2_656 ? Ni12 Ni4 Ni13 C20 41.2(3) . . . 2_656 ? Ni2 Ni4 Ni13 C20 -166.2(2) . . . 2_656 ? Ni1 Ni4 Ni13 C20 -114.6(2) . . . 2_656 ? Ni3 Ni4 Ni13 C20 -156.4(2) . . . 2_656 ? Ni10 Ni4 Ni13 C20 -24.9(2) . . . 2_656 ? Ni10 Ni4 Ni13 C20 -41.3(2) 2_656 . . 2_656 ? C15 Ni4 Ni13 C3 -170.3(4) . . . . ? C4 Ni4 Ni13 C3 28.2(4) . . . . ? Ni12 Ni4 Ni13 C3 143.1(2) . . . . ? Ni2 Ni4 Ni13 C3 -64.3(2) . . . . ? Ni1 Ni4 Ni13 C3 -12.7(2) . . . . ? Ni3 Ni4 Ni13 C3 -54.5(2) . . . . ? Ni10 Ni4 Ni13 C3 77.1(2) . . . . ? Ni10 Ni4 Ni13 C3 60.7(2) 2_656 . . . ? C15 Ni4 Ni13 Ni10 129.0(3) . . . 2_656 ? C4 Ni4 Ni13 Ni10 -32.5(3) . . . 2_656 ? C3 Ni4 Ni13 Ni10 -60.7(2) . . . 2_656 ? Ni12 Ni4 Ni13 Ni10 82.43(11) . . . 2_656 ? Ni2 Ni4 Ni13 Ni10 -124.93(7) . . . 2_656 ? Ni1 Ni4 Ni13 Ni10 -73.36(4) . . . 2_656 ? Ni3 Ni4 Ni13 Ni10 -115.13(4) . . . 2_656 ? Ni10 Ni4 Ni13 Ni10 16.42(4) . . . 2_656 ? C4 Ni4 Ni13 C15 -161.4(4) . . . . ? C3 Ni4 Ni13 C15 170.3(4) . . . . ? Ni12 Ni4 Ni13 C15 -46.6(3) . . . . ? Ni2 Ni4 Ni13 C15 106.1(3) . . . . ? Ni1 Ni4 Ni13 C15 157.6(3) . . . . ? Ni3 Ni4 Ni13 C15 115.9(3) . . . . ? Ni10 Ni4 Ni13 C15 -112.6(3) . . . . ? Ni10 Ni4 Ni13 C15 -129.0(3) 2_656 . . . ? C15 Ni4 Ni13 Ni3 -115.9(3) . . . . ? C4 Ni4 Ni13 Ni3 82.7(3) . . . . ? C3 Ni4 Ni13 Ni3 54.5(2) . . . . ? Ni12 Ni4 Ni13 Ni3 -162.44(11) . . . . ? Ni2 Ni4 Ni13 Ni3 -9.80(7) . . . . ? Ni1 Ni4 Ni13 Ni3 41.77(3) . . . . ? Ni10 Ni4 Ni13 Ni3 131.55(4) . . . . ? Ni10 Ni4 Ni13 Ni3 115.13(4) 2_656 . . . ? C15 Ni4 Ni13 Ni7 -168.2(3) . . . 2_656 ? C4 Ni4 Ni13 Ni7 30.3(3) . . . 2_656 ? C3 Ni4 Ni13 Ni7 2.1(2) . . . 2_656 ? Ni12 Ni4 Ni13 Ni7 145.20(10) . . . 2_656 ? Ni2 Ni4 Ni13 Ni7 -62.16(8) . . . 2_656 ? Ni1 Ni4 Ni13 Ni7 -10.60(4) . . . 2_656 ? Ni3 Ni4 Ni13 Ni7 -52.36(3) . . . 2_656 ? Ni10 Ni4 Ni13 Ni7 79.19(4) . . . 2_656 ? Ni10 Ni4 Ni13 Ni7 62.77(4) 2_656 . . 2_656 ? C6 Ni3 Ni13 C5 -16.8(4) . . . . ? C3 Ni3 Ni13 C5 168.8(4) . . . . ? C1 Ni3 Ni13 C5 151.1(4) . . . . ? Ni9 Ni3 Ni13 C5 36.3(3) . . . . ? Ni5 Ni3 Ni13 C5 -120.3(3) . . . . ? Ni1 Ni3 Ni13 C5 -171.8(3) . . . . ? Ni4 Ni3 Ni13 C5 -129.7(3) . . . . ? Ni7 Ni3 Ni13 C5 109.6(3) 2_656 . . . ? Ni6 Ni3 Ni13 C5 99.6(3) 2_656 . . . ? C6 Ni3 Ni13 C20 174.7(5) . . . 2_656 ? C3 Ni3 Ni13 C20 0.3(5) . . . 2_656 ? C1 Ni3 Ni13 C20 -17.4(6) . . . 2_656 ? Ni9 Ni3 Ni13 C20 -132.2(5) . . . 2_656 ? Ni5 Ni3 Ni13 C20 71.2(5) . . . 2_656 ? Ni1 Ni3 Ni13 C20 19.7(5) . . . 2_656 ? Ni4 Ni3 Ni13 C20 61.9(5) . . . 2_656 ? Ni7 Ni3 Ni13 C20 -58.9(5) 2_656 . . 2_656 ? Ni6 Ni3 Ni13 C20 -68.9(5) 2_656 . . 2_656 ? C6 Ni3 Ni13 C3 174.4(3) . . . . ? C1 Ni3 Ni13 C3 -17.7(4) . . . . ? Ni9 Ni3 Ni13 C3 -132.5(2) . . . . ? Ni5 Ni3 Ni13 C3 70.9(2) . . . . ? Ni1 Ni3 Ni13 C3 19.4(2) . . . . ? Ni4 Ni3 Ni13 C3 61.5(2) . . . . ? Ni7 Ni3 Ni13 C3 -59.2(2) 2_656 . . . ? Ni6 Ni3 Ni13 C3 -69.3(2) 2_656 . . . ? C6 Ni3 Ni13 Ni10 174.7(2) . . . 2_656 ? C3 Ni3 Ni13 Ni10 0.3(2) . . . 2_656 ? C1 Ni3 Ni13 Ni10 -17.4(3) . . . 2_656 ? Ni9 Ni3 Ni13 Ni10 -132.15(9) . . . 2_656 ? Ni5 Ni3 Ni13 Ni10 71.24(8) . . . 2_656 ? Ni1 Ni3 Ni13 Ni10 19.69(4) . . . 2_656 ? Ni4 Ni3 Ni13 Ni10 61.88(4) . . . 2_656 ? Ni7 Ni3 Ni13 Ni10 -58.88(4) 2_656 . . 2_656 ? Ni6 Ni3 Ni13 Ni10 -68.92(5) 2_656 . . 2_656 ? C6 Ni3 Ni13 C15 76.7(3) . . . . ? C3 Ni3 Ni13 C15 -97.6(3) . . . . ? C1 Ni3 Ni13 C15 -115.4(3) . . . . ? Ni9 Ni3 Ni13 C15 129.9(2) . . . . ? Ni5 Ni3 Ni13 C15 -26.7(2) . . . . ? Ni1 Ni3 Ni13 C15 -78.29(18) . . . . ? Ni4 Ni3 Ni13 C15 -36.11(18) . . . . ? Ni7 Ni3 Ni13 C15 -156.86(18) 2_656 . . . ? Ni6 Ni3 Ni13 C15 -166.90(18) 2_656 . . . ? C6 Ni3 Ni13 Ni4 112.8(2) . . . . ? C3 Ni3 Ni13 Ni4 -61.5(2) . . . . ? C1 Ni3 Ni13 Ni4 -79.3(3) . . . . ? Ni9 Ni3 Ni13 Ni4 165.97(10) . . . . ? Ni5 Ni3 Ni13 Ni4 9.36(7) . . . . ? Ni1 Ni3 Ni13 Ni4 -42.18(3) . . . . ? Ni7 Ni3 Ni13 Ni4 -120.75(4) 2_656 . . . ? Ni6 Ni3 Ni13 Ni4 -130.80(4) 2_656 . . . ? C6 Ni3 Ni13 Ni7 -126.4(2) . . . 2_656 ? C3 Ni3 Ni13 Ni7 59.2(2) . . . 2_656 ? C1 Ni3 Ni13 Ni7 41.5(3) . . . 2_656 ? Ni9 Ni3 Ni13 Ni7 -73.28(10) . . . 2_656 ? Ni5 Ni3 Ni13 Ni7 130.11(7) . . . 2_656 ? Ni1 Ni3 Ni13 Ni7 78.57(3) . . . 2_656 ? Ni4 Ni3 Ni13 Ni7 120.75(4) . . . 2_656 ? Ni6 Ni3 Ni13 Ni7 -10.04(4) 2_656 . . 2_656 ? C8 Ni5 C1 C2 -151.9(6) . . . 2_656 ? C2 Ni5 C1 C2 24.3(5) . . . 2_656 ? Ni9 Ni5 C1 C2 -145.9(6) . . . 2_656 ? Ni11 Ni5 C1 C2 0.4(7) . . . 2_656 ? Ni3 Ni5 C1 C2 136.3(6) . . . 2_656 ? Ni1 Ni5 C1 C2 57.5(5) . . . 2_656 ? Ni2 Ni5 C1 C2 67.3(6) . . . 2_656 ? Ni8 Ni5 C1 C2 -61.9(5) 2_656 . . 2_656 ? Ni8 Ni5 C1 C2 -21.9(5) . . . 2_656 ? C8 Ni5 C1 Ni9 -6.0(6) . . . . ? C2 Ni5 C1 Ni9 170.1(2) . . . . ? Ni11 Ni5 C1 Ni9 146.28(16) . . . . ? Ni3 Ni5 C1 Ni9 -77.83(17) . . . . ? Ni1 Ni5 C1 Ni9 -156.6(3) . . . . ? Ni2 Ni5 C1 Ni9 -146.80(9) . . . . ? Ni8 Ni5 C1 Ni9 83.95(19) 2_656 . . . ? Ni8 Ni5 C1 Ni9 124.00(14) . . . . ? C8 Ni5 C1 Ni6 -5.7(11) . . . 2_656 ? C2 Ni5 C1 Ni6 170.5(7) . . . 2_656 ? Ni9 Ni5 C1 Ni6 0.3(6) . . . 2_656 ? Ni11 Ni5 C1 Ni6 146.6(5) . . . 2_656 ? Ni3 Ni5 C1 Ni6 -77.5(7) . . . 2_656 ? Ni1 Ni5 C1 Ni6 -156.3(8) . . . 2_656 ? Ni2 Ni5 C1 Ni6 -146.5(7) . . . 2_656 ? Ni8 Ni5 C1 Ni6 84.3(7) 2_656 . . 2_656 ? Ni8 Ni5 C1 Ni6 124.3(7) . . . 2_656 ? C8 Ni5 C1 Ni3 71.9(6) . . . . ? C2 Ni5 C1 Ni3 -112.0(2) . . . . ? Ni9 Ni5 C1 Ni3 77.83(17) . . . . ? Ni11 Ni5 C1 Ni3 -135.89(18) . . . . ? Ni1 Ni5 C1 Ni3 -78.77(17) . . . . ? Ni2 Ni5 C1 Ni3 -68.97(18) . . . . ? Ni8 Ni5 C1 Ni3 161.8(3) 2_656 . . . ? Ni8 Ni5 C1 Ni3 -158.17(13) . . . . ? C8 Ni5 C1 Ni8 -89.9(6) . . . 2_656 ? C2 Ni5 C1 Ni8 86.2(2) . . . 2_656 ? Ni9 Ni5 C1 Ni8 -83.95(19) . . . 2_656 ? Ni11 Ni5 C1 Ni8 62.3(3) . . . 2_656 ? Ni3 Ni5 C1 Ni8 -161.8(3) . . . 2_656 ? Ni1 Ni5 C1 Ni8 119.4(2) . . . 2_656 ? Ni2 Ni5 C1 Ni8 129.25(12) . . . 2_656 ? Ni8 Ni5 C1 Ni8 40.05(15) . . . 2_656 ? C8 Ni5 C1 Ni1 150.6(5) . . . . ? C2 Ni5 C1 Ni1 -33.3(2) . . . . ? Ni9 Ni5 C1 Ni1 156.6(3) . . . . ? Ni11 Ni5 C1 Ni1 -57.1(3) . . . . ? Ni3 Ni5 C1 Ni1 78.77(17) . . . . ? Ni2 Ni5 C1 Ni1 9.8(2) . . . . ? Ni8 Ni5 C1 Ni1 -119.4(2) 2_656 . . . ? Ni8 Ni5 C1 Ni1 -79.40(13) . . . . ? C7 Ni9 C1 C2 117.2(8) . . . 2_656 ? C19 Ni9 C1 C2 -41.5(7) . . . 2_656 ? Ni6 Ni9 C1 C2 -39.4(6) 2_656 . . 2_656 ? Ni5 Ni9 C1 C2 140.7(7) . . . 2_656 ? Ni3 Ni9 C1 C2 -132.9(7) . . . 2_656 ? Ni8 Ni9 C1 C2 51.3(6) 2_656 . . 2_656 ? C7 Ni9 C1 Ni5 -23.5(7) . . . . ? C19 Ni9 C1 Ni5 177.8(3) . . . . ? Ni6 Ni9 C1 Ni5 179.9(3) 2_656 . . . ? Ni3 Ni9 C1 Ni5 86.38(19) . . . . ? Ni8 Ni9 C1 Ni5 -89.4(2) 2_656 . . . ? C7 Ni9 C1 Ni6 156.6(5) . . . 2_656 ? C19 Ni9 C1 Ni6 -2.1(3) . . . 2_656 ? Ni5 Ni9 C1 Ni6 -179.9(3) . . . 2_656 ? Ni3 Ni9 C1 Ni6 -93.48(17) . . . 2_656 ? Ni8 Ni9 C1 Ni6 90.77(18) 2_656 . . 2_656 ? C7 Ni9 C1 Ni3 -109.9(6) . . . . ? C19 Ni9 C1 Ni3 91.4(3) . . . . ? Ni6 Ni9 C1 Ni3 93.48(17) 2_656 . . . ? Ni5 Ni9 C1 Ni3 -86.38(19) . . . . ? Ni8 Ni9 C1 Ni3 -175.8(3) 2_656 . . . ? C7 Ni9 C1 Ni8 65.9(6) . . . 2_656 ? C19 Ni9 C1 Ni8 -92.8(3) . . . 2_656 ? Ni6 Ni9 C1 Ni8 -90.77(18) 2_656 . . 2_656 ? Ni5 Ni9 C1 Ni8 89.4(2) . . . 2_656 ? Ni3 Ni9 C1 Ni8 175.8(3) . . . 2_656 ? C7 Ni9 C1 Ni1 -76.6(9) . . . . ? C19 Ni9 C1 Ni1 124.7(6) . . . . ? Ni6 Ni9 C1 Ni1 126.8(6) 2_656 . . . ? Ni5 Ni9 C1 Ni1 -53.1(5) . . . . ? Ni3 Ni9 C1 Ni1 33.3(5) . . . . ? Ni8 Ni9 C1 Ni1 -142.4(7) 2_656 . . . ? C6 Ni3 C1 C2 158.3(5) . . . 2_656 ? C3 Ni3 C1 C2 -21.5(5) . . . 2_656 ? Ni13 Ni3 C1 C2 -7.8(7) . . . 2_656 ? Ni9 Ni3 C1 C2 140.7(6) . . . 2_656 ? Ni5 Ni3 C1 C2 -137.6(6) . . . 2_656 ? Ni1 Ni3 C1 C2 -55.3(5) . . . 2_656 ? Ni4 Ni3 C1 C2 -70.1(5) . . . 2_656 ? Ni7 Ni3 C1 C2 27.9(5) 2_656 . . 2_656 ? Ni6 Ni3 C1 C2 67.1(5) 2_656 . . 2_656 ? C6 Ni3 C1 Ni5 -64.1(3) . . . . ? C3 Ni3 C1 Ni5 116.0(2) . . . . ? Ni13 Ni3 C1 Ni5 129.7(2) . . . . ? Ni9 Ni3 C1 Ni5 -81.75(19) . . . . ? Ni1 Ni3 C1 Ni5 82.25(17) . . . . ? Ni4 Ni3 C1 Ni5 67.41(19) . . . . ? Ni7 Ni3 C1 Ni5 165.46(15) 2_656 . . . ? Ni6 Ni3 C1 Ni5 -155.3(3) 2_656 . . . ? C6 Ni3 C1 Ni9 17.6(4) . . . . ? C3 Ni3 C1 Ni9 -162.2(2) . . . . ? Ni13 Ni3 C1 Ni9 -148.54(16) . . . . ? Ni5 Ni3 C1 Ni9 81.75(19) . . . . ? Ni1 Ni3 C1 Ni9 164.0(2) . . . . ? Ni4 Ni3 C1 Ni9 149.16(9) . . . . ? Ni7 Ni3 C1 Ni9 -112.79(13) 2_656 . . . ? Ni6 Ni3 C1 Ni9 -73.56(17) 2_656 . . . ? C6 Ni3 C1 Ni6 91.2(3) . . . 2_656 ? C3 Ni3 C1 Ni6 -88.7(2) . . . 2_656 ? Ni13 Ni3 C1 Ni6 -75.0(3) . . . 2_656 ? Ni9 Ni3 C1 Ni6 73.56(17) . . . 2_656 ? Ni5 Ni3 C1 Ni6 155.3(3) . . . 2_656 ? Ni1 Ni3 C1 Ni6 -122.4(2) . . . 2_656 ? Ni4 Ni3 C1 Ni6 -137.28(12) . . . 2_656 ? Ni7 Ni3 C1 Ni6 -39.23(16) 2_656 . . 2_656 ? C6 Ni3 C1 Ni8 4.9(10) . . . 2_656 ? C3 Ni3 C1 Ni8 -175.0(9) . . . 2_656 ? Ni13 Ni3 C1 Ni8 -161.3(7) . . . 2_656 ? Ni9 Ni3 C1 Ni8 -12.7(7) . . . 2_656 ? Ni5 Ni3 C1 Ni8 69.0(8) . . . 2_656 ? Ni1 Ni3 C1 Ni8 151.3(10) . . . 2_656 ? Ni4 Ni3 C1 Ni8 136.4(8) . . . 2_656 ? Ni7 Ni3 C1 Ni8 -125.5(9) 2_656 . . 2_656 ? Ni6 Ni3 C1 Ni8 -86.3(9) 2_656 . . 2_656 ? C6 Ni3 C1 Ni1 -146.4(3) . . . . ? C3 Ni3 C1 Ni1 33.8(2) . . . . ? Ni13 Ni3 C1 Ni1 47.5(3) . . . . ? Ni9 Ni3 C1 Ni1 -164.0(2) . . . . ? Ni5 Ni3 C1 Ni1 -82.25(17) . . . . ? Ni4 Ni3 C1 Ni1 -14.84(18) . . . . ? Ni7 Ni3 C1 Ni1 83.21(12) 2_656 . . . ? Ni6 Ni3 C1 Ni1 122.4(2) 2_656 . . . ? C2 Ni1 C1 C2 -106.1(4) . . . 2_656 ? C4 Ni1 C1 C2 74.2(4) 2_656 . . 2_656 ? C4 Ni1 C1 C2 -179.0(4) . . . 2_656 ? C3 Ni1 C1 C2 108.8(4) . . . 2_656 ? C3 Ni1 C1 C2 44(11) 2_656 . . 2_656 ? C1 Ni1 C1 C2 -72.3(3) 2_656 . . 2_656 ? Ni5 Ni1 C1 C2 -32.1(3) 2_656 . . 2_656 ? Ni5 Ni1 C1 C2 -136.9(4) . . . 2_656 ? Ni2 Ni1 C1 C2 30.1(3) 2_656 . . 2_656 ? Ni2 Ni1 C1 C2 -146.1(3) . . . 2_656 ? C2 Ni1 C1 Ni5 30.75(19) . . . . ? C2 Ni1 C1 Ni5 136.9(4) 2_656 . . . ? C4 Ni1 C1 Ni5 -148.9(2) 2_656 . . . ? C4 Ni1 C1 Ni5 -42.1(4) . . . . ? C3 Ni1 C1 Ni5 -114.3(2) . . . . ? C3 Ni1 C1 Ni5 -179(100) 2_656 . . . ? C1 Ni1 C1 Ni5 64.59(15) 2_656 . . . ? Ni5 Ni1 C1 Ni5 104.75(16) 2_656 . . . ? Ni2 Ni1 C1 Ni5 166.95(19) 2_656 . . . ? Ni2 Ni1 C1 Ni5 -9.20(18) . . . . ? C2 Ni1 C1 Ni9 83.7(6) . . . . ? C2 Ni1 C1 Ni9 -170.2(8) 2_656 . . . ? C4 Ni1 C1 Ni9 -96.0(6) 2_656 . . . ? C4 Ni1 C1 Ni9 10.8(8) . . . . ? C3 Ni1 C1 Ni9 -61.3(6) . . . . ? C3 Ni1 C1 Ni9 -126(10) 2_656 . . . ? C1 Ni1 C1 Ni9 117.5(6) 2_656 . . . ? Ni5 Ni1 C1 Ni9 157.7(6) 2_656 . . . ? Ni5 Ni1 C1 Ni9 53.0(5) . . . . ? Ni2 Ni1 C1 Ni9 -140.1(6) 2_656 . . . ? Ni2 Ni1 C1 Ni9 43.8(6) . . . . ? C2 Ni1 C1 Ni6 -160.9(3) . . . 2_656 ? C2 Ni1 C1 Ni6 -54.8(3) 2_656 . . 2_656 ? C4 Ni1 C1 Ni6 19.4(3) 2_656 . . 2_656 ? C4 Ni1 C1 Ni6 126.2(3) . . . 2_656 ? C3 Ni1 C1 Ni6 54.1(3) . . . 2_656 ? C3 Ni1 C1 Ni6 -11(11) 2_656 . . 2_656 ? C1 Ni1 C1 Ni6 -127.1(4) 2_656 . . 2_656 ? Ni5 Ni1 C1 Ni6 -86.9(3) 2_656 . . 2_656 ? Ni5 Ni1 C1 Ni6 168.3(4) . . . 2_656 ? Ni2 Ni1 C1 Ni6 -24.7(2) 2_656 . . 2_656 ? Ni2 Ni1 C1 Ni6 159.1(2) . . . 2_656 ? C2 Ni1 C1 Ni3 116.9(2) . . . . ? C2 Ni1 C1 Ni3 -137.0(4) 2_656 . . . ? C4 Ni1 C1 Ni3 -62.8(2) 2_656 . . . ? C4 Ni1 C1 Ni3 44.0(4) . . . . ? C3 Ni1 C1 Ni3 -28.16(19) . . . . ? C3 Ni1 C1 Ni3 -93(11) 2_656 . . . ? C1 Ni1 C1 Ni3 150.7(2) 2_656 . . . ? Ni5 Ni1 C1 Ni3 -169.12(16) 2_656 . . . ? Ni5 Ni1 C1 Ni3 86.12(19) . . . . ? Ni2 Ni1 C1 Ni3 -106.92(15) 2_656 . . . ? Ni2 Ni1 C1 Ni3 76.92(14) . . . . ? C2 Ni1 C1 Ni8 -52.6(3) . . . 2_656 ? C2 Ni1 C1 Ni8 53.6(3) 2_656 . . 2_656 ? C4 Ni1 C1 Ni8 127.8(3) 2_656 . . 2_656 ? C4 Ni1 C1 Ni8 -125.4(3) . . . 2_656 ? C3 Ni1 C1 Ni8 162.4(3) . . . 2_656 ? C3 Ni1 C1 Ni8 97(11) 2_656 . . 2_656 ? C1 Ni1 C1 Ni8 -18.71(14) 2_656 . . 2_656 ? Ni5 Ni1 C1 Ni8 21.4(2) 2_656 . . 2_656 ? Ni5 Ni1 C1 Ni8 -83.3(3) . . . 2_656 ? Ni2 Ni1 C1 Ni8 83.6(3) 2_656 . . 2_656 ? Ni2 Ni1 C1 Ni8 -92.5(3) . . . 2_656 ? C17 Ni2 C2 C1 -146.1(7) . . . 2_656 ? C4 Ni2 C2 C1 26.0(6) . . . 2_656 ? Ni12 Ni2 C2 C1 1.5(7) . . . 2_656 ? Ni11 Ni2 C2 C1 -145.2(6) . . . 2_656 ? Ni5 Ni2 C2 C1 137.7(6) . . . 2_656 ? Ni1 Ni2 C2 C1 59.3(5) . . . 2_656 ? Ni4 Ni2 C2 C1 68.8(6) . . . 2_656 ? Ni6 Ni2 C2 C1 -61.7(5) . . . 2_656 ? Ni7 Ni2 C2 C1 -19.9(5) . . . 2_656 ? C17 Ni2 C2 Ni11 -0.8(7) . . . . ? C4 Ni2 C2 Ni11 171.2(2) . . . . ? Ni12 Ni2 C2 Ni11 146.75(15) . . . . ? Ni5 Ni2 C2 Ni11 -77.10(18) . . . . ? Ni1 Ni2 C2 Ni11 -155.4(3) . . . . ? Ni4 Ni2 C2 Ni11 -145.99(9) . . . . ? Ni6 Ni2 C2 Ni11 83.54(19) . . . . ? Ni7 Ni2 C2 Ni11 125.30(13) . . . . ? C17 Ni2 C2 Ni8 0.1(11) . . . . ? C4 Ni2 C2 Ni8 172.2(7) . . . . ? Ni12 Ni2 C2 Ni8 147.7(5) . . . . ? Ni11 Ni2 C2 Ni8 0.9(6) . . . . ? Ni5 Ni2 C2 Ni8 -76.2(7) . . . . ? Ni1 Ni2 C2 Ni8 -154.5(8) . . . . ? Ni4 Ni2 C2 Ni8 -145.1(6) . . . . ? Ni6 Ni2 C2 Ni8 84.5(7) . . . . ? Ni7 Ni2 C2 Ni8 126.2(7) . . . . ? C17 Ni2 C2 Ni5 76.3(7) . . . . ? C4 Ni2 C2 Ni5 -111.7(2) . . . . ? Ni12 Ni2 C2 Ni5 -136.15(17) . . . . ? Ni11 Ni2 C2 Ni5 77.10(18) . . . . ? Ni1 Ni2 C2 Ni5 -78.34(16) . . . . ? Ni4 Ni2 C2 Ni5 -68.89(19) . . . . ? Ni6 Ni2 C2 Ni5 160.6(3) . . . . ? Ni7 Ni2 C2 Ni5 -157.60(14) . . . . ? C17 Ni2 C2 Ni6 -84.4(7) . . . . ? C4 Ni2 C2 Ni6 87.7(2) . . . . ? Ni12 Ni2 C2 Ni6 63.2(3) . . . . ? Ni11 Ni2 C2 Ni6 -83.54(19) . . . . ? Ni5 Ni2 C2 Ni6 -160.6(3) . . . . ? Ni1 Ni2 C2 Ni6 121.0(2) . . . . ? Ni4 Ni2 C2 Ni6 130.47(12) . . . . ? Ni7 Ni2 C2 Ni6 41.76(16) . . . . ? C17 Ni2 C2 Ni1 154.6(6) . . . . ? C4 Ni2 C2 Ni1 -33.3(2) . . . . ? Ni12 Ni2 C2 Ni1 -57.8(3) . . . . ? Ni11 Ni2 C2 Ni1 155.4(3) . . . . ? Ni5 Ni2 C2 Ni1 78.34(16) . . . . ? Ni4 Ni2 C2 Ni1 9.5(2) . . . . ? Ni6 Ni2 C2 Ni1 -121.0(2) . . . . ? Ni7 Ni2 C2 Ni1 -79.26(13) . . . . ? C18 Ni11 C2 C1 122.2(8) . . . 2_656 ? C10 Ni11 C2 C1 -43.1(7) . . . 2_656 ? Ni8 Ni11 C2 C1 -39.7(5) . . . 2_656 ? C8 Ni11 C2 C1 -141.3(6) . . . 2_656 ? Ni2 Ni11 C2 C1 140.7(7) . . . 2_656 ? Ni5 Ni11 C2 C1 -131.5(7) . . . 2_656 ? Ni6 Ni11 C2 C1 51.1(6) . . . 2_656 ? C18 Ni11 C2 Ni2 -18.5(7) . . . . ? C10 Ni11 C2 Ni2 176.2(2) . . . . ? Ni8 Ni11 C2 Ni2 179.6(3) . . . . ? C8 Ni11 C2 Ni2 78.0(2) . . . . ? Ni5 Ni11 C2 Ni2 87.83(18) . . . . ? Ni6 Ni11 C2 Ni2 -89.6(2) . . . . ? C18 Ni11 C2 Ni8 161.9(6) . . . . ? C10 Ni11 C2 Ni8 -3.4(3) . . . . ? C8 Ni11 C2 Ni8 -101.6(2) . . . . ? Ni2 Ni11 C2 Ni8 -179.6(3) . . . . ? Ni5 Ni11 C2 Ni8 -91.76(17) . . . . ? Ni6 Ni11 C2 Ni8 90.77(18) . . . . ? C18 Ni11 C2 Ni5 -106.4(7) . . . . ? C10 Ni11 C2 Ni5 88.4(3) . . . . ? Ni8 Ni11 C2 Ni5 91.76(17) . . . . ? C8 Ni11 C2 Ni5 -9.8(2) . . . . ? Ni2 Ni11 C2 Ni5 -87.83(18) . . . . ? Ni6 Ni11 C2 Ni5 -177.5(3) . . . . ? C18 Ni11 C2 Ni6 71.1(7) . . . . ? C10 Ni11 C2 Ni6 -94.2(3) . . . . ? Ni8 Ni11 C2 Ni6 -90.77(18) . . . . ? C8 Ni11 C2 Ni6 167.7(2) . . . . ? Ni2 Ni11 C2 Ni6 89.6(2) . . . . ? Ni5 Ni11 C2 Ni6 177.5(3) . . . . ? C18 Ni11 C2 Ni1 -74.5(9) . . . . ? C10 Ni11 C2 Ni1 120.2(6) . . . . ? Ni8 Ni11 C2 Ni1 123.6(6) . . . . ? C8 Ni11 C2 Ni1 22.0(6) . . . . ? Ni2 Ni11 C2 Ni1 -56.0(5) . . . . ? Ni5 Ni11 C2 Ni1 31.8(5) . . . . ? Ni6 Ni11 C2 Ni1 -145.6(7) . . . . ? C9 Ni8 C2 C1 -13.5(10) . . . 2_656 ? C10 Ni8 C2 C1 155.7(4) . . . 2_656 ? Ni11 Ni8 C2 C1 152.4(4) . . . 2_656 ? Ni9 Ni8 C2 C1 24.5(3) 2_656 . . 2_656 ? Ni8 Ni8 C2 C1 -90.8(3) 2_656 . . 2_656 ? Ni5 Ni8 C2 C1 -30.9(3) 2_656 . . 2_656 ? Ni5 Ni8 C2 C1 -130.9(4) . . . 2_656 ? Ni6 Ni8 C2 C1 68.9(3) . . . 2_656 ? C9 Ni8 C2 Ni2 -166.8(8) . . . . ? C10 Ni8 C2 Ni2 2.4(8) . . . . ? C1 Ni8 C2 Ni2 -153.3(9) 2_656 . . . ? Ni11 Ni8 C2 Ni2 -0.9(6) . . . . ? Ni9 Ni8 C2 Ni2 -128.8(7) 2_656 . . . ? Ni8 Ni8 C2 Ni2 115.8(7) 2_656 . . . ? Ni5 Ni8 C2 Ni2 175.7(8) 2_656 . . . ? Ni5 Ni8 C2 Ni2 75.7(7) . . . . ? Ni6 Ni8 C2 Ni2 -84.4(7) . . . . ? C9 Ni8 C2 Ni11 -165.9(8) . . . . ? C10 Ni8 C2 Ni11 3.3(3) . . . . ? C1 Ni8 C2 Ni11 -152.4(4) 2_656 . . . ? Ni9 Ni8 C2 Ni11 -127.89(14) 2_656 . . . ? Ni8 Ni8 C2 Ni11 116.77(12) 2_656 . . . ? Ni5 Ni8 C2 Ni11 176.67(17) 2_656 . . . ? Ni5 Ni8 C2 Ni11 76.67(18) . . . . ? Ni6 Ni8 C2 Ni11 -83.45(18) . . . . ? C9 Ni8 C2 Ni5 117.5(8) . . . . ? C10 Ni8 C2 Ni5 -73.3(3) . . . . ? C1 Ni8 C2 Ni5 130.9(4) 2_656 . . . ? Ni11 Ni8 C2 Ni5 -76.67(18) . . . . ? Ni9 Ni8 C2 Ni5 155.43(18) 2_656 . . . ? Ni8 Ni8 C2 Ni5 40.10(16) 2_656 . . . ? Ni5 Ni8 C2 Ni5 100.00(16) 2_656 . . . ? Ni6 Ni8 C2 Ni5 -160.1(3) . . . . ? C9 Ni8 C2 Ni6 -82.4(8) . . . . ? C10 Ni8 C2 Ni6 86.8(3) . . . . ? C1 Ni8 C2 Ni6 -68.9(3) 2_656 . . . ? Ni11 Ni8 C2 Ni6 83.45(18) . . . . ? Ni9 Ni8 C2 Ni6 -44.44(14) 2_656 . . . ? Ni8 Ni8 C2 Ni6 -159.78(15) 2_656 . . . ? Ni5 Ni8 C2 Ni6 -99.87(17) 2_656 . . . ? Ni5 Ni8 C2 Ni6 160.1(3) . . . . ? C9 Ni8 C2 Ni1 42.8(9) . . . . ? C10 Ni8 C2 Ni1 -148.0(3) . . . . ? C1 Ni8 C2 Ni1 56.3(3) 2_656 . . . ? Ni11 Ni8 C2 Ni1 -151.3(4) . . . . ? Ni9 Ni8 C2 Ni1 80.8(3) 2_656 . . . ? Ni8 Ni8 C2 Ni1 -34.5(3) 2_656 . . . ? Ni5 Ni8 C2 Ni1 25.4(2) 2_656 . . . ? Ni5 Ni8 C2 Ni1 -74.6(3) . . . . ? Ni6 Ni8 C2 Ni1 125.2(4) . . . . ? C8 Ni5 C2 C1 155.0(5) . . . 2_656 ? C1 Ni5 C2 C1 -22.6(5) . . . 2_656 ? Ni9 Ni5 C2 C1 -8.4(7) . . . 2_656 ? Ni11 Ni5 C2 C1 139.1(6) . . . 2_656 ? Ni3 Ni5 C2 C1 -73.0(5) . . . 2_656 ? Ni1 Ni5 C2 C1 -56.4(5) . . . 2_656 ? Ni2 Ni5 C2 C1 -139.2(6) . . . 2_656 ? Ni8 Ni5 C2 C1 26.1(5) 2_656 . . 2_656 ? Ni8 Ni5 C2 C1 65.5(5) . . . 2_656 ? C8 Ni5 C2 Ni2 -65.8(4) . . . . ? C1 Ni5 C2 Ni2 116.6(2) . . . . ? Ni9 Ni5 C2 Ni2 130.8(2) . . . . ? Ni11 Ni5 C2 Ni2 -81.65(19) . . . . ? Ni3 Ni5 C2 Ni2 66.2(2) . . . . ? Ni1 Ni5 C2 Ni2 82.81(18) . . . . ? Ni8 Ni5 C2 Ni2 165.31(16) 2_656 . . . ? Ni8 Ni5 C2 Ni2 -155.3(3) . . . . ? C8 Ni5 C2 Ni11 15.8(4) . . . . ? C1 Ni5 C2 Ni11 -161.7(2) . . . . ? Ni9 Ni5 C2 Ni11 -147.51(17) . . . . ? Ni3 Ni5 C2 Ni11 147.82(9) . . . . ? Ni1 Ni5 C2 Ni11 164.5(2) . . . . ? Ni2 Ni5 C2 Ni11 81.65(19) . . . . ? Ni8 Ni5 C2 Ni11 -113.04(13) 2_656 . . . ? Ni8 Ni5 C2 Ni11 -73.68(17) . . . . ? C8 Ni5 C2 Ni8 89.5(3) . . . . ? C1 Ni5 C2 Ni8 -88.0(2) . . . . ? Ni9 Ni5 C2 Ni8 -73.8(3) . . . . ? Ni11 Ni5 C2 Ni8 73.68(17) . . . . ? Ni3 Ni5 C2 Ni8 -138.51(12) . . . . ? Ni1 Ni5 C2 Ni8 -121.9(2) . . . . ? Ni2 Ni5 C2 Ni8 155.3(3) . . . . ? Ni8 Ni5 C2 Ni8 -39.36(16) 2_656 . . . ? C8 Ni5 C2 Ni6 8.5(10) . . . . ? C1 Ni5 C2 Ni6 -169.0(9) . . . . ? Ni9 Ni5 C2 Ni6 -154.8(7) . . . . ? Ni11 Ni5 C2 Ni6 -7.3(7) . . . . ? Ni3 Ni5 C2 Ni6 140.5(8) . . . . ? Ni1 Ni5 C2 Ni6 157.1(10) . . . . ? Ni2 Ni5 C2 Ni6 74.3(8) . . . . ? Ni8 Ni5 C2 Ni6 -120.4(9) 2_656 . . . ? Ni8 Ni5 C2 Ni6 -81.0(8) . . . . ? C8 Ni5 C2 Ni1 -148.6(3) . . . . ? C1 Ni5 C2 Ni1 33.8(2) . . . . ? Ni9 Ni5 C2 Ni1 48.0(3) . . . . ? Ni11 Ni5 C2 Ni1 -164.5(2) . . . . ? Ni3 Ni5 C2 Ni1 -16.65(18) . . . . ? Ni2 Ni5 C2 Ni1 -82.81(18) . . . . ? Ni8 Ni5 C2 Ni1 82.50(12) 2_656 . . . ? Ni8 Ni5 C2 Ni1 121.9(2) . . . . ? C11 Ni6 C2 C1 175.6(4) . . . 2_656 ? C19 Ni6 C2 C1 -35.1(5) 2_656 . . 2_656 ? Ni9 Ni6 C2 C1 -20.8(3) 2_656 . . 2_656 ? Ni11 Ni6 C2 C1 -145.1(4) . . . 2_656 ? Ni7 Ni6 C2 C1 89.9(3) . . . 2_656 ? Ni2 Ni6 C2 C1 133.9(4) . . . 2_656 ? Ni8 Ni6 C2 C1 -71.4(3) . . . 2_656 ? Ni3 Ni6 C2 C1 34.2(3) 2_656 . . 2_656 ? C11 Ni6 C2 Ni2 41.7(4) . . . . ? C19 Ni6 C2 Ni2 -169.0(3) 2_656 . . . ? C1 Ni6 C2 Ni2 -133.9(4) 2_656 . . . ? Ni9 Ni6 C2 Ni2 -154.70(18) 2_656 . . . ? Ni11 Ni6 C2 Ni2 81.0(2) . . . . ? Ni7 Ni6 C2 Ni2 -43.99(18) . . . . ? Ni8 Ni6 C2 Ni2 154.7(3) . . . . ? Ni3 Ni6 C2 Ni2 -99.67(18) 2_656 . . . ? C11 Ni6 C2 Ni11 -39.3(4) . . . . ? C19 Ni6 C2 Ni11 109.9(4) 2_656 . . . ? C1 Ni6 C2 Ni11 145.1(4) 2_656 . . . ? Ni9 Ni6 C2 Ni11 124.28(15) 2_656 . . . ? Ni7 Ni6 C2 Ni11 -125.01(14) . . . . ? Ni2 Ni6 C2 Ni11 -81.0(2) . . . . ? Ni8 Ni6 C2 Ni11 73.66(18) . . . . ? Ni3 Ni6 C2 Ni11 179.31(19) 2_656 . . . ? C11 Ni6 C2 Ni8 -113.0(3) . . . . ? C19 Ni6 C2 Ni8 36.3(4) 2_656 . . . ? C1 Ni6 C2 Ni8 71.4(3) 2_656 . . . ? Ni9 Ni6 C2 Ni8 50.62(15) 2_656 . . . ? Ni11 Ni6 C2 Ni8 -73.66(18) . . . . ? Ni7 Ni6 C2 Ni8 161.33(15) . . . . ? Ni2 Ni6 C2 Ni8 -154.7(3) . . . . ? Ni3 Ni6 C2 Ni8 105.65(17) 2_656 . . . ? C11 Ni6 C2 Ni5 -32.1(10) . . . . ? C19 Ni6 C2 Ni5 117.1(9) 2_656 . . . ? C1 Ni6 C2 Ni5 152.2(11) 2_656 . . . ? Ni9 Ni6 C2 Ni5 131.4(9) 2_656 . . . ? Ni11 Ni6 C2 Ni5 7.2(7) . . . . ? Ni7 Ni6 C2 Ni5 -117.8(9) . . . . ? Ni2 Ni6 C2 Ni5 -73.9(8) . . . . ? Ni8 Ni6 C2 Ni5 80.8(9) . . . . ? Ni3 Ni6 C2 Ni5 -173.5(9) 2_656 . . . ? C11 Ni6 C2 Ni1 121.7(4) . . . . ? C19 Ni6 C2 Ni1 -89.0(4) 2_656 . . . ? C1 Ni6 C2 Ni1 -53.9(3) 2_656 . . . ? Ni9 Ni6 C2 Ni1 -74.7(3) 2_656 . . . ? Ni11 Ni6 C2 Ni1 161.0(4) . . . . ? Ni7 Ni6 C2 Ni1 36.0(3) . . . . ? Ni2 Ni6 C2 Ni1 80.0(3) . . . . ? Ni8 Ni6 C2 Ni1 -125.3(4) . . . . ? Ni3 Ni6 C2 Ni1 -19.7(2) 2_656 . . . ? C2 Ni1 C2 C1 73.9(3) 2_656 . . 2_656 ? C4 Ni1 C2 C1 134(17) 2_656 . . 2_656 ? C4 Ni1 C2 C1 -105.4(4) . . . 2_656 ? C3 Ni1 C2 C1 -178.6(4) . . . 2_656 ? C3 Ni1 C2 C1 -71.3(4) 2_656 . . 2_656 ? C1 Ni1 C2 C1 108.1(4) . . . 2_656 ? Ni5 Ni1 C2 C1 29.8(3) 2_656 . . 2_656 ? Ni5 Ni1 C2 C1 136.4(4) . . . 2_656 ? Ni2 Ni1 C2 C1 46.3(4) 2_656 . . 2_656 ? Ni2 Ni1 C2 C1 -136.3(4) . . . 2_656 ? C2 Ni1 C2 Ni2 -149.8(3) 2_656 . . . ? C4 Ni1 C2 Ni2 -90(17) 2_656 . . . ? C4 Ni1 C2 Ni2 30.8(2) . . . . ? C3 Ni1 C2 Ni2 -42.3(4) . . . . ? C3 Ni1 C2 Ni2 65.0(2) 2_656 . . . ? C1 Ni1 C2 Ni2 136.3(4) 2_656 . . . ? C1 Ni1 C2 Ni2 -115.7(2) . . . . ? Ni5 Ni1 C2 Ni2 166.1(2) 2_656 . . . ? Ni5 Ni1 C2 Ni2 -87.4(2) . . . . ? Ni2 Ni1 C2 Ni2 -177.46(4) 2_656 . . . ? C2 Ni1 C2 Ni11 -94.1(6) 2_656 . . . ? C4 Ni1 C2 Ni11 -34(17) 2_656 . . . ? C4 Ni1 C2 Ni11 86.6(6) . . . . ? C3 Ni1 C2 Ni11 13.4(8) . . . . ? C3 Ni1 C2 Ni11 120.7(6) 2_656 . . . ? C1 Ni1 C2 Ni11 -168.0(8) 2_656 . . . ? C1 Ni1 C2 Ni11 -59.9(6) . . . . ? Ni5 Ni1 C2 Ni11 -138.2(6) 2_656 . . . ? Ni5 Ni1 C2 Ni11 -31.7(5) . . . . ? Ni2 Ni1 C2 Ni11 -121.7(5) 2_656 . . . ? Ni2 Ni1 C2 Ni11 55.7(5) . . . . ? C2 Ni1 C2 Ni8 17.77(15) 2_656 . . . ? C4 Ni1 C2 Ni8 77(17) 2_656 . . . ? C4 Ni1 C2 Ni8 -161.5(3) . . . . ? C3 Ni1 C2 Ni8 125.3(3) . . . . ? C3 Ni1 C2 Ni8 -127.4(3) 2_656 . . . ? C1 Ni1 C2 Ni8 -56.1(3) 2_656 . . . ? C1 Ni1 C2 Ni8 51.9(3) . . . . ? Ni5 Ni1 C2 Ni8 -26.3(2) 2_656 . . . ? Ni5 Ni1 C2 Ni8 80.2(3) . . . . ? Ni2 Ni1 C2 Ni8 -9.8(4) 2_656 . . . ? Ni2 Ni1 C2 Ni8 167.6(4) . . . . ? C2 Ni1 C2 Ni5 -62.45(14) 2_656 . . . ? C4 Ni1 C2 Ni5 -3(17) 2_656 . . . ? C4 Ni1 C2 Ni5 118.2(2) . . . . ? C3 Ni1 C2 Ni5 45.1(4) . . . . ? C3 Ni1 C2 Ni5 152.3(2) 2_656 . . . ? C1 Ni1 C2 Ni5 -136.4(4) 2_656 . . . ? C1 Ni1 C2 Ni5 -28.27(18) . . . . ? Ni5 Ni1 C2 Ni5 -106.55(15) 2_656 . . . ? Ni2 Ni1 C2 Ni5 -90.07(18) 2_656 . . . ? Ni2 Ni1 C2 Ni5 87.4(2) . . . . ? C2 Ni1 C2 Ni6 126.5(4) 2_656 . . . ? C4 Ni1 C2 Ni6 -174(100) 2_656 . . . ? C4 Ni1 C2 Ni6 -52.8(3) . . . . ? C3 Ni1 C2 Ni6 -126.0(3) . . . . ? C3 Ni1 C2 Ni6 -18.7(3) 2_656 . . . ? C1 Ni1 C2 Ni6 52.6(3) 2_656 . . . ? C1 Ni1 C2 Ni6 160.6(3) . . . . ? Ni5 Ni1 C2 Ni6 82.4(3) 2_656 . . . ? Ni5 Ni1 C2 Ni6 -171.1(4) . . . . ? Ni2 Ni1 C2 Ni6 98.9(3) 2_656 . . . ? Ni2 Ni1 C2 Ni6 -83.7(3) . . . . ? C6 Ni3 C3 C4 -154.5(6) . . . 2_656 ? C1 Ni3 C3 C4 25.3(6) . . . 2_656 ? Ni13 Ni3 C3 C4 -145.0(6) . . . 2_656 ? Ni9 Ni3 C3 C4 2.5(7) . . . 2_656 ? Ni5 Ni3 C3 C4 69.1(6) . . . 2_656 ? Ni1 Ni3 C3 C4 58.6(5) . . . 2_656 ? Ni4 Ni3 C3 C4 137.9(6) . . . 2_656 ? Ni7 Ni3 C3 C4 -60.7(5) 2_656 . . 2_656 ? Ni6 Ni3 C3 C4 -19.9(5) 2_656 . . 2_656 ? C6 Ni3 C3 Ni13 -9.5(6) . . . . ? C1 Ni3 C3 Ni13 170.3(2) . . . . ? Ni9 Ni3 C3 Ni13 147.51(16) . . . . ? Ni5 Ni3 C3 Ni13 -145.93(10) . . . . ? Ni1 Ni3 C3 Ni13 -156.4(3) . . . . ? Ni4 Ni3 C3 Ni13 -77.1(2) . . . . ? Ni7 Ni3 C3 Ni13 84.28(19) 2_656 . . . ? Ni6 Ni3 C3 Ni13 125.14(14) 2_656 . . . ? C6 Ni3 C3 Ni4 67.6(5) . . . . ? C1 Ni3 C3 Ni4 -112.6(2) . . . . ? Ni13 Ni3 C3 Ni4 77.1(2) . . . . ? Ni9 Ni3 C3 Ni4 -135.37(18) . . . . ? Ni5 Ni3 C3 Ni4 -68.8(2) . . . . ? Ni1 Ni3 C3 Ni4 -79.26(17) . . . . ? Ni7 Ni3 C3 Ni4 161.4(3) 2_656 . . . ? Ni6 Ni3 C3 Ni4 -157.74(14) 2_656 . . . ? C6 Ni3 C3 Ni10 -10.4(11) . . . 2_656 ? C1 Ni3 C3 Ni10 169.3(8) . . . 2_656 ? Ni13 Ni3 C3 Ni10 -0.9(6) . . . 2_656 ? Ni9 Ni3 C3 Ni10 146.6(6) . . . 2_656 ? Ni5 Ni3 C3 Ni10 -146.8(7) . . . 2_656 ? Ni1 Ni3 C3 Ni10 -157.3(9) . . . 2_656 ? Ni4 Ni3 C3 Ni10 -78.0(8) . . . 2_656 ? Ni7 Ni3 C3 Ni10 83.4(7) 2_656 . . 2_656 ? Ni6 Ni3 C3 Ni10 124.2(7) 2_656 . . 2_656 ? C6 Ni3 C3 Ni7 -93.8(5) . . . 2_656 ? C1 Ni3 C3 Ni7 86.0(2) . . . 2_656 ? Ni13 Ni3 C3 Ni7 -84.28(19) . . . 2_656 ? Ni9 Ni3 C3 Ni7 63.2(3) . . . 2_656 ? Ni5 Ni3 C3 Ni7 129.79(12) . . . 2_656 ? Ni1 Ni3 C3 Ni7 119.3(3) . . . 2_656 ? Ni4 Ni3 C3 Ni7 -161.4(3) . . . 2_656 ? Ni6 Ni3 C3 Ni7 40.86(17) 2_656 . . 2_656 ? C6 Ni3 C3 Ni1 146.8(4) . . . . ? C1 Ni3 C3 Ni1 -33.4(2) . . . . ? Ni13 Ni3 C3 Ni1 156.4(3) . . . . ? Ni9 Ni3 C3 Ni1 -56.1(3) . . . . ? Ni5 Ni3 C3 Ni1 10.4(2) . . . . ? Ni4 Ni3 C3 Ni1 79.26(17) . . . . ? Ni7 Ni3 C3 Ni1 -119.3(3) 2_656 . . . ? Ni6 Ni3 C3 Ni1 -78.48(13) 2_656 . . . ? C5 Ni13 C3 C4 118.1(8) . . . 2_656 ? C20 Ni13 C3 C4 -39.3(7) 2_656 . . 2_656 ? Ni10 Ni13 C3 C4 -39.1(6) 2_656 . . 2_656 ? C15 Ni13 C3 C4 -136.4(7) . . . 2_656 ? Ni4 Ni13 C3 C4 -130.1(7) . . . 2_656 ? Ni3 Ni13 C3 C4 140.5(7) . . . 2_656 ? Ni7 Ni13 C3 C4 52.5(6) 2_656 . . 2_656 ? C5 Ni13 C3 Ni3 -22.5(7) . . . . ? C20 Ni13 C3 Ni3 -179.8(2) 2_656 . . . ? Ni10 Ni13 C3 Ni3 -179.6(3) 2_656 . . . ? C15 Ni13 C3 Ni3 83.0(3) . . . . ? Ni4 Ni13 C3 Ni3 89.4(2) . . . . ? Ni7 Ni13 C3 Ni3 -88.0(2) 2_656 . . . ? C5 Ni13 C3 Ni4 -111.8(6) . . . . ? C20 Ni13 C3 Ni4 90.8(3) 2_656 . . . ? Ni10 Ni13 C3 Ni4 91.04(18) 2_656 . . . ? C15 Ni13 C3 Ni4 -6.3(2) . . . . ? Ni3 Ni13 C3 Ni4 -89.4(2) . . . . ? Ni7 Ni13 C3 Ni4 -177.3(3) 2_656 . . . ? C5 Ni13 C3 Ni10 157.2(6) . . . 2_656 ? C20 Ni13 C3 Ni10 -0.2(3) 2_656 . . 2_656 ? C15 Ni13 C3 Ni10 -97.4(2) . . . 2_656 ? Ni4 Ni13 C3 Ni10 -91.04(18) . . . 2_656 ? Ni3 Ni13 C3 Ni10 179.6(3) . . . 2_656 ? Ni7 Ni13 C3 Ni10 91.62(19) 2_656 . . 2_656 ? C5 Ni13 C3 Ni7 65.5(7) . . . 2_656 ? C20 Ni13 C3 Ni7 -91.9(3) 2_656 . . 2_656 ? Ni10 Ni13 C3 Ni7 -91.62(19) 2_656 . . 2_656 ? C15 Ni13 C3 Ni7 171.0(2) . . . 2_656 ? Ni4 Ni13 C3 Ni7 177.3(3) . . . 2_656 ? Ni3 Ni13 C3 Ni7 88.0(2) . . . 2_656 ? C5 Ni13 C3 Ni1 -78.2(10) . . . . ? C20 Ni13 C3 Ni1 124.4(6) 2_656 . . . ? Ni10 Ni13 C3 Ni1 124.6(7) 2_656 . . . ? C15 Ni13 C3 Ni1 27.3(7) . . . . ? Ni4 Ni13 C3 Ni1 33.6(5) . . . . ? Ni3 Ni13 C3 Ni1 -55.8(6) . . . . ? Ni7 Ni13 C3 Ni1 -143.8(8) 2_656 . . . ? C15 Ni4 C3 C4 148.5(6) . . . 2_656 ? C4 Ni4 C3 C4 -25.3(5) . . . 2_656 ? Ni13 Ni4 C3 C4 138.4(6) . . . 2_656 ? Ni12 Ni4 C3 C4 -15.1(7) . . . 2_656 ? Ni2 Ni4 C3 C4 -74.8(5) . . . 2_656 ? Ni1 Ni4 C3 C4 -57.3(5) . . . 2_656 ? Ni3 Ni4 C3 C4 -139.8(6) . . . 2_656 ? Ni10 Ni4 C3 C4 24.5(5) . . . 2_656 ? Ni10 Ni4 C3 C4 64.4(5) 2_656 . . 2_656 ? C15 Ni4 C3 Ni3 -71.7(4) . . . . ? C4 Ni4 C3 Ni3 114.6(2) . . . . ? Ni13 Ni4 C3 Ni3 -81.8(2) . . . . ? Ni12 Ni4 C3 Ni3 124.7(2) . . . . ? Ni2 Ni4 C3 Ni3 65.0(2) . . . . ? Ni1 Ni4 C3 Ni3 82.5(2) . . . . ? Ni10 Ni4 C3 Ni3 164.32(16) . . . . ? Ni10 Ni4 C3 Ni3 -155.8(3) 2_656 . . . ? C15 Ni4 C3 Ni13 10.1(4) . . . . ? C4 Ni4 C3 Ni13 -163.7(2) . . . . ? Ni12 Ni4 C3 Ni13 -153.51(16) . . . . ? Ni2 Ni4 C3 Ni13 146.82(10) . . . . ? Ni1 Ni4 C3 Ni13 164.3(3) . . . . ? Ni3 Ni4 C3 Ni13 81.8(2) . . . . ? Ni10 Ni4 C3 Ni13 -113.90(14) . . . . ? Ni10 Ni4 C3 Ni13 -73.98(18) 2_656 . . . ? C15 Ni4 C3 Ni10 84.1(4) . . . 2_656 ? C4 Ni4 C3 Ni10 -89.7(2) . . . 2_656 ? Ni13 Ni4 C3 Ni10 73.98(18) . . . 2_656 ? Ni12 Ni4 C3 Ni10 -79.5(3) . . . 2_656 ? Ni2 Ni4 C3 Ni10 -139.21(12) . . . 2_656 ? Ni1 Ni4 C3 Ni10 -121.7(2) . . . 2_656 ? Ni3 Ni4 C3 Ni10 155.8(3) . . . 2_656 ? Ni10 Ni4 C3 Ni10 -39.93(17) . . . 2_656 ? C15 Ni4 C3 Ni7 2.1(11) . . . 2_656 ? C4 Ni4 C3 Ni7 -171.7(10) . . . 2_656 ? Ni13 Ni4 C3 Ni7 -8.0(8) . . . 2_656 ? Ni12 Ni4 C3 Ni7 -161.5(7) . . . 2_656 ? Ni2 Ni4 C3 Ni7 138.8(9) . . . 2_656 ? Ni1 Ni4 C3 Ni7 156.3(11) . . . 2_656 ? Ni3 Ni4 C3 Ni7 73.8(9) . . . 2_656 ? Ni10 Ni4 C3 Ni7 -121.9(10) . . . 2_656 ? Ni10 Ni4 C3 Ni7 -82.0(9) 2_656 . . 2_656 ? C15 Ni4 C3 Ni1 -154.2(3) . . . . ? C4 Ni4 C3 Ni1 32.0(2) . . . . ? Ni13 Ni4 C3 Ni1 -164.3(3) . . . . ? Ni12 Ni4 C3 Ni1 42.2(4) . . . . ? Ni2 Ni4 C3 Ni1 -17.49(19) . . . . ? Ni3 Ni4 C3 Ni1 -82.5(2) . . . . ? Ni10 Ni4 C3 Ni1 81.79(13) . . . . ? Ni10 Ni4 C3 Ni1 121.7(2) 2_656 . . . ? C2 Ni1 C3 C4 -179.0(4) . . . 2_656 ? C2 Ni1 C3 C4 -71.7(4) 2_656 . . 2_656 ? C4 Ni1 C3 C4 107.9(4) . . . 2_656 ? C3 Ni1 C3 C4 73.5(3) 2_656 . . 2_656 ? C1 Ni1 C3 C4 138(10) 2_656 . . 2_656 ? C1 Ni1 C3 C4 -105.4(4) . . . 2_656 ? Ni5 Ni1 C3 C4 -40.9(4) 2_656 . . 2_656 ? Ni5 Ni1 C3 C4 -146.0(3) . . . 2_656 ? Ni2 Ni1 C3 C4 -31.8(3) 2_656 . . 2_656 ? Ni2 Ni1 C3 C4 152.0(3) . . . 2_656 ? C2 Ni1 C3 Ni3 -42.8(4) . . . . ? C2 Ni1 C3 Ni3 64.5(2) 2_656 . . . ? C4 Ni1 C3 Ni3 136.2(4) 2_656 . . . ? C4 Ni1 C3 Ni3 -115.9(2) . . . . ? C3 Ni1 C3 Ni3 -150.3(3) 2_656 . . . ? C1 Ni1 C3 Ni3 -85(11) 2_656 . . . ? C1 Ni1 C3 Ni3 30.8(2) . . . . ? Ni5 Ni1 C3 Ni3 95.3(2) 2_656 . . . ? Ni5 Ni1 C3 Ni3 -9.7(2) . . . . ? Ni2 Ni1 C3 Ni3 104.44(17) 2_656 . . . ? Ni2 Ni1 C3 Ni3 -71.75(18) . . . . ? C2 Ni1 C3 Ni13 12.9(9) . . . . ? C2 Ni1 C3 Ni13 120.1(6) 2_656 . . . ? C4 Ni1 C3 Ni13 -168.2(9) 2_656 . . . ? C4 Ni1 C3 Ni13 -60.2(6) . . . . ? C3 Ni1 C3 Ni13 -94.7(7) 2_656 . . . ? C1 Ni1 C3 Ni13 -30(11) 2_656 . . . ? C1 Ni1 C3 Ni13 86.4(7) . . . . ? Ni5 Ni1 C3 Ni13 150.9(5) 2_656 . . . ? Ni5 Ni1 C3 Ni13 45.9(7) . . . . ? Ni2 Ni1 C3 Ni13 160.1(7) 2_656 . . . ? Ni2 Ni1 C3 Ni13 -16.1(7) . . . . ? C2 Ni1 C3 Ni4 46.1(4) . . . . ? C2 Ni1 C3 Ni4 153.4(2) 2_656 . . . ? C4 Ni1 C3 Ni4 -134.9(4) 2_656 . . . ? C4 Ni1 C3 Ni4 -26.96(19) . . . . ? C3 Ni1 C3 Ni4 -61.42(14) 2_656 . . . ? C1 Ni1 C3 Ni4 3(11) 2_656 . . . ? C1 Ni1 C3 Ni4 119.7(2) . . . . ? Ni5 Ni1 C3 Ni4 -175.80(6) 2_656 . . . ? Ni5 Ni1 C3 Ni4 79.16(15) . . . . ? Ni2 Ni1 C3 Ni4 -166.67(17) 2_656 . . . ? Ni2 Ni1 C3 Ni4 17.14(18) . . . . ? C2 Ni1 C3 Ni10 126.4(3) . . . 2_656 ? C2 Ni1 C3 Ni10 -126.3(3) 2_656 . . 2_656 ? C4 Ni1 C3 Ni10 -54.6(3) 2_656 . . 2_656 ? C4 Ni1 C3 Ni10 53.3(3) . . . 2_656 ? C3 Ni1 C3 Ni10 18.86(16) 2_656 . . 2_656 ? C1 Ni1 C3 Ni10 84(11) 2_656 . . 2_656 ? C1 Ni1 C3 Ni10 -160.0(3) . . . 2_656 ? Ni5 Ni1 C3 Ni10 -95.5(3) 2_656 . . 2_656 ? Ni5 Ni1 C3 Ni10 159.4(3) . . . 2_656 ? Ni2 Ni1 C3 Ni10 -86.4(3) 2_656 . . 2_656 ? Ni2 Ni1 C3 Ni10 97.4(3) . . . 2_656 ? C2 Ni1 C3 Ni7 -125.1(3) . . . 2_656 ? C2 Ni1 C3 Ni7 -17.9(3) 2_656 . . 2_656 ? C4 Ni1 C3 Ni7 53.8(3) 2_656 . . 2_656 ? C4 Ni1 C3 Ni7 161.8(3) . . . 2_656 ? C3 Ni1 C3 Ni7 127.3(4) 2_656 . . 2_656 ? C1 Ni1 C3 Ni7 -168(10) 2_656 . . 2_656 ? C1 Ni1 C3 Ni7 -51.6(3) . . . 2_656 ? Ni5 Ni1 C3 Ni7 12.9(4) 2_656 . . 2_656 ? Ni5 Ni1 C3 Ni7 -92.1(3) . . . 2_656 ? Ni2 Ni1 C3 Ni7 22.1(2) 2_656 . . 2_656 ? Ni2 Ni1 C3 Ni7 -154.1(2) . . . 2_656 ? C15 Ni4 C4 C3 -142.5(7) . . . 2_656 ? C3 Ni4 C4 C3 27.8(5) . . . 2_656 ? Ni13 Ni4 C4 C3 6.5(7) . . . 2_656 ? Ni12 Ni4 C4 C3 -145.0(6) . . . 2_656 ? Ni2 Ni4 C4 C3 138.1(6) . . . 2_656 ? Ni1 Ni4 C4 C3 59.5(5) . . . 2_656 ? Ni3 Ni4 C4 C3 70.4(6) . . . 2_656 ? Ni10 Ni4 C4 C3 -61.2(5) . . . 2_656 ? Ni10 Ni4 C4 C3 -19.0(6) 2_656 . . 2_656 ? C15 Ni4 C4 Ni12 2.5(6) . . . . ? C3 Ni4 C4 Ni12 172.8(2) . . . . ? Ni13 Ni4 C4 Ni12 151.58(15) . . . . ? Ni2 Ni4 C4 Ni12 -76.89(19) . . . . ? Ni1 Ni4 C4 Ni12 -155.5(3) . . . . ? Ni3 Ni4 C4 Ni12 -144.55(10) . . . . ? Ni10 Ni4 C4 Ni12 83.86(19) . . . . ? Ni10 Ni4 C4 Ni12 126.02(14) 2_656 . . . ? C15 Ni4 C4 Ni7 2.1(11) . . . . ? C3 Ni4 C4 Ni7 172.5(8) . . . . ? Ni13 Ni4 C4 Ni7 151.2(6) . . . . ? Ni12 Ni4 C4 Ni7 -0.4(6) . . . . ? Ni2 Ni4 C4 Ni7 -77.3(7) . . . . ? Ni1 Ni4 C4 Ni7 -155.8(9) . . . . ? Ni3 Ni4 C4 Ni7 -144.9(7) . . . . ? Ni10 Ni4 C4 Ni7 83.5(7) . . . . ? Ni10 Ni4 C4 Ni7 125.6(7) 2_656 . . . ? C15 Ni4 C4 Ni2 79.4(6) . . . . ? C3 Ni4 C4 Ni2 -110.3(2) . . . . ? Ni13 Ni4 C4 Ni2 -131.53(19) . . . . ? Ni12 Ni4 C4 Ni2 76.89(19) . . . . ? Ni1 Ni4 C4 Ni2 -78.57(17) . . . . ? Ni3 Ni4 C4 Ni2 -67.66(19) . . . . ? Ni10 Ni4 C4 Ni2 160.8(3) . . . . ? Ni10 Ni4 C4 Ni2 -157.08(14) 2_656 . . . ? C15 Ni4 C4 Ni10 -81.3(6) . . . . ? C3 Ni4 C4 Ni10 89.0(2) . . . . ? Ni13 Ni4 C4 Ni10 67.7(3) . . . . ? Ni12 Ni4 C4 Ni10 -83.86(19) . . . . ? Ni2 Ni4 C4 Ni10 -160.8(3) . . . . ? Ni1 Ni4 C4 Ni10 120.7(2) . . . . ? Ni3 Ni4 C4 Ni10 131.59(12) . . . . ? Ni10 Ni4 C4 Ni10 42.16(16) 2_656 . . . ? C15 Ni4 C4 Ni1 158.0(5) . . . . ? C3 Ni4 C4 Ni1 -31.7(2) . . . . ? Ni13 Ni4 C4 Ni1 -53.0(3) . . . . ? Ni12 Ni4 C4 Ni1 155.5(3) . . . . ? Ni2 Ni4 C4 Ni1 78.57(17) . . . . ? Ni3 Ni4 C4 Ni1 10.9(2) . . . . ? Ni10 Ni4 C4 Ni1 -120.7(2) . . . . ? Ni10 Ni4 C4 Ni1 -78.52(14) 2_656 . . . ? C16 Ni12 C4 C3 116.3(8) . . . 2_656 ? C13 Ni12 C4 C3 -42.6(7) . . . 2_656 ? Ni7 Ni12 C4 C3 -39.4(6) . . . 2_656 ? C17 Ni12 C4 C3 -140.0(7) . . . 2_656 ? Ni2 Ni12 C4 C3 -131.4(7) . . . 2_656 ? Ni4 Ni12 C4 C3 140.5(7) . . . 2_656 ? Ni10 Ni12 C4 C3 52.7(6) . . . 2_656 ? C16 Ni12 C4 Ni4 -24.2(7) . . . . ? C13 Ni12 C4 Ni4 176.9(3) . . . . ? Ni7 Ni12 C4 Ni4 -179.8(3) . . . . ? C17 Ni12 C4 Ni4 79.5(3) . . . . ? Ni2 Ni12 C4 Ni4 88.1(2) . . . . ? Ni10 Ni12 C4 Ni4 -87.8(2) . . . . ? C16 Ni12 C4 Ni7 155.7(6) . . . . ? C13 Ni12 C4 Ni7 -3.3(3) . . . . ? C17 Ni12 C4 Ni7 -100.6(3) . . . . ? Ni2 Ni12 C4 Ni7 -92.06(17) . . . . ? Ni4 Ni12 C4 Ni7 179.8(3) . . . . ? Ni10 Ni12 C4 Ni7 92.05(19) . . . . ? C16 Ni12 C4 Ni2 -112.3(6) . . . . ? C13 Ni12 C4 Ni2 88.8(3) . . . . ? Ni7 Ni12 C4 Ni2 92.06(17) . . . . ? C17 Ni12 C4 Ni2 -8.6(3) . . . . ? Ni4 Ni12 C4 Ni2 -88.1(2) . . . . ? Ni10 Ni12 C4 Ni2 -175.9(3) . . . . ? C16 Ni12 C4 Ni10 63.6(7) . . . . ? C13 Ni12 C4 Ni10 -95.3(3) . . . . ? Ni7 Ni12 C4 Ni10 -92.05(19) . . . . ? C17 Ni12 C4 Ni10 167.3(3) . . . . ? Ni2 Ni12 C4 Ni10 175.9(3) . . . . ? Ni4 Ni12 C4 Ni10 87.8(2) . . . . ? C16 Ni12 C4 Ni1 -82.0(9) . . . . ? C13 Ni12 C4 Ni1 119.1(6) . . . . ? Ni7 Ni12 C4 Ni1 122.4(7) . . . . ? C17 Ni12 C4 Ni1 21.7(6) . . . . ? Ni2 Ni12 C4 Ni1 30.3(5) . . . . ? Ni4 Ni12 C4 Ni1 -57.8(5) . . . . ? Ni10 Ni12 C4 Ni1 -145.6(7) . . . . ? C12 Ni7 C4 C3 -15.6(10) . . . 2_656 ? C13 Ni7 C4 C3 155.5(4) . . . 2_656 ? Ni12 Ni7 C4 C3 152.4(4) . . . 2_656 ? Ni13 Ni7 C4 C3 25.4(3) 2_656 . . 2_656 ? Ni3 Ni7 C4 C3 -30.7(3) 2_656 . . 2_656 ? Ni6 Ni7 C4 C3 -92.2(3) . . . 2_656 ? Ni2 Ni7 C4 C3 -131.2(4) . . . 2_656 ? Ni10 Ni7 C4 C3 69.2(3) . . . 2_656 ? C12 Ni7 C4 Ni4 -167.5(9) . . . . ? C13 Ni7 C4 Ni4 3.6(8) . . . . ? C3 Ni7 C4 Ni4 -152.0(10) 2_656 . . . ? Ni12 Ni7 C4 Ni4 0.4(6) . . . . ? Ni13 Ni7 C4 Ni4 -126.6(8) 2_656 . . . ? Ni3 Ni7 C4 Ni4 177.3(8) 2_656 . . . ? Ni6 Ni7 C4 Ni4 115.8(7) . . . . ? Ni2 Ni7 C4 Ni4 76.9(7) . . . . ? Ni10 Ni7 C4 Ni4 -82.8(7) . . . . ? C12 Ni7 C4 Ni12 -167.9(8) . . . . ? C13 Ni7 C4 Ni12 3.2(3) . . . . ? C3 Ni7 C4 Ni12 -152.4(4) 2_656 . . . ? Ni13 Ni7 C4 Ni12 -126.99(15) 2_656 . . . ? Ni3 Ni7 C4 Ni12 176.94(18) 2_656 . . . ? Ni6 Ni7 C4 Ni12 115.37(13) . . . . ? Ni2 Ni7 C4 Ni12 76.46(19) . . . . ? Ni10 Ni7 C4 Ni12 -83.16(19) . . . . ? C12 Ni7 C4 Ni2 115.6(9) . . . . ? C13 Ni7 C4 Ni2 -73.3(3) . . . . ? C3 Ni7 C4 Ni2 131.2(4) 2_656 . . . ? Ni12 Ni7 C4 Ni2 -76.46(19) . . . . ? Ni13 Ni7 C4 Ni2 156.55(18) 2_656 . . . ? Ni3 Ni7 C4 Ni2 100.48(17) 2_656 . . . ? Ni6 Ni7 C4 Ni2 38.91(17) . . . . ? Ni10 Ni7 C4 Ni2 -159.6(3) . . . . ? C12 Ni7 C4 Ni10 -84.8(9) . . . . ? C13 Ni7 C4 Ni10 86.3(3) . . . . ? C3 Ni7 C4 Ni10 -69.2(3) 2_656 . . . ? Ni12 Ni7 C4 Ni10 83.16(19) . . . . ? Ni13 Ni7 C4 Ni10 -43.84(14) 2_656 . . . ? Ni3 Ni7 C4 Ni10 -99.90(18) 2_656 . . . ? Ni6 Ni7 C4 Ni10 -161.47(15) . . . . ? Ni2 Ni7 C4 Ni10 159.6(3) . . . . ? C12 Ni7 C4 Ni1 40.3(10) . . . . ? C13 Ni7 C4 Ni1 -148.6(3) . . . . ? C3 Ni7 C4 Ni1 55.9(3) 2_656 . . . ? Ni12 Ni7 C4 Ni1 -151.7(4) . . . . ? Ni13 Ni7 C4 Ni1 81.3(3) 2_656 . . . ? Ni3 Ni7 C4 Ni1 25.2(2) 2_656 . . . ? Ni6 Ni7 C4 Ni1 -36.4(3) . . . . ? Ni2 Ni7 C4 Ni1 -75.3(3) . . . . ? Ni10 Ni7 C4 Ni1 125.1(4) . . . . ? C17 Ni2 C4 C3 152.7(6) . . . 2_656 ? C2 Ni2 C4 C3 -22.1(5) . . . 2_656 ? Ni12 Ni2 C4 C3 138.7(6) . . . 2_656 ? Ni11 Ni2 C4 C3 -9.6(7) . . . 2_656 ? Ni5 Ni2 C4 C3 -71.8(5) . . . 2_656 ? Ni1 Ni2 C4 C3 -55.9(5) . . . 2_656 ? Ni4 Ni2 C4 C3 -139.2(6) . . . 2_656 ? Ni6 Ni2 C4 C3 26.6(5) . . . 2_656 ? Ni7 Ni2 C4 C3 65.1(5) . . . 2_656 ? C17 Ni2 C4 Ni4 -68.1(5) . . . . ? C2 Ni2 C4 Ni4 117.1(2) . . . . ? Ni12 Ni2 C4 Ni4 -82.2(2) . . . . ? Ni11 Ni2 C4 Ni4 129.6(2) . . . . ? Ni5 Ni2 C4 Ni4 67.4(2) . . . . ? Ni1 Ni2 C4 Ni4 83.31(18) . . . . ? Ni6 Ni2 C4 Ni4 165.82(15) . . . . ? Ni7 Ni2 C4 Ni4 -155.7(3) . . . . ? C17 Ni2 C4 Ni12 14.0(5) . . . . ? C2 Ni2 C4 Ni12 -160.8(2) . . . . ? Ni11 Ni2 C4 Ni12 -148.24(17) . . . . ? Ni5 Ni2 C4 Ni12 149.55(9) . . . . ? Ni1 Ni2 C4 Ni12 165.5(2) . . . . ? Ni4 Ni2 C4 Ni12 82.2(2) . . . . ? Ni6 Ni2 C4 Ni12 -112.03(13) . . . . ? Ni7 Ni2 C4 Ni12 -73.60(17) . . . . ? C17 Ni2 C4 Ni7 87.6(4) . . . . ? C2 Ni2 C4 Ni7 -87.2(2) . . . . ? Ni12 Ni2 C4 Ni7 73.60(17) . . . . ? Ni11 Ni2 C4 Ni7 -74.6(3) . . . . ? Ni5 Ni2 C4 Ni7 -136.86(12) . . . . ? Ni1 Ni2 C4 Ni7 -120.9(2) . . . . ? Ni4 Ni2 C4 Ni7 155.7(3) . . . . ? Ni6 Ni2 C4 Ni7 -38.43(16) . . . . ? C17 Ni2 C4 Ni10 2.3(10) . . . . ? C2 Ni2 C4 Ni10 -172.6(8) . . . . ? Ni12 Ni2 C4 Ni10 -11.8(7) . . . . ? Ni11 Ni2 C4 Ni10 -160.0(6) . . . . ? Ni5 Ni2 C4 Ni10 137.8(8) . . . . ? Ni1 Ni2 C4 Ni10 153.7(10) . . . . ? Ni4 Ni2 C4 Ni10 70.4(8) . . . . ? Ni6 Ni2 C4 Ni10 -123.8(8) . . . . ? Ni7 Ni2 C4 Ni10 -85.4(8) . . . . ? C17 Ni2 C4 Ni1 -151.4(4) . . . . ? C2 Ni2 C4 Ni1 33.7(2) . . . . ? Ni12 Ni2 C4 Ni1 -165.5(2) . . . . ? Ni11 Ni2 C4 Ni1 46.3(3) . . . . ? Ni5 Ni2 C4 Ni1 -15.92(18) . . . . ? Ni4 Ni2 C4 Ni1 -83.31(18) . . . . ? Ni6 Ni2 C4 Ni1 82.51(12) . . . . ? Ni7 Ni2 C4 Ni1 120.9(2) . . . . ? C14 Ni10 C4 C3 173.3(4) . . . 2_656 ? C20 Ni10 C4 C3 -38.0(5) . . . 2_656 ? Ni13 Ni10 C4 C3 -21.0(3) 2_656 . . 2_656 ? Ni12 Ni10 C4 C3 -144.1(4) . . . 2_656 ? Ni4 Ni10 C4 C3 134.1(4) . . . 2_656 ? Ni10 Ni10 C4 C3 90.6(3) 2_656 . . 2_656 ? Ni4 Ni10 C4 C3 34.6(3) 2_656 . . 2_656 ? Ni7 Ni10 C4 C3 -70.6(3) . . . 2_656 ? C14 Ni10 C4 Ni4 39.2(4) . . . . ? C20 Ni10 C4 Ni4 -172.2(3) . . . . ? C3 Ni10 C4 Ni4 -134.1(4) 2_656 . . . ? Ni13 Ni10 C4 Ni4 -155.11(18) 2_656 . . . ? Ni12 Ni10 C4 Ni4 81.8(2) . . . . ? Ni10 Ni10 C4 Ni4 -43.49(17) 2_656 . . . ? Ni4 Ni10 C4 Ni4 -99.57(18) 2_656 . . . ? Ni7 Ni10 C4 Ni4 155.3(3) . . . . ? C14 Ni10 C4 Ni12 -42.6(4) . . . . ? C20 Ni10 C4 Ni12 106.0(3) . . . . ? C3 Ni10 C4 Ni12 144.1(4) 2_656 . . . ? Ni13 Ni10 C4 Ni12 123.10(16) 2_656 . . . ? Ni4 Ni10 C4 Ni12 -81.8(2) . . . . ? Ni10 Ni10 C4 Ni12 -125.27(15) 2_656 . . . ? Ni4 Ni10 C4 Ni12 178.65(19) 2_656 . . . ? Ni7 Ni10 C4 Ni12 73.50(18) . . . . ? C14 Ni10 C4 Ni7 -116.1(3) . . . . ? C20 Ni10 C4 Ni7 32.6(4) . . . . ? C3 Ni10 C4 Ni7 70.6(3) 2_656 . . . ? Ni13 Ni10 C4 Ni7 49.61(16) 2_656 . . . ? Ni12 Ni10 C4 Ni7 -73.50(18) . . . . ? Ni4 Ni10 C4 Ni7 -155.3(3) . . . . ? Ni10 Ni10 C4 Ni7 161.23(16) 2_656 . . . ? Ni4 Ni10 C4 Ni7 105.15(18) 2_656 . . . ? C14 Ni10 C4 Ni2 -31.1(10) . . . . ? C20 Ni10 C4 Ni2 117.6(8) . . . . ? C3 Ni10 C4 Ni2 155.6(11) 2_656 . . . ? Ni13 Ni10 C4 Ni2 134.6(9) 2_656 . . . ? Ni12 Ni10 C4 Ni2 11.5(7) . . . . ? Ni4 Ni10 C4 Ni2 -70.3(8) . . . . ? Ni10 Ni10 C4 Ni2 -113.8(8) 2_656 . . . ? Ni4 Ni10 C4 Ni2 -169.8(9) 2_656 . . . ? Ni7 Ni10 C4 Ni2 85.0(8) . . . . ? C14 Ni10 C4 Ni1 118.9(4) . . . . ? C20 Ni10 C4 Ni1 -92.5(4) . . . . ? C3 Ni10 C4 Ni1 -54.4(3) 2_656 . . . ? Ni13 Ni10 C4 Ni1 -75.4(3) 2_656 . . . ? Ni12 Ni10 C4 Ni1 161.5(4) . . . . ? Ni4 Ni10 C4 Ni1 79.7(3) . . . . ? Ni10 Ni10 C4 Ni1 36.2(3) 2_656 . . . ? Ni4 Ni10 C4 Ni1 -19.9(2) 2_656 . . . ? Ni7 Ni10 C4 Ni1 -125.0(4) . . . . ? C2 Ni1 C4 C3 108.4(4) . . . 2_656 ? C2 Ni1 C4 C3 49(17) 2_656 . . 2_656 ? C4 Ni1 C4 C3 -72.3(3) 2_656 . . 2_656 ? C3 Ni1 C4 C3 -106.5(4) . . . 2_656 ? C1 Ni1 C4 C3 74.2(4) 2_656 . . 2_656 ? C1 Ni1 C4 C3 -178.6(4) . . . 2_656 ? Ni5 Ni1 C4 C3 45.9(4) 2_656 . . 2_656 ? Ni5 Ni1 C4 C3 152.2(3) . . . 2_656 ? Ni2 Ni1 C4 C3 -40.7(4) 2_656 . . 2_656 ? Ni2 Ni1 C4 C3 136.7(4) . . . 2_656 ? C2 Ni1 C4 Ni4 -115.9(2) . . . . ? C2 Ni1 C4 Ni4 -176(100) 2_656 . . . ? C4 Ni1 C4 Ni4 63.44(15) 2_656 . . . ? C3 Ni1 C4 Ni4 29.2(2) . . . . ? C3 Ni1 C4 Ni4 135.7(4) 2_656 . . . ? C1 Ni1 C4 Ni4 -150.1(2) 2_656 . . . ? C1 Ni1 C4 Ni4 -42.9(4) . . . . ? Ni5 Ni1 C4 Ni4 -178.36(6) 2_656 . . . ? Ni5 Ni1 C4 Ni4 -72.08(18) . . . . ? Ni2 Ni1 C4 Ni4 95.0(2) 2_656 . . . ? Ni2 Ni1 C4 Ni4 -87.6(2) . . . . ? C2 Ni1 C4 Ni12 -58.3(6) . . . . ? C2 Ni1 C4 Ni12 -118(16) 2_656 . . . ? C4 Ni1 C4 Ni12 121.0(7) 2_656 . . . ? C3 Ni1 C4 Ni12 86.8(6) . . . . ? C3 Ni1 C4 Ni12 -166.8(8) 2_656 . . . ? C1 Ni1 C4 Ni12 -92.6(6) 2_656 . . . ? C1 Ni1 C4 Ni12 14.7(8) . . . . ? Ni5 Ni1 C4 Ni12 -120.8(5) 2_656 . . . ? Ni5 Ni1 C4 Ni12 -14.5(6) . . . . ? Ni2 Ni1 C4 Ni12 152.6(5) 2_656 . . . ? Ni2 Ni1 C4 Ni12 -30.1(5) . . . . ? C2 Ni1 C4 Ni7 52.7(3) . . . . ? C2 Ni1 C4 Ni7 -7(17) 2_656 . . . ? C4 Ni1 C4 Ni7 -128.0(4) 2_656 . . . ? C3 Ni1 C4 Ni7 -162.2(3) . . . . ? C3 Ni1 C4 Ni7 -55.7(4) 2_656 . . . ? C1 Ni1 C4 Ni7 18.4(3) 2_656 . . . ? C1 Ni1 C4 Ni7 125.7(3) . . . . ? Ni5 Ni1 C4 Ni7 -9.8(4) 2_656 . . . ? Ni5 Ni1 C4 Ni7 96.5(3) . . . . ? Ni2 Ni1 C4 Ni7 -96.4(3) 2_656 . . . ? Ni2 Ni1 C4 Ni7 80.9(3) . . . . ? C2 Ni1 C4 Ni2 -28.25(19) . . . . ? C2 Ni1 C4 Ni2 -88(17) 2_656 . . . ? C4 Ni1 C4 Ni2 151.1(3) 2_656 . . . ? C3 Ni1 C4 Ni2 116.8(2) . . . . ? C3 Ni1 C4 Ni2 -136.7(4) 2_656 . . . ? C1 Ni1 C4 Ni2 -62.5(2) 2_656 . . . ? C1 Ni1 C4 Ni2 44.8(4) . . . . ? Ni5 Ni1 C4 Ni2 -90.74(19) 2_656 . . . ? Ni5 Ni1 C4 Ni2 15.54(17) . . . . ? Ni2 Ni1 C4 Ni2 -177.33(4) 2_656 . . . ? C2 Ni1 C4 Ni10 162.0(3) . . . . ? C2 Ni1 C4 Ni10 102(17) 2_656 . . . ? C4 Ni1 C4 Ni10 -18.66(14) 2_656 . . . ? C3 Ni1 C4 Ni10 -52.9(3) . . . . ? C3 Ni1 C4 Ni10 53.6(3) 2_656 . . . ? C1 Ni1 C4 Ni10 127.8(3) 2_656 . . . ? C1 Ni1 C4 Ni10 -125.0(3) . . . . ? Ni5 Ni1 C4 Ni10 99.5(3) 2_656 . . . ? Ni5 Ni1 C4 Ni10 -154.2(2) . . . . ? Ni2 Ni1 C4 Ni10 13.0(4) 2_656 . . . ? Ni2 Ni1 C4 Ni10 -169.7(4) . . . . ? C20 Ni13 C5 O5 76(56) 2_656 . . . ? C3 Ni13 C5 O5 -82(56) . . . . ? Ni10 Ni13 C5 O5 59(56) 2_656 . . . ? C15 Ni13 C5 O5 173(100) . . . . ? Ni4 Ni13 C5 O5 -169(100) . . . . ? Ni3 Ni13 C5 O5 -99(56) . . . . ? Ni7 Ni13 C5 O5 -32(56) 2_656 . . . ? C3 Ni3 C6 O6 -20(5) . . . . ? C1 Ni3 C6 O6 161(5) . . . . ? Ni13 Ni3 C6 O6 -27(5) . . . . ? Ni9 Ni3 C6 O6 175(5) . . . . ? Ni5 Ni3 C6 O6 121(5) . . . . ? Ni1 Ni3 C6 O6 95(5) . . . . ? Ni4 Ni3 C6 O6 29(5) . . . . ? Ni7 Ni3 C6 O6 -85(5) 2_656 . . . ? Ni6 Ni3 C6 O6 -150(5) 2_656 . . . ? C19 Ni9 C7 O7 36(17) . . . . ? C1 Ni9 C7 O7 -123(17) . . . . ? Ni6 Ni9 C7 O7 17(18) 2_656 . . . ? Ni5 Ni9 C7 O7 -141(17) . . . . ? Ni3 Ni9 C7 O7 150(17) . . . . ? Ni8 Ni9 C7 O7 -72(17) 2_656 . . . ? C1 Ni5 C8 O8 -19(5) . . . . ? C2 Ni5 C8 O8 165(4) . . . . ? Ni9 Ni5 C8 O8 -24(4) . . . . ? Ni11 Ni5 C8 O8 178(4) . . . . ? Ni3 Ni5 C8 O8 33(4) . . . . ? Ni1 Ni5 C8 O8 103(4) . . . . ? Ni2 Ni5 C8 O8 125(4) . . . . ? Ni8 Ni5 C8 O8 -83(4) 2_656 . . . ? Ni8 Ni5 C8 O8 -146(4) . . . . ? C1 Ni5 C8 Ni11 162.8(4) . . . . ? C2 Ni5 C8 Ni11 -12.9(3) . . . . ? Ni9 Ni5 C8 Ni11 158.12(9) . . . . ? Ni3 Ni5 C8 Ni11 -144.53(8) . . . . ? Ni1 Ni5 C8 Ni11 -74.8(5) . . . . ? Ni2 Ni5 C8 Ni11 -52.58(12) . . . . ? Ni8 Ni5 C8 Ni11 99.30(17) 2_656 . . . ? Ni8 Ni5 C8 Ni11 36.23(18) . . . . ? C18 Ni11 C8 O8 -14.2(8) . . . . ? C10 Ni11 C8 O8 87.1(8) . . . . ? C2 Ni11 C8 O8 -167.4(7) . . . . ? Ni8 Ni11 C8 O8 137.5(7) . . . . ? Ni2 Ni11 C8 O8 -120.2(7) . . . . ? Ni5 Ni11 C8 O8 -179.6(9) . . . . ? Ni6 Ni11 C8 O8 -151.9(6) . . . . ? C18 Ni11 C8 Ni5 165.4(3) . . . . ? C10 Ni11 C8 Ni5 -93.3(3) . . . . ? C2 Ni11 C8 Ni5 12.1(3) . . . . ? Ni8 Ni11 C8 Ni5 -42.9(2) . . . . ? Ni2 Ni11 C8 Ni5 59.4(2) . . . . ? Ni6 Ni11 C8 Ni5 27.6(4) . . . . ? C10 Ni8 C9 O9 -4(15) . . . . ? C2 Ni8 C9 O9 166(15) . . . . ? C1 Ni8 C9 O9 156(15) 2_656 . . . ? Ni11 Ni8 C9 O9 7(16) . . . . ? Ni9 Ni8 C9 O9 128(15) 2_656 . . . ? Ni8 Ni8 C9 O9 -115(15) 2_656 . . . ? Ni5 Ni8 C9 O9 -178(100) 2_656 . . . ? Ni5 Ni8 C9 O9 -99(15) . . . . ? Ni6 Ni8 C9 O9 101(15) . . . . ? C18 Ni11 C10 O10 10.7(10) . . . . ? C2 Ni11 C10 O10 -176.0(9) . . . . ? Ni8 Ni11 C10 O10 -179.7(10) . . . . ? C8 Ni11 C10 O10 -80.8(9) . . . . ? Ni2 Ni11 C10 O10 -169.8(6) . . . . ? Ni5 Ni11 C10 O10 -121.8(9) . . . . ? Ni6 Ni11 C10 O10 132.1(9) . . . . ? C18 Ni11 C10 Ni8 -169.6(3) . . . . ? C2 Ni11 C10 Ni8 3.7(3) . . . . ? C8 Ni11 C10 Ni8 98.9(2) . . . . ? Ni2 Ni11 C10 Ni8 9.9(6) . . . . ? Ni5 Ni11 C10 Ni8 57.87(19) . . . . ? Ni6 Ni11 C10 Ni8 -48.3(2) . . . . ? C9 Ni8 C10 O10 -7.7(10) . . . . ? C2 Ni8 C10 O10 176.2(9) . . . . ? C1 Ni8 C10 O10 -163.1(8) 2_656 . . . ? Ni11 Ni8 C10 O10 179.7(11) . . . . ? Ni9 Ni8 C10 O10 -98.3(9) 2_656 . . . ? Ni8 Ni8 C10 O10 78.0(10) 2_656 . . . ? Ni5 Ni8 C10 O10 129.6(11) 2_656 . . . ? Ni5 Ni8 C10 O10 132.5(9) . . . . ? Ni6 Ni8 C10 O10 -137.7(9) . . . . ? C9 Ni8 C10 Ni11 172.7(3) . . . . ? C2 Ni8 C10 Ni11 -3.4(3) . . . . ? C1 Ni8 C10 Ni11 17.3(4) 2_656 . . . ? Ni9 Ni8 C10 Ni11 82.1(3) 2_656 . . . ? Ni8 Ni8 C10 Ni11 -101.70(18) 2_656 . . . ? Ni5 Ni8 C10 Ni11 -50.0(15) 2_656 . . . ? Ni5 Ni8 C10 Ni11 -47.17(17) . . . . ? Ni6 Ni8 C10 Ni11 42.67(19) . . . . ? C19 Ni6 C11 O11 -20(24) 2_656 . . . ? C1 Ni6 C11 O11 146(24) 2_656 . . . ? C2 Ni6 C11 O11 138(24) . . . . ? Ni9 Ni6 C11 O11 -11(25) 2_656 . . . ? Ni11 Ni6 C11 O11 110(24) . . . . ? Ni7 Ni6 C11 O11 -133(24) . . . . ? Ni2 Ni6 C11 O11 165(24) . . . . ? Ni8 Ni6 C11 O11 82(24) . . . . ? Ni3 Ni6 C11 O11 -116(24) 2_656 . . . ? C13 Ni7 C12 O12 -14(10) . . . . ? C4 Ni7 C12 O12 157(10) . . . . ? C3 Ni7 C12 O12 146(10) 2_656 . . . ? Ni12 Ni7 C12 O12 -5(11) . . . . ? Ni13 Ni7 C12 O12 117(10) 2_656 . . . ? Ni3 Ni7 C12 O12 172(10) 2_656 . . . ? Ni6 Ni7 C12 O12 -124(10) . . . . ? Ni2 Ni7 C12 O12 -108(10) . . . . ? Ni10 Ni7 C12 O12 91(10) . . . . ? C16 Ni12 C13 O13 13.0(10) . . . . ? C4 Ni12 C13 O13 -177.5(9) . . . . ? Ni7 Ni12 C13 O13 179.0(11) . . . . ? C17 Ni12 C13 O13 -82.3(10) . . . . ? Ni2 Ni12 C13 O13 -123.0(9) . . . . ? Ni4 Ni12 C13 O13 -172.4(6) . . . . ? Ni10 Ni12 C13 O13 130.3(9) . . . . ? C16 Ni12 C13 Ni7 -166.0(3) . . . . ? C4 Ni12 C13 Ni7 3.5(3) . . . . ? C17 Ni12 C13 Ni7 98.7(3) . . . . ? Ni2 Ni12 C13 Ni7 58.0(2) . . . . ? Ni4 Ni12 C13 Ni7 8.6(6) . . . . ? Ni10 Ni12 C13 Ni7 -48.7(2) . . . . ? C12 Ni7 C13 O13 -5.4(10) . . . . ? C4 Ni7 C13 O13 177.7(9) . . . . ? C3 Ni7 C13 O13 -161.3(8) 2_656 . . . ? Ni12 Ni7 C13 O13 -179.0(11) . . . . ? Ni13 Ni7 C13 O13 -97.5(9) 2_656 . . . ? Ni3 Ni7 C13 O13 130.2(13) 2_656 . . . ? Ni6 Ni7 C13 O13 79.6(10) . . . . ? Ni2 Ni7 C13 O13 134.1(10) . . . . ? Ni10 Ni7 C13 O13 -136.9(9) . . . . ? C12 Ni7 C13 Ni12 173.7(3) . . . . ? C4 Ni7 C13 Ni12 -3.2(3) . . . . ? C3 Ni7 C13 Ni12 17.8(5) 2_656 . . . ? Ni13 Ni7 C13 Ni12 81.5(3) 2_656 . . . ? Ni3 Ni7 C13 Ni12 -50.7(16) 2_656 . . . ? Ni6 Ni7 C13 Ni12 -101.41(19) . . . . ? Ni2 Ni7 C13 Ni12 -46.88(18) . . . . ? Ni10 Ni7 C13 Ni12 42.2(2) . . . . ? C20 Ni10 C14 O14 -64(18) . . . . ? C3 Ni10 C14 O14 105(18) 2_656 . . . ? C4 Ni10 C14 O14 93(18) . . . . ? Ni13 Ni10 C14 O14 -58(19) 2_656 . . . ? Ni12 Ni10 C14 O14 64(18) . . . . ? Ni4 Ni10 C14 O14 119(18) . . . . ? Ni10 Ni10 C14 O14 -179(100) 2_656 . . . ? Ni4 Ni10 C14 O14 -163(18) 2_656 . . . ? Ni7 Ni10 C14 O14 38(18) . . . . ? C4 Ni4 C15 O15 -11(4) . . . . ? Ni13 Ni4 C15 O15 -172(4) . . . . ? Ni12 Ni4 C15 O15 -9(4) . . . . ? Ni2 Ni4 C15 O15 46(4) . . . . ? Ni1 Ni4 C15 O15 121(4) . . . . ? Ni3 Ni4 C15 O15 139(4) . . . . ? Ni10 Ni4 C15 O15 -69(4) . . . . ? Ni10 Ni4 C15 O15 -132(4) 2_656 . . . ? C4 Ni4 C15 Ni13 160.9(4) . . . . ? C3 Ni4 C15 Ni13 -8.2(3) . . . . ? Ni12 Ni4 C15 Ni13 162.89(10) . . . . ? Ni2 Ni4 C15 Ni13 -142.14(10) . . . . ? Ni1 Ni4 C15 Ni13 -67.3(7) . . . . ? Ni3 Ni4 C15 Ni13 -49.61(15) . . . . ? Ni10 Ni4 C15 Ni13 102.72(16) . . . . ? Ni10 Ni4 C15 Ni13 39.99(17) 2_656 . . . ? C5 Ni13 C15 O15 -22.7(8) . . . . ? C20 Ni13 C15 O15 80.0(8) 2_656 . . . ? C3 Ni13 C15 O15 -174.2(8) . . . . ? Ni10 Ni13 C15 O15 130.0(8) 2_656 . . . ? Ni4 Ni13 C15 O15 178.0(10) . . . . ? Ni3 Ni13 C15 O15 -126.5(8) . . . . ? Ni7 Ni13 C15 O15 -162.6(6) 2_656 . . . ? C5 Ni13 C15 Ni4 159.3(3) . . . . ? C20 Ni13 C15 Ni4 -98.0(3) 2_656 . . . ? C3 Ni13 C15 Ni4 7.8(3) . . . . ? Ni10 Ni13 C15 Ni4 -48.0(3) 2_656 . . . ? Ni3 Ni13 C15 Ni4 55.5(2) . . . . ? Ni7 Ni13 C15 Ni4 19.4(5) 2_656 . . . ? C13 Ni12 C16 O16 18(60) . . . . ? C4 Ni12 C16 O16 -141(59) . . . . ? Ni7 Ni12 C16 O16 -3(60) . . . . ? C17 Ni12 C16 O16 115(60) . . . . ? Ni2 Ni12 C16 O16 131(59) . . . . ? Ni4 Ni12 C16 O16 -159(60) . . . . ? Ni10 Ni12 C16 O16 -93(60) . . . . ? C2 Ni2 C17 O17 -17(5) . . . . ? C4 Ni2 C17 O17 172(5) . . . . ? Ni12 Ni2 C17 O17 -176(5) . . . . ? Ni11 Ni2 C17 O17 -17(5) . . . . ? Ni5 Ni2 C17 O17 39(5) . . . . ? Ni1 Ni2 C17 O17 110(5) . . . . ? Ni4 Ni2 C17 O17 132(5) . . . . ? Ni6 Ni2 C17 O17 -76(5) . . . . ? Ni7 Ni2 C17 O17 -139(5) . . . . ? C2 Ni2 C17 Ni12 159.7(5) . . . . ? C4 Ni2 C17 Ni12 -11.4(4) . . . . ? Ni11 Ni2 C17 Ni12 159.02(12) . . . . ? Ni5 Ni2 C17 Ni12 -145.30(9) . . . . ? Ni1 Ni2 C17 Ni12 -73.6(7) . . . . ? Ni4 Ni2 C17 Ni12 -52.03(16) . . . . ? Ni6 Ni2 C17 Ni12 100.18(18) . . . . ? Ni7 Ni2 C17 Ni12 37.3(2) . . . . ? C16 Ni12 C17 O17 -19.0(10) . . . . ? C13 Ni12 C17 O17 83.9(10) . . . . ? C4 Ni12 C17 O17 -170.3(10) . . . . ? Ni7 Ni12 C17 O17 134.5(9) . . . . ? Ni2 Ni12 C17 O17 179.1(12) . . . . ? Ni4 Ni12 C17 O17 -122.8(10) . . . . ? Ni10 Ni12 C17 O17 -154.3(7) . . . . ? C16 Ni12 C17 Ni2 161.9(4) . . . . ? C13 Ni12 C17 Ni2 -95.2(4) . . . . ? C4 Ni12 C17 Ni2 10.7(3) . . . . ? Ni7 Ni12 C17 Ni2 -44.6(3) . . . . ? Ni4 Ni12 C17 Ni2 58.1(3) . . . . ? Ni10 Ni12 C17 Ni2 26.7(6) . . . . ? C10 Ni11 C18 O18 -53(15) . . . . ? C2 Ni11 C18 O18 141(15) . . . . ? Ni8 Ni11 C18 O18 -69(15) . . . . ? C8 Ni11 C18 O18 44(15) . . . . ? Ni2 Ni11 C18 O18 127(15) . . . . ? Ni5 Ni11 C18 O18 56(15) . . . . ? Ni6 Ni11 C18 O18 -164(15) . . . . ? C7 Ni9 C19 O19 12.3(11) . . . . ? C1 Ni9 C19 O19 -177.8(10) . . . . ? Ni6 Ni9 C19 O19 179.9(12) 2_656 . . . ? Ni5 Ni9 C19 O19 -174.1(7) . . . . ? Ni3 Ni9 C19 O19 -123.3(10) . . . . ? Ni8 Ni9 C19 O19 130.5(10) 2_656 . . . ? C7 Ni9 C19 Ni6 -167.6(3) . . . 2_656 ? C1 Ni9 C19 Ni6 2.2(3) . . . 2_656 ? Ni5 Ni9 C19 Ni6 5.9(7) . . . 2_656 ? Ni3 Ni9 C19 Ni6 56.8(2) . . . 2_656 ? Ni8 Ni9 C19 Ni6 -49.4(2) 2_656 . . 2_656 ? C14 Ni10 C20 O20 -3.3(10) . . . . ? C3 Ni10 C20 O20 -179.5(9) 2_656 . . . ? C4 Ni10 C20 O20 -156.7(8) . . . . ? Ni13 Ni10 C20 O20 -179.2(11) 2_656 . . . ? Ni12 Ni10 C20 O20 -94.9(10) . . . . ? Ni4 Ni10 C20 O20 148.0(14) . . . . ? Ni10 Ni10 C20 O20 82.8(10) 2_656 . . . ? Ni4 Ni10 C20 O20 136.0(10) 2_656 . . . ? Ni7 Ni10 C20 O20 -134.5(10) . . . . ? C14 Ni10 C20 Ni13 175.9(3) . . . 2_656 ? C3 Ni10 C20 Ni13 -0.2(3) 2_656 . . 2_656 ? C4 Ni10 C20 Ni13 22.5(4) . . . 2_656 ? Ni12 Ni10 C20 Ni13 84.3(3) . . . 2_656 ? Ni4 Ni10 C20 Ni13 -33(2) . . . 2_656 ? Ni10 Ni10 C20 Ni13 -98.0(2) 2_656 . . 2_656 ? Ni4 Ni10 C20 Ni13 -44.80(18) 2_656 . . 2_656 ? Ni7 Ni10 C20 Ni13 44.74(19) . . . 2_656 ? C103 N1 C101 C102 -60.4(10) . . . . ? C105 N1 C101 C102 179.1(8) . . . . ? C107 N1 C101 C102 59.0(10) . . . . ? C101 N1 C103 C104 -58.6(10) . . . . ? C105 N1 C103 C104 57.8(10) . . . . ? C107 N1 C103 C104 179.1(8) . . . . ? C101 N1 C105 C106 -178.3(8) . . . . ? C103 N1 C105 C106 61.0(10) . . . . ? C107 N1 C105 C106 -57.8(10) . . . . ? C101 N1 C107 C108 56.6(10) . . . . ? C103 N1 C107 C108 178.8(8) . . . . ? C105 N1 C107 C108 -59.6(10) . . . . ? C207 N2 C201 C202 62.8(9) . . . . ? C205 N2 C201 C202 -56.5(9) . . . . ? C203 N2 C201 C202 -174.8(7) . . . . ? C201 N2 C203 C204 -66.2(9) . . . . ? C207 N2 C203 C204 55.2(9) . . . . ? C205 N2 C203 C204 172.8(7) . . . . ? C201 N2 C205 C206 -57.5(9) . . . . ? C207 N2 C205 C206 -178.2(7) . . . . ? C203 N2 C205 C206 61.7(9) . . . . ? C201 N2 C207 C208 174.6(8) . . . . ? C205 N2 C207 C208 -63.7(9) . . . . ? C203 N2 C207 C208 53.7(10) . . . . ? _diffrn_measured_fraction_theta_max 0.999 _diffrn_reflns_theta_full 26.00 _diffrn_measured_fraction_theta_full 0.999 _refine_diff_density_max 0.878 _refine_diff_density_min -0.526 _refine_diff_density_rms 0.102 # Attachment '- ni1617P-1.CIF' data_p-1 _database_code_depnum_ccdc_archive 'CCDC 846299' #TrackingRef '- ni1617P-1.CIF' _audit_creation_method SHELXL-97 _chemical_name_systematic ; ? ; _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'C59.10 H80 N4 Ni16.12 O23.10' _chemical_formula_weight 2162.55 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ni Ni 0.3393 1.1124 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _symmetry_cell_setting triclinic _symmetry_space_group_name_H-M P-1 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 15.9735(18) _cell_length_b 20.278(2) _cell_length_c 22.581(3) _cell_angle_alpha 90.761(2) _cell_angle_beta 90.881(2) _cell_angle_gamma 92.375(2) _cell_volume 7306.4(14) _cell_formula_units_Z 4 _cell_measurement_temperature 100(2) _cell_measurement_reflns_used 6708 _cell_measurement_theta_min 2.5015 _cell_measurement_theta_max 28.346 _exptl_crystal_description prism _exptl_crystal_colour dark-brown _exptl_crystal_size_max 0.24 _exptl_crystal_size_mid 0.21 _exptl_crystal_size_min 0.15 _exptl_crystal_density_meas ? _exptl_crystal_density_diffrn 1.966 _exptl_crystal_density_method 'not measured' _exptl_crystal_F_000 4395 _exptl_absorpt_coefficient_mu 4.119 _exptl_absorpt_correction_type empirical _exptl_absorpt_correction_T_min 0.4381 _exptl_absorpt_correction_T_max 0.5770 _exptl_absorpt_process_details ? _exptl_special_details ; ? ; _diffrn_ambient_temperature 100(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_radiation_source 'fine-focus sealed tube' _diffrn_radiation_monochromator graphite _diffrn_measurement_device_type 'CCD area detector' _diffrn_measurement_method 'phi and omega scans' _diffrn_detector_area_resol_mean ? _diffrn_standards_number ? _diffrn_standards_interval_count ? _diffrn_standards_interval_time ? _diffrn_standards_decay_% ? _diffrn_reflns_number 66804 _diffrn_reflns_av_R_equivalents 0.0484 _diffrn_reflns_av_sigmaI/netI 0.0607 _diffrn_reflns_limit_h_min -18 _diffrn_reflns_limit_h_max 18 _diffrn_reflns_limit_k_min -24 _diffrn_reflns_limit_k_max 23 _diffrn_reflns_limit_l_min -26 _diffrn_reflns_limit_l_max 26 _diffrn_reflns_theta_min 1.28 _diffrn_reflns_theta_max 25.00 _reflns_number_total 25590 _reflns_number_gt 18020 _reflns_threshold_expression >2sigma(I) _computing_data_collection ? _computing_cell_refinement ? _computing_data_reduction ? _computing_structure_solution 'SHELXS-97 (Sheldrick, 1990)' _computing_structure_refinement 'SHELXL-97 (Sheldrick, 1997)' _computing_molecular_graphics ? _computing_publication_material ? _refine_special_details ; Refinement of F^2^ against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F^2^, conventional R-factors R are based on F, with F set to zero for negative F^2^. The threshold expression of F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F^2^ are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger. ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type fullcycle _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'calc w=1/[\s^2^(Fo^2^)+(0.0765P)^2^+1.3147P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef ? _refine_ls_number_reflns 25590 _refine_ls_number_parameters 1843 _refine_ls_number_restraints 1813 _refine_ls_R_factor_all 0.0762 _refine_ls_R_factor_gt 0.0482 _refine_ls_wR_factor_ref 0.1405 _refine_ls_wR_factor_gt 0.1229 _refine_ls_goodness_of_fit_ref 1.033 _refine_ls_restrained_S_all 1.022 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_symmetry_multiplicity _atom_site_calc_flag _atom_site_refinement_flags _atom_site_disorder_assembly _atom_site_disorder_group Ni1 Ni 0.60165(4) 0.41441(4) 0.26649(3) 0.01525(16) Uani 1 1 d U A . Ni2 Ni 0.62922(4) 0.48190(4) 0.18422(3) 0.01409(15) Uani 1 1 d U A . Ni3 Ni 0.66137(4) 0.60174(4) 0.26435(3) 0.01442(16) Uani 1 1 d U A . Ni4 Ni 0.62924(4) 0.52879(4) 0.34293(3) 0.01531(16) Uani 1 1 d U A . Ni5 Ni 0.72450(5) 0.33491(4) 0.26577(3) 0.01821(17) Uani 1 1 d U . . Ni6 Ni 0.71200(5) 0.36770(4) 0.16445(3) 0.01651(16) Uani 1 1 d U A . Ni7 Ni 0.72126(5) 0.46346(4) 0.10190(3) 0.01652(16) Uani 1 1 d U . . Ni8 Ni 0.75159(4) 0.56584(4) 0.18013(3) 0.01406(15) Uani 1 1 d U A . Ni9 Ni 0.78328(5) 0.67632(4) 0.24964(3) 0.01775(16) Uani 1 1 d U . . Ni10 Ni 0.78372(5) 0.63266(4) 0.34759(3) 0.01718(16) Uani 1 1 d U A . Ni11 Ni 0.76855(5) 0.53342(4) 0.40306(3) 0.01785(16) Uani 1 1 d U . . Ni12 Ni 0.73926(4) 0.44191(4) 0.32510(3) 0.01417(15) Uani 1 1 d U A . Ni13 Ni 0.84666(5) 0.41125(4) 0.23645(3) 0.02021(17) Uani 1 1 d U A . Ni14 Ni 0.86513(4) 0.48166(4) 0.15433(3) 0.01629(16) Uani 1 1 d U A . Ni15 Ni 0.89724(4) 0.58949(4) 0.23477(3) 0.01674(16) Uani 1 1 d U A . Ni16 Ni 0.87596(4) 0.52704(4) 0.32186(3) 0.01739(16) Uani 1 1 d U A . Ni90 Ni 0.8590(10) 0.6628(8) 0.1678(7) 0.026(6) Uiso 0.050(3) 1 d PU A . C51 C 0.7890(3) 0.5760(3) 0.2705(2) 0.0146(4) Uani 1 1 d U A . C52 C 0.7458(3) 0.5402(3) 0.3141(2) 0.0146(4) Uani 1 1 d U A . C53 C 0.7578(3) 0.4613(3) 0.1903(2) 0.0142(4) Uani 1 1 d U A . C54 C 0.7185(3) 0.4299(3) 0.2384(2) 0.0141(4) Uani 1 1 d U A . C1 C 0.5471(4) 0.3624(3) 0.3148(3) 0.0194(10) Uani 1 1 d U . . C2 C 0.5251(3) 0.4573(3) 0.2174(2) 0.0153(8) Uani 1 1 d U . . C3 C 0.6012(3) 0.4740(3) 0.1025(2) 0.0164(8) Uani 1 1 d U A . C4 C 0.6273(3) 0.5808(3) 0.1802(2) 0.0155(6) Uani 1 1 d U . . C5 C 0.6628(4) 0.6924(3) 0.2482(3) 0.0177(8) Uani 1 1 d U A . C6 C 0.5604(3) 0.5877(3) 0.3041(3) 0.0171(9) Uani 1 1 d U . . C7 C 0.5679(4) 0.4955(3) 0.3994(3) 0.0176(10) Uani 1 1 d U . . C8 C 0.7550(4) 0.4884(3) 0.0327(3) 0.0186(10) Uani 1 1 d U A . C9 C 0.6997(4) 0.3538(3) 0.0875(3) 0.0192(9) Uani 1 1 d U A . C10 C 0.6977(4) 0.2838(3) 0.1951(3) 0.0232(10) Uani 1 1 d U A . C11 C 0.7239(4) 0.2691(3) 0.3154(3) 0.0304(14) Uani 1 1 d U A . C12 C 0.7785(4) 0.6149(3) 0.1179(3) 0.0181(7) Uani 1 1 d U . . C13 C 0.8254(4) 0.7403(3) 0.2050(3) 0.0245(9) Uani 1 1 d U A . C14 C 0.8038(4) 0.7184(3) 0.3337(3) 0.0215(10) Uani 1 1 d U A . C15 C 0.7858(4) 0.6269(3) 0.4276(3) 0.0197(9) Uani 1 1 d U A . C16 C 0.7439(4) 0.5029(3) 0.4722(3) 0.0203(11) Uani 1 1 d U A . C17 C 0.7442(3) 0.3902(3) 0.3879(2) 0.0171(9) Uani 1 1 d U . . C18 C 0.8782(5) 0.3428(4) 0.2769(3) 0.0179(17) Uiso 0.779(7) 1 d PU A 1 O18 O 0.9132(4) 0.2987(3) 0.2998(3) 0.0365(16) Uiso 0.779(7) 1 d PU A 1 C18' C 0.8958(17) 0.3774(14) 0.2941(12) 0.020(3) Uiso 0.221(7) 1 d PU A 2 O18' O 0.9300(14) 0.3330(11) 0.3110(6) 0.037(2) Uiso 0.221(7) 1 d PU A 2 C19 C 0.9447(3) 0.4317(3) 0.1946(2) 0.0183(9) Uani 1 1 d U . . C20 C 0.9264(4) 0.5125(3) 0.0967(3) 0.0204(11) Uani 1 1 d U . . C21 C 0.9630(4) 0.6324(3) 0.1862(3) 0.0228(9) Uani 1 1 d U . . C22 C 0.9771(3) 0.5488(3) 0.2839(3) 0.0187(9) Uani 1 1 d U . . C23 C 0.9091(4) 0.4915(3) 0.3875(3) 0.0273(11) Uani 1 1 d U A . O1 O 0.5148(3) 0.3266(2) 0.3467(2) 0.0334(11) Uani 1 1 d U A . O2 O 0.4527(2) 0.4640(2) 0.21095(19) 0.0257(10) Uani 1 1 d U A . O3 O 0.5451(3) 0.4719(2) 0.06940(18) 0.0268(10) Uani 1 1 d U . . O4 O 0.5804(2) 0.61066(19) 0.15019(17) 0.0192(8) Uani 1 1 d U A . O5 O 0.6222(3) 0.7381(2) 0.2404(2) 0.0285(10) Uani 1 1 d U . . O6 O 0.4909(2) 0.6060(2) 0.30713(17) 0.0221(9) Uani 1 1 d U A . O7 O 0.5314(3) 0.4732(2) 0.43791(19) 0.0344(11) Uani 1 1 d U A . O8 O 0.7797(3) 0.5072(2) -0.01173(18) 0.0307(10) Uani 1 1 d U . . O9 O 0.6849(3) 0.3294(2) 0.04145(18) 0.0293(10) Uani 1 1 d U . . O10 O 0.6833(3) 0.2283(2) 0.18339(19) 0.0344(11) Uani 1 1 d U . . O11 O 0.7238(4) 0.2264(2) 0.3486(2) 0.0512(14) Uani 1 1 d U . . O12 O 0.7990(3) 0.6446(2) 0.07774(18) 0.0280(9) Uani 1 1 d U A . O13 O 0.8505(3) 0.7809(2) 0.1749(2) 0.0374(10) Uani 1 1 d U . . O14 O 0.8173(3) 0.7740(2) 0.3461(2) 0.0311(10) Uani 1 1 d U . . O15 O 0.7956(3) 0.6527(2) 0.47479(18) 0.0274(10) Uani 1 1 d U . . O16 O 0.7218(3) 0.4850(2) 0.51751(18) 0.0315(11) Uani 1 1 d U . . O17 O 0.7426(3) 0.3573(2) 0.42889(18) 0.0269(10) Uani 1 1 d U A . O19 O 1.0154(2) 0.4184(2) 0.19158(18) 0.0249(10) Uani 1 1 d U A . O20 O 0.9678(3) 0.5320(2) 0.0596(2) 0.0369(12) Uani 1 1 d U A . O21 O 1.0052(3) 0.6605(2) 0.1530(2) 0.0351(10) Uani 1 1 d U A . O22 O 1.0500(2) 0.5435(2) 0.28787(18) 0.0273(10) Uani 1 1 d U A . O23 O 0.9453(3) 0.4680(3) 0.4266(2) 0.0465(13) Uani 1 1 d U . . Ni17 Ni 0.18343(5) -0.11029(4) 0.25502(3) 0.02064(17) Uani 1 1 d U B . Ni18 Ni 0.32966(5) -0.12025(4) 0.27204(3) 0.02141(17) Uani 1 1 d U B . Ni19 Ni 0.33097(6) -0.01776(4) 0.36254(4) 0.0299(2) Uani 1 1 d U . . Ni20 Ni 0.18574(5) -0.00195(4) 0.35237(3) 0.02266(17) Uani 1 1 d U B . Ni21 Ni 0.11352(5) -0.09034(4) 0.15979(4) 0.02173(17) Uani 1 1 d U B . Ni22 Ni 0.25673(5) -0.12051(4) 0.14754(3) 0.02067(16) Uani 1 1 d U B . Ni23 Ni 0.39783(5) -0.08395(4) 0.17353(4) 0.02188(17) Uani 1 1 d U . . Ni24 Ni 0.37631(5) 0.00226(4) 0.25687(3) 0.01873(16) Uani 1 1 d U B . Ni25 Ni 0.38831(5) 0.09922(4) 0.32888(4) 0.02788(19) Uani 1 1 d U B . Ni26 Ni 0.24925(5) 0.12855(4) 0.35071(3) 0.02012(16) Uani 1 1 d U . . Ni27 Ni 0.10450(5) 0.09522(4) 0.33960(4) 0.02417(17) Uani 1 1 d U B . Ni28 Ni 0.11425(5) 0.00009(4) 0.25117(3) 0.01890(16) Uani 1 1 d U . . Ni29 Ni 0.16692(5) 0.03198(4) 0.14440(3) 0.01836(16) Uani 1 1 d U B . Ni30 Ni 0.31066(5) 0.00679(4) 0.14316(3) 0.01817(16) Uani 1 1 d U B . Ni31 Ni 0.29536(5) 0.11005(4) 0.22978(3) 0.01781(16) Uani 1 1 d U B . Ni32 Ni 0.14926(5) 0.12522(4) 0.23482(3) 0.01835(16) Uani 1 1 d U B . C39 C 0.0070(6) 0.0086(4) 0.2316(4) 0.0193(15) Uiso 0.8042(19) 1 d PU B 1 O39 O -0.0619(4) 0.0157(3) 0.2185(3) 0.0393(15) Uiso 0.8042(19) 1 d PU B 1 C42 C 0.0595(6) 0.1651(5) 0.2153(5) 0.0220(15) Uiso 0.8042(19) 1 d PU B 1 O42 O -0.0080(4) 0.1842(3) 0.2026(3) 0.0348(14) Uiso 0.8042(19) 1 d PU B 1 C46 C 0.0049(6) 0.1294(5) 0.3373(4) 0.0278(17) Uiso 0.8042(19) 1 d PU B 1 O46 O -0.0611(4) 0.1526(3) 0.3387(3) 0.0511(17) Uiso 0.8042(19) 1 d PU B 1 Ni33 Ni 0.0111(3) 0.0938(2) 0.2656(2) 0.0272(8) Uani 0.1958(19) 1 d PU B 2 C39' C 0.006(2) -0.0086(17) 0.2462(15) 0.019(3) Uiso 0.1958(19) 1 d PU B 2 O39' O -0.0615(16) -0.0370(13) 0.2380(11) 0.042(2) Uiso 0.1958(19) 1 d PU B 2 C42' C 0.043(2) 0.1521(19) 0.2199(19) 0.021(3) Uiso 0.1958(19) 1 d PU B 2 O42' O 0.0305(16) 0.2097(12) 0.1897(11) 0.034(2) Uiso 0.1958(19) 1 d PU B 2 C46' C 0.009(3) 0.126(2) 0.3573(15) 0.028(3) Uiso 0.1958(19) 1 d PU B 2 O46' O -0.0449(18) 0.1479(14) 0.3819(13) 0.051(3) Uiso 0.1958(19) 1 d PU B 2 C47' C -0.090(2) 0.117(2) 0.2547(18) 0.051(11) Uiso 0.1958(19) 1 d PDU B 2 O47' O -0.147(2) 0.1425(19) 0.2348(15) 0.119(15) Uiso 0.1958(19) 1 d PDU B 2 C61 C 0.2888(4) -0.0555(3) 0.2161(3) 0.0172(4) Uani 1 1 d U B . C62 C 0.2130(4) -0.0370(3) 0.1918(3) 0.0171(4) Uani 1 1 d U B . C63 C 0.2072(4) 0.0644(3) 0.2846(3) 0.0170(4) Uani 1 1 d U B . C64 C 0.2863(4) 0.0451(3) 0.3032(3) 0.0183(4) Uani 1 1 d U B . C24 C 0.0917(4) -0.1591(3) 0.2195(3) 0.0249(9) Uani 1 1 d U . . C25 C 0.2390(4) -0.1680(3) 0.3064(3) 0.0245(9) Uani 1 1 d U . . C26 C 0.4206(4) -0.1544(3) 0.2980(3) 0.0342(14) Uani 1 1 d U . . C27 C 0.1039(4) -0.0699(3) 0.3132(3) 0.0251(6) Uani 1 1 d U B . C28 C 0.0996(4) 0.0297(3) 0.4008(3) 0.0306(9) Uani 1 1 d U . . C29 C 0.2420(5) -0.0553(3) 0.4064(3) 0.0332(10) Uani 1 1 d U B . C30 C 0.4270(9) -0.0348(7) 0.3997(6) 0.028(2) Uiso 0.519(8) 1 d PU C 1 O30 O 0.4834(6) -0.0532(5) 0.4228(5) 0.050(2) Uiso 0.519(8) 1 d PU C 1 C30' C 0.4077(9) -0.0580(7) 0.3973(7) 0.026(2) Uiso 0.481(8) 1 d PU C 2 O30' O 0.4659(8) -0.0792(5) 0.4212(6) 0.046(2) Uiso 0.481(8) 1 d PU C 2 C31 C 0.0205(4) -0.0883(3) 0.1193(3) 0.0271(12) Uani 1 1 d U . . C32 C 0.1766(4) -0.1609(3) 0.1041(3) 0.0268(11) Uani 1 1 d U . . C33 C 0.3529(4) -0.1581(3) 0.1242(3) 0.0245(10) Uani 1 1 d U B . C34 C 0.5029(4) -0.1059(3) 0.1737(3) 0.0280(12) Uani 1 1 d U C . C35 C 0.4860(4) 0.0028(3) 0.2628(3) 0.0271(11) Uani 1 1 d U . . C36 C 0.4871(9) 0.1128(7) 0.3527(6) 0.026(2) Uiso 0.470(8) 1 d PU B 1 O36 O 0.5593(8) 0.1244(6) 0.3623(5) 0.052(2) Uiso 0.470(8) 1 d PU B 1 C36' C 0.4962(8) 0.1256(7) 0.3299(6) 0.026(2) Uiso 0.530(8) 1 d PU B 2 O36' O 0.5665(7) 0.1452(5) 0.3354(5) 0.053(2) Uiso 0.530(8) 1 d PU B 2 C37 C 0.3467(4) 0.1655(3) 0.3819(3) 0.0260(11) Uani 1 1 d U B . C38 C 0.1703(4) 0.1744(3) 0.3849(3) 0.0238(10) Uani 1 1 d U B . C40 C 0.4095(4) -0.0018(3) 0.1095(3) 0.0252(10) Uani 1 1 d U B . C41 C 0.2285(4) 0.1726(3) 0.1899(3) 0.0216(9) Uani 1 1 d U . . C43 C 0.0806(4) 0.0663(3) 0.1101(3) 0.0217(11) Uani 1 1 d U . . C44 C 0.2567(4) 0.0655(3) 0.0947(3) 0.0216(9) Uani 1 1 d U . . C45 C 0.3951(4) 0.1315(3) 0.2037(3) 0.0244(10) Uani 1 1 d U . . O24 O 0.0431(3) -0.2028(2) 0.2235(2) 0.0393(12) Uani 1 1 d U B . O25 O 0.2273(3) -0.2086(2) 0.3418(2) 0.0304(10) Uani 1 1 d U B . O26 O 0.4840(3) -0.1750(3) 0.3134(2) 0.0537(15) Uani 1 1 d U B . O27 O 0.0499(3) -0.0989(2) 0.3380(2) 0.0343(10) Uani 1 1 d U . . O28 O 0.0625(3) 0.0182(2) 0.4436(2) 0.0493(14) Uani 1 1 d U B . O29 O 0.2300(4) -0.0913(3) 0.4456(2) 0.0522(14) Uani 1 1 d U . . O31 O -0.0401(3) -0.0837(2) 0.0911(2) 0.0430(13) Uani 1 1 d U B . O32 O 0.1433(3) -0.1971(2) 0.0699(2) 0.0404(12) Uani 1 1 d U B . O33 O 0.3845(3) -0.1985(2) 0.0952(2) 0.0344(11) Uani 1 1 d U . . O34 O 0.5717(3) -0.1196(3) 0.1726(2) 0.0470(14) Uani 1 1 d U . . O35 O 0.5566(3) -0.0014(3) 0.2725(2) 0.0457(14) Uani 1 1 d U C . O37 O 0.3777(3) 0.2064(2) 0.4135(2) 0.0371(12) Uani 1 1 d U . . O38 O 0.1423(3) 0.2161(2) 0.4138(2) 0.0356(11) Uani 1 1 d U . . O40 O 0.4650(3) 0.0073(2) 0.0774(2) 0.0443(13) Uani 1 1 d U . . O41 O 0.2346(3) 0.2161(2) 0.15671(19) 0.0260(10) Uani 1 1 d U B . O43 O 0.0225(3) 0.0870(2) 0.0879(2) 0.0343(11) Uani 1 1 d U B . O44 O 0.2637(3) 0.1018(2) 0.05517(19) 0.0283(10) Uani 1 1 d U B . O45 O 0.4567(3) 0.1505(2) 0.1834(2) 0.0375(12) Uani 1 1 d U B . N1 N 0.2407(3) 0.3805(2) 0.3224(2) 0.0175(11) Uani 1 1 d D . . C100 C 0.1697(4) 0.3716(3) 0.2769(3) 0.0254(14) Uani 1 1 d DU . . H10A H 0.1321 0.4090 0.2812 0.030 Uiso 1 1 calc R . . H10B H 0.1939 0.3741 0.2368 0.030 Uiso 1 1 calc R . . C101 C 0.1181(4) 0.3085(3) 0.2808(3) 0.0291(14) Uani 1 1 d DU . . H10C H 0.0740 0.3074 0.2502 0.044 Uiso 1 1 calc R . . H10D H 0.0926 0.3057 0.3200 0.044 Uiso 1 1 calc R . . H10E H 0.1541 0.2710 0.2750 0.044 Uiso 1 1 calc R . . C102 C 0.2997(4) 0.3237(3) 0.3199(3) 0.0235(13) Uani 1 1 d DU . . H10F H 0.3428 0.3304 0.3516 0.028 Uiso 1 1 calc R . . H10G H 0.2673 0.2823 0.3284 0.028 Uiso 1 1 calc R . . C103 C 0.3435(4) 0.3149(3) 0.2617(3) 0.0294(14) Uani 1 1 d DU . . H10H H 0.3798 0.2772 0.2642 0.044 Uiso 1 1 calc R . . H10I H 0.3775 0.3549 0.2533 0.044 Uiso 1 1 calc R . . H10J H 0.3017 0.3069 0.2300 0.044 Uiso 1 1 calc R . . C104 C 0.2067(4) 0.3812(3) 0.3844(3) 0.0236(13) Uani 1 1 d DU . . H10K H 0.2537 0.3917 0.4125 0.028 Uiso 1 1 calc R . . H10L H 0.1844 0.3362 0.3934 0.028 Uiso 1 1 calc R . . C105 C 0.1383(4) 0.4294(3) 0.3956(3) 0.0298(14) Uani 1 1 d DU . . H10M H 0.1204 0.4261 0.4368 0.045 Uiso 1 1 calc R . . H10N H 0.0905 0.4189 0.3690 0.045 Uiso 1 1 calc R . . H10O H 0.1600 0.4745 0.3883 0.045 Uiso 1 1 calc R . . C106 C 0.2865(4) 0.4453(3) 0.3083(3) 0.0246(13) Uani 1 1 d DU . . H10P H 0.3056 0.4430 0.2669 0.030 Uiso 1 1 calc R . . H10Q H 0.2461 0.4809 0.3107 0.030 Uiso 1 1 calc R . . C107 C 0.3614(4) 0.4646(3) 0.3476(3) 0.0233(13) Uani 1 1 d DU . . H10R H 0.3863 0.5069 0.3346 0.035 Uiso 1 1 calc R . . H10S H 0.4029 0.4305 0.3449 0.035 Uiso 1 1 calc R . . H10T H 0.3433 0.4690 0.3887 0.035 Uiso 1 1 calc R . . N2 N 0.2936(3) 0.6200(2) 0.1660(2) 0.0195(11) Uani 1 1 d D . . C200 C 0.2322(4) 0.6739(3) 0.1743(3) 0.0336(15) Uani 1 1 d DU . . H20A H 0.1850 0.6663 0.1457 0.040 Uiso 1 1 calc R . . H20B H 0.2604 0.7168 0.1649 0.040 Uiso 1 1 calc R . . C201 C 0.1972(4) 0.6781(4) 0.2367(3) 0.0404(17) Uani 1 1 d DU . . H20C H 0.1577 0.7137 0.2388 0.061 Uiso 1 1 calc R . . H20D H 0.2433 0.6870 0.2652 0.061 Uiso 1 1 calc R . . H20E H 0.1681 0.6361 0.2462 0.061 Uiso 1 1 calc R . . C202 C 0.3698(4) 0.6303(3) 0.2054(3) 0.0326(15) Uani 1 1 d DU . . H20F H 0.4081 0.5941 0.1977 0.039 Uiso 1 1 calc R . . H20G H 0.3523 0.6271 0.2471 0.039 Uiso 1 1 calc R . . C203 C 0.4186(4) 0.6963(3) 0.1977(3) 0.0351(16) Uani 1 1 d DU . . H20H H 0.4672 0.6986 0.2248 0.053 Uiso 1 1 calc R . . H20I H 0.3822 0.7327 0.2066 0.053 Uiso 1 1 calc R . . H20J H 0.4377 0.6997 0.1568 0.053 Uiso 1 1 calc R . . C204 C 0.3170(4) 0.6211(3) 0.1010(3) 0.0292(14) Uani 1 1 d DU . . H20K H 0.2657 0.6112 0.0768 0.035 Uiso 1 1 calc R . . H20L H 0.3375 0.6664 0.0914 0.035 Uiso 1 1 calc R . . C205 C 0.3827(4) 0.5736(3) 0.0831(3) 0.0313(15) Uani 1 1 d DU . . H20M H 0.3936 0.5779 0.0407 0.047 Uiso 1 1 calc R . . H20N H 0.3627 0.5283 0.0912 0.047 Uiso 1 1 calc R . . H20O H 0.4346 0.5837 0.1058 0.047 Uiso 1 1 calc R . . C206 C 0.2541(4) 0.5544(3) 0.1822(3) 0.0336(15) Uani 1 1 d DU . . H20P H 0.2450 0.5545 0.2255 0.040 Uiso 1 1 calc R . . H20Q H 0.2943 0.5199 0.1735 0.040 Uiso 1 1 calc R . . C207 C 0.1709(4) 0.5352(3) 0.1511(3) 0.0332(15) Uani 1 1 d DU . . H20R H 0.1506 0.4919 0.1648 0.050 Uiso 1 1 calc R . . H20S H 0.1792 0.5333 0.1082 0.050 Uiso 1 1 calc R . . H20T H 0.1297 0.5681 0.1603 0.050 Uiso 1 1 calc R . . N3 N 0.0106(3) 0.2938(2) 0.0467(2) 0.0176(11) Uani 1 1 d D . . C300 C -0.0527(4) 0.2419(3) 0.0664(3) 0.0269(14) Uani 1 1 d DU . . H30A H -0.0222 0.2034 0.0803 0.032 Uiso 1 1 calc R . . H30B H -0.0873 0.2272 0.0316 0.032 Uiso 1 1 calc R . . C301 C -0.1108(4) 0.2632(3) 0.1152(3) 0.0283(14) Uani 1 1 d DU . . H30C H -0.1495 0.2262 0.1249 0.042 Uiso 1 1 calc R . . H30D H -0.1429 0.3004 0.1016 0.042 Uiso 1 1 calc R . . H30E H -0.0776 0.2766 0.1505 0.042 Uiso 1 1 calc R . . C302 C -0.0295(4) 0.3586(3) 0.0362(3) 0.0300(14) Uani 1 1 d DU . . H30F H 0.0144 0.3912 0.0238 0.036 Uiso 1 1 calc R . . H30G H -0.0521 0.3745 0.0741 0.036 Uiso 1 1 calc R . . C303 C -0.0997(4) 0.3564(3) -0.0101(3) 0.0298(14) Uani 1 1 d DU . . H30H H -0.1216 0.4005 -0.0143 0.045 Uiso 1 1 calc R . . H30I H -0.1448 0.3256 0.0023 0.045 Uiso 1 1 calc R . . H30J H -0.0780 0.3416 -0.0482 0.045 Uiso 1 1 calc R . . C304 C 0.0490(4) 0.2711(3) -0.0105(3) 0.0306(15) Uani 1 1 d DU . . H30K H 0.0828 0.3084 -0.0268 0.037 Uiso 1 1 calc R . . H30L H 0.0031 0.2598 -0.0394 0.037 Uiso 1 1 calc R . . C305 C 0.1046(4) 0.2116(3) -0.0053(3) 0.0347(16) Uani 1 1 d DU . . H30M H 0.1267 0.2007 -0.0443 0.052 Uiso 1 1 calc R . . H30N H 0.0715 0.1737 0.0094 0.052 Uiso 1 1 calc R . . H30O H 0.1513 0.2224 0.0223 0.052 Uiso 1 1 calc R . . C306 C 0.0760(4) 0.3033(3) 0.0954(3) 0.0323(15) Uani 1 1 d DU . . H30P H 0.1000 0.2600 0.1033 0.039 Uiso 1 1 calc R . . H30Q H 0.0477 0.3174 0.1319 0.039 Uiso 1 1 calc R . . C307 C 0.1476(4) 0.3527(3) 0.0836(3) 0.0319(15) Uani 1 1 d DU . . H30R H 0.1862 0.3549 0.1178 0.048 Uiso 1 1 calc R . . H30S H 0.1252 0.3963 0.0770 0.048 Uiso 1 1 calc R . . H30T H 0.1776 0.3387 0.0484 0.048 Uiso 1 1 calc R . . N4 N 0.4195(3) 0.2725(2) 0.0184(2) 0.0207(11) Uani 1 1 d D . . C400 C 0.4052(4) 0.2690(4) 0.0837(3) 0.0381(16) Uani 1 1 d DU . . H40A H 0.3926 0.2224 0.0942 0.046 Uiso 1 1 calc R . . H40B H 0.3556 0.2944 0.0934 0.046 Uiso 1 1 calc R . . C401 C 0.4803(4) 0.2957(4) 0.1219(3) 0.0395(16) Uani 1 1 d DU . . H40C H 0.4668 0.2917 0.1639 0.059 Uiso 1 1 calc R . . H40D H 0.4923 0.3422 0.1127 0.059 Uiso 1 1 calc R . . H40E H 0.5296 0.2702 0.1133 0.059 Uiso 1 1 calc R . . C402 C 0.4457(4) 0.3407(3) -0.0009(3) 0.0371(16) Uani 1 1 d DU . . H40F H 0.4514 0.3404 -0.0444 0.045 Uiso 1 1 calc R . . H40G H 0.5014 0.3527 0.0169 0.045 Uiso 1 1 calc R . . C403 C 0.3834(4) 0.3939(3) 0.0168(3) 0.0374(16) Uani 1 1 d DU . . H40H H 0.4040 0.4371 0.0028 0.056 Uiso 1 1 calc R . . H40I H 0.3787 0.3955 0.0600 0.056 Uiso 1 1 calc R . . H40J H 0.3283 0.3829 -0.0012 0.056 Uiso 1 1 calc R . . C404 C 0.4886(4) 0.2273(3) -0.0004(3) 0.0389(16) Uani 1 1 d DU . . H40K H 0.4959 0.2308 -0.0437 0.047 Uiso 1 1 calc R . . H40L H 0.5419 0.2430 0.0191 0.047 Uiso 1 1 calc R . . C405 C 0.4720(4) 0.1551(3) 0.0146(3) 0.0383(16) Uani 1 1 d DU . . H40M H 0.5186 0.1292 0.0008 0.057 Uiso 1 1 calc R . . H40N H 0.4199 0.1388 -0.0050 0.057 Uiso 1 1 calc R . . H40O H 0.4670 0.1508 0.0576 0.057 Uiso 1 1 calc R . . C406 C 0.3379(4) 0.2500(3) -0.0123(3) 0.0368(16) Uani 1 1 d DU . . H40P H 0.2946 0.2819 -0.0026 0.044 Uiso 1 1 calc R . . H40Q H 0.3193 0.2067 0.0037 0.044 Uiso 1 1 calc R . . C407 C 0.3431(5) 0.2436(4) -0.0800(3) 0.0430(17) Uani 1 1 d DU . . H40R H 0.2882 0.2288 -0.0964 0.064 Uiso 1 1 calc R . . H40S H 0.3847 0.2113 -0.0902 0.064 Uiso 1 1 calc R . . H40T H 0.3597 0.2865 -0.0965 0.064 Uiso 1 1 calc R . . N5 N 0.5226(3) 0.2863(2) 0.5409(2) 0.0199(11) Uani 1 1 d D . . C500 C 0.4551(4) 0.2344(3) 0.5535(3) 0.0253(14) Uani 1 1 d DU . . H50A H 0.4823 0.1932 0.5644 0.030 Uiso 1 1 calc R . . H50B H 0.4221 0.2253 0.5167 0.030 Uiso 1 1 calc R . . C501 C 0.3950(4) 0.2521(3) 0.6024(3) 0.0314(15) Uani 1 1 d DU . . H50C H 0.3535 0.2157 0.6073 0.047 Uiso 1 1 calc R . . H50D H 0.3664 0.2922 0.5918 0.047 Uiso 1 1 calc R . . H50E H 0.4265 0.2598 0.6397 0.047 Uiso 1 1 calc R . . C502 C 0.5658(4) 0.2683(3) 0.4837(3) 0.0288(14) Uani 1 1 d DU . . H50F H 0.6024 0.3063 0.4720 0.035 Uiso 1 1 calc R . . H50G H 0.5226 0.2609 0.4522 0.035 Uiso 1 1 calc R . . C503 C 0.6185(5) 0.2074(3) 0.4871(3) 0.0387(16) Uani 1 1 d DU . . H50H H 0.6439 0.1994 0.4486 0.058 Uiso 1 1 calc R . . H50I H 0.5827 0.1690 0.4976 0.058 Uiso 1 1 calc R . . H50J H 0.6627 0.2146 0.5174 0.058 Uiso 1 1 calc R . . C504 C 0.4853(4) 0.3530(3) 0.5324(3) 0.0258(14) Uani 1 1 d DU . . H50K H 0.5308 0.3850 0.5215 0.031 Uiso 1 1 calc R . . H50L H 0.4630 0.3679 0.5708 0.031 Uiso 1 1 calc R . . C505 C 0.4160(4) 0.3554(3) 0.4860(3) 0.0265(14) Uani 1 1 d DU . . H50M H 0.3963 0.4004 0.4837 0.040 Uiso 1 1 calc R . . H50N H 0.3694 0.3252 0.4968 0.040 Uiso 1 1 calc R . . H50O H 0.4375 0.3421 0.4474 0.040 Uiso 1 1 calc R . . C506 C 0.5836(4) 0.2907(3) 0.5927(3) 0.0254(14) Uani 1 1 d DU . . H50P H 0.5520 0.3010 0.6289 0.030 Uiso 1 1 calc R . . H50Q H 0.6071 0.2467 0.5981 0.030 Uiso 1 1 calc R . . C507 C 0.6551(4) 0.3406(3) 0.5880(3) 0.0339(15) Uani 1 1 d DU . . H50R H 0.6904 0.3395 0.6239 0.051 Uiso 1 1 calc R . . H50S H 0.6331 0.3847 0.5838 0.051 Uiso 1 1 calc R . . H50T H 0.6885 0.3301 0.5534 0.051 Uiso 1 1 calc R . . N6 N 0.0467(3) 0.7210(2) 0.4534(2) 0.0208(11) Uani 1 1 d D . . C600 C 0.0004(4) 0.6982(4) 0.5075(3) 0.0369(16) Uani 1 1 d DU . . H60A H -0.0527 0.7216 0.5095 0.044 Uiso 1 1 calc R . . H60B H -0.0142 0.6505 0.5027 0.044 Uiso 1 1 calc R . . C601 C 0.0468(4) 0.7088(4) 0.5651(3) 0.0484(18) Uani 1 1 d DU . . H60C H 0.0115 0.6931 0.5975 0.073 Uiso 1 1 calc R . . H60D H 0.0608 0.7560 0.5709 0.073 Uiso 1 1 calc R . . H60E H 0.0984 0.6843 0.5645 0.073 Uiso 1 1 calc R . . C602 C 0.0686(4) 0.7937(3) 0.4571(3) 0.0400(17) Uani 1 1 d DU . . H60F H 0.0970 0.8067 0.4201 0.048 Uiso 1 1 calc R . . H60G H 0.1093 0.8017 0.4901 0.048 Uiso 1 1 calc R . . C603 C -0.0044(5) 0.8382(3) 0.4661(3) 0.0455(18) Uani 1 1 d DU . . H60H H 0.0164 0.8843 0.4679 0.068 Uiso 1 1 calc R . . H60I H -0.0322 0.8270 0.5033 0.068 Uiso 1 1 calc R . . H60J H -0.0445 0.8320 0.4330 0.068 Uiso 1 1 calc R . . C604 C 0.1268(4) 0.6862(3) 0.4467(3) 0.0320(15) Uani 1 1 d DU . . H60K H 0.1618 0.6948 0.4828 0.038 Uiso 1 1 calc R . . H60L H 0.1575 0.7055 0.4129 0.038 Uiso 1 1 calc R . . C605 C 0.1169(4) 0.6118(3) 0.4368(3) 0.0355(16) Uani 1 1 d DU . . H60M H 0.1723 0.5933 0.4329 0.053 Uiso 1 1 calc R . . H60N H 0.0838 0.6025 0.4005 0.053 Uiso 1 1 calc R . . H60O H 0.0882 0.5918 0.4705 0.053 Uiso 1 1 calc R . . C606 C -0.0112(4) 0.7065(4) 0.4011(3) 0.0324(15) Uani 1 1 d DU . . H60P H -0.0263 0.6586 0.4004 0.039 Uiso 1 1 calc R . . H60Q H -0.0634 0.7301 0.4073 0.039 Uiso 1 1 calc R . . C607 C 0.0226(4) 0.7250(3) 0.3415(3) 0.0335(15) Uani 1 1 d DU . . H60R H -0.0195 0.7133 0.3107 0.050 Uiso 1 1 calc R . . H60S H 0.0736 0.7010 0.3341 0.050 Uiso 1 1 calc R . . H60T H 0.0358 0.7726 0.3409 0.050 Uiso 1 1 calc R . . N7 N 0.7540(6) 0.9693(5) 0.3933(4) 0.031(3) Uiso 0.515(5) 1 d PD D 1 C700 C 0.7776(9) 0.9284(11) 0.3398(8) 0.058(3) Uiso 0.515(5) 1 d PDU D 1 H70A H 0.8097 0.9569 0.3123 0.070 Uiso 0.515(5) 1 calc PR D 1 H70B H 0.8146 0.8933 0.3530 0.070 Uiso 0.515(5) 1 calc PR D 1 C701 C 0.7028(9) 0.8969(8) 0.3070(7) 0.059(3) Uiso 0.515(5) 1 d PDU D 1 H70C H 0.7220 0.8710 0.2733 0.089 Uiso 0.515(5) 1 calc PR D 1 H70D H 0.6666 0.9313 0.2928 0.089 Uiso 0.515(5) 1 calc PR D 1 H70E H 0.6713 0.8678 0.3338 0.089 Uiso 0.515(5) 1 calc PR D 1 C702 C 0.7881(9) 1.0389(6) 0.3790(6) 0.050(2) Uiso 0.515(5) 1 d PDU D 1 H70F H 0.7778 1.0685 0.4131 0.060 Uiso 0.515(5) 1 calc PR D 1 H70G H 0.8495 1.0377 0.3742 0.060 Uiso 0.515(5) 1 calc PR D 1 C703 C 0.7499(10) 1.0682(8) 0.3233(6) 0.052(3) Uiso 0.515(5) 1 d PDU D 1 H70H H 0.7133 1.1038 0.3346 0.079 Uiso 0.515(5) 1 calc PR D 1 H70I H 0.7172 1.0338 0.3014 0.079 Uiso 0.515(5) 1 calc PR D 1 H70J H 0.7948 1.0860 0.2982 0.079 Uiso 0.515(5) 1 calc PR D 1 C704 C 0.8027(9) 0.9502(7) 0.4467(6) 0.055(3) Uiso 0.515(5) 1 d PDU D 1 H70K H 0.7959 0.9830 0.4789 0.066 Uiso 0.515(5) 1 calc PR D 1 H70L H 0.8630 0.9494 0.4372 0.066 Uiso 0.515(5) 1 calc PR D 1 C705 C 0.7713(13) 0.8812(7) 0.4671(8) 0.055(3) Uiso 0.515(5) 1 d PDU D 1 H70M H 0.8037 0.8686 0.5021 0.082 Uiso 0.515(5) 1 calc PR D 1 H70N H 0.7785 0.8488 0.4352 0.082 Uiso 0.515(5) 1 calc PR D 1 H70O H 0.7119 0.8823 0.4770 0.082 Uiso 0.515(5) 1 calc PR D 1 C706 C 0.6650(6) 0.9742(8) 0.4070(6) 0.054(3) Uiso 0.515(5) 1 d PDU D 1 H70P H 0.6410 0.9289 0.4125 0.065 Uiso 0.515(5) 1 calc PR D 1 H70Q H 0.6365 0.9925 0.3720 0.065 Uiso 0.515(5) 1 calc PR D 1 C707 C 0.6435(8) 1.0154(8) 0.4609(7) 0.066(4) Uiso 0.515(5) 1 d PDU D 1 H70R H 0.5827 1.0133 0.4662 0.099 Uiso 0.515(5) 1 calc PR D 1 H70S H 0.6627 1.0613 0.4550 0.099 Uiso 0.515(5) 1 calc PR D 1 H70T H 0.6712 0.9982 0.4961 0.099 Uiso 0.515(5) 1 calc PR D 1 N7' N 0.7726(6) 0.9819(5) 0.3802(5) 0.034(3) Uiso 0.485(5) 1 d PD D 2 C710 C 0.7622(10) 0.9236(10) 0.3379(9) 0.059(3) Uiso 0.485(5) 1 d PDU D 2 H71A H 0.7441 0.8828 0.3586 0.070 Uiso 0.485(5) 1 calc PR D 2 H71B H 0.7220 0.9320 0.3053 0.070 Uiso 0.485(5) 1 calc PR D 2 C711 C 0.8504(9) 0.9203(9) 0.3160(8) 0.062(4) Uiso 0.485(5) 1 d PDU D 2 H71C H 0.8537 0.8834 0.2878 0.093 Uiso 0.485(5) 1 calc PR D 2 H71D H 0.8886 0.9136 0.3496 0.093 Uiso 0.485(5) 1 calc PR D 2 H71E H 0.8664 0.9616 0.2964 0.093 Uiso 0.485(5) 1 calc PR D 2 C712 C 0.7220(9) 1.0369(7) 0.3555(6) 0.045(3) Uiso 0.485(5) 1 d PDU D 2 H71F H 0.7192 1.0724 0.3858 0.053 Uiso 0.485(5) 1 calc PR D 2 H71G H 0.6641 1.0197 0.3469 0.053 Uiso 0.485(5) 1 calc PR D 2 C713 C 0.7598(8) 1.0661(7) 0.2981(5) 0.038(3) Uiso 0.485(5) 1 d PDU D 2 H71H H 0.7813 1.1114 0.3061 0.056 Uiso 0.485(5) 1 calc PR D 2 H71I H 0.7163 1.0663 0.2671 0.056 Uiso 0.485(5) 1 calc PR D 2 H71J H 0.8056 1.0391 0.2850 0.056 Uiso 0.485(5) 1 calc PR D 2 C714 C 0.8608(8) 1.0066(7) 0.3965(7) 0.047(3) Uiso 0.485(5) 1 d PDU D 2 H71K H 0.8916 1.0162 0.3596 0.057 Uiso 0.485(5) 1 calc PR D 2 H71L H 0.8897 0.9712 0.4172 0.057 Uiso 0.485(5) 1 calc PR D 2 C715 C 0.8647(10) 1.0689(7) 0.4360(7) 0.047(4) Uiso 0.485(5) 1 d PDU D 2 H71M H 0.9233 1.0825 0.4441 0.070 Uiso 0.485(5) 1 calc PR D 2 H71N H 0.8365 1.0594 0.4734 0.070 Uiso 0.485(5) 1 calc PR D 2 H71O H 0.8367 1.1045 0.4157 0.070 Uiso 0.485(5) 1 calc PR D 2 C716 C 0.7286(10) 0.9576(8) 0.4337(6) 0.054(3) Uiso 0.485(5) 1 d PDU D 2 H71P H 0.6720 0.9402 0.4215 0.065 Uiso 0.485(5) 1 calc PR D 2 H71Q H 0.7213 0.9956 0.4608 0.065 Uiso 0.485(5) 1 calc PR D 2 C717 C 0.7718(13) 0.9044(8) 0.4678(9) 0.054(3) Uiso 0.485(5) 1 d PDU D 2 H71R H 0.8325 0.9137 0.4682 0.081 Uiso 0.485(5) 1 calc PR D 2 H71S H 0.7592 0.8614 0.4486 0.081 Uiso 0.485(5) 1 calc PR D 2 H71T H 0.7516 0.9036 0.5085 0.081 Uiso 0.485(5) 1 calc PR D 2 N8 N 0.2604(3) 0.9522(3) 0.9170(3) 0.0321(14) Uani 1 1 d D . . C800 C 0.3092(5) 0.9164(4) 0.9640(3) 0.0498(19) Uani 1 1 d DU . . H80A H 0.2946 0.9339 1.0035 0.060 Uiso 1 1 calc R . . H80B H 0.3698 0.9260 0.9584 0.060 Uiso 1 1 calc R . . C801 C 0.2926(5) 0.8418(4) 0.9628(3) 0.0483(18) Uani 1 1 d DU . . H80C H 0.3264 0.8219 0.9939 0.073 Uiso 1 1 calc R . . H80D H 0.3077 0.8239 0.9241 0.073 Uiso 1 1 calc R . . H80E H 0.2331 0.8318 0.9698 0.073 Uiso 1 1 calc R . . C802 C 0.1674(4) 0.9453(4) 0.9277(3) 0.0323(15) Uani 1 1 d DU . . H80F H 0.1501 0.8979 0.9256 0.039 Uiso 1 1 calc R . . H80G H 0.1376 0.9676 0.8953 0.039 Uiso 1 1 calc R . . C803 C 0.1392(4) 0.9737(3) 0.9867(3) 0.0302(15) Uani 1 1 d DU . . H80H H 0.0782 0.9674 0.9897 0.045 Uiso 1 1 calc R . . H80I H 0.1548 1.0209 0.9891 0.045 Uiso 1 1 calc R . . H80J H 0.1664 0.9509 1.0193 0.045 Uiso 1 1 calc R . . C804 C 0.2907(5) 1.0239(4) 0.9186(5) 0.070(3) Uani 1 1 d DU . . H80K H 0.3517 1.0263 0.9112 0.084 Uiso 1 1 calc R . . H80L H 0.2819 1.0422 0.9588 0.084 Uiso 1 1 calc R . . C805 C 0.2469(5) 1.0672(4) 0.8733(5) 0.074(3) Uani 1 1 d DU . . H80M H 0.2693 1.1128 0.8772 0.111 Uiso 1 1 calc R . . H80N H 0.1865 1.0659 0.8805 0.111 Uiso 1 1 calc R . . H80O H 0.2569 1.0506 0.8331 0.111 Uiso 1 1 calc R . . C806 C 0.2741(4) 0.9225(4) 0.8562(3) 0.0400(17) Uani 1 1 d DU . . H80P H 0.2418 0.9471 0.8266 0.048 Uiso 1 1 calc R . . H80Q H 0.2515 0.8763 0.8555 0.048 Uiso 1 1 calc R . . C807 C 0.3654(4) 0.9231(4) 0.8375(3) 0.0493(18) Uani 1 1 d DU . . H80R H 0.3690 0.9033 0.7979 0.074 Uiso 1 1 calc RD . . H80S H 0.3979 0.8977 0.8658 0.074 Uiso 1 1 calc R . . H80T H 0.3881 0.9688 0.8370 0.074 Uiso 1 1 calc R . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Ni1 0.0100(4) 0.0178(4) 0.0182(4) 0.0034(3) -0.0011(3) 0.0033(3) Ni2 0.0088(3) 0.0172(4) 0.0166(4) 0.0024(3) -0.0019(3) 0.0049(3) Ni3 0.0099(3) 0.0161(4) 0.0177(4) 0.0020(3) -0.0019(3) 0.0057(3) Ni4 0.0107(4) 0.0171(4) 0.0186(4) 0.0028(3) -0.0002(3) 0.0063(3) Ni5 0.0190(4) 0.0150(4) 0.0211(4) 0.0025(3) 0.0006(3) 0.0064(3) Ni6 0.0150(4) 0.0157(4) 0.0191(4) 0.0002(3) -0.0026(3) 0.0062(3) Ni7 0.0136(4) 0.0195(4) 0.0168(4) 0.0014(3) -0.0008(3) 0.0047(3) Ni8 0.0107(3) 0.0157(4) 0.0162(4) 0.0030(3) -0.0017(3) 0.0049(3) Ni9 0.0136(4) 0.0153(4) 0.0246(4) 0.0032(3) -0.0023(3) 0.0042(3) Ni10 0.0143(4) 0.0169(4) 0.0206(4) 0.0001(3) -0.0052(3) 0.0055(3) Ni11 0.0156(4) 0.0218(4) 0.0163(4) 0.0015(3) -0.0029(3) 0.0035(3) Ni12 0.0111(4) 0.0155(4) 0.0163(4) 0.0033(3) -0.0018(3) 0.0061(3) Ni13 0.0099(4) 0.0320(5) 0.0196(4) 0.0075(3) -0.0005(3) 0.0100(3) Ni14 0.0102(4) 0.0175(4) 0.0217(4) 0.0027(3) 0.0015(3) 0.0057(3) Ni15 0.0098(4) 0.0210(4) 0.0196(4) 0.0023(3) -0.0017(3) 0.0037(3) Ni16 0.0092(3) 0.0209(4) 0.0226(4) 0.0049(3) -0.0024(3) 0.0061(3) C51 0.0104(9) 0.0158(10) 0.0180(9) 0.0025(8) -0.0022(9) 0.0047(11) C52 0.0099(9) 0.0167(9) 0.0174(10) 0.0028(9) -0.0034(10) 0.0045(11) C53 0.0097(9) 0.0162(9) 0.0172(10) 0.0017(9) -0.0007(9) 0.0060(10) C54 0.0096(9) 0.0156(10) 0.0175(9) 0.0021(7) -0.0014(10) 0.0061(12) C1 0.013(2) 0.023(3) 0.023(3) 0.0030(18) -0.0008(19) 0.0006(17) C2 0.0103(12) 0.017(2) 0.019(2) -0.0010(16) -0.0007(12) 0.0042(13) C3 0.0132(14) 0.018(2) 0.0181(15) 0.0028(17) -0.0030(13) 0.0037(17) C4 0.0117(13) 0.0172(13) 0.0181(14) 0.0017(12) -0.0018(12) 0.0059(12) C5 0.0152(16) 0.0171(16) 0.021(3) 0.0023(14) -0.0043(16) 0.0065(14) C6 0.0113(13) 0.020(2) 0.021(2) 0.0030(17) -0.0013(14) 0.0055(14) C7 0.013(2) 0.018(3) 0.022(2) 0.0043(16) -0.0002(17) 0.007(2) C8 0.020(3) 0.018(3) 0.0180(15) 0.0005(16) -0.0005(16) 0.005(2) C9 0.017(3) 0.0193(16) 0.0218(14) -0.0007(13) -0.004(2) 0.0063(17) C10 0.030(3) 0.0172(12) 0.0223(19) 0.0005(12) 0.000(2) 0.0072(16) C11 0.051(4) 0.017(2) 0.024(2) 0.0037(18) -0.003(3) 0.009(2) C12 0.0137(19) 0.0218(16) 0.0197(14) 0.0067(12) -0.0004(13) 0.0088(16) C13 0.022(3) 0.0172(15) 0.034(2) 0.0069(13) -0.005(2) -0.0003(14) C14 0.019(3) 0.0179(12) 0.0276(18) 0.0001(12) -0.012(2) 0.0069(17) C15 0.012(3) 0.0254(17) 0.0212(13) -0.0009(12) -0.0038(18) 0.0026(19) C16 0.021(3) 0.024(3) 0.0171(16) 0.0008(17) -0.0033(16) 0.011(2) C17 0.012(3) 0.0203(19) 0.0198(16) 0.0048(15) -0.0009(17) 0.0049(18) C19 0.0109(13) 0.026(2) 0.018(3) -0.0034(19) 0.0001(14) 0.0079(15) C20 0.018(2) 0.018(3) 0.027(2) 0.0029(17) 0.0064(19) 0.008(2) C21 0.0136(16) 0.028(2) 0.026(3) 0.0015(19) 0.0024(13) -0.0010(13) C22 0.0104(13) 0.022(3) 0.024(2) -0.0007(17) -0.0022(12) 0.0034(15) C23 0.0094(17) 0.035(3) 0.038(3) 0.018(2) -0.0049(14) 0.0060(17) O1 0.025(3) 0.037(3) 0.039(3) 0.018(2) 0.008(2) 0.004(2) O2 0.0110(15) 0.033(3) 0.033(2) 0.008(2) -0.0025(17) 0.0035(18) O3 0.021(2) 0.036(3) 0.024(2) -0.002(2) -0.0106(16) 0.010(2) O4 0.0145(19) 0.023(2) 0.0206(19) 0.0033(17) -0.0036(15) 0.0084(16) O5 0.023(2) 0.018(2) 0.045(3) 0.001(2) -0.006(2) 0.0111(17) O6 0.0123(17) 0.033(2) 0.022(2) 0.0078(19) -0.0011(16) 0.0083(17) O7 0.031(3) 0.044(3) 0.029(2) 0.010(2) 0.0081(19) -0.001(2) O8 0.036(3) 0.037(3) 0.020(2) 0.0035(19) 0.0084(19) 0.007(2) O9 0.038(3) 0.026(2) 0.0231(19) -0.0067(17) -0.003(2) 0.004(2) O10 0.058(3) 0.0179(17) 0.028(2) -0.0012(17) -0.003(2) 0.003(2) O11 0.081(3) 0.030(2) 0.043(3) 0.0147(18) -0.001(2) 0.005(2) O12 0.031(2) 0.030(2) 0.0232(16) 0.0112(13) 0.0022(15) 0.0079(19) O13 0.039(3) 0.0234(16) 0.050(3) 0.0137(15) 0.001(2) -0.0035(15) O14 0.036(3) 0.0188(17) 0.039(3) -0.0033(18) -0.013(2) 0.0068(19) O15 0.029(2) 0.029(2) 0.0242(18) -0.0061(17) -0.0034(19) 0.002(2) O16 0.038(3) 0.037(3) 0.021(2) 0.0049(19) 0.0049(19) 0.011(2) O17 0.033(3) 0.025(2) 0.023(2) 0.0087(16) -0.0011(19) 0.009(2) O19 0.0118(17) 0.031(2) 0.033(2) 0.002(2) 0.0002(17) 0.0092(17) O20 0.038(3) 0.034(3) 0.040(3) 0.010(2) 0.019(2) 0.007(2) O21 0.0220(17) 0.043(3) 0.040(3) 0.006(2) 0.0100(15) -0.0057(16) O22 0.0114(16) 0.042(3) 0.029(2) 0.006(2) -0.0028(16) 0.0055(18) O23 0.029(2) 0.069(3) 0.044(2) 0.029(2) 0.000(2) 0.020(2) Ni17 0.0194(4) 0.0180(4) 0.0249(4) 0.0056(3) -0.0022(3) 0.0039(3) Ni18 0.0216(4) 0.0176(4) 0.0259(4) 0.0047(3) -0.0024(3) 0.0109(3) Ni19 0.0373(5) 0.0304(5) 0.0235(4) 0.0041(3) -0.0064(4) 0.0192(4) Ni20 0.0287(4) 0.0186(4) 0.0208(4) 0.0036(3) -0.0015(3) 0.0021(3) Ni21 0.0185(4) 0.0211(4) 0.0254(4) 0.0035(3) -0.0055(3) -0.0002(3) Ni22 0.0214(4) 0.0167(4) 0.0240(4) -0.0012(3) -0.0025(3) 0.0045(3) Ni23 0.0178(4) 0.0206(4) 0.0280(4) -0.0003(3) 0.0013(3) 0.0097(3) Ni24 0.0128(4) 0.0173(4) 0.0264(4) -0.0002(3) -0.0053(3) 0.0067(3) Ni25 0.0190(4) 0.0251(4) 0.0395(5) -0.0094(4) -0.0125(4) 0.0086(3) Ni26 0.0223(4) 0.0170(4) 0.0214(4) -0.0003(3) -0.0008(3) 0.0053(3) Ni27 0.0233(4) 0.0218(4) 0.0278(4) 0.0012(3) 0.0050(3) 0.0047(3) Ni28 0.0132(4) 0.0189(4) 0.0247(4) 0.0030(3) -0.0018(3) 0.0030(3) Ni29 0.0153(4) 0.0181(4) 0.0220(4) 0.0045(3) -0.0039(3) 0.0044(3) Ni30 0.0154(4) 0.0174(4) 0.0221(4) 0.0030(3) -0.0007(3) 0.0052(3) Ni31 0.0126(4) 0.0161(4) 0.0253(4) 0.0034(3) 0.0007(3) 0.0070(3) Ni32 0.0137(4) 0.0167(4) 0.0252(4) 0.0033(3) -0.0015(3) 0.0078(3) Ni33 0.0130(11) 0.028(2) 0.0415(19) -0.0054(15) -0.0002(10) 0.0068(11) C61 0.0151(9) 0.0152(13) 0.0217(12) 0.0018(7) -0.0027(7) 0.0059(8) C62 0.0145(10) 0.0160(12) 0.0210(15) 0.0025(7) -0.0026(8) 0.0046(7) C63 0.0147(9) 0.0153(14) 0.0215(12) 0.0025(7) -0.0020(7) 0.0054(8) C64 0.0175(9) 0.0167(13) 0.0211(14) 0.0014(7) -0.0049(8) 0.0061(8) C24 0.025(2) 0.0190(17) 0.031(2) 0.0037(14) -0.0023(14) -0.0005(17) C25 0.028(2) 0.022(2) 0.024(2) 0.0057(15) -0.0003(16) 0.0089(14) C26 0.030(2) 0.036(3) 0.040(3) 0.014(2) 0.005(3) 0.026(3) C27 0.0272(17) 0.0191(13) 0.0292(15) 0.0034(11) 0.0064(13) 0.0009(12) C28 0.038(2) 0.025(2) 0.0282(16) 0.0020(14) 0.0093(18) -0.0007(17) C29 0.056(3) 0.026(2) 0.019(2) 0.0048(16) -0.0044(15) 0.0089(18) C31 0.023(2) 0.024(3) 0.034(3) -0.001(2) -0.010(2) -0.0001(19) C32 0.029(2) 0.021(2) 0.030(2) -0.0027(18) -0.0037(19) 0.0004(18) C33 0.0289(18) 0.0178(17) 0.027(2) 0.0000(17) 0.003(2) 0.0077(18) C34 0.0209(16) 0.022(3) 0.042(4) 0.000(2) 0.0052(19) 0.0105(19) C35 0.0161(15) 0.026(3) 0.040(3) -0.002(2) -0.0083(15) 0.0099(15) C37 0.0260(19) 0.024(2) 0.028(2) -0.0025(18) -0.007(2) 0.0060(19) C38 0.027(2) 0.0196(17) 0.025(2) 0.0011(17) 0.0033(19) 0.0059(18) C40 0.022(2) 0.023(2) 0.0316(19) 0.0022(16) 0.0072(19) 0.0057(16) C41 0.019(2) 0.0179(18) 0.028(2) 0.0056(14) 0.0014(17) 0.0080(15) C43 0.017(2) 0.022(3) 0.026(2) 0.003(2) -0.003(2) 0.007(2) C44 0.019(2) 0.022(2) 0.0239(17) 0.0057(14) -0.0016(15) 0.0028(17) C45 0.0156(18) 0.018(2) 0.040(2) 0.0016(19) 0.004(2) 0.0042(19) O24 0.041(3) 0.033(3) 0.043(3) 0.012(2) -0.011(2) -0.0138(18) O25 0.035(3) 0.020(2) 0.037(3) 0.0095(16) -0.0042(19) 0.0034(18) O26 0.039(2) 0.069(3) 0.056(3) 0.025(3) 0.000(2) 0.032(2) O27 0.035(3) 0.029(3) 0.039(3) 0.0042(18) 0.0126(18) -0.0061(17) O28 0.067(4) 0.034(3) 0.048(3) 0.015(2) 0.031(2) 0.008(3) O29 0.083(4) 0.039(3) 0.035(3) 0.019(2) -0.013(2) -0.001(3) O31 0.032(3) 0.043(3) 0.053(3) -0.004(3) -0.022(2) 0.006(2) O32 0.038(3) 0.037(3) 0.046(3) -0.017(2) -0.011(2) 0.001(2) O33 0.040(3) 0.028(3) 0.037(3) -0.0090(18) 0.000(2) 0.016(2) O34 0.023(2) 0.047(3) 0.073(4) 0.002(3) 0.013(2) 0.019(2) O35 0.0178(18) 0.057(3) 0.063(3) -0.019(3) -0.011(2) 0.016(2) O37 0.036(3) 0.032(3) 0.043(3) -0.0127(19) -0.016(2) 0.010(2) O38 0.041(3) 0.030(3) 0.037(3) -0.0082(19) 0.013(2) 0.004(2) O40 0.035(3) 0.043(3) 0.057(3) 0.022(2) 0.024(2) 0.017(2) O41 0.021(2) 0.025(2) 0.033(3) 0.0118(16) 0.0013(18) 0.0069(17) O43 0.025(2) 0.032(3) 0.046(3) 0.000(2) -0.017(2) 0.009(2) O44 0.026(2) 0.031(3) 0.028(2) 0.0127(17) -0.0016(18) 0.0035(19) O45 0.024(2) 0.034(3) 0.056(3) 0.014(2) 0.012(2) 0.004(2) N1 0.012(3) 0.019(3) 0.022(3) 0.008(2) -0.002(2) 0.007(2) C100 0.022(3) 0.029(3) 0.026(3) 0.004(3) -0.005(3) 0.008(3) C101 0.018(3) 0.028(3) 0.041(4) 0.000(3) -0.007(3) 0.006(3) C102 0.020(3) 0.018(3) 0.033(3) 0.003(3) -0.003(3) 0.005(2) C103 0.025(3) 0.025(3) 0.038(3) -0.004(3) 0.002(3) 0.000(3) C104 0.023(3) 0.023(3) 0.025(3) 0.008(2) -0.002(3) 0.005(3) C105 0.027(3) 0.031(3) 0.032(3) 0.003(3) 0.003(3) 0.010(3) C106 0.027(3) 0.019(3) 0.028(3) 0.006(3) 0.002(3) 0.005(3) C107 0.025(3) 0.018(3) 0.027(3) 0.001(2) 0.005(3) 0.000(2) N2 0.016(3) 0.015(3) 0.029(3) 0.005(2) -0.005(2) 0.006(2) C200 0.030(3) 0.029(3) 0.043(4) 0.002(3) -0.006(3) 0.016(3) C201 0.037(4) 0.037(4) 0.049(4) -0.008(3) 0.001(3) 0.020(3) C202 0.030(3) 0.033(3) 0.036(3) 0.002(3) -0.015(3) 0.014(3) C203 0.030(3) 0.034(3) 0.041(4) 0.002(3) -0.020(3) 0.006(3) C204 0.028(3) 0.030(3) 0.030(3) 0.003(3) -0.004(3) 0.004(3) C205 0.024(3) 0.040(4) 0.030(3) -0.002(3) 0.003(3) 0.008(3) C206 0.040(4) 0.023(3) 0.038(4) 0.003(3) 0.006(3) 0.006(3) C207 0.036(4) 0.028(3) 0.035(4) -0.003(3) 0.004(3) -0.004(3) N3 0.012(3) 0.016(3) 0.025(3) 0.001(2) 0.002(2) 0.006(2) C300 0.020(3) 0.024(3) 0.037(3) 0.002(3) 0.002(3) 0.007(3) C301 0.021(3) 0.027(3) 0.038(3) 0.010(3) 0.003(3) 0.010(3) C302 0.031(3) 0.029(3) 0.031(3) 0.004(3) -0.004(3) 0.009(3) C303 0.027(3) 0.033(3) 0.030(3) 0.009(3) -0.003(3) 0.013(3) C304 0.026(3) 0.029(3) 0.037(3) -0.003(3) 0.008(3) 0.004(3) C305 0.032(4) 0.028(3) 0.045(4) -0.008(3) 0.012(3) 0.009(3) C306 0.026(3) 0.032(4) 0.039(4) -0.002(3) -0.003(3) 0.012(3) C307 0.023(3) 0.030(4) 0.042(4) -0.005(3) -0.002(3) 0.001(3) N4 0.013(3) 0.024(3) 0.024(3) 0.000(2) -0.001(2) 0.004(2) C400 0.033(4) 0.040(4) 0.042(4) 0.004(3) 0.002(3) 0.009(3) C401 0.035(4) 0.047(4) 0.037(4) 0.004(3) -0.005(3) 0.002(3) C402 0.028(4) 0.031(4) 0.052(4) 0.007(3) -0.004(3) 0.003(3) C403 0.034(4) 0.019(3) 0.061(4) 0.004(3) -0.010(3) 0.010(3) C404 0.023(3) 0.039(4) 0.055(4) -0.005(3) 0.000(3) 0.010(3) C405 0.025(3) 0.026(3) 0.065(4) 0.001(3) -0.002(3) 0.012(3) C406 0.029(4) 0.030(4) 0.052(4) -0.001(3) -0.005(3) 0.011(3) C407 0.045(4) 0.033(4) 0.051(4) -0.006(3) -0.015(3) 0.011(3) N5 0.020(3) 0.021(3) 0.019(3) 0.006(2) 0.000(2) 0.008(2) C500 0.023(3) 0.022(3) 0.032(3) 0.007(3) 0.004(3) 0.006(3) C501 0.024(3) 0.033(3) 0.039(4) 0.015(3) 0.012(3) 0.010(3) C502 0.029(3) 0.033(4) 0.026(3) -0.001(3) 0.009(3) 0.010(3) C503 0.043(4) 0.043(4) 0.032(3) 0.002(3) 0.011(3) 0.020(3) C504 0.025(3) 0.025(3) 0.028(3) 0.001(3) -0.001(3) 0.012(3) C505 0.025(3) 0.025(3) 0.030(3) 0.009(3) -0.001(3) 0.010(3) C506 0.021(3) 0.030(3) 0.026(3) 0.005(3) -0.002(3) 0.010(3) C507 0.024(3) 0.040(4) 0.037(3) 0.001(3) -0.009(3) 0.006(3) N6 0.011(3) 0.023(3) 0.029(3) 0.001(2) -0.001(2) 0.006(2) C600 0.021(3) 0.059(4) 0.032(3) 0.004(3) 0.003(3) 0.011(3) C601 0.033(4) 0.076(5) 0.037(4) 0.006(4) 0.002(3) 0.016(3) C602 0.041(4) 0.032(4) 0.047(4) -0.005(3) 0.000(3) 0.008(3) C603 0.052(4) 0.032(4) 0.054(4) 0.000(3) 0.012(3) 0.017(3) C604 0.018(3) 0.040(4) 0.040(4) 0.002(3) 0.000(3) 0.017(3) C605 0.030(3) 0.037(4) 0.041(4) 0.007(3) -0.001(3) 0.012(3) C606 0.022(3) 0.044(4) 0.032(3) 0.002(3) -0.009(3) 0.009(3) C607 0.029(3) 0.042(4) 0.030(3) 0.002(3) -0.007(3) 0.006(3) N8 0.016(3) 0.027(3) 0.053(4) -0.006(3) 0.007(3) 0.001(2) C800 0.031(4) 0.066(4) 0.054(4) -0.010(4) -0.009(3) 0.017(4) C801 0.037(4) 0.059(4) 0.051(4) 0.007(4) -0.006(3) 0.018(4) C802 0.024(3) 0.040(4) 0.033(3) -0.003(3) -0.001(3) 0.001(3) C803 0.020(3) 0.038(4) 0.033(3) -0.005(3) -0.005(3) 0.007(3) C804 0.045(5) 0.030(4) 0.135(7) -0.022(4) 0.030(5) -0.001(3) C805 0.045(5) 0.028(4) 0.150(8) -0.003(4) 0.029(5) 0.003(3) C806 0.036(4) 0.032(4) 0.052(4) -0.003(3) 0.012(3) 0.008(3) C807 0.041(4) 0.042(4) 0.066(4) -0.006(4) 0.022(4) 0.005(3) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Ni1 C1 1.746(6) . ? Ni1 C2 1.885(5) . ? Ni1 C54 1.994(6) . ? Ni1 Ni2 2.3583(10) . ? Ni1 Ni12 2.5852(10) . ? Ni1 Ni5 2.5910(10) . ? Ni1 Ni4 2.8876(11) . ? Ni2 C2 1.885(6) . ? Ni2 C3 1.895(6) . ? Ni2 C4 2.011(6) . ? Ni2 C53 2.115(5) . ? Ni2 C54 2.180(5) . ? Ni2 Ni7 2.4222(10) . ? Ni2 Ni8 2.5417(11) . ? Ni2 Ni6 2.7488(10) . ? Ni3 C6 1.872(6) . ? Ni3 C5 1.878(6) . ? Ni3 C4 2.004(6) . ? Ni3 C51 2.128(5) . ? Ni3 C52 2.184(5) . ? Ni3 Ni4 2.3738(11) . ? Ni3 Ni9 2.4452(11) . ? Ni3 Ni8 2.5215(10) . ? Ni3 Ni10 2.7385(10) . ? Ni4 C7 1.747(6) . ? Ni4 C6 1.874(5) . ? Ni4 C52 1.988(6) . ? Ni4 Ni12 2.5717(10) . ? Ni4 Ni11 2.5867(10) . ? Ni5 C11 1.754(6) . ? Ni5 C10 1.924(6) . ? Ni5 C54 2.035(6) . ? Ni5 Ni6 2.3987(11) . ? Ni5 C18 2.463(8) . ? Ni5 Ni12 2.5355(10) . ? Ni5 Ni13 2.5414(11) . ? Ni6 C9 1.763(6) . ? Ni6 C10 1.852(6) . ? Ni6 C54 2.078(5) . ? Ni6 C53 2.079(6) . ? Ni6 Ni7 2.4172(11) . ? Ni6 Ni13 2.7833(11) . ? Ni7 C8 1.736(6) . ? Ni7 C3 1.938(6) . ? Ni7 C53 2.072(6) . ? Ni7 C9 2.254(6) . ? Ni7 Ni14 2.5795(11) . ? Ni7 Ni8 2.7311(10) . ? Ni8 C12 1.780(6) . ? Ni8 C4 2.021(5) . ? Ni8 C51 2.122(5) . ? Ni8 C53 2.141(6) . ? Ni8 Ni90 2.576(17) . ? Ni8 Ni14 2.6087(10) . ? Ni8 Ni15 2.6398(10) . ? Ni8 Ni9 2.7435(10) . ? Ni9 C13 1.771(6) . ? Ni9 C5 1.966(6) . ? Ni9 C14 2.086(6) . ? Ni9 C51 2.100(6) . ? Ni9 Ni90 2.244(16) . ? Ni9 Ni10 2.3932(11) . ? Ni9 Ni15 2.6069(10) . ? Ni10 C14 1.787(6) . ? Ni10 C15 1.811(6) . ? Ni10 C52 2.075(6) . ? Ni10 C51 2.078(6) . ? Ni10 Ni11 2.3904(11) . ? Ni10 Ni16 2.7113(10) . ? Ni11 C16 1.732(6) . ? Ni11 C15 1.974(6) . ? Ni11 C52 2.043(6) . ? Ni11 C23 2.463(6) . ? Ni11 Ni16 2.5360(11) . ? Ni11 Ni12 2.5648(10) . ? Ni12 C17 1.778(6) . ? Ni12 C54 1.990(5) . ? Ni12 C52 2.011(6) . ? Ni12 Ni16 2.7294(11) . ? Ni12 Ni13 2.7382(10) . ? Ni13 C18' 1.68(3) . ? Ni13 C18 1.759(8) . ? Ni13 C19 1.875(6) . ? Ni13 C53 2.058(5) . ? Ni13 C54 2.098(5) . ? Ni13 Ni14 2.3700(11) . ? Ni14 C20 1.748(6) . ? Ni14 C19 1.888(6) . ? Ni14 C53 1.939(6) . ? Ni14 Ni15 2.8488(11) . ? Ni15 C21 1.746(6) . ? Ni15 C22 1.900(6) . ? Ni15 C51 1.931(6) . ? Ni15 Ni90 2.230(17) . ? Ni15 Ni16 2.3745(11) . ? Ni16 C23 1.743(6) . ? Ni16 C22 1.880(6) . ? Ni16 C51 2.087(5) . ? Ni16 C52 2.112(5) . ? Ni90 C21 1.839(17) . ? Ni90 C13 1.874(17) . ? Ni90 C12 1.922(17) . ? Ni90 O12 2.255(17) . ? Ni90 O21 2.366(17) . ? Ni90 O13 2.407(17) . ? C51 C52 1.403(8) . ? C53 C54 1.411(8) . ? C1 O1 1.141(7) . ? C2 O2 1.177(6) . ? C3 O3 1.157(6) . ? C4 O4 1.192(6) . ? C5 O5 1.167(6) . ? C6 O6 1.187(6) . ? C7 O7 1.142(7) . ? C8 O8 1.148(7) . ? C9 O9 1.163(7) . ? C10 O10 1.165(7) . ? C11 O11 1.152(7) . ? C12 O12 1.141(7) . ? C13 O13 1.137(7) . ? C14 O14 1.170(7) . ? C15 O15 1.188(7) . ? C16 O16 1.146(7) . ? C17 O17 1.147(7) . ? C18 O18 1.193(9) . ? C18' O18' 1.14(3) . ? C19 O19 1.174(6) . ? C20 O20 1.140(7) . ? C21 O21 1.156(7) . ? C22 O22 1.176(7) . ? C23 O23 1.166(7) . ? Ni17 C25 1.896(6) . ? Ni17 C24 1.896(6) . ? Ni17 C27 2.031(6) . ? Ni17 C62 2.119(6) . ? Ni17 C61 2.181(6) . ? Ni17 Ni18 2.3786(11) . ? Ni17 Ni21 2.4539(11) . ? Ni17 Ni28 2.5389(11) . ? Ni17 Ni22 2.7198(11) . ? Ni18 C26 1.733(6) . ? Ni18 C25 1.890(7) . ? Ni18 C61 1.958(6) . ? Ni18 Ni24 2.5925(11) . ? Ni18 Ni23 2.5938(12) . ? Ni18 Ni19 2.8946(12) . ? Ni19 C30' 1.690(16) . ? Ni19 C30 1.786(15) . ? Ni19 C29 1.885(7) . ? Ni19 C64 2.005(6) . ? Ni19 Ni20 2.3632(12) . ? Ni19 Ni24 2.5372(12) . ? Ni19 Ni25 2.6329(13) . ? Ni20 C29 1.884(6) . ? Ni20 C28 1.897(7) . ? Ni20 C27 2.042(6) . ? Ni20 C63 2.074(6) . ? Ni20 C64 2.163(6) . ? Ni20 Ni27 2.4218(11) . ? Ni20 Ni28 2.5405(11) . ? Ni20 Ni26 2.7955(12) . ? Ni21 C31 1.735(6) . ? Ni21 C24 1.977(6) . ? Ni21 C62 2.005(6) . ? Ni21 C32 2.180(6) . ? Ni21 Ni22 2.4113(11) . ? Ni21 Ni29 2.6186(11) . ? Ni21 Ni28 2.7417(11) . ? Ni22 C32 1.766(6) . ? Ni22 C33 1.824(6) . ? Ni22 C61 2.064(6) . ? Ni22 C62 2.104(6) . ? Ni22 Ni23 2.4048(12) . ? Ni22 Ni30 2.6910(11) . ? Ni23 C34 1.754(6) . ? Ni23 C33 1.963(6) . ? Ni23 C61 2.100(6) . ? Ni23 C40 2.225(6) . ? Ni23 Ni30 2.4520(10) . ? Ni23 Ni24 2.5883(11) . ? Ni24 C35 1.755(6) . ? Ni24 C61 1.993(6) . ? Ni24 C64 2.011(6) . ? Ni24 Ni25 2.5337(11) . ? Ni24 Ni31 2.6587(10) . ? Ni24 Ni30 2.7628(11) . ? Ni25 C36 1.671(15) . ? Ni25 C36' 1.783(14) . ? Ni25 C37 1.934(6) . ? Ni25 C64 2.001(6) . ? Ni25 Ni26 2.3803(11) . ? Ni25 Ni31 2.6828(11) . ? Ni26 C38 1.776(6) . ? Ni26 C37 1.826(6) . ? Ni26 C63 2.052(6) . ? Ni26 C64 2.102(6) . ? Ni26 Ni27 2.3904(12) . ? Ni26 Ni31 2.8631(11) . ? Ni27 C46' 1.73(4) . ? Ni27 C46 1.763(10) . ? Ni27 C28 1.930(7) . ? Ni27 C38 2.124(6) . ? Ni27 C63 2.180(6) . ? Ni27 Ni33 2.222(4) . ? Ni27 Ni32 2.5561(11) . ? Ni27 Ni28 2.7687(11) . ? Ni28 C39' 1.73(4) . ? Ni28 C39 1.778(9) . ? Ni28 C27 2.011(6) . ? Ni28 C63 2.064(6) . ? Ni28 C62 2.234(6) . ? Ni28 Ni33 2.587(4) . ? Ni28 Ni32 2.6080(11) . ? Ni28 Ni29 2.6452(11) . ? Ni29 C43 1.746(6) . ? Ni29 C62 1.935(6) . ? Ni29 C44 1.941(6) . ? Ni29 Ni30 2.3732(11) . ? Ni29 Ni32 2.7898(11) . ? Ni30 C40 1.776(6) . ? Ni30 C44 1.857(6) . ? Ni30 C62 2.095(6) . ? Ni30 C61 2.114(6) . ? Ni30 Ni31 2.8667(11) . ? Ni31 C45 1.747(6) . ? Ni31 C41 1.917(6) . ? Ni31 C63 2.085(6) . ? Ni31 C64 2.134(6) . ? Ni31 Ni32 2.3708(10) . ? Ni32 C42 1.729(11) . ? Ni32 C42' 1.83(4) . ? Ni32 C41 1.875(6) . ? Ni32 C63 1.934(6) . ? Ni32 Ni33 2.388(4) . ? C39 O39 1.151(10) . ? C42 O42 1.194(12) . ? C46 O46 1.172(11) . ? Ni33 C42' 1.65(4) . ? Ni33 C47' 1.72(4) . ? Ni33 C39' 2.11(3) . ? Ni33 C46' 2.17(4) . ? C39' O39' 1.21(4) . ? C42' O42' 1.38(5) . ? C46' O46' 1.13(4) . ? C47' O47' 1.152(10) . ? C61 C62 1.389(8) . ? C63 C64 1.397(8) . ? C24 O24 1.159(7) . ? C25 O25 1.167(7) . ? C26 O26 1.161(7) . ? C27 O27 1.177(7) . ? C28 O28 1.162(7) . ? C29 O29 1.168(8) . ? C30 O30 1.112(16) . ? C30' O30' 1.168(18) . ? C31 O31 1.159(7) . ? C32 O32 1.167(7) . ? C33 O33 1.177(7) . ? C34 O34 1.145(7) . ? C35 O35 1.152(7) . ? C36 O36 1.184(17) . ? C36' O36' 1.179(16) . ? C37 O37 1.176(7) . ? C38 O38 1.170(7) . ? C40 O40 1.164(7) . ? C41 O41 1.168(7) . ? C43 O43 1.145(7) . ? C44 O44 1.169(7) . ? C45 O45 1.146(7) . ? N1 C104 1.509(7) . ? N1 C106 1.518(7) . ? N1 C102 1.520(7) . ? N1 C100 1.524(7) . ? C100 C101 1.499(8) . ? C100 H10A 0.9900 . ? C100 H10B 0.9900 . ? C101 H10C 0.9800 . ? C101 H10D 0.9800 . ? C101 H10E 0.9800 . ? C102 C103 1.509(8) . ? C102 H10F 0.9900 . ? C102 H10G 0.9900 . ? C103 H10H 0.9800 . ? C103 H10I 0.9800 . ? C103 H10J 0.9800 . ? C104 C105 1.517(7) . ? C104 H10K 0.9900 . ? C104 H10L 0.9900 . ? C105 H10M 0.9800 . ? C105 H10N 0.9800 . ? C105 H10O 0.9800 . ? C106 C107 1.512(8) . ? C106 H10P 0.9900 . ? C106 H10Q 0.9900 . ? C107 H10R 0.9800 . ? C107 H10S 0.9800 . ? C107 H10T 0.9800 . ? N2 C206 1.500(7) . ? N2 C202 1.503(7) . ? N2 C200 1.510(7) . ? N2 C204 1.521(7) . ? C200 C201 1.527(8) . ? C200 H20A 0.9900 . ? C200 H20B 0.9900 . ? C201 H20C 0.9800 . ? C201 H20D 0.9800 . ? C201 H20E 0.9800 . ? C202 C203 1.533(8) . ? C202 H20F 0.9900 . ? C202 H20G 0.9900 . ? C203 H20H 0.9800 . ? C203 H20I 0.9800 . ? C203 H20J 0.9800 . ? C204 C205 1.511(8) . ? C204 H20K 0.9900 . ? C204 H20L 0.9900 . ? C205 H20M 0.9800 . ? C205 H20N 0.9800 . ? C205 H20O 0.9800 . ? C206 C207 1.527(8) . ? C206 H20P 0.9900 . ? C206 H20Q 0.9900 . ? C207 H20R 0.9800 . ? C207 H20S 0.9800 . ? C207 H20T 0.9800 . ? N3 C302 1.505(7) . ? N3 C300 1.505(7) . ? N3 C306 1.509(7) . ? N3 C304 1.513(7) . ? C300 C301 1.522(8) . ? C300 H30A 0.9900 . ? C300 H30B 0.9900 . ? C301 H30C 0.9800 . ? C301 H30D 0.9800 . ? C301 H30E 0.9800 . ? C302 C303 1.520(8) . ? C302 H30F 0.9900 . ? C302 H30G 0.9900 . ? C303 H30H 0.9800 . ? C303 H30I 0.9800 . ? C303 H30J 0.9800 . ? C304 C305 1.533(8) . ? C304 H30K 0.9900 . ? C304 H30L 0.9900 . ? C305 H30M 0.9800 . ? C305 H30N 0.9800 . ? C305 H30O 0.9800 . ? C306 C307 1.518(8) . ? C306 H30P 0.9900 . ? C306 H30Q 0.9900 . ? C307 H30R 0.9800 . ? C307 H30S 0.9800 . ? C307 H30T 0.9800 . ? N4 C400 1.499(8) . ? N4 C402 1.499(8) . ? N4 C406 1.518(7) . ? N4 C404 1.525(7) . ? C400 C401 1.542(8) . ? C400 H40A 0.9900 . ? C400 H40B 0.9900 . ? C401 H40C 0.9800 . ? C401 H40D 0.9800 . ? C401 H40E 0.9800 . ? C402 C403 1.550(8) . ? C402 H40F 0.9900 . ? C402 H40G 0.9900 . ? C403 H40H 0.9800 . ? C403 H40I 0.9800 . ? C403 H40J 0.9800 . ? C404 C405 1.520(9) . ? C404 H40K 0.9900 . ? C404 H40L 0.9900 . ? C405 H40M 0.9800 . ? C405 H40N 0.9800 . ? C405 H40O 0.9800 . ? C406 C407 1.535(9) . ? C406 H40P 0.9900 . ? C406 H40Q 0.9900 . ? C407 H40R 0.9800 . ? C407 H40S 0.9800 . ? C407 H40T 0.9800 . ? N5 C500 1.507(7) . ? N5 C506 1.511(7) . ? N5 C504 1.514(7) . ? N5 C502 1.520(7) . ? C500 C501 1.523(8) . ? C500 H50A 0.9900 . ? C500 H50B 0.9900 . ? C501 H50C 0.9800 . ? C501 H50D 0.9800 . ? C501 H50E 0.9800 . ? C502 C503 1.526(8) . ? C502 H50F 0.9900 . ? C502 H50G 0.9900 . ? C503 H50H 0.9800 . ? C503 H50I 0.9800 . ? C503 H50J 0.9800 . ? C504 C505 1.515(8) . ? C504 H50K 0.9900 . ? C504 H50L 0.9900 . ? C505 H50M 0.9800 . ? C505 H50N 0.9800 . ? C505 H50O 0.9800 . ? C506 C507 1.500(8) . ? C506 H50P 0.9900 . ? C506 H50Q 0.9900 . ? C507 H50R 0.9800 . ? C507 H50S 0.9800 . ? C507 H50T 0.9800 . ? N6 C604 1.495(6) . ? N6 C602 1.502(7) . ? N6 C600 1.505(7) . ? N6 C606 1.507(7) . ? C600 C601 1.495(8) . ? C600 H60A 0.9900 . ? C600 H60B 0.9900 . ? C601 H60C 0.9800 . ? C601 H60D 0.9800 . ? C601 H60E 0.9800 . ? C602 C603 1.518(8) . ? C602 H60F 0.9900 . ? C602 H60G 0.9900 . ? C603 H60H 0.9800 . ? C603 H60I 0.9800 . ? C603 H60J 0.9800 . ? C604 C605 1.523(8) . ? C604 H60K 0.9900 . ? C604 H60L 0.9900 . ? C605 H60M 0.9800 . ? C605 H60N 0.9800 . ? C605 H60O 0.9800 . ? C606 C607 1.504(8) . ? C606 H60P 0.9900 . ? C606 H60Q 0.9900 . ? C607 H60R 0.9800 . ? C607 H60S 0.9800 . ? C607 H60T 0.9800 . ? N7 C706 1.466(10) . ? N7 C704 1.489(11) . ? N7 C700 1.517(11) . ? N7 C702 1.531(11) . ? C700 C701 1.510(12) . ? C700 H70A 0.9900 . ? C700 H70B 0.9900 . ? C701 H70C 0.9800 . ? C701 H70D 0.9800 . ? C701 H70E 0.9800 . ? C702 C703 1.527(12) . ? C702 H70F 0.9900 . ? C702 H70G 0.9900 . ? C703 H70H 0.9800 . ? C703 H70I 0.9800 . ? C703 H70J 0.9800 . ? C704 C705 1.546(12) . ? C704 H70K 0.9900 . ? C704 H70L 0.9900 . ? C705 H70M 0.9800 . ? C705 H70N 0.9800 . ? C705 H70O 0.9800 . ? C706 C707 1.518(12) . ? C706 H70P 0.9900 . ? C706 H70Q 0.9900 . ? C707 H70R 0.9800 . ? C707 H70S 0.9800 . ? C707 H70T 0.9800 . ? N7' C716 1.486(11) . ? N7' C712 1.510(11) . ? N7' C710 1.512(11) . ? N7' C714 1.514(11) . ? C710 C711 1.504(13) . ? C710 H71A 0.9900 . ? C710 H71B 0.9900 . ? C711 H71C 0.9800 . ? C711 H71D 0.9800 . ? C711 H71E 0.9800 . ? C712 C713 1.553(11) . ? C712 H71F 0.9900 . ? C712 H71G 0.9900 . ? C713 H71H 0.9800 . ? C713 H71I 0.9800 . ? C713 H71J 0.9800 . ? C714 C715 1.535(12) . ? C714 H71K 0.9900 . ? C714 H71L 0.9900 . ? C715 H71M 0.9800 . ? C715 H71N 0.9800 . ? C715 H71O 0.9800 . ? C716 C717 1.516(12) . ? C716 H71P 0.9900 . ? C716 H71Q 0.9900 . ? C717 H71R 0.9800 . ? C717 H71S 0.9800 . ? C717 H71T 0.9800 . ? N8 C802 1.510(7) . ? N8 C804 1.514(8) . ? N8 C806 1.515(8) . ? N8 C800 1.517(8) . ? C800 C801 1.525(10) . ? C800 H80A 0.9900 . ? C800 H80B 0.9900 . ? C801 H80C 0.9800 . ? C801 H80D 0.9800 . ? C801 H80E 0.9800 . ? C802 C803 1.527(8) . ? C802 H80F 0.9900 . ? C802 H80G 0.9900 . ? C803 H80H 0.9800 . ? C803 H80I 0.9800 . ? C803 H80J 0.9800 . ? C804 C805 1.536(11) . ? C804 H80K 0.9900 . ? C804 H80L 0.9900 . ? C805 H80M 0.9800 . ? C805 H80N 0.9800 . ? C805 H80O 0.9800 . ? C806 C807 1.524(8) . ? C806 H80P 0.9900 . ? C806 H80Q 0.9900 . ? C807 H80R 0.9800 . ? C807 H80S 0.9800 . ? C807 H80T 0.9800 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C1 Ni1 C2 109.7(3) . . ? C1 Ni1 C54 138.6(2) . . ? C2 Ni1 C54 110.7(2) . . ? C1 Ni1 Ni2 159.85(19) . . ? C2 Ni1 Ni2 51.29(17) . . ? C54 Ni1 Ni2 59.41(16) . . ? C1 Ni1 Ni12 102.19(19) . . ? C2 Ni1 Ni12 138.78(18) . . ? C54 Ni1 Ni12 49.48(16) . . ? Ni2 Ni1 Ni12 97.72(4) . . ? C1 Ni1 Ni5 90.13(19) . . ? C2 Ni1 Ni5 143.51(17) . . ? C54 Ni1 Ni5 50.68(16) . . ? Ni2 Ni1 Ni5 103.02(4) . . ? Ni12 Ni1 Ni5 58.66(3) . . ? C1 Ni1 Ni4 99.6(2) . . ? C2 Ni1 Ni4 92.94(17) . . ? C54 Ni1 Ni4 87.64(16) . . ? Ni2 Ni1 Ni4 88.98(3) . . ? Ni12 Ni1 Ni4 55.73(2) . . ? Ni5 Ni1 Ni4 114.28(3) . . ? C2 Ni2 C3 100.2(2) . . ? C2 Ni2 C4 103.8(2) . . ? C3 Ni2 C4 90.8(2) . . ? C2 Ni2 C53 141.2(2) . . ? C3 Ni2 C53 105.2(2) . . ? C4 Ni2 C53 104.8(2) . . ? C2 Ni2 C54 103.2(2) . . ? C3 Ni2 C54 131.0(2) . . ? C4 Ni2 C54 123.6(2) . . ? C53 Ni2 C54 38.3(2) . . ? C2 Ni2 Ni1 51.28(17) . . ? C3 Ni2 Ni1 133.37(18) . . ? C4 Ni2 Ni1 127.95(16) . . ? C53 Ni2 Ni1 90.18(16) . . ? C54 Ni2 Ni1 51.96(15) . . ? C2 Ni2 Ni7 144.52(17) . . ? C3 Ni2 Ni7 51.62(17) . . ? C4 Ni2 Ni7 98.25(16) . . ? C53 Ni2 Ni7 53.82(15) . . ? C54 Ni2 Ni7 86.79(15) . . ? Ni1 Ni2 Ni7 128.96(4) . . ? C2 Ni2 Ni8 147.75(17) . . ? C3 Ni2 Ni8 100.00(18) . . ? C4 Ni2 Ni8 51.09(16) . . ? C53 Ni2 Ni8 53.80(16) . . ? C54 Ni2 Ni8 81.70(15) . . ? Ni1 Ni2 Ni8 123.63(4) . . ? Ni7 Ni2 Ni8 66.71(3) . . ? C2 Ni2 Ni6 107.03(17) . . ? C3 Ni2 Ni6 83.99(17) . . ? C4 Ni2 Ni6 149.20(16) . . ? C53 Ni2 Ni6 48.48(15) . . ? C54 Ni2 Ni6 48.19(14) . . ? Ni1 Ni2 Ni6 73.89(3) . . ? Ni7 Ni2 Ni6 55.30(3) . . ? Ni8 Ni2 Ni6 99.89(3) . . ? C6 Ni3 C5 103.1(2) . . ? C6 Ni3 C4 102.1(2) . . ? C5 Ni3 C4 90.2(2) . . ? C6 Ni3 C51 139.8(2) . . ? C5 Ni3 C51 106.2(2) . . ? C4 Ni3 C51 104.6(2) . . ? C6 Ni3 C52 102.0(2) . . ? C5 Ni3 C52 133.1(2) . . ? C4 Ni3 C52 122.0(2) . . ? C51 Ni3 C52 38.0(2) . . ? C6 Ni3 Ni4 50.73(17) . . ? C5 Ni3 Ni4 139.52(18) . . ? C4 Ni3 Ni4 122.21(17) . . ? C51 Ni3 Ni4 89.46(15) . . ? C52 Ni3 Ni4 51.51(15) . . ? C6 Ni3 Ni9 146.13(18) . . ? C5 Ni3 Ni9 52.10(17) . . ? C4 Ni3 Ni9 100.71(17) . . ? C51 Ni3 Ni9 54.14(15) . . ? C52 Ni3 Ni9 86.47(15) . . ? Ni4 Ni3 Ni9 130.54(4) . . ? C6 Ni3 Ni8 146.24(18) . . ? C5 Ni3 Ni8 98.15(18) . . ? C4 Ni3 Ni8 51.50(16) . . ? C51 Ni3 Ni8 53.50(15) . . ? C52 Ni3 Ni8 81.39(15) . . ? Ni4 Ni3 Ni8 120.50(4) . . ? Ni9 Ni3 Ni8 67.04(3) . . ? C6 Ni3 Ni10 107.70(18) . . ? C5 Ni3 Ni10 86.33(17) . . ? C4 Ni3 Ni10 150.02(16) . . ? C51 Ni3 Ni10 48.60(15) . . ? C52 Ni3 Ni10 48.26(15) . . ? Ni4 Ni3 Ni10 76.47(3) . . ? Ni9 Ni3 Ni10 54.64(3) . . ? Ni8 Ni3 Ni10 99.53(3) . . ? C7 Ni4 C6 105.0(3) . . ? C7 Ni4 C52 144.0(2) . . ? C6 Ni4 C52 109.7(2) . . ? C7 Ni4 Ni3 155.34(18) . . ? C6 Ni4 Ni3 50.63(18) . . ? C52 Ni4 Ni3 59.30(16) . . ? C7 Ni4 Ni12 103.98(18) . . ? C6 Ni4 Ni12 143.02(18) . . ? C52 Ni4 Ni12 50.38(16) . . ? Ni3 Ni4 Ni12 99.84(3) . . ? C7 Ni4 Ni11 95.84(19) . . ? C6 Ni4 Ni11 137.92(18) . . ? C52 Ni4 Ni11 51.03(16) . . ? Ni3 Ni4 Ni11 101.66(4) . . ? Ni12 Ni4 Ni11 59.63(3) . . ? C7 Ni4 Ni1 93.48(19) . . ? C6 Ni4 Ni1 99.51(18) . . ? C52 Ni4 Ni1 90.23(16) . . ? Ni3 Ni4 Ni1 94.50(3) . . ? Ni12 Ni4 Ni1 56.17(3) . . ? Ni11 Ni4 Ni1 115.49(3) . . ? C11 Ni5 C10 97.3(3) . . ? C11 Ni5 C54 157.7(3) . . ? C10 Ni5 C54 103.5(2) . . ? C11 Ni5 Ni6 146.5(2) . . ? C10 Ni5 Ni6 49.25(18) . . ? C54 Ni5 Ni6 55.16(16) . . ? C11 Ni5 C18 88.1(3) . . ? C10 Ni5 C18 107.7(3) . . ? C54 Ni5 C18 93.0(2) . . ? Ni6 Ni5 C18 99.10(18) . . ? C11 Ni5 Ni12 108.3(2) . . ? C10 Ni5 Ni12 153.35(18) . . ? C54 Ni5 Ni12 50.17(15) . . ? Ni6 Ni5 Ni12 105.17(4) . . ? C18 Ni5 Ni12 81.01(18) . . ? C11 Ni5 Ni13 128.7(2) . . ? C10 Ni5 Ni13 104.3(2) . . ? C54 Ni5 Ni13 53.18(15) . . ? Ni6 Ni5 Ni13 68.51(3) . . ? C18 Ni5 Ni13 41.12(18) . . ? Ni12 Ni5 Ni13 65.28(3) . . ? C11 Ni5 Ni1 119.1(2) . . ? C10 Ni5 Ni1 100.72(18) . . ? C54 Ni5 Ni1 49.30(15) . . ? Ni6 Ni5 Ni1 76.28(3) . . ? C18 Ni5 Ni1 137.54(19) . . ? Ni12 Ni5 Ni1 60.56(3) . . ? Ni13 Ni5 Ni1 101.88(4) . . ? C9 Ni6 C10 103.0(3) . . ? C9 Ni6 C54 151.6(2) . . ? C10 Ni6 C54 104.5(2) . . ? C9 Ni6 C53 115.9(3) . . ? C10 Ni6 C53 139.7(2) . . ? C54 Ni6 C53 39.7(2) . . ? C9 Ni6 Ni5 154.8(2) . . ? C10 Ni6 Ni5 51.91(19) . . ? C54 Ni6 Ni5 53.51(15) . . ? C53 Ni6 Ni5 88.37(16) . . ? C9 Ni6 Ni7 62.98(19) . . ? C10 Ni6 Ni7 165.94(19) . . ? C54 Ni6 Ni7 89.24(16) . . ? C53 Ni6 Ni7 54.24(16) . . ? Ni5 Ni6 Ni7 142.13(4) . . ? C9 Ni6 Ni2 103.62(18) . . ? C10 Ni6 Ni2 131.86(19) . . ? C54 Ni6 Ni2 51.43(14) . . ? C53 Ni6 Ni2 49.63(15) . . ? Ni5 Ni6 Ni2 97.49(3) . . ? Ni7 Ni6 Ni2 55.48(3) . . ? C9 Ni6 Ni13 133.5(2) . . ? C10 Ni6 Ni13 97.77(19) . . ? C54 Ni6 Ni13 48.51(15) . . ? C53 Ni6 Ni13 47.40(15) . . ? Ni5 Ni6 Ni13 58.17(3) . . ? Ni7 Ni6 Ni13 93.62(3) . . ? Ni2 Ni6 Ni13 92.01(3) . . ? C8 Ni7 C3 106.4(3) . . ? C8 Ni7 C53 142.5(3) . . ? C3 Ni7 C53 105.2(2) . . ? C8 Ni7 C9 101.7(2) . . ? C3 Ni7 C9 90.0(2) . . ? C53 Ni7 C9 97.7(2) . . ? C8 Ni7 Ni6 141.61(19) . . ? C3 Ni7 Ni6 92.78(17) . . ? C53 Ni7 Ni6 54.52(16) . . ? C9 Ni7 Ni6 44.17(15) . . ? C8 Ni7 Ni2 147.35(19) . . ? C3 Ni7 Ni2 50.01(17) . . ? C53 Ni7 Ni2 55.50(15) . . ? C9 Ni7 Ni2 100.55(15) . . ? Ni6 Ni7 Ni2 69.22(3) . . ? C8 Ni7 Ni14 95.6(2) . . ? C3 Ni7 Ni14 148.68(17) . . ? C53 Ni7 Ni14 47.76(15) . . ? C9 Ni7 Ni14 107.28(15) . . ? Ni6 Ni7 Ni14 82.82(3) . . ? Ni2 Ni7 Ni14 100.21(4) . . ? C8 Ni7 Ni8 108.1(2) . . ? C3 Ni7 Ni8 92.74(17) . . ? C53 Ni7 Ni8 50.71(15) . . ? C9 Ni7 Ni8 147.81(15) . . ? Ni6 Ni7 Ni8 103.64(4) . . ? Ni2 Ni7 Ni8 58.74(3) . . ? Ni14 Ni7 Ni8 58.76(3) . . ? C12 Ni8 C4 98.2(2) . . ? C12 Ni8 C51 130.6(2) . . ? C4 Ni8 C51 104.3(2) . . ? C12 Ni8 C53 128.9(2) . . ? C4 Ni8 C53 103.5(2) . . ? C51 Ni8 C53 87.6(2) . . ? C12 Ni8 Ni3 125.03(18) . . ? C4 Ni8 Ni3 50.90(16) . . ? C51 Ni8 Ni3 53.72(15) . . ? C53 Ni8 Ni3 104.23(15) . . ? C12 Ni8 Ni2 125.50(19) . . ? C4 Ni8 Ni2 50.75(16) . . ? C51 Ni8 Ni2 102.45(16) . . ? C53 Ni8 Ni2 52.87(15) . . ? Ni3 Ni8 Ni2 73.58(3) . . ? C12 Ni8 Ni90 48.2(4) . . ? C4 Ni8 Ni90 120.9(4) . . ? C51 Ni8 Ni90 82.7(4) . . ? C53 Ni8 Ni90 135.5(4) . . ? Ni3 Ni8 Ni90 104.3(4) . . ? Ni2 Ni8 Ni90 170.9(4) . . ? C12 Ni8 Ni14 91.54(18) . . ? C4 Ni8 Ni14 144.64(16) . . ? C51 Ni8 Ni14 94.49(14) . . ? C53 Ni8 Ni14 46.93(15) . . ? Ni3 Ni8 Ni14 141.37(4) . . ? Ni2 Ni8 Ni14 96.36(3) . . ? Ni90 Ni8 Ni14 90.6(4) . . ? C12 Ni8 Ni15 93.98(19) . . ? C4 Ni8 Ni15 146.11(16) . . ? C51 Ni8 Ni15 46.27(15) . . ? C53 Ni8 Ni15 92.82(15) . . ? Ni3 Ni8 Ni15 96.59(3) . . ? Ni2 Ni8 Ni15 138.00(4) . . ? Ni90 Ni8 Ni15 50.6(4) . . ? Ni14 Ni8 Ni15 65.74(3) . . ? C12 Ni8 Ni7 87.03(19) . . ? C4 Ni8 Ni7 88.79(16) . . ? C51 Ni8 Ni7 136.04(15) . . ? C53 Ni8 Ni7 48.49(15) . . ? Ni3 Ni8 Ni7 127.98(4) . . ? Ni2 Ni8 Ni7 54.55(3) . . ? Ni90 Ni8 Ni7 126.2(4) . . ? Ni14 Ni8 Ni7 57.72(3) . . ? Ni15 Ni8 Ni7 123.46(3) . . ? C12 Ni8 Ni9 87.64(19) . . ? C4 Ni8 Ni9 91.05(16) . . ? C51 Ni8 Ni9 49.13(15) . . ? C53 Ni8 Ni9 136.64(15) . . ? Ni3 Ni8 Ni9 55.15(3) . . ? Ni2 Ni8 Ni9 128.72(4) . . ? Ni90 Ni8 Ni9 49.8(4) . . ? Ni14 Ni8 Ni9 123.40(3) . . ? Ni15 Ni8 Ni9 57.89(3) . . ? Ni7 Ni8 Ni9 174.59(4) . . ? C13 Ni9 C5 102.8(3) . . ? C13 Ni9 C14 100.4(3) . . ? C5 Ni9 C14 94.2(2) . . ? C13 Ni9 C51 144.8(3) . . ? C5 Ni9 C51 104.1(2) . . ? C14 Ni9 C51 99.8(2) . . ? C13 Ni9 Ni90 54.1(5) . . ? C5 Ni9 Ni90 123.7(5) . . ? C14 Ni9 Ni90 136.3(5) . . ? C51 Ni9 Ni90 91.9(5) . . ? C13 Ni9 Ni10 143.9(2) . . ? C5 Ni9 Ni10 94.73(17) . . ? C14 Ni9 Ni10 46.40(17) . . ? C51 Ni9 Ni10 54.63(15) . . ? Ni90 Ni9 Ni10 135.7(4) . . ? C13 Ni9 Ni3 144.4(2) . . ? C5 Ni9 Ni3 48.93(17) . . ? C14 Ni9 Ni3 102.65(18) . . ? C51 Ni9 Ni3 55.20(15) . . ? Ni90 Ni9 Ni3 118.3(4) . . ? Ni10 Ni9 Ni3 68.93(3) . . ? C13 Ni9 Ni15 99.4(2) . . ? C5 Ni9 Ni15 145.86(17) . . ? C14 Ni9 Ni15 106.97(16) . . ? C51 Ni9 Ni15 46.91(15) . . ? Ni90 Ni9 Ni15 54.1(4) . . ? Ni10 Ni9 Ni15 81.87(3) . . ? Ni3 Ni9 Ni15 99.39(4) . . ? C13 Ni9 Ni8 108.8(2) . . ? C5 Ni9 Ni8 89.13(17) . . ? C14 Ni9 Ni8 149.08(17) . . ? C51 Ni9 Ni8 49.82(15) . . ? Ni90 Ni9 Ni8 61.2(4) . . ? Ni10 Ni9 Ni8 102.71(4) . . ? Ni3 Ni9 Ni8 57.81(3) . . ? Ni15 Ni9 Ni8 59.06(3) . . ? C14 Ni10 C15 104.5(3) . . ? C14 Ni10 C52 147.7(2) . . ? C15 Ni10 C52 107.1(3) . . ? C14 Ni10 C51 111.7(3) . . ? C15 Ni10 C51 142.4(2) . . ? C52 Ni10 C51 39.5(2) . . ? C14 Ni10 Ni11 158.31(19) . . ? C15 Ni10 Ni11 53.93(19) . . ? C52 Ni10 Ni11 53.90(16) . . ? C51 Ni10 Ni11 89.16(16) . . ? C14 Ni10 Ni9 57.70(19) . . ? C15 Ni10 Ni9 162.0(2) . . ? C52 Ni10 Ni9 90.33(16) . . ? C51 Ni10 Ni9 55.49(15) . . ? Ni11 Ni10 Ni9 143.93(4) . . ? C14 Ni10 Ni16 130.3(2) . . ? C15 Ni10 Ni16 98.53(19) . . ? C52 Ni10 Ni16 50.24(15) . . ? C51 Ni10 Ni16 49.53(15) . . ? Ni11 Ni10 Ni16 59.22(3) . . ? Ni9 Ni10 Ni16 96.04(3) . . ? C14 Ni10 Ni3 101.03(18) . . ? C15 Ni10 Ni3 132.11(19) . . ? C52 Ni10 Ni3 51.75(15) . . ? C51 Ni10 Ni3 50.17(15) . . ? Ni11 Ni10 Ni3 97.00(4) . . ? Ni9 Ni10 Ni3 56.43(3) . . ? Ni16 Ni10 Ni3 94.74(3) . . ? C16 Ni11 C15 97.0(3) . . ? C16 Ni11 C52 151.4(3) . . ? C15 Ni11 C52 102.3(2) . . ? C16 Ni11 Ni10 143.4(2) . . ? C15 Ni11 Ni10 47.87(17) . . ? C52 Ni11 Ni10 55.14(16) . . ? C16 Ni11 C23 102.2(2) . . ? C15 Ni11 C23 106.2(2) . . ? C52 Ni11 C23 92.4(2) . . ? Ni10 Ni11 C23 98.48(15) . . ? C16 Ni11 Ni16 142.42(19) . . ? C15 Ni11 Ni16 100.13(18) . . ? C52 Ni11 Ni16 53.62(15) . . ? Ni10 Ni11 Ni16 66.71(3) . . ? C23 Ni11 Ni16 40.77(15) . . ? C16 Ni11 Ni12 108.8(2) . . ? C15 Ni11 Ni12 152.52(18) . . ? C52 Ni11 Ni12 50.21(16) . . ? Ni10 Ni11 Ni12 104.85(4) . . ? C23 Ni11 Ni12 77.84(16) . . ? Ni16 Ni11 Ni12 64.70(3) . . ? C16 Ni11 Ni4 105.6(2) . . ? C15 Ni11 Ni4 104.82(17) . . ? C52 Ni11 Ni4 49.14(16) . . ? Ni10 Ni11 Ni4 79.22(3) . . ? C23 Ni11 Ni4 134.85(16) . . ? Ni16 Ni11 Ni4 101.90(4) . . ? Ni12 Ni11 Ni4 59.90(3) . . ? C17 Ni12 C54 136.7(2) . . ? C17 Ni12 C52 133.9(2) . . ? C54 Ni12 C52 89.4(2) . . ? C17 Ni12 Ni5 85.16(19) . . ? C54 Ni12 Ni5 51.76(16) . . ? C52 Ni12 Ni5 140.95(16) . . ? C17 Ni12 Ni11 82.67(19) . . ? C54 Ni12 Ni11 140.65(16) . . ? C52 Ni12 Ni11 51.31(16) . . ? Ni5 Ni12 Ni11 166.96(4) . . ? C17 Ni12 Ni4 108.96(18) . . ? C54 Ni12 Ni4 97.11(15) . . ? C52 Ni12 Ni4 49.57(16) . . ? Ni5 Ni12 Ni4 128.74(4) . . ? Ni11 Ni12 Ni4 60.48(3) . . ? C17 Ni12 Ni1 109.30(19) . . ? C54 Ni12 Ni1 49.62(16) . . ? C52 Ni12 Ni1 98.89(15) . . ? Ni5 Ni12 Ni1 60.78(3) . . ? Ni11 Ni12 Ni1 128.18(4) . . ? Ni4 Ni12 Ni1 68.10(3) . . ? C17 Ni12 Ni16 110.91(19) . . ? C54 Ni12 Ni16 98.97(17) . . ? C52 Ni12 Ni16 50.15(15) . . ? Ni5 Ni12 Ni16 124.06(4) . . ? Ni11 Ni12 Ni16 57.14(3) . . ? Ni4 Ni12 Ni16 97.22(3) . . ? Ni1 Ni12 Ni16 139.76(4) . . ? C17 Ni12 Ni13 114.62(18) . . ? C54 Ni12 Ni13 49.64(15) . . ? C52 Ni12 Ni13 96.69(16) . . ? Ni5 Ni12 Ni13 57.46(3) . . ? Ni11 Ni12 Ni13 124.35(4) . . ? Ni4 Ni12 Ni13 136.42(4) . . ? Ni1 Ni12 Ni13 96.90(3) . . ? Ni16 Ni12 Ni13 67.44(3) . . ? C18' Ni13 C18 28.0(9) . . ? C18' Ni13 C19 95.3(10) . . ? C18 Ni13 C19 100.5(3) . . ? C18' Ni13 C53 159.1(9) . . ? C18 Ni13 C53 151.6(3) . . ? C19 Ni13 C53 102.5(2) . . ? C18' Ni13 C54 121.6(9) . . ? C18 Ni13 C54 116.0(3) . . ? C19 Ni13 C54 142.1(2) . . ? C53 Ni13 C54 39.7(2) . . ? C18' Ni13 Ni14 144.2(10) . . ? C18 Ni13 Ni14 149.2(2) . . ? C19 Ni13 Ni14 51.22(18) . . ? C53 Ni13 Ni14 51.36(16) . . ? C54 Ni13 Ni14 90.94(15) . . ? C18' Ni13 Ni5 83.9(10) . . ? C18 Ni13 Ni5 67.0(3) . . ? C19 Ni13 Ni5 153.21(18) . . ? C53 Ni13 Ni5 85.05(16) . . ? C54 Ni13 Ni5 50.96(16) . . ? Ni14 Ni13 Ni5 131.47(4) . . ? C18' Ni13 Ni12 80.2(9) . . ? C18 Ni13 Ni12 89.7(2) . . ? C19 Ni13 Ni12 149.11(18) . . ? C53 Ni13 Ni12 78.90(15) . . ? C54 Ni13 Ni12 46.30(15) . . ? Ni14 Ni13 Ni12 120.74(4) . . ? Ni5 Ni13 Ni12 57.26(3) . . ? C18' Ni13 Ni6 132.7(10) . . ? C18 Ni13 Ni6 106.9(3) . . ? C19 Ni13 Ni6 113.69(18) . . ? C53 Ni13 Ni6 48.03(16) . . ? C54 Ni13 Ni6 47.90(15) . . ? Ni14 Ni13 Ni6 79.41(3) . . ? Ni5 Ni13 Ni6 53.31(3) . . ? Ni12 Ni13 Ni6 90.46(3) . . ? C20 Ni14 C19 100.1(3) . . ? C20 Ni14 C53 152.0(3) . . ? C19 Ni14 C53 106.6(2) . . ? C20 Ni14 Ni13 150.48(19) . . ? C19 Ni14 Ni13 50.72(18) . . ? C53 Ni14 Ni13 55.99(16) . . ? C20 Ni14 Ni7 101.4(2) . . ? C19 Ni14 Ni7 138.63(19) . . ? C53 Ni14 Ni7 52.27(16) . . ? Ni13 Ni14 Ni7 100.21(4) . . ? C20 Ni14 Ni8 109.33(19) . . ? C19 Ni14 Ni8 138.16(17) . . ? C53 Ni14 Ni8 53.76(16) . . ? Ni13 Ni14 Ni8 98.23(4) . . ? Ni7 Ni14 Ni8 63.52(3) . . ? C20 Ni14 Ni15 96.8(2) . . ? C19 Ni14 Ni15 90.55(18) . . ? C53 Ni14 Ni15 91.20(17) . . ? Ni13 Ni14 Ni15 88.93(3) . . ? Ni7 Ni14 Ni15 121.17(3) . . ? Ni8 Ni14 Ni15 57.65(3) . . ? C21 Ni15 C22 100.9(3) . . ? C21 Ni15 C51 150.1(3) . . ? C22 Ni15 C51 107.5(2) . . ? C21 Ni15 Ni90 53.4(5) . . ? C22 Ni15 Ni90 153.2(5) . . ? C51 Ni15 Ni90 97.0(5) . . ? C21 Ni15 Ni16 151.0(2) . . ? C22 Ni15 Ni16 50.70(18) . . ? C51 Ni15 Ni16 56.88(16) . . ? Ni90 Ni15 Ni16 152.9(4) . . ? C21 Ni15 Ni9 99.8(2) . . ? C22 Ni15 Ni9 135.88(18) . . ? C51 Ni15 Ni9 52.61(16) . . ? Ni90 Ni15 Ni9 54.6(4) . . ? Ni16 Ni15 Ni9 99.34(4) . . ? C21 Ni15 Ni8 107.9(2) . . ? C22 Ni15 Ni8 141.77(19) . . ? C51 Ni15 Ni8 52.58(16) . . ? Ni90 Ni15 Ni8 63.2(4) . . ? Ni16 Ni15 Ni8 100.12(4) . . ? Ni9 Ni15 Ni8 63.05(3) . . ? C21 Ni15 Ni14 93.7(2) . . ? C22 Ni15 Ni14 97.57(18) . . ? C51 Ni15 Ni14 91.73(17) . . ? Ni90 Ni15 Ni14 92.3(4) . . ? Ni16 Ni15 Ni14 95.55(4) . . ? Ni9 Ni15 Ni14 119.44(3) . . ? Ni8 Ni15 Ni14 56.60(3) . . ? C23 Ni16 C22 103.1(3) . . ? C23 Ni16 C51 152.5(3) . . ? C22 Ni16 C51 102.2(2) . . ? C23 Ni16 C52 115.4(3) . . ? C22 Ni16 C52 141.1(2) . . ? C51 Ni16 C52 39.0(2) . . ? C23 Ni16 Ni15 153.5(2) . . ? C22 Ni16 Ni15 51.46(18) . . ? C51 Ni16 Ni15 50.78(16) . . ? C52 Ni16 Ni15 89.66(16) . . ? C23 Ni16 Ni11 67.3(2) . . ? C22 Ni16 Ni11 155.58(18) . . ? C51 Ni16 Ni11 85.12(15) . . ? C52 Ni16 Ni11 51.16(15) . . ? Ni15 Ni16 Ni11 131.96(4) . . ? C23 Ni16 Ni10 109.3(2) . . ? C22 Ni16 Ni10 113.87(18) . . ? C51 Ni16 Ni10 49.25(15) . . ? C52 Ni16 Ni10 49.04(15) . . ? Ni15 Ni16 Ni10 80.03(3) . . ? Ni11 Ni16 Ni10 54.07(3) . . ? C23 Ni16 Ni12 87.0(2) . . ? C22 Ni16 Ni12 145.91(18) . . ? C51 Ni16 Ni12 78.22(16) . . ? C52 Ni16 Ni12 46.99(15) . . ? Ni15 Ni16 Ni12 118.03(4) . . ? Ni11 Ni16 Ni12 58.16(3) . . ? Ni10 Ni16 Ni12 92.45(3) . . ? C21 Ni90 C13 118.8(9) . . ? C21 Ni90 C12 123.2(9) . . ? C13 Ni90 C12 117.8(9) . . ? C21 Ni90 Ni15 49.7(4) . . ? C13 Ni90 Ni15 110.8(8) . . ? C12 Ni90 Ni15 104.3(8) . . ? C21 Ni90 Ni9 111.2(8) . . ? C13 Ni90 Ni9 50.0(4) . . ? C12 Ni90 Ni9 100.5(7) . . ? Ni15 Ni90 Ni9 71.3(5) . . ? C21 Ni90 O12 121.4(8) . . ? C13 Ni90 O12 113.3(8) . . ? C12 Ni90 O12 30.4(3) . . ? Ni15 Ni90 O12 128.8(8) . . ? Ni9 Ni90 O12 122.3(7) . . ? C21 Ni90 O21 28.5(3) . . ? C13 Ni90 O21 113.8(8) . . ? C12 Ni90 O21 122.8(8) . . ? Ni15 Ni90 O21 78.2(5) . . ? Ni9 Ni90 O21 132.1(7) . . ? O12 Ni90 O21 105.7(7) . . ? C21 Ni90 O13 114.3(8) . . ? C13 Ni90 O13 27.4(3) . . ? C12 Ni90 O13 118.0(8) . . ? Ni15 Ni90 O13 130.9(7) . . ? Ni9 Ni90 O13 77.3(5) . . ? O12 Ni90 O13 99.8(6) . . ? O21 Ni90 O13 97.2(6) . . ? C21 Ni90 Ni8 107.4(8) . . ? C13 Ni90 Ni8 112.2(8) . . ? C12 Ni90 Ni8 43.7(4) . . ? Ni15 Ni90 Ni8 66.2(4) . . ? Ni9 Ni90 Ni8 69.0(5) . . ? O12 Ni90 Ni8 74.0(5) . . ? O21 Ni90 Ni8 129.2(7) . . ? O13 Ni90 Ni8 133.5(7) . . ? C52 C51 Ni15 143.3(4) . . ? C52 C51 Ni10 70.1(3) . . ? Ni15 C51 Ni10 109.8(3) . . ? C52 C51 Ni16 71.4(3) . . ? Ni15 C51 Ni16 72.34(18) . . ? Ni10 C51 Ni16 81.2(2) . . ? C52 C51 Ni9 129.0(4) . . ? Ni15 C51 Ni9 80.5(2) . . ? Ni10 C51 Ni9 69.88(17) . . ? Ni16 C51 Ni9 130.3(3) . . ? C52 C51 Ni8 120.3(4) . . ? Ni15 C51 Ni8 81.1(2) . . ? Ni10 C51 Ni8 146.1(3) . . ? Ni16 C51 Ni8 132.2(3) . . ? Ni9 C51 Ni8 81.05(19) . . ? C52 C51 Ni3 73.2(3) . . ? Ni15 C51 Ni3 143.4(3) . . ? Ni10 C51 Ni3 81.23(19) . . ? Ni16 C51 Ni3 144.1(3) . . ? Ni9 C51 Ni3 70.66(17) . . ? Ni8 C51 Ni3 72.79(17) . . ? C51 C52 Ni4 138.1(4) . . ? C51 C52 Ni12 127.9(4) . . ? Ni4 C52 Ni12 80.0(2) . . ? C51 C52 Ni11 130.8(4) . . ? Ni4 C52 Ni11 79.8(2) . . ? Ni12 C52 Ni11 78.5(2) . . ? C51 C52 Ni10 70.4(3) . . ? Ni4 C52 Ni10 102.9(2) . . ? Ni12 C52 Ni10 148.1(3) . . ? Ni11 C52 Ni10 70.96(18) . . ? C51 C52 Ni16 69.5(3) . . ? Ni4 C52 Ni16 152.1(3) . . ? Ni12 C52 Ni16 82.9(2) . . ? Ni11 C52 Ni16 75.21(18) . . ? Ni10 C52 Ni16 80.7(2) . . ? C51 C52 Ni3 68.9(3) . . ? Ni4 C52 Ni3 69.19(17) . . ? Ni12 C52 Ni3 128.9(3) . . ? Ni11 C52 Ni3 131.1(3) . . ? Ni10 C52 Ni3 80.00(19) . . ? Ni16 C52 Ni3 138.0(3) . . ? C54 C53 Ni14 144.1(4) . . ? C54 C53 Ni13 71.7(3) . . ? Ni14 C53 Ni13 72.65(18) . . ? C54 C53 Ni7 129.9(4) . . ? Ni14 C53 Ni7 80.0(2) . . ? Ni13 C53 Ni7 133.9(3) . . ? C54 C53 Ni6 70.1(3) . . ? Ni14 C53 Ni6 110.7(3) . . ? Ni13 C53 Ni6 84.6(2) . . ? Ni7 C53 Ni6 71.24(18) . . ? C54 C53 Ni2 73.3(3) . . ? Ni14 C53 Ni2 142.4(3) . . ? Ni13 C53 Ni2 145.0(3) . . ? Ni7 C53 Ni2 70.68(17) . . ? Ni6 C53 Ni2 81.9(2) . . ? C54 C53 Ni8 120.2(4) . . ? Ni14 C53 Ni8 79.3(2) . . ? Ni13 C53 Ni8 127.6(3) . . ? Ni7 C53 Ni8 80.8(2) . . ? Ni6 C53 Ni8 147.5(3) . . ? Ni2 C53 Ni8 73.33(17) . . ? C53 C54 Ni12 130.0(4) . . ? C53 C54 Ni1 136.8(4) . . ? Ni12 C54 Ni1 80.9(2) . . ? C53 C54 Ni5 129.6(4) . . ? Ni12 C54 Ni5 78.1(2) . . ? Ni1 C54 Ni5 80.0(2) . . ? C53 C54 Ni6 70.2(3) . . ? Ni12 C54 Ni6 149.0(3) . . ? Ni1 C54 Ni6 98.5(2) . . ? Ni5 C54 Ni6 71.34(18) . . ? C53 C54 Ni13 68.6(3) . . ? Ni12 C54 Ni13 84.1(2) . . ? Ni1 C54 Ni13 153.7(3) . . ? Ni5 C54 Ni13 75.87(18) . . ? Ni6 C54 Ni13 83.60(19) . . ? C53 C54 Ni2 68.4(3) . . ? Ni12 C54 Ni2 126.6(3) . . ? Ni1 C54 Ni2 68.63(16) . . ? Ni5 C54 Ni2 133.7(3) . . ? Ni6 C54 Ni2 80.38(19) . . ? Ni13 C54 Ni2 137.0(3) . . ? O1 C1 Ni1 176.7(5) . . ? O2 C2 Ni1 140.9(5) . . ? O2 C2 Ni2 141.6(5) . . ? Ni1 C2 Ni2 77.4(2) . . ? O3 C3 Ni2 142.8(5) . . ? O3 C3 Ni7 138.6(5) . . ? Ni2 C3 Ni7 78.4(2) . . ? O4 C4 Ni3 126.6(4) . . ? O4 C4 Ni2 125.1(4) . . ? Ni3 C4 Ni2 98.1(2) . . ? O4 C4 Ni8 135.3(5) . . ? Ni3 C4 Ni8 77.60(19) . . ? Ni2 C4 Ni8 78.16(19) . . ? O5 C5 Ni3 145.6(5) . . ? O5 C5 Ni9 135.4(5) . . ? Ni3 C5 Ni9 79.0(2) . . ? O6 C6 Ni3 142.8(5) . . ? O6 C6 Ni4 138.5(5) . . ? Ni3 C6 Ni4 78.6(2) . . ? O7 C7 Ni4 176.5(5) . . ? O8 C8 Ni7 176.7(6) . . ? O9 C9 Ni6 163.1(5) . . ? O9 C9 Ni7 123.6(5) . . ? Ni6 C9 Ni7 72.8(2) . . ? O10 C10 Ni6 144.8(5) . . ? O10 C10 Ni5 136.3(5) . . ? Ni6 C10 Ni5 78.8(2) . . ? O11 C11 Ni5 179.1(6) . . ? O12 C12 Ni8 176.8(5) . . ? O12 C12 Ni90 91.2(7) . . ? Ni8 C12 Ni90 88.1(6) . . ? O13 C13 Ni9 177.8(6) . . ? O13 C13 Ni90 103.4(7) . . ? Ni9 C13 Ni90 75.9(6) . . ? O14 C14 Ni10 156.0(5) . . ? O14 C14 Ni9 128.1(5) . . ? Ni10 C14 Ni9 75.9(2) . . ? O15 C15 Ni10 149.5(5) . . ? O15 C15 Ni11 132.1(5) . . ? Ni10 C15 Ni11 78.2(2) . . ? O16 C16 Ni11 174.7(5) . . ? O17 C17 Ni12 176.1(5) . . ? O18 C18 Ni13 168.3(7) . . ? O18 C18 Ni5 119.1(6) . . ? Ni13 C18 Ni5 71.8(3) . . ? O18' C18' Ni13 146(2) . . ? O19 C19 Ni13 142.0(5) . . ? O19 C19 Ni14 139.8(5) . . ? Ni13 C19 Ni14 78.1(2) . . ? O20 C20 Ni14 178.6(6) . . ? O21 C21 Ni15 178.5(6) . . ? O21 C21 Ni90 102.0(7) . . ? Ni15 C21 Ni90 76.9(6) . . ? O22 C22 Ni16 142.6(5) . . ? O22 C22 Ni15 139.6(5) . . ? Ni16 C22 Ni15 77.8(2) . . ? O23 C23 Ni16 167.7(6) . . ? O23 C23 Ni11 120.1(5) . . ? Ni16 C23 Ni11 71.88(19) . . ? C12 O12 Ni90 58.4(6) . . ? C13 O13 Ni90 49.2(5) . . ? C21 O21 Ni90 49.5(5) . . ? C25 Ni17 C24 107.3(3) . . ? C25 Ni17 C27 99.6(3) . . ? C24 Ni17 C27 89.5(3) . . ? C25 Ni17 C62 139.2(3) . . ? C24 Ni17 C62 103.5(2) . . ? C27 Ni17 C62 106.8(2) . . ? C25 Ni17 C61 101.6(2) . . ? C24 Ni17 C61 131.2(2) . . ? C27 Ni17 C61 123.5(2) . . ? C62 Ni17 C61 37.7(2) . . ? C25 Ni17 Ni18 51.0(2) . . ? C24 Ni17 Ni18 139.08(19) . . ? C27 Ni17 Ni18 124.82(19) . . ? C62 Ni17 Ni18 88.26(15) . . ? C61 Ni17 Ni18 50.63(14) . . ? C25 Ni17 Ni21 149.78(19) . . ? C24 Ni17 Ni21 52.17(19) . . ? C27 Ni17 Ni21 101.82(18) . . ? C62 Ni17 Ni21 51.37(16) . . ? C61 Ni17 Ni21 83.99(15) . . ? Ni18 Ni17 Ni21 126.71(4) . . ? C25 Ni17 Ni28 143.15(19) . . ? C24 Ni17 Ni28 95.12(19) . . ? C27 Ni17 Ni28 50.75(18) . . ? C62 Ni17 Ni28 56.46(15) . . ? C61 Ni17 Ni28 83.66(14) . . ? Ni18 Ni17 Ni28 123.06(4) . . ? Ni21 Ni17 Ni28 66.59(3) . . ? C25 Ni17 Ni22 106.81(19) . . ? C24 Ni17 Ni22 85.6(2) . . ? C27 Ni17 Ni22 153.43(18) . . ? C62 Ni17 Ni22 49.66(15) . . ? C61 Ni17 Ni22 48.29(15) . . ? Ni18 Ni17 Ni22 72.47(3) . . ? Ni21 Ni17 Ni22 55.27(3) . . ? Ni28 Ni17 Ni22 103.68(4) . . ? C26 Ni18 C25 106.9(3) . . ? C26 Ni18 C61 142.3(3) . . ? C25 Ni18 C61 110.6(2) . . ? C26 Ni18 Ni17 157.7(2) . . ? C25 Ni18 Ni17 51.19(18) . . ? C61 Ni18 Ni17 59.45(17) . . ? C26 Ni18 Ni24 102.7(3) . . ? C25 Ni18 Ni24 137.57(18) . . ? C61 Ni18 Ni24 49.57(17) . . ? Ni17 Ni18 Ni24 98.09(4) . . ? C26 Ni18 Ni23 92.9(2) . . ? C25 Ni18 Ni23 145.20(19) . . ? C61 Ni18 Ni23 52.71(17) . . ? Ni17 Ni18 Ni23 104.47(4) . . ? Ni24 Ni18 Ni23 59.88(3) . . ? C26 Ni18 Ni19 94.4(2) . . ? C25 Ni18 Ni19 92.94(19) . . ? C61 Ni18 Ni19 87.91(17) . . ? Ni17 Ni18 Ni19 91.13(3) . . ? Ni24 Ni18 Ni19 54.75(3) . . ? Ni23 Ni18 Ni19 114.22(4) . . ? C30' Ni19 C30 18.0(6) . . ? C30' Ni19 C29 96.0(5) . . ? C30 Ni19 C29 108.1(5) . . ? C30' Ni19 C64 154.2(5) . . ? C30 Ni19 C64 139.7(5) . . ? C29 Ni19 C64 109.8(3) . . ? C30' Ni19 Ni20 147.1(5) . . ? C30 Ni19 Ni20 157.0(5) . . ? C29 Ni19 Ni20 51.1(2) . . ? C64 Ni19 Ni20 58.67(17) . . ? C30' Ni19 Ni24 107.7(5) . . ? C30 Ni19 Ni24 103.0(5) . . ? C29 Ni19 Ni24 141.6(2) . . ? C64 Ni19 Ni24 50.92(17) . . ? Ni20 Ni19 Ni24 100.02(4) . . ? C30' Ni19 Ni25 110.1(5) . . ? C30 Ni19 Ni25 92.6(4) . . ? C29 Ni19 Ni25 139.3(2) . . ? C64 Ni19 Ni25 48.84(17) . . ? Ni20 Ni19 Ni25 99.13(4) . . ? Ni24 Ni19 Ni25 58.66(3) . . ? C30' Ni19 Ni18 87.6(5) . . ? C30 Ni19 Ni18 99.3(4) . . ? C29 Ni19 Ni18 96.0(2) . . ? C64 Ni19 Ni18 89.81(17) . . ? Ni20 Ni19 Ni18 93.50(4) . . ? Ni24 Ni19 Ni18 56.56(3) . . ? Ni25 Ni19 Ni18 115.18(4) . . ? C29 Ni20 C28 100.8(3) . . ? C29 Ni20 C27 100.8(3) . . ? C28 Ni20 C27 90.9(3) . . ? C29 Ni20 C63 142.0(3) . . ? C28 Ni20 C63 108.6(3) . . ? C27 Ni20 C63 102.2(2) . . ? C29 Ni20 C64 103.5(3) . . ? C28 Ni20 C64 134.1(3) . . ? C27 Ni20 C64 121.4(2) . . ? C63 Ni20 C64 38.4(2) . . ? C29 Ni20 Ni19 51.2(2) . . ? C28 Ni20 Ni19 136.6(2) . . ? C27 Ni20 Ni19 123.20(18) . . ? C63 Ni20 Ni19 90.79(16) . . ? C64 Ni20 Ni19 52.37(15) . . ? C29 Ni20 Ni27 146.2(2) . . ? C28 Ni20 Ni27 51.3(2) . . ? C27 Ni20 Ni27 98.56(18) . . ? C63 Ni20 Ni27 57.37(15) . . ? C64 Ni20 Ni27 89.41(15) . . ? Ni19 Ni20 Ni27 133.05(5) . . ? C29 Ni20 Ni28 144.4(2) . . ? C28 Ni20 Ni28 100.5(2) . . ? C27 Ni20 Ni28 50.65(18) . . ? C63 Ni20 Ni28 51.94(16) . . ? C64 Ni20 Ni28 81.08(15) . . ? Ni19 Ni20 Ni28 121.43(4) . . ? Ni27 Ni20 Ni28 67.78(3) . . ? C29 Ni20 Ni26 113.6(2) . . ? C28 Ni20 Ni26 86.5(2) . . ? C27 Ni20 Ni26 145.31(18) . . ? C63 Ni20 Ni26 47.02(16) . . ? C64 Ni20 Ni26 48.11(15) . . ? Ni19 Ni20 Ni26 79.13(4) . . ? Ni27 Ni20 Ni26 53.96(3) . . ? Ni28 Ni20 Ni26 95.86(3) . . ? C31 Ni21 C24 104.3(3) . . ? C31 Ni21 C62 145.4(3) . . ? C24 Ni21 C62 104.9(2) . . ? C31 Ni21 C32 98.1(3) . . ? C24 Ni21 C32 90.5(3) . . ? C62 Ni21 C32 99.9(2) . . ? C31 Ni21 Ni22 139.8(2) . . ? C24 Ni21 Ni22 92.85(18) . . ? C62 Ni21 Ni22 55.99(16) . . ? C32 Ni21 Ni22 44.90(17) . . ? C31 Ni21 Ni17 148.0(2) . . ? C24 Ni21 Ni17 49.24(18) . . ? C62 Ni21 Ni17 55.66(17) . . ? C32 Ni21 Ni17 99.60(17) . . ? Ni22 Ni21 Ni17 67.97(3) . . ? C31 Ni21 Ni29 98.4(2) . . ? C24 Ni21 Ni29 144.44(19) . . ? C62 Ni21 Ni29 47.22(16) . . ? C32 Ni21 Ni29 113.18(18) . . ? Ni22 Ni21 Ni29 86.93(4) . . ? Ni17 Ni21 Ni29 98.90(4) . . ? C31 Ni21 Ni28 110.2(2) . . ? C24 Ni21 Ni28 87.22(18) . . ? C62 Ni21 Ni28 53.46(16) . . ? C32 Ni21 Ni28 151.28(17) . . ? Ni22 Ni21 Ni28 106.60(4) . . ? Ni17 Ni21 Ni28 58.19(3) . . ? Ni29 Ni21 Ni28 59.09(3) . . ? C32 Ni22 C33 104.7(3) . . ? C32 Ni22 C61 148.0(3) . . ? C33 Ni22 C61 107.1(2) . . ? C32 Ni22 C62 111.5(3) . . ? C33 Ni22 C62 142.0(3) . . ? C61 Ni22 C62 38.9(2) . . ? C32 Ni22 Ni23 156.2(2) . . ? C33 Ni22 Ni23 53.2(2) . . ? C61 Ni22 Ni23 55.41(16) . . ? C62 Ni22 Ni23 89.09(16) . . ? C32 Ni22 Ni21 60.6(2) . . ? C33 Ni22 Ni21 165.3(2) . . ? C61 Ni22 Ni21 87.60(16) . . ? C62 Ni22 Ni21 52.18(16) . . ? Ni23 Ni22 Ni21 141.26(4) . . ? C32 Ni22 Ni30 127.7(2) . . ? C33 Ni22 Ni30 98.2(2) . . ? C61 Ni22 Ni30 50.72(16) . . ? C62 Ni22 Ni30 50.00(16) . . ? Ni23 Ni22 Ni30 57.19(3) . . ? Ni21 Ni22 Ni30 91.86(3) . . ? C32 Ni22 Ni17 102.2(2) . . ? C33 Ni22 Ni17 132.1(2) . . ? C61 Ni22 Ni17 52.07(17) . . ? C62 Ni22 Ni17 50.15(16) . . ? Ni23 Ni22 Ni17 100.07(4) . . ? Ni21 Ni22 Ni17 56.76(3) . . ? Ni30 Ni22 Ni17 95.59(3) . . ? C34 Ni23 C33 97.1(3) . . ? C34 Ni23 C61 152.5(3) . . ? C33 Ni23 C61 100.7(2) . . ? C34 Ni23 C40 97.6(3) . . ? C33 Ni23 C40 103.0(2) . . ? C61 Ni23 C40 98.5(2) . . ? C34 Ni23 Ni22 144.5(2) . . ? C33 Ni23 Ni22 48.07(18) . . ? C61 Ni23 Ni22 54.03(16) . . ? C40 Ni23 Ni22 97.45(17) . . ? C34 Ni23 Ni30 140.1(2) . . ? C33 Ni23 Ni30 102.64(18) . . ? C61 Ni23 Ni30 54.68(16) . . ? C40 Ni23 Ni30 44.31(15) . . ? Ni22 Ni23 Ni30 67.28(3) . . ? C34 Ni23 Ni24 109.5(2) . . ? C33 Ni23 Ni24 149.24(19) . . ? C61 Ni23 Ni24 48.96(16) . . ? C40 Ni23 Ni24 88.84(16) . . ? Ni22 Ni23 Ni24 102.79(4) . . ? Ni30 Ni23 Ni24 66.42(3) . . ? C34 Ni23 Ni18 109.3(2) . . ? C33 Ni23 Ni18 97.19(19) . . ? C61 Ni23 Ni18 47.89(16) . . ? C40 Ni23 Ni18 143.84(16) . . ? Ni22 Ni23 Ni18 74.41(3) . . ? Ni30 Ni23 Ni18 102.23(4) . . ? Ni24 Ni23 Ni18 60.04(3) . . ? C35 Ni24 C61 135.0(3) . . ? C35 Ni24 C64 134.2(3) . . ? C61 Ni24 C64 89.5(2) . . ? C35 Ni24 Ni25 85.0(2) . . ? C61 Ni24 Ni25 139.85(16) . . ? C64 Ni24 Ni25 50.66(17) . . ? C35 Ni24 Ni19 102.8(2) . . ? C61 Ni24 Ni19 97.90(17) . . ? C64 Ni24 Ni19 50.73(16) . . ? Ni25 Ni24 Ni19 62.56(3) . . ? C35 Ni24 Ni23 83.6(2) . . ? C61 Ni24 Ni23 52.62(16) . . ? C64 Ni24 Ni23 141.97(17) . . ? Ni25 Ni24 Ni23 165.94(4) . . ? Ni19 Ni24 Ni23 128.25(4) . . ? C35 Ni24 Ni18 104.1(2) . . ? C61 Ni24 Ni18 48.41(16) . . ? C64 Ni24 Ni18 98.81(17) . . ? Ni25 Ni24 Ni18 131.21(4) . . ? Ni19 Ni24 Ni18 68.70(3) . . ? Ni23 Ni24 Ni18 60.09(3) . . ? C35 Ni24 Ni31 121.9(2) . . ? C61 Ni24 Ni31 91.53(16) . . ? C64 Ni24 Ni31 52.17(17) . . ? Ni25 Ni24 Ni31 62.16(3) . . ? Ni19 Ni24 Ni31 101.97(3) . . ? Ni23 Ni24 Ni31 118.02(4) . . ? Ni18 Ni24 Ni31 133.81(4) . . ? C35 Ni24 Ni30 115.9(2) . . ? C61 Ni24 Ni30 49.60(17) . . ? C64 Ni24 Ni30 101.07(16) . . ? Ni25 Ni24 Ni30 124.96(4) . . ? Ni19 Ni24 Ni30 140.73(4) . . ? Ni23 Ni24 Ni30 54.43(3) . . ? Ni18 Ni24 Ni30 94.33(3) . . ? Ni31 Ni24 Ni30 63.81(3) . . ? C36 Ni25 C36' 19.6(5) . . ? C36 Ni25 C37 92.7(5) . . ? C36' Ni25 C37 98.7(5) . . ? C36 Ni25 C64 156.3(5) . . ? C36' Ni25 C64 156.6(4) . . ? C37 Ni25 C64 104.6(3) . . ? C36 Ni25 Ni26 141.0(5) . . ? C36' Ni25 Ni26 145.7(4) . . ? C37 Ni25 Ni26 48.75(19) . . ? C64 Ni25 Ni26 56.55(16) . . ? C36 Ni25 Ni24 111.2(5) . . ? C36' Ni25 Ni24 105.7(4) . . ? C37 Ni25 Ni24 155.5(2) . . ? C64 Ni25 Ni24 51.01(16) . . ? Ni26 Ni25 Ni24 106.87(4) . . ? C36 Ni25 Ni19 110.2(5) . . ? C36' Ni25 Ni19 124.6(4) . . ? C37 Ni25 Ni19 108.7(2) . . ? C64 Ni25 Ni19 48.99(17) . . ? Ni26 Ni25 Ni19 82.25(4) . . ? Ni24 Ni25 Ni19 58.78(3) . . ? C36 Ni25 Ni31 139.6(5) . . ? C36' Ni25 Ni31 120.1(4) . . ? C37 Ni25 Ni31 104.16(18) . . ? C64 Ni25 Ni31 51.75(17) . . ? Ni26 Ni25 Ni31 68.57(3) . . ? Ni24 Ni25 Ni31 61.21(3) . . ? Ni19 Ni25 Ni31 98.85(4) . . ? C38 Ni26 C37 103.6(3) . . ? C38 Ni26 C63 115.1(3) . . ? C37 Ni26 C63 140.6(3) . . ? C38 Ni26 C64 150.6(3) . . ? C37 Ni26 C64 104.6(3) . . ? C63 Ni26 C64 39.3(2) . . ? C38 Ni26 Ni25 156.4(2) . . ? C37 Ni26 Ni25 52.8(2) . . ? C63 Ni26 Ni25 88.27(16) . . ? C64 Ni26 Ni25 52.58(16) . . ? C38 Ni26 Ni27 59.1(2) . . ? C37 Ni26 Ni27 160.9(2) . . ? C63 Ni26 Ni27 58.16(16) . . ? C64 Ni26 Ni27 91.72(16) . . ? Ni25 Ni26 Ni27 144.29(4) . . ? C38 Ni26 Ni20 104.1(2) . . ? C37 Ni26 Ni20 130.2(2) . . ? C63 Ni26 Ni20 47.69(16) . . ? C64 Ni26 Ni20 49.99(17) . . ? Ni25 Ni26 Ni20 94.36(4) . . ? Ni27 Ni26 Ni20 55.01(3) . . ? C38 Ni26 Ni31 132.8(2) . . ? C37 Ni26 Ni31 100.7(2) . . ? C63 Ni26 Ni31 46.68(17) . . ? C64 Ni26 Ni31 47.95(16) . . ? Ni25 Ni26 Ni31 60.72(3) . . ? Ni27 Ni26 Ni31 97.55(4) . . ? Ni20 Ni26 Ni31 89.51(3) . . ? C46' Ni27 C46 15.1(11) . . ? C46' Ni27 C28 93.7(12) . . ? C46 Ni27 C28 106.0(4) . . ? C46' Ni27 C38 91.9(14) . . ? C46 Ni27 C38 98.0(4) . . ? C28 Ni27 C38 100.9(3) . . ? C46' Ni27 C63 158.6(11) . . ? C46 Ni27 C63 143.5(3) . . ? C28 Ni27 C63 103.4(2) . . ? C38 Ni27 C63 97.4(2) . . ? C46' Ni27 Ni33 65.1(11) . . ? C46 Ni27 Ni33 51.2(3) . . ? C28 Ni27 Ni33 121.4(2) . . ? C38 Ni27 Ni33 131.6(2) . . ? C63 Ni27 Ni33 94.67(18) . . ? C46' Ni27 Ni26 137.5(14) . . ? C46 Ni27 Ni26 140.3(3) . . ? C28 Ni27 Ni26 98.2(2) . . ? C38 Ni27 Ni26 45.87(16) . . ? C63 Ni27 Ni26 53.12(15) . . ? Ni33 Ni27 Ni26 135.11(12) . . ? C46' Ni27 Ni20 141.1(13) . . ? C46 Ni27 Ni20 147.8(3) . . ? C28 Ni27 Ni20 50.1(2) . . ? C38 Ni27 Ni20 107.05(17) . . ? C63 Ni27 Ni20 53.27(15) . . ? Ni33 Ni27 Ni20 117.51(11) . . ? Ni26 Ni27 Ni20 71.03(4) . . ? C46' Ni27 Ni32 112.4(11) . . ? C46 Ni27 Ni32 97.8(3) . . ? C28 Ni27 Ni32 147.5(2) . . ? C38 Ni27 Ni32 97.35(17) . . ? C63 Ni27 Ni32 47.40(15) . . ? Ni33 Ni27 Ni32 59.47(12) . . ? Ni26 Ni27 Ni32 75.86(3) . . ? Ni20 Ni27 Ni32 98.81(4) . . ? C46' Ni27 Ni28 120.0(13) . . ? C46 Ni27 Ni28 109.7(3) . . ? C28 Ni27 Ni28 92.24(19) . . ? C38 Ni27 Ni28 144.74(17) . . ? C63 Ni27 Ni28 47.48(15) . . ? Ni33 Ni27 Ni28 61.29(11) . . ? Ni26 Ni27 Ni28 100.18(4) . . ? Ni20 Ni27 Ni28 58.15(3) . . ? Ni32 Ni27 Ni28 58.49(3) . . ? C39' Ni28 C39 15.8(10) . . ? C39' Ni28 C27 84.8(10) . . ? C39 Ni28 C27 100.6(3) . . ? C39' Ni28 C63 140.3(12) . . ? C39 Ni28 C63 133.7(3) . . ? C27 Ni28 C63 103.7(2) . . ? C39' Ni28 C62 130.7(12) . . ? C39 Ni28 C62 125.9(3) . . ? C27 Ni28 C62 103.3(2) . . ? C63 Ni28 C62 85.6(2) . . ? C39' Ni28 Ni17 112.4(11) . . ? C39 Ni28 Ni17 123.4(3) . . ? C27 Ni28 Ni17 51.43(17) . . ? C63 Ni28 Ni17 102.45(15) . . ? C62 Ni28 Ni17 52.24(15) . . ? C39' Ni28 Ni20 119.2(11) . . ? C39 Ni28 Ni20 130.3(3) . . ? C27 Ni28 Ni20 51.73(18) . . ? C63 Ni28 Ni20 52.31(16) . . ? C62 Ni28 Ni20 102.24(15) . . ? Ni17 Ni28 Ni20 74.83(3) . . ? C39' Ni28 Ni33 54.4(11) . . ? C39 Ni28 Ni33 46.6(3) . . ? C27 Ni28 Ni33 113.1(2) . . ? C63 Ni28 Ni33 87.44(18) . . ? C62 Ni28 Ni33 143.52(18) . . ? Ni17 Ni28 Ni33 163.03(11) . . ? Ni20 Ni28 Ni33 101.53(10) . . ? C39' Ni28 Ni32 105.3(11) . . ? C39 Ni28 Ni32 92.1(3) . . ? C27 Ni28 Ni32 143.69(18) . . ? C63 Ni28 Ni32 47.16(15) . . ? C62 Ni28 Ni32 96.09(15) . . ? Ni17 Ni28 Ni32 141.29(4) . . ? Ni20 Ni28 Ni32 94.50(4) . . ? Ni33 Ni28 Ni32 54.72(10) . . ? C39' Ni28 Ni29 106.7(10) . . ? C39 Ni28 Ni29 93.3(3) . . ? C27 Ni28 Ni29 147.04(18) . . ? C63 Ni28 Ni29 87.20(16) . . ? C62 Ni28 Ni29 45.78(14) . . ? Ni17 Ni28 Ni29 96.08(3) . . ? Ni20 Ni28 Ni29 133.35(4) . . ? Ni33 Ni28 Ni29 98.16(11) . . ? Ni32 Ni28 Ni29 64.15(3) . . ? C39' Ni28 Ni21 85.4(12) . . ? C39 Ni28 Ni21 85.0(3) . . ? C27 Ni28 Ni21 93.25(18) . . ? C63 Ni28 Ni21 131.57(16) . . ? C62 Ni28 Ni21 46.14(15) . . ? Ni17 Ni28 Ni21 55.22(3) . . ? Ni20 Ni28 Ni21 129.98(4) . . ? Ni33 Ni28 Ni21 126.86(10) . . ? Ni32 Ni28 Ni21 121.87(4) . . ? Ni29 Ni28 Ni21 58.14(3) . . ? C39' Ni28 Ni27 91.1(12) . . ? C39 Ni28 Ni27 91.0(3) . . ? C27 Ni28 Ni27 88.95(18) . . ? C63 Ni28 Ni27 51.11(16) . . ? C62 Ni28 Ni27 136.72(15) . . ? Ni17 Ni28 Ni27 128.71(4) . . ? Ni20 Ni28 Ni27 54.07(3) . . ? Ni33 Ni28 Ni27 48.88(10) . . ? Ni32 Ni28 Ni27 56.68(3) . . ? Ni29 Ni28 Ni27 120.78(4) . . ? Ni21 Ni28 Ni27 175.74(4) . . ? C43 Ni29 C62 149.6(3) . . ? C43 Ni29 C44 100.6(3) . . ? C62 Ni29 C44 106.6(2) . . ? C43 Ni29 Ni30 149.6(2) . . ? C62 Ni29 Ni30 57.11(17) . . ? C44 Ni29 Ni30 49.75(17) . . ? C43 Ni29 Ni21 102.2(2) . . ? C62 Ni29 Ni21 49.50(17) . . ? C44 Ni29 Ni21 128.88(18) . . ? Ni30 Ni29 Ni21 94.57(4) . . ? C43 Ni29 Ni28 104.5(2) . . ? C62 Ni29 Ni28 55.82(17) . . ? C44 Ni29 Ni28 148.73(18) . . ? Ni30 Ni29 Ni28 105.66(4) . . ? Ni21 Ni29 Ni28 62.78(3) . . ? C43 Ni29 Ni32 86.7(2) . . ? C62 Ni29 Ni32 97.99(17) . . ? C44 Ni29 Ni32 106.69(18) . . ? Ni30 Ni29 Ni32 106.80(4) . . ? Ni21 Ni29 Ni32 119.66(4) . . ? Ni28 Ni29 Ni32 57.28(3) . . ? C40 Ni30 C44 103.9(3) . . ? C40 Ni30 C62 147.7(3) . . ? C44 Ni30 C62 103.5(2) . . ? C40 Ni30 C61 114.5(3) . . ? C44 Ni30 C61 141.3(2) . . ? C62 Ni30 C61 38.5(2) . . ? C40 Ni30 Ni29 154.5(2) . . ? C44 Ni30 Ni29 52.92(19) . . ? C62 Ni30 Ni29 50.87(15) . . ? C61 Ni30 Ni29 88.44(15) . . ? C40 Ni30 Ni23 61.0(2) . . ? C44 Ni30 Ni23 160.09(19) . . ? C62 Ni30 Ni23 88.03(15) . . ? C61 Ni30 Ni23 54.14(15) . . ? Ni29 Ni30 Ni23 137.68(4) . . ? C40 Ni30 Ni22 100.4(2) . . ? C44 Ni30 Ni22 120.57(19) . . ? C62 Ni30 Ni22 50.29(15) . . ? C61 Ni30 Ni22 49.09(16) . . ? Ni29 Ni30 Ni22 86.06(3) . . ? Ni23 Ni30 Ni22 55.52(3) . . ? C40 Ni30 Ni24 93.7(2) . . ? C44 Ni30 Ni24 138.93(19) . . ? C62 Ni30 Ni24 76.27(16) . . ? C61 Ni30 Ni24 45.89(16) . . ? Ni29 Ni30 Ni24 110.92(4) . . ? Ni23 Ni30 Ni24 59.16(3) . . ? Ni22 Ni30 Ni24 91.40(3) . . ? C40 Ni30 Ni31 118.1(2) . . ? C44 Ni30 Ni31 82.75(19) . . ? C62 Ni30 Ni31 81.98(16) . . ? C61 Ni30 Ni31 83.55(15) . . ? Ni29 Ni30 Ni31 73.39(3) . . ? Ni23 Ni30 Ni31 115.28(4) . . ? Ni22 Ni30 Ni31 129.07(4) . . ? Ni24 Ni30 Ni31 56.33(3) . . ? C45 Ni31 C41 101.3(3) . . ? C45 Ni31 C63 156.7(3) . . ? C41 Ni31 C63 101.3(2) . . ? C45 Ni31 C64 118.1(3) . . ? C41 Ni31 C64 138.8(2) . . ? C63 Ni31 C64 38.7(2) . . ? C45 Ni31 Ni32 151.8(2) . . ? C41 Ni31 Ni32 50.52(19) . . ? C63 Ni31 Ni32 50.97(15) . . ? C64 Ni31 Ni32 89.41(16) . . ? C45 Ni31 Ni24 79.5(2) . . ? C41 Ni31 Ni24 163.16(19) . . ? C63 Ni31 Ni24 80.52(15) . . ? C64 Ni31 Ni24 48.09(15) . . ? Ni32 Ni31 Ni24 127.39(4) . . ? C45 Ni31 Ni25 79.2(2) . . ? C41 Ni31 Ni25 140.19(19) . . ? C63 Ni31 Ni25 79.90(16) . . ? C64 Ni31 Ni25 47.41(16) . . ? Ni32 Ni31 Ni25 120.72(4) . . ? Ni24 Ni31 Ni25 56.63(3) . . ? C45 Ni31 Ni26 122.9(2) . . ? C41 Ni31 Ni26 102.07(18) . . ? C63 Ni31 Ni26 45.74(16) . . ? C64 Ni31 Ni26 47.01(15) . . ? Ni32 Ni31 Ni26 70.39(3) . . ? Ni24 Ni31 Ni26 91.20(3) . . ? Ni25 Ni31 Ni26 50.71(3) . . ? C45 Ni31 Ni30 80.7(2) . . ? C41 Ni31 Ni30 103.49(18) . . ? C63 Ni31 Ni30 99.43(16) . . ? C64 Ni31 Ni30 94.86(15) . . ? Ni32 Ni31 Ni30 104.50(4) . . ? Ni24 Ni31 Ni30 59.86(3) . . ? Ni25 Ni31 Ni30 115.66(3) . . ? Ni26 Ni31 Ni30 140.37(4) . . ? C42 Ni32 C42' 11.8(12) . . ? C42 Ni32 C41 100.2(3) . . ? C42' Ni32 C41 111.4(11) . . ? C42 Ni32 C63 150.6(3) . . ? C42' Ni32 C63 139.9(11) . . ? C41 Ni32 C63 108.7(2) . . ? C42 Ni32 Ni31 152.3(3) . . ? C42' Ni32 Ni31 163.1(12) . . ? C41 Ni32 Ni31 52.09(17) . . ? C63 Ni32 Ni31 56.85(17) . . ? C42 Ni32 Ni33 55.0(3) . . ? C42' Ni32 Ni33 43.6(11) . . ? C41 Ni32 Ni33 154.8(2) . . ? C63 Ni32 Ni33 96.4(2) . . ? Ni31 Ni32 Ni33 152.62(11) . . ? C42 Ni32 Ni27 96.5(3) . . ? C42' Ni32 Ni27 88.8(12) . . ? C41 Ni32 Ni27 144.94(19) . . ? C63 Ni32 Ni27 56.03(17) . . ? Ni31 Ni32 Ni27 107.06(4) . . ? Ni33 Ni32 Ni27 53.29(11) . . ? C42 Ni32 Ni28 110.2(3) . . ? C42' Ni32 Ni28 98.8(11) . . ? C41 Ni32 Ni28 134.35(18) . . ? C63 Ni32 Ni28 51.48(17) . . ? Ni31 Ni32 Ni28 93.19(3) . . ? Ni33 Ni32 Ni28 62.19(10) . . ? Ni27 Ni32 Ni28 64.83(3) . . ? C42 Ni32 Ni29 104.3(3) . . ? C42' Ni32 Ni29 101.4(13) . . ? C41 Ni32 Ni29 81.83(19) . . ? C63 Ni32 Ni29 85.74(17) . . ? Ni31 Ni32 Ni29 74.92(3) . . ? Ni33 Ni32 Ni29 99.28(11) . . ? Ni27 Ni32 Ni29 123.36(4) . . ? Ni28 Ni32 Ni29 58.57(3) . . ? O39 C39 Ni28 178.3(7) . . ? O42 C42 Ni32 170.8(8) . . ? O46 C46 Ni27 176.7(8) . . ? C42' Ni33 C47' 89(2) . . ? C42' Ni33 C39' 125.3(17) . . ? C47' Ni33 C39' 104.2(17) . . ? C42' Ni33 C46' 113.7(18) . . ? C47' Ni33 C46' 90.8(18) . . ? C39' Ni33 C46' 118.7(14) . . ? C42' Ni33 Ni27 106.0(14) . . ? C47' Ni33 Ni27 137.2(14) . . ? C39' Ni33 Ni27 98.9(9) . . ? C46' Ni33 Ni27 46.4(11) . . ? C42' Ni33 Ni32 49.9(15) . . ? C47' Ni33 Ni32 139.1(14) . . ? C39' Ni33 Ni32 101.6(10) . . ? C46' Ni33 Ni32 104.0(11) . . ? Ni27 Ni33 Ni32 67.24(12) . . ? C42' Ni33 Ni28 104.9(15) . . ? C47' Ni33 Ni28 145.1(14) . . ? C39' Ni33 Ni28 41.8(10) . . ? C46' Ni33 Ni28 111.3(11) . . ? Ni27 Ni33 Ni28 69.82(11) . . ? Ni32 Ni33 Ni28 63.09(10) . . ? O39' C39' Ni28 157(3) . . ? O39' C39' Ni33 119(3) . . ? Ni28 C39' Ni33 83.9(15) . . ? O42' C42' Ni33 151(3) . . ? O42' C42' Ni32 121(2) . . ? Ni33 C42' Ni32 87(2) . . ? O46' C46' Ni27 163(3) . . ? O46' C46' Ni33 128(3) . . ? Ni27 C46' Ni33 68.5(13) . . ? O47' C47' Ni33 161(4) . . ? C62 C61 Ni18 138.6(5) . . ? C62 C61 Ni24 127.5(4) . . ? Ni18 C61 Ni24 82.0(2) . . ? C62 C61 Ni22 72.1(3) . . ? Ni18 C61 Ni22 97.6(2) . . ? Ni24 C61 Ni22 148.4(3) . . ? C62 C61 Ni23 129.5(4) . . ? Ni18 C61 Ni23 79.4(2) . . ? Ni24 C61 Ni23 78.4(2) . . ? Ni22 C61 Ni23 70.56(18) . . ? C62 C61 Ni30 70.0(3) . . ? Ni18 C61 Ni30 149.5(3) . . ? Ni24 C61 Ni30 84.5(2) . . ? Ni22 C61 Ni30 80.2(2) . . ? Ni23 C61 Ni30 71.18(19) . . ? C62 C61 Ni17 68.8(3) . . ? Ni18 C61 Ni17 69.92(19) . . ? Ni24 C61 Ni17 128.3(3) . . ? Ni22 C61 Ni17 79.6(2) . . ? Ni23 C61 Ni17 133.5(3) . . ? Ni30 C61 Ni17 137.9(3) . . ? C61 C62 Ni29 140.5(5) . . ? C61 C62 Ni21 131.7(4) . . ? Ni29 C62 Ni21 83.3(2) . . ? C61 C62 Ni30 71.5(3) . . ? Ni29 C62 Ni30 72.0(2) . . ? Ni21 C62 Ni30 127.1(3) . . ? C61 C62 Ni22 69.0(3) . . ? Ni29 C62 Ni22 118.0(3) . . ? Ni21 C62 Ni22 71.83(19) . . ? Ni30 C62 Ni22 79.7(2) . . ? C61 C62 Ni17 73.6(3) . . ? Ni29 C62 Ni17 143.9(3) . . ? Ni21 C62 Ni17 73.0(2) . . ? Ni30 C62 Ni17 144.0(3) . . ? Ni22 C62 Ni17 80.2(2) . . ? C61 C62 Ni28 119.5(4) . . ? Ni29 C62 Ni28 78.39(19) . . ? Ni21 C62 Ni28 80.4(2) . . ? Ni30 C62 Ni28 135.2(3) . . ? Ni22 C62 Ni28 144.9(3) . . ? Ni17 C62 Ni28 71.30(18) . . ? C64 C63 Ni32 144.1(5) . . ? C64 C63 Ni26 72.3(3) . . ? Ni32 C63 Ni26 99.5(2) . . ? C64 C63 Ni28 123.9(4) . . ? Ni32 C63 Ni28 81.4(2) . . ? Ni26 C63 Ni28 148.8(3) . . ? C64 C63 Ni20 74.2(3) . . ? Ni32 C63 Ni20 141.2(3) . . ? Ni26 C63 Ni20 85.3(2) . . ? Ni28 C63 Ni20 75.7(2) . . ? C64 C63 Ni31 72.6(4) . . ? Ni32 C63 Ni31 72.2(2) . . ? Ni26 C63 Ni31 87.6(2) . . ? Ni28 C63 Ni31 121.6(3) . . ? Ni20 C63 Ni31 146.6(3) . . ? C64 C63 Ni27 127.8(4) . . ? Ni32 C63 Ni27 76.57(19) . . ? Ni26 C63 Ni27 68.71(17) . . ? Ni28 C63 Ni27 81.4(2) . . ? Ni20 C63 Ni27 69.36(18) . . ? Ni31 C63 Ni27 136.7(3) . . ? C63 C64 Ni25 130.5(4) . . ? C63 C64 Ni19 136.3(5) . . ? Ni25 C64 Ni19 82.2(2) . . ? C63 C64 Ni24 129.8(4) . . ? Ni25 C64 Ni24 78.3(2) . . ? Ni19 C64 Ni24 78.4(2) . . ? C63 C64 Ni26 68.4(3) . . ? Ni25 C64 Ni26 70.88(19) . . ? Ni19 C64 Ni26 107.0(3) . . ? Ni24 C64 Ni26 147.4(3) . . ? C63 C64 Ni31 68.8(3) . . ? Ni25 C64 Ni31 80.8(2) . . ? Ni19 C64 Ni31 154.5(3) . . ? Ni24 C64 Ni31 79.7(2) . . ? Ni26 C64 Ni31 85.0(2) . . ? C63 C64 Ni20 67.4(3) . . ? Ni25 C64 Ni20 132.2(3) . . ? Ni19 C64 Ni20 68.96(19) . . ? Ni24 C64 Ni20 128.3(3) . . ? Ni26 C64 Ni20 81.9(2) . . ? Ni31 C64 Ni20 136.0(3) . . ? O24 C24 Ni17 146.9(5) . . ? O24 C24 Ni21 134.5(5) . . ? Ni17 C24 Ni21 78.6(2) . . ? O25 C25 Ni18 139.2(5) . . ? O25 C25 Ni17 142.9(5) . . ? Ni18 C25 Ni17 77.8(2) . . ? O26 C26 Ni18 176.4(7) . . ? O27 C27 Ni28 137.6(5) . . ? O27 C27 Ni17 125.3(5) . . ? Ni28 C27 Ni17 77.8(2) . . ? O27 C27 Ni20 124.6(5) . . ? Ni28 C27 Ni20 77.6(2) . . ? Ni17 C27 Ni20 98.5(3) . . ? O28 C28 Ni20 142.5(6) . . ? O28 C28 Ni27 139.0(6) . . ? Ni20 C28 Ni27 78.5(2) . . ? O29 C29 Ni20 142.0(6) . . ? O29 C29 Ni19 140.4(6) . . ? Ni20 C29 Ni19 77.7(3) . . ? O30 C30 Ni19 171.6(13) . . ? O30' C30' Ni19 172.4(13) . . ? O31 C31 Ni21 176.3(6) . . ? O32 C32 Ni22 160.4(6) . . ? O32 C32 Ni21 125.1(5) . . ? Ni22 C32 Ni21 74.5(2) . . ? O33 C33 Ni22 147.9(6) . . ? O33 C33 Ni23 133.2(5) . . ? Ni22 C33 Ni23 78.7(2) . . ? O34 C34 Ni23 178.5(7) . . ? O35 C35 Ni24 172.0(6) . . ? O36 C36 Ni25 171.5(13) . . ? O36' C36' Ni25 174.2(12) . . ? O37 C37 Ni26 146.4(5) . . ? O37 C37 Ni25 135.0(5) . . ? Ni26 C37 Ni25 78.5(2) . . ? O38 C38 Ni26 157.3(6) . . ? O38 C38 Ni27 127.7(5) . . ? Ni26 C38 Ni27 75.0(2) . . ? O40 C40 Ni30 159.9(6) . . ? O40 C40 Ni23 125.3(5) . . ? Ni30 C40 Ni23 74.6(2) . . ? O41 C41 Ni32 141.7(5) . . ? O41 C41 Ni31 140.9(5) . . ? Ni32 C41 Ni31 77.4(2) . . ? O43 C43 Ni29 177.7(6) . . ? O44 C44 Ni30 145.7(5) . . ? O44 C44 Ni29 136.9(5) . . ? Ni30 C44 Ni29 77.3(2) . . ? O45 C45 Ni31 173.0(6) . . ? C104 N1 C106 111.5(5) . . ? C104 N1 C102 106.1(4) . . ? C106 N1 C102 110.9(4) . . ? C104 N1 C100 110.6(4) . . ? C106 N1 C100 106.3(4) . . ? C102 N1 C100 111.5(4) . . ? C101 C100 N1 115.4(5) . . ? C101 C100 H10A 108.4 . . ? N1 C100 H10A 108.4 . . ? C101 C100 H10B 108.4 . . ? N1 C100 H10B 108.4 . . ? H10A C100 H10B 107.5 . . ? C100 C101 H10C 109.5 . . ? C100 C101 H10D 109.5 . . ? H10C C101 H10D 109.5 . . ? C100 C101 H10E 109.5 . . ? H10C C101 H10E 109.5 . . ? H10D C101 H10E 109.5 . . ? C103 C102 N1 115.3(5) . . ? C103 C102 H10F 108.4 . . ? N1 C102 H10F 108.4 . . ? C103 C102 H10G 108.4 . . ? N1 C102 H10G 108.4 . . ? H10F C102 H10G 107.5 . . ? C102 C103 H10H 109.5 . . ? C102 C103 H10I 109.5 . . ? H10H C103 H10I 109.5 . . ? C102 C103 H10J 109.5 . . ? H10H C103 H10J 109.5 . . ? H10I C103 H10J 109.5 . . ? N1 C104 C105 115.7(5) . . ? N1 C104 H10K 108.4 . . ? C105 C104 H10K 108.4 . . ? N1 C104 H10L 108.4 . . ? C105 C104 H10L 108.4 . . ? H10K C104 H10L 107.4 . . ? C104 C105 H10M 109.5 . . ? C104 C105 H10N 109.5 . . ? H10M C105 H10N 109.5 . . ? C104 C105 H10O 109.5 . . ? H10M C105 H10O 109.5 . . ? H10N C105 H10O 109.5 . . ? C107 C106 N1 116.1(5) . . ? C107 C106 H10P 108.3 . . ? N1 C106 H10P 108.3 . . ? C107 C106 H10Q 108.3 . . ? N1 C106 H10Q 108.3 . . ? H10P C106 H10Q 107.4 . . ? C106 C107 H10R 109.5 . . ? C106 C107 H10S 109.5 . . ? H10R C107 H10S 109.5 . . ? C106 C107 H10T 109.5 . . ? H10R C107 H10T 109.5 . . ? H10S C107 H10T 109.5 . . ? C206 N2 C202 106.3(5) . . ? C206 N2 C200 110.3(5) . . ? C202 N2 C200 112.0(5) . . ? C206 N2 C204 111.2(5) . . ? C202 N2 C204 111.1(5) . . ? C200 N2 C204 106.0(4) . . ? N2 C200 C201 113.9(5) . . ? N2 C200 H20A 108.8 . . ? C201 C200 H20A 108.8 . . ? N2 C200 H20B 108.8 . . ? C201 C200 H20B 108.8 . . ? H20A C200 H20B 107.7 . . ? C200 C201 H20C 109.5 . . ? C200 C201 H20D 109.5 . . ? H20C C201 H20D 109.5 . . ? C200 C201 H20E 109.5 . . ? H20C C201 H20E 109.5 . . ? H20D C201 H20E 109.5 . . ? N2 C202 C203 115.1(5) . . ? N2 C202 H20F 108.5 . . ? C203 C202 H20F 108.5 . . ? N2 C202 H20G 108.5 . . ? C203 C202 H20G 108.5 . . ? H20F C202 H20G 107.5 . . ? C202 C203 H20H 109.5 . . ? C202 C203 H20I 109.5 . . ? H20H C203 H20I 109.5 . . ? C202 C203 H20J 109.5 . . ? H20H C203 H20J 109.5 . . ? H20I C203 H20J 109.5 . . ? C205 C204 N2 115.4(5) . . ? C205 C204 H20K 108.4 . . ? N2 C204 H20K 108.4 . . ? C205 C204 H20L 108.4 . . ? N2 C204 H20L 108.4 . . ? H20K C204 H20L 107.5 . . ? C204 C205 H20M 109.5 . . ? C204 C205 H20N 109.5 . . ? H20M C205 H20N 109.5 . . ? C204 C205 H20O 109.5 . . ? H20M C205 H20O 109.5 . . ? H20N C205 H20O 109.5 . . ? N2 C206 C207 116.0(5) . . ? N2 C206 H20P 108.3 . . ? C207 C206 H20P 108.3 . . ? N2 C206 H20Q 108.3 . . ? C207 C206 H20Q 108.3 . . ? H20P C206 H20Q 107.4 . . ? C206 C207 H20R 109.5 . . ? C206 C207 H20S 109.5 . . ? H20R C207 H20S 109.5 . . ? C206 C207 H20T 109.5 . . ? H20R C207 H20T 109.5 . . ? H20S C207 H20T 109.5 . . ? C302 N3 C300 111.3(5) . . ? C302 N3 C306 108.9(4) . . ? C300 N3 C306 107.7(5) . . ? C302 N3 C304 108.6(5) . . ? C300 N3 C304 109.0(5) . . ? C306 N3 C304 111.4(5) . . ? N3 C300 C301 115.5(5) . . ? N3 C300 H30A 108.4 . . ? C301 C300 H30A 108.4 . . ? N3 C300 H30B 108.4 . . ? C301 C300 H30B 108.4 . . ? H30A C300 H30B 107.5 . . ? C300 C301 H30C 109.5 . . ? C300 C301 H30D 109.5 . . ? H30C C301 H30D 109.5 . . ? C300 C301 H30E 109.5 . . ? H30C C301 H30E 109.5 . . ? H30D C301 H30E 109.5 . . ? N3 C302 C303 115.2(5) . . ? N3 C302 H30F 108.5 . . ? C303 C302 H30F 108.5 . . ? N3 C302 H30G 108.5 . . ? C303 C302 H30G 108.5 . . ? H30F C302 H30G 107.5 . . ? C302 C303 H30H 109.5 . . ? C302 C303 H30I 109.5 . . ? H30H C303 H30I 109.5 . . ? C302 C303 H30J 109.5 . . ? H30H C303 H30J 109.5 . . ? H30I C303 H30J 109.5 . . ? N3 C304 C305 115.3(5) . . ? N3 C304 H30K 108.4 . . ? C305 C304 H30K 108.4 . . ? N3 C304 H30L 108.4 . . ? C305 C304 H30L 108.4 . . ? H30K C304 H30L 107.5 . . ? C304 C305 H30M 109.5 . . ? C304 C305 H30N 109.5 . . ? H30M C305 H30N 109.5 . . ? C304 C305 H30O 109.5 . . ? H30M C305 H30O 109.5 . . ? H30N C305 H30O 109.5 . . ? N3 C306 C307 116.2(6) . . ? N3 C306 H30P 108.2 . . ? C307 C306 H30P 108.2 . . ? N3 C306 H30Q 108.2 . . ? C307 C306 H30Q 108.2 . . ? H30P C306 H30Q 107.4 . . ? C306 C307 H30R 109.5 . . ? C306 C307 H30S 109.5 . . ? H30R C307 H30S 109.5 . . ? C306 C307 H30T 109.5 . . ? H30R C307 H30T 109.5 . . ? H30S C307 H30T 109.5 . . ? C400 N4 C402 112.5(5) . . ? C400 N4 C406 107.0(5) . . ? C402 N4 C406 110.2(5) . . ? C400 N4 C404 111.2(5) . . ? C402 N4 C404 106.7(5) . . ? C406 N4 C404 109.3(5) . . ? N4 C400 C401 113.8(5) . . ? N4 C400 H40A 108.8 . . ? C401 C400 H40A 108.8 . . ? N4 C400 H40B 108.8 . . ? C401 C400 H40B 108.8 . . ? H40A C400 H40B 107.7 . . ? C400 C401 H40C 109.5 . . ? C400 C401 H40D 109.5 . . ? H40C C401 H40D 109.5 . . ? C400 C401 H40E 109.5 . . ? H40C C401 H40E 109.5 . . ? H40D C401 H40E 109.5 . . ? N4 C402 C403 113.7(5) . . ? N4 C402 H40F 108.8 . . ? C403 C402 H40F 108.8 . . ? N4 C402 H40G 108.8 . . ? C403 C402 H40G 108.8 . . ? H40F C402 H40G 107.7 . . ? C402 C403 H40H 109.5 . . ? C402 C403 H40I 109.5 . . ? H40H C403 H40I 109.5 . . ? C402 C403 H40J 109.5 . . ? H40H C403 H40J 109.5 . . ? H40I C403 H40J 109.5 . . ? C405 C404 N4 114.2(5) . . ? C405 C404 H40K 108.7 . . ? N4 C404 H40K 108.7 . . ? C405 C404 H40L 108.7 . . ? N4 C404 H40L 108.7 . . ? H40K C404 H40L 107.6 . . ? C404 C405 H40M 109.5 . . ? C404 C405 H40N 109.5 . . ? H40M C405 H40N 109.5 . . ? C404 C405 H40O 109.5 . . ? H40M C405 H40O 109.5 . . ? H40N C405 H40O 109.5 . . ? N4 C406 C407 114.4(6) . . ? N4 C406 H40P 108.7 . . ? C407 C406 H40P 108.7 . . ? N4 C406 H40Q 108.7 . . ? C407 C406 H40Q 108.7 . . ? H40P C406 H40Q 107.6 . . ? C406 C407 H40R 109.5 . . ? C406 C407 H40S 109.5 . . ? H40R C407 H40S 109.5 . . ? C406 C407 H40T 109.5 . . ? H40R C407 H40T 109.5 . . ? H40S C407 H40T 109.5 . . ? C500 N5 C506 108.7(5) . . ? C500 N5 C504 110.8(5) . . ? C506 N5 C504 109.0(4) . . ? C500 N5 C502 109.3(5) . . ? C506 N5 C502 111.5(5) . . ? C504 N5 C502 107.5(4) . . ? N5 C500 C501 115.4(5) . . ? N5 C500 H50A 108.4 . . ? C501 C500 H50A 108.4 . . ? N5 C500 H50B 108.4 . . ? C501 C500 H50B 108.4 . . ? H50A C500 H50B 107.5 . . ? C500 C501 H50C 109.5 . . ? C500 C501 H50D 109.5 . . ? H50C C501 H50D 109.5 . . ? C500 C501 H50E 109.5 . . ? H50C C501 H50E 109.5 . . ? H50D C501 H50E 109.5 . . ? N5 C502 C503 114.9(5) . . ? N5 C502 H50F 108.5 . . ? C503 C502 H50F 108.5 . . ? N5 C502 H50G 108.5 . . ? C503 C502 H50G 108.5 . . ? H50F C502 H50G 107.5 . . ? C502 C503 H50H 109.5 . . ? C502 C503 H50I 109.5 . . ? H50H C503 H50I 109.5 . . ? C502 C503 H50J 109.5 . . ? H50H C503 H50J 109.5 . . ? H50I C503 H50J 109.5 . . ? N5 C504 C505 115.7(5) . . ? N5 C504 H50K 108.4 . . ? C505 C504 H50K 108.4 . . ? N5 C504 H50L 108.4 . . ? C505 C504 H50L 108.4 . . ? H50K C504 H50L 107.4 . . ? C504 C505 H50M 109.5 . . ? C504 C505 H50N 109.5 . . ? H50M C505 H50N 109.5 . . ? C504 C505 H50O 109.5 . . ? H50M C505 H50O 109.5 . . ? H50N C505 H50O 109.5 . . ? C507 C506 N5 116.2(5) . . ? C507 C506 H50P 108.2 . . ? N5 C506 H50P 108.2 . . ? C507 C506 H50Q 108.2 . . ? N5 C506 H50Q 108.2 . . ? H50P C506 H50Q 107.4 . . ? C506 C507 H50R 109.5 . . ? C506 C507 H50S 109.5 . . ? H50R C507 H50S 109.5 . . ? C506 C507 H50T 109.5 . . ? H50R C507 H50T 109.5 . . ? H50S C507 H50T 109.5 . . ? C604 N6 C602 107.4(5) . . ? C604 N6 C600 111.3(5) . . ? C602 N6 C600 111.1(5) . . ? C604 N6 C606 110.8(5) . . ? C602 N6 C606 109.7(5) . . ? C600 N6 C606 106.6(4) . . ? C601 C600 N6 115.5(6) . . ? C601 C600 H60A 108.4 . . ? N6 C600 H60A 108.4 . . ? C601 C600 H60B 108.4 . . ? N6 C600 H60B 108.4 . . ? H60A C600 H60B 107.5 . . ? C600 C601 H60C 109.5 . . ? C600 C601 H60D 109.5 . . ? H60C C601 H60D 109.5 . . ? C600 C601 H60E 109.5 . . ? H60C C601 H60E 109.5 . . ? H60D C601 H60E 109.5 . . ? N6 C602 C603 115.8(6) . . ? N6 C602 H60F 108.3 . . ? C603 C602 H60F 108.3 . . ? N6 C602 H60G 108.3 . . ? C603 C602 H60G 108.3 . . ? H60F C602 H60G 107.4 . . ? C602 C603 H60H 109.5 . . ? C602 C603 H60I 109.5 . . ? H60H C603 H60I 109.5 . . ? C602 C603 H60J 109.5 . . ? H60H C603 H60J 109.5 . . ? H60I C603 H60J 109.5 . . ? N6 C604 C605 115.2(5) . . ? N6 C604 H60K 108.5 . . ? C605 C604 H60K 108.5 . . ? N6 C604 H60L 108.5 . . ? C605 C604 H60L 108.5 . . ? H60K C604 H60L 107.5 . . ? C604 C605 H60M 109.5 . . ? C604 C605 H60N 109.5 . . ? H60M C605 H60N 109.5 . . ? C604 C605 H60O 109.5 . . ? H60M C605 H60O 109.5 . . ? H60N C605 H60O 109.5 . . ? C607 C606 N6 115.9(5) . . ? C607 C606 H60P 108.3 . . ? N6 C606 H60P 108.3 . . ? C607 C606 H60Q 108.3 . . ? N6 C606 H60Q 108.3 . . ? H60P C606 H60Q 107.4 . . ? C606 C607 H60R 109.5 . . ? C606 C607 H60S 109.5 . . ? H60R C607 H60S 109.5 . . ? C606 C607 H60T 109.5 . . ? H60R C607 H60T 109.5 . . ? H60S C607 H60T 109.5 . . ? C706 N7 C704 110.8(10) . . ? C706 N7 C700 118.6(10) . . ? C704 N7 C700 110.5(11) . . ? C706 N7 C702 107.4(10) . . ? C704 N7 C702 104.8(9) . . ? C700 N7 C702 103.7(11) . . ? C701 C700 N7 113.3(11) . . ? C701 C700 H70A 108.9 . . ? N7 C700 H70A 108.9 . . ? C701 C700 H70B 108.9 . . ? N7 C700 H70B 108.9 . . ? H70A C700 H70B 107.7 . . ? C700 C701 H70C 109.5 . . ? C700 C701 H70D 109.5 . . ? H70C C701 H70D 109.5 . . ? C700 C701 H70E 109.5 . . ? H70C C701 H70E 109.5 . . ? H70D C701 H70E 109.5 . . ? C703 C702 N7 114.5(11) . . ? C703 C702 H70F 108.6 . . ? N7 C702 H70F 108.6 . . ? C703 C702 H70G 108.6 . . ? N7 C702 H70G 108.6 . . ? H70F C702 H70G 107.6 . . ? C702 C703 H70H 109.5 . . ? C702 C703 H70I 109.5 . . ? H70H C703 H70I 109.5 . . ? C702 C703 H70J 109.5 . . ? H70H C703 H70J 109.5 . . ? H70I C703 H70J 109.5 . . ? N7 C704 C705 109.7(11) . . ? N7 C704 H70K 109.7 . . ? C705 C704 H70K 109.7 . . ? N7 C704 H70L 109.7 . . ? C705 C704 H70L 109.7 . . ? H70K C704 H70L 108.2 . . ? C704 C705 H70M 109.5 . . ? C704 C705 H70N 109.5 . . ? H70M C705 H70N 109.5 . . ? C704 C705 H70O 109.5 . . ? H70M C705 H70O 109.5 . . ? H70N C705 H70O 109.5 . . ? N7 C706 C707 117.3(9) . . ? N7 C706 H70P 108.0 . . ? C707 C706 H70P 108.0 . . ? N7 C706 H70Q 108.0 . . ? C707 C706 H70Q 108.0 . . ? H70P C706 H70Q 107.2 . . ? C706 C707 H70R 109.5 . . ? C706 C707 H70S 109.5 . . ? H70R C707 H70S 109.5 . . ? C706 C707 H70T 109.5 . . ? H70R C707 H70T 109.5 . . ? H70S C707 H70T 109.5 . . ? C716 N7' C712 106.9(9) . . ? C716 N7' C710 102.5(12) . . ? C712 N7' C710 107.6(12) . . ? C716 N7' C714 110.2(10) . . ? C712 N7' C714 111.0(10) . . ? C710 N7' C714 117.9(10) . . ? C711 C710 N7' 100.1(11) . . ? C711 C710 H71A 111.8 . . ? N7' C710 H71A 111.8 . . ? C711 C710 H71B 111.8 . . ? N7' C710 H71B 111.8 . . ? H71A C710 H71B 109.5 . . ? C710 C711 H71C 109.5 . . ? C710 C711 H71D 109.5 . . ? H71C C711 H71D 109.5 . . ? C710 C711 H71E 109.5 . . ? H71C C711 H71E 109.5 . . ? H71D C711 H71E 109.5 . . ? N7' C712 C713 112.5(10) . . ? N7' C712 H71F 109.1 . . ? C713 C712 H71F 109.1 . . ? N7' C712 H71G 109.1 . . ? C713 C712 H71G 109.1 . . ? H71F C712 H71G 107.8 . . ? C712 C713 H71H 109.5 . . ? C712 C713 H71I 109.5 . . ? H71H C713 H71I 109.5 . . ? C712 C713 H71J 109.5 . . ? H71H C713 H71J 109.5 . . ? H71I C713 H71J 109.5 . . ? N7' C714 C715 113.9(11) . . ? N7' C714 H71K 108.8 . . ? C715 C714 H71K 108.8 . . ? N7' C714 H71L 108.8 . . ? C715 C714 H71L 108.8 . . ? H71K C714 H71L 107.7 . . ? C714 C715 H71M 109.5 . . ? C714 C715 H71N 109.5 . . ? H71M C715 H71N 109.5 . . ? C714 C715 H71O 109.5 . . ? H71M C715 H71O 109.5 . . ? H71N C715 H71O 109.5 . . ? N7' C716 C717 115.7(13) . . ? N7' C716 H71P 108.4 . . ? C717 C716 H71P 108.4 . . ? N7' C716 H71Q 108.4 . . ? C717 C716 H71Q 108.4 . . ? H71P C716 H71Q 107.4 . . ? C716 C717 H71R 109.5 . . ? C716 C717 H71S 109.5 . . ? H71R C717 H71S 109.5 . . ? C716 C717 H71T 109.5 . . ? H71R C717 H71T 109.5 . . ? H71S C717 H71T 109.5 . . ? C802 N8 C804 111.2(5) . . ? C802 N8 C806 106.3(5) . . ? C804 N8 C806 109.9(6) . . ? C802 N8 C800 110.9(6) . . ? C804 N8 C800 107.7(6) . . ? C806 N8 C800 110.8(5) . . ? N8 C800 C801 113.7(6) . . ? N8 C800 H80A 108.8 . . ? C801 C800 H80A 108.8 . . ? N8 C800 H80B 108.8 . . ? C801 C800 H80B 108.8 . . ? H80A C800 H80B 107.7 . . ? C800 C801 H80C 109.5 . . ? C800 C801 H80D 109.5 . . ? H80C C801 H80D 109.5 . . ? C800 C801 H80E 109.5 . . ? H80C C801 H80E 109.5 . . ? H80D C801 H80E 109.5 . . ? N8 C802 C803 115.1(5) . . ? N8 C802 H80F 108.5 . . ? C803 C802 H80F 108.5 . . ? N8 C802 H80G 108.5 . . ? C803 C802 H80G 108.5 . . ? H80F C802 H80G 107.5 . . ? C802 C803 H80H 109.5 . . ? C802 C803 H80I 109.5 . . ? H80H C803 H80I 109.5 . . ? C802 C803 H80J 109.5 . . ? H80H C803 H80J 109.5 . . ? H80I C803 H80J 109.5 . . ? N8 C804 C805 114.3(7) . . ? N8 C804 H80K 108.7 . . ? C805 C804 H80K 108.7 . . ? N8 C804 H80L 108.7 . . ? C805 C804 H80L 108.7 . . ? H80K C804 H80L 107.6 . . ? C804 C805 H80M 109.5 . . ? C804 C805 H80N 109.5 . . ? H80M C805 H80N 109.5 . . ? C804 C805 H80O 109.5 . . ? H80M C805 H80O 109.5 . . ? H80N C805 H80O 109.5 . . ? N8 C806 C807 114.4(6) . . ? N8 C806 H80P 108.6 . . ? C807 C806 H80P 108.6 . . ? N8 C806 H80Q 108.6 . . ? C807 C806 H80Q 108.6 . . ? H80P C806 H80Q 107.6 . . ? C806 C807 H80R 109.5 . . ? C806 C807 H80S 109.5 . . ? H80R C807 H80S 109.5 . . ? C806 C807 H80T 109.5 . . ? H80R C807 H80T 109.5 . . ? H80S C807 H80T 109.5 . . ? _diffrn_measured_fraction_theta_max 0.995 _diffrn_reflns_theta_full 25.00 _diffrn_measured_fraction_theta_full 0.995 _refine_diff_density_max 1.766 _refine_diff_density_min -1.102 _refine_diff_density_rms 0.161